WA-28815_48034_CA_CLO_20210831

UST CLOSURE REPORT

Site:

SHEETZ STORE 391
2100 COUNTY HOME ROAD
GREENVILLE, PITT COUNTY, NORTH CAROLINA

Submitted To:

MR. MATHEW CUTSHALL
SHEETZ, INC.
351 SHEETZ WAY
CLAYSBURG, PENNSYLVANIA 16625

Prepared By:

ENVIROTRAC LTD.
7343 WEST FRIENDLY AVENUE, SUITE J
GREENSBORO, NORTH CAROLINA 27410
[phone]

AUGUST 2021

11.SZ0391.00 i August 31, 2021
© 2021 EnviroTrac

Report Prepared for:

Mr. Mathew Cutshall
Sheetz, Inc.
135 Sheetz Way
Claysburg, Pennsylvania 16625

UST CLOSURE REPORT
SHEETZ STORE 391
2100 COUNTY HOME ROAD
GREENVILLE, NORTH CAROLINA

Prepared by:

Annamarie Blauser, P.G.
Senior Scientist

Reviewed by:

Craig D. Neil, P.G.
Senior Project Manager

EnviroTrac Ltd.
7343 W. Friendly Avenue, Suite J
Greensboro, North Carolina 27410

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© 2021 EnviroTrac

TABLE OF CONTENTS
____________________________________________________________________________
1 SITE INFORMATION ...................................................................................................... 1
2 UST CLOSURE ............................................................................................................... 1
3 UST REMOVAL SOIL SAMPLE RESULTS .................................................................... 3
4 GROUNDWATER SAMPLNG AND RESULTS ............................................................... 4
5 CONCLUSION AND RECOMMENDATIONS .................................................................. 5
6 LIMITATIONS ................................................................................................................. 5

TABLES

1 Site History and UST Information
2A UST Soil Sample Analytical Summary
2B Product Line Soil Sample Analytical Summary
3 Groundwater Sample Analytical Summary

FIGURES

1 Site Vicinity Map
2 Site Location Map
3 Receptor Map
4 Sample Location Map
5 Sample Location Results

APPENDICES

A Liquid and Tank Disposal Manifests
B UST Permanent Closure or Change-in-Service Forms (UST-2A)
C Site Photographs
D UST Laboratory Report and Chain-of-Custody
E Product Line Laboratory Report and Chain-of-Custody
F Groundwater Laboratory Report and Chain-of-Custody

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© 2021 EnviroTrac
UST CLOSURE REPORT
SHEETZ STORE 391
2100 COUNTY HOME ROAD
GREENVILLE, NORTH CAROLINA

1 SITE INFORMATION
____________________________________________________________________________

The site is located at 2100 County Home Road in Greenville, North Carolina (Figures 1 and 2).
The site consists of one tax parcel (Parcel Identification Number 4686847654), currently owned
by L P PTM. The underground storage tanks (USTs) were reportedly installed on June 1, 2006.

The site is located in a commercial area consisting of shopping centers, retail stores, restaurants,
and fuel stations. Residential properties are south less than 1,000 feet from the site. Neighboring
land use areas are shown on Figure 3.

Three 15,000-gallon USTs formerly contained gasoline, one 12,000-gallon UST formerly
contained diesel, and one 8,000-gallon UST formerly contained kerosene. The five USTs were
registered with the North Carolina Department of Environment Quality (NCDEQ).

The tanks were removed during a major remodel of the Sheetz Store 391.

2 UST CLOSURE
____________________________________________________________________________

Northstar Petroleum Solution LLC (Northstar) of Virginia Beach, Virginia performed the UST
closures on June 16, 2021. Prior to removing the USTs, 154 gallons of oily water and 3,500
gallons of pressure cleaning water were removed from the tanks. During the UST closures, no
petroleum odors or stained soil was observed in the soil. The base of the excavation was filled
with shallow groundwater. A copy of the liquid disposal manifest is included in Appendix A.

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The three 15,000-gallon gasoline USTs were constructed of coated steel double walled and were
approximately 10 feet in diameter and 26 feet long. The 12,000-gallon diesel UST was
constructed of coated steel double walled and was approximately 10 feet in diameter and 22 feet
long. The 8,000-gallon kerosene UST was constructed of coated steel double walled and was
approximately 8 feet in diameter and 22 feet long. The UST information is summarized in Table
1. The exterior surface of the USTs appeared to be in good condition and no holes or corrosion
were observed. The USTs were loaded onto trucks and transported by Northstar to Mills Metals
Recycling Inc., in Vanceboro, North Carolina for disposal. A copy of the tank disposal manifest
is included in Appendix A. A copy of the UST-2A – UST Permanent Closure or Change-in-
Service is included in Appendix B. Site photographs of the tank removal process are included
in Appendix C.

Following removal of the USTs, 20 soil samples (SS-15 through SS-34) were collected from the
sidewalls of the 30’ x 72’ excavation area. Due to shallow ground water in the excavation,
samples were collected from a depth of 2-3’ below ground surface (bgs). Soil samples around
the tank excavation were collected every 10 feet. Soils consisted of sandy silt. In addition to the
20 soil samples around tank field, 14 soil samples were collected along the gasoline and diesel
products lines and beneath the dispensers (SS-1 through SS-14), and 7 soil samples (K1 through
K7) were collected along the kerosene product line.

The soil samples associated with the gasoline USTs and product lines were analyzed for volatile
organic compounds by EPA Method 8260 and for total petroleum hydrocarbons (TPH) by EPA
Method 8015B including gasoline range organics (GRO). Soil samples associated with the diesel
UST and kerosene UST were analyzed for TPH by EPA Method 8015B including diesel range
organics (DRO) and GRO.

The samples were placed in laboratory-supplied bottles, maintained on ice, and transported under
chain-of-custody to Pace Analytical Laboratories. The sample locations are shown on Figure 4.

The product lines from the five USTs and between the dispenser islands were uncovered except
for the kerosene line. Fourteen soil samples were collected along the product lines and under the
island dispensers approximately ten feet apart (Samples 1 through 14). The soil samples along
the product lines were collected on June 15, 2021 with a shovel. The soil samples were collected
approximately two feet beneath the product lines and dispensers. On August 6, 2021, using a

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© 2021 EnviroTrac
track mounted Geoprobe® operated by GeoExploration, seven soil samples (K1 through K7) were
collected along the former kerosene product line. Samples were collected approximately 2 to 3
feet below the ground surface. Each sample was screened with a Photoionization Detector (PID).
The sample locations are shown on Figure 4.

Soil samples 12, 13, 15 and 16 were analyzed for volatile organic compounds (VOCs) by EPA
Methods 8260 and for TPH by EPA Method 8015B including GRO and DRO. Soil samples 1
through 11, and 17 through 29 were analyzed for VOCs by EPA Methods 8260 and for TPH by
EPA Method 8015B including GRO. Soil samples 14 and 30 through 34 were analyzed for TPH
by EPA Method 8015B including GRO and DRO. Soil samples K1 through K7 were analyzed for
TPH by EPA Method 8015B including GRO, DRO and Oil Range Organics (ORO).

3 UST REMOVAL SOIL SAMPLE RESULTS
____________________________________________________________________________

The laboratory analysis of the soil samples collected around the USTs on June 16, 2021 did not
detect any compounds at concentrations exceeding the Soil-to-Groundwater MSCCs The
laboratory results are summarized in Table 2A and shown on Figure 5. The laboratory report
and associated chain-of-custody document are included in Appendix D.

The laboratory analysis of the soil samples collected under the product lines and dispenser
islands on June 15, 2021, were below the Soil-to-Groundwater MSCCs, State Action Limit and/or
laboratory detection limit. The laboratory results are summarized in Table 2B and shown on
Figure 5. The laboratory report and associated chain-of-custody document are included in
Appendix E.

The laboratory analysis of the soil samples collected under the former kerosene product line on
August 6, 2021, were below the Soil-to-Groundwater MSCCs, State Action Limit and/or laboratory
detection limit. The laboratory results are summarized in Table 2B and shown on Figure 5. The
laboratory report and associated chain-of-custody document are included in Appendix E.

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4 GROUNDWATER SAMPLNG AND RESULTS
____________________________________________________________________________

Prior to the UST closure, EnviroTrac collected groundwater samples from the three monitoring
wells (MW-1, MW-2 and MW-3) around the tank field. Groundwater depth ranged from 3.00 to
3.80 feet below ground surface. Prior to collecting groundwater samples, a minimum of three well
volumes of water were removed using a new disposable bailer. After allowing the groundwater to
recharge within the monitoring wells, groundwater samples were collected with the bailer. The
samples were placed in laboratory-supplied bottles, maintained on ice, and transported under
chain-of-custody to Pace Analytical Laboratories (Pace) to be analyzed for MADEP VPH, MADEP
EPH, and 8260 VOC.

Analytical results of the three monitoring wells (MW-1, MW-2, and MW-3) did not detect
compounds above the North Carolina Groundwater Quality 2L Standard (2L Standard) and/or the
Gross Contamination Levels (GCLs) for Groundwater. The laboratory results are summarized in
Table 3. The laboratory report and associated chain-of-custody document are included in
Appendix F.

On August 6, 2021, GeoExploration installed a 1 inch temporary monitoring well. The temporary
well was installed to a depth of 15 feet with a 10 foot slotted screen. Groundwater was collected
using a check valve and polyethylene tubing. Groundwater sample (GW-1) was placed in
laboratory-supplied bottles, maintained on ice, and transported under chain-of-custody to Pace
Analytical Laboratories (Pace) to be analyzed for MADEP VPH, MADEP EPH, 6200B VOC, and
625 semi volatile organic compounds (SVOCs).

Analytical results of the temporary well (GW-1) did not detect compounds above the 2L Standard,
GCLs and/or the laboratory detection limit. The laboratory results are summarized in Table 3.
The laboratory report and associated chain-of-custody document are included in Appendix F.

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5 CONCLUSION AND RECOMMENDATIONS
____________________________________________________________________________

Based on the field observations and results of the laboratory analysis, EnviroTrac presents the
following conclusions and recommendations:

• Three 15,000-gallon gasoline USTs were closed by removal on June 16, 2021.
The double walled USTs were constructed of coated steel.
• One 12,000-gallon diesel UST was closed by removal on June 16, 2021. The
double walled UST was constructed of coated steel.
• One 8,000-gallon kerosene UST was closed by removal on June 16, 2021. The
double walled UST was constructed of coated steel.
• Laboratory analysis of soil collected around the UST excavation did not detect any
compounds at concentrations exceeding the Soil-to-Groundwater MSCCs or the
State Action Limit.
• Laboratory analysis of the soil collected beneath the product lines and dispensers
did not detect an compounds at concentrations exceeding the Soil-to-Groundwater
MSCCs or State Action Limit.
• Laboratory analysis for the groundwater samples did not detect any compounds at
concentrations exceeding the 2L Standard.
Based on the results of our fieldwork and the results of laboratory analysis of samples collected,
EnviroTrac recommends that no further action is warranted for the incident.

6 LIMITATIONS
____________________________________________________________________________

EnviroTrac offers various levels of investigative and engineering services to suit the varying needs
of different clients. It should be recognized that definition and evaluation of geologic and
environmental conditions are a difficult and inexact science. Judgments leading to conclusions
and recommendations are generally made with incomplete knowledge of the subsurface

11.SZ0391.00 Page 6 of 6 August 31, 2021
© 2021 EnviroTrac
conditions present due to the limitations of data from field studies. Although risk can never be
eliminated, more-detailed and extensive studies yield more information, which may help
understand and manage the level of risk. Since detailed study and analysis involves greater
expense, our clients participate in determining levels of service that provide adequate information
for their purposes at acceptable levels of risk.

The information included on graphic representations in the UST Closure Report has been
compiled from a variety of sources and is subject to change without notice. EnviroTrac makes no
representations or warranties, express or implied, as to accuracy, completeness, timeliness, or
rights to the use of such information. These documents are not intended for use as a land survey
product, nor are they designed or intended as a construction design document. The use of the
information contained on these graphic representations is at the sole risk of the party using the
information.

TABLES

TABLE 1: SITE HISTORY AND UST INFORMATIONUST IDNumberLast ContentsUseCapacity (in Gallons)Construction DetailsTank DeminsionsLast Date UsedInstallation DateStatus ReleaseUST-1Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 6/1/2006Closed by Removal 6/16/2021NoUST-2Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 6/1/2006Closed by Removal 6/16/2021NoUST-3Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 6/1/2006Closed by Removal 6/16/2021NoUST-4Diesel, Diesel MixFuel Station 12,000Coated Steel Double WalledCylindrical10' x 22' Unknown 6/1/2006Closed by Removal 6/16/2021NoUST-5 Kerosene Fuel Station 8,000Coated Steel Double WalledCylindrical8' x 22' Unknown 6/1/2006Closed by Removal 6/16/2021NoNote:Locations of the USTs are shown on Figure 2.11.SZ0391.00Copyright 2021 EnviroTracAugust 2021
TABLE 2A: UST SOIL SAMPLE ANALYTICAL SUMMARY ParameterANALYTICAL RESULTSSample IDKerosene UST 5SS-15Kerosene UST 5SS-16Diesel UST 4 SS-17GAS UST 3 SS-18GAS UST 3 SS-19GAS UST 2 SS-20GAS UST 2 SS-21GAS UST 1 SS-22GAS UST 1 SS-23GAS UST 1 SS-24Collection Depth (feet bgs)3333333333Collection Date06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)DROBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 100 - - -GROBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 50 - - -Volatile Organic Compounds by EPA Method 8260 (mg/kg)Acetone0.000128 BDL BDL BDL BDL BDL BDL BDL BDL BDL - 24.000 14,000 210,000Methylene Chloride0.000178 0.000145 0.000175 0.000154 0.000131 BDL BDL BDL BDL BDL 0.023 94 1,400TolueneBDL BDL BDL BDL BDL 0.0000083 BDL BDL BDL BDL - 5.4 1,250 18,600Total XyleneBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - 6.0 3,120 46,700ParameterANALYTICAL RESULTSSample IDGAS UST 1 SS-25GAS UST 1 SS-26GAS UST 2 SS-27GAS UST 3 SS-28Diesel UST 4 SS-29Kerosene UST 5 SS-30KeroseneUST 5 SS-31Kerosene UST 5SS-32Kerosene UST 5SS-33Kerosene UST 5SS-34Collection Depth (feet bgs)3333333333Collection Date06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21 06/16/21Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)DROBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 100 - - -GROBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 50 - - -Volatile Organic Compounds by EPA Method 8260 (mg/kg)AcetoneBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - 24.000 14,000 210,000Methylene ChlorideBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.023 94 1,400TolueneBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - 5.400 1,250 18,600Total XyleneBDL 0.0000055 BDL BDL BDL BDL BDL BDL BDL BDL - 6.000 3,120 46,700Notes:Results presented in mg/kgMSCC = Maximum Soil Contaminant Concentration feet bgs = feet below ground surfaceBold denotes concentration is greater than the comparison criteriaBDL = Not detected at or above adjusted reporting limitNA = Not analyzed by this methodCOMPARISON CRITERIASoil-to-Groundwater MSCCResidential MSCCIndustrialMSCCState Action Level COMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCC11.SZ0391.00Copyright 2021 EnviroTracAugust 2021
TABLE 2B: PRODUCT LINE SOIL SAMPLE ANALYTICAL SUMMARYParameter ANALYTICAL RESULTSSample IDSS-1 SS-2 SS-3 SS-4 SS-5 SS-6 SS-7Collection Depth (feet bgs)2.5 2.5 2.5 2.5 2.5 2.5 2.5Collection Date06/15/21 06/15/21 06/15/21 06/15/21 06/15/21 06/15/21 06/15/21Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)DROBDL BDL BDL BDL BDL BDL BDL 100 - - -GROBDL BDL BDL BDL BDL BDL BDL 50 - - -Volatile Organic Compounds by EPA Method 8260 (mg/kg)TolueneBDL BDL BDL 0.0000106 0.0000073 0.0000131 BDL - 5.4 1,250 18,6001,3,5-TrimethylbenzeneBDL BDL BDL 0.0000072 BDL BDL BDL - 6.6 156 2,330Total XyleneBDL BDL BDL 0.0000283 BDL 0.0000228 BDL - 6.0 3,120 46,700Parameter ANALYTICAL RESULTSSample IDSS-8 SS-9 SS-10 SS-11 SS-12 SS-13Collection Depth (feet bgs)2.5 2.5 2.5 2.5 2.5 2.5 2.5Collection Date06/15/21 06/15/21 06/15/21 06/15/21 06/15/21 06/15/21 06/16/21Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)DROBDL BDL BDL BDL BDL 8.4 12 100 - - -GRO BDL BDL BDL BDL BDL BDL BDL 50 - - -Volatile Organic Compounds by EPA Method 8260 (mg/kg)TolueneBDL BDL BDL BDL BDL BDL BDL - 5.4 1,250 18,6001,3,5-TrimethylbenzeneBDL BDL BDL BDL BDL BDL BDL - 6.6 156 2,330Total Xylene BDL BDL BDL BDL BDL BDL BDL - 6.0 3,120 46,700Parameter ANALYTICAL RESULTSSample IDK-1 K-2 K-3 K-4 K-5 K-6 K-7Collection Depth (feet bgs)2.0 3.0 2.5 3.0 3.0 3.0 2.5Collection Date08/06/21 08/06/21 08/06/21 08/06/21 08/06/21 08/06/21 08/06/21Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)DROBDLBDLBDL15.1BDLBDLBDL100 - - -GRO BDL BDL BDL BDL BDL BDL BDL 50 - - -Volatile Organic Compounds by EPA Method 8260 (mg/kg)TolueneBDL BDL BDL BDL BDL BDL BDL - 5.4 1,250 18,6001,3,5-TrimethylbenzeneBDL BDL BDL BDL BDL BDL BDL - 6.6 156 2,330Total Xylene BDL BDL BDL BDL BDL BDL BDL - 6.0 3,120 46,700Notes:Results presented in mg/kg.MSCC = Maximum Soil Contaminant Concentration feet bgs = feet below ground surfaceBDL = Not detected at or above adjusted reporting limitCOMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCCCOMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCCKerosene SS-14COMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCC11.SZ0391.00Copyright 2021 EnviroTrac1 of 1August 2021
TABLE 3: GROUNDWATER SAMPLE ANALYTICAL SUMMARYParameter ANALYTICAL RESULTSSample IDMW-1 MW-2 MW-3 GW-1Collection Date02/09/21 02/09/21 02/09/21 08/06/21Aliphatic (C09-C18) BDL BDL BDL BDL 700-Aliphatic (C19-C36) BDL BDL BDL BDL 10,000-Aliphatic (C11-C22)BDLBDL BDL BDL 200 -Aliphatic (C05-C08) BDL BDL BDL BDL 400-Aliphatic (C09-C12) BDL BDL BDL BDL 700-Total VPH121BDL BDL BDL--EthylbenzeneBDL 1.3BDL BDL600 80,000TolueneBDL 5.5BDL BDL600 260,000Xylene (Total)BDl25.9 BDL BDL500 50,000Notes:Results presented in microgram per liter (µg/L)2L Standard = North Carolina Groundwater Quality StandardsGCL = Gross Contamination Levels for Groundwater Bold denotes concentration is greater than the comparison criteriaBDL = Not detected at or above adjusted reporting limitNA = Not analyzed by this methodfeet bgs = feet below ground surfaceEPA 8260DMADEP VPH2L Standard GCLsCOMPARISONCRITERIAMADEP EPH11.SZ0391.00Copyright 2021 EnviroTracAugust 2021

FIGURES

APPENDIX A
LIQUID and TANK DISPOSAL MANIFESTS

APPENDIX B
UST PERMANENT CLOUSRE OR
CHANGE-IN-SERVICE FORMS (UST-2A)
____________________________________________________________________________

UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY: Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City County Street Address
State

Zip Code

City

County

Zip Code

Phone Number
Phone Number

III. CONTACT PERSONNEL
Contact for Facility:

Job Title:

Phone #:

Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #

Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #

IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/ concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016

Sheetz Inc
5700 6th Ave
Altoona Blair
PA 16602
814-239-1402
Sheetz #391
00-0-0000036857
2100 County Home Road
Greenville 27858Pitt
252-353-9021
John Sieger Env Comp Mgr 814-239-9714
Scott Perkins Northstar Petroleum Solutions 2601 Performance Ct V
757-270-6025
Chris Hay EnviroTrac Ltd 7343 W. Friendly Ave,336-763-6025
■■■
John Sieger
7/14/21

APPENDIX C
SITE PHOTOGRAHS
____________________________________________________________________________

Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 1: View east of UST excavation.

Photograph 2: View south of kerosene (UST 5) and diesel (UST 4).
Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 3: View of gasoline UST 2.

Photograph 4: View of gasoline UST 2 loaded on the truck.
Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 5: View of UST 3, 4, and 5 in the tank field.

Photograph 6: View of gasoline UST 3.

Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 7: View of Gasoline UST 3 being loaded on truck.

Photograph 8: View of diesel UST 4.

Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 9: View of diesel UST 4.

Photograph 10: View of kerosene UST 5.

Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 11: View of UST tank field excavation.

Photograph 12: View of west of dispensers and product line.
Photographic Documentation
Sheetz Store 391
2100 County Home Road
Greenville, North Carolina

Photograph 13: View north along former kerosene product line.

