WA-28525_47774_CA_SCH_20210415

An Equal Opportunity Employer

November 18, 2020

Ms. Brenda Hafshejani, P.E.
NCDEQ, UST Section
Raleigh Regional Office
300 Barrett Drive,
Raleigh, North Carolina 27609

Re: Site Check Report
Speedway #8211
1602 Martin L. King Jr Parkway,
Wilson, Wilson County, NC
Incident Number: Pending
GRI Project Number: 3381

Dear Ms. Hafshejani:

Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do
not hesitate to contact Scarlett Forrest and/or Nicole Long with Geological Resources, Inc. at 704-845-4010.

Sincerely,
Speedway, LLC.
Charles Chiara
Environmental Representative

Enclosure

Speedway LLC

Speedway Office
P.O. Box 1500
Springfield, OH 45501
Telephone [phone]

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Site Check Report
Speedway #8211
1602 Martin L. King Jr Parkway S.E.,
Wilson, Wilson County
North Carolina
Facility ID Number: 0-021716
Incident Number: N/A
GRI Project Number: 3381

Prepared for:

Charles Chiara
Speedway, LLC
500 Speedway Drive
Enon, Ohio 45323

November 18, 2020

Nicole Long
Project Manager
Scarlett Forrest
Junior Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
i
EXECUTIVE SUMMARY
The Speedway #8211 site is located at 1602 Martin L. King Jr Parkway S.E., in Wilson, Wilson County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered
by concrete, asphalt, and grass. There are three 10,000-gallon gasoline, one 10,000-gallon diesel and one
10,000-gallon kerosene USTs currently in use at the site with six associated dispenser islands.

On September 28, 2020, during annual compliance testing activities, one non-passing spill bucket was
reported for one of the 10,000-gallon regular gasoline USTs (UST #1). On October 2, 2020, during spill
bucket repair activities, free product was discovered in the STP sump of the other 10,000-gallon regular
gasoline UST (UST #2). Emergency response activities were initiated and upon further investigation, a
hole in the pipe elbow of the STP sump in UST #2 was observed. Free product was removed from the STP
sump and PID readings were taken around the UST basin and associated conduits and manholes. No odors
or PID detections were observed at that time. During the repair activities, it was observed that the spill
bucket collar on the 10,000-gallon premium gasoline UST (UST #3) was damaged, however no free product
was observed in that spill bucket at that time. The spill bucket for UST #3 was repaired for general
maintenance purposes. Speedway LLC received a Notice of Violation on October 5, 2020, in response to
those activities. Repairs were completed on the spill buckets for UST #1 and UST #3, and the STP sump
for UST #2, and received passing compliance testing results on October 26, 2020.

On October 26, 2020, GRI conducted a site check in the area of the three 10,000-gallon gasoline UST spill
buckets and STP sump. Soil boring SB-11 was advanced beneath the STP sump associated with UST #2,
soil boring SB-12 was advanced beneath the spill bucket associated with UST #3, and soil boring SB-13 was
advanced beneath the spill bucket associated with UST #1. The three soil borings (SB-11, SB-12, and SB-
13) were advanced to approximately 3 feet bgs. Soil sample SB-12 did not have any reported contaminant
concentrations above applicable standards. The Regulatory Action Levels (RALs) and Soil to Groundwater
Maximum Contaminant Concentrations (MCCs) were below reported concentrations of petroleum
constituents in soil samples SB-11 and SB-13. The Residential Soil Cleanup Level (SCL) was below the
reported concentration of benzene in soil sample SB-13.

As part of the site check activities, a ground water sample was collected from an existing observation well
(MW-A) at the site on October 30, 2020. The ground water sample collected from MW-A did not have
any detections of petroleum constituents that were above laboratory reporting limits.

Although there is shallow impact below the two newly repaired spill buckets, there was a previous release
at the site that was issued an NRP in 2016. Because the observation well did not have detectable
concentrations of petroleum constituents, it appears that a significant new release has not occurred, and
closure under the current NRP is requested.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
ii
SITE INFORMATION
1. Site Identification
 Speedway #8211 (Facility ID 0-021716)
 Incident Number N/A – Risk Ranking Undetermined
 Location of Source Area: 1602 Martin L. King Jr Parkway S.E.,
Wilson, NC 27893
Wilson County
35.7149166°N, 77.8947361°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Speedway, LLC (Table 1)
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069

UST/AST Operator
Speedway, LLC
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069

Property Owner
William Family Heirs, LLC
539 South Main Street
Findlay, Ohio 45840
Email Unknown
Phone No. Unknown

Property Occupant
Speedway, LLC
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Pace Analytical
12065 Lebanon Road
Mt. Juliet, TN 37122
State Certification No. 375
615-758-5858
3. Information about Release
 On September 28, 2020, during annual compliance testing activities, one non-passing spill bucket was
reported for one of the 10,000-gallon regular gasoline USTs.
 On October 2, 2020, during spill bucket repair activities, free product was discovered in the STP sump
of the other 10,000-gallon regular gasoline UST. Emergency response activities were initiated and upon
further investigation, a hole in the pipe elbow of the STP sump was observed.
 Three 10,000-gallon gasoline USTs, one 10,000-gallon diesel UST, and one 10,000-gallon kerosene UST
are in use at the site.

Certification:

I, John M. Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381

TABLE OF CONTENTS

A. SITE HISTORY AND CHARACTERIZATION .....................................................................1
B. SITE CHECK PROCEDURES ...........................................................................................2
C. SITE INVESTIGATION ..................................................................................................2
D. SUMMARY AND CONCLUSIONS ..................................................................................4
E. LIMITATIONS .............................................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Soil Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results
Table 4: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: UST Suspected Release 24 Hour Notice Form (UST-17A)
Appendix B: UST Suspected Release 7 Day Notice Form (UST-17B)
Appendix C: Certificate of Storage Tank System Testing (UST-23A/B)
Appendix D: Notice of Violation
Appendix E: Subsurface Logs
Appendix F: Laboratory Analytical Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
1
A. SITE HISTORY AND CHARACTERIZATION
1. UST Owner and Operator Information:
In accordance with the Site Check Report guidelines, the underground storage tank (UST) owner and
operator information has been summarized in the attached Table 1.

2. UST System Information:
In accordance with the Site Check Report guidelines, the UST system information has been summarized
in the attached Table 2. There are three 10,000-gallon gasoline, one 10,000-gallon diesel, and one
10,000-gallon kerosene USTs currently in use at the site with six associated dispensers. The dispensers
are located on both sides of the store building. A copy of the NCDEQ Registered Tank Report is shown
below:

3. Non-UST Information:
There are currently no above ground petroleum storage tanks (ASTs) and no known ASTs formerly at
the site.

4. Comprehensive Description of the Release:
Annual compliance testing was completed on September 28, 2020. Based on the testing, non-passing
hydrostatic results were reported for one of the 10,000-gallon regular gasoline UST (UST #1) spill buckets.
On October 2, 2020, during spill bucket repair activities, free product was discovered in the STP sump of
the other 10,000-gallon regular gasoline UST (UST #2). Emergency response activities were initiated, and
free product was removed from the STP sump. Upon further investigation, a hole in the pipe elbow of the
STP sump was observed. The non-passing spill bucket and the hole in the pipe elbow of the STP sump
were repaired and received passing compliance test results on October 26, 2020. Copies of the UST
Suspected Release 24 Hour Notice (UST-17A) form and the UST Suspected Release 7 Day Notice (UST-17B)
form are included as Appendices A and B, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
2
A site check was required according to the North Carolina Department of Environmental Quality (NCDEQ).
Soil sample results indicate surficial impact beneath the two, newly repaired spill buckets. Two
observation wells are present at the site as part of the UST system, and observation well MW-A was
sampled as part of the site check. The results of the ground water sampling event indicated that there
were no detectable concentrations of petroleum constituents reported in observation well MW-A.

5. Description of the Site Characteristics:
The Speedway #8211 site is located at 1602 Martin L. King Jr Parkway S.E., in Wilson, Wilson County, North
Carolina. (Figure 1). The property operates as a petroleum retail facility and convenience store. The site
is covered by concrete and grass. There are three 10,000-gallon gasoline, one 10,000-gallon diesel, and
one 10,000-gallon kerosene USTs currently in use at the site with six associated dispensers. The
surrounding properties are commercial and residential. A Site Map has been included as Figure 2.

B. SITE CHECK PROCEDURES
1. Results of Tank and Line Tightness Testing:
On September 28, 2020, during annual compliance testing activities, one non-passing spill bucket was
reported for one of the three 10,000-gallon gasoline USTs (UST #1). On October 2, 2020, during spill bucket
repair and emergency response activities, a hole in the pipe elbow of the STP sump in the other 10,000-
gallon regular gasoline UST (UST #2) was observed. Speedway LLC received a Notice of Violation on
October 5, 2020. Repairs were completed on the spill bucket and STP sump, and passing compliance
testing results were received on October 26, 2020. A copy of the retesting results are provided as
Appendix C, and a copy of the Notice of Violation is provided as Appendix D.