APPENDIX D
UST LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
June 24, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92545088
92545088
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz 391 11.SZ0391.00
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 69
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92545088001 SS-14 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088002 SS-30 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088003 SS-31 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088004 SS-32 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088005 SS-33 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088006 SS-34 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92545088007 SS-15 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088008 SS-16 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088009 SS-17 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088010 SS-18 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088011 SS-19 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088012 SS-20 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
92545088013 SS-21 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088014 SS-22 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088015 SS-23 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088016 SS-24 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088017 SS-25 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088018 SS-26 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088019 SS-27 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088020 SS-28 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92545088021 SS-29 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 69
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92545088001 SS-14
Diesel Range Organics(C10-C28)12.0 mg/kg 06/22/21 11:306.2EPA 8015C Modified
Percent Moisture 19.2 %06/18/21 14:24 N20.10SW-846
92545088002 SS-30
Percent Moisture 6.0 %06/18/21 14:24 N20.10SW-846
92545088003 SS-31
Percent Moisture 14.5 %06/18/21 14:24 N20.10SW-846
92545088004 SS-32
Percent Moisture 6.4 %06/18/21 14:24 N20.10SW-846
92545088005 SS-33
Percent Moisture 11.5 %06/18/21 15:42 N20.10SW-846
92545088006 SS-34
Percent Moisture 10.5 %06/18/21 15:42 N20.10SW-846
92545088007 SS-15
Acetone 128 ug/kg 06/18/21 05:45105EPA 8260D
Methylene Chloride 178 ug/kg 06/18/21 05:45 C921.0EPA 8260D
Percent Moisture 4.6 %06/18/21 15:42 N20.10SW-846
92545088008 SS-16
Methylene Chloride 145 ug/kg 06/18/21 06:20 C921.4EPA 8260D
Percent Moisture 7.2 %06/18/21 15:42 N20.10SW-846
92545088009 SS-17
Methylene Chloride 175 ug/kg 06/18/21 06:38 C922.3EPA 8260D
Percent Moisture 6.5 %06/18/21 15:42 N20.10SW-846
92545088010 SS-18
Methylene Chloride 154 ug/kg 06/18/21 06:55 C921.1EPA 8260D
Percent Moisture 4.5 %06/18/21 15:42 N20.10SW-846
92545088011 SS-19
Methylene Chloride 131 ug/kg 06/18/21 07:13 C922.1EPA 8260D
Percent Moisture 11.7 %06/18/21 15:42 N20.10SW-846
92545088012 SS-20
Toluene 8.3 ug/kg 06/18/21 07:33 C76.1EPA 8260D
Percent Moisture 8.7 %06/18/21 15:43 N20.10SW-846
92545088013 SS-21
Percent Moisture 4.9 %06/18/21 15:43 N20.10SW-846
92545088014 SS-22
Percent Moisture 6.2 %06/18/21 15:43 N20.10SW-846
92545088015 SS-23
Percent Moisture 8.5 %06/18/21 15:43 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 69
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92545088016 SS-24
Percent Moisture 6.7 %06/18/21 15:43 N20.10SW-846
92545088017 SS-25
Percent Moisture 10.1 %06/18/21 15:43 N20.10SW-846
92545088018 SS-26
o-Xylene 5.5 ug/kg 06/18/21 09:405.3EPA 8260D
Percent Moisture 11.7 %06/18/21 15:43 N20.10SW-846
92545088019 SS-27
Percent Moisture 8.3 %06/18/21 15:43 N20.10SW-846
92545088020 SS-28
Percent Moisture 6.8 %06/18/21 15:43 N20.10SW-846
92545088021 SS-29
Percent Moisture 13.0 %06/18/21 15:43 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-14 Lab ID:92545088001 Collected:06/16/21 09:20 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)12.0 mg/kg 06/22/21 11:3006/18/21 10:346.2 1
Surrogates
n-Pentacosane (S)75 %06/22/21 11:30 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 04:1006/18/21 12:268.3 1
Surrogates
4-Bromofluorobenzene (S)94 %06/20/21 04:10 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.2 %06/18/21 14:24 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-30 Lab ID:92545088002 Collected:06/16/21 10:28 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 11:5406/18/21 10:345.3 1
Surrogates
n-Pentacosane (S)75 %06/22/21 11:54 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 04:3906/18/21 12:266.4 1
Surrogates
4-Bromofluorobenzene (S)93 %06/20/21 04:39 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.0 %06/18/21 14:24 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-31 Lab ID:92545088003 Collected:06/16/21 10:33 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 11:5406/18/21 10:345.9 1
Surrogates
n-Pentacosane (S)65 %06/22/21 11:54 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 05:0706/18/21 12:268.0 1
Surrogates
4-Bromofluorobenzene (S)93 %06/20/21 05:07 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.5 %06/18/21 14:24 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-32 Lab ID:92545088004 Collected:06/16/21 10:38 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 12:1906/18/21 10:345.4 1
Surrogates
n-Pentacosane (S)83 %06/22/21 12:19 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 05:3506/18/21 12:267.5 1
Surrogates
4-Bromofluorobenzene (S)92 %06/20/21 05:35 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.4 %06/18/21 14:24 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-33 Lab ID:92545088005 Collected:06/16/21 10:41 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 12:1906/18/21 10:345.7 1
Surrogates
n-Pentacosane (S)64 %06/22/21 12:19 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 06:0306/18/21 12:267.4 1
Surrogates
4-Bromofluorobenzene (S)93 %06/20/21 06:03 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.5 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-34 Lab ID:92545088006 Collected:06/16/21 10:45 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 12:4306/18/21 10:345.6 1
Surrogates
n-Pentacosane (S)77 %06/22/21 12:43 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 06:3106/18/21 12:266.9 1
Surrogates
4-Bromofluorobenzene (S)94 %06/20/21 06:31 460-00-406/18/21 12:2666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.5 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-15 Lab ID:92545088007 Collected:06/16/21 09:38 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 13:0706/18/21 10:345.2 1
Surrogates
n-Pentacosane (S)62 %06/22/21 13:07 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 01:2006/21/21 09:238.6 1
Surrogates
4-Bromofluorobenzene (S)92 %06/23/21 01:20 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 128 ug/kg 06/18/21 05:45 67-64-106/17/21 18:191051
Benzene ND ug/kg 06/18/21 05:45 71-43-206/17/21 18:195.3 1
Bromobenzene ND ug/kg 06/18/21 05:45 108-86-106/17/21 18:195.3 1
Bromochloromethane ND ug/kg 06/18/21 05:45 74-97-506/17/21 18:195.3 1
Bromodichloromethane ND ug/kg 06/18/21 05:45 75-27-406/17/21 18:195.3 1
Bromoform ND ug/kg 06/18/21 05:45 75-25-206/17/21 18:195.3 1
Bromomethane ND ug/kg 06/18/21 05:45 74-83-9 IK,L1,v106/17/21 18:1910.5 1
2-Butanone (MEK)ND ug/kg 06/18/21 05:45 78-93-306/17/21 18:191051
n-Butylbenzene ND ug/kg 06/18/21 05:45 104-51-806/17/21 18:195.3 1
sec-Butylbenzene ND ug/kg 06/18/21 05:45 135-98-806/17/21 18:195.3 1
tert-Butylbenzene ND ug/kg 06/18/21 05:45 98-06-6 v206/17/21 18:195.3 1
Carbon tetrachloride ND ug/kg 06/18/21 05:45 56-23-506/17/21 18:195.3 1
Chlorobenzene ND ug/kg 06/18/21 05:45 108-90-706/17/21 18:195.3 1
Chloroethane ND ug/kg 06/18/21 05:45 75-00-306/17/21 18:1910.5 1
Chloroform ND ug/kg 06/18/21 05:45 67-66-306/17/21 18:195.3 1
Chloromethane ND ug/kg 06/18/21 05:45 74-87-306/17/21 18:1910.5 1
2-Chlorotoluene ND ug/kg 06/18/21 05:45 95-49-806/17/21 18:195.3 1
4-Chlorotoluene ND ug/kg 06/18/21 05:45 106-43-406/17/21 18:195.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 05:45 96-12-806/17/21 18:195.3 1
Dibromochloromethane ND ug/kg 06/18/21 05:45 124-48-106/17/21 18:195.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 05:45 106-93-406/17/21 18:195.3 1
Dibromomethane ND ug/kg 06/18/21 05:45 74-95-306/17/21 18:195.3 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 05:45 95-50-106/17/21 18:195.3 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 05:45 541-73-106/17/21 18:195.3 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 05:45 106-46-706/17/21 18:195.3 1
Dichlorodifluoromethane ND ug/kg 06/18/21 05:45 75-71-806/17/21 18:1910.5 1
1,1-Dichloroethane ND ug/kg 06/18/21 05:45 75-34-306/17/21 18:195.3 1
1,2-Dichloroethane ND ug/kg 06/18/21 05:45 107-06-206/17/21 18:195.3 1
1,1-Dichloroethene ND ug/kg 06/18/21 05:45 75-35-406/17/21 18:195.3 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 05:45 156-59-206/17/21 18:195.3 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 05:45 156-60-506/17/21 18:195.3 1
1,2-Dichloropropane ND ug/kg 06/18/21 05:45 78-87-506/17/21 18:195.3 1
1,3-Dichloropropane ND ug/kg 06/18/21 05:45 142-28-906/17/21 18:195.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-15 Lab ID:92545088007 Collected:06/16/21 09:38 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 06/18/21 05:45 594-20-706/17/21 18:195.3 1
1,1-Dichloropropene ND ug/kg 06/18/21 05:45 563-58-606/17/21 18:195.3 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 05:45 10061-01-506/17/21 18:195.3 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 05:45 10061-02-606/17/21 18:195.3 1
Diisopropyl ether ND ug/kg 06/18/21 05:45 108-20-306/17/21 18:195.3 1
Ethylbenzene ND ug/kg 06/18/21 05:45 100-41-406/17/21 18:195.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 05:45 87-68-306/17/21 18:1910.5 1
2-Hexanone ND ug/kg 06/18/21 05:45 591-78-606/17/21 18:1952.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 05:45 98-82-806/17/21 18:195.3 1
p-Isopropyltoluene ND ug/kg 06/18/21 05:45 99-87-606/17/21 18:195.3 1
Methylene Chloride 178 ug/kg 06/18/21 05:45 75-09-2 C906/17/21 18:1921.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 05:45 108-10-106/17/21 18:1952.5 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 05:45 1634-04-406/17/21 18:195.3 1
Naphthalene ND ug/kg 06/18/21 05:45 91-20-306/17/21 18:195.3 1
n-Propylbenzene ND ug/kg 06/18/21 05:45 103-65-106/17/21 18:195.3 1
Styrene ND ug/kg 06/18/21 05:45 100-42-506/17/21 18:195.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 05:45 630-20-606/17/21 18:195.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 05:45 79-34-506/17/21 18:195.3 1
Tetrachloroethene ND ug/kg 06/18/21 05:45 127-18-406/17/21 18:195.3 1
Toluene ND ug/kg 06/18/21 05:45 108-88-306/17/21 18:195.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 05:45 87-61-606/17/21 18:195.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 05:45 120-82-106/17/21 18:195.3 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 05:45 71-55-606/17/21 18:195.3 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 05:45 79-00-506/17/21 18:195.3 1
Trichloroethene ND ug/kg 06/18/21 05:45 79-01-606/17/21 18:195.3 1
Trichlorofluoromethane ND ug/kg 06/18/21 05:45 75-69-406/17/21 18:195.3 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 05:45 96-18-406/17/21 18:195.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 05:45 95-63-606/17/21 18:195.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 05:45 108-67-806/17/21 18:195.3 1
Vinyl acetate ND ug/kg 06/18/21 05:45 108-05-406/17/21 18:1952.5 1
Vinyl chloride ND ug/kg 06/18/21 05:45 75-01-406/17/21 18:1910.5 1
Xylene (Total)ND ug/kg 06/18/21 05:45 1330-20-706/17/21 18:1910.5 1
m&p-Xylene ND ug/kg 06/18/21 05:45 179601-23-106/17/21 18:1910.5 1
o-Xylene ND ug/kg 06/18/21 05:45 95-47-606/17/21 18:195.3 1
Surrogates
Toluene-d8 (S)104 %06/18/21 05:45 2037-26-506/17/21 18:1970-130 1
4-Bromofluorobenzene (S)95 %06/18/21 05:45 460-00-406/17/21 18:1969-134 1
1,2-Dichloroethane-d4 (S)104 %06/18/21 05:45 17060-07-006/17/21 18:1970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.6 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-16 Lab ID:92545088008 Collected:06/16/21 09:44 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 13:3006/18/21 10:345.3 1
Surrogates
n-Pentacosane (S)70 %06/22/21 13:30 629-99-206/18/21 10:3432-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 06:5906/18/21 12:266.3 1
Surrogates
4-Bromofluorobenzene (S)93 %06/20/21 06:59 460-00-406/18/21 12:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 06:20 67-64-106/17/21 18:191071
Benzene ND ug/kg 06/18/21 06:20 71-43-206/17/21 18:195.3 1
Bromobenzene ND ug/kg 06/18/21 06:20 108-86-106/17/21 18:195.3 1
Bromochloromethane ND ug/kg 06/18/21 06:20 74-97-506/17/21 18:195.3 1
Bromodichloromethane ND ug/kg 06/18/21 06:20 75-27-406/17/21 18:195.3 1
Bromoform ND ug/kg 06/18/21 06:20 75-25-206/17/21 18:195.3 1
Bromomethane ND ug/kg 06/18/21 06:20 74-83-9 IK,L1,v106/17/21 18:1910.7 1
2-Butanone (MEK)ND ug/kg 06/18/21 06:20 78-93-306/17/21 18:191071
n-Butylbenzene ND ug/kg 06/18/21 06:20 104-51-806/17/21 18:195.3 1
sec-Butylbenzene ND ug/kg 06/18/21 06:20 135-98-806/17/21 18:195.3 1
tert-Butylbenzene ND ug/kg 06/18/21 06:20 98-06-6 v206/17/21 18:195.3 1
Carbon tetrachloride ND ug/kg 06/18/21 06:20 56-23-506/17/21 18:195.3 1
Chlorobenzene ND ug/kg 06/18/21 06:20 108-90-706/17/21 18:195.3 1
Chloroethane ND ug/kg 06/18/21 06:20 75-00-306/17/21 18:1910.7 1
Chloroform ND ug/kg 06/18/21 06:20 67-66-306/17/21 18:195.3 1
Chloromethane ND ug/kg 06/18/21 06:20 74-87-3 M106/17/21 18:1910.7 1
2-Chlorotoluene ND ug/kg 06/18/21 06:20 95-49-806/17/21 18:195.3 1
4-Chlorotoluene ND ug/kg 06/18/21 06:20 106-43-406/17/21 18:195.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 06:20 96-12-806/17/21 18:195.3 1
Dibromochloromethane ND ug/kg 06/18/21 06:20 124-48-106/17/21 18:195.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 06:20 106-93-406/17/21 18:195.3 1
Dibromomethane ND ug/kg 06/18/21 06:20 74-95-306/17/21 18:195.3 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 06:20 95-50-106/17/21 18:195.3 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 06:20 541-73-106/17/21 18:195.3 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 06:20 106-46-706/17/21 18:195.3 1
Dichlorodifluoromethane ND ug/kg 06/18/21 06:20 75-71-806/17/21 18:1910.7 1
1,1-Dichloroethane ND ug/kg 06/18/21 06:20 75-34-306/17/21 18:195.3 1
1,2-Dichloroethane ND ug/kg 06/18/21 06:20 107-06-206/17/21 18:195.3 1
1,1-Dichloroethene ND ug/kg 06/18/21 06:20 75-35-406/17/21 18:195.3 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 06:20 156-59-206/17/21 18:195.3 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 06:20 156-60-506/17/21 18:195.3 1
1,2-Dichloropropane ND ug/kg 06/18/21 06:20 78-87-506/17/21 18:195.3 1
1,3-Dichloropropane ND ug/kg 06/18/21 06:20 142-28-906/17/21 18:195.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-16 Lab ID:92545088008 Collected:06/16/21 09:44 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 06/18/21 06:20 594-20-706/17/21 18:195.3 1
1,1-Dichloropropene ND ug/kg 06/18/21 06:20 563-58-606/17/21 18:195.3 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 06:20 10061-01-506/17/21 18:195.3 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 06:20 10061-02-606/17/21 18:195.3 1
Diisopropyl ether ND ug/kg 06/18/21 06:20 108-20-306/17/21 18:195.3 1
Ethylbenzene ND ug/kg 06/18/21 06:20 100-41-406/17/21 18:195.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 06:20 87-68-306/17/21 18:1910.7 1
2-Hexanone ND ug/kg 06/18/21 06:20 591-78-606/17/21 18:1953.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 06:20 98-82-806/17/21 18:195.3 1
p-Isopropyltoluene ND ug/kg 06/18/21 06:20 99-87-606/17/21 18:195.3 1
Methylene Chloride 145 ug/kg 06/18/21 06:20 75-09-2 C906/17/21 18:1921.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 06:20 108-10-106/17/21 18:1953.4 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 06:20 1634-04-406/17/21 18:195.3 1
Naphthalene ND ug/kg 06/18/21 06:20 91-20-306/17/21 18:195.3 1
n-Propylbenzene ND ug/kg 06/18/21 06:20 103-65-106/17/21 18:195.3 1
Styrene ND ug/kg 06/18/21 06:20 100-42-506/17/21 18:195.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 06:20 630-20-606/17/21 18:195.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 06:20 79-34-506/17/21 18:195.3 1
Tetrachloroethene ND ug/kg 06/18/21 06:20 127-18-406/17/21 18:195.3 1
Toluene ND ug/kg 06/18/21 06:20 108-88-306/17/21 18:195.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 06:20 87-61-606/17/21 18:195.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 06:20 120-82-106/17/21 18:195.3 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 06:20 71-55-606/17/21 18:195.3 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 06:20 79-00-506/17/21 18:195.3 1
Trichloroethene ND ug/kg 06/18/21 06:20 79-01-606/17/21 18:195.3 1
Trichlorofluoromethane ND ug/kg 06/18/21 06:20 75-69-406/17/21 18:195.3 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 06:20 96-18-406/17/21 18:195.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 06:20 95-63-606/17/21 18:195.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 06:20 108-67-806/17/21 18:195.3 1
Vinyl acetate ND ug/kg 06/18/21 06:20 108-05-406/17/21 18:1953.4 1
Vinyl chloride ND ug/kg 06/18/21 06:20 75-01-406/17/21 18:1910.7 1
Xylene (Total)ND ug/kg 06/18/21 06:20 1330-20-706/17/21 18:1910.7 1
m&p-Xylene ND ug/kg 06/18/21 06:20 179601-23-106/17/21 18:1910.7 1
o-Xylene ND ug/kg 06/18/21 06:20 95-47-606/17/21 18:195.3 1
Surrogates
Toluene-d8 (S)103 %06/18/21 06:20 2037-26-506/17/21 18:1970-130 1
4-Bromofluorobenzene (S)94 %06/18/21 06:20 460-00-406/17/21 18:1969-134 1
1,2-Dichloroethane-d4 (S)100 %06/18/21 06:20 17060-07-006/17/21 18:1970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.2 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-17 Lab ID:92545088009 Collected:06/16/21 09:48 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 07:2706/18/21 12:266.3 1
Surrogates
4-Bromofluorobenzene (S)89 %06/20/21 07:27 460-00-406/18/21 12:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 06:38 67-64-106/17/21 18:191121
Benzene ND ug/kg 06/18/21 06:38 71-43-206/17/21 18:195.6 1
Bromobenzene ND ug/kg 06/18/21 06:38 108-86-106/17/21 18:195.6 1
Bromochloromethane ND ug/kg 06/18/21 06:38 74-97-506/17/21 18:195.6 1
Bromodichloromethane ND ug/kg 06/18/21 06:38 75-27-406/17/21 18:195.6 1
Bromoform ND ug/kg 06/18/21 06:38 75-25-206/17/21 18:195.6 1
Bromomethane ND ug/kg 06/18/21 06:38 74-83-9 IK,L1,v106/17/21 18:1911.2 1
2-Butanone (MEK)ND ug/kg 06/18/21 06:38 78-93-306/17/21 18:191121
n-Butylbenzene ND ug/kg 06/18/21 06:38 104-51-806/17/21 18:195.6 1
sec-Butylbenzene ND ug/kg 06/18/21 06:38 135-98-806/17/21 18:195.6 1
tert-Butylbenzene ND ug/kg 06/18/21 06:38 98-06-6 v206/17/21 18:195.6 1
Carbon tetrachloride ND ug/kg 06/18/21 06:38 56-23-506/17/21 18:195.6 1
Chlorobenzene ND ug/kg 06/18/21 06:38 108-90-706/17/21 18:195.6 1
Chloroethane ND ug/kg 06/18/21 06:38 75-00-306/17/21 18:1911.2 1
Chloroform ND ug/kg 06/18/21 06:38 67-66-306/17/21 18:195.6 1
Chloromethane ND ug/kg 06/18/21 06:38 74-87-306/17/21 18:1911.2 1
2-Chlorotoluene ND ug/kg 06/18/21 06:38 95-49-806/17/21 18:195.6 1
4-Chlorotoluene ND ug/kg 06/18/21 06:38 106-43-406/17/21 18:195.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 06:38 96-12-806/17/21 18:195.6 1
Dibromochloromethane ND ug/kg 06/18/21 06:38 124-48-106/17/21 18:195.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 06:38 106-93-406/17/21 18:195.6 1
Dibromomethane ND ug/kg 06/18/21 06:38 74-95-306/17/21 18:195.6 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 06:38 95-50-106/17/21 18:195.6 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 06:38 541-73-106/17/21 18:195.6 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 06:38 106-46-706/17/21 18:195.6 1
Dichlorodifluoromethane ND ug/kg 06/18/21 06:38 75-71-806/17/21 18:1911.2 1
1,1-Dichloroethane ND ug/kg 06/18/21 06:38 75-34-306/17/21 18:195.6 1
1,2-Dichloroethane ND ug/kg 06/18/21 06:38 107-06-206/17/21 18:195.6 1
1,1-Dichloroethene ND ug/kg 06/18/21 06:38 75-35-406/17/21 18:195.6 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 06:38 156-59-206/17/21 18:195.6 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 06:38 156-60-506/17/21 18:195.6 1
1,2-Dichloropropane ND ug/kg 06/18/21 06:38 78-87-506/17/21 18:195.6 1
1,3-Dichloropropane ND ug/kg 06/18/21 06:38 142-28-906/17/21 18:195.6 1
2,2-Dichloropropane ND ug/kg 06/18/21 06:38 594-20-706/17/21 18:195.6 1
1,1-Dichloropropene ND ug/kg 06/18/21 06:38 563-58-606/17/21 18:195.6 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 06:38 10061-01-506/17/21 18:195.6 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 06:38 10061-02-606/17/21 18:195.6 1
Diisopropyl ether ND ug/kg 06/18/21 06:38 108-20-306/17/21 18:195.6 1
Ethylbenzene ND ug/kg 06/18/21 06:38 100-41-406/17/21 18:195.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-17 Lab ID:92545088009 Collected:06/16/21 09:48 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 06:38 87-68-306/17/21 18:1911.2 1
2-Hexanone ND ug/kg 06/18/21 06:38 591-78-606/17/21 18:1955.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 06:38 98-82-806/17/21 18:195.6 1
p-Isopropyltoluene ND ug/kg 06/18/21 06:38 99-87-606/17/21 18:195.6 1
Methylene Chloride 175 ug/kg 06/18/21 06:38 75-09-2 C906/17/21 18:1922.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 06:38 108-10-106/17/21 18:1955.8 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 06:38 1634-04-406/17/21 18:195.6 1
Naphthalene ND ug/kg 06/18/21 06:38 91-20-306/17/21 18:195.6 1
n-Propylbenzene ND ug/kg 06/18/21 06:38 103-65-106/17/21 18:195.6 1
Styrene ND ug/kg 06/18/21 06:38 100-42-506/17/21 18:195.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 06:38 630-20-606/17/21 18:195.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 06:38 79-34-506/17/21 18:195.6 1
Tetrachloroethene ND ug/kg 06/18/21 06:38 127-18-406/17/21 18:195.6 1
Toluene ND ug/kg 06/18/21 06:38 108-88-306/17/21 18:195.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 06:38 87-61-606/17/21 18:195.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 06:38 120-82-106/17/21 18:195.6 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 06:38 71-55-606/17/21 18:195.6 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 06:38 79-00-506/17/21 18:195.6 1
Trichloroethene ND ug/kg 06/18/21 06:38 79-01-606/17/21 18:195.6 1
Trichlorofluoromethane ND ug/kg 06/18/21 06:38 75-69-406/17/21 18:195.6 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 06:38 96-18-406/17/21 18:195.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 06:38 95-63-606/17/21 18:195.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 06:38 108-67-806/17/21 18:195.6 1
Vinyl acetate ND ug/kg 06/18/21 06:38 108-05-406/17/21 18:1955.8 1
Vinyl chloride ND ug/kg 06/18/21 06:38 75-01-406/17/21 18:1911.2 1
Xylene (Total)ND ug/kg 06/18/21 06:38 1330-20-706/17/21 18:1911.2 1
m&p-Xylene ND ug/kg 06/18/21 06:38 179601-23-106/17/21 18:1911.2 1
o-Xylene ND ug/kg 06/18/21 06:38 95-47-606/17/21 18:195.6 1
Surrogates
Toluene-d8 (S)101 %06/18/21 06:38 2037-26-506/17/21 18:1970-130 1
4-Bromofluorobenzene (S)96 %06/18/21 06:38 460-00-406/17/21 18:1969-134 1
1,2-Dichloroethane-d4 (S)102 %06/18/21 06:38 17060-07-006/17/21 18:1970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.5 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-18 Lab ID:92545088010 Collected:06/16/21 09:57 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 07:5506/18/21 12:266.5 1
Surrogates
4-Bromofluorobenzene (S)89 %06/20/21 07:55 460-00-406/18/21 12:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 06:55 67-64-106/17/21 18:191051
Benzene ND ug/kg 06/18/21 06:55 71-43-206/17/21 18:195.3 1
Bromobenzene ND ug/kg 06/18/21 06:55 108-86-106/17/21 18:195.3 1
Bromochloromethane ND ug/kg 06/18/21 06:55 74-97-506/17/21 18:195.3 1
Bromodichloromethane ND ug/kg 06/18/21 06:55 75-27-406/17/21 18:195.3 1
Bromoform ND ug/kg 06/18/21 06:55 75-25-206/17/21 18:195.3 1
Bromomethane ND ug/kg 06/18/21 06:55 74-83-9 IK,L1,v106/17/21 18:1910.5 1
2-Butanone (MEK)ND ug/kg 06/18/21 06:55 78-93-306/17/21 18:191051
n-Butylbenzene ND ug/kg 06/18/21 06:55 104-51-806/17/21 18:195.3 1
sec-Butylbenzene ND ug/kg 06/18/21 06:55 135-98-806/17/21 18:195.3 1
tert-Butylbenzene ND ug/kg 06/18/21 06:55 98-06-6 v206/17/21 18:195.3 1
Carbon tetrachloride ND ug/kg 06/18/21 06:55 56-23-506/17/21 18:195.3 1
Chlorobenzene ND ug/kg 06/18/21 06:55 108-90-706/17/21 18:195.3 1
Chloroethane ND ug/kg 06/18/21 06:55 75-00-306/17/21 18:1910.5 1
Chloroform ND ug/kg 06/18/21 06:55 67-66-306/17/21 18:195.3 1
Chloromethane ND ug/kg 06/18/21 06:55 74-87-306/17/21 18:1910.5 1
2-Chlorotoluene ND ug/kg 06/18/21 06:55 95-49-806/17/21 18:195.3 1
4-Chlorotoluene ND ug/kg 06/18/21 06:55 106-43-406/17/21 18:195.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 06:55 96-12-806/17/21 18:195.3 1
Dibromochloromethane ND ug/kg 06/18/21 06:55 124-48-106/17/21 18:195.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 06:55 106-93-406/17/21 18:195.3 1
Dibromomethane ND ug/kg 06/18/21 06:55 74-95-306/17/21 18:195.3 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 06:55 95-50-106/17/21 18:195.3 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 06:55 541-73-106/17/21 18:195.3 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 06:55 106-46-706/17/21 18:195.3 1
Dichlorodifluoromethane ND ug/kg 06/18/21 06:55 75-71-806/17/21 18:1910.5 1
1,1-Dichloroethane ND ug/kg 06/18/21 06:55 75-34-306/17/21 18:195.3 1
1,2-Dichloroethane ND ug/kg 06/18/21 06:55 107-06-206/17/21 18:195.3 1
1,1-Dichloroethene ND ug/kg 06/18/21 06:55 75-35-406/17/21 18:195.3 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 06:55 156-59-206/17/21 18:195.3 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 06:55 156-60-506/17/21 18:195.3 1
1,2-Dichloropropane ND ug/kg 06/18/21 06:55 78-87-506/17/21 18:195.3 1
1,3-Dichloropropane ND ug/kg 06/18/21 06:55 142-28-906/17/21 18:195.3 1
2,2-Dichloropropane ND ug/kg 06/18/21 06:55 594-20-706/17/21 18:195.3 1
1,1-Dichloropropene ND ug/kg 06/18/21 06:55 563-58-606/17/21 18:195.3 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 06:55 10061-01-506/17/21 18:195.3 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 06:55 10061-02-606/17/21 18:195.3 1
Diisopropyl ether ND ug/kg 06/18/21 06:55 108-20-306/17/21 18:195.3 1
Ethylbenzene ND ug/kg 06/18/21 06:55 100-41-406/17/21 18:195.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-18 Lab ID:92545088010 Collected:06/16/21 09:57 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 06:55 87-68-306/17/21 18:1910.5 1
2-Hexanone ND ug/kg 06/18/21 06:55 591-78-606/17/21 18:1952.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 06:55 98-82-806/17/21 18:195.3 1
p-Isopropyltoluene ND ug/kg 06/18/21 06:55 99-87-606/17/21 18:195.3 1
Methylene Chloride 154 ug/kg 06/18/21 06:55 75-09-2 C906/17/21 18:1921.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 06:55 108-10-106/17/21 18:1952.6 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 06:55 1634-04-406/17/21 18:195.3 1
Naphthalene ND ug/kg 06/18/21 06:55 91-20-306/17/21 18:195.3 1
n-Propylbenzene ND ug/kg 06/18/21 06:55 103-65-106/17/21 18:195.3 1
Styrene ND ug/kg 06/18/21 06:55 100-42-506/17/21 18:195.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 06:55 630-20-606/17/21 18:195.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 06:55 79-34-506/17/21 18:195.3 1
Tetrachloroethene ND ug/kg 06/18/21 06:55 127-18-406/17/21 18:195.3 1
Toluene ND ug/kg 06/18/21 06:55 108-88-306/17/21 18:195.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 06:55 87-61-606/17/21 18:195.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 06:55 120-82-106/17/21 18:195.3 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 06:55 71-55-606/17/21 18:195.3 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 06:55 79-00-506/17/21 18:195.3 1
Trichloroethene ND ug/kg 06/18/21 06:55 79-01-606/17/21 18:195.3 1
Trichlorofluoromethane ND ug/kg 06/18/21 06:55 75-69-406/17/21 18:195.3 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 06:55 96-18-406/17/21 18:195.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 06:55 95-63-606/17/21 18:195.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 06:55 108-67-806/17/21 18:195.3 1
Vinyl acetate ND ug/kg 06/18/21 06:55 108-05-406/17/21 18:1952.6 1
Vinyl chloride ND ug/kg 06/18/21 06:55 75-01-406/17/21 18:1910.5 1
Xylene (Total)ND ug/kg 06/18/21 06:55 1330-20-706/17/21 18:1910.5 1
m&p-Xylene ND ug/kg 06/18/21 06:55 179601-23-106/17/21 18:1910.5 1
o-Xylene ND ug/kg 06/18/21 06:55 95-47-606/17/21 18:195.3 1
Surrogates
Toluene-d8 (S)103 %06/18/21 06:55 2037-26-506/17/21 18:1970-130 1
4-Bromofluorobenzene (S)96 %06/18/21 06:55 460-00-406/17/21 18:1969-134 1
1,2-Dichloroethane-d4 (S)104 %06/18/21 06:55 17060-07-006/17/21 18:1970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.5 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-19 Lab ID:92545088011 Collected:06/16/21 09:54 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 08:5106/18/21 12:2611.8 1
Surrogates
4-Bromofluorobenzene (S)93 %06/20/21 08:51 460-00-406/18/21 12:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 07:13 67-64-106/17/21 18:191111
Benzene ND ug/kg 06/18/21 07:13 71-43-206/17/21 18:195.5 1
Bromobenzene ND ug/kg 06/18/21 07:13 108-86-106/17/21 18:195.5 1
Bromochloromethane ND ug/kg 06/18/21 07:13 74-97-506/17/21 18:195.5 1
Bromodichloromethane ND ug/kg 06/18/21 07:13 75-27-406/17/21 18:195.5 1
Bromoform ND ug/kg 06/18/21 07:13 75-25-206/17/21 18:195.5 1
Bromomethane ND ug/kg 06/18/21 07:13 74-83-9 IK,L1,v106/17/21 18:1911.1 1
2-Butanone (MEK)ND ug/kg 06/18/21 07:13 78-93-306/17/21 18:191111
n-Butylbenzene ND ug/kg 06/18/21 07:13 104-51-806/17/21 18:195.5 1
sec-Butylbenzene ND ug/kg 06/18/21 07:13 135-98-806/17/21 18:195.5 1
tert-Butylbenzene ND ug/kg 06/18/21 07:13 98-06-6 v206/17/21 18:195.5 1
Carbon tetrachloride ND ug/kg 06/18/21 07:13 56-23-506/17/21 18:195.5 1
Chlorobenzene ND ug/kg 06/18/21 07:13 108-90-706/17/21 18:195.5 1
Chloroethane ND ug/kg 06/18/21 07:13 75-00-306/17/21 18:1911.1 1
Chloroform ND ug/kg 06/18/21 07:13 67-66-306/17/21 18:195.5 1
Chloromethane ND ug/kg 06/18/21 07:13 74-87-306/17/21 18:1911.1 1
2-Chlorotoluene ND ug/kg 06/18/21 07:13 95-49-806/17/21 18:195.5 1
4-Chlorotoluene ND ug/kg 06/18/21 07:13 106-43-406/17/21 18:195.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 07:13 96-12-806/17/21 18:195.5 1
Dibromochloromethane ND ug/kg 06/18/21 07:13 124-48-106/17/21 18:195.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 07:13 106-93-406/17/21 18:195.5 1
Dibromomethane ND ug/kg 06/18/21 07:13 74-95-306/17/21 18:195.5 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 07:13 95-50-106/17/21 18:195.5 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 07:13 541-73-106/17/21 18:195.5 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 07:13 106-46-706/17/21 18:195.5 1
Dichlorodifluoromethane ND ug/kg 06/18/21 07:13 75-71-806/17/21 18:1911.1 1
1,1-Dichloroethane ND ug/kg 06/18/21 07:13 75-34-306/17/21 18:195.5 1
1,2-Dichloroethane ND ug/kg 06/18/21 07:13 107-06-206/17/21 18:195.5 1
1,1-Dichloroethene ND ug/kg 06/18/21 07:13 75-35-406/17/21 18:195.5 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 07:13 156-59-206/17/21 18:195.5 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 07:13 156-60-506/17/21 18:195.5 1
1,2-Dichloropropane ND ug/kg 06/18/21 07:13 78-87-506/17/21 18:195.5 1
1,3-Dichloropropane ND ug/kg 06/18/21 07:13 142-28-906/17/21 18:195.5 1
2,2-Dichloropropane ND ug/kg 06/18/21 07:13 594-20-706/17/21 18:195.5 1
1,1-Dichloropropene ND ug/kg 06/18/21 07:13 563-58-606/17/21 18:195.5 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 07:13 10061-01-506/17/21 18:195.5 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 07:13 10061-02-606/17/21 18:195.5 1
Diisopropyl ether ND ug/kg 06/18/21 07:13 108-20-306/17/21 18:195.5 1
Ethylbenzene ND ug/kg 06/18/21 07:13 100-41-406/17/21 18:195.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-19 Lab ID:92545088011 Collected:06/16/21 09:54 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 07:13 87-68-306/17/21 18:1911.1 1
2-Hexanone ND ug/kg 06/18/21 07:13 591-78-606/17/21 18:1955.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 07:13 98-82-806/17/21 18:195.5 1
p-Isopropyltoluene ND ug/kg 06/18/21 07:13 99-87-606/17/21 18:195.5 1
Methylene Chloride 131 ug/kg 06/18/21 07:13 75-09-2 C906/17/21 18:1922.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 07:13 108-10-106/17/21 18:1955.3 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 07:13 1634-04-406/17/21 18:195.5 1
Naphthalene ND ug/kg 06/18/21 07:13 91-20-306/17/21 18:195.5 1
n-Propylbenzene ND ug/kg 06/18/21 07:13 103-65-106/17/21 18:195.5 1
Styrene ND ug/kg 06/18/21 07:13 100-42-506/17/21 18:195.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 07:13 630-20-606/17/21 18:195.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 07:13 79-34-506/17/21 18:195.5 1
Tetrachloroethene ND ug/kg 06/18/21 07:13 127-18-406/17/21 18:195.5 1
Toluene ND ug/kg 06/18/21 07:13 108-88-306/17/21 18:195.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 07:13 87-61-606/17/21 18:195.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 07:13 120-82-106/17/21 18:195.5 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 07:13 71-55-606/17/21 18:195.5 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 07:13 79-00-506/17/21 18:195.5 1
Trichloroethene ND ug/kg 06/18/21 07:13 79-01-606/17/21 18:195.5 1
Trichlorofluoromethane ND ug/kg 06/18/21 07:13 75-69-406/17/21 18:195.5 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 07:13 96-18-406/17/21 18:195.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 07:13 95-63-606/17/21 18:195.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 07:13 108-67-806/17/21 18:195.5 1
Vinyl acetate ND ug/kg 06/18/21 07:13 108-05-406/17/21 18:1955.3 1
Vinyl chloride ND ug/kg 06/18/21 07:13 75-01-406/17/21 18:1911.1 1
Xylene (Total)ND ug/kg 06/18/21 07:13 1330-20-706/17/21 18:1911.1 1
m&p-Xylene ND ug/kg 06/18/21 07:13 179601-23-106/17/21 18:1911.1 1
o-Xylene ND ug/kg 06/18/21 07:13 95-47-606/17/21 18:195.5 1
Surrogates
Toluene-d8 (S)103 %06/18/21 07:13 2037-26-506/17/21 18:1970-130 1
4-Bromofluorobenzene (S)96 %06/18/21 07:13 460-00-406/17/21 18:1969-134 1
1,2-Dichloroethane-d4 (S)101 %06/18/21 07:13 17060-07-006/17/21 18:1970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %06/18/21 15:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-20 Lab ID:92545088012 Collected:06/16/21 09:58 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/20/21 08:2306/18/21 12:266.6 1
Surrogates
4-Bromofluorobenzene (S)92 %06/20/21 08:23 460-00-406/18/21 12:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 07:33 67-64-106/17/21 18:241211
Benzene ND ug/kg 06/18/21 07:33 71-43-206/17/21 18:246.1 1
Bromobenzene ND ug/kg 06/18/21 07:33 108-86-106/17/21 18:246.1 1
Bromochloromethane ND ug/kg 06/18/21 07:33 74-97-506/17/21 18:246.1 1
Bromodichloromethane ND ug/kg 06/18/21 07:33 75-27-406/17/21 18:246.1 1
Bromoform ND ug/kg 06/18/21 07:33 75-25-206/17/21 18:246.1 1
Bromomethane ND ug/kg 06/18/21 07:33 74-83-9 IK,L1,v106/17/21 18:2412.1 1
2-Butanone (MEK)ND ug/kg 06/18/21 07:33 78-93-306/17/21 18:241211
n-Butylbenzene ND ug/kg 06/18/21 07:33 104-51-806/17/21 18:246.1 1
sec-Butylbenzene ND ug/kg 06/18/21 07:33 135-98-806/17/21 18:246.1 1
tert-Butylbenzene ND ug/kg 06/18/21 07:33 98-06-606/17/21 18:246.1 1
Carbon tetrachloride ND ug/kg 06/18/21 07:33 56-23-506/17/21 18:246.1 1
Chlorobenzene ND ug/kg 06/18/21 07:33 108-90-706/17/21 18:246.1 1
Chloroethane ND ug/kg 06/18/21 07:33 75-00-306/17/21 18:2412.1 1
Chloroform ND ug/kg 06/18/21 07:33 67-66-306/17/21 18:246.1 1
Chloromethane ND ug/kg 06/18/21 07:33 74-87-306/17/21 18:2412.1 1
2-Chlorotoluene ND ug/kg 06/18/21 07:33 95-49-806/17/21 18:246.1 1
4-Chlorotoluene ND ug/kg 06/18/21 07:33 106-43-406/17/21 18:246.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 07:33 96-12-806/17/21 18:246.1 1
Dibromochloromethane ND ug/kg 06/18/21 07:33 124-48-106/17/21 18:246.1 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 07:33 106-93-406/17/21 18:246.1 1
Dibromomethane ND ug/kg 06/18/21 07:33 74-95-306/17/21 18:246.1 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 07:33 95-50-106/17/21 18:246.1 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 07:33 541-73-106/17/21 18:246.1 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 07:33 106-46-706/17/21 18:246.1 1
Dichlorodifluoromethane ND ug/kg 06/18/21 07:33 75-71-806/17/21 18:2412.1 1
1,1-Dichloroethane ND ug/kg 06/18/21 07:33 75-34-306/17/21 18:246.1 1
1,2-Dichloroethane ND ug/kg 06/18/21 07:33 107-06-206/17/21 18:246.1 1
1,1-Dichloroethene ND ug/kg 06/18/21 07:33 75-35-406/17/21 18:246.1 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 07:33 156-59-206/17/21 18:246.1 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 07:33 156-60-506/17/21 18:246.1 1
1,2-Dichloropropane ND ug/kg 06/18/21 07:33 78-87-506/17/21 18:246.1 1
1,3-Dichloropropane ND ug/kg 06/18/21 07:33 142-28-906/17/21 18:246.1 1
2,2-Dichloropropane ND ug/kg 06/18/21 07:33 594-20-706/17/21 18:246.1 1
1,1-Dichloropropene ND ug/kg 06/18/21 07:33 563-58-606/17/21 18:246.1 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 07:33 10061-01-506/17/21 18:246.1 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 07:33 10061-02-606/17/21 18:246.1 1
Diisopropyl ether ND ug/kg 06/18/21 07:33 108-20-306/17/21 18:246.1 1
Ethylbenzene ND ug/kg 06/18/21 07:33 100-41-406/17/21 18:246.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-20 Lab ID:92545088012 Collected:06/16/21 09:58 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 07:33 87-68-306/17/21 18:2412.1 1
2-Hexanone ND ug/kg 06/18/21 07:33 591-78-606/17/21 18:2460.7 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 07:33 98-82-806/17/21 18:246.1 1
p-Isopropyltoluene ND ug/kg 06/18/21 07:33 99-87-606/17/21 18:246.1 1
Methylene Chloride ND ug/kg 06/18/21 07:33 75-09-206/17/21 18:2424.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 07:33 108-10-106/17/21 18:2460.7 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 07:33 1634-04-406/17/21 18:246.1 1
Naphthalene ND ug/kg 06/18/21 07:33 91-20-306/17/21 18:246.1 1
n-Propylbenzene ND ug/kg 06/18/21 07:33 103-65-106/17/21 18:246.1 1
Styrene ND ug/kg 06/18/21 07:33 100-42-506/17/21 18:246.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 07:33 630-20-606/17/21 18:246.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 07:33 79-34-506/17/21 18:246.1 1
Tetrachloroethene ND ug/kg 06/18/21 07:33 127-18-406/17/21 18:246.1 1
Toluene 8.3 ug/kg 06/18/21 07:33 108-88-3 C706/17/21 18:246.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 07:33 87-61-606/17/21 18:246.1 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 07:33 120-82-106/17/21 18:246.1 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 07:33 71-55-606/17/21 18:246.1 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 07:33 79-00-506/17/21 18:246.1 1
Trichloroethene ND ug/kg 06/18/21 07:33 79-01-606/17/21 18:246.1 1
Trichlorofluoromethane ND ug/kg 06/18/21 07:33 75-69-406/17/21 18:246.1 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 07:33 96-18-406/17/21 18:246.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 07:33 95-63-606/17/21 18:246.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 07:33 108-67-806/17/21 18:246.1 1
Vinyl acetate ND ug/kg 06/18/21 07:33 108-05-406/17/21 18:2460.7 1
Vinyl chloride ND ug/kg 06/18/21 07:33 75-01-406/17/21 18:2412.1 1
Xylene (Total)ND ug/kg 06/18/21 07:33 1330-20-706/17/21 18:2412.1 1
m&p-Xylene ND ug/kg 06/18/21 07:33 179601-23-106/17/21 18:2412.1 1
o-Xylene ND ug/kg 06/18/21 07:33 95-47-606/17/21 18:246.1 1
Surrogates
Toluene-d8 (S)103 %06/18/21 07:33 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)101 %06/18/21 07:33 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 07:33 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 8.7 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-21 Lab ID:92545088013 Collected:06/16/21 10:02 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 01:4806/21/21 09:236.5 1
Surrogates
4-Bromofluorobenzene (S)94 %06/23/21 01:48 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 08:09 67-64-106/17/21 18:241021
Benzene ND ug/kg 06/18/21 08:09 71-43-206/17/21 18:245.1 1
Bromobenzene ND ug/kg 06/18/21 08:09 108-86-106/17/21 18:245.1 1
Bromochloromethane ND ug/kg 06/18/21 08:09 74-97-506/17/21 18:245.1 1
Bromodichloromethane ND ug/kg 06/18/21 08:09 75-27-406/17/21 18:245.1 1
Bromoform ND ug/kg 06/18/21 08:09 75-25-2 M106/17/21 18:245.1 1
Bromomethane ND ug/kg 06/18/21 08:09 74-83-9 IK,L1,v106/17/21 18:2410.2 1
2-Butanone (MEK)ND ug/kg 06/18/21 08:09 78-93-306/17/21 18:241021
n-Butylbenzene ND ug/kg 06/18/21 08:09 104-51-806/17/21 18:245.1 1
sec-Butylbenzene ND ug/kg 06/18/21 08:09 135-98-806/17/21 18:245.1 1
tert-Butylbenzene ND ug/kg 06/18/21 08:09 98-06-606/17/21 18:245.1 1
Carbon tetrachloride ND ug/kg 06/18/21 08:09 56-23-506/17/21 18:245.1 1
Chlorobenzene ND ug/kg 06/18/21 08:09 108-90-706/17/21 18:245.1 1
Chloroethane ND ug/kg 06/18/21 08:09 75-00-306/17/21 18:2410.2 1
Chloroform ND ug/kg 06/18/21 08:09 67-66-306/17/21 18:245.1 1
Chloromethane ND ug/kg 06/18/21 08:09 74-87-306/17/21 18:2410.2 1
2-Chlorotoluene ND ug/kg 06/18/21 08:09 95-49-806/17/21 18:245.1 1
4-Chlorotoluene ND ug/kg 06/18/21 08:09 106-43-406/17/21 18:245.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 08:09 96-12-806/17/21 18:245.1 1
Dibromochloromethane ND ug/kg 06/18/21 08:09 124-48-1 M106/17/21 18:245.1 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 08:09 106-93-406/17/21 18:245.1 1
Dibromomethane ND ug/kg 06/18/21 08:09 74-95-306/17/21 18:245.1 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 08:09 95-50-106/17/21 18:245.1 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 08:09 541-73-106/17/21 18:245.1 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 08:09 106-46-706/17/21 18:245.1 1
Dichlorodifluoromethane ND ug/kg 06/18/21 08:09 75-71-806/17/21 18:2410.2 1
1,1-Dichloroethane ND ug/kg 06/18/21 08:09 75-34-306/17/21 18:245.1 1
1,2-Dichloroethane ND ug/kg 06/18/21 08:09 107-06-206/17/21 18:245.1 1
1,1-Dichloroethene ND ug/kg 06/18/21 08:09 75-35-406/17/21 18:245.1 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 08:09 156-59-206/17/21 18:245.1 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 08:09 156-60-506/17/21 18:245.1 1
1,2-Dichloropropane ND ug/kg 06/18/21 08:09 78-87-506/17/21 18:245.1 1
1,3-Dichloropropane ND ug/kg 06/18/21 08:09 142-28-906/17/21 18:245.1 1
2,2-Dichloropropane ND ug/kg 06/18/21 08:09 594-20-706/17/21 18:245.1 1
1,1-Dichloropropene ND ug/kg 06/18/21 08:09 563-58-606/17/21 18:245.1 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 08:09 10061-01-506/17/21 18:245.1 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 08:09 10061-02-606/17/21 18:245.1 1
Diisopropyl ether ND ug/kg 06/18/21 08:09 108-20-306/17/21 18:245.1 1
Ethylbenzene ND ug/kg 06/18/21 08:09 100-41-406/17/21 18:245.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-21 Lab ID:92545088013 Collected:06/16/21 10:02 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 08:09 87-68-306/17/21 18:2410.2 1
2-Hexanone ND ug/kg 06/18/21 08:09 591-78-606/17/21 18:2450.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 08:09 98-82-806/17/21 18:245.1 1
p-Isopropyltoluene ND ug/kg 06/18/21 08:09 99-87-606/17/21 18:245.1 1
Methylene Chloride ND ug/kg 06/18/21 08:09 75-09-206/17/21 18:2420.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 08:09 108-10-106/17/21 18:2450.9 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 08:09 1634-04-406/17/21 18:245.1 1
Naphthalene ND ug/kg 06/18/21 08:09 91-20-306/17/21 18:245.1 1
n-Propylbenzene ND ug/kg 06/18/21 08:09 103-65-106/17/21 18:245.1 1
Styrene ND ug/kg 06/18/21 08:09 100-42-506/17/21 18:245.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 08:09 630-20-606/17/21 18:245.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 08:09 79-34-506/17/21 18:245.1 1
Tetrachloroethene ND ug/kg 06/18/21 08:09 127-18-4 M106/17/21 18:245.1 1
Toluene ND ug/kg 06/18/21 08:09 108-88-306/17/21 18:245.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 08:09 87-61-606/17/21 18:245.1 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 08:09 120-82-106/17/21 18:245.1 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 08:09 71-55-606/17/21 18:245.1 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 08:09 79-00-506/17/21 18:245.1 1
Trichloroethene ND ug/kg 06/18/21 08:09 79-01-606/17/21 18:245.1 1
Trichlorofluoromethane ND ug/kg 06/18/21 08:09 75-69-406/17/21 18:245.1 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 08:09 96-18-406/17/21 18:245.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 08:09 95-63-606/17/21 18:245.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 08:09 108-67-806/17/21 18:245.1 1
Vinyl acetate ND ug/kg 06/18/21 08:09 108-05-406/17/21 18:2450.9 1
Vinyl chloride ND ug/kg 06/18/21 08:09 75-01-406/17/21 18:2410.2 1
Xylene (Total)ND ug/kg 06/18/21 08:09 1330-20-706/17/21 18:2410.2 1
m&p-Xylene ND ug/kg 06/18/21 08:09 179601-23-106/17/21 18:2410.2 1
o-Xylene ND ug/kg 06/18/21 08:09 95-47-606/17/21 18:245.1 1
Surrogates
Toluene-d8 (S)103 %06/18/21 08:09 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)102 %06/18/21 08:09 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)117 %06/18/21 08:09 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.9 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-22 Lab ID:92545088014 Collected:06/16/21 10:05 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 02:1606/21/21 09:236.6 1
Surrogates
4-Bromofluorobenzene (S)95 %06/23/21 02:16 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 08:27 67-64-106/17/21 18:241511
Benzene ND ug/kg 06/18/21 08:27 71-43-206/17/21 18:247.6 1
Bromobenzene ND ug/kg 06/18/21 08:27 108-86-106/17/21 18:247.6 1
Bromochloromethane ND ug/kg 06/18/21 08:27 74-97-506/17/21 18:247.6 1
Bromodichloromethane ND ug/kg 06/18/21 08:27 75-27-406/17/21 18:247.6 1
Bromoform ND ug/kg 06/18/21 08:27 75-25-206/17/21 18:247.6 1
Bromomethane ND ug/kg 06/18/21 08:27 74-83-9 IK,L1,v106/17/21 18:2415.1 1
2-Butanone (MEK)ND ug/kg 06/18/21 08:27 78-93-306/17/21 18:241511
n-Butylbenzene ND ug/kg 06/18/21 08:27 104-51-806/17/21 18:247.6 1
sec-Butylbenzene ND ug/kg 06/18/21 08:27 135-98-806/17/21 18:247.6 1
tert-Butylbenzene ND ug/kg 06/18/21 08:27 98-06-606/17/21 18:247.6 1
Carbon tetrachloride ND ug/kg 06/18/21 08:27 56-23-506/17/21 18:247.6 1
Chlorobenzene ND ug/kg 06/18/21 08:27 108-90-706/17/21 18:247.6 1
Chloroethane ND ug/kg 06/18/21 08:27 75-00-306/17/21 18:2415.1 1
Chloroform ND ug/kg 06/18/21 08:27 67-66-306/17/21 18:247.6 1
Chloromethane ND ug/kg 06/18/21 08:27 74-87-306/17/21 18:2415.1 1
2-Chlorotoluene ND ug/kg 06/18/21 08:27 95-49-806/17/21 18:247.6 1
4-Chlorotoluene ND ug/kg 06/18/21 08:27 106-43-406/17/21 18:247.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 08:27 96-12-806/17/21 18:247.6 1
Dibromochloromethane ND ug/kg 06/18/21 08:27 124-48-106/17/21 18:247.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 08:27 106-93-406/17/21 18:247.6 1
Dibromomethane ND ug/kg 06/18/21 08:27 74-95-306/17/21 18:247.6 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 08:27 95-50-106/17/21 18:247.6 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 08:27 541-73-106/17/21 18:247.6 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 08:27 106-46-706/17/21 18:247.6 1
Dichlorodifluoromethane ND ug/kg 06/18/21 08:27 75-71-806/17/21 18:2415.1 1
1,1-Dichloroethane ND ug/kg 06/18/21 08:27 75-34-306/17/21 18:247.6 1
1,2-Dichloroethane ND ug/kg 06/18/21 08:27 107-06-206/17/21 18:247.6 1
1,1-Dichloroethene ND ug/kg 06/18/21 08:27 75-35-406/17/21 18:247.6 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 08:27 156-59-206/17/21 18:247.6 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 08:27 156-60-506/17/21 18:247.6 1
1,2-Dichloropropane ND ug/kg 06/18/21 08:27 78-87-506/17/21 18:247.6 1
1,3-Dichloropropane ND ug/kg 06/18/21 08:27 142-28-906/17/21 18:247.6 1
2,2-Dichloropropane ND ug/kg 06/18/21 08:27 594-20-706/17/21 18:247.6 1
1,1-Dichloropropene ND ug/kg 06/18/21 08:27 563-58-606/17/21 18:247.6 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 08:27 10061-01-506/17/21 18:247.6 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 08:27 10061-02-606/17/21 18:247.6 1
Diisopropyl ether ND ug/kg 06/18/21 08:27 108-20-306/17/21 18:247.6 1
Ethylbenzene ND ug/kg 06/18/21 08:27 100-41-406/17/21 18:247.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-22 Lab ID:92545088014 Collected:06/16/21 10:05 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 08:27 87-68-306/17/21 18:2415.1 1
2-Hexanone ND ug/kg 06/18/21 08:27 591-78-606/17/21 18:2475.7 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 08:27 98-82-806/17/21 18:247.6 1
p-Isopropyltoluene ND ug/kg 06/18/21 08:27 99-87-606/17/21 18:247.6 1
Methylene Chloride ND ug/kg 06/18/21 08:27 75-09-206/17/21 18:2430.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 08:27 108-10-106/17/21 18:2475.7 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 08:27 1634-04-406/17/21 18:247.6 1
Naphthalene ND ug/kg 06/18/21 08:27 91-20-306/17/21 18:247.6 1
n-Propylbenzene ND ug/kg 06/18/21 08:27 103-65-106/17/21 18:247.6 1
Styrene ND ug/kg 06/18/21 08:27 100-42-506/17/21 18:247.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 08:27 630-20-606/17/21 18:247.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 08:27 79-34-506/17/21 18:247.6 1
Tetrachloroethene ND ug/kg 06/18/21 08:27 127-18-406/17/21 18:247.6 1
Toluene ND ug/kg 06/18/21 08:27 108-88-306/17/21 18:247.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 08:27 87-61-606/17/21 18:247.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 08:27 120-82-106/17/21 18:247.6 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 08:27 71-55-606/17/21 18:247.6 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 08:27 79-00-506/17/21 18:247.6 1
Trichloroethene ND ug/kg 06/18/21 08:27 79-01-606/17/21 18:247.6 1
Trichlorofluoromethane ND ug/kg 06/18/21 08:27 75-69-406/17/21 18:247.6 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 08:27 96-18-406/17/21 18:247.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 08:27 95-63-606/17/21 18:247.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 08:27 108-67-806/17/21 18:247.6 1
Vinyl acetate ND ug/kg 06/18/21 08:27 108-05-406/17/21 18:2475.7 1
Vinyl chloride ND ug/kg 06/18/21 08:27 75-01-406/17/21 18:2415.1 1
Xylene (Total)ND ug/kg 06/18/21 08:27 1330-20-706/17/21 18:2415.1 1
m&p-Xylene ND ug/kg 06/18/21 08:27 179601-23-106/17/21 18:2415.1 1
o-Xylene ND ug/kg 06/18/21 08:27 95-47-606/17/21 18:247.6 1
Surrogates
Toluene-d8 (S)102 %06/18/21 08:27 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)99 %06/18/21 08:27 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 08:27 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.2 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-23 Lab ID:92545088015 Collected:06/16/21 10:07 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 02:4406/21/21 09:236.0 1
Surrogates
4-Bromofluorobenzene (S)91 %06/23/21 02:44 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 08:45 67-64-106/17/21 18:241291
Benzene ND ug/kg 06/18/21 08:45 71-43-206/17/21 18:246.5 1
Bromobenzene ND ug/kg 06/18/21 08:45 108-86-106/17/21 18:246.5 1
Bromochloromethane ND ug/kg 06/18/21 08:45 74-97-506/17/21 18:246.5 1
Bromodichloromethane ND ug/kg 06/18/21 08:45 75-27-406/17/21 18:246.5 1
Bromoform ND ug/kg 06/18/21 08:45 75-25-206/17/21 18:246.5 1
Bromomethane ND ug/kg 06/18/21 08:45 74-83-9 IK,L1,v106/17/21 18:2412.9 1
2-Butanone (MEK)ND ug/kg 06/18/21 08:45 78-93-306/17/21 18:241291
n-Butylbenzene ND ug/kg 06/18/21 08:45 104-51-806/17/21 18:246.5 1
sec-Butylbenzene ND ug/kg 06/18/21 08:45 135-98-806/17/21 18:246.5 1
tert-Butylbenzene ND ug/kg 06/18/21 08:45 98-06-606/17/21 18:246.5 1
Carbon tetrachloride ND ug/kg 06/18/21 08:45 56-23-506/17/21 18:246.5 1
Chlorobenzene ND ug/kg 06/18/21 08:45 108-90-706/17/21 18:246.5 1
Chloroethane ND ug/kg 06/18/21 08:45 75-00-306/17/21 18:2412.9 1
Chloroform ND ug/kg 06/18/21 08:45 67-66-306/17/21 18:246.5 1
Chloromethane ND ug/kg 06/18/21 08:45 74-87-306/17/21 18:2412.9 1
2-Chlorotoluene ND ug/kg 06/18/21 08:45 95-49-806/17/21 18:246.5 1
4-Chlorotoluene ND ug/kg 06/18/21 08:45 106-43-406/17/21 18:246.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 08:45 96-12-806/17/21 18:246.5 1
Dibromochloromethane ND ug/kg 06/18/21 08:45 124-48-106/17/21 18:246.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 08:45 106-93-406/17/21 18:246.5 1
Dibromomethane ND ug/kg 06/18/21 08:45 74-95-306/17/21 18:246.5 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 08:45 95-50-106/17/21 18:246.5 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 08:45 541-73-106/17/21 18:246.5 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 08:45 106-46-706/17/21 18:246.5 1
Dichlorodifluoromethane ND ug/kg 06/18/21 08:45 75-71-806/17/21 18:2412.9 1
1,1-Dichloroethane ND ug/kg 06/18/21 08:45 75-34-306/17/21 18:246.5 1
1,2-Dichloroethane ND ug/kg 06/18/21 08:45 107-06-206/17/21 18:246.5 1
1,1-Dichloroethene ND ug/kg 06/18/21 08:45 75-35-406/17/21 18:246.5 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 08:45 156-59-206/17/21 18:246.5 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 08:45 156-60-506/17/21 18:246.5 1
1,2-Dichloropropane ND ug/kg 06/18/21 08:45 78-87-506/17/21 18:246.5 1
1,3-Dichloropropane ND ug/kg 06/18/21 08:45 142-28-906/17/21 18:246.5 1
2,2-Dichloropropane ND ug/kg 06/18/21 08:45 594-20-706/17/21 18:246.5 1
1,1-Dichloropropene ND ug/kg 06/18/21 08:45 563-58-606/17/21 18:246.5 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 08:45 10061-01-506/17/21 18:246.5 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 08:45 10061-02-606/17/21 18:246.5 1
Diisopropyl ether ND ug/kg 06/18/21 08:45 108-20-306/17/21 18:246.5 1
Ethylbenzene ND ug/kg 06/18/21 08:45 100-41-406/17/21 18:246.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-23 Lab ID:92545088015 Collected:06/16/21 10:07 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 08:45 87-68-306/17/21 18:2412.9 1
2-Hexanone ND ug/kg 06/18/21 08:45 591-78-606/17/21 18:2464.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 08:45 98-82-806/17/21 18:246.5 1
p-Isopropyltoluene ND ug/kg 06/18/21 08:45 99-87-606/17/21 18:246.5 1
Methylene Chloride ND ug/kg 06/18/21 08:45 75-09-206/17/21 18:2425.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 08:45 108-10-106/17/21 18:2464.5 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 08:45 1634-04-406/17/21 18:246.5 1
Naphthalene ND ug/kg 06/18/21 08:45 91-20-306/17/21 18:246.5 1
n-Propylbenzene ND ug/kg 06/18/21 08:45 103-65-106/17/21 18:246.5 1
Styrene ND ug/kg 06/18/21 08:45 100-42-506/17/21 18:246.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 08:45 630-20-606/17/21 18:246.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 08:45 79-34-506/17/21 18:246.5 1
Tetrachloroethene ND ug/kg 06/18/21 08:45 127-18-406/17/21 18:246.5 1
Toluene ND ug/kg 06/18/21 08:45 108-88-306/17/21 18:246.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 08:45 87-61-606/17/21 18:246.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 08:45 120-82-106/17/21 18:246.5 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 08:45 71-55-606/17/21 18:246.5 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 08:45 79-00-506/17/21 18:246.5 1
Trichloroethene ND ug/kg 06/18/21 08:45 79-01-606/17/21 18:246.5 1
Trichlorofluoromethane ND ug/kg 06/18/21 08:45 75-69-406/17/21 18:246.5 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 08:45 96-18-406/17/21 18:246.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 08:45 95-63-606/17/21 18:246.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 08:45 108-67-806/17/21 18:246.5 1
Vinyl acetate ND ug/kg 06/18/21 08:45 108-05-406/17/21 18:2464.5 1
Vinyl chloride ND ug/kg 06/18/21 08:45 75-01-406/17/21 18:2412.9 1
Xylene (Total)ND ug/kg 06/18/21 08:45 1330-20-706/17/21 18:2412.9 1
m&p-Xylene ND ug/kg 06/18/21 08:45 179601-23-106/17/21 18:2412.9 1
o-Xylene ND ug/kg 06/18/21 08:45 95-47-606/17/21 18:246.5 1
Surrogates
Toluene-d8 (S)103 %06/18/21 08:45 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)101 %06/18/21 08:45 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 08:45 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 8.5 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-24 Lab ID:92545088016 Collected:06/16/21 10:10 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 03:1206/21/21 09:236.3 1
Surrogates
4-Bromofluorobenzene (S)90 %06/23/21 03:12 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 09:04 67-64-106/17/21 18:241081
Benzene ND ug/kg 06/18/21 09:04 71-43-206/17/21 18:245.4 1
Bromobenzene ND ug/kg 06/18/21 09:04 108-86-106/17/21 18:245.4 1
Bromochloromethane ND ug/kg 06/18/21 09:04 74-97-506/17/21 18:245.4 1
Bromodichloromethane ND ug/kg 06/18/21 09:04 75-27-406/17/21 18:245.4 1
Bromoform ND ug/kg 06/18/21 09:04 75-25-206/17/21 18:245.4 1
Bromomethane ND ug/kg 06/18/21 09:04 74-83-9 IK,L1,v106/17/21 18:2410.8 1
2-Butanone (MEK)ND ug/kg 06/18/21 09:04 78-93-306/17/21 18:241081
n-Butylbenzene ND ug/kg 06/18/21 09:04 104-51-806/17/21 18:245.4 1
sec-Butylbenzene ND ug/kg 06/18/21 09:04 135-98-806/17/21 18:245.4 1
tert-Butylbenzene ND ug/kg 06/18/21 09:04 98-06-606/17/21 18:245.4 1
Carbon tetrachloride ND ug/kg 06/18/21 09:04 56-23-506/17/21 18:245.4 1
Chlorobenzene ND ug/kg 06/18/21 09:04 108-90-706/17/21 18:245.4 1
Chloroethane ND ug/kg 06/18/21 09:04 75-00-306/17/21 18:2410.8 1
Chloroform ND ug/kg 06/18/21 09:04 67-66-306/17/21 18:245.4 1
Chloromethane ND ug/kg 06/18/21 09:04 74-87-306/17/21 18:2410.8 1
2-Chlorotoluene ND ug/kg 06/18/21 09:04 95-49-806/17/21 18:245.4 1
4-Chlorotoluene ND ug/kg 06/18/21 09:04 106-43-406/17/21 18:245.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 09:04 96-12-806/17/21 18:245.4 1
Dibromochloromethane ND ug/kg 06/18/21 09:04 124-48-106/17/21 18:245.4 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 09:04 106-93-406/17/21 18:245.4 1
Dibromomethane ND ug/kg 06/18/21 09:04 74-95-306/17/21 18:245.4 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 09:04 95-50-106/17/21 18:245.4 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 09:04 541-73-106/17/21 18:245.4 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 09:04 106-46-706/17/21 18:245.4 1
Dichlorodifluoromethane ND ug/kg 06/18/21 09:04 75-71-806/17/21 18:2410.8 1
1,1-Dichloroethane ND ug/kg 06/18/21 09:04 75-34-306/17/21 18:245.4 1
1,2-Dichloroethane ND ug/kg 06/18/21 09:04 107-06-206/17/21 18:245.4 1
1,1-Dichloroethene ND ug/kg 06/18/21 09:04 75-35-406/17/21 18:245.4 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 09:04 156-59-206/17/21 18:245.4 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 09:04 156-60-506/17/21 18:245.4 1
1,2-Dichloropropane ND ug/kg 06/18/21 09:04 78-87-506/17/21 18:245.4 1
1,3-Dichloropropane ND ug/kg 06/18/21 09:04 142-28-906/17/21 18:245.4 1
2,2-Dichloropropane ND ug/kg 06/18/21 09:04 594-20-706/17/21 18:245.4 1
1,1-Dichloropropene ND ug/kg 06/18/21 09:04 563-58-606/17/21 18:245.4 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 09:04 10061-01-506/17/21 18:245.4 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 09:04 10061-02-606/17/21 18:245.4 1
Diisopropyl ether ND ug/kg 06/18/21 09:04 108-20-306/17/21 18:245.4 1
Ethylbenzene ND ug/kg 06/18/21 09:04 100-41-406/17/21 18:245.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-24 Lab ID:92545088016 Collected:06/16/21 10:10 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 09:04 87-68-306/17/21 18:2410.8 1
2-Hexanone ND ug/kg 06/18/21 09:04 591-78-606/17/21 18:2453.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 09:04 98-82-806/17/21 18:245.4 1
p-Isopropyltoluene ND ug/kg 06/18/21 09:04 99-87-606/17/21 18:245.4 1
Methylene Chloride ND ug/kg 06/18/21 09:04 75-09-206/17/21 18:2421.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 09:04 108-10-106/17/21 18:2453.9 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 09:04 1634-04-406/17/21 18:245.4 1
Naphthalene ND ug/kg 06/18/21 09:04 91-20-306/17/21 18:245.4 1
n-Propylbenzene ND ug/kg 06/18/21 09:04 103-65-106/17/21 18:245.4 1
Styrene ND ug/kg 06/18/21 09:04 100-42-506/17/21 18:245.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 09:04 630-20-606/17/21 18:245.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 09:04 79-34-506/17/21 18:245.4 1
Tetrachloroethene ND ug/kg 06/18/21 09:04 127-18-406/17/21 18:245.4 1
Toluene ND ug/kg 06/18/21 09:04 108-88-306/17/21 18:245.4 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 09:04 87-61-606/17/21 18:245.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 09:04 120-82-106/17/21 18:245.4 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 09:04 71-55-606/17/21 18:245.4 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 09:04 79-00-506/17/21 18:245.4 1
Trichloroethene ND ug/kg 06/18/21 09:04 79-01-606/17/21 18:245.4 1
Trichlorofluoromethane ND ug/kg 06/18/21 09:04 75-69-406/17/21 18:245.4 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 09:04 96-18-406/17/21 18:245.4 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 09:04 95-63-606/17/21 18:245.4 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 09:04 108-67-806/17/21 18:245.4 1
Vinyl acetate ND ug/kg 06/18/21 09:04 108-05-406/17/21 18:2453.9 1
Vinyl chloride ND ug/kg 06/18/21 09:04 75-01-406/17/21 18:2410.8 1
Xylene (Total)ND ug/kg 06/18/21 09:04 1330-20-706/17/21 18:2410.8 1
m&p-Xylene ND ug/kg 06/18/21 09:04 179601-23-106/17/21 18:2410.8 1
o-Xylene ND ug/kg 06/18/21 09:04 95-47-606/17/21 18:245.4 1
Surrogates
Toluene-d8 (S)103 %06/18/21 09:04 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)101 %06/18/21 09:04 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 09:04 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.7 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-25 Lab ID:92545088017 Collected:06/16/21 10:13 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 03:4106/21/21 09:237.5 1
Surrogates
4-Bromofluorobenzene (S)93 %06/23/21 03:41 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 09:22 67-64-106/17/21 18:241131
Benzene ND ug/kg 06/18/21 09:22 71-43-206/17/21 18:245.7 1
Bromobenzene ND ug/kg 06/18/21 09:22 108-86-106/17/21 18:245.7 1
Bromochloromethane ND ug/kg 06/18/21 09:22 74-97-506/17/21 18:245.7 1
Bromodichloromethane ND ug/kg 06/18/21 09:22 75-27-406/17/21 18:245.7 1
Bromoform ND ug/kg 06/18/21 09:22 75-25-206/17/21 18:245.7 1
Bromomethane ND ug/kg 06/18/21 09:22 74-83-9 IK,L1,v106/17/21 18:2411.3 1
2-Butanone (MEK)ND ug/kg 06/18/21 09:22 78-93-306/17/21 18:241131
n-Butylbenzene ND ug/kg 06/18/21 09:22 104-51-806/17/21 18:245.7 1
sec-Butylbenzene ND ug/kg 06/18/21 09:22 135-98-806/17/21 18:245.7 1
tert-Butylbenzene ND ug/kg 06/18/21 09:22 98-06-606/17/21 18:245.7 1
Carbon tetrachloride ND ug/kg 06/18/21 09:22 56-23-506/17/21 18:245.7 1
Chlorobenzene ND ug/kg 06/18/21 09:22 108-90-706/17/21 18:245.7 1
Chloroethane ND ug/kg 06/18/21 09:22 75-00-306/17/21 18:2411.3 1
Chloroform ND ug/kg 06/18/21 09:22 67-66-306/17/21 18:245.7 1
Chloromethane ND ug/kg 06/18/21 09:22 74-87-306/17/21 18:2411.3 1
2-Chlorotoluene ND ug/kg 06/18/21 09:22 95-49-806/17/21 18:245.7 1
4-Chlorotoluene ND ug/kg 06/18/21 09:22 106-43-406/17/21 18:245.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 09:22 96-12-806/17/21 18:245.7 1
Dibromochloromethane ND ug/kg 06/18/21 09:22 124-48-106/17/21 18:245.7 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 09:22 106-93-406/17/21 18:245.7 1
Dibromomethane ND ug/kg 06/18/21 09:22 74-95-306/17/21 18:245.7 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 09:22 95-50-106/17/21 18:245.7 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 09:22 541-73-106/17/21 18:245.7 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 09:22 106-46-706/17/21 18:245.7 1
Dichlorodifluoromethane ND ug/kg 06/18/21 09:22 75-71-806/17/21 18:2411.3 1
1,1-Dichloroethane ND ug/kg 06/18/21 09:22 75-34-306/17/21 18:245.7 1
1,2-Dichloroethane ND ug/kg 06/18/21 09:22 107-06-206/17/21 18:245.7 1
1,1-Dichloroethene ND ug/kg 06/18/21 09:22 75-35-406/17/21 18:245.7 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 09:22 156-59-206/17/21 18:245.7 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 09:22 156-60-506/17/21 18:245.7 1
1,2-Dichloropropane ND ug/kg 06/18/21 09:22 78-87-506/17/21 18:245.7 1
1,3-Dichloropropane ND ug/kg 06/18/21 09:22 142-28-906/17/21 18:245.7 1
2,2-Dichloropropane ND ug/kg 06/18/21 09:22 594-20-706/17/21 18:245.7 1
1,1-Dichloropropene ND ug/kg 06/18/21 09:22 563-58-606/17/21 18:245.7 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 09:22 10061-01-506/17/21 18:245.7 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 09:22 10061-02-606/17/21 18:245.7 1
Diisopropyl ether ND ug/kg 06/18/21 09:22 108-20-306/17/21 18:245.7 1
Ethylbenzene ND ug/kg 06/18/21 09:22 100-41-406/17/21 18:245.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-25 Lab ID:92545088017 Collected:06/16/21 10:13 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 09:22 87-68-306/17/21 18:2411.3 1
2-Hexanone ND ug/kg 06/18/21 09:22 591-78-606/17/21 18:2456.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 09:22 98-82-806/17/21 18:245.7 1
p-Isopropyltoluene ND ug/kg 06/18/21 09:22 99-87-606/17/21 18:245.7 1
Methylene Chloride ND ug/kg 06/18/21 09:22 75-09-206/17/21 18:2422.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 09:22 108-10-106/17/21 18:2456.5 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 09:22 1634-04-406/17/21 18:245.7 1
Naphthalene ND ug/kg 06/18/21 09:22 91-20-306/17/21 18:245.7 1
n-Propylbenzene ND ug/kg 06/18/21 09:22 103-65-106/17/21 18:245.7 1
Styrene ND ug/kg 06/18/21 09:22 100-42-506/17/21 18:245.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 09:22 630-20-606/17/21 18:245.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 09:22 79-34-506/17/21 18:245.7 1
Tetrachloroethene ND ug/kg 06/18/21 09:22 127-18-406/17/21 18:245.7 1
Toluene ND ug/kg 06/18/21 09:22 108-88-306/17/21 18:245.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 09:22 87-61-606/17/21 18:245.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 09:22 120-82-106/17/21 18:245.7 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 09:22 71-55-606/17/21 18:245.7 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 09:22 79-00-506/17/21 18:245.7 1
Trichloroethene ND ug/kg 06/18/21 09:22 79-01-606/17/21 18:245.7 1
Trichlorofluoromethane ND ug/kg 06/18/21 09:22 75-69-406/17/21 18:245.7 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 09:22 96-18-406/17/21 18:245.7 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 09:22 95-63-606/17/21 18:245.7 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 09:22 108-67-806/17/21 18:245.7 1
Vinyl acetate ND ug/kg 06/18/21 09:22 108-05-406/17/21 18:2456.5 1
Vinyl chloride ND ug/kg 06/18/21 09:22 75-01-406/17/21 18:2411.3 1
Xylene (Total)ND ug/kg 06/18/21 09:22 1330-20-706/17/21 18:2411.3 1
m&p-Xylene ND ug/kg 06/18/21 09:22 179601-23-106/17/21 18:2411.3 1
o-Xylene ND ug/kg 06/18/21 09:22 95-47-606/17/21 18:245.7 1
Surrogates
Toluene-d8 (S)102 %06/18/21 09:22 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)102 %06/18/21 09:22 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 09:22 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.1 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-26 Lab ID:92545088018 Collected:06/16/21 10:15 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 04:0906/21/21 09:238.0 1
Surrogates
4-Bromofluorobenzene (S)93 %06/23/21 04:09 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 09:40 67-64-106/17/21 18:241071
Benzene ND ug/kg 06/18/21 09:40 71-43-206/17/21 18:245.3 1
Bromobenzene ND ug/kg 06/18/21 09:40 108-86-106/17/21 18:245.3 1
Bromochloromethane ND ug/kg 06/18/21 09:40 74-97-506/17/21 18:245.3 1
Bromodichloromethane ND ug/kg 06/18/21 09:40 75-27-406/17/21 18:245.3 1
Bromoform ND ug/kg 06/18/21 09:40 75-25-206/17/21 18:245.3 1
Bromomethane ND ug/kg 06/18/21 09:40 74-83-9 IK,L1,v106/17/21 18:2410.7 1
2-Butanone (MEK)ND ug/kg 06/18/21 09:40 78-93-306/17/21 18:241071
n-Butylbenzene ND ug/kg 06/18/21 09:40 104-51-806/17/21 18:245.3 1
sec-Butylbenzene ND ug/kg 06/18/21 09:40 135-98-806/17/21 18:245.3 1
tert-Butylbenzene ND ug/kg 06/18/21 09:40 98-06-606/17/21 18:245.3 1
Carbon tetrachloride ND ug/kg 06/18/21 09:40 56-23-506/17/21 18:245.3 1
Chlorobenzene ND ug/kg 06/18/21 09:40 108-90-706/17/21 18:245.3 1
Chloroethane ND ug/kg 06/18/21 09:40 75-00-306/17/21 18:2410.7 1
Chloroform ND ug/kg 06/18/21 09:40 67-66-306/17/21 18:245.3 1
Chloromethane ND ug/kg 06/18/21 09:40 74-87-306/17/21 18:2410.7 1
2-Chlorotoluene ND ug/kg 06/18/21 09:40 95-49-806/17/21 18:245.3 1
4-Chlorotoluene ND ug/kg 06/18/21 09:40 106-43-406/17/21 18:245.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 09:40 96-12-806/17/21 18:245.3 1
Dibromochloromethane ND ug/kg 06/18/21 09:40 124-48-106/17/21 18:245.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 09:40 106-93-406/17/21 18:245.3 1
Dibromomethane ND ug/kg 06/18/21 09:40 74-95-306/17/21 18:245.3 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 09:40 95-50-106/17/21 18:245.3 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 09:40 541-73-106/17/21 18:245.3 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 09:40 106-46-706/17/21 18:245.3 1
Dichlorodifluoromethane ND ug/kg 06/18/21 09:40 75-71-806/17/21 18:2410.7 1
1,1-Dichloroethane ND ug/kg 06/18/21 09:40 75-34-306/17/21 18:245.3 1
1,2-Dichloroethane ND ug/kg 06/18/21 09:40 107-06-206/17/21 18:245.3 1
1,1-Dichloroethene ND ug/kg 06/18/21 09:40 75-35-406/17/21 18:245.3 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 09:40 156-59-206/17/21 18:245.3 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 09:40 156-60-506/17/21 18:245.3 1
1,2-Dichloropropane ND ug/kg 06/18/21 09:40 78-87-506/17/21 18:245.3 1
1,3-Dichloropropane ND ug/kg 06/18/21 09:40 142-28-906/17/21 18:245.3 1
2,2-Dichloropropane ND ug/kg 06/18/21 09:40 594-20-706/17/21 18:245.3 1
1,1-Dichloropropene ND ug/kg 06/18/21 09:40 563-58-606/17/21 18:245.3 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 09:40 10061-01-506/17/21 18:245.3 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 09:40 10061-02-606/17/21 18:245.3 1
Diisopropyl ether ND ug/kg 06/18/21 09:40 108-20-306/17/21 18:245.3 1
Ethylbenzene ND ug/kg 06/18/21 09:40 100-41-406/17/21 18:245.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-26 Lab ID:92545088018 Collected:06/16/21 10:15 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 09:40 87-68-306/17/21 18:2410.7 1
2-Hexanone ND ug/kg 06/18/21 09:40 591-78-606/17/21 18:2453.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 09:40 98-82-806/17/21 18:245.3 1
p-Isopropyltoluene ND ug/kg 06/18/21 09:40 99-87-606/17/21 18:245.3 1
Methylene Chloride ND ug/kg 06/18/21 09:40 75-09-206/17/21 18:2421.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 09:40 108-10-106/17/21 18:2453.5 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 09:40 1634-04-406/17/21 18:245.3 1
Naphthalene ND ug/kg 06/18/21 09:40 91-20-306/17/21 18:245.3 1
n-Propylbenzene ND ug/kg 06/18/21 09:40 103-65-106/17/21 18:245.3 1
Styrene ND ug/kg 06/18/21 09:40 100-42-506/17/21 18:245.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 09:40 630-20-606/17/21 18:245.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 09:40 79-34-506/17/21 18:245.3 1
Tetrachloroethene ND ug/kg 06/18/21 09:40 127-18-406/17/21 18:245.3 1
Toluene ND ug/kg 06/18/21 09:40 108-88-306/17/21 18:245.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 09:40 87-61-606/17/21 18:245.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 09:40 120-82-106/17/21 18:245.3 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 09:40 71-55-606/17/21 18:245.3 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 09:40 79-00-506/17/21 18:245.3 1
Trichloroethene ND ug/kg 06/18/21 09:40 79-01-606/17/21 18:245.3 1
Trichlorofluoromethane ND ug/kg 06/18/21 09:40 75-69-406/17/21 18:245.3 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 09:40 96-18-406/17/21 18:245.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 09:40 95-63-606/17/21 18:245.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 09:40 108-67-806/17/21 18:245.3 1
Vinyl acetate ND ug/kg 06/18/21 09:40 108-05-406/17/21 18:2453.5 1
Vinyl chloride ND ug/kg 06/18/21 09:40 75-01-406/17/21 18:2410.7 1
Xylene (Total)ND ug/kg 06/18/21 09:40 1330-20-706/17/21 18:2410.7 1
m&p-Xylene ND ug/kg 06/18/21 09:40 179601-23-106/17/21 18:2410.7 1
o-Xylene 5.5 ug/kg 06/18/21 09:40 95-47-606/17/21 18:245.3 1
Surrogates
Toluene-d8 (S)102 %06/18/21 09:40 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)103 %06/18/21 09:40 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)114 %06/18/21 09:40 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-27 Lab ID:92545088019 Collected:06/16/21 10:20 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 04:3706/21/21 09:236.4 1
Surrogates
4-Bromofluorobenzene (S)91 %06/23/21 04:37 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 09:58 67-64-106/17/21 18:241151
Benzene ND ug/kg 06/18/21 09:58 71-43-206/17/21 18:245.8 1
Bromobenzene ND ug/kg 06/18/21 09:58 108-86-106/17/21 18:245.8 1
Bromochloromethane ND ug/kg 06/18/21 09:58 74-97-506/17/21 18:245.8 1
Bromodichloromethane ND ug/kg 06/18/21 09:58 75-27-406/17/21 18:245.8 1
Bromoform ND ug/kg 06/18/21 09:58 75-25-206/17/21 18:245.8 1
Bromomethane ND ug/kg 06/18/21 09:58 74-83-9 IK,L1,v106/17/21 18:2411.5 1
2-Butanone (MEK)ND ug/kg 06/18/21 09:58 78-93-306/17/21 18:241151
n-Butylbenzene ND ug/kg 06/18/21 09:58 104-51-806/17/21 18:245.8 1
sec-Butylbenzene ND ug/kg 06/18/21 09:58 135-98-806/17/21 18:245.8 1
tert-Butylbenzene ND ug/kg 06/18/21 09:58 98-06-606/17/21 18:245.8 1
Carbon tetrachloride ND ug/kg 06/18/21 09:58 56-23-506/17/21 18:245.8 1
Chlorobenzene ND ug/kg 06/18/21 09:58 108-90-706/17/21 18:245.8 1
Chloroethane ND ug/kg 06/18/21 09:58 75-00-306/17/21 18:2411.5 1
Chloroform ND ug/kg 06/18/21 09:58 67-66-306/17/21 18:245.8 1
Chloromethane ND ug/kg 06/18/21 09:58 74-87-306/17/21 18:2411.5 1
2-Chlorotoluene ND ug/kg 06/18/21 09:58 95-49-806/17/21 18:245.8 1
4-Chlorotoluene ND ug/kg 06/18/21 09:58 106-43-406/17/21 18:245.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 09:58 96-12-806/17/21 18:245.8 1
Dibromochloromethane ND ug/kg 06/18/21 09:58 124-48-106/17/21 18:245.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 09:58 106-93-406/17/21 18:245.8 1
Dibromomethane ND ug/kg 06/18/21 09:58 74-95-306/17/21 18:245.8 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 09:58 95-50-106/17/21 18:245.8 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 09:58 541-73-106/17/21 18:245.8 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 09:58 106-46-706/17/21 18:245.8 1
Dichlorodifluoromethane ND ug/kg 06/18/21 09:58 75-71-806/17/21 18:2411.5 1
1,1-Dichloroethane ND ug/kg 06/18/21 09:58 75-34-306/17/21 18:245.8 1
1,2-Dichloroethane ND ug/kg 06/18/21 09:58 107-06-206/17/21 18:245.8 1
1,1-Dichloroethene ND ug/kg 06/18/21 09:58 75-35-406/17/21 18:245.8 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 09:58 156-59-206/17/21 18:245.8 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 09:58 156-60-506/17/21 18:245.8 1
1,2-Dichloropropane ND ug/kg 06/18/21 09:58 78-87-506/17/21 18:245.8 1
1,3-Dichloropropane ND ug/kg 06/18/21 09:58 142-28-906/17/21 18:245.8 1
2,2-Dichloropropane ND ug/kg 06/18/21 09:58 594-20-706/17/21 18:245.8 1
1,1-Dichloropropene ND ug/kg 06/18/21 09:58 563-58-606/17/21 18:245.8 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 09:58 10061-01-506/17/21 18:245.8 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 09:58 10061-02-606/17/21 18:245.8 1
Diisopropyl ether ND ug/kg 06/18/21 09:58 108-20-306/17/21 18:245.8 1
Ethylbenzene ND ug/kg 06/18/21 09:58 100-41-406/17/21 18:245.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-27 Lab ID:92545088019 Collected:06/16/21 10:20 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 09:58 87-68-306/17/21 18:2411.5 1
2-Hexanone ND ug/kg 06/18/21 09:58 591-78-606/17/21 18:2457.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 09:58 98-82-806/17/21 18:245.8 1
p-Isopropyltoluene ND ug/kg 06/18/21 09:58 99-87-606/17/21 18:245.8 1
Methylene Chloride ND ug/kg 06/18/21 09:58 75-09-206/17/21 18:2423.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 09:58 108-10-106/17/21 18:2457.6 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 09:58 1634-04-406/17/21 18:245.8 1
Naphthalene ND ug/kg 06/18/21 09:58 91-20-306/17/21 18:245.8 1
n-Propylbenzene ND ug/kg 06/18/21 09:58 103-65-106/17/21 18:245.8 1
Styrene ND ug/kg 06/18/21 09:58 100-42-506/17/21 18:245.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 09:58 630-20-606/17/21 18:245.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 09:58 79-34-506/17/21 18:245.8 1
Tetrachloroethene ND ug/kg 06/18/21 09:58 127-18-406/17/21 18:245.8 1
Toluene ND ug/kg 06/18/21 09:58 108-88-306/17/21 18:245.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 09:58 87-61-606/17/21 18:245.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 09:58 120-82-106/17/21 18:245.8 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 09:58 71-55-606/17/21 18:245.8 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 09:58 79-00-506/17/21 18:245.8 1
Trichloroethene ND ug/kg 06/18/21 09:58 79-01-606/17/21 18:245.8 1
Trichlorofluoromethane ND ug/kg 06/18/21 09:58 75-69-406/17/21 18:245.8 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 09:58 96-18-406/17/21 18:245.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 09:58 95-63-606/17/21 18:245.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 09:58 108-67-806/17/21 18:245.8 1
Vinyl acetate ND ug/kg 06/18/21 09:58 108-05-406/17/21 18:2457.6 1
Vinyl chloride ND ug/kg 06/18/21 09:58 75-01-406/17/21 18:2411.5 1
Xylene (Total)ND ug/kg 06/18/21 09:58 1330-20-706/17/21 18:2411.5 1
m&p-Xylene ND ug/kg 06/18/21 09:58 179601-23-106/17/21 18:2411.5 1
o-Xylene ND ug/kg 06/18/21 09:58 95-47-606/17/21 18:245.8 1
Surrogates
Toluene-d8 (S)103 %06/18/21 09:58 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)102 %06/18/21 09:58 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)117 %06/18/21 09:58 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 8.3 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-28 Lab ID:92545088020 Collected:06/16/21 10:22 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 05:0506/21/21 09:236.3 1
Surrogates
4-Bromofluorobenzene (S)89 %06/23/21 05:05 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 10:16 67-64-106/17/21 18:241071