2. Summary of Site Check Procedure:
GRI performed a site check on October 26, 2020, that included the collection of three soil samples at the
spill buckets and STP sump associated with the three 10,000-gallon gasoline USTs. Soil boring SB-11 was
advanced beneath the STP sump associated with UST #2, soil boring SB-12 was advanced beneath the spill
bucket associated with UST #3, and soil boring SB-13 was advanced beneath the spill bucket associated
with UST #1. The three soil borings (SB-11, SB-12, and SB-13) were advanced to approximately 3 feet bgs,
and soil samples were collected from the bottom of the borings. Soil boring logs are provided as Appendix
E.
As part of the site check activities, a ground water sample was collected from an existing observation well
(MW-A) at the site on October 30, 2020.

3. Soil Excavation Activities:
No soil excavation activities were conducted.

C. SITE INVESTIGATION
1. Field Screening:
During the October 2, 2020, emergency response activities, PID readings were taken from the UST basin

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
3
conduits and manholes. The PID did not detect volatile organic compound (VOC) vapors during the site
investigation. Soil samples (SB-11, SB-12 and SB-13) collected on October 26, 2020, were not screened
with a PID for VOCs.

2. Soil Sampling Information:
Soil samples (SB-11, SB-12 and SB-13) were collected on October 26, 2020, and submitted for laboratory
analyses of total petroleum hydrocarbons (TPH) gasoline-range organics (GRO) by EPA Method 8015D and
BTEX by EPA Method 8260B. Soil sample SB-12 did not have any reported contaminant concentrations
above applicable standards. The Regulatory Action Levels (RALs) and Soil to Groundwater Maximum
Contaminant Concentrations (MCCs) were below reported concentrations of petroleum constituents in
soil samples SB-11 and SB-13. The Residential Soil Cleanup Level (SCL) was below the reported
concentration of benzene in soil sample SB-13. A soil quality map is presented as Figure 3. A summary of
soil sample analytical results is presented in Table 3. The laboratory analytical report is provided as
Appendix F. A summary of the soil sampling data from the October 2020 Site Check activities is show
below:
Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) Gasoline-Range TPH Benzene Toluene Ethylbenzene Total Xylenes RAL (mg/kg) 50 NE NE NE NE
Soil to Water MCC (mg/kg) NE 0.0056 4.3 4.9 4.6
Residential SCLs (mg/kg) NE 18 1,200 1,560 3,129
SB-11 (3') 10/26/20 3 822 0.523 0.133 19.7 4.05
SB-12 (3') 10/26/20 3 <3.32 <0.00133 0.00781 <0.00332 0.0155
SB-13 (3') 10/26/20 3 6,150 18.2 167 106 537
Trip Blank 10/26/20 NA NR <1.00 <1.00 <1.00 <3.00

3. Ground Water and Surface Water Sampling Information:
A ground water sample was collected from observation well MW-A on October 30, 2020 and submitted
for analysis of VOC by EPA Method 6200B. The depth to ground water in MW-A was 4.10 feet below the
top of well casing. The groundwater sample collected from MW-A did not have any detections of
petroleum constituents that were above laboratory reporting limits. Well gauging information is
presented in Table 4. A summary of ground water sample analytical results is presented in Table 5. The
laboratory analytical report is provided as Appendix F. A summary of the ground water sampling data
from the October 2020 Site Check activities is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
4

Contaminant of
Concern
 Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MAC (μg/l) 1 600 600 500 20 6
GCL (μg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-A <1.00 <1.00 <1.00 <3.00 <1.00 <5.00

4. Quality-Control Measures:
Clean, disposable nitrile gloves were used for the collection of the soil and ground water samples. The
samples were collected in laboratory supplied containers and shipped to the laboratory in a cooler
following proper chain-of-custody procedures. A laboratory supplied trip blank was included in the
sample cooler with the soil samples. No detectable concentrations of requested method constituents
were reported in the trip blank.

D. SUMMARY AND CONCLUSIONS
 The site is commercial and surrounding properties are commercial and residential.
 On September 28, 2020, one non-passing spill bucket was reported for one of the 10,000-gallon
regular gasoline USTs (UST #1). The non-passing spill bucket was repaired and received passing
compliance test results on October 26, 2020.
 On October 2, 2020, during spill bucket repair activities, free product was discovered in the STP
sump of the other 10,000-gallon regular gasoline UST (UST #2). Emergency response activities
were initiated and upon further investigation, a hole in the pipe elbow of the STP sump in UST #2
was observed. Free product was removed from the STP sump and PID readings were taken around
the UST basin and associated conduits and manholes. No odors or PID detections were observed
at that time. The STP sump was repaired and received passing compliance test results on October
26, 2020.
 During the repair activities, it was observed that the spill bucket collar on the 10,000-gallon
premium gasoline UST (UST #3) was damaged, however no free product was observed in that spill
bucket at that time. The spill bucket for UST #3 was repaired for general maintenance purposes.
 A Site Check was conducted on October 26, 2020, to determine if a petroleum release had
occurred.
 Three soil borings (SB-11, SB-12 and SB-13) were advanced in the area of the three 10,000-gallon

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Site Check Report
Prepared on: November 18, 2020 Speedway #8211
Project Manager: Nicole Long GRI Project No. 3381
5
gasoline UST spill buckets and STP sump. Soil boring SB-11 was advanced beneath the STP sump
associated with UST #2, soil boring SB-12 was advanced beneath the spill bucket associated with
UST #3, and soil boring SB-13 was advanced beneath the spill bucket associated with UST #1.
 Soil sample SB-12 did not have any reported contaminant concentrations above applicable
standards. The Regulatory Action Levels (RALs) and Soil to Groundwater Maximum Contaminant
Concentrations (MCCs) were below reported concentrations of petroleum constituents in soil
samples SB-11 and SB-13. The Residential Soil Cleanup Level (SCL) was below the reported
concentration of benzene in soil sample SB-13.
 A ground water sample was collected from existing observation well MW-A on October 30, 2020.
The groundwater sample collected from MW-A did not have any detections of petroleum
constituents that were above laboratory reporting limits.
 Although there is shallow impact below the two newly repaired spill buckets, there was a previous
release at the site that was issued an NRP in 2016. Because the observation well did not have
detectable concentrations of petroleum constituents, it appears that a significant new release has
not occurred, and closure under the current NRP is requested.
E. LIMITATIONS
This report has been prepared for the exclusive use of Speedway, LLC for the specific application to the
referenced site in Wilson County, North Carolina. The assessment was conducted based on the scope of
work and level of effort specified by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
Copyright (C) 2009 MyTopo, 2006-2018 TomTom
077.9166666° W
077.9166666° W
077.9000000° W
077.9000000° W
077.8833333° W
077.8833333° W35.7333333° N35.7333333° N35.7166666° N35.7166666° N35.7000000° N35.7000000° NSCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 9.64° W
MN Figure 1
Site Location Map
Speedway #8211
1602 Martin Luther King Jr. Parkway
Wilson, Wilson County, NC
Incident No. N/A
GRI Project No. 3381
Date: 12/11/18
Scale: 1 inch = 2,000 ft.Copyright (C) 2009 MyTopo
Location: 035.7149166° N 077.8947361° W

TABLES
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Operator/Operator
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
3602 Highway 264 East, Greenville, NC 27834 N/A
0-021716
Name of Owner or Operator Dates of Ownership / Operation
Trade Oil Company 01/1/1988 - 06/01/2005
Address Telephone Number
5446 University Parkway, Winston-Salem, NC 27105 N/A
0-021716
Name of Owner or Operator Dates of Ownership / Operation
WilcoHess, LLC.06/01/2005 - 01/01/2016
0-021716
TABLE 1
UST OWNER/OPERATOR INFORMATION
SPEEDWAY #8211 (INCIDENT NO. N/A)
500 Speedway Drive, Enon, Ohio 45323 1-937-863-6507
Name of Owner or Operator Dates of Ownership / Operation
Speedway, LLC.01/01/2016 - Current
Address Telephone Number
Page 1 of 4
Date: 11/11/2020
Was Release
Associated
with UST
System?
(Yes / No)
1 Diesel NA 10,000 5/1/1988 Single Wall
Steel/FR Unknown Single Wall
Fiberglass Current No
2 Kerosene NA 10,000 5/1/1988 Single Wall
Steel/FR Unknown Single Wall
Fiberglass Current No
3 Gasoline NA 10,000 5/1/1988 Single Wall
Steel/FR Unknown Single Wall
Fiberglass Current Yes
4 Gasoline NA 10,000 5/1/1988 Single Wall
Steel/FR Unknown Single Wall
Fiberglass Current Yes
5 Gasoline NA 10,000 5/1/1988 Single Wall
Steel/FR Unknown Single Wall
Fiberglass Current Yes
TABLE 2
UST SYSTEM INFORMATION
SPEEDWAY #8211 (INCIDENT NO. N/A)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 0-021716
Page 2 of 4
Date: 11/11/20
5030/
8015D
Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)Gasoline-Range TPHBenzeneTolueneEthylbenzeneTotal Xylenes50 NE NE NE NE
NE 0.0056 4.3 4.9 4.6
NE 18 1,200 1,560 3,129
SB-11 (3')10/26/20 3 822 0.523 0.133 19.7 4.05
SB-12 (3')10/26/20 3 <3.32 <0.00133 0.00781 <0.00332 0.0115
SB-13 (3')10/26/20 3 6,150 18.2 167 106 537
Trip Blank 10/26/20 NA NR <1.00 <1.00 <1.00 <3.00
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• Trip Blank results reported in ug/l (micrograms per liter)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• NE: Not Established
• NR: Not Requested.
• Concentrations in bold face type indicate the soil-to-water MCCs were below the reported
concentrations.
• Concentrations in italic type indicate the residential SCLs were below the reported
concentrations.
Facility ID #: 0-021716
TABLE 4
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
SPEEDWAY #8211 (INCIDENT NO. N/A)
EPA Method 8260B
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
Analytical Method 
Page 3 of 4
Date: 11/11/20 Facility ID # : 0-021716
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
MW-A 10/30/20 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
MAC (μg/l)
GCL (μg/l)MTBENaphthaleneContaminant of Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SPEEDWAY #8211 (INCIDENT NO. N/A)
Analytical Method
EPA 6200B
Page 4 of 4