Benzene ND ug/kg 06/18/21 10:16 71-43-206/17/21 18:245.3 1
Bromobenzene ND ug/kg 06/18/21 10:16 108-86-106/17/21 18:245.3 1
Bromochloromethane ND ug/kg 06/18/21 10:16 74-97-506/17/21 18:245.3 1
Bromodichloromethane ND ug/kg 06/18/21 10:16 75-27-406/17/21 18:245.3 1
Bromoform ND ug/kg 06/18/21 10:16 75-25-206/17/21 18:245.3 1
Bromomethane ND ug/kg 06/18/21 10:16 74-83-9 IK,L1,v106/17/21 18:2410.7 1
2-Butanone (MEK)ND ug/kg 06/18/21 10:16 78-93-306/17/21 18:241071
n-Butylbenzene ND ug/kg 06/18/21 10:16 104-51-806/17/21 18:245.3 1
sec-Butylbenzene ND ug/kg 06/18/21 10:16 135-98-806/17/21 18:245.3 1
tert-Butylbenzene ND ug/kg 06/18/21 10:16 98-06-606/17/21 18:245.3 1
Carbon tetrachloride ND ug/kg 06/18/21 10:16 56-23-506/17/21 18:245.3 1
Chlorobenzene ND ug/kg 06/18/21 10:16 108-90-706/17/21 18:245.3 1
Chloroethane ND ug/kg 06/18/21 10:16 75-00-306/17/21 18:2410.7 1
Chloroform ND ug/kg 06/18/21 10:16 67-66-306/17/21 18:245.3 1
Chloromethane ND ug/kg 06/18/21 10:16 74-87-306/17/21 18:2410.7 1
2-Chlorotoluene ND ug/kg 06/18/21 10:16 95-49-806/17/21 18:245.3 1
4-Chlorotoluene ND ug/kg 06/18/21 10:16 106-43-406/17/21 18:245.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 10:16 96-12-806/17/21 18:245.3 1
Dibromochloromethane ND ug/kg 06/18/21 10:16 124-48-106/17/21 18:245.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 10:16 106-93-406/17/21 18:245.3 1
Dibromomethane ND ug/kg 06/18/21 10:16 74-95-306/17/21 18:245.3 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 10:16 95-50-106/17/21 18:245.3 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 10:16 541-73-106/17/21 18:245.3 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 10:16 106-46-706/17/21 18:245.3 1
Dichlorodifluoromethane ND ug/kg 06/18/21 10:16 75-71-806/17/21 18:2410.7 1
1,1-Dichloroethane ND ug/kg 06/18/21 10:16 75-34-306/17/21 18:245.3 1
1,2-Dichloroethane ND ug/kg 06/18/21 10:16 107-06-206/17/21 18:245.3 1
1,1-Dichloroethene ND ug/kg 06/18/21 10:16 75-35-406/17/21 18:245.3 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 10:16 156-59-206/17/21 18:245.3 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 10:16 156-60-506/17/21 18:245.3 1
1,2-Dichloropropane ND ug/kg 06/18/21 10:16 78-87-506/17/21 18:245.3 1
1,3-Dichloropropane ND ug/kg 06/18/21 10:16 142-28-906/17/21 18:245.3 1
2,2-Dichloropropane ND ug/kg 06/18/21 10:16 594-20-706/17/21 18:245.3 1
1,1-Dichloropropene ND ug/kg 06/18/21 10:16 563-58-606/17/21 18:245.3 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 10:16 10061-01-506/17/21 18:245.3 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 10:16 10061-02-606/17/21 18:245.3 1
Diisopropyl ether ND ug/kg 06/18/21 10:16 108-20-306/17/21 18:245.3 1
Ethylbenzene ND ug/kg 06/18/21 10:16 100-41-406/17/21 18:245.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-28 Lab ID:92545088020 Collected:06/16/21 10:22 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 10:16 87-68-306/17/21 18:2410.7 1
2-Hexanone ND ug/kg 06/18/21 10:16 591-78-606/17/21 18:2453.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 10:16 98-82-806/17/21 18:245.3 1
p-Isopropyltoluene ND ug/kg 06/18/21 10:16 99-87-606/17/21 18:245.3 1
Methylene Chloride ND ug/kg 06/18/21 10:16 75-09-206/17/21 18:2421.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 10:16 108-10-106/17/21 18:2453.3 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 10:16 1634-04-406/17/21 18:245.3 1
Naphthalene ND ug/kg 06/18/21 10:16 91-20-306/17/21 18:245.3 1
n-Propylbenzene ND ug/kg 06/18/21 10:16 103-65-106/17/21 18:245.3 1
Styrene ND ug/kg 06/18/21 10:16 100-42-506/17/21 18:245.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 10:16 630-20-606/17/21 18:245.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 10:16 79-34-506/17/21 18:245.3 1
Tetrachloroethene ND ug/kg 06/18/21 10:16 127-18-406/17/21 18:245.3 1
Toluene ND ug/kg 06/18/21 10:16 108-88-306/17/21 18:245.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 10:16 87-61-606/17/21 18:245.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 10:16 120-82-106/17/21 18:245.3 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 10:16 71-55-606/17/21 18:245.3 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 10:16 79-00-506/17/21 18:245.3 1
Trichloroethene ND ug/kg 06/18/21 10:16 79-01-606/17/21 18:245.3 1
Trichlorofluoromethane ND ug/kg 06/18/21 10:16 75-69-406/17/21 18:245.3 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 10:16 96-18-406/17/21 18:245.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 10:16 95-63-606/17/21 18:245.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 10:16 108-67-806/17/21 18:245.3 1
Vinyl acetate ND ug/kg 06/18/21 10:16 108-05-406/17/21 18:2453.3 1
Vinyl chloride ND ug/kg 06/18/21 10:16 75-01-406/17/21 18:2410.7 1
Xylene (Total)ND ug/kg 06/18/21 10:16 1330-20-706/17/21 18:2410.7 1
m&p-Xylene ND ug/kg 06/18/21 10:16 179601-23-106/17/21 18:2410.7 1
o-Xylene ND ug/kg 06/18/21 10:16 95-47-606/17/21 18:245.3 1
Surrogates
Toluene-d8 (S)102 %06/18/21 10:16 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)100 %06/18/21 10:16 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 10:16 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.8 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-29 Lab ID:92545088021 Collected:06/16/21 10:25 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 05:3306/21/21 09:236.9 1
Surrogates
4-Bromofluorobenzene (S)93 %06/23/21 05:33 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/18/21 10:34 67-64-106/17/21 18:241111
Benzene ND ug/kg 06/18/21 10:34 71-43-206/17/21 18:245.5 1
Bromobenzene ND ug/kg 06/18/21 10:34 108-86-106/17/21 18:245.5 1
Bromochloromethane ND ug/kg 06/18/21 10:34 74-97-506/17/21 18:245.5 1
Bromodichloromethane ND ug/kg 06/18/21 10:34 75-27-406/17/21 18:245.5 1
Bromoform ND ug/kg 06/18/21 10:34 75-25-206/17/21 18:245.5 1
Bromomethane ND ug/kg 06/18/21 10:34 74-83-9 IK,L1,v106/17/21 18:2411.1 1
2-Butanone (MEK)ND ug/kg 06/18/21 10:34 78-93-306/17/21 18:241111
n-Butylbenzene ND ug/kg 06/18/21 10:34 104-51-806/17/21 18:245.5 1
sec-Butylbenzene ND ug/kg 06/18/21 10:34 135-98-806/17/21 18:245.5 1
tert-Butylbenzene ND ug/kg 06/18/21 10:34 98-06-606/17/21 18:245.5 1
Carbon tetrachloride ND ug/kg 06/18/21 10:34 56-23-506/17/21 18:245.5 1
Chlorobenzene ND ug/kg 06/18/21 10:34 108-90-706/17/21 18:245.5 1
Chloroethane ND ug/kg 06/18/21 10:34 75-00-306/17/21 18:2411.1 1
Chloroform ND ug/kg 06/18/21 10:34 67-66-306/17/21 18:245.5 1
Chloromethane ND ug/kg 06/18/21 10:34 74-87-306/17/21 18:2411.1 1
2-Chlorotoluene ND ug/kg 06/18/21 10:34 95-49-806/17/21 18:245.5 1
4-Chlorotoluene ND ug/kg 06/18/21 10:34 106-43-406/17/21 18:245.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/18/21 10:34 96-12-806/17/21 18:245.5 1
Dibromochloromethane ND ug/kg 06/18/21 10:34 124-48-106/17/21 18:245.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/18/21 10:34 106-93-406/17/21 18:245.5 1
Dibromomethane ND ug/kg 06/18/21 10:34 74-95-306/17/21 18:245.5 1
1,2-Dichlorobenzene ND ug/kg 06/18/21 10:34 95-50-106/17/21 18:245.5 1
1,3-Dichlorobenzene ND ug/kg 06/18/21 10:34 541-73-106/17/21 18:245.5 1
1,4-Dichlorobenzene ND ug/kg 06/18/21 10:34 106-46-706/17/21 18:245.5 1
Dichlorodifluoromethane ND ug/kg 06/18/21 10:34 75-71-806/17/21 18:2411.1 1
1,1-Dichloroethane ND ug/kg 06/18/21 10:34 75-34-306/17/21 18:245.5 1
1,2-Dichloroethane ND ug/kg 06/18/21 10:34 107-06-206/17/21 18:245.5 1
1,1-Dichloroethene ND ug/kg 06/18/21 10:34 75-35-406/17/21 18:245.5 1
cis-1,2-Dichloroethene ND ug/kg 06/18/21 10:34 156-59-206/17/21 18:245.5 1
trans-1,2-Dichloroethene ND ug/kg 06/18/21 10:34 156-60-506/17/21 18:245.5 1
1,2-Dichloropropane ND ug/kg 06/18/21 10:34 78-87-506/17/21 18:245.5 1
1,3-Dichloropropane ND ug/kg 06/18/21 10:34 142-28-906/17/21 18:245.5 1
2,2-Dichloropropane ND ug/kg 06/18/21 10:34 594-20-706/17/21 18:245.5 1
1,1-Dichloropropene ND ug/kg 06/18/21 10:34 563-58-606/17/21 18:245.5 1
cis-1,3-Dichloropropene ND ug/kg 06/18/21 10:34 10061-01-506/17/21 18:245.5 1
trans-1,3-Dichloropropene ND ug/kg 06/18/21 10:34 10061-02-606/17/21 18:245.5 1
Diisopropyl ether ND ug/kg 06/18/21 10:34 108-20-306/17/21 18:245.5 1
Ethylbenzene ND ug/kg 06/18/21 10:34 100-41-406/17/21 18:245.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Sample:SS-29 Lab ID:92545088021 Collected:06/16/21 10:25 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/18/21 10:34 87-68-306/17/21 18:2411.1 1
2-Hexanone ND ug/kg 06/18/21 10:34 591-78-606/17/21 18:2455.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/18/21 10:34 98-82-806/17/21 18:245.5 1
p-Isopropyltoluene ND ug/kg 06/18/21 10:34 99-87-606/17/21 18:245.5 1
Methylene Chloride ND ug/kg 06/18/21 10:34 75-09-206/17/21 18:2422.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/18/21 10:34 108-10-106/17/21 18:2455.4 1
Methyl-tert-butyl ether ND ug/kg 06/18/21 10:34 1634-04-406/17/21 18:245.5 1
Naphthalene ND ug/kg 06/18/21 10:34 91-20-306/17/21 18:245.5 1
n-Propylbenzene ND ug/kg 06/18/21 10:34 103-65-106/17/21 18:245.5 1
Styrene ND ug/kg 06/18/21 10:34 100-42-506/17/21 18:245.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/18/21 10:34 630-20-606/17/21 18:245.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/18/21 10:34 79-34-506/17/21 18:245.5 1
Tetrachloroethene ND ug/kg 06/18/21 10:34 127-18-406/17/21 18:245.5 1
Toluene ND ug/kg 06/18/21 10:34 108-88-306/17/21 18:245.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/18/21 10:34 87-61-606/17/21 18:245.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/18/21 10:34 120-82-106/17/21 18:245.5 1
1,1,1-Trichloroethane ND ug/kg 06/18/21 10:34 71-55-606/17/21 18:245.5 1
1,1,2-Trichloroethane ND ug/kg 06/18/21 10:34 79-00-506/17/21 18:245.5 1
Trichloroethene ND ug/kg 06/18/21 10:34 79-01-606/17/21 18:245.5 1
Trichlorofluoromethane ND ug/kg 06/18/21 10:34 75-69-406/17/21 18:245.5 1
1,2,3-Trichloropropane ND ug/kg 06/18/21 10:34 96-18-406/17/21 18:245.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/18/21 10:34 95-63-606/17/21 18:245.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/18/21 10:34 108-67-806/17/21 18:245.5 1
Vinyl acetate ND ug/kg 06/18/21 10:34 108-05-406/17/21 18:2455.4 1
Vinyl chloride ND ug/kg 06/18/21 10:34 75-01-406/17/21 18:2411.1 1
Xylene (Total)ND ug/kg 06/18/21 10:34 1330-20-706/17/21 18:2411.1 1
m&p-Xylene ND ug/kg 06/18/21 10:34 179601-23-106/17/21 18:2411.1 1
o-Xylene ND ug/kg 06/18/21 10:34 95-47-606/17/21 18:245.5 1
Surrogates
Toluene-d8 (S)103 %06/18/21 10:34 2037-26-506/17/21 18:2470-130 1
4-Bromofluorobenzene (S)103 %06/18/21 10:34 460-00-406/17/21 18:2469-134 1
1,2-Dichloroethane-d4 (S)115 %06/18/21 10:34 17060-07-006/17/21 18:2470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.0 %06/18/21 15:43 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628176
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088001, 92545088002, 92545088003, 92545088004, 92545088005, 92545088006, 92545088008,
92545088009, 92545088010, 92545088011, 92545088012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3302237
Associated Lab Samples:92545088001, 92545088002, 92545088003, 92545088004, 92545088005, 92545088006, 92545088008,
92545088009, 92545088010, 92545088011, 92545088012
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/19/21 15:33
4-Bromofluorobenzene (S)%90 66-131 06/19/21 15:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3302238LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 48.650.4 96 70-130
4-Bromofluorobenzene (S)%94 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3302240MATRIX SPIKE SAMPLE:
MSSpike
Result
92544881001
Gas Range Organics (C6-C10)mg/kg 67.673.5 92 70-145ND
4-Bromofluorobenzene (S)%95 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92544791005
3302239SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg 2.5JND
4-Bromofluorobenzene (S)%9696
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628394
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088007, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3303213
Associated Lab Samples:92545088007, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/22/21 15:29
4-Bromofluorobenzene (S)%99 66-131 06/22/21 15:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3303214LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 45.150 90 70-130
4-Bromofluorobenzene (S)%95 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3303216MATRIX SPIKE SAMPLE:
MSSpike
Result
92545021003
Gas Range Organics (C6-C10)mg/kg 63.265.2 97 70-145ND
4-Bromofluorobenzene (S)%105 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92545021002
3303215SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9598
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628013
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088007, 92545088008, 92545088009, 92545088010, 92545088011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301644
Associated Lab Samples:92545088007, 92545088008, 92545088009, 92545088010, 92545088011
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/18/21 03:42
1,1,1-Trichloroethane ug/kg ND 5.0 06/18/21 03:42
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/18/21 03:42
1,1,2-Trichloroethane ug/kg ND 5.0 06/18/21 03:42
1,1-Dichloroethane ug/kg ND 5.0 06/18/21 03:42
1,1-Dichloroethene ug/kg ND 5.0 06/18/21 03:42
1,1-Dichloropropene ug/kg ND 5.0 06/18/21 03:42
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/18/21 03:42
1,2,3-Trichloropropane ug/kg ND 5.0 06/18/21 03:42
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/18/21 03:42
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/18/21 03:42
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/18/21 03:42
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/18/21 03:42
1,2-Dichlorobenzene ug/kg ND 5.0 06/18/21 03:42
1,2-Dichloroethane ug/kg ND 5.0 06/18/21 03:42
1,2-Dichloropropane ug/kg ND 5.0 06/18/21 03:42
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/18/21 03:42
1,3-Dichlorobenzene ug/kg ND 5.0 06/18/21 03:42
1,3-Dichloropropane ug/kg ND 5.0 06/18/21 03:42
1,4-Dichlorobenzene ug/kg ND 5.0 06/18/21 03:42
2,2-Dichloropropane ug/kg ND 5.0 06/18/21 03:42
2-Butanone (MEK)ug/kg ND 100 06/18/21 03:42
2-Chlorotoluene ug/kg ND 5.0 06/18/21 03:42
2-Hexanone ug/kg ND 50.0 06/18/21 03:42
4-Chlorotoluene ug/kg ND 5.0 06/18/21 03:42
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/18/21 03:42
Acetone ug/kg ND 100 06/18/21 03:42
Benzene ug/kg ND 5.0 06/18/21 03:42
Bromobenzene ug/kg ND 5.0 06/18/21 03:42
Bromochloromethane ug/kg ND 5.0 06/18/21 03:42
Bromodichloromethane ug/kg ND 5.0 06/18/21 03:42
Bromoform ug/kg ND 5.0 06/18/21 03:42
Bromomethane ug/kg ND 10.0 IK,v106/18/21 03:42
Carbon tetrachloride ug/kg ND 5.0 06/18/21 03:42
Chlorobenzene ug/kg ND 5.0 06/18/21 03:42
Chloroethane ug/kg ND 10.0 06/18/21 03:42
Chloroform ug/kg ND 5.0 06/18/21 03:42
Chloromethane ug/kg ND 10.0 06/18/21 03:42
cis-1,2-Dichloroethene ug/kg ND 5.0 06/18/21 03:42
cis-1,3-Dichloropropene ug/kg ND 5.0 06/18/21 03:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301644
Associated Lab Samples:92545088007, 92545088008, 92545088009, 92545088010, 92545088011
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/18/21 03:42
Dibromomethane ug/kg ND 5.0 06/18/21 03:42
Dichlorodifluoromethane ug/kg ND 10.0 06/18/21 03:42
Diisopropyl ether ug/kg ND 5.0 06/18/21 03:42
Ethylbenzene ug/kg ND 5.0 06/18/21 03:42
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/18/21 03:42
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/18/21 03:42
m&p-Xylene ug/kg ND 10.0 06/18/21 03:42
Methyl-tert-butyl ether ug/kg ND 5.0 06/18/21 03:42
Methylene Chloride ug/kg ND 20.0 06/18/21 03:42
n-Butylbenzene ug/kg ND 5.0 06/18/21 03:42
n-Propylbenzene ug/kg ND 5.0 06/18/21 03:42
Naphthalene ug/kg ND 5.0 06/18/21 03:42
o-Xylene ug/kg ND 5.0 06/18/21 03:42
p-Isopropyltoluene ug/kg ND 5.0 06/18/21 03:42
sec-Butylbenzene ug/kg ND 5.0 06/18/21 03:42
Styrene ug/kg ND 5.0 06/18/21 03:42
tert-Butylbenzene ug/kg ND 5.0 v206/18/21 03:42
Tetrachloroethene ug/kg ND 5.0 06/18/21 03:42
Toluene ug/kg ND 5.0 06/18/21 03:42
trans-1,2-Dichloroethene ug/kg ND 5.0 06/18/21 03:42
trans-1,3-Dichloropropene ug/kg ND 5.0 06/18/21 03:42
Trichloroethene ug/kg ND 5.0 06/18/21 03:42
Trichlorofluoromethane ug/kg ND 5.0 06/18/21 03:42
Vinyl acetate ug/kg ND 50.0 06/18/21 03:42
Vinyl chloride ug/kg ND 10.0 06/18/21 03:42
Xylene (Total)ug/kg ND 10.0 06/18/21 03:42
1,2-Dichloroethane-d4 (S)%105 70-130 06/18/21 03:42
4-Bromofluorobenzene (S)%94 69-134 06/18/21 03:42
Toluene-d8 (S)%101 70-130 06/18/21 03:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301645LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12101250 97 70-130
1,1,1-Trichloroethane ug/kg 11301250 90 70-130
1,1,2,2-Tetrachloroethane ug/kg 12001250 96 70-130
1,1,2-Trichloroethane ug/kg 11901250 95 70-130
1,1-Dichloroethane ug/kg 13701250 109 70-130
1,1-Dichloroethene ug/kg 13801250 110 70-130
1,1-Dichloropropene ug/kg 12801250 102 70-130
1,2,3-Trichlorobenzene ug/kg 11401250 91 65-130
1,2,3-Trichloropropane ug/kg 12101250 97 70-130
1,2,4-Trichlorobenzene ug/kg 11501250 92 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301645LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12701250 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 11101250 89 70-130
1,2-Dibromoethane (EDB)ug/kg 12901250 103 70-130
1,2-Dichlorobenzene ug/kg 12301250 99 70-130
1,2-Dichloroethane ug/kg 12601250 100 63-130
1,2-Dichloropropane ug/kg 13401250 107 70-130
1,3,5-Trimethylbenzene ug/kg 11501250 92 70-130
1,3-Dichlorobenzene ug/kg 12501250 100 70-130
1,3-Dichloropropane ug/kg 13201250 106 70-130
1,4-Dichlorobenzene ug/kg 12401250 99 70-130
2,2-Dichloropropane ug/kg 11201250 89 66-130
2-Butanone (MEK)ug/kg 25402500 102 70-130
2-Chlorotoluene ug/kg 12301250 98 70-130
2-Hexanone ug/kg 26302500 105 70-130
4-Chlorotoluene ug/kg 11701250 94 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 26302500 105 70-130
Acetone ug/kg 25702500 103 69-130
Benzene ug/kg 12801250 102 70-130
Bromobenzene ug/kg 12801250 103 70-130
Bromochloromethane ug/kg 14001250 112 70-130
Bromodichloromethane ug/kg 11701250 94 69-130
Bromoform ug/kg 11801250 94 70-130
Bromomethane ug/kg 2080 IK,L1,v1125016652-130
Carbon tetrachloride ug/kg 11801250 94 70-130
Chlorobenzene ug/kg 13201250 105 70-130
Chloroethane ug/kg 13501250 108 65-130
Chloroform ug/kg 12101250 97 70-130
Chloromethane ug/kg 13901250 111 55-130
cis-1,2-Dichloroethene ug/kg 13401250 107 70-130
cis-1,3-Dichloropropene ug/kg 12301250 99 70-130
Dibromochloromethane ug/kg 12201250 97 70-130
Dibromomethane ug/kg 13101250 105 70-130
Dichlorodifluoromethane ug/kg 12601250 100 45-156
Diisopropyl ether ug/kg 12201250 98 70-130
Ethylbenzene ug/kg 12301250 98 70-130
Hexachloro-1,3-butadiene ug/kg 11401250 91 66-130
Isopropylbenzene (Cumene)ug/kg 12801250 102 70-130
m&p-Xylene ug/kg 24802500 99 70-130
Methyl-tert-butyl ether ug/kg 12301250 98 70-130
Methylene Chloride ug/kg 14701250 117 65-130
n-Butylbenzene ug/kg 11701250 94 67-130
n-Propylbenzene ug/kg 11801250 94 70-130
Naphthalene ug/kg 10701250 86 70-130
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 11401250 92 67-130
sec-Butylbenzene ug/kg 11601250 93 69-130
Styrene ug/kg 12901250 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301645LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 915 v312507367-130
Tetrachloroethene ug/kg 13001250 104 70-130
Toluene ug/kg 12001250 96 70-130
trans-1,2-Dichloroethene ug/kg 13501250 108 70-130
trans-1,3-Dichloropropene ug/kg 12001250 96 68-130
Trichloroethene ug/kg 12701250 102 70-130
Trichlorofluoromethane ug/kg 11801250 94 70-130
Vinyl acetate ug/kg 27402500 109 70-130
Vinyl chloride ug/kg 13201250 105 61-130
Xylene (Total)ug/kg 37203750 99 70-130
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3301647MATRIX SPIKE SAMPLE:
MSSpike
Result
92545088008
1,1,1,2-Tetrachloroethane ug/kg 540534 101 70-131ND
1,1,1-Trichloroethane ug/kg 528534 99 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 532534 100 66-130ND
1,1,2-Trichloroethane ug/kg 530534 99 66-133ND
1,1-Dichloroethane ug/kg 605534 113 65-130ND
1,1-Dichloroethene ug/kg 672534 126 10-158ND
1,1-Dichloropropene ug/kg 598534 112 68-133ND
1,2,3-Trichlorobenzene ug/kg 496534 93 27-138ND
1,2,3-Trichloropropane ug/kg 513534 96 67-130ND
1,2,4-Trichlorobenzene ug/kg 516534 97 51-134ND
1,2,4-Trimethylbenzene ug/kg 554534 104 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 431534 81 32-130ND
1,2-Dibromoethane (EDB)ug/kg 572534 107 70-130ND
1,2-Dichlorobenzene ug/kg 555534 104 69-130ND
1,2-Dichloroethane ug/kg 563534 105 59-130ND
1,2-Dichloropropane ug/kg 624534 117 70-130ND
1,3,5-Trimethylbenzene ug/kg 508534 95 65-137ND
1,3-Dichlorobenzene ug/kg 551534 103 70-130ND
1,3-Dichloropropane ug/kg 599534 112 70-130ND
1,4-Dichlorobenzene ug/kg 548534 103 68-130ND
2,2-Dichloropropane ug/kg 451534 84 32-130ND
2-Butanone (MEK)ug/kg 10501070 98 10-136ND
2-Chlorotoluene ug/kg 544534 102 69-141ND
2-Hexanone ug/kg 10901070 102 10-144ND
4-Chlorotoluene ug/kg 521534 98 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 11101070 104 25-143ND
Acetone ug/kg 9981070 89 10-130ND
Benzene ug/kg 603534 113 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3301647MATRIX SPIKE SAMPLE:
MSSpike
Result
92545088008
Bromobenzene ug/kg 562534 105 70-130ND
Bromochloromethane ug/kg 628534 118 69-134ND
Bromodichloromethane ug/kg 496534 93 64-130ND
Bromoform ug/kg 447534 84 62-130ND
Bromomethane ug/kg 489 IK,v15349120-176ND
Carbon tetrachloride ug/kg 529534 99 65-140ND
Chlorobenzene ug/kg 598534 112 70-130ND
Chloroethane ug/kg 163534 31 10-130ND
Chloroform ug/kg 559534 105 63-130ND
Chloromethane ug/kg 756 M153414158-130ND
cis-1,2-Dichloroethene ug/kg 623534 117 66-130ND
cis-1,3-Dichloropropene ug/kg 528534 99 67-130ND
Dibromochloromethane ug/kg 497534 93 67-130ND
Dibromomethane ug/kg 581534 109 63-131ND
Dichlorodifluoromethane ug/kg 639534 120 44-180ND
Diisopropyl ether ug/kg 557534 104 63-130ND
Ethylbenzene ug/kg 565534 106 66-130ND
Hexachloro-1,3-butadiene ug/kg 570534 107 64-150ND
Isopropylbenzene (Cumene)ug/kg 595534 111 69-135ND
m&p-Xylene ug/kg 11201070 105 60-133ND
Methyl-tert-butyl ether ug/kg 546534 102 65-130ND
Methylene Chloride ug/kg 804534 123 61-130145
n-Butylbenzene ug/kg 530534 99 65-140ND
n-Propylbenzene ug/kg 530534 99 67-140ND
Naphthalene ug/kg 442534 83 15-145ND
o-Xylene ug/kg 575534 108 66-133ND
p-Isopropyltoluene ug/kg 526534 98 56-147ND
sec-Butylbenzene ug/kg 553534 103 65-139ND
Styrene ug/kg 580534 109 70-132ND
tert-Butylbenzene ug/kg 432 v35348162-135ND
Tetrachloroethene ug/kg 585534 109 70-135ND
Toluene ug/kg 562534 105 67-130ND
trans-1,2-Dichloroethene ug/kg 634534 119 69-130ND
trans-1,3-Dichloropropene ug/kg 511534 96 62-130ND
Trichloroethene ug/kg 601534 112 70-135ND
Trichlorofluoromethane ug/kg 197534 37 10-130ND
Vinyl acetate ug/kg 10801070 101 53-130ND
Vinyl chloride ug/kg 680534 127 61-148ND
Xylene (Total)ug/kg 17001610 106 63-132ND
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545088007
3301646SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 135 5128
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IK,v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545088007
3301646SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 159 C911178
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg ND v2ND
Tetrachloroethene ug/kg 3.3JND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%103104
4-Bromofluorobenzene (S)%9695
Toluene-d8 (S)%103104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628014
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088012, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301650
Associated Lab Samples:92545088012, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/18/21 05:26
1,1,1-Trichloroethane ug/kg ND 5.0 06/18/21 05:26
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/18/21 05:26
1,1,2-Trichloroethane ug/kg ND 5.0 06/18/21 05:26
1,1-Dichloroethane ug/kg ND 5.0 06/18/21 05:26
1,1-Dichloroethene ug/kg ND 5.0 06/18/21 05:26
1,1-Dichloropropene ug/kg ND 5.0 06/18/21 05:26
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/18/21 05:26
1,2,3-Trichloropropane ug/kg ND 5.0 06/18/21 05:26
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/18/21 05:26
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/18/21 05:26
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/18/21 05:26
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/18/21 05:26
1,2-Dichlorobenzene ug/kg ND 5.0 06/18/21 05:26
1,2-Dichloroethane ug/kg ND 5.0 06/18/21 05:26
1,2-Dichloropropane ug/kg ND 5.0 06/18/21 05:26
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/18/21 05:26
1,3-Dichlorobenzene ug/kg ND 5.0 06/18/21 05:26
1,3-Dichloropropane ug/kg ND 5.0 06/18/21 05:26
1,4-Dichlorobenzene ug/kg ND 5.0 06/18/21 05:26
2,2-Dichloropropane ug/kg ND 5.0 06/18/21 05:26
2-Butanone (MEK)ug/kg ND 100 06/18/21 05:26
2-Chlorotoluene ug/kg ND 5.0 06/18/21 05:26
2-Hexanone ug/kg ND 50.0 06/18/21 05:26
4-Chlorotoluene ug/kg ND 5.0 06/18/21 05:26
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/18/21 05:26
Acetone ug/kg ND 100 06/18/21 05:26
Benzene ug/kg ND 5.0 06/18/21 05:26
Bromobenzene ug/kg ND 5.0 06/18/21 05:26
Bromochloromethane ug/kg ND 5.0 06/18/21 05:26
Bromodichloromethane ug/kg ND 5.0 06/18/21 05:26
Bromoform ug/kg ND 5.0 06/18/21 05:26
Bromomethane ug/kg ND 10.0 IK,v106/18/21 05:26
Carbon tetrachloride ug/kg ND 5.0 06/18/21 05:26
Chlorobenzene ug/kg ND 5.0 06/18/21 05:26
Chloroethane ug/kg ND 10.0 06/18/21 05:26
Chloroform ug/kg ND 5.0 06/18/21 05:26
Chloromethane ug/kg ND 10.0 06/18/21 05:26
cis-1,2-Dichloroethene ug/kg ND 5.0 06/18/21 05:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301650
Associated Lab Samples:92545088012, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Matrix:Solid
Analyzed
cis-1,3-Dichloropropene ug/kg ND 5.0 06/18/21 05:26
Dibromochloromethane ug/kg ND 5.0 06/18/21 05:26
Dibromomethane ug/kg ND 5.0 06/18/21 05:26
Dichlorodifluoromethane ug/kg ND 10.0 06/18/21 05:26
Diisopropyl ether ug/kg ND 5.0 06/18/21 05:26
Ethylbenzene ug/kg ND 5.0 06/18/21 05:26
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/18/21 05:26
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/18/21 05:26
m&p-Xylene ug/kg ND 10.0 06/18/21 05:26
Methyl-tert-butyl ether ug/kg ND 5.0 06/18/21 05:26
Methylene Chloride ug/kg ND 20.0 06/18/21 05:26
n-Butylbenzene ug/kg ND 5.0 06/18/21 05:26
n-Propylbenzene ug/kg ND 5.0 06/18/21 05:26
Naphthalene ug/kg ND 5.0 06/18/21 05:26
o-Xylene ug/kg ND 5.0 06/18/21 05:26
p-Isopropyltoluene ug/kg ND 5.0 06/18/21 05:26
sec-Butylbenzene ug/kg ND 5.0 06/18/21 05:26
Styrene ug/kg ND 5.0 06/18/21 05:26
tert-Butylbenzene ug/kg ND 5.0 06/18/21 05:26
Tetrachloroethene ug/kg ND 5.0 06/18/21 05:26
Toluene ug/kg ND 5.0 06/18/21 05:26
trans-1,2-Dichloroethene ug/kg ND 5.0 06/18/21 05:26
trans-1,3-Dichloropropene ug/kg ND 5.0 06/18/21 05:26
Trichloroethene ug/kg ND 5.0 06/18/21 05:26
Trichlorofluoromethane ug/kg ND 5.0 06/18/21 05:26
Vinyl acetate ug/kg ND 50.0 06/18/21 05:26
Vinyl chloride ug/kg ND 10.0 06/18/21 05:26
Xylene (Total)ug/kg ND 10.0 06/18/21 05:26
1,2-Dichloroethane-d4 (S)%117 70-130 06/18/21 05:26
4-Bromofluorobenzene (S)%101 69-134 06/18/21 05:26
Toluene-d8 (S)%102 70-130 06/18/21 05:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301651LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11701250 94 70-130
1,1,1-Trichloroethane ug/kg 11001250 88 70-130
1,1,2,2-Tetrachloroethane ug/kg 11501250 92 70-130
1,1,2-Trichloroethane ug/kg 10801250 86 70-130
1,1-Dichloroethane ug/kg 12701250 101 70-130
1,1-Dichloroethene ug/kg 12601250 101 70-130
1,1-Dichloropropene ug/kg 12001250 96 70-130
1,2,3-Trichlorobenzene ug/kg 11701250 94 65-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301651LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 12001250 96 70-130
1,2,4-Trichlorobenzene ug/kg 11801250 95 68-130
1,2,4-Trimethylbenzene ug/kg 12101250 97 70-130
1,2-Dibromo-3-chloropropane ug/kg 11501250 92 70-130
1,2-Dibromoethane (EDB)ug/kg 11701250 94 70-130
1,2-Dichlorobenzene ug/kg 11501250 92 70-130
1,2-Dichloroethane ug/kg 11901250 95 63-130
1,2-Dichloropropane ug/kg 12201250 98 70-130
1,3,5-Trimethylbenzene ug/kg 11901250 96 70-130
1,3-Dichlorobenzene ug/kg 11501250 92 70-130
1,3-Dichloropropane ug/kg 12001250 96 70-130
1,4-Dichlorobenzene ug/kg 11801250 95 70-130
2,2-Dichloropropane ug/kg 10601250 85 66-130
2-Butanone (MEK)ug/kg 25402500 102 70-130
2-Chlorotoluene ug/kg 12401250 99 70-130
2-Hexanone ug/kg 26202500 105 70-130
4-Chlorotoluene ug/kg 11601250 93 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25702500 103 70-130
Acetone ug/kg 26602500 106 69-130
Benzene ug/kg 11801250 94 70-130
Bromobenzene ug/kg 11901250 95 70-130
Bromochloromethane ug/kg 12001250 96 70-130
Bromodichloromethane ug/kg 10801250 86 69-130
Bromoform ug/kg 11101250 89 70-130
Bromomethane ug/kg 1720 IK,L1,v1125013852-130
Carbon tetrachloride ug/kg 11501250 92 70-130
Chlorobenzene ug/kg 11901250 95 70-130
Chloroethane ug/kg 14201250 114 65-130
Chloroform ug/kg 13001250 104 70-130
Chloromethane ug/kg 11701250 94 55-130
cis-1,2-Dichloroethene ug/kg 12401250 100 70-130
cis-1,3-Dichloropropene ug/kg 11801250 94 70-130
Dibromochloromethane ug/kg 11501250 92 70-130
Dibromomethane ug/kg 11401250 91 70-130
Dichlorodifluoromethane ug/kg 11001250 88 45-156
Diisopropyl ether ug/kg 12001250 96 70-130
Ethylbenzene ug/kg 13201250 106 70-130
Hexachloro-1,3-butadiene ug/kg 12201250 98 66-130
Isopropylbenzene (Cumene)ug/kg 12301250 99 70-130
m&p-Xylene ug/kg 24202500 97 70-130
Methyl-tert-butyl ether ug/kg 11501250 92 70-130
Methylene Chloride ug/kg 13701250 110 65-130
n-Butylbenzene ug/kg 12601250 101 67-130
n-Propylbenzene ug/kg 12601250 101 70-130
Naphthalene ug/kg 11501250 92 70-130
o-Xylene ug/kg 12101250 97 70-130
p-Isopropyltoluene ug/kg 12101250 97 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301651LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 12001250 96 69-130
Styrene ug/kg 12101250 97 70-130
tert-Butylbenzene ug/kg 11501250 92 67-130
Tetrachloroethene ug/kg 10501250 84 70-130
Toluene ug/kg 11501250 92 70-130
trans-1,2-Dichloroethene ug/kg 12701250 102 70-130
trans-1,3-Dichloropropene ug/kg 11801250 94 68-130
Trichloroethene ug/kg 11701250 93 70-130
Trichlorofluoromethane ug/kg 11801250 95 70-130
Vinyl acetate ug/kg 27502500 110 70-130
Vinyl chloride ug/kg 12801250 102 61-130
Xylene (Total)ug/kg 36303750 97 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3301653MATRIX SPIKE SAMPLE:
MSSpike
Result
92545088013
1,1,1,2-Tetrachloroethane ug/kg 361509 71 70-131ND
1,1,1-Trichloroethane ug/kg 372509 73 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 347509 68 66-130ND
1,1,2-Trichloroethane ug/kg 347509 68 66-133ND
1,1-Dichloroethane ug/kg 430509 84 65-130ND
1,1-Dichloroethene ug/kg 489509 96 10-158ND
1,1-Dichloropropene ug/kg 417509 82 68-133ND
1,2,3-Trichlorobenzene ug/kg 401509 79 27-138ND
1,2,3-Trichloropropane ug/kg 353509 69 67-130ND
1,2,4-Trichlorobenzene ug/kg 394509 77 51-134ND
1,2,4-Trimethylbenzene ug/kg 381509 75 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 312509 61 32-130ND
1,2-Dibromoethane (EDB)ug/kg 368509 72 70-130ND
1,2-Dichlorobenzene ug/kg 371509 73 69-130ND
1,2-Dichloroethane ug/kg 406509 80 59-130ND
1,2-Dichloropropane ug/kg 418509 82 70-130ND
1,3,5-Trimethylbenzene ug/kg 397509 78 65-137ND
1,3-Dichlorobenzene ug/kg 365509 72 70-130ND
1,3-Dichloropropane ug/kg 402509 79 70-130ND
1,4-Dichlorobenzene ug/kg 377509 74 68-130ND
2,2-Dichloropropane ug/kg 337509 66 32-130ND
2-Butanone (MEK)ug/kg 7361020 72 10-136ND
2-Chlorotoluene ug/kg 406509 80 69-141ND
2-Hexanone ug/kg 7291020 72 10-144ND
4-Chlorotoluene ug/kg 382509 75 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 7701020 76 25-143ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3301653MATRIX SPIKE SAMPLE:
MSSpike
Result
92545088013
Acetone ug/kg 6661020 62 10-130ND
Benzene ug/kg 402509 79 67-130ND
Bromobenzene ug/kg 380509 75 70-130ND
Bromochloromethane ug/kg 380509 75 69-134ND
Bromodichloromethane ug/kg 331509 65 64-130ND
Bromoform ug/kg 286 M15095662-130ND
Bromomethane ug/kg 390 IK,v15097720-176ND
Carbon tetrachloride ug/kg 361509 71 65-140ND
Chlorobenzene ug/kg 389509 76 70-130ND
Chloroethane ug/kg 179509 35 10-130ND
Chloroform ug/kg 423509 83 63-130ND
Chloromethane ug/kg 466509 92 58-130ND
cis-1,2-Dichloroethene ug/kg 425509 83 66-130ND
cis-1,3-Dichloropropene ug/kg 372509 73 67-130ND
Dibromochloromethane ug/kg 321 M15096367-130ND
Dibromomethane ug/kg 359509 70 63-131ND
Dichlorodifluoromethane ug/kg 414509 81 44-180ND
Diisopropyl ether ug/kg 399509 78 63-130ND
Ethylbenzene ug/kg 434509 85 66-130ND
Hexachloro-1,3-butadiene ug/kg 414509 81 64-150ND
Isopropylbenzene (Cumene)ug/kg 406509 80 69-135ND
m&p-Xylene ug/kg 8031020 79 60-133ND
Methyl-tert-butyl ether ug/kg 370509 73 65-130ND
Methylene Chloride ug/kg 539509 106 61-130ND
n-Butylbenzene ug/kg 433509 85 65-140ND
n-Propylbenzene ug/kg 422509 83 67-140ND
Naphthalene ug/kg 365509 72 15-145ND
o-Xylene ug/kg 393509 77 66-133ND
p-Isopropyltoluene ug/kg 409509 80 56-147ND
sec-Butylbenzene ug/kg 419509 82 65-139ND
Styrene ug/kg 379509 74 70-132ND
tert-Butylbenzene ug/kg 388509 76 62-135ND
Tetrachloroethene ug/kg 351 M15096970-135ND
Toluene ug/kg 385509 76 67-130ND
trans-1,2-Dichloroethene ug/kg 437509 86 69-130ND
trans-1,3-Dichloropropene ug/kg 365509 72 62-130ND
Trichloroethene ug/kg 384509 75 70-135ND
Trichlorofluoromethane ug/kg 136509 27 10-130ND
Vinyl acetate ug/kg 8671020 85 53-130ND
Vinyl chloride ug/kg 463509 91 61-148ND
Xylene (Total)ug/kg 12001520 78 63-132ND
1,2-Dichloroethane-d4 (S)%127 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545088012
3301652SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IK,v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545088012
3301652SAMPLE DUPLICATE:
m&p-Xylene ug/kg 6.4JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 7.5 C798.3
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%113115
4-Bromofluorobenzene (S)%99101
Toluene-d8 (S)%103103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628112
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088001, 92545088002, 92545088003, 92545088004, 92545088005, 92545088006, 92545088007,
92545088008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301838
Associated Lab Samples:92545088001, 92545088002, 92545088003, 92545088004, 92545088005, 92545088006, 92545088007,
92545088008
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 06/22/21 09:10
n-Pentacosane (S)%64 32-130 06/22/21 09:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301839LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 52.666.4 79 47-130
n-Pentacosane (S)%76 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3301840MATRIX SPIKE SAMPLE:
MSSpike
Result
92545088005
Diesel Range Organics(C10-C28)mg/kg 55.975.6 73 10-133ND
n-Pentacosane (S)%72 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92545088006
3301841SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%7277
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628008
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088001, 92545088002, 92545088003, 92545088004
Parameter Units
Dup
Result QualifiersRPDResult
92544529013
3301632SAMPLE DUPLICATE:
Percent Moisture %13.6 N2113.5
Parameter Units
Dup
Result QualifiersRPDResult
92545036001
3301633SAMPLE DUPLICATE:
Percent Moisture %0.25 D6,N2330.18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628011
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545088005, 92545088006, 92545088007, 92545088008, 92545088009, 92545088010, 92545088011,
92545088012, 92545088013, 92545088014, 92545088015, 92545088016, 92545088017, 92545088018,
92545088019, 92545088020, 92545088021
Parameter Units
Dup
Result QualifiersRPDResult
92545088005
3301642SAMPLE DUPLICATE:
Percent Moisture %11.5 N2011.5
Parameter Units
Dup
Result QualifiersRPDResult
92544826001
3302470SAMPLE DUPLICATE:
Percent Moisture %97.0 N2097.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 69
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92545088001 628112 628384SS-14 EPA 3546 EPA 8015C Modified
92545088002 628112 628384SS-30 EPA 3546 EPA 8015C Modified
92545088003 628112 628384SS-31 EPA 3546 EPA 8015C Modified
92545088004 628112 628384SS-32 EPA 3546 EPA 8015C Modified
92545088005 628112 628384SS-33 EPA 3546 EPA 8015C Modified
92545088006 628112 628384SS-34 EPA 3546 EPA 8015C Modified
92545088007 628112 628384SS-15 EPA 3546 EPA 8015C Modified
92545088008 628112 628384SS-16 EPA 3546 EPA 8015C Modified
92545088001 628176 628218SS-14 EPA 5030B EPA 8015C Modified
92545088002 628176 628218SS-30 EPA 5030B EPA 8015C Modified
92545088003 628176 628218SS-31 EPA 5030B EPA 8015C Modified
92545088004 628176 628218SS-32 EPA 5030B EPA 8015C Modified
92545088005 628176 628218SS-33 EPA 5030B EPA 8015C Modified
92545088006 628176 628218SS-34 EPA 5030B EPA 8015C Modified
92545088007 628394 628536SS-15 EPA 5030B EPA 8015C Modified
92545088008 628176 628218SS-16 EPA 5030B EPA 8015C Modified
92545088009 628176 628218SS-17 EPA 5030B EPA 8015C Modified
92545088010 628176 628218SS-18 EPA 5030B EPA 8015C Modified
92545088011 628176 628218SS-19 EPA 5030B EPA 8015C Modified
92545088012 628176 628218SS-20 EPA 5030B EPA 8015C Modified
92545088013 628394 628536SS-21 EPA 5030B EPA 8015C Modified
92545088014 628394 628536SS-22 EPA 5030B EPA 8015C Modified
92545088015 628394 628536SS-23 EPA 5030B EPA 8015C Modified
92545088016 628394 628536SS-24 EPA 5030B EPA 8015C Modified
92545088017 628394 628536SS-25 EPA 5030B EPA 8015C Modified
92545088018 628394 628536SS-26 EPA 5030B EPA 8015C Modified
92545088019 628394 628536SS-27 EPA 5030B EPA 8015C Modified
92545088020 628394 628536SS-28 EPA 5030B EPA 8015C Modified
92545088021 628394 628536SS-29 EPA 5030B EPA 8015C Modified
92545088007 628013 628031SS-15 EPA 5035A/5030B EPA 8260D
92545088008 628013 628031SS-16 EPA 5035A/5030B EPA 8260D
92545088009 628013 628031SS-17 EPA 5035A/5030B EPA 8260D
92545088010 628013 628031SS-18 EPA 5035A/5030B EPA 8260D
92545088011 628013 628031SS-19 EPA 5035A/5030B EPA 8260D
92545088012 628014 628030SS-20 EPA 5035A/5030B EPA 8260D
92545088013 628014 628030SS-21 EPA 5035A/5030B EPA 8260D
92545088014 628014 628030SS-22 EPA 5035A/5030B EPA 8260D
92545088015 628014 628030SS-23 EPA 5035A/5030B EPA 8260D
92545088016 628014 628030SS-24 EPA 5035A/5030B EPA 8260D
92545088017 628014 628030SS-25 EPA 5035A/5030B EPA 8260D
92545088018 628014 628030SS-26 EPA 5035A/5030B EPA 8260D
92545088019 628014 628030SS-27 EPA 5035A/5030B EPA 8260D
92545088020 628014 628030SS-28 EPA 5035A/5030B EPA 8260D
92545088021 628014 628030SS-29 EPA 5035A/5030B EPA 8260D
92545088001 628008SS-14 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92545088
Sheetz 391 11.SZ0391.00
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92545088002 628008SS-30 SW-846
92545088003 628008SS-31 SW-846
92545088004 628008SS-32 SW-846
92545088005 628011SS-33 SW-846
92545088006 628011SS-34 SW-846
92545088007 628011SS-15 SW-846
92545088008 628011SS-16 SW-846
92545088009 628011SS-17 SW-846
92545088010 628011SS-18 SW-846
92545088011 628011SS-19 SW-846
92545088012 628011SS-20 SW-846
92545088013 628011SS-21 SW-846
92545088014 628011SS-22 SW-846
92545088015 628011SS-23 SW-846
92545088016 628011SS-24 SW-846
92545088017 628011SS-25 SW-846
92545088018 628011SS-26 SW-846
92545088019 628011SS-27 SW-846
92545088020 628011SS-28 SW-846
92545088021 628011SS-29 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 69
Page 65 of 69
Page 66 of 69
Page 67 of 69
Page 68 of 69
Page 69 of 69

APPENDIX E
PRODUCT LINE LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
June 24, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92545119
92545119
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz 39 Greenville
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 61
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 61
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92545119001 SS-1 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119002 SS-2 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119003 SS-3 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119004 SS-4 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119005 SS-5 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119006 SS-6 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119007 SS-7 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119008 SS-8 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119009 SS-9 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119010 SS-10 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119011 SS-11 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92545119012 SS-12 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 61
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92545119013 SS-13 EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 61
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92545119001 SS-1
Percent Moisture 6.2 %06/18/21 17:41 N20.10SW-846
92545119002 SS-2
Percent Moisture 12.6 %06/18/21 17:41 N20.10SW-846
92545119003 SS-3
Percent Moisture 12.8 %06/18/21 17:41 N20.10SW-846
92545119004 SS-4
Toluene 10.6 ug/kg 06/22/21 16:44 C76.2EPA 8260D
1,3,5-Trimethylbenzene 7.2 ug/kg 06/22/21 16:446.2EPA 8260D
Xylene (Total)28.3 ug/kg 06/22/21 16:4412.5EPA 8260D
m&p-Xylene 16.3 ug/kg 06/22/21 16:4412.5EPA 8260D
o-Xylene 12.0 ug/kg 06/22/21 16:446.2EPA 8260D
Percent Moisture 18.2 %06/18/21 17:41 N20.10SW-846
92545119005 SS-5
Toluene 7.3 ug/kg 06/22/21 17:01 C75.7EPA 8260D
Percent Moisture 16.4 %06/18/21 17:41 N20.10SW-846
92545119006 SS-6
Toluene 13.1 ug/kg 06/22/21 17:19 C75.6EPA 8260D
Xylene (Total)22.8 ug/kg 06/22/21 17:1911.3EPA 8260D
m&p-Xylene 13.3 ug/kg 06/22/21 17:1911.3EPA 8260D
o-Xylene 9.5 ug/kg 06/22/21 17:195.6EPA 8260D
Percent Moisture 9.9 %06/18/21 17:41 N20.10SW-846
92545119007 SS-7
Percent Moisture 7.1 %06/18/21 17:41 N20.10SW-846
92545119008 SS-8
Percent Moisture 11.8 %06/18/21 17:41 N20.10SW-846
92545119009 SS-9
Percent Moisture 13.0 %06/18/21 17:42 N20.10SW-846
92545119010 SS-10
Percent Moisture 9.0 %06/18/21 17:42 N20.10SW-846
92545119011 SS-11
Percent Moisture 12.3 %06/18/21 17:42 N20.10SW-846
92545119012 SS-12
Percent Moisture 11.2 %06/18/21 17:42 N20.10SW-846
92545119013 SS-13
Diesel Range Organics(C10-C28)8.4 mg/kg 06/22/21 13:386.1EPA 8015C Modified
Percent Moisture 18.6 %06/18/21 17:42 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-1 Lab ID:92545119001 Collected:06/15/21 11:25 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 06:3006/21/21 09:237.3 1
Surrogates
4-Bromofluorobenzene (S)92 %06/23/21 06:30 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 15:51 67-64-106/22/21 10:591411
Benzene ND ug/kg 06/22/21 15:51 71-43-206/22/21 10:597.0 1
Bromobenzene ND ug/kg 06/22/21 15:51 108-86-106/22/21 10:597.0 1
Bromochloromethane ND ug/kg 06/22/21 15:51 74-97-506/22/21 10:597.0 1
Bromodichloromethane ND ug/kg 06/22/21 15:51 75-27-406/22/21 10:597.0 1
Bromoform ND ug/kg 06/22/21 15:51 75-25-206/22/21 10:597.0 1
Bromomethane ND ug/kg 06/22/21 15:51 74-83-9 IK,L1,v106/22/21 10:5914.1 1
2-Butanone (MEK)ND ug/kg 06/22/21 15:51 78-93-306/22/21 10:591411
n-Butylbenzene ND ug/kg 06/22/21 15:51 104-51-806/22/21 10:597.0 1
sec-Butylbenzene ND ug/kg 06/22/21 15:51 135-98-806/22/21 10:597.0 1
tert-Butylbenzene ND ug/kg 06/22/21 15:51 98-06-6 v206/22/21 10:597.0 1
Carbon tetrachloride ND ug/kg 06/22/21 15:51 56-23-506/22/21 10:597.0 1
Chlorobenzene ND ug/kg 06/22/21 15:51 108-90-706/22/21 10:597.0 1
Chloroethane ND ug/kg 06/22/21 15:51 75-00-306/22/21 10:5914.1 1
Chloroform ND ug/kg 06/22/21 15:51 67-66-306/22/21 10:597.0 1
Chloromethane ND ug/kg 06/22/21 15:51 74-87-306/22/21 10:5914.1 1
2-Chlorotoluene ND ug/kg 06/22/21 15:51 95-49-806/22/21 10:597.0 1
4-Chlorotoluene ND ug/kg 06/22/21 15:51 106-43-406/22/21 10:597.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 15:51 96-12-806/22/21 10:597.0 1
Dibromochloromethane ND ug/kg 06/22/21 15:51 124-48-106/22/21 10:597.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 15:51 106-93-406/22/21 10:597.0 1
Dibromomethane ND ug/kg 06/22/21 15:51 74-95-306/22/21 10:597.0 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 15:51 95-50-106/22/21 10:597.0 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 15:51 541-73-106/22/21 10:597.0 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 15:51 106-46-706/22/21 10:597.0 1
Dichlorodifluoromethane ND ug/kg 06/22/21 15:51 75-71-8 v206/22/21 10:5914.1 1
1,1-Dichloroethane ND ug/kg 06/22/21 15:51 75-34-306/22/21 10:597.0 1
1,2-Dichloroethane ND ug/kg 06/22/21 15:51 107-06-206/22/21 10:597.0 1
1,1-Dichloroethene ND ug/kg 06/22/21 15:51 75-35-406/22/21 10:597.0 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 15:51 156-59-206/22/21 10:597.0 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 15:51 156-60-506/22/21 10:597.0 1
1,2-Dichloropropane ND ug/kg 06/22/21 15:51 78-87-506/22/21 10:597.0 1
1,3-Dichloropropane ND ug/kg 06/22/21 15:51 142-28-906/22/21 10:597.0 1
2,2-Dichloropropane ND ug/kg 06/22/21 15:51 594-20-706/22/21 10:597.0 1
1,1-Dichloropropene ND ug/kg 06/22/21 15:51 563-58-606/22/21 10:597.0 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 15:51 10061-01-506/22/21 10:597.0 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 15:51 10061-02-606/22/21 10:597.0 1
Diisopropyl ether ND ug/kg 06/22/21 15:51 108-20-306/22/21 10:597.0 1
Ethylbenzene ND ug/kg 06/22/21 15:51 100-41-406/22/21 10:597.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-1 Lab ID:92545119001 Collected:06/15/21 11:25 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 15:51 87-68-306/22/21 10:5914.1 1
2-Hexanone ND ug/kg 06/22/21 15:51 591-78-606/22/21 10:5970.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 15:51 98-82-806/22/21 10:597.0 1
p-Isopropyltoluene ND ug/kg 06/22/21 15:51 99-87-606/22/21 10:597.0 1
Methylene Chloride ND ug/kg 06/22/21 15:51 75-09-206/22/21 10:5928.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 15:51 108-10-106/22/21 10:5970.4 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 15:51 1634-04-406/22/21 10:597.0 1
Naphthalene ND ug/kg 06/22/21 15:51 91-20-3 v206/22/21 10:597.0 1
n-Propylbenzene ND ug/kg 06/22/21 15:51 103-65-106/22/21 10:597.0 1
Styrene ND ug/kg 06/22/21 15:51 100-42-506/22/21 10:597.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 15:51 630-20-606/22/21 10:597.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 15:51 79-34-506/22/21 10:597.0 1
Tetrachloroethene ND ug/kg 06/22/21 15:51 127-18-406/22/21 10:597.0 1
Toluene ND ug/kg 06/22/21 15:51 108-88-306/22/21 10:597.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 15:51 87-61-606/22/21 10:597.0 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 15:51 120-82-106/22/21 10:597.0 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 15:51 71-55-606/22/21 10:597.0 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 15:51 79-00-506/22/21 10:597.0 1
Trichloroethene ND ug/kg 06/22/21 15:51 79-01-606/22/21 10:597.0 1
Trichlorofluoromethane ND ug/kg 06/22/21 15:51 75-69-406/22/21 10:597.0 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 15:51 96-18-406/22/21 10:597.0 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 15:51 95-63-606/22/21 10:597.0 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 15:51 108-67-806/22/21 10:597.0 1
Vinyl acetate ND ug/kg 06/22/21 15:51 108-05-406/22/21 10:5970.4 1
Vinyl chloride ND ug/kg 06/22/21 15:51 75-01-406/22/21 10:5914.1 1
Xylene (Total)ND ug/kg 06/22/21 15:51 1330-20-706/22/21 10:5914.1 1
m&p-Xylene ND ug/kg 06/22/21 15:51 179601-23-106/22/21 10:5914.1 1
o-Xylene ND ug/kg 06/22/21 15:51 95-47-606/22/21 10:597.0 1
Surrogates
Toluene-d8 (S)104 %06/22/21 15:51 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)97 %06/22/21 15:51 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)111 %06/22/21 15:51 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.2 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-2 Lab ID:92545119002 Collected:06/15/21 11:29 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 07:2606/21/21 09:2311.4 1
Surrogates
4-Bromofluorobenzene (S)88 %06/23/21 07:26 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 16:08 67-64-106/22/21 10:591551
Benzene ND ug/kg 06/22/21 16:08 71-43-206/22/21 10:597.8 1
Bromobenzene ND ug/kg 06/22/21 16:08 108-86-106/22/21 10:597.8 1
Bromochloromethane ND ug/kg 06/22/21 16:08 74-97-506/22/21 10:597.8 1
Bromodichloromethane ND ug/kg 06/22/21 16:08 75-27-406/22/21 10:597.8 1
Bromoform ND ug/kg 06/22/21 16:08 75-25-206/22/21 10:597.8 1
Bromomethane ND ug/kg 06/22/21 16:08 74-83-9 IK,L1,v106/22/21 10:5915.5 1
2-Butanone (MEK)ND ug/kg 06/22/21 16:08 78-93-306/22/21 10:591551
n-Butylbenzene ND ug/kg 06/22/21 16:08 104-51-806/22/21 10:597.8 1
sec-Butylbenzene ND ug/kg 06/22/21 16:08 135-98-806/22/21 10:597.8 1
tert-Butylbenzene ND ug/kg 06/22/21 16:08 98-06-6 v206/22/21 10:597.8 1
Carbon tetrachloride ND ug/kg 06/22/21 16:08 56-23-506/22/21 10:597.8 1
Chlorobenzene ND ug/kg 06/22/21 16:08 108-90-706/22/21 10:597.8 1
Chloroethane ND ug/kg 06/22/21 16:08 75-00-306/22/21 10:5915.5 1
Chloroform ND ug/kg 06/22/21 16:08 67-66-306/22/21 10:597.8 1
Chloromethane ND ug/kg 06/22/21 16:08 74-87-306/22/21 10:5915.5 1
2-Chlorotoluene ND ug/kg 06/22/21 16:08 95-49-806/22/21 10:597.8 1
4-Chlorotoluene ND ug/kg 06/22/21 16:08 106-43-406/22/21 10:597.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 16:08 96-12-806/22/21 10:597.8 1
Dibromochloromethane ND ug/kg 06/22/21 16:08 124-48-106/22/21 10:597.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 16:08 106-93-406/22/21 10:597.8 1
Dibromomethane ND ug/kg 06/22/21 16:08 74-95-306/22/21 10:597.8 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 16:08 95-50-106/22/21 10:597.8 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 16:08 541-73-106/22/21 10:597.8 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 16:08 106-46-706/22/21 10:597.8 1
Dichlorodifluoromethane ND ug/kg 06/22/21 16:08 75-71-8 v206/22/21 10:5915.5 1
1,1-Dichloroethane ND ug/kg 06/22/21 16:08 75-34-306/22/21 10:597.8 1
1,2-Dichloroethane ND ug/kg 06/22/21 16:08 107-06-206/22/21 10:597.8 1
1,1-Dichloroethene ND ug/kg 06/22/21 16:08 75-35-406/22/21 10:597.8 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 16:08 156-59-206/22/21 10:597.8 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 16:08 156-60-506/22/21 10:597.8 1
1,2-Dichloropropane ND ug/kg 06/22/21 16:08 78-87-506/22/21 10:597.8 1
1,3-Dichloropropane ND ug/kg 06/22/21 16:08 142-28-906/22/21 10:597.8 1
2,2-Dichloropropane ND ug/kg 06/22/21 16:08 594-20-706/22/21 10:597.8 1
1,1-Dichloropropene ND ug/kg 06/22/21 16:08 563-58-606/22/21 10:597.8 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 16:08 10061-01-506/22/21 10:597.8 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 16:08 10061-02-606/22/21 10:597.8 1
Diisopropyl ether ND ug/kg 06/22/21 16:08 108-20-306/22/21 10:597.8 1
Ethylbenzene ND ug/kg 06/22/21 16:08 100-41-406/22/21 10:597.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-2 Lab ID:92545119002 Collected:06/15/21 11:29 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 16:08 87-68-306/22/21 10:5915.5 1
2-Hexanone ND ug/kg 06/22/21 16:08 591-78-606/22/21 10:5977.7 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 16:08 98-82-806/22/21 10:597.8 1
p-Isopropyltoluene ND ug/kg 06/22/21 16:08 99-87-606/22/21 10:597.8 1
Methylene Chloride ND ug/kg 06/22/21 16:08 75-09-206/22/21 10:5931.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 16:08 108-10-106/22/21 10:5977.7 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 16:08 1634-04-406/22/21 10:597.8 1
Naphthalene ND ug/kg 06/22/21 16:08 91-20-3 v206/22/21 10:597.8 1
n-Propylbenzene ND ug/kg 06/22/21 16:08 103-65-106/22/21 10:597.8 1
Styrene ND ug/kg 06/22/21 16:08 100-42-506/22/21 10:597.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 16:08 630-20-606/22/21 10:597.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 16:08 79-34-506/22/21 10:597.8 1
Tetrachloroethene ND ug/kg 06/22/21 16:08 127-18-406/22/21 10:597.8 1
Toluene ND ug/kg 06/22/21 16:08 108-88-306/22/21 10:597.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 16:08 87-61-606/22/21 10:597.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 16:08 120-82-106/22/21 10:597.8 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 16:08 71-55-606/22/21 10:597.8 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 16:08 79-00-506/22/21 10:597.8 1
Trichloroethene ND ug/kg 06/22/21 16:08 79-01-606/22/21 10:597.8 1
Trichlorofluoromethane ND ug/kg 06/22/21 16:08 75-69-406/22/21 10:597.8 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 16:08 96-18-406/22/21 10:597.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 16:08 95-63-606/22/21 10:597.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 16:08 108-67-806/22/21 10:597.8 1
Vinyl acetate ND ug/kg 06/22/21 16:08 108-05-406/22/21 10:5977.7 1
Vinyl chloride ND ug/kg 06/22/21 16:08 75-01-406/22/21 10:5915.5 1
Xylene (Total)ND ug/kg 06/22/21 16:08 1330-20-706/22/21 10:5915.5 1
m&p-Xylene ND ug/kg 06/22/21 16:08 179601-23-106/22/21 10:5915.5 1
o-Xylene ND ug/kg 06/22/21 16:08 95-47-606/22/21 10:597.8 1
Surrogates
Toluene-d8 (S)104 %06/22/21 16:08 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)97 %06/22/21 16:08 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)113 %06/22/21 16:08 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.6 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-3 Lab ID:92545119003 Collected:06/15/21 11:32 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 06:5806/21/21 09:239.4 1
Surrogates
4-Bromofluorobenzene (S)92 %06/23/21 06:58 460-00-406/21/21 09:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 16:26 67-64-106/22/21 10:591161
Benzene ND ug/kg 06/22/21 16:26 71-43-206/22/21 10:595.8 1
Bromobenzene ND ug/kg 06/22/21 16:26 108-86-106/22/21 10:595.8 1
Bromochloromethane ND ug/kg 06/22/21 16:26 74-97-506/22/21 10:595.8 1
Bromodichloromethane ND ug/kg 06/22/21 16:26 75-27-406/22/21 10:595.8 1
Bromoform ND ug/kg 06/22/21 16:26 75-25-206/22/21 10:595.8 1
Bromomethane ND ug/kg 06/22/21 16:26 74-83-9 IK,L1,v106/22/21 10:5911.6 1
2-Butanone (MEK)ND ug/kg 06/22/21 16:26 78-93-306/22/21 10:591161
n-Butylbenzene ND ug/kg 06/22/21 16:26 104-51-806/22/21 10:595.8 1
sec-Butylbenzene ND ug/kg 06/22/21 16:26 135-98-806/22/21 10:595.8 1
tert-Butylbenzene ND ug/kg 06/22/21 16:26 98-06-6 v206/22/21 10:595.8 1
Carbon tetrachloride ND ug/kg 06/22/21 16:26 56-23-506/22/21 10:595.8 1
Chlorobenzene ND ug/kg 06/22/21 16:26 108-90-706/22/21 10:595.8 1
Chloroethane ND ug/kg 06/22/21 16:26 75-00-306/22/21 10:5911.6 1
Chloroform ND ug/kg 06/22/21 16:26 67-66-306/22/21 10:595.8 1
Chloromethane ND ug/kg 06/22/21 16:26 74-87-306/22/21 10:5911.6 1
2-Chlorotoluene ND ug/kg 06/22/21 16:26 95-49-806/22/21 10:595.8 1
4-Chlorotoluene ND ug/kg 06/22/21 16:26 106-43-406/22/21 10:595.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 16:26 96-12-806/22/21 10:595.8 1
Dibromochloromethane ND ug/kg 06/22/21 16:26 124-48-106/22/21 10:595.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 16:26 106-93-406/22/21 10:595.8 1
Dibromomethane ND ug/kg 06/22/21 16:26 74-95-306/22/21 10:595.8 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 16:26 95-50-106/22/21 10:595.8 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 16:26 541-73-106/22/21 10:595.8 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 16:26 106-46-706/22/21 10:595.8 1
Dichlorodifluoromethane ND ug/kg 06/22/21 16:26 75-71-8 v206/22/21 10:5911.6 1
1,1-Dichloroethane ND ug/kg 06/22/21 16:26 75-34-306/22/21 10:595.8 1
1,2-Dichloroethane ND ug/kg 06/22/21 16:26 107-06-206/22/21 10:595.8 1
1,1-Dichloroethene ND ug/kg 06/22/21 16:26 75-35-406/22/21 10:595.8 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 16:26 156-59-206/22/21 10:595.8 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 16:26 156-60-506/22/21 10:595.8 1
1,2-Dichloropropane ND ug/kg 06/22/21 16:26 78-87-506/22/21 10:595.8 1
1,3-Dichloropropane ND ug/kg 06/22/21 16:26 142-28-906/22/21 10:595.8 1
2,2-Dichloropropane ND ug/kg 06/22/21 16:26 594-20-706/22/21 10:595.8 1
1,1-Dichloropropene ND ug/kg 06/22/21 16:26 563-58-606/22/21 10:595.8 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 16:26 10061-01-506/22/21 10:595.8 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 16:26 10061-02-606/22/21 10:595.8 1
Diisopropyl ether ND ug/kg 06/22/21 16:26 108-20-306/22/21 10:595.8 1
Ethylbenzene ND ug/kg 06/22/21 16:26 100-41-406/22/21 10:595.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-3 Lab ID:92545119003 Collected:06/15/21 11:32 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 16:26 87-68-306/22/21 10:5911.6 1
2-Hexanone ND ug/kg 06/22/21 16:26 591-78-606/22/21 10:5958.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 16:26 98-82-806/22/21 10:595.8 1
p-Isopropyltoluene ND ug/kg 06/22/21 16:26 99-87-606/22/21 10:595.8 1
Methylene Chloride ND ug/kg 06/22/21 16:26 75-09-206/22/21 10:5923.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 16:26 108-10-106/22/21 10:5958.0 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 16:26 1634-04-406/22/21 10:595.8 1
Naphthalene ND ug/kg 06/22/21 16:26 91-20-3 v206/22/21 10:595.8 1
n-Propylbenzene ND ug/kg 06/22/21 16:26 103-65-106/22/21 10:595.8 1
Styrene ND ug/kg 06/22/21 16:26 100-42-506/22/21 10:595.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 16:26 630-20-606/22/21 10:595.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 16:26 79-34-506/22/21 10:595.8 1
Tetrachloroethene ND ug/kg 06/22/21 16:26 127-18-406/22/21 10:595.8 1
Toluene ND ug/kg 06/22/21 16:26 108-88-306/22/21 10:595.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 16:26 87-61-606/22/21 10:595.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 16:26 120-82-106/22/21 10:595.8 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 16:26 71-55-606/22/21 10:595.8 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 16:26 79-00-506/22/21 10:595.8 1
Trichloroethene ND ug/kg 06/22/21 16:26 79-01-606/22/21 10:595.8 1
Trichlorofluoromethane ND ug/kg 06/22/21 16:26 75-69-406/22/21 10:595.8 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 16:26 96-18-406/22/21 10:595.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 16:26 95-63-606/22/21 10:595.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 16:26 108-67-806/22/21 10:595.8 1
Vinyl acetate ND ug/kg 06/22/21 16:26 108-05-406/22/21 10:5958.0 1
Vinyl chloride ND ug/kg 06/22/21 16:26 75-01-406/22/21 10:5911.6 1
Xylene (Total)ND ug/kg 06/22/21 16:26 1330-20-706/22/21 10:5911.6 1
m&p-Xylene ND ug/kg 06/22/21 16:26 179601-23-106/22/21 10:5911.6 1
o-Xylene ND ug/kg 06/22/21 16:26 95-47-606/22/21 10:595.8 1
Surrogates
Toluene-d8 (S)104 %06/22/21 16:26 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)95 %06/22/21 16:26 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)108 %06/22/21 16:26 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.8 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-4 Lab ID:92545119004 Collected:06/15/21 11:35 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 14:5306/21/21 10:2313.7 1
Surrogates
4-Bromofluorobenzene (S)99 %06/23/21 14:53 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 16:44 67-64-106/22/21 10:591251
Benzene ND ug/kg 06/22/21 16:44 71-43-206/22/21 10:596.2 1
Bromobenzene ND ug/kg 06/22/21 16:44 108-86-106/22/21 10:596.2 1
Bromochloromethane ND ug/kg 06/22/21 16:44 74-97-506/22/21 10:596.2 1
Bromodichloromethane ND ug/kg 06/22/21 16:44 75-27-406/22/21 10:596.2 1
Bromoform ND ug/kg 06/22/21 16:44 75-25-206/22/21 10:596.2 1
Bromomethane ND ug/kg 06/22/21 16:44 74-83-9 IK,L1,v106/22/21 10:5912.5 1
2-Butanone (MEK)ND ug/kg 06/22/21 16:44 78-93-306/22/21 10:591251
n-Butylbenzene ND ug/kg 06/22/21 16:44 104-51-806/22/21 10:596.2 1
sec-Butylbenzene ND ug/kg 06/22/21 16:44 135-98-806/22/21 10:596.2 1
tert-Butylbenzene ND ug/kg 06/22/21 16:44 98-06-6 v206/22/21 10:596.2 1
Carbon tetrachloride ND ug/kg 06/22/21 16:44 56-23-506/22/21 10:596.2 1
Chlorobenzene ND ug/kg 06/22/21 16:44 108-90-706/22/21 10:596.2 1
Chloroethane ND ug/kg 06/22/21 16:44 75-00-306/22/21 10:5912.5 1
Chloroform ND ug/kg 06/22/21 16:44 67-66-306/22/21 10:596.2 1
Chloromethane ND ug/kg 06/22/21 16:44 74-87-306/22/21 10:5912.5 1
2-Chlorotoluene ND ug/kg 06/22/21 16:44 95-49-806/22/21 10:596.2 1
4-Chlorotoluene ND ug/kg 06/22/21 16:44 106-43-406/22/21 10:596.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 16:44 96-12-806/22/21 10:596.2 1
Dibromochloromethane ND ug/kg 06/22/21 16:44 124-48-106/22/21 10:596.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 16:44 106-93-406/22/21 10:596.2 1
Dibromomethane ND ug/kg 06/22/21 16:44 74-95-306/22/21 10:596.2 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 16:44 95-50-106/22/21 10:596.2 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 16:44 541-73-106/22/21 10:596.2 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 16:44 106-46-706/22/21 10:596.2 1
Dichlorodifluoromethane ND ug/kg 06/22/21 16:44 75-71-8 v206/22/21 10:5912.5 1
1,1-Dichloroethane ND ug/kg 06/22/21 16:44 75-34-306/22/21 10:596.2 1
1,2-Dichloroethane ND ug/kg 06/22/21 16:44 107-06-206/22/21 10:596.2 1
1,1-Dichloroethene ND ug/kg 06/22/21 16:44 75-35-406/22/21 10:596.2 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 16:44 156-59-206/22/21 10:596.2 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 16:44 156-60-506/22/21 10:596.2 1
1,2-Dichloropropane ND ug/kg 06/22/21 16:44 78-87-506/22/21 10:596.2 1
1,3-Dichloropropane ND ug/kg 06/22/21 16:44 142-28-906/22/21 10:596.2 1
2,2-Dichloropropane ND ug/kg 06/22/21 16:44 594-20-706/22/21 10:596.2 1
1,1-Dichloropropene ND ug/kg 06/22/21 16:44 563-58-606/22/21 10:596.2 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 16:44 10061-01-506/22/21 10:596.2 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 16:44 10061-02-606/22/21 10:596.2 1
Diisopropyl ether ND ug/kg 06/22/21 16:44 108-20-306/22/21 10:596.2 1
Ethylbenzene ND ug/kg 06/22/21 16:44 100-41-406/22/21 10:596.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-4 Lab ID:92545119004 Collected:06/15/21 11:35 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 16:44 87-68-306/22/21 10:5912.5 1
2-Hexanone ND ug/kg 06/22/21 16:44 591-78-606/22/21 10:5962.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 16:44 98-82-806/22/21 10:596.2 1
p-Isopropyltoluene ND ug/kg 06/22/21 16:44 99-87-606/22/21 10:596.2 1
Methylene Chloride ND ug/kg 06/22/21 16:44 75-09-206/22/21 10:5924.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 16:44 108-10-106/22/21 10:5962.3 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 16:44 1634-04-406/22/21 10:596.2 1
Naphthalene ND ug/kg 06/22/21 16:44 91-20-3 v206/22/21 10:596.2 1
n-Propylbenzene ND ug/kg 06/22/21 16:44 103-65-106/22/21 10:596.2 1
Styrene ND ug/kg 06/22/21 16:44 100-42-506/22/21 10:596.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 16:44 630-20-606/22/21 10:596.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 16:44 79-34-506/22/21 10:596.2 1
Tetrachloroethene ND ug/kg 06/22/21 16:44 127-18-406/22/21 10:596.2 1
Toluene 10.6 ug/kg 06/22/21 16:44 108-88-3 C706/22/21 10:596.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 16:44 87-61-606/22/21 10:596.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 16:44 120-82-106/22/21 10:596.2 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 16:44 71-55-606/22/21 10:596.2 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 16:44 79-00-506/22/21 10:596.2 1
Trichloroethene ND ug/kg 06/22/21 16:44 79-01-606/22/21 10:596.2 1
Trichlorofluoromethane ND ug/kg 06/22/21 16:44 75-69-406/22/21 10:596.2 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 16:44 96-18-406/22/21 10:596.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 16:44 95-63-606/22/21 10:596.2 1
1,3,5-Trimethylbenzene 7.2 ug/kg 06/22/21 16:44 108-67-806/22/21 10:596.2 1
Vinyl acetate ND ug/kg 06/22/21 16:44 108-05-406/22/21 10:5962.3 1
Vinyl chloride ND ug/kg 06/22/21 16:44 75-01-406/22/21 10:5912.5 1
Xylene (Total)28.3 ug/kg 06/22/21 16:44 1330-20-706/22/21 10:5912.5 1
m&p-Xylene 16.3 ug/kg 06/22/21 16:44 179601-23-106/22/21 10:5912.5 1
o-Xylene 12.0 ug/kg 06/22/21 16:44 95-47-606/22/21 10:596.2 1
Surrogates
Toluene-d8 (S)103 %06/22/21 16:44 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)96 %06/22/21 16:44 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)108 %06/22/21 16:44 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-5 Lab ID:92545119005 Collected:06/15/21 11:38 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 15:4906/21/21 10:237.0 1
Surrogates
4-Bromofluorobenzene (S)100 %06/23/21 15:49 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 17:01 67-64-106/22/21 10:591141
Benzene ND ug/kg 06/22/21 17:01 71-43-206/22/21 10:595.7 1
Bromobenzene ND ug/kg 06/22/21 17:01 108-86-106/22/21 10:595.7 1
Bromochloromethane ND ug/kg 06/22/21 17:01 74-97-506/22/21 10:595.7 1
Bromodichloromethane ND ug/kg 06/22/21 17:01 75-27-406/22/21 10:595.7 1
Bromoform ND ug/kg 06/22/21 17:01 75-25-206/22/21 10:595.7 1
Bromomethane ND ug/kg 06/22/21 17:01 74-83-9 IK,L1,v106/22/21 10:5911.4 1
2-Butanone (MEK)ND ug/kg 06/22/21 17:01 78-93-306/22/21 10:591141
n-Butylbenzene ND ug/kg 06/22/21 17:01 104-51-806/22/21 10:595.7 1
sec-Butylbenzene ND ug/kg 06/22/21 17:01 135-98-806/22/21 10:595.7 1
tert-Butylbenzene ND ug/kg 06/22/21 17:01 98-06-6 v206/22/21 10:595.7 1
Carbon tetrachloride ND ug/kg 06/22/21 17:01 56-23-506/22/21 10:595.7 1
Chlorobenzene ND ug/kg 06/22/21 17:01 108-90-706/22/21 10:595.7 1
Chloroethane ND ug/kg 06/22/21 17:01 75-00-306/22/21 10:5911.4 1
Chloroform ND ug/kg 06/22/21 17:01 67-66-306/22/21 10:595.7 1
Chloromethane ND ug/kg 06/22/21 17:01 74-87-306/22/21 10:5911.4 1
2-Chlorotoluene ND ug/kg 06/22/21 17:01 95-49-806/22/21 10:595.7 1
4-Chlorotoluene ND ug/kg 06/22/21 17:01 106-43-406/22/21 10:595.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 17:01 96-12-806/22/21 10:595.7 1
Dibromochloromethane ND ug/kg 06/22/21 17:01 124-48-106/22/21 10:595.7 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 17:01 106-93-406/22/21 10:595.7 1
Dibromomethane ND ug/kg 06/22/21 17:01 74-95-306/22/21 10:595.7 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 17:01 95-50-106/22/21 10:595.7 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 17:01 541-73-106/22/21 10:595.7 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 17:01 106-46-706/22/21 10:595.7 1
Dichlorodifluoromethane ND ug/kg 06/22/21 17:01 75-71-8 v206/22/21 10:5911.4 1
1,1-Dichloroethane ND ug/kg 06/22/21 17:01 75-34-306/22/21 10:595.7 1
1,2-Dichloroethane ND ug/kg 06/22/21 17:01 107-06-206/22/21 10:595.7 1
1,1-Dichloroethene ND ug/kg 06/22/21 17:01 75-35-406/22/21 10:595.7 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 17:01 156-59-206/22/21 10:595.7 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 17:01 156-60-506/22/21 10:595.7 1
1,2-Dichloropropane ND ug/kg 06/22/21 17:01 78-87-506/22/21 10:595.7 1
1,3-Dichloropropane ND ug/kg 06/22/21 17:01 142-28-906/22/21 10:595.7 1
2,2-Dichloropropane ND ug/kg 06/22/21 17:01 594-20-706/22/21 10:595.7 1
1,1-Dichloropropene ND ug/kg 06/22/21 17:01 563-58-606/22/21 10:595.7 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 17:01 10061-01-506/22/21 10:595.7 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 17:01 10061-02-606/22/21 10:595.7 1
Diisopropyl ether ND ug/kg 06/22/21 17:01 108-20-306/22/21 10:595.7 1
Ethylbenzene ND ug/kg 06/22/21 17:01 100-41-406/22/21 10:595.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-5 Lab ID:92545119005 Collected:06/15/21 11:38 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 17:01 87-68-306/22/21 10:5911.4 1
2-Hexanone ND ug/kg 06/22/21 17:01 591-78-606/22/21 10:5957.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 17:01 98-82-806/22/21 10:595.7 1
p-Isopropyltoluene ND ug/kg 06/22/21 17:01 99-87-606/22/21 10:595.7 1
Methylene Chloride ND ug/kg 06/22/21 17:01 75-09-206/22/21 10:5922.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 17:01 108-10-106/22/21 10:5957.2 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 17:01 1634-04-406/22/21 10:595.7 1
Naphthalene ND ug/kg 06/22/21 17:01 91-20-3 v206/22/21 10:595.7 1
n-Propylbenzene ND ug/kg 06/22/21 17:01 103-65-106/22/21 10:595.7 1
Styrene ND ug/kg 06/22/21 17:01 100-42-506/22/21 10:595.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 17:01 630-20-606/22/21 10:595.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 17:01 79-34-506/22/21 10:595.7 1
Tetrachloroethene ND ug/kg 06/22/21 17:01 127-18-406/22/21 10:595.7 1
Toluene 7.3 ug/kg 06/22/21 17:01 108-88-3 C706/22/21 10:595.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 17:01 87-61-606/22/21 10:595.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 17:01 120-82-106/22/21 10:595.7 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 17:01 71-55-606/22/21 10:595.7 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 17:01 79-00-506/22/21 10:595.7 1
Trichloroethene ND ug/kg 06/22/21 17:01 79-01-606/22/21 10:595.7 1
Trichlorofluoromethane ND ug/kg 06/22/21 17:01 75-69-406/22/21 10:595.7 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 17:01 96-18-406/22/21 10:595.7 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 17:01 95-63-606/22/21 10:595.7 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 17:01 108-67-806/22/21 10:595.7 1
Vinyl acetate ND ug/kg 06/22/21 17:01 108-05-406/22/21 10:5957.2 1
Vinyl chloride ND ug/kg 06/22/21 17:01 75-01-406/22/21 10:5911.4 1
Xylene (Total)ND ug/kg 06/22/21 17:01 1330-20-706/22/21 10:5911.4 1
m&p-Xylene ND ug/kg 06/22/21 17:01 179601-23-106/22/21 10:5911.4 1
o-Xylene ND ug/kg 06/22/21 17:01 95-47-606/22/21 10:595.7 1
Surrogates
Toluene-d8 (S)103 %06/22/21 17:01 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)98 %06/22/21 17:01 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)110 %06/22/21 17:01 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.4 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-6 Lab ID:92545119006 Collected:06/15/21 11:41 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 16:1706/21/21 10:237.1 1
Surrogates
4-Bromofluorobenzene (S)97 %06/23/21 16:17 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 17:19 67-64-106/22/21 10:591131
Benzene ND ug/kg 06/22/21 17:19 71-43-206/22/21 10:595.6 1
Bromobenzene ND ug/kg 06/22/21 17:19 108-86-106/22/21 10:595.6 1
Bromochloromethane ND ug/kg 06/22/21 17:19 74-97-506/22/21 10:595.6 1
Bromodichloromethane ND ug/kg 06/22/21 17:19 75-27-406/22/21 10:595.6 1
Bromoform ND ug/kg 06/22/21 17:19 75-25-206/22/21 10:595.6 1
Bromomethane ND ug/kg 06/22/21 17:19 74-83-9 IK,L1,v106/22/21 10:5911.3 1
2-Butanone (MEK)ND ug/kg 06/22/21 17:19 78-93-306/22/21 10:591131
n-Butylbenzene ND ug/kg 06/22/21 17:19 104-51-806/22/21 10:595.6 1
sec-Butylbenzene ND ug/kg 06/22/21 17:19 135-98-806/22/21 10:595.6 1
tert-Butylbenzene ND ug/kg 06/22/21 17:19 98-06-6 v206/22/21 10:595.6 1
Carbon tetrachloride ND ug/kg 06/22/21 17:19 56-23-506/22/21 10:595.6 1
Chlorobenzene ND ug/kg 06/22/21 17:19 108-90-706/22/21 10:595.6 1
Chloroethane ND ug/kg 06/22/21 17:19 75-00-306/22/21 10:5911.3 1
Chloroform ND ug/kg 06/22/21 17:19 67-66-306/22/21 10:595.6 1
Chloromethane ND ug/kg 06/22/21 17:19 74-87-306/22/21 10:5911.3 1
2-Chlorotoluene ND ug/kg 06/22/21 17:19 95-49-806/22/21 10:595.6 1
4-Chlorotoluene ND ug/kg 06/22/21 17:19 106-43-406/22/21 10:595.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 17:19 96-12-806/22/21 10:595.6 1
Dibromochloromethane ND ug/kg 06/22/21 17:19 124-48-106/22/21 10:595.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 17:19 106-93-406/22/21 10:595.6 1
Dibromomethane ND ug/kg 06/22/21 17:19 74-95-306/22/21 10:595.6 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 17:19 95-50-106/22/21 10:595.6 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 17:19 541-73-106/22/21 10:595.6 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 17:19 106-46-706/22/21 10:595.6 1
Dichlorodifluoromethane ND ug/kg 06/22/21 17:19 75-71-8 v206/22/21 10:5911.3 1
1,1-Dichloroethane ND ug/kg 06/22/21 17:19 75-34-306/22/21 10:595.6 1
1,2-Dichloroethane ND ug/kg 06/22/21 17:19 107-06-206/22/21 10:595.6 1
1,1-Dichloroethene ND ug/kg 06/22/21 17:19 75-35-406/22/21 10:595.6 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 17:19 156-59-206/22/21 10:595.6 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 17:19 156-60-506/22/21 10:595.6 1
1,2-Dichloropropane ND ug/kg 06/22/21 17:19 78-87-506/22/21 10:595.6 1
1,3-Dichloropropane ND ug/kg 06/22/21 17:19 142-28-906/22/21 10:595.6 1
2,2-Dichloropropane ND ug/kg 06/22/21 17:19 594-20-706/22/21 10:595.6 1
1,1-Dichloropropene ND ug/kg 06/22/21 17:19 563-58-606/22/21 10:595.6 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 17:19 10061-01-506/22/21 10:595.6 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 17:19 10061-02-606/22/21 10:595.6 1
Diisopropyl ether ND ug/kg 06/22/21 17:19 108-20-306/22/21 10:595.6 1
Ethylbenzene ND ug/kg 06/22/21 17:19 100-41-406/22/21 10:595.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-6 Lab ID:92545119006 Collected:06/15/21 11:41 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 17:19 87-68-306/22/21 10:5911.3 1
2-Hexanone ND ug/kg 06/22/21 17:19 591-78-606/22/21 10:5956.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 17:19 98-82-806/22/21 10:595.6 1
p-Isopropyltoluene ND ug/kg 06/22/21 17:19 99-87-606/22/21 10:595.6 1
Methylene Chloride ND ug/kg 06/22/21 17:19 75-09-206/22/21 10:5922.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 17:19 108-10-106/22/21 10:5956.4 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 17:19 1634-04-406/22/21 10:595.6 1
Naphthalene ND ug/kg 06/22/21 17:19 91-20-3 v206/22/21 10:595.6 1
n-Propylbenzene ND ug/kg 06/22/21 17:19 103-65-106/22/21 10:595.6 1
Styrene ND ug/kg 06/22/21 17:19 100-42-506/22/21 10:595.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 17:19 630-20-606/22/21 10:595.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 17:19 79-34-506/22/21 10:595.6 1
Tetrachloroethene ND ug/kg 06/22/21 17:19 127-18-406/22/21 10:595.6 1
Toluene 13.1 ug/kg 06/22/21 17:19 108-88-3 C706/22/21 10:595.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 17:19 87-61-606/22/21 10:595.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 17:19 120-82-106/22/21 10:595.6 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 17:19 71-55-606/22/21 10:595.6 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 17:19 79-00-506/22/21 10:595.6 1
Trichloroethene ND ug/kg 06/22/21 17:19 79-01-606/22/21 10:595.6 1
Trichlorofluoromethane ND ug/kg 06/22/21 17:19 75-69-406/22/21 10:595.6 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 17:19 96-18-406/22/21 10:595.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 17:19 95-63-606/22/21 10:595.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 17:19 108-67-806/22/21 10:595.6 1
Vinyl acetate ND ug/kg 06/22/21 17:19 108-05-406/22/21 10:5956.4 1
Vinyl chloride ND ug/kg 06/22/21 17:19 75-01-406/22/21 10:5911.3 1
Xylene (Total)22.8 ug/kg 06/22/21 17:19 1330-20-706/22/21 10:5911.3 1
m&p-Xylene 13.3 ug/kg 06/22/21 17:19 179601-23-106/22/21 10:5911.3 1
o-Xylene 9.5 ug/kg 06/22/21 17:19 95-47-606/22/21 10:595.6 1
Surrogates
Toluene-d8 (S)103 %06/22/21 17:19 2037-26-506/22/21 10:5970-130 1
4-Bromofluorobenzene (S)97 %06/22/21 17:19 460-00-406/22/21 10:5969-134 1
1,2-Dichloroethane-d4 (S)110 %06/22/21 17:19 17060-07-006/22/21 10:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.9 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-7 Lab ID:92545119007 Collected:06/15/21 11:43 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 16:4506/21/21 10:236.8 1
Surrogates
4-Bromofluorobenzene (S)94 %06/23/21 16:45 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 17:37 67-64-106/22/21 08:531081
Benzene ND ug/kg 06/22/21 17:37 71-43-206/22/21 08:535.4 1
Bromobenzene ND ug/kg 06/22/21 17:37 108-86-106/22/21 08:535.4 1
Bromochloromethane ND ug/kg 06/22/21 17:37 74-97-506/22/21 08:535.4 1
Bromodichloromethane ND ug/kg 06/22/21 17:37 75-27-406/22/21 08:535.4 1
Bromoform ND ug/kg 06/22/21 17:37 75-25-206/22/21 08:535.4 1
Bromomethane ND ug/kg 06/22/21 17:37 74-83-9 IK,L1,v106/22/21 08:5310.8 1
2-Butanone (MEK)ND ug/kg 06/22/21 17:37 78-93-306/22/21 08:531081
n-Butylbenzene ND ug/kg 06/22/21 17:37 104-51-806/22/21 08:535.4 1
sec-Butylbenzene ND ug/kg 06/22/21 17:37 135-98-806/22/21 08:535.4 1
tert-Butylbenzene ND ug/kg 06/22/21 17:37 98-06-6 v206/22/21 08:535.4 1
Carbon tetrachloride ND ug/kg 06/22/21 17:37 56-23-506/22/21 08:535.4 1
Chlorobenzene ND ug/kg 06/22/21 17:37 108-90-706/22/21 08:535.4 1
Chloroethane ND ug/kg 06/22/21 17:37 75-00-306/22/21 08:5310.8 1
Chloroform ND ug/kg 06/22/21 17:37 67-66-306/22/21 08:535.4 1
Chloromethane ND ug/kg 06/22/21 17:37 74-87-306/22/21 08:5310.8 1
2-Chlorotoluene ND ug/kg 06/22/21 17:37 95-49-806/22/21 08:535.4 1
4-Chlorotoluene ND ug/kg 06/22/21 17:37 106-43-406/22/21 08:535.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 17:37 96-12-806/22/21 08:535.4 1
Dibromochloromethane ND ug/kg 06/22/21 17:37 124-48-106/22/21 08:535.4 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 17:37 106-93-406/22/21 08:535.4 1
Dibromomethane ND ug/kg 06/22/21 17:37 74-95-306/22/21 08:535.4 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 17:37 95-50-106/22/21 08:535.4 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 17:37 541-73-106/22/21 08:535.4 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 17:37 106-46-706/22/21 08:535.4 1
Dichlorodifluoromethane ND ug/kg 06/22/21 17:37 75-71-8 v206/22/21 08:5310.8 1
1,1-Dichloroethane ND ug/kg 06/22/21 17:37 75-34-306/22/21 08:535.4 1
1,2-Dichloroethane ND ug/kg 06/22/21 17:37 107-06-206/22/21 08:535.4 1
1,1-Dichloroethene ND ug/kg 06/22/21 17:37 75-35-406/22/21 08:535.4 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 17:37 156-59-206/22/21 08:535.4 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 17:37 156-60-506/22/21 08:535.4 1
1,2-Dichloropropane ND ug/kg 06/22/21 17:37 78-87-506/22/21 08:535.4 1
1,3-Dichloropropane ND ug/kg 06/22/21 17:37 142-28-906/22/21 08:535.4 1
2,2-Dichloropropane ND ug/kg 06/22/21 17:37 594-20-706/22/21 08:535.4 1
1,1-Dichloropropene ND ug/kg 06/22/21 17:37 563-58-606/22/21 08:535.4 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 17:37 10061-01-506/22/21 08:535.4 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 17:37 10061-02-606/22/21 08:535.4 1
Diisopropyl ether ND ug/kg 06/22/21 17:37 108-20-306/22/21 08:535.4 1
Ethylbenzene ND ug/kg 06/22/21 17:37 100-41-406/22/21 08:535.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-7 Lab ID:92545119007 Collected:06/15/21 11:43 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 17:37 87-68-306/22/21 08:5310.8 1
2-Hexanone ND ug/kg 06/22/21 17:37 591-78-606/22/21 08:5354.1 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 17:37 98-82-806/22/21 08:535.4 1
p-Isopropyltoluene ND ug/kg 06/22/21 17:37 99-87-606/22/21 08:535.4 1
Methylene Chloride ND ug/kg 06/22/21 17:37 75-09-206/22/21 08:5321.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 17:37 108-10-106/22/21 08:5354.1 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 17:37 1634-04-406/22/21 08:535.4 1
Naphthalene ND ug/kg 06/22/21 17:37 91-20-3 v206/22/21 08:535.4 1
n-Propylbenzene ND ug/kg 06/22/21 17:37 103-65-106/22/21 08:535.4 1
Styrene ND ug/kg 06/22/21 17:37 100-42-506/22/21 08:535.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 17:37 630-20-606/22/21 08:535.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 17:37 79-34-506/22/21 08:535.4 1
Tetrachloroethene ND ug/kg 06/22/21 17:37 127-18-406/22/21 08:535.4 1
Toluene ND ug/kg 06/22/21 17:37 108-88-306/22/21 08:535.4 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 17:37 87-61-606/22/21 08:535.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 17:37 120-82-106/22/21 08:535.4 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 17:37 71-55-606/22/21 08:535.4 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 17:37 79-00-506/22/21 08:535.4 1
Trichloroethene ND ug/kg 06/22/21 17:37 79-01-606/22/21 08:535.4 1
Trichlorofluoromethane ND ug/kg 06/22/21 17:37 75-69-406/22/21 08:535.4 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 17:37 96-18-406/22/21 08:535.4 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 17:37 95-63-606/22/21 08:535.4 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 17:37 108-67-806/22/21 08:535.4 1
Vinyl acetate ND ug/kg 06/22/21 17:37 108-05-406/22/21 08:5354.1 1
Vinyl chloride ND ug/kg 06/22/21 17:37 75-01-406/22/21 08:5310.8 1
Xylene (Total)ND ug/kg 06/22/21 17:37 1330-20-706/22/21 08:5310.8 1
m&p-Xylene ND ug/kg 06/22/21 17:37 179601-23-106/22/21 08:5310.8 1
o-Xylene ND ug/kg 06/22/21 17:37 95-47-606/22/21 08:535.4 1
Surrogates
Toluene-d8 (S)104 %06/22/21 17:37 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)98 %06/22/21 17:37 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)112 %06/22/21 17:37 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.1 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-8 Lab ID:92545119008 Collected:06/15/21 11:45 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 17:1306/21/21 10:237.1 1
Surrogates
4-Bromofluorobenzene (S)94 %06/23/21 17:13 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 18:12 67-64-106/22/21 08:531101
Benzene ND ug/kg 06/22/21 18:12 71-43-206/22/21 08:535.5 1
Bromobenzene ND ug/kg 06/22/21 18:12 108-86-106/22/21 08:535.5 1
Bromochloromethane ND ug/kg 06/22/21 18:12 74-97-506/22/21 08:535.5 1
Bromodichloromethane ND ug/kg 06/22/21 18:12 75-27-406/22/21 08:535.5 1
Bromoform ND ug/kg 06/22/21 18:12 75-25-206/22/21 08:535.5 1
Bromomethane ND ug/kg 06/22/21 18:12 74-83-9 IK,L1,v106/22/21 08:5311.0 1
2-Butanone (MEK)ND ug/kg 06/22/21 18:12 78-93-306/22/21 08:531101
n-Butylbenzene ND ug/kg 06/22/21 18:12 104-51-806/22/21 08:535.5 1
sec-Butylbenzene ND ug/kg 06/22/21 18:12 135-98-806/22/21 08:535.5 1
tert-Butylbenzene ND ug/kg 06/22/21 18:12 98-06-6 v206/22/21 08:535.5 1
Carbon tetrachloride ND ug/kg 06/22/21 18:12 56-23-506/22/21 08:535.5 1
Chlorobenzene ND ug/kg 06/22/21 18:12 108-90-706/22/21 08:535.5 1
Chloroethane ND ug/kg 06/22/21 18:12 75-00-306/22/21 08:5311.0 1
Chloroform ND ug/kg 06/22/21 18:12 67-66-306/22/21 08:535.5 1
Chloromethane ND ug/kg 06/22/21 18:12 74-87-306/22/21 08:5311.0 1
2-Chlorotoluene ND ug/kg 06/22/21 18:12 95-49-806/22/21 08:535.5 1
4-Chlorotoluene ND ug/kg 06/22/21 18:12 106-43-406/22/21 08:535.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 18:12 96-12-806/22/21 08:535.5 1
Dibromochloromethane ND ug/kg 06/22/21 18:12 124-48-106/22/21 08:535.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 18:12 106-93-406/22/21 08:535.5 1
Dibromomethane ND ug/kg 06/22/21 18:12 74-95-306/22/21 08:535.5 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 18:12 95-50-106/22/21 08:535.5 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 18:12 541-73-106/22/21 08:535.5 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 18:12 106-46-706/22/21 08:535.5 1
Dichlorodifluoromethane ND ug/kg 06/22/21 18:12 75-71-8 v2,v306/22/21 08:5311.0 1
1,1-Dichloroethane ND ug/kg 06/22/21 18:12 75-34-306/22/21 08:535.5 1
1,2-Dichloroethane ND ug/kg 06/22/21 18:12 107-06-206/22/21 08:535.5 1
1,1-Dichloroethene ND ug/kg 06/22/21 18:12 75-35-406/22/21 08:535.5 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 18:12 156-59-206/22/21 08:535.5 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 18:12 156-60-506/22/21 08:535.5 1
1,2-Dichloropropane ND ug/kg 06/22/21 18:12 78-87-506/22/21 08:535.5 1
1,3-Dichloropropane ND ug/kg 06/22/21 18:12 142-28-906/22/21 08:535.5 1
2,2-Dichloropropane ND ug/kg 06/22/21 18:12 594-20-706/22/21 08:535.5 1
1,1-Dichloropropene ND ug/kg 06/22/21 18:12 563-58-606/22/21 08:535.5 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 18:12 10061-01-506/22/21 08:535.5 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 18:12 10061-02-606/22/21 08:535.5 1
Diisopropyl ether ND ug/kg 06/22/21 18:12 108-20-306/22/21 08:535.5 1
Ethylbenzene ND ug/kg 06/22/21 18:12 100-41-406/22/21 08:535.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-8 Lab ID:92545119008 Collected:06/15/21 11:45 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 18:12 87-68-306/22/21 08:5311.0 1
2-Hexanone ND ug/kg 06/22/21 18:12 591-78-606/22/21 08:5354.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 18:12 98-82-806/22/21 08:535.5 1
p-Isopropyltoluene ND ug/kg 06/22/21 18:12 99-87-606/22/21 08:535.5 1
Methylene Chloride ND ug/kg 06/22/21 18:12 75-09-206/22/21 08:5321.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 18:12 108-10-106/22/21 08:5354.8 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 18:12 1634-04-406/22/21 08:535.5 1
Naphthalene ND ug/kg 06/22/21 18:12 91-20-3 v206/22/21 08:535.5 1
n-Propylbenzene ND ug/kg 06/22/21 18:12 103-65-106/22/21 08:535.5 1
Styrene ND ug/kg 06/22/21 18:12 100-42-506/22/21 08:535.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 18:12 630-20-606/22/21 08:535.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 18:12 79-34-506/22/21 08:535.5 1
Tetrachloroethene ND ug/kg 06/22/21 18:12 127-18-406/22/21 08:535.5 1
Toluene ND ug/kg 06/22/21 18:12 108-88-306/22/21 08:535.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 18:12 87-61-606/22/21 08:535.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 18:12 120-82-106/22/21 08:535.5 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 18:12 71-55-606/22/21 08:535.5 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 18:12 79-00-506/22/21 08:535.5 1
Trichloroethene ND ug/kg 06/22/21 18:12 79-01-606/22/21 08:535.5 1
Trichlorofluoromethane ND ug/kg 06/22/21 18:12 75-69-4 M106/22/21 08:535.5 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 18:12 96-18-406/22/21 08:535.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 18:12 95-63-606/22/21 08:535.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 18:12 108-67-806/22/21 08:535.5 1
Vinyl acetate ND ug/kg 06/22/21 18:12 108-05-406/22/21 08:5354.8 1
Vinyl chloride ND ug/kg 06/22/21 18:12 75-01-406/22/21 08:5311.0 1
Xylene (Total)ND ug/kg 06/22/21 18:12 1330-20-706/22/21 08:5311.0 1
m&p-Xylene ND ug/kg 06/22/21 18:12 179601-23-106/22/21 08:5311.0 1
o-Xylene ND ug/kg 06/22/21 18:12 95-47-606/22/21 08:535.5 1
Surrogates
Toluene-d8 (S)105 %06/22/21 18:12 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)95 %06/22/21 18:12 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)113 %06/22/21 18:12 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.8 %06/18/21 17:41 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-9 Lab ID:92545119009 Collected:06/15/21 11:47 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 17:4206/21/21 10:236.7 1
Surrogates
4-Bromofluorobenzene (S)94 %06/23/21 17:42 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 18:29 67-64-106/22/21 08:531131
Benzene ND ug/kg 06/22/21 18:29 71-43-206/22/21 08:535.7 1
Bromobenzene ND ug/kg 06/22/21 18:29 108-86-106/22/21 08:535.7 1
Bromochloromethane ND ug/kg 06/22/21 18:29 74-97-506/22/21 08:535.7 1
Bromodichloromethane ND ug/kg 06/22/21 18:29 75-27-406/22/21 08:535.7 1
Bromoform ND ug/kg 06/22/21 18:29 75-25-206/22/21 08:535.7 1
Bromomethane ND ug/kg 06/22/21 18:29 74-83-9 IK,L1,v106/22/21 08:5311.3 1
2-Butanone (MEK)ND ug/kg 06/22/21 18:29 78-93-306/22/21 08:531131
n-Butylbenzene ND ug/kg 06/22/21 18:29 104-51-806/22/21 08:535.7 1
sec-Butylbenzene ND ug/kg 06/22/21 18:29 135-98-806/22/21 08:535.7 1
tert-Butylbenzene ND ug/kg 06/22/21 18:29 98-06-6 v206/22/21 08:535.7 1
Carbon tetrachloride ND ug/kg 06/22/21 18:29 56-23-506/22/21 08:535.7 1
Chlorobenzene ND ug/kg 06/22/21 18:29 108-90-706/22/21 08:535.7 1
Chloroethane ND ug/kg 06/22/21 18:29 75-00-306/22/21 08:5311.3 1
Chloroform ND ug/kg 06/22/21 18:29 67-66-306/22/21 08:535.7 1
Chloromethane ND ug/kg 06/22/21 18:29 74-87-306/22/21 08:5311.3 1
2-Chlorotoluene ND ug/kg 06/22/21 18:29 95-49-806/22/21 08:535.7 1
4-Chlorotoluene ND ug/kg 06/22/21 18:29 106-43-406/22/21 08:535.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 18:29 96-12-806/22/21 08:535.7 1
Dibromochloromethane ND ug/kg 06/22/21 18:29 124-48-106/22/21 08:535.7 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 18:29 106-93-406/22/21 08:535.7 1
Dibromomethane ND ug/kg 06/22/21 18:29 74-95-306/22/21 08:535.7 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 18:29 95-50-106/22/21 08:535.7 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 18:29 541-73-106/22/21 08:535.7 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 18:29 106-46-706/22/21 08:535.7 1
Dichlorodifluoromethane ND ug/kg 06/22/21 18:29 75-71-8 v206/22/21 08:5311.3 1
1,1-Dichloroethane ND ug/kg 06/22/21 18:29 75-34-306/22/21 08:535.7 1
1,2-Dichloroethane ND ug/kg 06/22/21 18:29 107-06-206/22/21 08:535.7 1
1,1-Dichloroethene ND ug/kg 06/22/21 18:29 75-35-406/22/21 08:535.7 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 18:29 156-59-206/22/21 08:535.7 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 18:29 156-60-506/22/21 08:535.7 1
1,2-Dichloropropane ND ug/kg 06/22/21 18:29 78-87-506/22/21 08:535.7 1
1,3-Dichloropropane ND ug/kg 06/22/21 18:29 142-28-906/22/21 08:535.7 1
2,2-Dichloropropane ND ug/kg 06/22/21 18:29 594-20-706/22/21 08:535.7 1
1,1-Dichloropropene ND ug/kg 06/22/21 18:29 563-58-606/22/21 08:535.7 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 18:29 10061-01-506/22/21 08:535.7 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 18:29 10061-02-606/22/21 08:535.7 1
Diisopropyl ether ND ug/kg 06/22/21 18:29 108-20-306/22/21 08:535.7 1
Ethylbenzene ND ug/kg 06/22/21 18:29 100-41-406/22/21 08:535.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-9 Lab ID:92545119009 Collected:06/15/21 11:47 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 18:29 87-68-306/22/21 08:5311.3 1
2-Hexanone ND ug/kg 06/22/21 18:29 591-78-606/22/21 08:5356.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 18:29 98-82-806/22/21 08:535.7 1
p-Isopropyltoluene ND ug/kg 06/22/21 18:29 99-87-606/22/21 08:535.7 1
Methylene Chloride ND ug/kg 06/22/21 18:29 75-09-206/22/21 08:5322.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 18:29 108-10-106/22/21 08:5356.6 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 18:29 1634-04-406/22/21 08:535.7 1
Naphthalene ND ug/kg 06/22/21 18:29 91-20-3 v206/22/21 08:535.7 1
n-Propylbenzene ND ug/kg 06/22/21 18:29 103-65-106/22/21 08:535.7 1
Styrene ND ug/kg 06/22/21 18:29 100-42-506/22/21 08:535.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 18:29 630-20-606/22/21 08:535.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 18:29 79-34-506/22/21 08:535.7 1
Tetrachloroethene ND ug/kg 06/22/21 18:29 127-18-406/22/21 08:535.7 1