APPENDICES

Appendix A
UST Suspected Release 24 Hour Notice Form (UST-17A)
UST-17A UST Suspected Release 24 Hour Notice
Do not use this form to report a 24 hour notice of a Pollution Incident. You must use form UST-61, 24 Hour Release and UST Leak
Reporting Form.
➢ This form must be used to report to DEQ, within 24 hours of discovery, a Suspected Release from any of the following:
a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as “Increase”, which
indicates the level in the UST system has increased more than 0.2 gph.
b) Unusual operating conditions which can include, but are not limited to: the erratic behavior of dispensing equipment; the
unexplained presence of water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of
any equipment or element of an underground storage tank system to the point where that equipment or element can not reasonably
be expected to perform its intended function.
c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release
could have occurred.
➢ If you have more than four UST systems to report suspected releases, then attach additional sheets of the UST-17A form. You only
need to list the UST systems at your site that have suspected releases.
➢ Within 7 days of discovery, submit a UST-17B form to document the response activities taken to investigate the suspected release.
➢ Please submit this form to: NCDEQ/DWM, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
OR
Fax to [phone] OR [e-mail]
I. UST OWNER II. UST FACILITY
Name:

Name:

Facility ID:

Address:

Address:

City:

State:

Zip:

City:

County:

Person Reporting:

Title of Person Reporting:

Telephone Number:
( )
Date Submitted:

III. UST INFORMATION
Tank Number / Size: / / / /
Product Stored:
Location and/or source of
suspected release: (check all that apply)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Leak detection method or
other observation that
indicates a suspected
release. (e.g., ATG, SIR,
visual contamination, fuel
in sump, etc.):

Failed/Inconclusive date or
date that leak detection
method suspected release discovered:

IV. COMMENTS

UST-17A Revised 10/2018 http://www.wastenotnc.org/

Speedway LLC
500 Speedway Drive
Enon OH
Speedway 8211 021716
1602 Martin L. King Jr Pkwy Se
Wilson Wilson
Andrew McMillan Environmental Compliance Coordinator 919 268-7176
1 10,000
RUL
n
Product identifed in STP
10-2-20
n
10/2/2020

Appendix B
UST Suspected Release 7 Day Notice Form (UST-17B)
UST-17B UST Suspected Release 7 Day Notice
¾ This form must be used to report to DEQ, within 7 days of discovery, the investigation results for a Suspected Release from any of the following:
a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as “Increase”, which indicates the level in the
UST system has increased more than 0.2 gph.
b) Unusual operating conditions which can include, but are not limited to, the erratic behavior of dispensing equipment; the unexplained presence of
water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground
storage tank system to the point where that equipment or element can not reasonably be expected to perform its intended function.
c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release could have occurred.
¾ If you have more than four UST systems to report suspected release investigations, then attach additional sheets of the UST-17B form.
¾ Please submit this form along with the supporting documentation to:
NCDEQ/DWM, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
OR
Fax to [phone] OR [e-mail]
I. UST OWNER II. UST FACILITY
Name:

Name:

Facility ID:

Address:

Address:

City:

State:

Zip:

City:

County:

Person Reporting:

Title of Person Reporting:

Telephone Number:
( )
III. INVESTIGATION RESULTS
Tank Number / Size: / / / /
Product Stored:
Reason for Suspected
Release Investigation
(Check all that apply):
You must attach the
supporting documentation
specified in the footnote for
the reason(s) selected.
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
1 Conduct a tank and/or line tightness test and attach the results, along with all of the supporting data sheets for the test method, to this form for submittal.
The summary page listing the results by itself is not acceptable. If the tightness test results are fail, then you must repair or replace your UST system and
conduct a site check in accordance with 15A NCAC 2N .0603.
2 Provide sales receipts or other comparable documentation that shows fuel was being dispensed from the UST during the test.
3 Provide invoices (with a description of the work completed) or other documentation that shows the equipment has been repaired.
4 Correct your leak detection results using the correct tank chart and submit copies with this form.
5 Repair the UST in accordance with the manufacturer’s instructions or a national standard (e.g., PEI API 1631) and conduct a site check in accordance with
15A NCAC 2N .0603. If the UST is not repaired, then it must be permanently closed in accordance with the latest version of the UST Sections Guidelines
for Tank Closure.
6 Correct your leak detection results using the amount your meter was adjusted following calibration and submit copies of the meter calibration and leak
detection results with this form.
7 Conduct a tightness test (e.g., hydrostatic test) of the sump and submit the test result along with this form. If the test results are fail, then you must repair
or replace the containment sump and conduct a site check in accordance with 15A NCAC 2N .0603.
8 Submit documentation from your UST equipment contractor explaining how they determined the UST was tilted. Correct your leak detection results using a
tank chart adjusted for the tilt and submit with this form.
Note: Tank, piping, spill bucket and containment sump replacements must be done in accordance with 15A NCAC 2N .0900
UST-17B Revised 10/2015 http://www.wastenotnc.org/web/wm/

Failed STP
Hydro test
Speedway LLC
500 Speedway Drive
Enon OH
Speedway 8211 21716
1602 Martin L. King Jr Pkwy Se
Wilson Wilson
Andrew McMillan Environmental Compliance Coordinator 919 268-7176
1 10k
RUL

Appendix C
Certificate of Storage Tank System Testing (UST23A/B)

Appendix D
Notice of Violation

NORTH CAROLINA Environmental Quality
ROY COOPER Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director

North Carolina Department of Environmental Quality | Division of Waste Management
217 West Jones Street | 1646 Mail Service Center | Raleigh, North Carolina 27699-1646
919.707.8171

October 05, 2020 CERTIFIED MAIL RETURN RECEIPT REQUESTED CT Corporation System, Registered Agent
Speedway LLC 160 Mine Lake Ct Ste 200 Raleigh, NC 27615-6417 Re: NOTICE OF VIOLATION OF 15A NCAC 2N .0302(UPG10), .0603(RLS5, RLS7) Speedway #8211
1605 Martin Luther King Pkwy Se, Wilson, NC 27893 Wilson County Facility ID#: 00-0-0000021716
Dear CT Corporation System:
On October 02, 2020, I conducted a compliance inspection at the above-referenced facility. I observed that underground storage tanks (USTs) at Speedway #8211 are not in compliance with North Carolina UST regulations (North Carolina Administrative Code [NCAC] 2N "Criteria and Standards Applicable to Underground Storage Tanks). According to those rules (15A NCAC 2N .0203) Speedway LLC is identified as the owner and/or operator
of UST(s) at Speedway #8211.
The following violations of the state rules (15A NCAC 2N) were observed on October 02, 2020 at Speedway #8211. Following each violation are the actions required to correct the violations:
Violation 1: 15A NCAC 2N .0302 UPG10; Failure to meet the spill prevention requirements of an 'existing tank system' as required by federal regulation 40 CFR 280.21(d) (as incorporated by 15A NCAC 2N .0302). Corrective Action(s):
All UST systems installed before December 22, 1988 are defined as 'existing tank systems.' All "existing tank systems" that are filled by transfers of more than 25 gallons at one time are required to have spill prevention equipment. Please complete one of the following actions: 1) Repair your spill prevention equipment. If the spill prevention equipment is replaced as part of the repair then the spill prevention equipment must meet the secondary containment requirements of 15A NCAC 2N .0900 and must have an integrity test conducted after installation that is documented on a UST-23A form Triennial UST Spill
Bucket Integrity Testing.
Submit a copy of invoices, designs or other documentation of the completed work within 30 days of receipt of this NOV to the inspector at the address provided. In addition, if spill prevention is added, please submit a UST-8 form, Notification for Activities Involving USTs, identifying methods (i.e., catchment basin) used along with a UST-23A form, Triennial UST Spill Bucket Integrity Testing.
Comment: The regular slave tank spill bucket failed a tightness test 9/28/2020.

Violation 2: 15A NCAC 2N .0603 RLS5; Failure to investigate a suspected release in accordance with federal regulation 40 CFR 280.52 (as incorporated by 15A NCAC 2N .0603) after an unusual operating condition has been observed. ("Unusual operating conditions" include, but are not limited to, the erratic behavior of dispensing equipment; the unexplained presence of water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground storage tank system to
the point where that equipment or element can not reasonably be expected to perform its intended function.). Corrective Action(s): Tank owners or operators must investigate a suspected release as directed below. 1) Empty* and clean the containment sumps and/or under dispenser containment. Investigate cause and repair the components that caused the release of liquid to the containment sumps. 2) Conduct a tightness test of the regular tank STP containment sump integrity in accordance with the
manufacturer's recommendations* or a code of practice developed by a nationally recognized association. If a testing standard is not available then you must fill the containment sump with clean water above all piping and conduit penetrations; mark the water level; wait a minimum of 3 hours and re-check the level. A containment sump fails the tightness test if there has been any change in level. Submit a copy of the test results to the inspector at the address provided. If any containment sump fails the tightness test, you must complete all of the following tasks: (a) Conduct a site check around the areas listed above in accordance with 40 CFR 280.52(b) (as incorporated
by 15A NCAC 2N .0603) using the sampling protocol and methodology of the most recent version of the UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement and submit , within 30 days of receipt of this notice, a site check report or initial abatement report (whichever is applicable) to the inspector at the address provided; AND (b) Repair or replace the containment sump and test the tightness of the containment
sump in accordance with the manufacturer's recommendations, a code of practice developed by a nationally recognized association, or the alternate instructions listed above if no standard is available. If the containment sump
is replaced as part of this repair then the containment sump must meet the secondary containment requirements of 15A NCAC 2N .0900.
Within 30 days of receipt of this notice submit a UST-17B, UST Suspected Release 7 Day Notice, with the results and any supporting information for all equipment repairs, equipment replacements, tightness test(s), and site check
as required in the above sections to the inspector at the address provided. * Proper disposal of liquids in accordance with State and Federal requirements is required. See the attached document "Recommended ways to dispose of
small quantities of petroleum and petroleum/water mixtures" for some suggested methods.
Comment: Release#1: The regular tank STP sump had a release that was discovered 10/1/2020. The sump was clean and dry at the time of the UST compliance inspection 10/2/2020 and the release had been repaired. Due to the regular STP tank sump hydrostatic fail 10/2/2020 UST-23B as part of the investigation of the suspected release, a site check is required for the regular tank STP sump. UST-17A/B forms were submitted 10/2/2020.

Violation 3: 15A NCAC 2N .0603 RLS7; Failure to investigate a suspected release in accordance with federal regulation 40 CFR 280.52 (as incorporated by 15A NCAC 2N .0603) after a failing tightness test of the spill containment, the presence of fuel in spill containment buckets or the degradation of the spill containment equipment to the point where that equipment can not reasonably be expected to perform its intended function was observed. Corrective Action(s): Tank owners or operators must investigate a suspected release as directed below. 1) The spill containment bucket failed a tightness test or the condition of the spill containment bucket has deteriorated such that it may need repairing or replacing. All replaced spill buckets must meet the secondary containment requirements of 15A NCAC 2N .0900. You must complete the actions listed below.
Conduct a tightness test (if one has not already been completed) of the existing regular slave tank spill containment
bucket integrity (prior to repair/replacement) in accordance with the manufacturer's recommendations* or a code of practice developed by a nationally recognized association. If a testing standard is not available then you must fill the spill containment bucket(s) with clean water to within 1.5 inches of the top of the spill bucket; mark the water level; wait a minimum of 1 hour and re-check the level. A spill containment bucket fails the tightness test if there has been any change in level. Submit a copy of the test results to the inspector at the address provided. If any spill containment bucket fails the tightness test, you must complete all of the following tasks: (a) Conduct a site
check around the spill containment bucket for the tanks listed above in accordance with 40 CFR 280.52(b) (as incorporated by 15A NCAC 2N .0603) using the sampling protocol and methodology of the most recent version of the UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement and submit, within 30 days of receipt of this notice, a site check report or initial abatement report (whichever is applicable) to the
inspector at the address provided; AND (b) Repair or replace the spill containment bucket and test the tightness of the spill containment bucket in accordance with the manufacturer's recommendations, a code of practice developed
by a nationally recognized association, or the alternate instructions listed above if no standard is available. All replaced spill buckets must meet the secondary containment requirements of 15A NCAC 2N .0900. Within 30 days of receipt of this notice, unless noted differently above, submit a UST-17B, UST Suspected Release 7 Day Notice, with the results and any supporting information for all equipment repairs, equipment replacements, tightness test(s),
and site check as required in the above sections to the inspector at the address provided. * Proper disposal of liquids in accordance with State and Federal requirements is required. See the attached document Recommended ways to
dispose of small quantities of petroleum and petroleum/water mixtures for some suggested methods.
Comment: Tank #4 - REG2: The regular slave tank spill bucket failed a tightness test 9/28/2020. Conduct a site check around the spill bucket. Repair or replace the spill bucket and test the tightness (Submit form UST-23A). UST-17A/B forms were submitted 9/30/2020. Notice of Deficiency: Deficiency 1: NCGS 143-215.94NN-SS OPTR4; Failure to maintain compliance with UST regulations which requires Primary Operator retraining as required by NCGS 143-215.94NN - 143.215.94SS. Corrective Action(s): Please perform the following corrective action: 1) Within 30 days of receipt of this notice, the Primary Operator designated for this facility must go to the following website http://tankschool.nc.gov and register for one of the next Tank School courses being conducted over the next 90 days or take the NC DEQ on-line course for retraining. Retraining as a Primary Operator must be completed and a Primary Operator training certificate achieved within 90 days of receipt of this notice.

Corrective actions must be completed and reported to the inspector at the address provided within 30 days of receipt of this notice, unless otherwise noted in one of the corrective actions listed above. Assessment of civil penalties may be recommended for violations described in this NOV, as well as, operating permit revocation/denial unless the violations are corrected. If Speedway LLC believes that the inspection findings are in error, or if Speedway LLC has any questions pertaining to this NOV and/or corrective actions please have it contact me at [phone] or [e-mail].
Sincerely,
Ed Owen, Environmental Specialist Division of Waste Management, NC DEQ
Enclosures cc: Steve Booe w/ Enclosures (electronic) Files (electronic)

Please email or fax all corrective actions to:
Email: [e-mail] Fax: [phone]
Phone: [phone] Or mail to:
Ed Owen NC DEQ-UST Section
1646 Mail Service Center Raleigh, NC 27699-1646

Appendix E
Subsurface Logs

Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #8211
Address 1602 Martin L. King Jr Pkway S.E., Wilson, Wilson County, NC, 27893
Boring Number SB-11 (3') Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Completed to 3'; abandoned with soil cuttings & concrete subsequent to sampling
Driller GRI Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
SB-11 (3')3'NA Total depth = 3'
4

6
8
10

12
14

16

18
20

22

24
26

28

30
32
34

36

38

40
10/26/20
0' - 3' Gray medium sand

Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #8211
Address 1602 Martin L. King Jr Pkway S.E., Wilson, Wilson County, NC, 27893
Boring Number SB-12 (3')Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Completed to 3'; abandoned with soil cuttings & concrete subsequent to sampling
Driller GRI Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
SB-12 (3')3'NA Total depth = 3'
4

6
8
10

12
14

16

18
20

22

24
26

28

30
32
34

36

38

40
10/26/20
0' - 3' Tan medium sand

Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #8211
Address 1602 Martin L. King Jr Pkway S.E., Wilson, Wilson County, NC, 27893
Boring Number SB-13 (3')Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Completed to 3'; abandoned with soil cuttings & concrete subsequent to sampling
Driller GRI Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
SB-13 (3')3'NA Total depth = 3'
4