Toluene ND ug/kg 06/22/21 18:29 108-88-306/22/21 08:535.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 18:29 87-61-606/22/21 08:535.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 18:29 120-82-106/22/21 08:535.7 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 18:29 71-55-606/22/21 08:535.7 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 18:29 79-00-506/22/21 08:535.7 1
Trichloroethene ND ug/kg 06/22/21 18:29 79-01-606/22/21 08:535.7 1
Trichlorofluoromethane ND ug/kg 06/22/21 18:29 75-69-406/22/21 08:535.7 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 18:29 96-18-406/22/21 08:535.7 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 18:29 95-63-606/22/21 08:535.7 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 18:29 108-67-806/22/21 08:535.7 1
Vinyl acetate ND ug/kg 06/22/21 18:29 108-05-406/22/21 08:5356.6 1
Vinyl chloride ND ug/kg 06/22/21 18:29 75-01-406/22/21 08:5311.3 1
Xylene (Total)ND ug/kg 06/22/21 18:29 1330-20-706/22/21 08:5311.3 1
m&p-Xylene ND ug/kg 06/22/21 18:29 179601-23-106/22/21 08:5311.3 1
o-Xylene ND ug/kg 06/22/21 18:29 95-47-606/22/21 08:535.7 1
Surrogates
Toluene-d8 (S)104 %06/22/21 18:29 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)96 %06/22/21 18:29 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)113 %06/22/21 18:29 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.0 %06/18/21 17:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-10 Lab ID:92545119010 Collected:06/15/21 11:49 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 18:1006/21/21 10:236.7 1
Surrogates
4-Bromofluorobenzene (S)96 %06/23/21 18:10 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 18:47 67-64-106/22/21 08:531051
Benzene ND ug/kg 06/22/21 18:47 71-43-206/22/21 08:535.2 1
Bromobenzene ND ug/kg 06/22/21 18:47 108-86-106/22/21 08:535.2 1
Bromochloromethane ND ug/kg 06/22/21 18:47 74-97-506/22/21 08:535.2 1
Bromodichloromethane ND ug/kg 06/22/21 18:47 75-27-406/22/21 08:535.2 1
Bromoform ND ug/kg 06/22/21 18:47 75-25-206/22/21 08:535.2 1
Bromomethane ND ug/kg 06/22/21 18:47 74-83-9 IK,L1,v106/22/21 08:5310.5 1
2-Butanone (MEK)ND ug/kg 06/22/21 18:47 78-93-306/22/21 08:531051
n-Butylbenzene ND ug/kg 06/22/21 18:47 104-51-806/22/21 08:535.2 1
sec-Butylbenzene ND ug/kg 06/22/21 18:47 135-98-806/22/21 08:535.2 1
tert-Butylbenzene ND ug/kg 06/22/21 18:47 98-06-6 v206/22/21 08:535.2 1
Carbon tetrachloride ND ug/kg 06/22/21 18:47 56-23-506/22/21 08:535.2 1
Chlorobenzene ND ug/kg 06/22/21 18:47 108-90-706/22/21 08:535.2 1
Chloroethane ND ug/kg 06/22/21 18:47 75-00-306/22/21 08:5310.5 1
Chloroform ND ug/kg 06/22/21 18:47 67-66-306/22/21 08:535.2 1
Chloromethane ND ug/kg 06/22/21 18:47 74-87-306/22/21 08:5310.5 1
2-Chlorotoluene ND ug/kg 06/22/21 18:47 95-49-806/22/21 08:535.2 1
4-Chlorotoluene ND ug/kg 06/22/21 18:47 106-43-406/22/21 08:535.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 18:47 96-12-806/22/21 08:535.2 1
Dibromochloromethane ND ug/kg 06/22/21 18:47 124-48-106/22/21 08:535.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 18:47 106-93-406/22/21 08:535.2 1
Dibromomethane ND ug/kg 06/22/21 18:47 74-95-306/22/21 08:535.2 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 18:47 95-50-106/22/21 08:535.2 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 18:47 541-73-106/22/21 08:535.2 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 18:47 106-46-706/22/21 08:535.2 1
Dichlorodifluoromethane ND ug/kg 06/22/21 18:47 75-71-8 v206/22/21 08:5310.5 1
1,1-Dichloroethane ND ug/kg 06/22/21 18:47 75-34-306/22/21 08:535.2 1
1,2-Dichloroethane ND ug/kg 06/22/21 18:47 107-06-206/22/21 08:535.2 1
1,1-Dichloroethene ND ug/kg 06/22/21 18:47 75-35-406/22/21 08:535.2 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 18:47 156-59-206/22/21 08:535.2 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 18:47 156-60-506/22/21 08:535.2 1
1,2-Dichloropropane ND ug/kg 06/22/21 18:47 78-87-506/22/21 08:535.2 1
1,3-Dichloropropane ND ug/kg 06/22/21 18:47 142-28-906/22/21 08:535.2 1
2,2-Dichloropropane ND ug/kg 06/22/21 18:47 594-20-706/22/21 08:535.2 1
1,1-Dichloropropene ND ug/kg 06/22/21 18:47 563-58-606/22/21 08:535.2 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 18:47 10061-01-506/22/21 08:535.2 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 18:47 10061-02-606/22/21 08:535.2 1
Diisopropyl ether ND ug/kg 06/22/21 18:47 108-20-306/22/21 08:535.2 1
Ethylbenzene ND ug/kg 06/22/21 18:47 100-41-406/22/21 08:535.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-10 Lab ID:92545119010 Collected:06/15/21 11:49 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 18:47 87-68-306/22/21 08:5310.5 1
2-Hexanone ND ug/kg 06/22/21 18:47 591-78-606/22/21 08:5352.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 18:47 98-82-806/22/21 08:535.2 1
p-Isopropyltoluene ND ug/kg 06/22/21 18:47 99-87-606/22/21 08:535.2 1
Methylene Chloride ND ug/kg 06/22/21 18:47 75-09-206/22/21 08:5320.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 18:47 108-10-106/22/21 08:5352.3 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 18:47 1634-04-406/22/21 08:535.2 1
Naphthalene ND ug/kg 06/22/21 18:47 91-20-3 v206/22/21 08:535.2 1
n-Propylbenzene ND ug/kg 06/22/21 18:47 103-65-106/22/21 08:535.2 1
Styrene ND ug/kg 06/22/21 18:47 100-42-506/22/21 08:535.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 18:47 630-20-606/22/21 08:535.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 18:47 79-34-506/22/21 08:535.2 1
Tetrachloroethene ND ug/kg 06/22/21 18:47 127-18-406/22/21 08:535.2 1
Toluene ND ug/kg 06/22/21 18:47 108-88-306/22/21 08:535.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 18:47 87-61-606/22/21 08:535.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 18:47 120-82-106/22/21 08:535.2 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 18:47 71-55-606/22/21 08:535.2 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 18:47 79-00-506/22/21 08:535.2 1
Trichloroethene ND ug/kg 06/22/21 18:47 79-01-606/22/21 08:535.2 1
Trichlorofluoromethane ND ug/kg 06/22/21 18:47 75-69-406/22/21 08:535.2 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 18:47 96-18-406/22/21 08:535.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 18:47 95-63-606/22/21 08:535.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 18:47 108-67-806/22/21 08:535.2 1
Vinyl acetate ND ug/kg 06/22/21 18:47 108-05-406/22/21 08:5352.3 1
Vinyl chloride ND ug/kg 06/22/21 18:47 75-01-406/22/21 08:5310.5 1
Xylene (Total)ND ug/kg 06/22/21 18:47 1330-20-706/22/21 08:5310.5 1
m&p-Xylene ND ug/kg 06/22/21 18:47 179601-23-106/22/21 08:5310.5 1
o-Xylene ND ug/kg 06/22/21 18:47 95-47-606/22/21 08:535.2 1
Surrogates
Toluene-d8 (S)103 %06/22/21 18:47 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)98 %06/22/21 18:47 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)113 %06/22/21 18:47 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.0 %06/18/21 17:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-11 Lab ID:92545119011 Collected:06/15/21 11:51 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/24/21 07:4606/21/21 10:239.2 1
Surrogates
4-Bromofluorobenzene (S)97 %06/24/21 07:46 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 19:04 67-64-106/22/21 08:531101
Benzene ND ug/kg 06/22/21 19:04 71-43-206/22/21 08:535.5 1
Bromobenzene ND ug/kg 06/22/21 19:04 108-86-106/22/21 08:535.5 1
Bromochloromethane ND ug/kg 06/22/21 19:04 74-97-506/22/21 08:535.5 1
Bromodichloromethane ND ug/kg 06/22/21 19:04 75-27-406/22/21 08:535.5 1
Bromoform ND ug/kg 06/22/21 19:04 75-25-206/22/21 08:535.5 1
Bromomethane ND ug/kg 06/22/21 19:04 74-83-9 IK,L1,v106/22/21 08:5311.0 1
2-Butanone (MEK)ND ug/kg 06/22/21 19:04 78-93-306/22/21 08:531101
n-Butylbenzene ND ug/kg 06/22/21 19:04 104-51-806/22/21 08:535.5 1
sec-Butylbenzene ND ug/kg 06/22/21 19:04 135-98-806/22/21 08:535.5 1
tert-Butylbenzene ND ug/kg 06/22/21 19:04 98-06-6 v206/22/21 08:535.5 1
Carbon tetrachloride ND ug/kg 06/22/21 19:04 56-23-506/22/21 08:535.5 1
Chlorobenzene ND ug/kg 06/22/21 19:04 108-90-706/22/21 08:535.5 1
Chloroethane ND ug/kg 06/22/21 19:04 75-00-306/22/21 08:5311.0 1
Chloroform ND ug/kg 06/22/21 19:04 67-66-306/22/21 08:535.5 1
Chloromethane ND ug/kg 06/22/21 19:04 74-87-306/22/21 08:5311.0 1
2-Chlorotoluene ND ug/kg 06/22/21 19:04 95-49-806/22/21 08:535.5 1
4-Chlorotoluene ND ug/kg 06/22/21 19:04 106-43-406/22/21 08:535.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 19:04 96-12-806/22/21 08:535.5 1
Dibromochloromethane ND ug/kg 06/22/21 19:04 124-48-106/22/21 08:535.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 19:04 106-93-406/22/21 08:535.5 1
Dibromomethane ND ug/kg 06/22/21 19:04 74-95-306/22/21 08:535.5 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 19:04 95-50-106/22/21 08:535.5 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 19:04 541-73-106/22/21 08:535.5 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 19:04 106-46-706/22/21 08:535.5 1
Dichlorodifluoromethane ND ug/kg 06/22/21 19:04 75-71-8 v206/22/21 08:5311.0 1
1,1-Dichloroethane ND ug/kg 06/22/21 19:04 75-34-306/22/21 08:535.5 1
1,2-Dichloroethane ND ug/kg 06/22/21 19:04 107-06-206/22/21 08:535.5 1
1,1-Dichloroethene ND ug/kg 06/22/21 19:04 75-35-406/22/21 08:535.5 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 19:04 156-59-206/22/21 08:535.5 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 19:04 156-60-506/22/21 08:535.5 1
1,2-Dichloropropane ND ug/kg 06/22/21 19:04 78-87-506/22/21 08:535.5 1
1,3-Dichloropropane ND ug/kg 06/22/21 19:04 142-28-906/22/21 08:535.5 1
2,2-Dichloropropane ND ug/kg 06/22/21 19:04 594-20-706/22/21 08:535.5 1
1,1-Dichloropropene ND ug/kg 06/22/21 19:04 563-58-606/22/21 08:535.5 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 19:04 10061-01-506/22/21 08:535.5 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 19:04 10061-02-606/22/21 08:535.5 1
Diisopropyl ether ND ug/kg 06/22/21 19:04 108-20-306/22/21 08:535.5 1
Ethylbenzene ND ug/kg 06/22/21 19:04 100-41-406/22/21 08:535.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-11 Lab ID:92545119011 Collected:06/15/21 11:51 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 19:04 87-68-306/22/21 08:5311.0 1
2-Hexanone ND ug/kg 06/22/21 19:04 591-78-606/22/21 08:5355.1 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 19:04 98-82-806/22/21 08:535.5 1
p-Isopropyltoluene ND ug/kg 06/22/21 19:04 99-87-606/22/21 08:535.5 1
Methylene Chloride ND ug/kg 06/22/21 19:04 75-09-206/22/21 08:5322.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 19:04 108-10-106/22/21 08:5355.1 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 19:04 1634-04-406/22/21 08:535.5 1
Naphthalene ND ug/kg 06/22/21 19:04 91-20-3 v206/22/21 08:535.5 1
n-Propylbenzene ND ug/kg 06/22/21 19:04 103-65-106/22/21 08:535.5 1
Styrene ND ug/kg 06/22/21 19:04 100-42-506/22/21 08:535.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 19:04 630-20-606/22/21 08:535.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 19:04 79-34-506/22/21 08:535.5 1
Tetrachloroethene ND ug/kg 06/22/21 19:04 127-18-406/22/21 08:535.5 1
Toluene ND ug/kg 06/22/21 19:04 108-88-306/22/21 08:535.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 19:04 87-61-606/22/21 08:535.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 19:04 120-82-106/22/21 08:535.5 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 19:04 71-55-606/22/21 08:535.5 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 19:04 79-00-506/22/21 08:535.5 1
Trichloroethene ND ug/kg 06/22/21 19:04 79-01-606/22/21 08:535.5 1
Trichlorofluoromethane ND ug/kg 06/22/21 19:04 75-69-406/22/21 08:535.5 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 19:04 96-18-406/22/21 08:535.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 19:04 95-63-606/22/21 08:535.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 19:04 108-67-806/22/21 08:535.5 1
Vinyl acetate ND ug/kg 06/22/21 19:04 108-05-406/22/21 08:5355.1 1
Vinyl chloride ND ug/kg 06/22/21 19:04 75-01-406/22/21 08:5311.0 1
Xylene (Total)ND ug/kg 06/22/21 19:04 1330-20-706/22/21 08:5311.0 1
m&p-Xylene ND ug/kg 06/22/21 19:04 179601-23-106/22/21 08:5311.0 1
o-Xylene ND ug/kg 06/22/21 19:04 95-47-606/22/21 08:535.5 1
Surrogates
Toluene-d8 (S)104 %06/22/21 19:04 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)97 %06/22/21 19:04 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)111 %06/22/21 19:04 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.3 %06/18/21 17:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-12 Lab ID:92545119012 Collected:06/15/21 11:54 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 06/22/21 13:3806/21/21 10:195.6 1
Surrogates
n-Pentacosane (S)78 %06/22/21 13:38 629-99-206/21/21 10:1932-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 18:3806/21/21 10:236.7 1
Surrogates
4-Bromofluorobenzene (S)93 %06/23/21 18:38 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/22/21 19:22 67-64-106/22/21 08:531121
Benzene ND ug/kg 06/22/21 19:22 71-43-206/22/21 08:535.6 1
Bromobenzene ND ug/kg 06/22/21 19:22 108-86-106/22/21 08:535.6 1
Bromochloromethane ND ug/kg 06/22/21 19:22 74-97-506/22/21 08:535.6 1
Bromodichloromethane ND ug/kg 06/22/21 19:22 75-27-406/22/21 08:535.6 1
Bromoform ND ug/kg 06/22/21 19:22 75-25-206/22/21 08:535.6 1
Bromomethane ND ug/kg 06/22/21 19:22 74-83-9 IK,L1,v106/22/21 08:5311.2 1
2-Butanone (MEK)ND ug/kg 06/22/21 19:22 78-93-306/22/21 08:531121
n-Butylbenzene ND ug/kg 06/22/21 19:22 104-51-806/22/21 08:535.6 1
sec-Butylbenzene ND ug/kg 06/22/21 19:22 135-98-806/22/21 08:535.6 1
tert-Butylbenzene ND ug/kg 06/22/21 19:22 98-06-6 v206/22/21 08:535.6 1
Carbon tetrachloride ND ug/kg 06/22/21 19:22 56-23-506/22/21 08:535.6 1
Chlorobenzene ND ug/kg 06/22/21 19:22 108-90-706/22/21 08:535.6 1
Chloroethane ND ug/kg 06/22/21 19:22 75-00-306/22/21 08:5311.2 1
Chloroform ND ug/kg 06/22/21 19:22 67-66-306/22/21 08:535.6 1
Chloromethane ND ug/kg 06/22/21 19:22 74-87-306/22/21 08:5311.2 1
2-Chlorotoluene ND ug/kg 06/22/21 19:22 95-49-806/22/21 08:535.6 1
4-Chlorotoluene ND ug/kg 06/22/21 19:22 106-43-406/22/21 08:535.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/22/21 19:22 96-12-806/22/21 08:535.6 1
Dibromochloromethane ND ug/kg 06/22/21 19:22 124-48-106/22/21 08:535.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/22/21 19:22 106-93-406/22/21 08:535.6 1
Dibromomethane ND ug/kg 06/22/21 19:22 74-95-306/22/21 08:535.6 1
1,2-Dichlorobenzene ND ug/kg 06/22/21 19:22 95-50-106/22/21 08:535.6 1
1,3-Dichlorobenzene ND ug/kg 06/22/21 19:22 541-73-106/22/21 08:535.6 1
1,4-Dichlorobenzene ND ug/kg 06/22/21 19:22 106-46-706/22/21 08:535.6 1
Dichlorodifluoromethane ND ug/kg 06/22/21 19:22 75-71-8 v206/22/21 08:5311.2 1
1,1-Dichloroethane ND ug/kg 06/22/21 19:22 75-34-306/22/21 08:535.6 1
1,2-Dichloroethane ND ug/kg 06/22/21 19:22 107-06-206/22/21 08:535.6 1
1,1-Dichloroethene ND ug/kg 06/22/21 19:22 75-35-406/22/21 08:535.6 1
cis-1,2-Dichloroethene ND ug/kg 06/22/21 19:22 156-59-206/22/21 08:535.6 1
trans-1,2-Dichloroethene ND ug/kg 06/22/21 19:22 156-60-506/22/21 08:535.6 1
1,2-Dichloropropane ND ug/kg 06/22/21 19:22 78-87-506/22/21 08:535.6 1
1,3-Dichloropropane ND ug/kg 06/22/21 19:22 142-28-906/22/21 08:535.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-12 Lab ID:92545119012 Collected:06/15/21 11:54 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 06/22/21 19:22 594-20-706/22/21 08:535.6 1
1,1-Dichloropropene ND ug/kg 06/22/21 19:22 563-58-606/22/21 08:535.6 1
cis-1,3-Dichloropropene ND ug/kg 06/22/21 19:22 10061-01-506/22/21 08:535.6 1
trans-1,3-Dichloropropene ND ug/kg 06/22/21 19:22 10061-02-606/22/21 08:535.6 1
Diisopropyl ether ND ug/kg 06/22/21 19:22 108-20-306/22/21 08:535.6 1
Ethylbenzene ND ug/kg 06/22/21 19:22 100-41-406/22/21 08:535.6 1
Hexachloro-1,3-butadiene ND ug/kg 06/22/21 19:22 87-68-306/22/21 08:5311.2 1
2-Hexanone ND ug/kg 06/22/21 19:22 591-78-606/22/21 08:5356.1 1
Isopropylbenzene (Cumene)ND ug/kg 06/22/21 19:22 98-82-806/22/21 08:535.6 1
p-Isopropyltoluene ND ug/kg 06/22/21 19:22 99-87-606/22/21 08:535.6 1
Methylene Chloride ND ug/kg 06/22/21 19:22 75-09-206/22/21 08:5322.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/22/21 19:22 108-10-106/22/21 08:5356.1 1
Methyl-tert-butyl ether ND ug/kg 06/22/21 19:22 1634-04-406/22/21 08:535.6 1
Naphthalene ND ug/kg 06/22/21 19:22 91-20-3 v206/22/21 08:535.6 1
n-Propylbenzene ND ug/kg 06/22/21 19:22 103-65-106/22/21 08:535.6 1
Styrene ND ug/kg 06/22/21 19:22 100-42-506/22/21 08:535.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/22/21 19:22 630-20-606/22/21 08:535.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/22/21 19:22 79-34-506/22/21 08:535.6 1
Tetrachloroethene ND ug/kg 06/22/21 19:22 127-18-406/22/21 08:535.6 1
Toluene ND ug/kg 06/22/21 19:22 108-88-306/22/21 08:535.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/22/21 19:22 87-61-606/22/21 08:535.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/22/21 19:22 120-82-106/22/21 08:535.6 1
1,1,1-Trichloroethane ND ug/kg 06/22/21 19:22 71-55-606/22/21 08:535.6 1
1,1,2-Trichloroethane ND ug/kg 06/22/21 19:22 79-00-506/22/21 08:535.6 1
Trichloroethene ND ug/kg 06/22/21 19:22 79-01-606/22/21 08:535.6 1
Trichlorofluoromethane ND ug/kg 06/22/21 19:22 75-69-406/22/21 08:535.6 1
1,2,3-Trichloropropane ND ug/kg 06/22/21 19:22 96-18-406/22/21 08:535.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/22/21 19:22 95-63-606/22/21 08:535.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/22/21 19:22 108-67-806/22/21 08:535.6 1
Vinyl acetate ND ug/kg 06/22/21 19:22 108-05-406/22/21 08:5356.1 1
Vinyl chloride ND ug/kg 06/22/21 19:22 75-01-406/22/21 08:5311.2 1
Xylene (Total)ND ug/kg 06/22/21 19:22 1330-20-706/22/21 08:5311.2 1
m&p-Xylene ND ug/kg 06/22/21 19:22 179601-23-106/22/21 08:5311.2 1
o-Xylene ND ug/kg 06/22/21 19:22 95-47-606/22/21 08:535.6 1
Surrogates
Toluene-d8 (S)104 %06/22/21 19:22 2037-26-506/22/21 08:5370-130 1
4-Bromofluorobenzene (S)97 %06/22/21 19:22 460-00-406/22/21 08:5369-134 1
1,2-Dichloroethane-d4 (S)108 %06/22/21 19:22 17060-07-006/22/21 08:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.2 %06/18/21 17:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-13 Lab ID:92545119013 Collected:06/15/21 11:58 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)8.4 mg/kg 06/22/21 13:3806/21/21 10:196.1 1
Surrogates
n-Pentacosane (S)67 %06/22/21 13:38 629-99-206/21/21 10:1932-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 06/23/21 19:0606/21/21 10:237.5 1
Surrogates
4-Bromofluorobenzene (S)94 %06/23/21 19:06 460-00-406/21/21 10:2366-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/23/21 19:10 67-64-106/22/21 12:591261
Benzene ND ug/kg 06/23/21 19:10 71-43-206/22/21 12:596.3 1
Bromobenzene ND ug/kg 06/23/21 19:10 108-86-106/22/21 12:596.3 1
Bromochloromethane ND ug/kg 06/23/21 19:10 74-97-506/22/21 12:596.3 1
Bromodichloromethane ND ug/kg 06/23/21 19:10 75-27-406/22/21 12:596.3 1
Bromoform ND ug/kg 06/23/21 19:10 75-25-206/22/21 12:596.3 1
Bromomethane ND ug/kg 06/23/21 19:10 74-83-9 IK,L1,v106/22/21 12:5912.6 1
2-Butanone (MEK)ND ug/kg 06/23/21 19:10 78-93-306/22/21 12:591261
n-Butylbenzene ND ug/kg 06/23/21 19:10 104-51-806/22/21 12:596.3 1
sec-Butylbenzene ND ug/kg 06/23/21 19:10 135-98-806/22/21 12:596.3 1
tert-Butylbenzene ND ug/kg 06/23/21 19:10 98-06-606/22/21 12:596.3 1
Carbon tetrachloride ND ug/kg 06/23/21 19:10 56-23-506/22/21 12:596.3 1
Chlorobenzene ND ug/kg 06/23/21 19:10 108-90-706/22/21 12:596.3 1
Chloroethane ND ug/kg 06/23/21 19:10 75-00-306/22/21 12:5912.6 1
Chloroform ND ug/kg 06/23/21 19:10 67-66-306/22/21 12:596.3 1
Chloromethane ND ug/kg 06/23/21 19:10 74-87-306/22/21 12:5912.6 1
2-Chlorotoluene ND ug/kg 06/23/21 19:10 95-49-806/22/21 12:596.3 1
4-Chlorotoluene ND ug/kg 06/23/21 19:10 106-43-406/22/21 12:596.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/23/21 19:10 96-12-806/22/21 12:596.3 1
Dibromochloromethane ND ug/kg 06/23/21 19:10 124-48-106/22/21 12:596.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/23/21 19:10 106-93-406/22/21 12:596.3 1
Dibromomethane ND ug/kg 06/23/21 19:10 74-95-306/22/21 12:596.3 1
1,2-Dichlorobenzene ND ug/kg 06/23/21 19:10 95-50-106/22/21 12:596.3 1
1,3-Dichlorobenzene ND ug/kg 06/23/21 19:10 541-73-106/22/21 12:596.3 1
1,4-Dichlorobenzene ND ug/kg 06/23/21 19:10 106-46-706/22/21 12:596.3 1
Dichlorodifluoromethane ND ug/kg 06/23/21 19:10 75-71-806/22/21 12:5912.6 1
1,1-Dichloroethane ND ug/kg 06/23/21 19:10 75-34-306/22/21 12:596.3 1
1,2-Dichloroethane ND ug/kg 06/23/21 19:10 107-06-206/22/21 12:596.3 1
1,1-Dichloroethene ND ug/kg 06/23/21 19:10 75-35-406/22/21 12:596.3 1
cis-1,2-Dichloroethene ND ug/kg 06/23/21 19:10 156-59-206/22/21 12:596.3 1
trans-1,2-Dichloroethene ND ug/kg 06/23/21 19:10 156-60-506/22/21 12:596.3 1
1,2-Dichloropropane ND ug/kg 06/23/21 19:10 78-87-506/22/21 12:596.3 1
1,3-Dichloropropane ND ug/kg 06/23/21 19:10 142-28-906/22/21 12:596.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 61
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Sample:SS-13 Lab ID:92545119013 Collected:06/15/21 11:58 Received:06/17/21 11:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 06/23/21 19:10 594-20-706/22/21 12:596.3 1
1,1-Dichloropropene ND ug/kg 06/23/21 19:10 563-58-606/22/21 12:596.3 1
cis-1,3-Dichloropropene ND ug/kg 06/23/21 19:10 10061-01-506/22/21 12:596.3 1
trans-1,3-Dichloropropene ND ug/kg 06/23/21 19:10 10061-02-606/22/21 12:596.3 1
Diisopropyl ether ND ug/kg 06/23/21 19:10 108-20-306/22/21 12:596.3 1
Ethylbenzene ND ug/kg 06/23/21 19:10 100-41-406/22/21 12:596.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/23/21 19:10 87-68-306/22/21 12:5912.6 1
2-Hexanone ND ug/kg 06/23/21 19:10 591-78-606/22/21 12:5963.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/23/21 19:10 98-82-806/22/21 12:596.3 1
p-Isopropyltoluene ND ug/kg 06/23/21 19:10 99-87-606/22/21 12:596.3 1
Methylene Chloride ND ug/kg 06/23/21 19:10 75-09-206/22/21 12:5925.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/23/21 19:10 108-10-106/22/21 12:5963.2 1
Methyl-tert-butyl ether ND ug/kg 06/23/21 19:10 1634-04-406/22/21 12:596.3 1
Naphthalene ND ug/kg 06/23/21 19:10 91-20-306/22/21 12:596.3 1
n-Propylbenzene ND ug/kg 06/23/21 19:10 103-65-106/22/21 12:596.3 1
Styrene ND ug/kg 06/23/21 19:10 100-42-506/22/21 12:596.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/23/21 19:10 630-20-606/22/21 12:596.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/23/21 19:10 79-34-506/22/21 12:596.3 1
Tetrachloroethene ND ug/kg 06/23/21 19:10 127-18-406/22/21 12:596.3 1
Toluene ND ug/kg 06/23/21 19:10 108-88-306/22/21 12:596.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/23/21 19:10 87-61-606/22/21 12:596.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/23/21 19:10 120-82-106/22/21 12:596.3 1
1,1,1-Trichloroethane ND ug/kg 06/23/21 19:10 71-55-606/22/21 12:596.3 1
1,1,2-Trichloroethane ND ug/kg 06/23/21 19:10 79-00-506/22/21 12:596.3 1
Trichloroethene ND ug/kg 06/23/21 19:10 79-01-606/22/21 12:596.3 1
Trichlorofluoromethane ND ug/kg 06/23/21 19:10 75-69-406/22/21 12:596.3 1
1,2,3-Trichloropropane ND ug/kg 06/23/21 19:10 96-18-406/22/21 12:596.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/23/21 19:10 95-63-606/22/21 12:596.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/23/21 19:10 108-67-806/22/21 12:596.3 1
Vinyl acetate ND ug/kg 06/23/21 19:10 108-05-4 v106/22/21 12:5963.2 1
Vinyl chloride ND ug/kg 06/23/21 19:10 75-01-406/22/21 12:5912.6 1
Xylene (Total)ND ug/kg 06/23/21 19:10 1330-20-706/22/21 12:5912.6 1
m&p-Xylene ND ug/kg 06/23/21 19:10 179601-23-106/22/21 12:5912.6 1
o-Xylene ND ug/kg 06/23/21 19:10 95-47-606/22/21 12:596.3 1
Surrogates
Toluene-d8 (S)102 %06/23/21 19:10 2037-26-506/22/21 12:5970-130 1
4-Bromofluorobenzene (S)102 %06/23/21 19:10 460-00-406/22/21 12:5969-134 1
1,2-Dichloroethane-d4 (S)111 %06/23/21 19:10 17060-07-006/22/21 12:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %06/18/21 17:42 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628394
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119001, 92545119002, 92545119003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3303213
Associated Lab Samples:92545119001, 92545119002, 92545119003
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/22/21 15:29
4-Bromofluorobenzene (S)%99 66-131 06/22/21 15:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3303214LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 45.150 90 70-130
4-Bromofluorobenzene (S)%95 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3303216MATRIX SPIKE SAMPLE:
MSSpike
Result
92545021003
Gas Range Organics (C6-C10)mg/kg 63.265.2 97 70-145ND
4-Bromofluorobenzene (S)%105 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92545021002
3303215SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9598
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628418
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119004, 92545119005, 92545119006, 92545119007, 92545119008, 92545119009, 92545119010,
92545119011, 92545119012, 92545119013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3303347
Associated Lab Samples:92545119004, 92545119005, 92545119006, 92545119007, 92545119008, 92545119009, 92545119010,
92545119011, 92545119012, 92545119013
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 06/23/21 14:24
4-Bromofluorobenzene (S)%97 66-131 06/23/21 14:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3303348LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 46.450 93 70-130
4-Bromofluorobenzene (S)%104 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3303350MATRIX SPIKE SAMPLE:
MSSpike
Result
92545119005
Gas Range Organics (C6-C10)mg/kg 52.257.9 90 70-145ND
4-Bromofluorobenzene (S)%99 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92545119004
3303349SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9599
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
627930
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119001, 92545119002, 92545119003, 92545119004, 92545119005, 92545119006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3300968
Associated Lab Samples:92545119001, 92545119002, 92545119003, 92545119004, 92545119005, 92545119006
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/22/21 11:46
1,1,1-Trichloroethane ug/kg ND 5.0 06/22/21 11:46
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/22/21 11:46
1,1,2-Trichloroethane ug/kg ND 5.0 06/22/21 11:46
1,1-Dichloroethane ug/kg ND 5.0 06/22/21 11:46
1,1-Dichloroethene ug/kg ND 5.0 06/22/21 11:46
1,1-Dichloropropene ug/kg ND 5.0 06/22/21 11:46
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/22/21 11:46
1,2,3-Trichloropropane ug/kg ND 5.0 06/22/21 11:46
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/22/21 11:46
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/22/21 11:46
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/22/21 11:46
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/22/21 11:46
1,2-Dichlorobenzene ug/kg ND 5.0 06/22/21 11:46
1,2-Dichloroethane ug/kg ND 5.0 06/22/21 11:46
1,2-Dichloropropane ug/kg ND 5.0 06/22/21 11:46
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/22/21 11:46
1,3-Dichlorobenzene ug/kg ND 5.0 06/22/21 11:46
1,3-Dichloropropane ug/kg ND 5.0 06/22/21 11:46
1,4-Dichlorobenzene ug/kg ND 5.0 06/22/21 11:46
2,2-Dichloropropane ug/kg ND 5.0 06/22/21 11:46
2-Butanone (MEK)ug/kg ND 100 06/22/21 11:46
2-Chlorotoluene ug/kg ND 5.0 06/22/21 11:46
2-Hexanone ug/kg ND 50.0 06/22/21 11:46
4-Chlorotoluene ug/kg ND 5.0 06/22/21 11:46
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/22/21 11:46
Acetone ug/kg ND 100 06/22/21 11:46
Benzene ug/kg ND 5.0 06/22/21 11:46
Bromobenzene ug/kg ND 5.0 06/22/21 11:46
Bromochloromethane ug/kg ND 5.0 06/22/21 11:46
Bromodichloromethane ug/kg ND 5.0 06/22/21 11:46
Bromoform ug/kg ND 5.0 06/22/21 11:46
Bromomethane ug/kg ND 10.0 IK,v106/22/21 11:46
Carbon tetrachloride ug/kg ND 5.0 06/22/21 11:46
Chlorobenzene ug/kg ND 5.0 06/22/21 11:46
Chloroethane ug/kg ND 10.0 06/22/21 11:46
Chloroform ug/kg ND 5.0 06/22/21 11:46
Chloromethane ug/kg ND 10.0 06/22/21 11:46
cis-1,2-Dichloroethene ug/kg ND 5.0 06/22/21 11:46
cis-1,3-Dichloropropene ug/kg ND 5.0 06/22/21 11:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3300968
Associated Lab Samples:92545119001, 92545119002, 92545119003, 92545119004, 92545119005, 92545119006
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/22/21 11:46
Dibromomethane ug/kg ND 5.0 06/22/21 11:46
Dichlorodifluoromethane ug/kg ND 10.0 v206/22/21 11:46
Diisopropyl ether ug/kg ND 5.0 06/22/21 11:46
Ethylbenzene ug/kg ND 5.0 06/22/21 11:46
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/22/21 11:46
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/22/21 11:46
m&p-Xylene ug/kg ND 10.0 06/22/21 11:46
Methyl-tert-butyl ether ug/kg ND 5.0 06/22/21 11:46
Methylene Chloride ug/kg ND 20.0 06/22/21 11:46
n-Butylbenzene ug/kg ND 5.0 06/22/21 11:46
n-Propylbenzene ug/kg ND 5.0 06/22/21 11:46
Naphthalene ug/kg ND 5.0 v206/22/21 11:46
o-Xylene ug/kg ND 5.0 06/22/21 11:46
p-Isopropyltoluene ug/kg ND 5.0 06/22/21 11:46
sec-Butylbenzene ug/kg ND 5.0 06/22/21 11:46
Styrene ug/kg ND 5.0 06/22/21 11:46
tert-Butylbenzene ug/kg ND 5.0 v206/22/21 11:46
Tetrachloroethene ug/kg ND 5.0 06/22/21 11:46
Toluene ug/kg ND 5.0 06/22/21 11:46
trans-1,2-Dichloroethene ug/kg ND 5.0 06/22/21 11:46
trans-1,3-Dichloropropene ug/kg ND 5.0 06/22/21 11:46
Trichloroethene ug/kg ND 5.0 06/22/21 11:46
Trichlorofluoromethane ug/kg ND 5.0 06/22/21 11:46
Vinyl acetate ug/kg ND 50.0 06/22/21 11:46
Vinyl chloride ug/kg ND 10.0 06/22/21 11:46
Xylene (Total)ug/kg ND 10.0 06/22/21 11:46
1,2-Dichloroethane-d4 (S)%109 70-130 06/22/21 11:46
4-Bromofluorobenzene (S)%94 69-134 06/22/21 11:46
Toluene-d8 (S)%103 70-130 06/22/21 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3300969LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11701250 94 70-130
1,1,1-Trichloroethane ug/kg 11001250 88 70-130
1,1,2,2-Tetrachloroethane ug/kg 11401250 91 70-130
1,1,2-Trichloroethane ug/kg 11001250 88 70-130
1,1-Dichloroethane ug/kg 12701250 102 70-130
1,1-Dichloroethene ug/kg 12701250 102 70-130
1,1-Dichloropropene ug/kg 12001250 96 70-130
1,2,3-Trichlorobenzene ug/kg 10301250 83 65-130
1,2,3-Trichloropropane ug/kg 11601250 93 70-130
1,2,4-Trichlorobenzene ug/kg 10701250 86 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3300969LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11601250 93 70-130
1,2-Dibromo-3-chloropropane ug/kg 10401250 83 70-130
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 11201250 89 70-130
1,2-Dichloroethane ug/kg 11601250 93 63-130
1,2-Dichloropropane ug/kg 12501250 100 70-130
1,3,5-Trimethylbenzene ug/kg 10601250 85 70-130
1,3-Dichlorobenzene ug/kg 11501250 92 70-130
1,3-Dichloropropane ug/kg 12501250 100 70-130
1,4-Dichlorobenzene ug/kg 11501250 92 70-130
2,2-Dichloropropane ug/kg 11701250 94 66-130
2-Butanone (MEK)ug/kg 22302500 89 70-130
2-Chlorotoluene ug/kg 11401250 91 70-130
2-Hexanone ug/kg 24102500 97 70-130
4-Chlorotoluene ug/kg 10801250 87 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23802500 95 70-130
Acetone ug/kg 22302500 89 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 11601250 92 70-130
Bromochloromethane ug/kg 13001250 104 70-130
Bromodichloromethane ug/kg 11301250 90 69-130
Bromoform ug/kg 11801250 94 70-130
Bromomethane ug/kg 1960 IK,L1,v1125015752-130
Carbon tetrachloride ug/kg 11501250 92 70-130
Chlorobenzene ug/kg 12401250 99 70-130
Chloroethane ug/kg 12201250 98 65-130
Chloroform ug/kg 11401250 91 70-130
Chloromethane ug/kg 11001250 88 55-130
cis-1,2-Dichloroethene ug/kg 12401250 99 70-130
cis-1,3-Dichloropropene ug/kg 11901250 95 70-130
Dibromochloromethane ug/kg 12001250 96 70-130
Dibromomethane ug/kg 12301250 98 70-130
Dichlorodifluoromethane ug/kg 908 v312507345-156
Diisopropyl ether ug/kg 11101250 89 70-130
Ethylbenzene ug/kg 11701250 93 70-130
Hexachloro-1,3-butadiene ug/kg 11101250 89 66-130
Isopropylbenzene (Cumene)ug/kg 12201250 98 70-130
m&p-Xylene ug/kg 23202500 93 70-130
Methyl-tert-butyl ether ug/kg 11201250 90 70-130
Methylene Chloride ug/kg 12901250 103 65-130
n-Butylbenzene ug/kg 11201250 90 67-130
n-Propylbenzene ug/kg 11001250 88 70-130
Naphthalene ug/kg 971 v312507870-130
o-Xylene ug/kg 11901250 95 70-130
p-Isopropyltoluene ug/kg 10801250 86 67-130
sec-Butylbenzene ug/kg 11101250 89 69-130
Styrene ug/kg 12301250 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3300969LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 848 v312506867-130
Tetrachloroethene ug/kg 12501250 100 70-130
Toluene ug/kg 11301250 91 70-130
trans-1,2-Dichloroethene ug/kg 12201250 98 70-130
trans-1,3-Dichloropropene ug/kg 11601250 93 68-130
Trichloroethene ug/kg 12001250 96 70-130
Trichlorofluoromethane ug/kg 11201250 90 70-130
Vinyl acetate ug/kg 24602500 98 70-130
Vinyl chloride ug/kg 11401250 92 61-130
Xylene (Total)ug/kg 35203750 94 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3305165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92544529016
3305166
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 1070 105 70-13198 71070ND11201050
1,1,1-Trichloroethane ug/kg 1070 113 65-133105 71070ND12001120
1,1,2,2-Tetrachloroethane ug/kg 1070 107 66-13098 91070ND11501050
1,1,2-Trichloroethane ug/kg 1070 106 66-13398 81070ND11301050
1,1-Dichloroethane ug/kg M1107013465-130123 81070ND14301310
1,1-Dichloroethene ug/kg 1070 131 10-158124 61070ND14001320
1,1-Dichloropropene ug/kg 1070 124 68-133117 61070ND13301240
1,2,3-Trichlorobenzene ug/kg 1070 95 27-13890 61070ND1020960
1,2,3-Trichloropropane ug/kg 1070 99 67-13091 81070ND1060975
1,2,4-Trichlorobenzene ug/kg 1070 92 51-13490 21070ND982959
1,2,4-Trimethylbenzene ug/kg 1070 108 63-136100 71070ND11501070
1,2-Dibromo-3-chloropropane ug/kg 1070 89 32-13080 111070ND946851
1,2-Dibromoethane (EDB)ug/kg 1070 112 70-130104 71070ND11901110
1,2-Dichlorobenzene ug/kg 1070 106 69-13099 61070ND11301060
1,2-Dichloroethane ug/kg 1070 122 59-130113 81070ND13001200
1,2-Dichloropropane ug/kg 1070 122 70-130113 81070ND13101210
1,3,5-Trimethylbenzene ug/kg 1070 97 65-13790 81070ND1040958
1,3-Dichlorobenzene ug/kg 1070 107 70-130100 71070ND11401070
1,3-Dichloropropane ug/kg 1070 119 70-130109 81070ND12701170
1,4-Dichlorobenzene ug/kg 1070 107 68-130100 71070ND11401070
2,2-Dichloropropane ug/kg 1070 57 32-13053 81070ND607562
2-Butanone (MEK)ug/kg 2140 117 10-136106 102140ND25002270
2-Chlorotoluene ug/kg 1070 104 69-14198 71070ND11201040
2-Hexanone ug/kg 2140 112 10-144103 82140ND23802200
4-Chlorotoluene ug/kg 1070 101 70-13295 61070ND10701020
4-Methyl-2-pentanone (MIBK)ug/kg 2140 115 25-143105 92140ND24502240
Acetone ug/kg 2140 128 10-130122 52140ND27402620
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3305165MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92544529016
3305166
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzene ug/kg 1070 119 67-130111 71070ND12701180
Bromobenzene ug/kg 1070 111 70-130102 81070ND11901090
Bromochloromethane ug/kg 1070 132 69-134122 81070ND14001300
Bromodichloromethane ug/kg 1070 100 64-13092 81070ND1070985
Bromoform ug/kg 1070 90 62-13084 71070ND962895
Bromomethane ug/kg IK,v1107014420-176120 181070ND15301280
Carbon tetrachloride ug/kg 1070 105 65-14099 51070ND11201060
Chlorobenzene ug/kg 1070 117 70-130109 71070ND12501160
Chloroethane ug/kg R110702310-13015 411070ND248164
Chloroform ug/kg 1070 120 63-130112 71070ND12801190
Chloromethane ug/kg M1107013258-130123 61070ND14101320
cis-1,2-Dichloroethene ug/kg 1070 129 66-130121 6107014015201440
cis-1,3-Dichloropropene ug/kg 1070 98 67-13089 91070ND1040949
Dibromochloromethane ug/kg 1070 99 67-13090 101070ND1060957
Dibromomethane ug/kg 1070 116 63-131106 91070ND12401130
Dichlorodifluoromethane ug/kg v3107010244-18096 61070ND10901030
Diisopropyl ether ug/kg 1070 116 63-130108 81070ND12401150
Ethylbenzene ug/kg 1070 109 66-130103 61070ND11701100
Hexachloro-1,3-butadiene ug/kg 1070 94 64-15091 41070ND1010971
Isopropylbenzene (Cumene)ug/kg 1070 114 69-135107 61070ND12201140
m&p-Xylene ug/kg 2140 109 60-133101 82140ND23402160
Methyl-tert-butyl ether ug/kg 1070 115 65-130107 71070ND12301150
Methylene Chloride ug/kg M1107014061-130131 61070ND15001400
n-Butylbenzene ug/kg 1070 92 65-14089 31070ND986954
n-Propylbenzene ug/kg 1070 101 67-14096 51070ND10801020
Naphthalene ug/kg v310708715-14584 41070ND934896
o-Xylene ug/kg 1070 108 66-133101 61070ND11501080
p-Isopropyltoluene ug/kg 1070 95 56-14789 61070ND1020955
sec-Butylbenzene ug/kg 1070 101 65-13995 51070ND10701020
Styrene ug/kg 1070 109 70-132102 71070ND11701090
tert-Butylbenzene ug/kg v310708162-13575 71070ND865806
Tetrachloroethene ug/kg 1070 106 70-135104 0107092701040010400
Toluene ug/kg 1070 110 67-130101 81070ND11801090
trans-1,2-Dichloroethene ug/kg 1070 129 69-130122 61070ND13801300
trans-1,3-Dichloropropene ug/kg 1070 94 62-13086 81070ND1000921
Trichloroethene ug/kg 1070 121 70-135112 5107070720001910
Trichlorofluoromethane ug/kg 1070 60 10-13059 21070ND643631
Vinyl acetate ug/kg 2140 113 53-130104 82140ND24102220
Vinyl chloride ug/kg 1070 128 61-148122 41070ND13701310
Xylene (Total)ug/kg 3200 109 63-132101 73200ND34903240
1,2-Dichloroethane-d4 (S)%130 70-130127
4-Bromofluorobenzene (S)%98 69-13498
Toluene-d8 (S)%102 70-130103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628594
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119007, 92545119008, 92545119009, 92545119010, 92545119011, 92545119012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3304132
Associated Lab Samples:92545119007, 92545119008, 92545119009, 92545119010, 92545119011, 92545119012
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/22/21 12:03
1,1,1-Trichloroethane ug/kg ND 5.0 06/22/21 12:03
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/22/21 12:03
1,1,2-Trichloroethane ug/kg ND 5.0 06/22/21 12:03
1,1-Dichloroethane ug/kg ND 5.0 06/22/21 12:03
1,1-Dichloroethene ug/kg ND 5.0 06/22/21 12:03
1,1-Dichloropropene ug/kg ND 5.0 06/22/21 12:03
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/22/21 12:03
1,2,3-Trichloropropane ug/kg ND 5.0 06/22/21 12:03
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/22/21 12:03
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/22/21 12:03
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/22/21 12:03
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/22/21 12:03
1,2-Dichlorobenzene ug/kg ND 5.0 06/22/21 12:03
1,2-Dichloroethane ug/kg ND 5.0 06/22/21 12:03
1,2-Dichloropropane ug/kg ND 5.0 06/22/21 12:03
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/22/21 12:03
1,3-Dichlorobenzene ug/kg ND 5.0 06/22/21 12:03
1,3-Dichloropropane ug/kg ND 5.0 06/22/21 12:03
1,4-Dichlorobenzene ug/kg ND 5.0 06/22/21 12:03
2,2-Dichloropropane ug/kg ND 5.0 06/22/21 12:03
2-Butanone (MEK)ug/kg ND 100 06/22/21 12:03
2-Chlorotoluene ug/kg ND 5.0 06/22/21 12:03
2-Hexanone ug/kg ND 50.0 06/22/21 12:03
4-Chlorotoluene ug/kg ND 5.0 06/22/21 12:03
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/22/21 12:03
Acetone ug/kg ND 100 06/22/21 12:03
Benzene ug/kg ND 5.0 06/22/21 12:03
Bromobenzene ug/kg ND 5.0 06/22/21 12:03
Bromochloromethane ug/kg ND 5.0 06/22/21 12:03
Bromodichloromethane ug/kg ND 5.0 06/22/21 12:03
Bromoform ug/kg ND 5.0 06/22/21 12:03
Bromomethane ug/kg ND 10.0 IK,v106/22/21 12:03
Carbon tetrachloride ug/kg ND 5.0 06/22/21 12:03
Chlorobenzene ug/kg ND 5.0 06/22/21 12:03
Chloroethane ug/kg ND 10.0 06/22/21 12:03
Chloroform ug/kg ND 5.0 06/22/21 12:03
Chloromethane ug/kg ND 10.0 06/22/21 12:03
cis-1,2-Dichloroethene ug/kg ND 5.0 06/22/21 12:03
cis-1,3-Dichloropropene ug/kg ND 5.0 06/22/21 12:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3304132
Associated Lab Samples:92545119007, 92545119008, 92545119009, 92545119010, 92545119011, 92545119012
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/22/21 12:03
Dibromomethane ug/kg ND 5.0 06/22/21 12:03
Dichlorodifluoromethane ug/kg ND 10.0 v206/22/21 12:03
Diisopropyl ether ug/kg ND 5.0 06/22/21 12:03
Ethylbenzene ug/kg ND 5.0 06/22/21 12:03
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/22/21 12:03
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/22/21 12:03
m&p-Xylene ug/kg ND 10.0 06/22/21 12:03
Methyl-tert-butyl ether ug/kg ND 5.0 06/22/21 12:03
Methylene Chloride ug/kg ND 20.0 06/22/21 12:03
n-Butylbenzene ug/kg ND 5.0 06/22/21 12:03
n-Propylbenzene ug/kg ND 5.0 06/22/21 12:03
Naphthalene ug/kg ND 5.0 v206/22/21 12:03
o-Xylene ug/kg ND 5.0 06/22/21 12:03
p-Isopropyltoluene ug/kg ND 5.0 06/22/21 12:03
sec-Butylbenzene ug/kg ND 5.0 06/22/21 12:03
Styrene ug/kg ND 5.0 06/22/21 12:03
tert-Butylbenzene ug/kg ND 5.0 v206/22/21 12:03
Tetrachloroethene ug/kg ND 5.0 06/22/21 12:03
Toluene ug/kg ND 5.0 06/22/21 12:03
trans-1,2-Dichloroethene ug/kg ND 5.0 06/22/21 12:03
trans-1,3-Dichloropropene ug/kg ND 5.0 06/22/21 12:03
Trichloroethene ug/kg ND 5.0 06/22/21 12:03
Trichlorofluoromethane ug/kg ND 5.0 06/22/21 12:03
Vinyl acetate ug/kg ND 50.0 06/22/21 12:03
Vinyl chloride ug/kg ND 10.0 06/22/21 12:03
Xylene (Total)ug/kg ND 10.0 06/22/21 12:03
1,2-Dichloroethane-d4 (S)%111 70-130 06/22/21 12:03
4-Bromofluorobenzene (S)%96 69-134 06/22/21 12:03
Toluene-d8 (S)%104 70-130 06/22/21 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304133LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11601250 93 70-130
1,1,1-Trichloroethane ug/kg 11101250 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 11501250 92 70-130
1,1,2-Trichloroethane ug/kg 11301250 90 70-130
1,1-Dichloroethane ug/kg 12901250 103 70-130
1,1-Dichloroethene ug/kg 13001250 104 70-130
1,1-Dichloropropene ug/kg 12501250 100 70-130
1,2,3-Trichlorobenzene ug/kg 10701250 85 65-130
1,2,3-Trichloropropane ug/kg 11801250 95 70-130
1,2,4-Trichlorobenzene ug/kg 11001250 88 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304133LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11901250 95 70-130
1,2-Dibromo-3-chloropropane ug/kg 10901250 88 70-130
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 11501250 92 70-130
1,2-Dichloroethane ug/kg 11901250 95 63-130
1,2-Dichloropropane ug/kg 12701250 102 70-130
1,3,5-Trimethylbenzene ug/kg 10801250 86 70-130
1,3-Dichlorobenzene ug/kg 11701250 93 70-130
1,3-Dichloropropane ug/kg 12601250 100 70-130
1,4-Dichlorobenzene ug/kg 11701250 93 70-130
2,2-Dichloropropane ug/kg 12001250 96 66-130
2-Butanone (MEK)ug/kg 23402500 94 70-130
2-Chlorotoluene ug/kg 11501250 92 70-130
2-Hexanone ug/kg 24602500 98 70-130
4-Chlorotoluene ug/kg 11101250 89 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24602500 98 70-130
Acetone ug/kg 23802500 95 69-130
Benzene ug/kg 12001250 96 70-130
Bromobenzene ug/kg 12001250 96 70-130
Bromochloromethane ug/kg 13301250 106 70-130
Bromodichloromethane ug/kg 11301250 91 69-130
Bromoform ug/kg 11701250 94 70-130
Bromomethane ug/kg 2000 IK,L1,v1125016052-130
Carbon tetrachloride ug/kg 11501250 92 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 12301250 99 65-130
Chloroform ug/kg 11701250 93 70-130
Chloromethane ug/kg 11301250 91 55-130
cis-1,2-Dichloroethene ug/kg 12701250 102 70-130
cis-1,3-Dichloropropene ug/kg 12101250 97 70-130
Dibromochloromethane ug/kg 11901250 95 70-130
Dibromomethane ug/kg 12601250 101 70-130
Dichlorodifluoromethane ug/kg 933 v312507545-156
Diisopropyl ether ug/kg 11301250 90 70-130
Ethylbenzene ug/kg 11601250 93 70-130
Hexachloro-1,3-butadiene ug/kg 11201250 90 66-130
Isopropylbenzene (Cumene)ug/kg 12301250 99 70-130
m&p-Xylene ug/kg 23402500 94 70-130
Methyl-tert-butyl ether ug/kg 11401250 92 70-130
Methylene Chloride ug/kg 13201250 106 65-130
n-Butylbenzene ug/kg 11501250 92 67-130
n-Propylbenzene ug/kg 11201250 89 70-130
Naphthalene ug/kg 1010 v312508170-130
o-Xylene ug/kg 11901250 96 70-130
p-Isopropyltoluene ug/kg 11001250 88 67-130
sec-Butylbenzene ug/kg 11301250 91 69-130
Styrene ug/kg 12301250 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304133LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 873 v312507067-130
Tetrachloroethene ug/kg 12401250 99 70-130
Toluene ug/kg 11501250 92 70-130
trans-1,2-Dichloroethene ug/kg 12401250 99 70-130
trans-1,3-Dichloropropene ug/kg 11801250 94 68-130
Trichloroethene ug/kg 12201250 98 70-130
Trichlorofluoromethane ug/kg 11501250 92 70-130
Vinyl acetate ug/kg 25302500 101 70-130
Vinyl chloride ug/kg 11601250 93 61-130
Xylene (Total)ug/kg 35403750 94 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%97 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3304135MATRIX SPIKE SAMPLE:
MSSpike
Result
92545119008
1,1,1,2-Tetrachloroethane ug/kg 460548 84 70-131ND
1,1,1-Trichloroethane ug/kg 481548 88 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 458548 84 66-130ND
1,1,2-Trichloroethane ug/kg 460548 84 66-133ND
1,1-Dichloroethane ug/kg 553548 101 65-130ND
1,1-Dichloroethene ug/kg 554548 101 10-158ND
1,1-Dichloropropene ug/kg 544548 99 68-133ND
1,2,3-Trichlorobenzene ug/kg 433548 79 27-138ND
1,2,3-Trichloropropane ug/kg 444548 81 67-130ND
1,2,4-Trichlorobenzene ug/kg 455548 83 51-134ND
1,2,4-Trimethylbenzene ug/kg 475548 87 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 362548 66 32-130ND
1,2-Dibromoethane (EDB)ug/kg 485548 89 70-130ND
1,2-Dichlorobenzene ug/kg 469548 86 69-130ND
1,2-Dichloroethane ug/kg 526548 96 59-130ND
1,2-Dichloropropane ug/kg 529548 96 70-130ND
1,3,5-Trimethylbenzene ug/kg 441548 80 65-137ND
1,3-Dichlorobenzene ug/kg 482548 88 70-130ND
1,3-Dichloropropane ug/kg 524548 96 70-130ND
1,4-Dichlorobenzene ug/kg 476548 87 68-130ND
2,2-Dichloropropane ug/kg 454548 83 32-130ND
2-Butanone (MEK)ug/kg 9121100 83 10-136ND
2-Chlorotoluene ug/kg 469548 86 69-141ND
2-Hexanone ug/kg 9311100 85 10-144ND
4-Chlorotoluene ug/kg 451548 82 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 9571100 87 25-143ND
Acetone ug/kg 8631100 79 10-130ND
Benzene ug/kg 524548 96 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3304135MATRIX SPIKE SAMPLE:
MSSpike
Result
92545119008
Bromobenzene ug/kg 475548 87 70-130ND
Bromochloromethane ug/kg 563548 103 69-134ND
Bromodichloromethane ug/kg 430548 78 64-130ND
Bromoform ug/kg 387548 71 62-130ND
Bromomethane ug/kg 530 IK,v15489720-176ND
Carbon tetrachloride ug/kg 443548 81 65-140ND
Chlorobenzene ug/kg 518548 95 70-130ND
Chloroethane ug/kg 182548 33 10-130ND
Chloroform ug/kg 514548 94 63-130ND
Chloromethane ug/kg 619548 113 58-130ND
cis-1,2-Dichloroethene ug/kg 565548 103 66-130ND
cis-1,3-Dichloropropene ug/kg 461548 84 67-130ND
Dibromochloromethane ug/kg 424548 77 67-130ND
Dibromomethane ug/kg 496548 90 63-131ND
Dichlorodifluoromethane ug/kg 421 v35487744-180ND
Diisopropyl ether ug/kg 504548 92 63-130ND
Ethylbenzene ug/kg 493548 90 66-130ND
Hexachloro-1,3-butadiene ug/kg 502548 92 64-150ND
Isopropylbenzene (Cumene)ug/kg 524548 96 69-135ND
m&p-Xylene ug/kg 9711100 89 60-133ND
Methyl-tert-butyl ether ug/kg 495548 90 65-130ND
Methylene Chloride ug/kg 541548 99 61-130ND
n-Butylbenzene ug/kg 469548 86 65-140ND
n-Propylbenzene ug/kg 461548 84 67-140ND
Naphthalene ug/kg 373 v35486815-145ND
o-Xylene ug/kg 498548 91 66-133ND
p-Isopropyltoluene ug/kg 463548 85 56-147ND
sec-Butylbenzene ug/kg 485548 88 65-139ND
Styrene ug/kg 497548 91 70-132ND
tert-Butylbenzene ug/kg 372 v35486862-135ND
Tetrachloroethene ug/kg 523548 95 70-135ND
Toluene ug/kg 487548 89 67-130ND
trans-1,2-Dichloroethene ug/kg 561548 102 69-130ND
trans-1,3-Dichloropropene ug/kg 442548 81 62-130ND
Trichloroethene ug/kg 524548 96 70-135ND
Trichlorofluoromethane ug/kg ND M1548010-130ND
Vinyl acetate ug/kg 9931100 91 53-130ND
Vinyl chloride ug/kg 571548 104 61-148ND
Xylene (Total)ug/kg 14701640 89 63-132ND
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545119007
3304134SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IK,v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND v2ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545119007
3304134SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg ND v2ND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg ND v2ND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%112112
4-Bromofluorobenzene (S)%9798
Toluene-d8 (S)%104104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628599
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3304153
Associated Lab Samples:92545119013
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/23/21 15:19
1,1,1-Trichloroethane ug/kg ND 5.0 06/23/21 15:19
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/23/21 15:19
1,1,2-Trichloroethane ug/kg ND 5.0 06/23/21 15:19
1,1-Dichloroethane ug/kg ND 5.0 06/23/21 15:19
1,1-Dichloroethene ug/kg ND 5.0 06/23/21 15:19
1,1-Dichloropropene ug/kg ND 5.0 06/23/21 15:19
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/23/21 15:19
1,2,3-Trichloropropane ug/kg ND 5.0 06/23/21 15:19
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/23/21 15:19
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/23/21 15:19
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/23/21 15:19
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/23/21 15:19
1,2-Dichlorobenzene ug/kg ND 5.0 06/23/21 15:19
1,2-Dichloroethane ug/kg ND 5.0 06/23/21 15:19
1,2-Dichloropropane ug/kg ND 5.0 06/23/21 15:19
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/23/21 15:19
1,3-Dichlorobenzene ug/kg ND 5.0 06/23/21 15:19
1,3-Dichloropropane ug/kg ND 5.0 06/23/21 15:19
1,4-Dichlorobenzene ug/kg ND 5.0 06/23/21 15:19
2,2-Dichloropropane ug/kg ND 5.0 06/23/21 15:19
2-Butanone (MEK)ug/kg ND 100 06/23/21 15:19
2-Chlorotoluene ug/kg ND 5.0 06/23/21 15:19
2-Hexanone ug/kg ND 50.0 06/23/21 15:19
4-Chlorotoluene ug/kg ND 5.0 06/23/21 15:19
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/23/21 15:19
Acetone ug/kg ND 100 06/23/21 15:19
Benzene ug/kg ND 5.0 06/23/21 15:19
Bromobenzene ug/kg ND 5.0 06/23/21 15:19
Bromochloromethane ug/kg ND 5.0 06/23/21 15:19
Bromodichloromethane ug/kg ND 5.0 06/23/21 15:19
Bromoform ug/kg ND 5.0 06/23/21 15:19
Bromomethane ug/kg ND 10.0 IK,v106/23/21 15:19
Carbon tetrachloride ug/kg ND 5.0 06/23/21 15:19
Chlorobenzene ug/kg ND 5.0 06/23/21 15:19
Chloroethane ug/kg ND 10.0 06/23/21 15:19
Chloroform ug/kg ND 5.0 06/23/21 15:19
Chloromethane ug/kg ND 10.0 06/23/21 15:19
cis-1,2-Dichloroethene ug/kg ND 5.0 06/23/21 15:19
cis-1,3-Dichloropropene ug/kg ND 5.0 06/23/21 15:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3304153
Associated Lab Samples:92545119013
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/23/21 15:19
Dibromomethane ug/kg ND 5.0 06/23/21 15:19
Dichlorodifluoromethane ug/kg ND 10.0 06/23/21 15:19
Diisopropyl ether ug/kg ND 5.0 06/23/21 15:19
Ethylbenzene ug/kg ND 5.0 06/23/21 15:19
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/23/21 15:19
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/23/21 15:19
m&p-Xylene ug/kg ND 10.0 06/23/21 15:19
Methyl-tert-butyl ether ug/kg ND 5.0 06/23/21 15:19
Methylene Chloride ug/kg ND 20.0 06/23/21 15:19
n-Butylbenzene ug/kg ND 5.0 06/23/21 15:19
n-Propylbenzene ug/kg ND 5.0 06/23/21 15:19
Naphthalene ug/kg ND 5.0 06/23/21 15:19
o-Xylene ug/kg ND 5.0 06/23/21 15:19
p-Isopropyltoluene ug/kg ND 5.0 06/23/21 15:19
sec-Butylbenzene ug/kg ND 5.0 06/23/21 15:19
Styrene ug/kg ND 5.0 06/23/21 15:19
tert-Butylbenzene ug/kg ND 5.0 06/23/21 15:19
Tetrachloroethene ug/kg ND 5.0 06/23/21 15:19
Toluene ug/kg ND 5.0 06/23/21 15:19
trans-1,2-Dichloroethene ug/kg ND 5.0 06/23/21 15:19
trans-1,3-Dichloropropene ug/kg ND 5.0 06/23/21 15:19
Trichloroethene ug/kg ND 5.0 06/23/21 15:19
Trichlorofluoromethane ug/kg ND 5.0 06/23/21 15:19
Vinyl acetate ug/kg ND 50.0 v106/23/21 15:19
Vinyl chloride ug/kg ND 10.0 06/23/21 15:19
Xylene (Total)ug/kg ND 10.0 06/23/21 15:19