6
8
10

12
14

16

18
20

22

24
26

28

30
32
34

36

38

40
10/26/20
0' - 3' Gray medium sand

Appendix F
Laboratory Analytical Reports

ANALYTICAL REPORT
November 05, 2020
Geological Resources- NC Speedway
Sample Delivery Group:L1278387
Samples Received:10/27/2020
Project Number:3381
Description:Speedway 8211
Site:8211
Report To:Ms. Nicole Long
3502 Hayes Rd.
Charlotte, NC 28110
Entire Report Reviewed By:
November 05, 2020
[Preliminary Report]
Christl M Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:49 1 of 23
November 05, 2020
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:54 1 of 23
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TRIP BLANK L1278387-01 5
SB-11 (3') L1278387-02 7
SB-12 (3') L1278387-03 8
SB-13 (3') L1278387-04 9
Qc: Quality Control Summary 10
Total Solids by Method 2540 G-2011 10
Volatile Organic Compounds (GC) by Method 8015D/GRO 11
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 12
Volatile Organic Compounds (GC/MS) by Method 8260D 16
Gl: Glossary of Terms 17
Al: Accreditations & Locations 18
Sc: Sample Chain of Custody 19
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:49 2 of 23
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:54 2 of 23
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TRIP BLANK L1278387-01 GW Ethan Rogerson 10/26/20 10:00 10/27/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1568909 1 10/31/20 15:05 10/31/20 15:05 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-11 (3') L1278387-02 Solid Ethan Rogerson 10/26/20 10:03 10/27/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1568775 1 11/02/20 15:34 11/02/20 15:40 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1570180 250 10/26/20 10:03 11/03/20 21:00 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1568930 10 10/26/20 10:03 11/04/20 06:30 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-12 (3') L1278387-03 Solid Ethan Rogerson 10/26/20 10:20 10/27/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1568775 1 11/02/20 15:34 11/02/20 15:40 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1570180 25 10/26/20 10:20 11/03/20 21:22 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1568930 1 10/26/20 10:20 11/04/20 03:38 ADM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-13 (3') L1278387-04 Solid Ethan Rogerson 10/26/20 12:15 10/27/20 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1568775 1 11/02/20 15:34 11/02/20 15:40 KBC Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1570180 5000 10/26/20 12:15 11/03/20 21:45 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1568930 400 10/26/20 12:15 11/04/20 06:49 ADM Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:49 3 of 23
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:54 3 of 23
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Christl M Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:49 4 of 23
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1278387 11/05/20 13:54 4 of 23
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1278387
TRIP BLANK
Collected date/time: 10/26/20 10:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,1,1-Trichloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,1,2,2-Tetrachloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,1,2-Trichloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,1-Dichloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,1-Dichloroethene ND 1.00 1 10/31/2020 15:05 WG1568909
1,1-Dichloropropene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2,3-Trichlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2,3-Trichloropropane ND 2.50 1 10/31/2020 15:05 WG1568909
1,2,3-Trimethylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2,4-Trichlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2,4-Trimethylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/31/2020 15:05 WG1568909
1,2-Dibromoethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,2-Dichlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,2-Dichloroethane ND 1.00 1 10/31/2020 15:05 WG1568909
1,2-Dichloropropane ND 1.00 1 10/31/2020 15:05 WG1568909
1,3,5-Trimethylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,3-Dichlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
1,3-Dichloropropane ND 1.00 1 10/31/2020 15:05 WG1568909
1,4-Dichlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
2,2-Dichloropropane ND 1.00 1 10/31/2020 15:05 WG1568909
Benzene ND 1.00 1 10/31/2020 15:05 WG1568909
Bromobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
Bromochloromethane ND 1.00 1 10/31/2020 15:05 WG1568909
Bromodichloromethane ND 1.00 1 10/31/2020 15:05 WG1568909
Bromoform ND 1.00 1 10/31/2020 15:05 WG1568909
Carbon tetrachloride ND 1.00 1 10/31/2020 15:05 WG1568909
Chlorobenzene ND 1.00 1 10/31/2020 15:05 WG1568909
Chloroethane ND 5.00 1 10/31/2020 15:05 WG1568909
Chloroform ND 5.00 1 10/31/2020 15:05 WG1568909
Chlorodibromomethane ND 1.00 1 10/31/2020 15:05 WG1568909
Dichlorodifluoromethane ND 5.00 1 10/31/2020 15:05 WG1568909
Di-isopropyl ether ND 1.00 1 10/31/2020 15:05 WG1568909
Ethylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
Hexachloro-1,3-butadiene ND 1.00 1 10/31/2020 15:05 WG1568909
Isopropylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
Bromomethane ND 5.00 1 10/31/2020 15:05 WG1568909
Chloromethane ND 2.50 1 10/31/2020 15:05 WG1568909
Methyl tert-butyl ether ND 1.00 1 10/31/2020 15:05 WG1568909
Dibromomethane ND 1.00 1 10/31/2020 15:05 WG1568909
Methylene Chloride ND 5.00 1 10/31/2020 15:05 WG1568909
Naphthalene ND 5.00 1 10/31/2020 15:05 WG1568909
Styrene ND 1.00 1 10/31/2020 15:05 WG1568909
Tetrachloroethene ND 1.00 1 10/31/2020 15:05 WG1568909
Toluene ND 1.00 1 10/31/2020 15:05 WG1568909
Trichloroethene ND 1.00 1 10/31/2020 15:05 WG1568909
Trichlorofluoromethane ND 5.00 1 10/31/2020 15:05 WG1568909
Vinyl chloride ND 1.00 1 10/31/2020 15:05 WG1568909
Total Xylenes ND 3.00 1 10/31/2020 15:05 WG1568909
cis-1,2-Dichloroethene ND 1.00 1 10/31/2020 15:05 WG1568909
cis-1,3-Dichloropropene ND 1.00 1 10/31/2020 15:05 WG1568909
n-Butylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
n-Propylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
2-Chlorotoluene ND 1.00 1 10/31/2020 15:05 WG1568909
p-Isopropyltoluene ND 1.00 1 10/31/2020 15:05 WG1568909
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1278387
TRIP BLANK
Collected date/time: 10/26/20 10:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorotoluene ND 1.00 1 10/31/2020 15:05 WG1568909
sec-Butylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
tert-Butylbenzene ND 1.00 1 10/31/2020 15:05 WG1568909
trans-1,2-Dichloroethene ND 1.00 1 10/31/2020 15:05 WG1568909
trans-1,3-Dichloropropene ND 1.00 1 10/31/2020 15:05 WG1568909
(S) Toluene-d8 109 80.0-120 10/31/2020 15:05 WG1568909
(S) 4-Bromofluorobenzene 96.4 77.0-126 10/31/2020 15:05 WG1568909
(S) 1,2-Dichloroethane-d4 101 70.0-130 10/31/2020 15:05 WG1568909
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1278387
SB-11 (3')
Collected date/time: 10/26/20 10:03
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 90.3 1 11/02/2020 15:40 WG1568775
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 822 30.7 250 11/03/2020 21:00 WG1570180
(S) a,a,a-Trifluorotoluene(FID)95.6 77.0-120 11/03/2020 21:00 WG1570180
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzene 0.523 0.0123 10 11/04/2020 06:30 WG1568930
Toluene 0.133 0.0615 10 11/04/2020 06:30 WG1568930
Ethylbenzene 19.7 0.0307 10 11/04/2020 06:30 WG1568930
Total Xylenes 4.05 0.0799 10 11/04/2020 06:30 WG1568930
(S) Toluene-d8 105 75.0-131 11/04/2020 06:30 WG1568930
(S) 4-Bromofluorobenzene 110 67.0-138 11/04/2020 06:30 WG1568930
(S) 1,2-Dichloroethane-d4 107 70.0-130 11/04/2020 06:30 WG1568930
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1278387
SB-12 (3')
Collected date/time: 10/26/20 10:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.9 1 11/02/2020 15:40 WG1568775
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.32 25 11/03/2020 21:22 WG1570180
(S) a,a,a-Trifluorotoluene(FID)99.4 77.0-120 11/03/2020 21:22 WG1570180
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzene ND 0.00133 1 11/04/2020 03:38 WG1568930
Toluene 0.00781 0.00663 1 11/04/2020 03:38 WG1568930
Ethylbenzene ND 0.00332 1 11/04/2020 03:38 WG1568930
Total Xylenes 0.0115 0.00862 1 11/04/2020 03:38 WG1568930
(S) Toluene-d8 111 75.0-131 11/04/2020 03:38 WG1568930
(S) 4-Bromofluorobenzene 94.5 67.0-138 11/04/2020 03:38 WG1568930
(S) 1,2-Dichloroethane-d4 100 70.0-130 11/04/2020 03:38 WG1568930
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1278387
SB-13 (3')
Collected date/time: 10/26/20 12:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 96.1 1 11/02/2020 15:40 WG1568775
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 6150 544 5000 11/03/2020 21:45 WG1570180
(S) a,a,a-Trifluorotoluene(FID)89.5 77.0-120 11/03/2020 21:45 WG1570180
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzene 18.2 0.435 400 11/04/2020 06:49 WG1568930
Toluene 167 2.18 400 11/04/2020 06:49 WG1568930
Ethylbenzene 106 1.09 400 11/04/2020 06:49 WG1568930
Total Xylenes 537 2.83 400 11/04/2020 06:49 WG1568930
(S) Toluene-d8 103 75.0-131 11/04/2020 06:49 WG1568930
(S) 4-Bromofluorobenzene 105 67.0-138 11/04/2020 06:49 WG1568930
(S) 1,2-Dichloroethane-d4 97.6 70.0-130 11/04/2020 06:49 WG1568930
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568775
Total Solids by Method 2540 G-2011 L1278387-02,03,04
Method Blank (MB)
(MB) R3588653-1 11/02/20 15:40
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1278383-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1278383-05 11/02/20 15:40 • (DUP) R3588653-3 11/02/20 15:40
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 86.4 90.1 1 4.23 10
Laboratory Control Sample (LCS)
(LCS) R3588653-2 11/02/20 15:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1570180
Volatile Organic Compounds (GC) by Method 8015D/GRO L1278387-02,03,04
Method Blank (MB)
(MB) R3588942-3 11/03/20 13:03
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)98.3 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3588942-2 11/03/20 12:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.80 105 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 100 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568909
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1278387-01
Method Blank (MB)
(MB) R3589709-2 10/31/20 13:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568909
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1278387-01
Method Blank (MB)
(MB) R3589709-2 10/31/20 13:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,3-Trimethylbenzene U 0.104 1.00
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 96.1 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3589709-1 10/31/20 12:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.08 102 70.0-123
Bromobenzene 5.00 5.16 103 73.0-121
Bromodichloromethane 5.00 4.71 94.2 75.0-120
Bromochloromethane 5.00 5.22 104 76.0-122
Bromoform 5.00 3.97 79.4 68.0-132
Bromomethane 5.00 5.87 117 10.0-160
n-Butylbenzene 5.00 5.13 103 73.0-125
sec-Butylbenzene 5.00 5.35 107 75.0-125
tert-Butylbenzene 5.00 5.19 104 76.0-124
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568909
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1278387-01
Laboratory Control Sample (LCS)
(LCS) R3589709-1 10/31/20 12:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Carbon tetrachloride 5.00 4.69 93.8 68.0-126
Chlorobenzene 5.00 5.24 105 80.0-121
Chlorodibromomethane 5.00 4.58 91.6 77.0-125
Chloroethane 5.00 5.68 114 47.0-150
Chloroform 5.00 4.83 96.6 73.0-120
Chloromethane 5.00 5.16 103 41.0-142
2-Chlorotoluene 5.00 5.17 103 76.0-123
4-Chlorotoluene 5.00 5.06 101 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.17 83.4 58.0-134
1,2-Dibromoethane 5.00 5.24 105 80.0-122
Dibromomethane 5.00 4.81 96.2 80.0-120
1,2-Dichlorobenzene 5.00 5.18 104 79.0-121
1,3-Dichlorobenzene 5.00 5.06 101 79.0-120
1,4-Dichlorobenzene 5.00 5.02 100 79.0-120
Dichlorodifluoromethane 5.00 6.14 123 51.0-149
1,1-Dichloroethane 5.00 5.12 102 70.0-126
1,2-Dichloroethane 5.00 5.21 104 70.0-128
1,1-Dichloroethene 5.00 5.02 100 71.0-124
cis-1,2-Dichloroethene 5.00 4.98 99.6 73.0-120
trans-1,2-Dichloroethene 5.00 4.85 97.0 73.0-120
1,2-Dichloropropane 5.00 4.83 96.6 77.0-125
1,1-Dichloropropene 5.00 5.20 104 74.0-126
1,3-Dichloropropane 5.00 5.35 107 80.0-120
cis-1,3-Dichloropropene 5.00 4.60 92.0 80.0-123
trans-1,3-Dichloropropene 5.00 4.97 99.4 78.0-124
2,2-Dichloropropane 5.00 5.14 103 58.0-130
Di-isopropyl ether 5.00 5.03 101 58.0-138
Ethylbenzene 5.00 5.22 104 79.0-123
Hexachloro-1,3-butadiene 5.00 5.15 103 54.0-138
Isopropylbenzene 5.00 5.18 104 76.0-127
p-Isopropyltoluene 5.00 5.03 101 76.0-125
Methylene Chloride 5.00 5.32 106 67.0-120
Methyl tert-butyl ether 5.00 5.05 101 68.0-125
Naphthalene 5.00 4.53 90.6 54.0-135
n-Propylbenzene 5.00 5.40 108 77.0-124
Styrene 5.00 5.03 101 73.0-130
1,1,1,2-Tetrachloroethane 5.00 5.17 103 75.0-125
1,1,2,2-Tetrachloroethane 5.00 5.57 111 65.0-130
Tetrachloroethene 5.00 5.38 108 72.0-132
Toluene 5.00 5.42 108 79.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568909
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1278387-01
Laboratory Control Sample (LCS)
(LCS) R3589709-1 10/31/20 12:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,2,3-Trichlorobenzene 5.00 4.67 93.4 50.0-138
1,2,4-Trichlorobenzene 5.00 5.05 101 57.0-137
1,1,1-Trichloroethane 5.00 4.96 99.2 73.0-124
1,1,2-Trichloroethane 5.00 5.42 108 80.0-120
Trichloroethene 5.00 5.00 100 78.0-124
Trichlorofluoromethane 5.00 5.49 110 59.0-147
1,2,3-Trichloropropane 5.00 5.31 106 73.0-130
1,2,3-Trimethylbenzene 5.00 4.97 99.4 77.0-120
1,2,4-Trimethylbenzene 5.00 5.03 101 76.0-121
1,3,5-Trimethylbenzene 5.00 4.91 98.2 76.0-122
Vinyl chloride 5.00 5.81 116 67.0-131
Xylenes, Total 15.0 15.7 105 79.0-123
(S) Toluene-d8 109 80.0-120
(S) 4-Bromofluorobenzene 96.5 77.0-126
(S) 1,2-Dichloroethane-d4 104 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1568930
Volatile Organic Compounds (GC/MS) by Method 8260D L1278387-02,03,04
Method Blank (MB)
(MB) R3589110-3 11/03/20 21:51
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Benzene U 0.000467 0.00100
Ethylbenzene U 0.000737 0.00250
Toluene U 0.00130 0.00500
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 109 75.0-131
(S) 4-Bromofluorobenzene 97.6 67.0-138
(S) 1,2-Dichloroethane-d4 98.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3589110-1 11/03/20 20:35 • (LCSD) R3589110-2 11/03/20 20:54
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Benzene 0.125 0.120 0.117 96.0 93.6 70.0-123 2.53 20
Ethylbenzene 0.125 0.134 0.132 107 106 74.0-126 1.50 20
Toluene 0.125 0.122 0.122 97.6 97.6 75.0-121 0.000 20
Xylenes, Total 0.375 0.407 0.387 109 103 72.0-127 5.04 20
(S) Toluene-d8 101 105 75.0-131
(S) 4-Bromofluorobenzene 106 100 67.0-138
(S) 1,2-Dichloroethane-d4 108 109 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 1 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210008211 Facility ID 0-021716
Address:1602 Martin L King Jr Pkwy Se
City:Wilson State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:200281 Work Order #:1104801136

COC ID # 00039038
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Ethan Rogerson
Shipped:FedExp
Tracking #:918625060804
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
SB-11 (3')10/26/2020 10:03am S 3 VOA MEOH/NAHSO4BTEX Only 8260D
4 OZ COOL Total Solids 2540 G
4 OZ MEOH TPH-GRO 8015
SB-12 (3')10/26/2020 10:20am S 3 VOA MEOH/NAHSO4BTEX Only 8260D
4 OZ COOL Total Solids 2540 G
4 OZ MEOH TPH-GRO 8015
SB-13 (3')10/26/2020 12:15pm S 3 VOA MEOH/NAHSO4BTEX Only 8260D
4 OZ COOL Total Solids 2540 G
4 OZ MEOH TPH-GRO 8015
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/2 https://www.speedway-ids.com
Page 2 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210008211 Facility ID 0-021716
Address:1602 Martin L King Jr Pkwy Se
City:Wilson State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:200281 Work Order #:1104801136

COC ID # 00039038
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Ethan Rogerson
Shipped:FedExp
Tracking #:918625060804
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
TRIP BLANK 10/26/2020 10:00am W 1 VOA HCL BTEX by 6200B NC task code 2726200B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 39038 Printed: 12/21/2020
Analysis Name: BTEX Only ( Soil )
Analysis Description / Method:BTEX Only / 8260D
Container Type / Preservative:VOA / MEOH/NAHSO4
Analytes: Benzene mg/Kg, Ethylbenzene mg/Kg, Toluene mg/Kg, Total Xylenes mg/Kg

Analysis Name: BTEX by 6200B NC task code 272 ( Water )
Analysis Description / Method:6200B / 6200B
Container Type / Preservative:VOA / HCL
Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethylene ug/L, 1,1-Dichloropropene ug/L,
1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,3-Trimethylbenzene ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L,
1,2-Dichlorobenzene ug/L, 1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethylbenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L,
Benzene ug/L, Bromobenzene ug/L, Bromochloromethane ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chloroethane ug/L, Chloroform ug/L,
Dibromochloromethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Hexachlorobutadiene ug/L, Isopropylbenzene ug/L, Methyl bromide ug/L, Methyl chloride ug/L, Methyl tert butyl
ether ug/L, Methylene bromide ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethyllene ug/L, Toluene ug/L, Trichloroethylene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, Xylene
ug/L, cis-1,2-Dichloroethylene ug/L, cis-1,3-Dichloropropene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Chlorotoluene ug/L, p-Isopropyltoluene ug/L, p-chlorotoluene ug/L, sec-Butylbenzene ug/L,
tert-Butylbenzene ug/L, trans-1,2-Dichloroethylene ug/L, trans-1,3-Dichloropropene ug/L