1,2-Dichloroethane-d4 (S)%114 70-130 06/23/21 15:19
4-Bromofluorobenzene (S)%103 69-134 06/23/21 15:19
Toluene-d8 (S)%102 70-130 06/23/21 15:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304154LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11701250 94 70-130
1,1,1-Trichloroethane ug/kg 11301250 90 70-130
1,1,2,2-Tetrachloroethane ug/kg 11201250 90 70-130
1,1,2-Trichloroethane ug/kg 11201250 89 70-130
1,1-Dichloroethane ug/kg 12701250 102 70-130
1,1-Dichloroethene ug/kg 13301250 106 70-130
1,1-Dichloropropene ug/kg 12201250 98 70-130
1,2,3-Trichlorobenzene ug/kg 12201250 98 65-130
1,2,3-Trichloropropane ug/kg 11801250 95 70-130
1,2,4-Trichlorobenzene ug/kg 12101250 97 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304154LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12101250 97 70-130
1,2-Dibromo-3-chloropropane ug/kg 11301250 91 70-130
1,2-Dibromoethane (EDB)ug/kg 11801250 94 70-130
1,2-Dichlorobenzene ug/kg 11601250 92 70-130
1,2-Dichloroethane ug/kg 12201250 97 63-130
1,2-Dichloropropane ug/kg 12401250 99 70-130
1,3,5-Trimethylbenzene ug/kg 11801250 95 70-130
1,3-Dichlorobenzene ug/kg 11801250 94 70-130
1,3-Dichloropropane ug/kg 12001250 96 70-130
1,4-Dichlorobenzene ug/kg 11501250 92 70-130
2,2-Dichloropropane ug/kg 11701250 93 66-130
2-Butanone (MEK)ug/kg 25302500 101 70-130
2-Chlorotoluene ug/kg 12401250 99 70-130
2-Hexanone ug/kg 24802500 99 70-130
4-Chlorotoluene ug/kg 11701250 94 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25302500 101 70-130
Acetone ug/kg 24602500 99 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 12201250 98 70-130
Bromochloromethane ug/kg 12201250 98 70-130
Bromodichloromethane ug/kg 11101250 89 69-130
Bromoform ug/kg 11501250 92 70-130
Bromomethane ug/kg 1710 IK,L1,v1125013652-130
Carbon tetrachloride ug/kg 12201250 98 70-130
Chlorobenzene ug/kg 12001250 96 70-130
Chloroethane ug/kg 13801250 110 65-130
Chloroform ug/kg 13301250 106 70-130
Chloromethane ug/kg 12101250 97 55-130
cis-1,2-Dichloroethene ug/kg 12601250 101 70-130
cis-1,3-Dichloropropene ug/kg 12201250 98 70-130
Dibromochloromethane ug/kg 11801250 94 70-130
Dibromomethane ug/kg 11801250 94 70-130
Dichlorodifluoromethane ug/kg 12701250 101 45-156
Diisopropyl ether ug/kg 12101250 97 70-130
Ethylbenzene ug/kg 13201250 105 70-130
Hexachloro-1,3-butadiene ug/kg 13201250 105 66-130
Isopropylbenzene (Cumene)ug/kg 12201250 98 70-130
m&p-Xylene ug/kg 24302500 97 70-130
Methyl-tert-butyl ether ug/kg 11701250 94 70-130
Methylene Chloride ug/kg 13501250 108 65-130
n-Butylbenzene ug/kg 12901250 103 67-130
n-Propylbenzene ug/kg 12601250 101 70-130
Naphthalene ug/kg 11501250 92 70-130
o-Xylene ug/kg 11901250 95 70-130
p-Isopropyltoluene ug/kg 12001250 96 67-130
sec-Butylbenzene ug/kg 12001250 96 69-130
Styrene ug/kg 12001250 96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
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Page 48 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304154LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11601250 92 67-130
Tetrachloroethene ug/kg 10801250 87 70-130
Toluene ug/kg 11601250 93 70-130
trans-1,2-Dichloroethene ug/kg 12801250 103 70-130
trans-1,3-Dichloropropene ug/kg 12301250 98 68-130
Trichloroethene ug/kg 11901250 95 70-130
Trichlorofluoromethane ug/kg 12601250 100 70-130
Vinyl acetate ug/kg 2840 v1250011470-130
Vinyl chloride ug/kg 13001250 104 61-130
Xylene (Total)ug/kg 36203750 96 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%103 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3304156MATRIX SPIKE SAMPLE:
MSSpike
Result
92545256007
1,1,1,2-Tetrachloroethane ug/kg 678646 105 70-131ND
1,1,1-Trichloroethane ug/kg 660646 102 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 646646 100 66-130ND
1,1,2-Trichloroethane ug/kg 642646 99 66-133ND
1,1-Dichloroethane ug/kg 756646 117 65-130ND
1,1-Dichloroethene ug/kg 785646 121 10-158ND
1,1-Dichloropropene ug/kg 749646 116 68-133ND
1,2,3-Trichlorobenzene ug/kg 572646 89 27-138ND
1,2,3-Trichloropropane ug/kg 616646 95 67-130ND
1,2,4-Trichlorobenzene ug/kg 585646 91 51-134ND
1,2,4-Trimethylbenzene ug/kg 661646 101 63-1360.012 mg/kg
1,2-Dibromo-3-chloropropane ug/kg 545646 84 32-130ND
1,2-Dibromoethane (EDB)ug/kg 714646 111 70-130ND
1,2-Dichlorobenzene ug/kg 665646 103 69-130ND
1,2-Dichloroethane ug/kg 708646 110 59-130ND
1,2-Dichloropropane ug/kg 747646 116 70-130ND
1,3,5-Trimethylbenzene ug/kg 611646 95 65-137ND
1,3-Dichlorobenzene ug/kg 676646 105 70-130ND
1,3-Dichloropropane ug/kg 745646 115 70-130ND
1,4-Dichlorobenzene ug/kg 671646 104 68-130ND
2,2-Dichloropropane ug/kg 500646 77 32-130ND
2-Butanone (MEK)ug/kg 12701290 94 10-136ND
2-Chlorotoluene ug/kg 664646 103 69-141ND
2-Hexanone ug/kg 13101290 102 10-144ND
4-Chlorotoluene ug/kg 636646 98 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 13001290 101 25-143ND
Acetone ug/kg 12901290 100 10-130ND
Benzene ug/kg 734646 113 67-130ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3304156MATRIX SPIKE SAMPLE:
MSSpike
Result
92545256007
Bromobenzene ug/kg 711646 110 70-130ND
Bromochloromethane ug/kg 752646 116 69-134ND
Bromodichloromethane ug/kg 608646 94 64-130ND
Bromoform ug/kg 569646 88 62-130ND
Bromomethane ug/kg 520 IK,v16468020-176ND
Carbon tetrachloride ug/kg 662646 102 65-140ND
Chlorobenzene ug/kg 752646 117 70-130ND
Chloroethane ug/kg 174646 27 10-130ND
Chloroform ug/kg 694646 107 63-130ND
Chloromethane ug/kg 1050 M1,v164616358-130ND
cis-1,2-Dichloroethene ug/kg 766646 119 66-130ND
cis-1,3-Dichloropropene ug/kg 625646 97 67-130ND
Dibromochloromethane ug/kg 625646 97 67-130ND
Dibromomethane ug/kg 716646 111 63-131ND
Dichlorodifluoromethane ug/kg 860646 133 44-180ND
Diisopropyl ether ug/kg 674646 104 63-130ND
Ethylbenzene ug/kg 698646 108 66-130ND
Hexachloro-1,3-butadiene ug/kg 601646 93 64-150ND
Isopropylbenzene (Cumene)ug/kg 701646 109 69-135ND
m&p-Xylene ug/kg 14101290 106 60-1330.042 mg/kg
Methyl-tert-butyl ether ug/kg 683646 106 65-130ND
Methylene Chloride ug/kg 794 v164612361-130ND
n-Butylbenzene ug/kg 585646 91 65-140ND
n-Propylbenzene ug/kg 634646 98 67-140ND
Naphthalene ug/kg 564646 83 15-1450.029 mg/kg
o-Xylene ug/kg 698646 105 66-1330.017 mg/kg
p-Isopropyltoluene ug/kg 595646 91 56-147ND
sec-Butylbenzene ug/kg 616646 95 65-139ND
Styrene ug/kg 701646 109 70-132ND
tert-Butylbenzene ug/kg 499 v36467762-135ND
Tetrachloroethene ug/kg 731646 113 70-135ND
Toluene ug/kg 741646 100 67-1300.092 mg/kg
trans-1,2-Dichloroethene ug/kg 758646 117 69-130ND
trans-1,3-Dichloropropene ug/kg 599646 93 62-130ND
Trichloroethene ug/kg 753646 117 70-135ND
Trichlorofluoromethane ug/kg 222646 34 10-130ND
Vinyl acetate ug/kg 12801290 99 53-130ND
Vinyl chloride ug/kg 833646 129 61-148ND
Xylene (Total)ug/kg 21001940 106 63-1320.060 mg/kg
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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Page 50 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545119013
3304155SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IK,v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92545119013
3304155SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg ND v1ND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%111111
4-Bromofluorobenzene (S)%103102
Toluene-d8 (S)%103102
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628383
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119012, 92545119013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3303183
Associated Lab Samples:92545119012, 92545119013
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 4.9 06/22/21 09:33
n-Pentacosane (S)%71 32-130 06/22/21 09:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3303184LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 50.767.1 76 47-130
n-Pentacosane (S)%75 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3303185MATRIX SPIKE SAMPLE:
MSSpike
Result
92545306002
Diesel Range Organics(C10-C28)mg/kg 56.682.4 47 10-13318.0
n-Pentacosane (S)%52 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92545306003
3303186SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 10.2 2212.7
n-Pentacosane (S)%6163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 61
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628265
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545119001, 92545119002, 92545119003, 92545119004, 92545119005, 92545119006, 92545119007,
92545119008, 92545119009, 92545119010, 92545119011, 92545119012, 92545119013
Parameter Units
Dup
Result QualifiersRPDResult
92545117003
3302829SAMPLE DUPLICATE:
Percent Moisture %19.2 N2219.5
Parameter Units
Dup
Result QualifiersRPDResult
92545283002
3302830SAMPLE DUPLICATE:
Percent Moisture %25.6 N2727.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
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Huntersville, NC 28078
[phone]
Page 54 of 61
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 61
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92545119
Sheetz 39 Greenville
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92545119012 628383 628507SS-12 EPA 3546 EPA 8015C Modified
92545119013 628383 628507SS-13 EPA 3546 EPA 8015C Modified
92545119001 628394 628536SS-1 EPA 5030B EPA 8015C Modified
92545119002 628394 628536SS-2 EPA 5030B EPA 8015C Modified
92545119003 628394 628536SS-3 EPA 5030B EPA 8015C Modified
92545119004 628418 628535SS-4 EPA 5030B EPA 8015C Modified
92545119005 628418 628535SS-5 EPA 5030B EPA 8015C Modified
92545119006 628418 628535SS-6 EPA 5030B EPA 8015C Modified
92545119007 628418 628535SS-7 EPA 5030B EPA 8015C Modified
92545119008 628418 628535SS-8 EPA 5030B EPA 8015C Modified
92545119009 628418 628535SS-9 EPA 5030B EPA 8015C Modified
92545119010 628418 628535SS-10 EPA 5030B EPA 8015C Modified
92545119011 628418 628535SS-11 EPA 5030B EPA 8015C Modified
92545119012 628418 628535SS-12 EPA 5030B EPA 8015C Modified
92545119013 628418 628535SS-13 EPA 5030B EPA 8015C Modified
92545119001 627930 627937SS-1 EPA 5035A/5030B EPA 8260D
92545119002 627930 627937SS-2 EPA 5035A/5030B EPA 8260D
92545119003 627930 627937SS-3 EPA 5035A/5030B EPA 8260D
92545119004 627930 627937SS-4 EPA 5035A/5030B EPA 8260D
92545119005 627930 627937SS-5 EPA 5035A/5030B EPA 8260D
92545119006 627930 627937SS-6 EPA 5035A/5030B EPA 8260D
92545119007 628594 628672SS-7 EPA 5035A/5030B EPA 8260D
92545119008 628594 628672SS-8 EPA 5035A/5030B EPA 8260D
92545119009 628594 628672SS-9 EPA 5035A/5030B EPA 8260D
92545119010 628594 628672SS-10 EPA 5035A/5030B EPA 8260D
92545119011 628594 628672SS-11 EPA 5035A/5030B EPA 8260D
92545119012 628594 628672SS-12 EPA 5035A/5030B EPA 8260D
92545119013 628599 628758SS-13 EPA 5035A/5030B EPA 8260D
92545119001 628265SS-1 SW-846
92545119002 628265SS-2 SW-846
92545119003 628265SS-3 SW-846
92545119004 628265SS-4 SW-846
92545119005 628265SS-5 SW-846
92545119006 628265SS-6 SW-846
92545119007 628265SS-7 SW-846
92545119008 628265SS-8 SW-846
92545119009 628265SS-9 SW-846
92545119010 628265SS-10 SW-846
92545119011 628265SS-11 SW-846
92545119012 628265SS-12 SW-846
92545119013 628265SS-13 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/24/2021 05:12 PM
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[phone]
Page 56 of 61
Page 57 of 61
Page 58 of 61
Page 59 of 61
Page 60 of 61
Page 61 of 61
#=CL#
August 18, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92554623
92554623
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
391
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on August 09, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lindsey N Wooten
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92554623
391
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92554623
391
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92554623001 K1 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623002 K2 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623003 K3 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623004 K4 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623005 K5 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623006 K6 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623007 K7 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CAP2
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92554623008 GW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PASI-CMAD
EPA 625.1 58 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92554623
391
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92554623001 K1
Percent Moisture 7.1 %08/11/21 14:51 N20.10SW-846
92554623002 K2
Percent Moisture 11.7 %08/11/21 14:51 N20.10SW-846
92554623003 K3
Percent Moisture 15.4 %08/11/21 14:51 N20.10SW-846
92554623004 K4
Diesel Range Organics(C10-C28)15.1 mg/kg 08/12/21 16:086.3EPA 8015C Modified
Percent Moisture 21.8 %08/11/21 14:51 N20.10SW-846
92554623005 K5
Percent Moisture 15.5 %08/11/21 14:51 N20.10SW-846
92554623006 K6
Percent Moisture 17.3 %08/11/21 14:51 N20.10SW-846
92554623007 K7
Percent Moisture 17.3 %08/11/21 14:52 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K1 Lab ID:92554623001 Collected:08/06/21 08:06 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 15:2008/11/21 11:025.3 1
Surrogates
n-Pentacosane (S)55 %08/12/21 15:20 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 19:2508/16/21 16:5516.0 1
Surrogates
n-Pentacosane (S)40 %08/17/21 19:25 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 19:2808/11/21 13:035.8 1
Surrogates
4-Bromofluorobenzene (S)92 %08/11/21 19:28 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.1 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K2 Lab ID:92554623002 Collected:08/06/21 08:14 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 15:4408/11/21 11:025.7 1
Surrogates
n-Pentacosane (S)62 %08/12/21 15:44 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 19:2508/16/21 16:5517.0 1
Surrogates
n-Pentacosane (S)53 %08/17/21 19:25 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 19:5608/11/21 13:036.2 1
Surrogates
4-Bromofluorobenzene (S)94 %08/11/21 19:56 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.7 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K3 Lab ID:92554623003 Collected:08/06/21 08:22 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 15:4408/11/21 11:0218.1 1
Surrogates
n-Pentacosane (S)61 %08/12/21 15:44 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 19:4808/16/21 16:5517.7 1
Surrogates
n-Pentacosane (S)46 %08/17/21 19:48 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 20:2408/11/21 13:036.8 1
Surrogates
4-Bromofluorobenzene (S)96 %08/11/21 20:24 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.4 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K4 Lab ID:92554623004 Collected:08/06/21 08:33 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)15.1 mg/kg 08/12/21 16:0808/11/21 11:026.3 1
Surrogates
n-Pentacosane (S)80 %08/12/21 16:08 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 19:4808/16/21 16:5518.9 1
Surrogates
n-Pentacosane (S)61 %08/17/21 19:48 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 20:5208/11/21 13:038.1 1
Surrogates
4-Bromofluorobenzene (S)92 %08/11/21 20:52 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.8 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K5 Lab ID:92554623005 Collected:08/06/21 08:40 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 16:0808/11/21 11:026.0 1
Surrogates
n-Pentacosane (S)63 %08/12/21 16:08 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 20:1208/16/21 16:5517.6 1
Surrogates
n-Pentacosane (S)59 %08/17/21 20:12 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 21:2108/11/21 13:036.8 1
Surrogates
4-Bromofluorobenzene (S)94 %08/11/21 21:21 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.5 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K6 Lab ID:92554623006 Collected:08/06/21 08:50 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 16:3208/11/21 11:026.0 1
Surrogates
n-Pentacosane (S)78 %08/12/21 16:32 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 20:1208/16/21 16:5518.1 1
Surrogates
n-Pentacosane (S)59 %08/17/21 20:12 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 21:4908/11/21 13:036.8 1
Surrogates
4-Bromofluorobenzene (S)94 %08/11/21 21:49 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.3 %08/11/21 14:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:K7 Lab ID:92554623007 Collected:08/06/21 09:00 Received:08/09/21 09:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 08/12/21 16:3208/11/21 11:026.1 1
Surrogates
n-Pentacosane (S)61 %08/12/21 16:32 629-99-208/11/21 11:0232-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 08/17/21 20:3608/16/21 16:5518.1 1
Surrogates
n-Pentacosane (S)63 %08/17/21 20:36 629-99-208/16/21 16:5532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/11/21 22:1708/11/21 13:037.0 1
Surrogates
4-Bromofluorobenzene (S)92 %08/11/21 22:17 460-00-408/11/21 13:0366-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.3 %08/11/21 14:52 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:GW-1 Lab ID:92554623008 Collected:08/06/21 09:20 Received:08/09/21 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 08/17/21 10:04 N208/13/21 08:2099.0 1
Aliphatic (C19-C36)ND ug/L 08/17/21 10:04 N208/13/21 08:2099.0 1
Aromatic (C11-C22)ND ug/L 08/17/21 10:04 N208/13/21 08:2099.0 1
Surrogates
1-Chlorooctadecane (S)31 %08/17/21 10:04 3386-33-2 1g,S008/13/21 08:2040-140 1
o-Terphenyl (S)59 %08/17/21 10:04 84-15-108/13/21 08:2040-140 1
2-Fluorobiphenyl (S)66 %08/17/21 10:04 321-60-808/13/21 08:2040-140 1
2-Bromonaphthalene (S)62 %08/17/21 10:04 580-13-208/13/21 08:2040-140 1
Analytical Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Water
Aliphatic (C05-C08)ND ug/L 08/13/21 19:07 N250.0 1
Aliphatic(C09-C12) Adjusted ND ug/L 08/13/21 19:07 N250.0 1
Aromatic (C09-C10)ND ug/L 08/13/21 19:07 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %08/13/21 19:07 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)106 %08/13/21 19:07 460-00-470-130 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 08/13/21 02:55 83-32-908/12/21 05:265.0 1
Acenaphthylene ND ug/L 08/13/21 02:55 208-96-808/12/21 05:265.0 1
Anthracene ND ug/L 08/13/21 02:55 120-12-708/12/21 05:265.0 1
Benzo(a)anthracene ND ug/L 08/13/21 02:55 56-55-308/12/21 05:265.0 1
Benzo(a)pyrene ND ug/L 08/13/21 02:55 50-32-808/12/21 05:265.0 1
Benzo(b)fluoranthene ND ug/L 08/13/21 02:55 205-99-208/12/21 05:265.0 1
Benzo(g,h,i)perylene ND ug/L 08/13/21 02:55 191-24-208/12/21 05:265.0 1
Benzo(k)fluoranthene ND ug/L 08/13/21 02:55 207-08-908/12/21 05:265.0 1
4-Bromophenylphenyl ether ND ug/L 08/13/21 02:55 101-55-308/12/21 05:265.0 1
Butylbenzylphthalate ND ug/L 08/13/21 02:55 85-68-708/12/21 05:265.0 1
4-Chloro-3-methylphenol ND ug/L 08/13/21 02:55 59-50-708/12/21 05:265.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/13/21 02:55 111-91-108/12/21 05:2610.0 1
bis(2-Chloroethyl) ether ND ug/L 08/13/21 02:55 111-44-408/12/21 05:265.0 1
2-Chloronaphthalene ND ug/L 08/13/21 02:55 91-58-708/12/21 05:265.0 1
2-Chlorophenol ND ug/L 08/13/21 02:55 95-57-808/12/21 05:265.0 1
4-Chlorophenylphenyl ether ND ug/L 08/13/21 02:55 7005-72-308/12/21 05:265.0 1
Chrysene ND ug/L 08/13/21 02:55 218-01-908/12/21 05:265.0 1
Dibenz(a,h)anthracene ND ug/L 08/13/21 02:55 53-70-308/12/21 05:265.0 1
3,3'-Dichlorobenzidine ND ug/L 08/13/21 02:55 91-94-108/12/21 05:2610.0 1
2,4-Dichlorophenol ND ug/L 08/13/21 02:55 120-83-208/12/21 05:265.0 1
Diethylphthalate ND ug/L 08/13/21 02:55 84-66-208/12/21 05:265.0 1
2,4-Dimethylphenol ND ug/L 08/13/21 02:55 105-67-908/12/21 05:2610.0 1
Dimethylphthalate ND ug/L 08/13/21 02:55 131-11-308/12/21 05:265.0 1
Di-n-butylphthalate ND ug/L 08/13/21 02:55 84-74-208/12/21 05:265.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/13/21 02:55 534-52-108/12/21 05:2610.0 1
2,4-Dinitrophenol ND ug/L 08/13/21 02:55 51-28-508/12/21 05:2650.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:GW-1 Lab ID:92554623008 Collected:08/06/21 09:20 Received:08/09/21 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
2,4-Dinitrotoluene ND ug/L 08/13/21 02:55 121-14-208/12/21 05:265.0 1
2,6-Dinitrotoluene ND ug/L 08/13/21 02:55 606-20-208/12/21 05:265.0 1
Di-n-octylphthalate ND ug/L 08/13/21 02:55 117-84-008/12/21 05:265.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/13/21 02:55 117-81-708/12/21 05:265.0 1
Fluoranthene ND ug/L 08/13/21 02:55 206-44-008/12/21 05:265.0 1
Fluorene ND ug/L 08/13/21 02:55 86-73-708/12/21 05:265.0 1
Hexachloro-1,3-butadiene ND ug/L 08/13/21 02:55 87-68-308/12/21 05:265.0 1
Hexachlorobenzene ND ug/L 08/13/21 02:55 118-74-108/12/21 05:265.0 1
Hexachlorocyclopentadiene ND ug/L 08/13/21 02:55 77-47-408/12/21 05:2610.0 1
Hexachloroethane ND ug/L 08/13/21 02:55 67-72-108/12/21 05:265.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/13/21 02:55 193-39-508/12/21 05:265.0 1
Isophorone ND ug/L 08/13/21 02:55 78-59-108/12/21 05:2610.0 1
Naphthalene ND ug/L 08/13/21 02:55 91-20-308/12/21 05:265.0 1
Nitrobenzene ND ug/L 08/13/21 02:55 98-95-308/12/21 05:265.0 1
2-Nitrophenol ND ug/L 08/13/21 02:55 88-75-508/12/21 05:265.0 1
4-Nitrophenol ND ug/L 08/13/21 02:55 100-02-708/12/21 05:2610.0 1
N-Nitrosodimethylamine ND ug/L 08/13/21 02:55 62-75-908/12/21 05:265.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/13/21 02:55 621-64-708/12/21 05:265.0 1
N-Nitrosodiphenylamine ND ug/L 08/13/21 02:55 86-30-608/12/21 05:2610.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/13/21 02:55 108-60-108/12/21 05:265.0 1
Pentachlorophenol ND ug/L 08/13/21 02:55 87-86-508/12/21 05:2610.0 1
Phenanthrene ND ug/L 08/13/21 02:55 85-01-808/12/21 05:265.0 1
Phenol ND ug/L 08/13/21 02:55 108-95-208/12/21 05:265.0 1
Pyrene ND ug/L 08/13/21 02:55 129-00-008/12/21 05:265.0 1
1,2,4-Trichlorobenzene ND ug/L 08/13/21 02:55 120-82-108/12/21 05:265.0 1
2,4,6-Trichlorophenol ND ug/L 08/13/21 02:55 88-06-208/12/21 05:2610.0 1
Surrogates
Nitrobenzene-d5 (S)82 %08/13/21 02:55 4165-60-008/12/21 05:2610-120 1
2-Fluorobiphenyl (S)74 %08/13/21 02:55 321-60-808/12/21 05:2615-120 1
Terphenyl-d14 (S)81 %08/13/21 02:55 1718-51-008/12/21 05:2611-131 1
Phenol-d6 (S)45 %08/13/21 02:55 13127-88-308/12/21 05:2610-120 1
2-Fluorophenol (S)61 %08/13/21 02:55 367-12-408/12/21 05:2610-120 1
2,4,6-Tribromophenol (S)89 %08/13/21 02:55 118-79-608/12/21 05:2610-137 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 08/13/21 15:25 71-43-20.50 1
Bromobenzene ND ug/L 08/13/21 15:25 108-86-10.50 1
Bromochloromethane ND ug/L 08/13/21 15:25 74-97-50.50 1
Bromodichloromethane ND ug/L 08/13/21 15:25 75-27-40.50 1
Bromoform ND ug/L 08/13/21 15:25 75-25-20.50 1
Bromomethane ND ug/L 08/13/21 15:25 74-83-95.0 1
n-Butylbenzene ND ug/L 08/13/21 15:25 104-51-80.50 1
sec-Butylbenzene ND ug/L 08/13/21 15:25 135-98-80.50 1
tert-Butylbenzene ND ug/L 08/13/21 15:25 98-06-60.50 1
Carbon tetrachloride ND ug/L 08/13/21 15:25 56-23-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:GW-1 Lab ID:92554623008 Collected:08/06/21 09:20 Received:08/09/21 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 08/13/21 15:25 108-90-70.50 1
Chloroethane ND ug/L 08/13/21 15:25 75-00-31.0 1
Chloroform ND ug/L 08/13/21 15:25 67-66-30.50 1
Chloromethane ND ug/L 08/13/21 15:25 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/13/21 15:25 95-49-80.50 1
4-Chlorotoluene ND ug/L 08/13/21 15:25 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 08/13/21 15:25 96-12-81.0 1
Dibromochloromethane ND ug/L 08/13/21 15:25 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 08/13/21 15:25 106-93-40.50 1
Dibromomethane ND ug/L 08/13/21 15:25 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 08/13/21 15:25 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 08/13/21 15:25 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 08/13/21 15:25 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 08/13/21 15:25 75-71-80.50 1
1,1-Dichloroethane ND ug/L 08/13/21 15:25 75-34-30.50 1
1,2-Dichloroethane ND ug/L 08/13/21 15:25 107-06-20.50 1
1,1-Dichloroethene ND ug/L 08/13/21 15:25 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 08/13/21 15:25 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 08/13/21 15:25 156-60-50.50 1
1,2-Dichloropropane ND ug/L 08/13/21 15:25 78-87-50.50 1
1,3-Dichloropropane ND ug/L 08/13/21 15:25 142-28-90.50 1
2,2-Dichloropropane ND ug/L 08/13/21 15:25 594-20-70.50 1
1,1-Dichloropropene ND ug/L 08/13/21 15:25 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 08/13/21 15:25 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 08/13/21 15:25 10061-02-60.50 1
Diisopropyl ether ND ug/L 08/13/21 15:25 108-20-30.50 1
Ethylbenzene ND ug/L 08/13/21 15:25 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 08/13/21 15:25 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 08/13/21 15:25 98-82-80.50 1
Methylene Chloride ND ug/L 08/13/21 15:25 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 08/13/21 15:25 1634-04-40.50 1
Naphthalene ND ug/L 08/13/21 15:25 91-20-32.0 1
n-Propylbenzene ND ug/L 08/13/21 15:25 103-65-10.50 1
Styrene ND ug/L 08/13/21 15:25 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 08/13/21 15:25 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 08/13/21 15:25 79-34-50.50 1
Tetrachloroethene ND ug/L 08/13/21 15:25 127-18-40.50 1
Toluene ND ug/L 08/13/21 15:25 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 08/13/21 15:25 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 08/13/21 15:25 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 08/13/21 15:25 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 08/13/21 15:25 79-00-50.50 1
Trichloroethene ND ug/L 08/13/21 15:25 79-01-60.50 1
Trichlorofluoromethane ND ug/L 08/13/21 15:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/13/21 15:25 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 08/13/21 15:25 95-63-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554623
391
Sample:GW-1 Lab ID:92554623008 Collected:08/06/21 09:20 Received:08/09/21 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3,5-Trimethylbenzene ND ug/L 08/13/21 15:25 108-67-80.50 1
Vinyl chloride ND ug/L 08/13/21 15:25 75-01-41.0 1
m&p-Xylene ND ug/L 08/13/21 15:25 179601-23-11.0 1
o-Xylene ND ug/L 08/13/21 15:25 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %08/13/21 15:25 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %08/13/21 15:25 460-00-470-130 1
Toluene-d8 (S)98 %08/13/21 15:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
639568
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357097
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/11/21 13:50
4-Bromofluorobenzene (S)%103 66-131 08/11/21 13:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357098LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.449.8 99 70-130
4-Bromofluorobenzene (S)%98 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3357100MATRIX SPIKE SAMPLE:
MSSpike
Result
92553987002
Gas Range Organics (C6-C10)mg/kg 162150 108 70-145ND
4-Bromofluorobenzene (S)%93 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92553984002
3357099SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%9697
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
640315
MADEP VPH
MADEP VPH
VPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3360721
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N208/13/21 13:51
Aromatic (C09-C10)ug/L ND 50.0 N208/13/21 13:51
4-Bromofluorobenzene (FID) (S)%89 70-130 08/13/21 13:51
4-Bromofluorobenzene (PID) (S)%95 70-130 08/13/21 13:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3360722LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3360723
Aliphatic (C05-C08)ug/L 332 N230011170-13096289 14 25
Aromatic (C09-C10)ug/L 119 N210011970-130112112 7 25
4-Bromofluorobenzene (FID) (S)%104 70-130102
4-Bromofluorobenzene (PID) (S)%107 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
640221
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3360027
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/13/21 11:48
1,1,1-Trichloroethane ug/L ND 0.50 08/13/21 11:48
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/13/21 11:48
1,1,2-Trichloroethane ug/L ND 0.50 08/13/21 11:48
1,1-Dichloroethane ug/L ND 0.50 08/13/21 11:48
1,1-Dichloroethene ug/L ND 0.50 08/13/21 11:48
1,1-Dichloropropene ug/L ND 0.50 08/13/21 11:48
1,2,3-Trichlorobenzene ug/L ND 2.0 08/13/21 11:48
1,2,3-Trichloropropane ug/L ND 0.50 08/13/21 11:48
1,2,4-Trichlorobenzene ug/L ND 2.0 08/13/21 11:48
1,2,4-Trimethylbenzene ug/L ND 0.50 08/13/21 11:48
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/13/21 11:48
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/13/21 11:48
1,2-Dichlorobenzene ug/L ND 0.50 08/13/21 11:48
1,2-Dichloroethane ug/L ND 0.50 08/13/21 11:48
1,2-Dichloropropane ug/L ND 0.50 08/13/21 11:48
1,3,5-Trimethylbenzene ug/L ND 0.50 08/13/21 11:48
1,3-Dichlorobenzene ug/L ND 0.50 08/13/21 11:48
1,3-Dichloropropane ug/L ND 0.50 08/13/21 11:48
1,4-Dichlorobenzene ug/L ND 0.50 08/13/21 11:48
2,2-Dichloropropane ug/L ND 0.50 08/13/21 11:48
2-Chlorotoluene ug/L ND 0.50 08/13/21 11:48
4-Chlorotoluene ug/L ND 0.50 08/13/21 11:48
Benzene ug/L ND 0.50 08/13/21 11:48
Bromobenzene ug/L ND 0.50 08/13/21 11:48
Bromochloromethane ug/L ND 0.50 08/13/21 11:48
Bromodichloromethane ug/L ND 0.50 08/13/21 11:48
Bromoform ug/L ND 0.50 08/13/21 11:48
Bromomethane ug/L ND 5.0 08/13/21 11:48
Carbon tetrachloride ug/L ND 0.50 08/13/21 11:48
Chlorobenzene ug/L ND 0.50 08/13/21 11:48
Chloroethane ug/L ND 1.0 08/13/21 11:48
Chloroform ug/L ND 0.50 08/13/21 11:48
Chloromethane ug/L ND 1.0 08/13/21 11:48
cis-1,2-Dichloroethene ug/L ND 0.50 08/13/21 11:48
cis-1,3-Dichloropropene ug/L ND 0.50 08/13/21 11:48
Dibromochloromethane ug/L ND 0.50 08/13/21 11:48
Dibromomethane ug/L ND 0.50 08/13/21 11:48
Dichlorodifluoromethane ug/L ND 0.50 08/13/21 11:48
Diisopropyl ether ug/L ND 0.50 08/13/21 11:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3360027
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 08/13/21 11:48
Hexachloro-1,3-butadiene ug/L ND 2.0 08/13/21 11:48
Isopropylbenzene (Cumene)ug/L ND 0.50 08/13/21 11:48
m&p-Xylene ug/L ND 1.0 08/13/21 11:48
Methyl-tert-butyl ether ug/L ND 0.50 08/13/21 11:48
Methylene Chloride ug/L ND 2.0 08/13/21 11:48
n-Butylbenzene ug/L ND 0.50 08/13/21 11:48
n-Propylbenzene ug/L ND 0.50 08/13/21 11:48
Naphthalene ug/L ND 2.0 08/13/21 11:48
o-Xylene ug/L ND 0.50 08/13/21 11:48
sec-Butylbenzene ug/L ND 0.50 08/13/21 11:48
Styrene ug/L ND 0.50 08/13/21 11:48
tert-Butylbenzene ug/L ND 0.50 08/13/21 11:48
Tetrachloroethene ug/L ND 0.50 08/13/21 11:48
Toluene ug/L ND 0.50 08/13/21 11:48
trans-1,2-Dichloroethene ug/L ND 0.50 08/13/21 11:48
trans-1,3-Dichloropropene ug/L ND 0.50 08/13/21 11:48
Trichloroethene ug/L ND 0.50 08/13/21 11:48
Trichlorofluoromethane ug/L ND 1.0 08/13/21 11:48
Vinyl chloride ug/L ND 1.0 08/13/21 11:48
1,2-Dichloroethane-d4 (S)%99 70-130 08/13/21 11:48
4-Bromofluorobenzene (S)%98 70-130 08/13/21 11:48
Toluene-d8 (S)%100 70-130 08/13/21 11:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3360028LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.550 99 60-140
1,1,1-Trichloroethane ug/L 51.450 103 60-140
1,1,2,2-Tetrachloroethane ug/L 46.550 93 60-140
1,1,2-Trichloroethane ug/L 47.050 94 60-140
1,1-Dichloroethane ug/L 49.950 100 60-140
1,1-Dichloroethene ug/L 52.150 104 60-140
1,1-Dichloropropene ug/L 51.050 102 60-140
1,2,3-Trichlorobenzene ug/L 46.250 92 60-140
1,2,3-Trichloropropane ug/L 46.450 93 60-140
1,2,4-Trichlorobenzene ug/L 47.650 95 60-140
1,2,4-Trimethylbenzene ug/L 49.450 99 60-140
1,2-Dibromo-3-chloropropane ug/L 44.450 89 60-140
1,2-Dibromoethane (EDB)ug/L 48.750 97 60-140
1,2-Dichlorobenzene ug/L 50.050 100 60-140
1,2-Dichloroethane ug/L 47.150 94 60-140
1,2-Dichloropropane ug/L 49.050 98 60-140
1,3,5-Trimethylbenzene ug/L 49.050 98 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3360028LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.150 102 60-140
1,3-Dichloropropane ug/L 47.350 95 60-140
1,4-Dichlorobenzene ug/L 49.950 100 60-140
2,2-Dichloropropane ug/L 51.850 104 60-140
2-Chlorotoluene ug/L 50.650 101 60-140
4-Chlorotoluene ug/L 50.050 100 60-140
Benzene ug/L 50.050 100 60-140
Bromobenzene ug/L 48.450 97 60-140
Bromochloromethane ug/L 49.750 99 60-140
Bromodichloromethane ug/L 46.550 93 60-140
Bromoform ug/L 51.150 102 60-140
Bromomethane ug/L 47.350 95 60-140
Carbon tetrachloride ug/L 50.850 102 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 48.350 97 60-140
Chloroform ug/L 49.350 99 60-140
Chloromethane ug/L 42.150 84 60-140
cis-1,2-Dichloroethene ug/L 48.450 97 60-140
cis-1,3-Dichloropropene ug/L 49.950 100 60-140
Dibromochloromethane ug/L 50.850 102 60-140
Dibromomethane ug/L 50.150 100 60-140
Dichlorodifluoromethane ug/L 44.850 90 60-140
Diisopropyl ether ug/L 46.950 94 60-140
Ethylbenzene ug/L 49.650 99 60-140
Hexachloro-1,3-butadiene ug/L 48.450 97 60-140
Isopropylbenzene (Cumene)ug/L 51.250 102 60-140
m&p-Xylene ug/L 99.2100 99 60-140
Methyl-tert-butyl ether ug/L 45.350 91 60-140
Methylene Chloride ug/L 49.750 99 60-140
n-Butylbenzene ug/L 51.450 103 60-140
n-Propylbenzene ug/L 49.950 100 60-140
Naphthalene ug/L 44.350 89 60-140
o-Xylene ug/L 49.250 98 60-140
sec-Butylbenzene ug/L 49.750 99 60-140
Styrene ug/L 50.950 102 60-140
tert-Butylbenzene ug/L 42.350 85 60-140
Tetrachloroethene ug/L 50.250 100 60-140
Toluene ug/L 49.750 99 60-140
trans-1,2-Dichloroethene ug/L 49.750 99 60-140
trans-1,3-Dichloropropene ug/L 49.750 99 60-140
Trichloroethene ug/L 50.950 102 60-140
Trichlorofluoromethane ug/L 47.150 94 60-140
Vinyl chloride ug/L 46.750 93 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3360029MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92554005005
3360030
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 80 95 60-140103 880ND76.1 82.6
1,1,1-Trichloroethane ug/L 80 104 60-140113 880ND83.4 90.2
1,1,2,2-Tetrachloroethane ug/L 80 95 60-140101 780ND75.8 81.2
1,1,2-Trichloroethane ug/L 80 96 60-140103 780ND76.9 82.8
1,1-Dichloroethane ug/L 80 102 60-140108 580ND82.0 86.3
1,1-Dichloroethene ug/L 80 107 60-140114 780ND85.5 91.5
1,1-Dichloropropene ug/L 80 107 60-140112 580ND85.6 89.9
1,2,3-Trichlorobenzene ug/L 80 88 60-14099 1180ND70.4 79.0
1,2,3-Trichloropropane ug/L 80 96 60-140102 680ND77.1 81.9
1,2,4-Trichlorobenzene ug/L 80 86 60-14097 1280ND68.9 77.9
1,2,4-Trimethylbenzene ug/L 80 91 60-14098 780ND73.1 78.3
1,2-Dibromo-3-chloropropane ug/L 80 91 60-140102 1180ND73.2 81.3
1,2-Dibromoethane (EDB)ug/L 80 97 60-140103 680ND77.3 82.5
1,2-Dichlorobenzene ug/L 80 91 60-140101 1080ND73.0 80.7
1,2-Dichloroethane ug/L 80 97 60-140102 580ND77.5 81.9
1,2-Dichloropropane ug/L 80 99 60-140105 580ND79.3 83.6
1,3,5-Trimethylbenzene ug/L 80 92 60-140102 1080ND73.8 81.4
1,3-Dichlorobenzene ug/L 80 92 60-140102 1080ND73.4 81.4
1,3-Dichloropropane ug/L 80 96 60-140102 780ND76.4 81.6
1,4-Dichlorobenzene ug/L 80 90 60-14099 1080ND71.7 79.3
2,2-Dichloropropane ug/L 80 104 60-140111 680ND83.1 88.6
2-Chlorotoluene ug/L 80 96 60-140105 980ND76.6 83.7
4-Chlorotoluene ug/L 80 92 60-140100 880ND73.4 79.7
Benzene ug/L 80 101 60-140108 6802.3 83.3 88.6
Bromobenzene ug/L 80 90 60-14099 980ND72.3 79.3
Bromochloromethane ug/L 80 102 60-140111 880ND81.9 88.6
Bromodichloromethane ug/L 80 92 60-14098 780ND73.3 78.7
Bromoform ug/L 80 95 60-140102 780ND76.3 81.9
Bromomethane ug/L 80 89 60-140103 1480ND71.5 82.2
Carbon tetrachloride ug/L 80 105 60-140110 580ND83.7 88.2
Chlorobenzene ug/L 80 96 60-140104 880ND76.8 83.3
Chloroethane ug/L 80 92 60-140107 1580ND73.5 85.4
Chloroform ug/L 80 101 60-140109 780ND81.0 86.9
Chloromethane ug/L 80 82 60-14091 1180ND65.5 72.9
cis-1,2-Dichloroethene ug/L 80 98 60-140106 880ND78.3 84.8
cis-1,3-Dichloropropene ug/L 80 97 60-140102 580ND77.8 81.7
Dibromochloromethane ug/L 80 98 60-140107 980ND78.3 85.7
Dibromomethane ug/L 80 104 60-140108 380ND83.5 86.2
Dichlorodifluoromethane ug/L 80 95 60-140103 880ND76.0 82.3
Diisopropyl ether ug/L 80 95 60-140102 68012.7 88.9 94.0
Ethylbenzene ug/L 80 97 60-140104 780ND77.7 83.2
Hexachloro-1,3-butadiene ug/L 80 97 60-140106 980ND77.5 84.5
Isopropylbenzene (Cumene)ug/L 80 99 60-140107 880ND78.8 85.7
m&p-Xylene ug/L 160 96 60-140104 7160ND154166
Methyl-tert-butyl ether ug/L 80 114 60-140119 180400491495
Methylene Chloride ug/L 80 108 60-140112 380ND86.5 89.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3360029MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92554005005
3360030
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 80 94 60-140106 1280ND75.1 85.0
n-Propylbenzene ug/L 80 95 60-140104 980ND75.6 82.8
Naphthalene ug/L 80 85 60-14096 1180ND68.3 76.6
o-Xylene ug/L 80 93 60-140101 880ND74.3 80.5
sec-Butylbenzene ug/L 80 95 60-140104 980ND76.2 83.5
Styrene ug/L 80 92 60-140100 780ND74.0 79.6
tert-Butylbenzene ug/L 80 80 60-14089 1080ND64.2 71.0
Tetrachloroethene ug/L 80 100 60-140107 780ND79.9 85.5
Toluene ug/L 80 100 60-140106 680ND80.2 84.8
trans-1,2-Dichloroethene ug/L 80 104 60-140111 780ND82.9 89.1
trans-1,3-Dichloropropene ug/L 80 97 60-140103 580ND77.9 82.3
Trichloroethene ug/L 80 102 60-140110 880ND81.5 88.1
Trichlorofluoromethane ug/L 80 100 60-140108 880ND80.4 86.8
Vinyl chloride ug/L 80 96 60-140107 1180ND76.6 85.6
1,2-Dichloroethane-d4 (S)%102 70-130102
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
639742
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3358037
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 08/12/21 13:30
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 08/12/21 13:30
2,4,6-Trichlorophenol ug/L ND 10.0 08/12/21 13:30
2,4-Dichlorophenol ug/L ND 5.0 08/12/21 13:30
2,4-Dimethylphenol ug/L ND 10.0 08/12/21 13:30
2,4-Dinitrophenol ug/L ND 50.0 08/12/21 13:30
2,4-Dinitrotoluene ug/L ND 5.0 08/12/21 13:30
2,6-Dinitrotoluene ug/L ND 5.0 08/12/21 13:30
2-Chloronaphthalene ug/L ND 5.0 08/12/21 13:30
2-Chlorophenol ug/L ND 5.0 08/12/21 13:30
2-Nitrophenol ug/L ND 5.0 08/12/21 13:30
3,3'-Dichlorobenzidine ug/L ND 10.0 08/12/21 13:30
4,6-Dinitro-2-methylphenol ug/L ND 10.0 08/12/21 13:30
4-Bromophenylphenyl ether ug/L ND 5.0 08/12/21 13:30
4-Chloro-3-methylphenol ug/L ND 5.0 08/12/21 13:30
4-Chlorophenylphenyl ether ug/L ND 5.0 08/12/21 13:30
4-Nitrophenol ug/L ND 10.0 08/12/21 13:30
Acenaphthene ug/L ND 5.0 08/12/21 13:30
Acenaphthylene ug/L ND 5.0 08/12/21 13:30
Anthracene ug/L ND 5.0 08/12/21 13:30
Benzo(a)anthracene ug/L ND 5.0 08/12/21 13:30
Benzo(a)pyrene ug/L ND 5.0 08/12/21 13:30
Benzo(b)fluoranthene ug/L ND 5.0 08/12/21 13:30
Benzo(g,h,i)perylene ug/L ND 5.0 08/12/21 13:30
Benzo(k)fluoranthene ug/L ND 5.0 08/12/21 13:30
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/12/21 13:30
bis(2-Chloroethyl) ether ug/L ND 5.0 08/12/21 13:30
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 08/12/21 13:30
Butylbenzylphthalate ug/L ND 5.0 08/12/21 13:30
Chrysene ug/L ND 5.0 08/12/21 13:30
Di-n-butylphthalate ug/L ND 5.0 08/12/21 13:30
Di-n-octylphthalate ug/L ND 5.0 08/12/21 13:30
Dibenz(a,h)anthracene ug/L ND 5.0 08/12/21 13:30
Diethylphthalate ug/L ND 5.0 08/12/21 13:30
Dimethylphthalate ug/L ND 5.0 08/12/21 13:30
Fluoranthene ug/L ND 5.0 08/12/21 13:30
Fluorene ug/L ND 5.0 08/12/21 13:30
Hexachloro-1,3-butadiene ug/L ND 5.0 08/12/21 13:30
Hexachlorobenzene ug/L ND 5.0 08/12/21 13:30
Hexachlorocyclopentadiene ug/L ND 10.0 08/12/21 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3358037
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 08/12/21 13:30
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 08/12/21 13:30
Isophorone ug/L ND 10.0 08/12/21 13:30
N-Nitroso-di-n-propylamine ug/L ND 5.0 08/12/21 13:30
N-Nitrosodimethylamine ug/L ND 5.0 08/12/21 13:30
N-Nitrosodiphenylamine ug/L ND 10.0 08/12/21 13:30
Naphthalene ug/L ND 5.0 08/12/21 13:30
Nitrobenzene ug/L ND 5.0 08/12/21 13:30
Pentachlorophenol ug/L ND 10.0 08/12/21 13:30
Phenanthrene ug/L ND 5.0 08/12/21 13:30
Phenol ug/L ND 5.0 08/12/21 13:30
Pyrene ug/L ND 5.0 08/12/21 13:30
2,4,6-Tribromophenol (S)%96 10-137 08/12/21 13:30
2-Fluorobiphenyl (S)%90 15-120 08/12/21 13:30
2-Fluorophenol (S)%62 10-120 08/12/21 13:30
Nitrobenzene-d5 (S)%83 10-120 08/12/21 13:30
Phenol-d6 (S)%46 10-120 08/12/21 13:30
Terphenyl-d14 (S)%103 11-131 08/12/21 13:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3358038LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 43.550 87 44-142
2,2'-Oxybis(1-chloropropane)ug/L 45.150 90 36-166
2,4,6-Trichlorophenol ug/L 54.950 110 37-144
2,4-Dichlorophenol ug/L 52.150 104 1-191
2,4-Dimethylphenol ug/L 51.150 102 32-119
2,4-Dinitrophenol ug/L 274250 110 1-181
2,4-Dinitrotoluene ug/L 51.450 103 39-139
2,6-Dinitrotoluene ug/L 54.150 108 50-158
2-Chloronaphthalene ug/L 50.550 101 60-118
2-Chlorophenol ug/L 49.850 100 23-134
2-Nitrophenol ug/L 51.850 104 29-182
3,3'-Dichlorobenzidine ug/L 116100 116 1-262
4,6-Dinitro-2-methylphenol ug/L 117100 117 1-181
4-Bromophenylphenyl ether ug/L 53.250 106 53-127
4-Chloro-3-methylphenol ug/L 95.6100 96 22-147
4-Chlorophenylphenyl ether ug/L 48.750 97 25-158
4-Nitrophenol ug/L 154250 61 1-132
Acenaphthene ug/L 52.650 105 47-145
Acenaphthylene ug/L 53.950 108 33-145
Anthracene ug/L 54.450 109 1-166
Benzo(a)anthracene ug/L 52.850 106 33-143
Benzo(a)pyrene ug/L 54.150 108 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3358038LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 53.050 106 24-159
Benzo(g,h,i)perylene ug/L 48.950 98 1-219
Benzo(k)fluoranthene ug/L 53.450 107 11-162
bis(2-Chloroethoxy)methane ug/L 46.150 92 33-184
bis(2-Chloroethyl) ether ug/L 57.250 114 12-158
bis(2-Ethylhexyl)phthalate ug/L 58.550 117 8-158
Butylbenzylphthalate ug/L 59.050 118 1-152
Chrysene ug/L 52.750 105 17-168
Di-n-butylphthalate ug/L 58.650 117 1-118
Di-n-octylphthalate ug/L 60.050 120 4-146
Dibenz(a,h)anthracene ug/L 50.150 100 1-227
Diethylphthalate ug/L 49.850 100 1-114
Dimethylphthalate ug/L 50.050 100 1-112
Fluoranthene ug/L 54.050 108 26-137
Fluorene ug/L 50.950 102 59-121
Hexachloro-1,3-butadiene ug/L 39.750 79 24-116
Hexachlorobenzene ug/L 49.550 99 1-152
Hexachlorocyclopentadiene ug/L 46.350 93 25-150
Hexachloroethane ug/L 42.050 84 40-113
Indeno(1,2,3-cd)pyrene ug/L 50.650 101 1-171
Isophorone ug/L 47.250 94 21-196
N-Nitroso-di-n-propylamine ug/L 49.750 99 1-230
N-Nitrosodimethylamine ug/L 43.750 87 25-150
N-Nitrosodiphenylamine ug/L 54.250 108 25-150
Naphthalene ug/L 49.550 99 21-133
Nitrobenzene ug/L 47.350 95 35-180
Pentachlorophenol ug/L 93.4100 93 14-176
Phenanthrene ug/L 52.450 105 54-120
Phenol ug/L 32.550 65 5-112
Pyrene ug/L 55.350 111 52-115
2,4,6-Tribromophenol (S)%132 10-137
2-Fluorobiphenyl (S)%110 15-120
2-Fluorophenol (S)%78 10-120
Nitrobenzene-d5 (S)%99 10-120
Phenol-d6 (S)%63 10-120
Terphenyl-d14 (S)%112 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3358039MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35654271001
3358040
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 69 44-14271 3501.7U 34.5 35.5
2,2'-Oxybis(1-chloropropane)ug/L 50 81 36-16681 0501.2U 40.5 40.6
2,4,6-Trichlorophenol ug/L M1501837-14482501.6U 9.2J 41.0
2,4-Dichlorophenol ug/L R150511-19194 59501.4U 25.6 47.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3358039MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35654271001
3358040
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L 50 91 32-11992 1501.7U 45.3 45.8
2,4-Dinitrophenol ug/L M125001-181525026.0U ND ND
2,4-Dinitrotoluene ug/L 50 88 39-13991 3501.6U 44.2 45.5
2,6-Dinitrotoluene ug/L 50 83 50-15889 6501.7U 41.7 44.5
2-Chloronaphthalene ug/L 50 80 60-11882 2501.7U 40.2 41.1
2-Chlorophenol ug/L R1504823-13485 54501.2U 24.2 42.3
2-Nitrophenol ug/L R1504629-18290 64501.4U 23.2 45.0
3,3'-Dichlorobenzidine ug/L 100 74 1-26278 51008.1U 74.2 78.1
4,6-Dinitro-2-methylphenol ug/L 100 4 1-181331003.4U 3.5J 32.5
4-Bromophenylphenyl ether ug/L 50 90 53-12793 4501.8U 45.1 46.7
4-Chloro-3-methylphenol ug/L 100 92 22-147100 91003.3U 92.1 100
4-Chlorophenylphenyl ether ug/L 50 88 25-15890 2502.0U 44.0 45.1
4-Nitrophenol ug/L M125001-132222506.6U ND 53.8
Acenaphthene ug/L 50 86 47-14588 2502.0U 43.2 43.9
Acenaphthylene ug/L 50 88 33-14590 2502.0U 44.1 44.8
Anthracene ug/L 50 90 1-16694 4502.3U 44.9 46.8
Benzo(a)anthracene ug/L 50 90 33-14397 8502.7U 45.0 48.7
Benzo(a)pyrene ug/L 50 91 17-16396 5502.8U 45.6 47.9
Benzo(b)fluoranthene ug/L 50 89 24-15996 7502.6U 44.7 48.0
Benzo(g,h,i)perylene ug/L 50 94 1-21999 5502.8U 46.9 49.4
Benzo(k)fluoranthene ug/L 50 92 11-16294 3502.7U 46.0 47.2
bis(2-Chloroethoxy)methane ug/L 50 87 33-18489 2501.8U 43.4 44.3
bis(2-Chloroethyl) ether ug/L 50 92 12-15893 2501.9U 45.8 46.6
bis(2-Ethylhexyl)phthalate ug/L 50 96 8-158100 4503.7U 48.2 50.1
Butylbenzylphthalate ug/L 50 96 1-152101 5503.1U 47.8 50.4
Chrysene ug/L 50 89 17-16895 7502.8U 44.3 47.6
Di-n-butylphthalate ug/L 50 91 1-11898 7502.2U 45.7 48.8
Di-n-octylphthalate ug/L 50 98 4-146103 6503.9U 48.8 51.6
Dibenz(a,h)anthracene ug/L 50 96 1-227100 5503.0U 47.8 50.2
Diethylphthalate ug/L 50 86 1-11490 4502.0U 43.1 45.0
Dimethylphthalate ug/L 50 85 1-11287 2502.1U 42.7 43.6
Fluoranthene ug/L 50 91 26-13796 6502.2U 45.5 48.1
Fluorene ug/L 50 88 59-12191 3502.1U 43.9 45.5
Hexachloro-1,3-butadiene ug/L 50 66 24-11668 4501.8U 33.0 34.2
Hexachlorobenzene ug/L 50 85 1-15289 5502.2U 42.7 44.7
Hexachlorocyclopentadiene ug/L 50 65 25-15067 3501.6U 32.3 33.3
Hexachloroethane ug/L 50 69 40-11369 1501.4U 34.3 34.6
Indeno(1,2,3-cd)pyrene ug/L 50 95 1-17199 5502.9U 47.5 49.7
Isophorone ug/L 50 87 21-19689 3501.7U 43.3 44.5
N-Nitroso-di-n-propylamine ug/L 50 89 1-23088 1501.3U 44.6 44.2
N-Nitrosodimethylamine ug/L 50 70 25-15071 2501.9U 34.8 35.6
N-Nitrosodiphenylamine ug/L 50 89 25-15094 5503.0U 44.4 46.9
Naphthalene ug/L 50 76 21-13378 3502.1U 37.9 38.9
Nitrobenzene ug/L 50 90 35-18091 1501.9U 44.8 45.4
Pentachlorophenol ug/L M1100714-176631003.8U 7.3J 62.9
Phenanthrene ug/L 50 89 54-12093 5502.0U 44.3 46.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3358039MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35654271001
3358040
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L R150395-11255 35501.4U 19.4 27.6
Pyrene ug/L 50 89 52-11595 7502.2U 44.3 47.6
2,4,6-Tribromophenol (S)%34 10-13796
2-Fluorobiphenyl (S)%81 15-12084
2-Fluorophenol (S)%20 10-12064
Nitrobenzene-d5 (S)%84 10-12089
Phenol-d6 (S)%39 10-12053
Terphenyl-d14 (S)%90 11-13197
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
639453
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3356568
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.1 08/12/21 11:47
n-Pentacosane (S)%65 32-130 08/12/21 11:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3356569LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 57.066.2 86 47-130
n-Pentacosane (S)%82 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3356570MATRIX SPIKE SAMPLE:
MSSpike
Result
92554238001
Diesel Range Organics(C10-C28)mg/kg 476 M185.5 144 10-133353
n-Pentacosane (S)%73 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92554238002
3356571SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 385 D662731
n-Pentacosane (S)%6371
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
640746
EPA 3546
EPA 8015C Modified
8015 Solid GCSV ORO
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3362803
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Matrix:Solid
Analyzed
Oil Range Organics (C28-C40)mg/kg ND 14.8 08/17/21 17:50
n-Pentacosane (S)%43 32-130 08/17/21 17:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3362804LABORATORY CONTROL SAMPLE:
LCSSpike
Oil Range Organics (C28-C40)mg/kg 67.182.5 81 50-130
n-Pentacosane (S)%65 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3362805MATRIX SPIKE SAMPLE:
MSSpike
Result
92554619001
Oil Range Organics (C28-C40)mg/kg 11098.3 71 37-13040.6
n-Pentacosane (S)%43 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92554619002
3362806SAMPLE DUPLICATE:
Oil Range Organics (C28-C40)mg/kg 7.2JND
n-Pentacosane (S)%5554
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
640108
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3359670
Associated Lab Samples:92554623008
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N208/16/21 08:13
Aliphatic (C19-C36)ug/L ND 100 N208/16/21 08:13
Aromatic (C11-C22)ug/L ND 100 N208/16/21 08:13
1-Chlorooctadecane (S)%24 40-140 S008/16/21 08:13
2-Bromonaphthalene (S)%67 40-140 08/16/21 08:13
2-Fluorobiphenyl (S)%67 40-140 08/16/21 08:13
o-Terphenyl (S)%36 40-140 S008/16/21 08:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3359671LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3359672
Aliphatic (C09-C18)ug/L 148 N23004940-14073220 39 50
Aliphatic (C19-C36)ug/L 262 N24006640-14092368 34 50
Aromatic (C11-C22)ug/L 414 N28504940-14078662 46 50
1-Chlorooctadecane (S)%42 40-14061
2-Bromonaphthalene (S)%60 40-14077
2-Fluorobiphenyl (S)%62 40-14078
o-Terphenyl (S)%53 40-14082
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/18/2021 11:23 AM
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Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554623
391
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
639609
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92554623001, 92554623002, 92554623003, 92554623004, 92554623005, 92554623006, 92554623007
Parameter Units
Dup
Result QualifiersRPDResult
92554313006
3357388SAMPLE DUPLICATE:
Percent Moisture %25.8 N2424.8
Parameter Units
Dup
Result QualifiersRPDResult
92554354001
3357389SAMPLE DUPLICATE:
Percent Moisture %79.1 N2178.3
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92554623
391
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was re-extracted within hold time. Results from re-extraction confirm initial analysis.1g
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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Page 32 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92554623
391
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92554623001 639453 639853K1EPA 3546 EPA 8015C Modified
92554623002 639453 639853K2EPA 3546 EPA 8015C Modified
92554623003 639453 639853K3EPA 3546 EPA 8015C Modified
92554623004 639453 639853K4EPA 3546 EPA 8015C Modified
92554623005 639453 639853K5EPA 3546 EPA 8015C Modified
92554623006 639453 639853K6EPA 3546 EPA 8015C Modified
92554623007 639453 639853K7EPA 3546 EPA 8015C Modified
92554623001 640746 640862K1EPA 3546 EPA 8015C Modified
92554623002 640746 640862K2EPA 3546 EPA 8015C Modified
92554623003 640746 640862K3EPA 3546 EPA 8015C Modified
92554623004 640746 640862K4EPA 3546 EPA 8015C Modified
92554623005 640746 640862K5EPA 3546 EPA 8015C Modified
92554623006 640746 640862K6EPA 3546 EPA 8015C Modified
92554623007 640746 640862K7EPA 3546 EPA 8015C Modified
92554623008 640108 640559GW-1 MADEP EPH MADEP EPH
92554623001 639568 639588K1EPA 5030B EPA 8015C Modified
92554623002 639568 639588K2EPA 5030B EPA 8015C Modified
92554623003 639568 639588K3EPA 5030B EPA 8015C Modified
92554623004 639568 639588K4EPA 5030B EPA 8015C Modified
92554623005 639568 639588K5EPA 5030B EPA 8015C Modified
92554623006 639568 639588K6EPA 5030B EPA 8015C Modified
92554623007 639568 639588K7EPA 5030B EPA 8015C Modified
92554623008 640315GW-1 MADEP VPH
92554623008 639742 639974GW-1 EPA 625.1 EPA 625.1
92554623008 640221GW-1 SM 6200B
92554623001 639609K1SW-846
92554623002 639609K2SW-846
92554623003 639609K3SW-846
92554623004 639609K4SW-846
92554623005 639609K5SW-846
92554623006 639609K6SW-846
92554623007 639609K7SW-846
REPORT OF LABORATORY ANALYSIS
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Page 34 of 36
Page 35 of 36
Page 36 of 36