Analysis Name: TPH-GRO ( Soil )
Analysis Description / Method:GRO 5030/8015B NC TC#350 / 8015
Container Type / Preservative:4 OZ / MEOH
Analytes: Gasoline Range Organics mg/Kg

Speedway LLC.1/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 39038 Printed: 12/21/2020
Analysis Name: Total Solids ( Soil )
Analysis Description / Method:Total Solids / 2540 G
Container Type / Preservative:4 OZ / COOL
Analytes: Solids,Total %

Speedway LLC.2/2 https://www.speedway-ids.com
ANALYTICAL REPORT
November 11, 2020
Geological Resources- NC Speedway
Sample Delivery Group:L1281079
Samples Received:11/03/2020
Project Number:3381
Description:Speedway 8211
Site:8211
Report To:Ms. Nicole Long
3502 Hayes Rd.
Charlotte, NC 28110
Entire Report Reviewed By:
November 11, 2020
[Preliminary Report]
Christl M Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1281079 11/11/20 09:46 1 of 18
November 11, 2020
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3381 L1281079 11/11/20 11:34 1 of 18
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-A L1281079-01 5
Qc: Quality Control Summary 7
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 7
Gl: Glossary of Terms 13
Al: Accreditations & Locations 14
Sc: Sample Chain of Custody 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-A L1281079-01 GW Ethan Rogerson 10/30/20 13:21 11/03/20 09:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1573085 1 11/08/20 13:47 11/08/20 13:47 JAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Christl M Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1281079
MW-A
Collected date/time: 10/30/20 13:21
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,1,1-Trichloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,1,2,2-Tetrachloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,1,2-Trichloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,1-Dichloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,1-Dichloroethene ND 1.00 1 11/08/2020 13:47 WG1573085
1,1-Dichloropropene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2,3-Trichlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2,3-Trichloropropane ND 2.50 1 11/08/2020 13:47 WG1573085
1,2,3-Trimethylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2,4-Trichlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2,4-Trimethylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2-Dibromo-3-Chloropropane ND 5.00 1 11/08/2020 13:47 WG1573085
1,2-Dibromoethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,2-Dichlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,2-Dichloroethane ND 1.00 1 11/08/2020 13:47 WG1573085
1,2-Dichloropropane ND 1.00 1 11/08/2020 13:47 WG1573085
1,3,5-Trimethylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,3-Dichlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
1,3-Dichloropropane ND 1.00 1 11/08/2020 13:47 WG1573085
1,4-Dichlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
2,2-Dichloropropane ND 1.00 1 11/08/2020 13:47 WG1573085
Benzene ND 1.00 1 11/08/2020 13:47 WG1573085
Bromobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
Bromochloromethane ND 1.00 1 11/08/2020 13:47 WG1573085
Bromodichloromethane ND 1.00 1 11/08/2020 13:47 WG1573085
Bromoform ND 1.00 1 11/08/2020 13:47 WG1573085
Carbon tetrachloride ND 1.00 1 11/08/2020 13:47 WG1573085
Chlorobenzene ND 1.00 1 11/08/2020 13:47 WG1573085
Chloroethane ND 5.00 1 11/08/2020 13:47 WG1573085
Chloroform ND 5.00 1 11/08/2020 13:47 WG1573085
Chlorodibromomethane ND 1.00 1 11/08/2020 13:47 WG1573085
Dichlorodifluoromethane ND 5.00 1 11/08/2020 13:47 WG1573085
Di-isopropyl ether ND 1.00 1 11/08/2020 13:47 WG1573085
Ethylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
Hexachloro-1,3-butadiene ND 1.00 1 11/08/2020 13:47 WG1573085
Isopropylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
Bromomethane ND 5.00 1 11/08/2020 13:47 WG1573085
Chloromethane ND 2.50 1 11/08/2020 13:47 WG1573085
Methyl tert-butyl ether ND 1.00 1 11/08/2020 13:47 WG1573085
Dibromomethane ND 1.00 1 11/08/2020 13:47 WG1573085
Methylene Chloride ND 5.00 1 11/08/2020 13:47 WG1573085
Naphthalene ND 5.00 1 11/08/2020 13:47 WG1573085
Styrene ND 1.00 1 11/08/2020 13:47 WG1573085
Tetrachloroethene ND 1.00 1 11/08/2020 13:47 WG1573085
Toluene ND 1.00 1 11/08/2020 13:47 WG1573085
Trichloroethene ND 1.00 1 11/08/2020 13:47 WG1573085
Trichlorofluoromethane ND 5.00 1 11/08/2020 13:47 WG1573085
Vinyl chloride ND 1.00 1 11/08/2020 13:47 WG1573085
Total Xylenes ND 3.00 1 11/08/2020 13:47 WG1573085
cis-1,2-Dichloroethene ND 1.00 1 11/08/2020 13:47 WG1573085
cis-1,3-Dichloropropene ND 1.00 1 11/08/2020 13:47 WG1573085
n-Butylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
n-Propylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
2-Chlorotoluene ND 1.00 1 11/08/2020 13:47 WG1573085
p-Isopropyltoluene ND 1.00 1 11/08/2020 13:47 WG1573085
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1281079
MW-A
Collected date/time: 10/30/20 13:21
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorotoluene ND 1.00 1 11/08/2020 13:47 WG1573085
sec-Butylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
tert-Butylbenzene ND 1.00 1 11/08/2020 13:47 WG1573085
trans-1,2-Dichloroethene ND 1.00 1 11/08/2020 13:47 WG1573085
trans-1,3-Dichloropropene ND 1.00 1 11/08/2020 13:47 WG1573085
(S) Toluene-d8 104 80.0-120 11/08/2020 13:47 WG1573085
(S) 4-Bromofluorobenzene 97.7 77.0-126 11/08/2020 13:47 WG1573085
(S) 1,2-Dichloroethane-d4 104 70.0-130 11/08/2020 13:47 WG1573085
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
Method Blank (MB)
(MB) R3590854-2 11/08/20 10:21
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromochloromethane U 0.128 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
Method Blank (MB)
(MB) R3590854-2 11/08/20 10:21
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methylene Chloride U 0.430 5.00
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene 0.252 J 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,2,3-Trimethylbenzene U 0.104 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 99.1 77.0-126
(S) 1,2-Dichloroethane-d4 104 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3590854-1 11/08/20 09:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.06 101 70.0-123
Bromobenzene 5.00 5.35 107 73.0-121
Bromochloromethane 5.00 5.03 101 76.0-122
Bromodichloromethane 5.00 4.53 90.6 75.0-120
Bromoform 5.00 4.41 88.2 68.0-132
Bromomethane 5.00 6.03 121 10.0-160
n-Butylbenzene 5.00 4.52 90.4 73.0-125
sec-Butylbenzene 5.00 4.84 96.8 75.0-125
tert-Butylbenzene 5.00 4.69 93.8 76.0-124
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
Laboratory Control Sample (LCS)
(LCS) R3590854-1 11/08/20 09:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Carbon tetrachloride 5.00 5.03 101 68.0-126