APPENDIX F
GROUNDWATER LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
February 22, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92521416
92521416
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz 391, Greenville, NC
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on February 10, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92521416001 MW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PANTPR
EPA 8260D 63 PASI-CCL
92521416002 MW-2 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PANTPR
EPA 8260D 63 PASI-CCL
92521416003 MW-3 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PANTPR
EPA 8260D 63 PASI-CCL
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92521416001 MW-1
Total VPH 121 ug/L 02/14/21 06:55100MADEP VPH
92521416002 MW-2
Ethylbenzene 1.3 ug/L 02/12/21 15:071.0EPA 8260D
Toluene 5.5 ug/L 02/12/21 15:071.0EPA 8260D
Xylene (Total)25.9 ug/L 02/12/21 15:071.0EPA 8260D
m&p-Xylene 12.1 ug/L 02/12/21 15:072.0EPA 8260D
o-Xylene 13.8 ug/L 02/12/21 15:071.0EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-1 Lab ID:92521416001 Collected:02/09/21 12:04 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 02/17/21 18:12 N202/15/21 11:091001
Aliphatic (C19-C36)ND ug/L 02/17/21 18:12 N202/15/21 11:091001
Aromatic (C11-C22)ND ug/L 02/17/21 18:12 N202/15/21 11:091001
Surrogates
1-Chlorooctadecane (S)22 %02/17/21 18:12 3386-33-2 P2,S002/15/21 11:0940-140 1
o-Terphenyl (S)64 %02/17/21 18:12 84-15-102/15/21 11:0940-140 1
2-Fluorobiphenyl (S)97 %02/17/21 18:12 321-60-802/15/21 11:0940-140 1
2-Bromonaphthalene (S)102 %02/17/21 18:12 580-13-202/15/21 11:0940-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND ug/L 02/14/21 06:5502/14/21 06:551001
Aliphatic (C09-C12)ND ug/L 02/14/21 06:5502/14/21 06:551001
Aromatic (C09-C10),Unadjusted ND ug/L 02/14/21 06:55 TPHC9C10A02/14/21 06:551001
Total VPH 121 ug/L 02/14/21 06:55 VPH02/14/21 06:551001
Surrogates
2,5-Dibromotoluene (FID)97.3 %02/14/21 06:55 615-59-8FID02/14/21 06:5570.0-130 1
2,5-Dibromotoluene (PID)82.3 %02/14/21 06:55 615-59-8PID02/14/21 06:5570.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/12/21 14:50 67-64-125.0 1
Benzene ND ug/L 02/12/21 14:50 71-43-21.0 1
Bromobenzene ND ug/L 02/12/21 14:50 108-86-11.0 1
Bromochloromethane ND ug/L 02/12/21 14:50 74-97-51.0 1
Bromodichloromethane ND ug/L 02/12/21 14:50 75-27-41.0 1
Bromoform ND ug/L 02/12/21 14:50 75-25-21.0 1
Bromomethane ND ug/L 02/12/21 14:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 02/12/21 14:50 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/12/21 14:50 56-23-51.0 1
Chlorobenzene ND ug/L 02/12/21 14:50 108-90-71.0 1
Chloroethane ND ug/L 02/12/21 14:50 75-00-31.0 1
Chloroform ND ug/L 02/12/21 14:50 67-66-35.0 1
Chloromethane ND ug/L 02/12/21 14:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/12/21 14:50 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/12/21 14:50 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/12/21 14:50 96-12-85.0 1
Dibromochloromethane ND ug/L 02/12/21 14:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/12/21 14:50 106-93-41.0 1
Dibromomethane ND ug/L 02/12/21 14:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/12/21 14:50 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/12/21 14:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/12/21 14:50 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/12/21 14:50 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/12/21 14:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/12/21 14:50 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-1 Lab ID:92521416001 Collected:02/09/21 12:04 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1-Dichloroethene ND ug/L 02/12/21 14:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/12/21 14:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/12/21 14:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/12/21 14:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/12/21 14:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/12/21 14:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/12/21 14:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/12/21 14:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/12/21 14:50 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/12/21 14:50 108-20-31.0 1
Ethylbenzene ND ug/L 02/12/21 14:50 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/12/21 14:50 87-68-31.0 1
2-Hexanone ND ug/L 02/12/21 14:50 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/12/21 14:50 99-87-61.0 1
Methylene Chloride ND ug/L 02/12/21 14:50 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/12/21 14:50 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/12/21 14:50 1634-04-41.0 1
Naphthalene ND ug/L 02/12/21 14:50 91-20-31.0 1
Styrene ND ug/L 02/12/21 14:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/12/21 14:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/12/21 14:50 79-34-51.0 1
Tetrachloroethene ND ug/L 02/12/21 14:50 127-18-41.0 1
Toluene ND ug/L 02/12/21 14:50 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/12/21 14:50 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/12/21 14:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/12/21 14:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/12/21 14:50 79-00-51.0 1
Trichloroethene ND ug/L 02/12/21 14:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/12/21 14:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/12/21 14:50 96-18-41.0 1
Vinyl acetate ND ug/L 02/12/21 14:50 108-05-42.0 1
Vinyl chloride ND ug/L 02/12/21 14:50 75-01-41.0 1
Xylene (Total)ND ug/L 02/12/21 14:50 1330-20-71.0 1
m&p-Xylene ND ug/L 02/12/21 14:50 179601-23-12.0 1
o-Xylene ND ug/L 02/12/21 14:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %02/12/21 14:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/12/21 14:50 17060-07-070-130 1
Toluene-d8 (S)106 %02/12/21 14:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-2 Lab ID:92521416002 Collected:02/09/21 15:00 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 02/17/21 18:39 N202/15/21 11:091001
Aliphatic (C19-C36)ND ug/L 02/17/21 18:39 N202/15/21 11:091001
Aromatic (C11-C22)ND ug/L 02/17/21 18:39 N202/15/21 11:091001
Surrogates
1-Chlorooctadecane (S)28 %02/17/21 18:39 3386-33-2 P2,S002/15/21 11:0940-140 1
o-Terphenyl (S)65 %02/17/21 18:39 84-15-102/15/21 11:0940-140 1
2-Fluorobiphenyl (S)106 %02/17/21 18:39 321-60-802/15/21 11:0940-140 1
2-Bromonaphthalene (S)106 %02/17/21 18:39 580-13-202/15/21 11:0940-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND ug/L 02/14/21 07:2802/14/21 07:281001
Aliphatic (C09-C12)ND ug/L 02/14/21 07:2802/14/21 07:281001
Aromatic (C09-C10),Unadjusted ND ug/L 02/14/21 07:28 TPHC9C10A02/14/21 07:281001
Total VPH ND ug/L 02/14/21 07:28 VPH02/14/21 07:281001
Surrogates
2,5-Dibromotoluene (FID)98.9 %02/14/21 07:28 615-59-8FID02/14/21 07:2870.0-130 1
2,5-Dibromotoluene (PID)83.6 %02/14/21 07:28 615-59-8PID02/14/21 07:2870.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/12/21 15:07 67-64-125.0 1
Benzene ND ug/L 02/12/21 15:07 71-43-21.0 1
Bromobenzene ND ug/L 02/12/21 15:07 108-86-11.0 1
Bromochloromethane ND ug/L 02/12/21 15:07 74-97-51.0 1
Bromodichloromethane ND ug/L 02/12/21 15:07 75-27-41.0 1
Bromoform ND ug/L 02/12/21 15:07 75-25-21.0 1
Bromomethane ND ug/L 02/12/21 15:07 74-83-92.0 1
2-Butanone (MEK)ND ug/L 02/12/21 15:07 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/12/21 15:07 56-23-51.0 1
Chlorobenzene ND ug/L 02/12/21 15:07 108-90-71.0 1
Chloroethane ND ug/L 02/12/21 15:07 75-00-31.0 1
Chloroform ND ug/L 02/12/21 15:07 67-66-35.0 1
Chloromethane ND ug/L 02/12/21 15:07 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/12/21 15:07 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/12/21 15:07 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/12/21 15:07 96-12-85.0 1
Dibromochloromethane ND ug/L 02/12/21 15:07 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/12/21 15:07 106-93-41.0 1
Dibromomethane ND ug/L 02/12/21 15:07 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/12/21 15:07 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/12/21 15:07 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/12/21 15:07 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/12/21 15:07 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/12/21 15:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/12/21 15:07 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-2 Lab ID:92521416002 Collected:02/09/21 15:00 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1-Dichloroethene ND ug/L 02/12/21 15:07 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/12/21 15:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/12/21 15:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/12/21 15:07 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/12/21 15:07 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/12/21 15:07 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/12/21 15:07 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/12/21 15:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/12/21 15:07 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/12/21 15:07 108-20-31.0 1
Ethylbenzene 1.3 ug/L 02/12/21 15:07 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/12/21 15:07 87-68-31.0 1
2-Hexanone ND ug/L 02/12/21 15:07 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/12/21 15:07 99-87-61.0 1
Methylene Chloride ND ug/L 02/12/21 15:07 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/12/21 15:07 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/12/21 15:07 1634-04-41.0 1
Naphthalene ND ug/L 02/12/21 15:07 91-20-31.0 1
Styrene ND ug/L 02/12/21 15:07 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/12/21 15:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/12/21 15:07 79-34-51.0 1
Tetrachloroethene ND ug/L 02/12/21 15:07 127-18-41.0 1
Toluene 5.5 ug/L 02/12/21 15:07 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/12/21 15:07 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/12/21 15:07 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/12/21 15:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/12/21 15:07 79-00-51.0 1
Trichloroethene ND ug/L 02/12/21 15:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/12/21 15:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/12/21 15:07 96-18-41.0 1
Vinyl acetate ND ug/L 02/12/21 15:07 108-05-42.0 1
Vinyl chloride ND ug/L 02/12/21 15:07 75-01-41.0 1
Xylene (Total)25.9 ug/L 02/12/21 15:07 1330-20-71.0 1
m&p-Xylene 12.1 ug/L 02/12/21 15:07 179601-23-12.0 1
o-Xylene 13.8 ug/L 02/12/21 15:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %02/12/21 15:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/12/21 15:07 17060-07-070-130 1
Toluene-d8 (S)110 %02/12/21 15:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-3 Lab ID:92521416003 Collected:02/09/21 13:36 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 02/17/21 19:07 N202/15/21 11:091001
Aliphatic (C19-C36)ND ug/L 02/17/21 19:07 N202/15/21 11:091001
Aromatic (C11-C22)ND ug/L 02/17/21 19:07 N202/15/21 11:091001
Surrogates
1-Chlorooctadecane (S)29 %02/17/21 19:07 3386-33-2 P2,S002/15/21 11:0940-140 1
o-Terphenyl (S)68 %02/17/21 19:07 84-15-102/15/21 11:0940-140 1
2-Fluorobiphenyl (S)98 %02/17/21 19:07 321-60-802/15/21 11:0940-140 1
2-Bromonaphthalene (S)103 %02/17/21 19:07 580-13-202/15/21 11:0940-140 1
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)ND ug/L 02/14/21 08:0202/14/21 08:021001
Aliphatic (C09-C12)ND ug/L 02/14/21 08:0202/14/21 08:021001
Aromatic (C09-C10),Unadjusted ND ug/L 02/14/21 08:02 TPHC9C10A02/14/21 08:021001
Total VPH ND ug/L 02/14/21 08:02 VPH02/14/21 08:021001
Surrogates
2,5-Dibromotoluene (FID)101 %02/14/21 08:02 615-59-8FID02/14/21 08:0270.0-130 1
2,5-Dibromotoluene (PID)85.2 %02/14/21 08:02 615-59-8PID02/14/21 08:0270.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/12/21 15:25 67-64-125.0 1
Benzene ND ug/L 02/12/21 15:25 71-43-21.0 1
Bromobenzene ND ug/L 02/12/21 15:25 108-86-11.0 1
Bromochloromethane ND ug/L 02/12/21 15:25 74-97-51.0 1
Bromodichloromethane ND ug/L 02/12/21 15:25 75-27-41.0 1
Bromoform ND ug/L 02/12/21 15:25 75-25-21.0 1
Bromomethane ND ug/L 02/12/21 15:25 74-83-92.0 1
2-Butanone (MEK)ND ug/L 02/12/21 15:25 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/12/21 15:25 56-23-51.0 1
Chlorobenzene ND ug/L 02/12/21 15:25 108-90-71.0 1
Chloroethane ND ug/L 02/12/21 15:25 75-00-31.0 1
Chloroform ND ug/L 02/12/21 15:25 67-66-35.0 1
Chloromethane ND ug/L 02/12/21 15:25 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/12/21 15:25 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/12/21 15:25 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/12/21 15:25 96-12-85.0 1
Dibromochloromethane ND ug/L 02/12/21 15:25 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 02/12/21 15:25 106-93-41.0 1
Dibromomethane ND ug/L 02/12/21 15:25 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/12/21 15:25 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/12/21 15:25 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/12/21 15:25 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/12/21 15:25 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/12/21 15:25 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/12/21 15:25 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Sample:MW-3 Lab ID:92521416003 Collected:02/09/21 13:36 Received:02/10/21 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1-Dichloroethene ND ug/L 02/12/21 15:25 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/12/21 15:25 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/12/21 15:25 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/12/21 15:25 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/12/21 15:25 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/12/21 15:25 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/12/21 15:25 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/12/21 15:25 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/12/21 15:25 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/12/21 15:25 108-20-31.0 1
Ethylbenzene ND ug/L 02/12/21 15:25 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/12/21 15:25 87-68-31.0 1
2-Hexanone ND ug/L 02/12/21 15:25 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/12/21 15:25 99-87-61.0 1
Methylene Chloride ND ug/L 02/12/21 15:25 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/12/21 15:25 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/12/21 15:25 1634-04-41.0 1
Naphthalene ND ug/L 02/12/21 15:25 91-20-31.0 1
Styrene ND ug/L 02/12/21 15:25 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/12/21 15:25 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/12/21 15:25 79-34-51.0 1
Tetrachloroethene ND ug/L 02/12/21 15:25 127-18-41.0 1
Toluene ND ug/L 02/12/21 15:25 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/12/21 15:25 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/12/21 15:25 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/12/21 15:25 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/12/21 15:25 79-00-51.0 1
Trichloroethene ND ug/L 02/12/21 15:25 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/12/21 15:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/12/21 15:25 96-18-41.0 1
Vinyl acetate ND ug/L 02/12/21 15:25 108-05-42.0 1
Vinyl chloride ND ug/L 02/12/21 15:25 75-01-41.0 1
Xylene (Total)ND ug/L 02/12/21 15:25 1330-20-71.0 1
m&p-Xylene ND ug/L 02/12/21 15:25 179601-23-12.0 1
o-Xylene ND ug/L 02/12/21 15:25 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %02/12/21 15:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/12/21 15:25 17060-07-070-130 1
Toluene-d8 (S)106 %02/12/21 15:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1621153
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92521416001, 92521416002, 92521416003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3623075-3
Associated Lab Samples:92521416001, 92521416002, 92521416003
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 100 02/14/21 02:30
Aliphatic (C09-C12)ug/L ND 100 02/14/21 02:30
Aromatic (C09-C10),Unadjusted ug/L ND 100 02/14/21 02:30
Total VPH ug/L ND 100 02/14/21 02:30
2,5-Dibromotoluene (FID)%94.9 70.0-130 02/14/21 02:30
2,5-Dibromotoluene (PID)%80.4 70.0-130 02/14/21 02:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3623075-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3623075-2
Aliphatic (C05-C08)ug/L 11501200 95.8 70.0-1301031230 6.72 25
Aliphatic (C09-C12)ug/L 16201400 116 70.0-1301221710 5.41 25
Aromatic (C09-C10),Unadjusted ug/L 191200 95.5 70.0-130101202 5.60 25
Total VPH ug/L 29602800 106 70.0-1301123140 5.90 25
2,5-Dibromotoluene (FID)%101 70.0-13097.9
2,5-Dibromotoluene (PID)%88.2 70.0-13084.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
599739
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92521416001, 92521416002, 92521416003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3161615
Associated Lab Samples:92521416001, 92521416002, 92521416003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/12/21 11:37
1,1,1-Trichloroethane ug/L ND 1.0 02/12/21 11:37
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/12/21 11:37
1,1,2-Trichloroethane ug/L ND 1.0 02/12/21 11:37
1,1-Dichloroethane ug/L ND 1.0 02/12/21 11:37
1,1-Dichloroethene ug/L ND 1.0 02/12/21 11:37
1,1-Dichloropropene ug/L ND 1.0 02/12/21 11:37
1,2,3-Trichlorobenzene ug/L ND 1.0 02/12/21 11:37
1,2,3-Trichloropropane ug/L ND 1.0 02/12/21 11:37
1,2,4-Trichlorobenzene ug/L ND 1.0 02/12/21 11:37
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/12/21 11:37
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/12/21 11:37
1,2-Dichlorobenzene ug/L ND 1.0 02/12/21 11:37
1,2-Dichloroethane ug/L ND 1.0 02/12/21 11:37
1,2-Dichloropropane ug/L ND 1.0 02/12/21 11:37
1,3-Dichlorobenzene ug/L ND 1.0 02/12/21 11:37
1,3-Dichloropropane ug/L ND 1.0 02/12/21 11:37
1,4-Dichlorobenzene ug/L ND 1.0 02/12/21 11:37
2,2-Dichloropropane ug/L ND 1.0 02/12/21 11:37
2-Butanone (MEK)ug/L ND 5.0 02/12/21 11:37
2-Chlorotoluene ug/L ND 1.0 02/12/21 11:37
2-Hexanone ug/L ND 5.0 02/12/21 11:37
4-Chlorotoluene ug/L ND 1.0 02/12/21 11:37
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/12/21 11:37
Acetone ug/L ND 25.0 02/12/21 11:37
Benzene ug/L ND 1.0 02/12/21 11:37
Bromobenzene ug/L ND 1.0 02/12/21 11:37
Bromochloromethane ug/L ND 1.0 02/12/21 11:37
Bromodichloromethane ug/L ND 1.0 02/12/21 11:37
Bromoform ug/L ND 1.0 02/12/21 11:37
Bromomethane ug/L ND 2.0 02/12/21 11:37
Carbon tetrachloride ug/L ND 1.0 02/12/21 11:37
Chlorobenzene ug/L ND 1.0 02/12/21 11:37
Chloroethane ug/L ND 1.0 02/12/21 11:37
Chloroform ug/L ND 5.0 02/12/21 11:37
Chloromethane ug/L ND 1.0 02/12/21 11:37
cis-1,2-Dichloroethene ug/L ND 1.0 02/12/21 11:37
cis-1,3-Dichloropropene ug/L ND 1.0 02/12/21 11:37
Dibromochloromethane ug/L ND 1.0 02/12/21 11:37
Dibromomethane ug/L ND 1.0 02/12/21 11:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3161615
Associated Lab Samples:92521416001, 92521416002, 92521416003
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 02/12/21 11:37
Diisopropyl ether ug/L ND 1.0 02/12/21 11:37
Ethylbenzene ug/L ND 1.0 02/12/21 11:37
Hexachloro-1,3-butadiene ug/L ND 1.0 02/12/21 11:37
m&p-Xylene ug/L ND 2.0 02/12/21 11:37
Methyl-tert-butyl ether ug/L ND 1.0 02/12/21 11:37
Methylene Chloride ug/L ND 5.0 02/12/21 11:37
Naphthalene ug/L ND 1.0 02/12/21 11:37
o-Xylene ug/L ND 1.0 02/12/21 11:37
p-Isopropyltoluene ug/L ND 1.0 02/12/21 11:37
Styrene ug/L ND 1.0 02/12/21 11:37
Tetrachloroethene ug/L ND 1.0 02/12/21 11:37
Toluene ug/L ND 1.0 02/12/21 11:37
trans-1,2-Dichloroethene ug/L ND 1.0 02/12/21 11:37
trans-1,3-Dichloropropene ug/L ND 1.0 02/12/21 11:37
Trichloroethene ug/L ND 1.0 02/12/21 11:37
Trichlorofluoromethane ug/L ND 1.0 02/12/21 11:37
Vinyl acetate ug/L ND 2.0 02/12/21 11:37
Vinyl chloride ug/L ND 1.0 02/12/21 11:37
Xylene (Total)ug/L ND 1.0 02/12/21 11:37
1,2-Dichloroethane-d4 (S)%104 70-130 02/12/21 11:37
4-Bromofluorobenzene (S)%107 70-130 02/12/21 11:37
Toluene-d8 (S)%107 70-130 02/12/21 11:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3161616LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 70-130
1,1,1-Trichloroethane ug/L 54.550 109 70-130
1,1,2,2-Tetrachloroethane ug/L 47.450 95 70-130
1,1,2-Trichloroethane ug/L 50.150 100 70-130
1,1-Dichloroethane ug/L 48.550 97 70-130
1,1-Dichloroethene ug/L 57.050 114 70-132
1,1-Dichloropropene ug/L 52.750 105 70-131
1,2,3-Trichlorobenzene ug/L 51.150 102 70-134
1,2,3-Trichloropropane ug/L 44.050 88 70-130
1,2,4-Trichlorobenzene ug/L 51.550 103 70-130
1,2-Dibromo-3-chloropropane ug/L 53.350 107 70-132
1,2-Dibromoethane (EDB)ug/L 52.850 106 70-130
1,2-Dichlorobenzene ug/L 50.650 101 70-130
1,2-Dichloroethane ug/L 52.950 106 70-130
1,2-Dichloropropane ug/L 48.950 98 70-130
1,3-Dichlorobenzene ug/L 50.950 102 70-130
1,3-Dichloropropane ug/L 50.750 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3161616LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 50.850 102 70-130
2,2-Dichloropropane ug/L 54.250 108 70-130
2-Butanone (MEK)ug/L 107100 107 70-133
2-Chlorotoluene ug/L 50.950 102 70-130
2-Hexanone ug/L 100100 100 70-130
4-Chlorotoluene ug/L 50.350 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 97.0100 97 70-130
Acetone ug/L 115100 115 70-144
Benzene ug/L 49.050 98 70-130
Bromobenzene ug/L 49.750 99 70-130
Bromochloromethane ug/L 53.350 107 70-130
Bromodichloromethane ug/L 50.550 101 70-130
Bromoform ug/L 56.550 113 70-131
Bromomethane ug/L 50.150 100 30-177
Carbon tetrachloride ug/L 55.950 112 70-130
Chlorobenzene ug/L 50.650 101 70-130
Chloroethane ug/L 59.450 119 46-131
Chloroform ug/L 48.550 97 70-130
Chloromethane ug/L 48.050 96 49-130
cis-1,2-Dichloroethene ug/L 48.850 98 70-130
cis-1,3-Dichloropropene ug/L 55.350 111 70-130
Dibromochloromethane ug/L 57.450 115 70-130
Dibromomethane ug/L 51.350 103 70-130
Dichlorodifluoromethane ug/L 51.250 102 52-134
Diisopropyl ether ug/L 52.450 105 70-131
Ethylbenzene ug/L 49.250 98 70-130
Hexachloro-1,3-butadiene ug/L 50.750 101 70-131
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 54.150 108 70-130
Methylene Chloride ug/L 53.550 107 68-130
Naphthalene ug/L 49.650 99 70-133
o-Xylene ug/L 51.350 103 70-130
p-Isopropyltoluene ug/L 54.450 109 70-130
Styrene ug/L 50.550 101 70-130
Tetrachloroethene ug/L 49.850 100 70-130
Toluene ug/L 48.450 97 70-130
trans-1,2-Dichloroethene ug/L 52.150 104 70-130
trans-1,3-Dichloropropene ug/L 54.750 109 70-130
Trichloroethene ug/L 54.850 110 70-130
Trichlorofluoromethane ug/L 53.650 107 61-130
Vinyl acetate ug/L 117100 117 70-140
Vinyl chloride ug/L 44.050 88 59-142
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3161617MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92521292004
3161618
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 88 70-13582 620ND17.5 16.5
1,1,1-Trichloroethane ug/L 20 113 70-14895 1720ND22.6 19.0
1,1,2,2-Tetrachloroethane ug/L 20 81 70-13177 520ND16.2 15.5
1,1,2-Trichloroethane ug/L 20 88 70-13681 920ND17.6 16.1
1,1-Dichloroethane ug/L 20 107 70-14788 1920ND21.4 17.7
1,1-Dichloroethene ug/L 20 123 70-158106 1520ND24.5 21.2
1,1-Dichloropropene ug/L 20 102 70-14990 1220ND20.3 18.1
1,2,3-Trichlorobenzene ug/L 20 91 68-14086 620ND18.2 17.1
1,2,3-Trichloropropane ug/L 20 86 67-13786 020ND17.2 17.2
1,2,4-Trichlorobenzene ug/L 20 96 70-13988 920ND19.2 17.5
1,2-Dibromo-3-chloropropane ug/L 20 87 69-13684 420ND17.4 16.7
1,2-Dibromoethane (EDB)ug/L 20 89 70-13777 1420ND17.7 15.4
1,2-Dichlorobenzene ug/L 20 90 70-13385 620ND17.9 16.9
1,2-Dichloroethane ug/L 20 103 67-13888 1620ND20.6 17.6
1,2-Dichloropropane ug/L 20 94 70-13887 820ND18.8 17.3
1,3-Dichlorobenzene ug/L 20 92 70-13385 820ND18.4 17.0
1,3-Dichloropropane ug/L 20 87 70-13677 1320ND17.4 15.3
1,4-Dichlorobenzene ug/L 20 92 70-13385 820ND18.3 17.0
2,2-Dichloropropane ug/L 20 112 52-155101 1020ND22.3 20.2
2-Butanone (MEK)ug/L M140-9 61-147-19 124038.6 34.8 30.9
2-Chlorotoluene ug/L 20 95 70-14186 1020ND19.1 17.2
2-Hexanone ug/L 40 72 67-13967 640ND33.2 31.4
4-Chlorotoluene ug/L 20 92 70-13589 320ND18.4 17.8
4-Methyl-2-pentanone (MIBK)ug/L 40 77 67-13676 240ND32.6 32.1
Acetone ug/L M140-799 55-159-816 184036242.8 35.9
Benzene ug/L M120-220 67-150-230 122062.9 19.0 16.9
Bromobenzene ug/L 20 84 70-13480 520ND16.8 16.0
Bromochloromethane ug/L 20 109 70-14695 1420ND21.9 19.0
Bromodichloromethane ug/L 20 99 70-13888 1120ND19.8 17.7
Bromoform ug/L 20 89 57-13882 820ND17.8 16.5
Bromomethane ug/L 20 115 10-20094 2120ND23.1 18.7
Carbon tetrachloride ug/L 20 107 70-147100 720ND21.4 20.0
Chlorobenzene ug/L 20 91 70-13785 720ND18.2 17.1
Chloroethane ug/L 20 119 51-166104 1320ND23.7 20.8
Chloroform ug/L M12016570-144151 920ND33.0 30.2
Chloromethane ug/L 20 82 24-16166 18203.2 19.7 16.4
cis-1,2-Dichloroethene ug/L 20 104 67-14888 1620ND20.8 17.7
cis-1,3-Dichloropropene ug/L 20 95 70-14288 720ND19.0 17.6
Dibromochloromethane ug/L 20 89 68-13884 620ND17.8 16.8
Dibromomethane ug/L 20 101 70-13492 1020ND20.2 18.4
Dichlorodifluoromethane ug/L 20 114 43-15595 1820ND22.8 19.1
Diisopropyl ether ug/L 20 83 65-14673 1220ND16.6 14.7
Ethylbenzene ug/L M1204868-14340 8209.0 18.5 17.0
Hexachloro-1,3-butadiene ug/L 20 101 62-15191 1120ND20.1 18.1
m&p-Xylene ug/L M1405953-15749 104015.3 38.7 35.0
Methyl-tert-butyl ether ug/L 20 93 59-15681 1420ND18.6 16.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3161617MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92521292004
3161618
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 104 64-14887 1720ND20.7 17.4
Naphthalene ug/L M1205257-15050 2206.7 17.1 16.7
o-Xylene ug/L M1206968-14362 8204.7 18.5 17.1
p-Isopropyltoluene ug/L 20 98 70-14191 720ND20.3 18.8
Styrene ug/L 20 93 70-13684 1020ND18.6 16.8
Tetrachloroethene ug/L 20 86 70-13984 320ND17.3 16.8
Toluene ug/L M1205347-15746 8208.4 19.1 17.6
trans-1,2-Dichloroethene ug/L 20 110 70-14997 1320ND21.9 19.3
trans-1,3-Dichloropropene ug/L 20 94 70-13883 1220ND18.8 16.7
Trichloroethene ug/L 20 97 70-14987 1120ND19.5 17.4
Trichlorofluoromethane ug/L 20 111 61-15499 1120ND22.2 19.8
Vinyl acetate ug/L 40 89 48-15682 740ND35.4 32.9
Vinyl chloride ug/L 20 103 55-17287 1720ND20.5 17.3
Xylene (Total)ug/L MS606266-14553 96020.0 57.2 52.1
1,2-Dichloroethane-d4 (S)%117 70-130113
4-Bromofluorobenzene (S)%103 70-130101
Toluene-d8 (S)%102 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
599980
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92521416001, 92521416002, 92521416003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3162894
Associated Lab Samples:92521416001, 92521416002, 92521416003
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N202/17/21 09:39
Aliphatic (C19-C36)ug/L ND 100 N202/17/21 09:39
Aromatic (C11-C22)ug/L ND 100 N202/17/21 09:39
1-Chlorooctadecane (S)%55 40-140 02/17/21 09:39
2-Bromonaphthalene (S)%100 40-140 02/17/21 09:39
2-Fluorobiphenyl (S)%100 40-140 02/17/21 09:39
o-Terphenyl (S)%106 40-140 02/17/21 09:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3162895LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3162896
Aliphatic (C09-C18)ug/L 201 N23006740-14061183 9 50
Aliphatic (C19-C36)ug/L 306 N24007640-14077307 0 50
Aromatic (C11-C22)ug/L 538 N28506340-14067571 6 50
1-Chlorooctadecane (S)%S03840-14032
2-Bromonaphthalene (S)%91 40-140106
2-Fluorobiphenyl (S)%92 40-140103
o-Terphenyl (S)%66 40-14081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92521416
Sheetz 391, Greenville, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92521416001 599980 600570MW-1 MADEP EPH MADEP EPH
92521416002 599980 600570MW-2 MADEP EPH MADEP EPH
92521416003 599980 600570MW-3 MADEP EPH MADEP EPH
92521416001 1621153 1621153MW-1 MADEPV MADEP VPH
92521416002 1621153 1621153MW-2 MADEPV MADEP VPH
92521416003 1621153 1621153MW-3 MADEPV MADEP VPH
92521416001 599739MW-1 EPA 8260D
92521416002 599739MW-2 EPA 8260D
92521416003 599739MW-3 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 21
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