Chlorobenzene 5.00 4.79 95.8 80.0-121
Chlorodibromomethane 5.00 4.50 90.0 77.0-125
Chloroethane 5.00 5.04 101 47.0-150
Chloroform 5.00 4.75 95.0 73.0-120
Chloromethane 5.00 5.30 106 41.0-142
2-Chlorotoluene 5.00 5.49 110 76.0-123
4-Chlorotoluene 5.00 5.12 102 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.72 94.4 58.0-134
1,2-Dibromoethane 5.00 4.50 90.0 80.0-122
Dibromomethane 5.00 4.58 91.6 80.0-120
1,2-Dichlorobenzene 5.00 4.98 99.6 79.0-121
1,3-Dichlorobenzene 5.00 5.10 102 79.0-120
1,4-Dichlorobenzene 5.00 4.92 98.4 79.0-120
Dichlorodifluoromethane 5.00 5.24 105 51.0-149
1,1-Dichloroethane 5.00 5.04 101 70.0-126
1,2-Dichloroethane 5.00 4.98 99.6 70.0-128
1,1-Dichloroethene 5.00 4.68 93.6 71.0-124
cis-1,2-Dichloroethene 5.00 5.19 104 73.0-120
trans-1,2-Dichloroethene 5.00 5.28 106 73.0-120
1,2-Dichloropropane 5.00 5.23 105 77.0-125
1,1-Dichloropropene 5.00 5.18 104 74.0-126
1,3-Dichloropropane 5.00 4.74 94.8 80.0-120
cis-1,3-Dichloropropene 5.00 4.76 95.2 80.0-123
trans-1,3-Dichloropropene 5.00 4.61 92.2 78.0-124
2,2-Dichloropropane 5.00 4.48 89.6 58.0-130
Di-isopropyl ether 5.00 4.82 96.4 58.0-138
Ethylbenzene 5.00 4.83 96.6 79.0-123
Hexachloro-1,3-butadiene 5.00 4.89 97.8 54.0-138
Isopropylbenzene 5.00 4.70 94.0 76.0-127
p-Isopropyltoluene 5.00 4.81 96.2 76.0-125
Methylene Chloride 5.00 5.63 113 67.0-120
Methyl tert-butyl ether 5.00 4.96 99.2 68.0-125
Naphthalene 5.00 4.83 96.6 54.0-135
n-Propylbenzene 5.00 5.37 107 77.0-124
Styrene 5.00 4.72 94.4 73.0-130
1,1,1,2-Tetrachloroethane 5.00 4.42 88.4 75.0-125
1,1,2,2-Tetrachloroethane 5.00 5.49 110 65.0-130
Tetrachloroethene 5.00 4.90 98.0 72.0-132
Toluene 5.00 4.70 94.0 79.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
Laboratory Control Sample (LCS)
(LCS) R3590854-1 11/08/20 09:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,2,3-Trichlorobenzene 5.00 5.06 101 50.0-138
1,2,4-Trichlorobenzene 5.00 5.10 102 57.0-137
1,1,1-Trichloroethane 5.00 5.00 100 73.0-124
1,1,2-Trichloroethane 5.00 4.27 85.4 80.0-120
Trichloroethene 5.00 5.06 101 78.0-124
Trichlorofluoromethane 5.00 5.31 106 59.0-147
1,2,3-Trichloropropane 5.00 5.50 110 73.0-130
1,2,4-Trimethylbenzene 5.00 4.96 99.2 76.0-121
1,2,3-Trimethylbenzene 5.00 4.81 96.2 77.0-120
1,3,5-Trimethylbenzene 5.00 5.06 101 76.0-122
Vinyl chloride 5.00 4.99 99.8 67.0-131
Xylenes, Total 15.0 14.5 96.7 79.0-123
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 95.7 77.0-126
(S) 1,2-Dichloroethane-d4 106 70.0-130
L1280740-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1280740-01 11/08/20 13:26 • (MS) R3590854-3 11/08/20 20:06 • (MSD) R3590854-4 11/08/20 20:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Benzene 5.00 ND 5.81 3.91 116 78.2 1 17.0-158 J3 39.1 27
Bromobenzene 5.00 ND 6.25 4.11 125 82.2 1 30.0-149 J3 41.3 28
Bromodichloromethane 5.00 ND 5.20 3.91 104 78.2 1 31.0-150 J3 28.3 27
Bromoform 5.00 ND 5.48 4.19 110 83.8 1 29.0-150 26.7 29
Bromomethane 5.00 ND 5.64 ND 113 77.2 1 10.0-160 37.5 38
n-Butylbenzene 5.00 ND 6.04 3.31 121 66.2 1 31.0-150 J3 58.4 30
sec-Butylbenzene 5.00 ND 6.19 3.47 124 69.4 1 33.0-155 J3 56.3 29
tert-Butylbenzene 5.00 ND 6.30 3.55 126 71.0 1 34.0-153 J3 55.8 28
Carbon tetrachloride 5.00 ND 6.49 4.18 130 83.6 1 23.0-159 J3 43.3 28
Chlorobenzene 5.00 ND 5.82 4.00 116 80.0 1 33.0-152 J3 37.1 27
Chlorodibromomethane 5.00 ND 5.25 4.07 105 81.4 1 37.0-149 25.3 27
Chloroethane 5.00 ND ND ND 98.0 69.4 1 10.0-160 J3 34.2 30
Bromochloromethane 5.00 ND 5.59 4.28 112 85.6 1 38.0-142 J3 26.5 26
Chloroform 5.00 ND 5.88 ND 118 78.8 1 29.0-154 J3 39.5 28
Chloromethane 5.00 ND 5.55 3.71 111 74.2 1 10.0-160 J3 39.7 29
2-Chlorotoluene 5.00 ND 6.39 3.97 128 79.4 1 32.0-153 J3 46.7 28
4-Chlorotoluene 5.00 ND 5.90 3.60 118 72.0 1 32.0-150 J3 48.4 28
1,2-Dibromo-3-Chloropropane 5.00 ND 5.29 ND 106 86.2 1 22.0-151 20.4 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
L1280740-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1280740-01 11/08/20 13:26 • (MS) R3590854-3 11/08/20 20:06 • (MSD) R3590854-4 11/08/20 20:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
1,2-Dibromoethane 5.00 ND 5.33 4.18 107 83.6 1 34.0-147 24.2 27
Dibromomethane 5.00 ND 5.07 4.32 101 86.4 1 30.0-151 16.0 27
1,2-Dichlorobenzene 5.00 ND 5.69 4.14 114 82.8 1 34.0-149 J3 31.5 28
1,3-Dichlorobenzene 5.00 ND 5.88 3.71 118 74.2 1 36.0-146 J3 45.3 27
1,4-Dichlorobenzene 5.00 ND 6.14 3.97 123 79.4 1 35.0-142 J3 42.9 27
Dichlorodifluoromethane 5.00 ND 7.01 ND 140 89.8 1 10.0-160 J3 43.8 29
1,1-Dichloroethane 5.00 ND 5.70 4.00 114 80.0 1 25.0-158 J3 35.1 27
1,2-Dichloroethane 5.00 ND 5.20 4.23 104 84.6 1 29.0-151 20.6 27
1,1-Dichloroethene 5.00 ND 5.83 3.68 117 73.6 1 11.0-160 J3 45.2 29
cis-1,2-Dichloroethene 5.00 ND 5.52 3.86 110 77.2 1 10.0-160 J3 35.4 27
trans-1,2-Dichloroethene 5.00 ND 6.34 3.75 127 75.0 1 17.0-153 J3 51.3 27
1,2-Dichloropropane 5.00 ND 6.09 4.32 122 86.4 1 30.0-156 J3 34.0 27
1,1-Dichloropropene 5.00 ND 6.16 3.78 123 75.6 1 25.0-158 J3 47.9 27
1,3-Dichloropropane 5.00 ND 5.56 4.52 111 90.4 1 38.0-147 20.6 27
cis-1,3-Dichloropropene 5.00 ND 5.46 4.22 109 84.4 1 34.0-149 25.6 28
trans-1,3-Dichloropropene 5.00 ND 5.46 4.36 109 87.2 1 32.0-149 22.4 28
2,2-Dichloropropane 5.00 ND 5.92 3.90 118 78.0 1 24.0-152 J3 41.1 29
Di-isopropyl ether 5.00 ND 5.30 4.02 106 80.4 1 21.0-160 27.5 28
Ethylbenzene 5.00 ND 6.53 3.88 131 77.6 1 30.0-155 J3 50.9 27
Hexachloro-1,3-butadiene 5.00 ND 5.65 3.79 113 75.8 1 20.0-154 J3 39.4 34
Isopropylbenzene 5.00 ND 5.98 3.60 120 72.0 1 28.0-157 J3 49.7 27
p-Isopropyltoluene 5.00 ND 6.12 3.43 122 68.6 1 30.0-154 J3 56.3 29
Methylene Chloride 5.00 ND 5.58 ND 112 78.0 1 23.0-144 J3 35.4 28
Methyl tert-butyl ether 5.00 ND 5.47 4.59 109 91.8 1 28.0-150 17.5 29
Naphthalene 5.00 ND 31.8 5.94 636 119 1 12.0-156 J5 J3 137 35
n-Propylbenzene 5.00 ND 6.98 3.86 140 77.2 1 31.0-154 J3 57.6 28
Styrene 5.00 ND 5.75 3.84 115 76.8 1 33.0-155 J3 39.8 28
1,1,1,2-Tetrachloroethane 5.00 ND 5.43 3.59 109 71.8 1 36.0-151 J3 40.8 29
1,1,2,2-Tetrachloroethane 5.00 ND 6.48 5.19 130 104 1 33.0-150 22.1 28
Tetrachloroethene 5.00 ND 6.06 3.55 121 71.0 1 10.0-160 J3 52.2 27
Toluene 5.00 ND 6.47 4.02 129 80.4 1 26.0-154 J3 46.7 28
1,2,3-Trichlorobenzene 5.00 ND 5.39 4.02 108 80.4 1 17.0-150 29.1 36
1,2,4-Trichlorobenzene 5.00 ND 5.82 3.99 116 79.8 1 24.0-150 J3 37.3 33
1,1,1-Trichloroethane 5.00 ND 6.10 3.77 122 75.4 1 23.0-160 J3 47.2 28
1,1,2-Trichloroethane 5.00 ND 5.23 4.11 105 82.2 1 35.0-147 24.0 27
Trichloroethene 5.00 ND 5.83 3.77 117 75.4 1 10.0-160 J3 42.9 25
Trichlorofluoromethane 5.00 ND 6.83 ND 137 82.8 1 17.0-160 J3 49.0 31
1,2,3-Trichloropropane 5.00 ND 5.84 5.08 117 102 1 34.0-151 13.9 29
1,2,4-Trimethylbenzene 5.00 ND 8.19 4.15 164 83.0 1 26.0-154 J5 J3 65.5 27
1,2,3-Trimethylbenzene 5.00 ND 6.79 3.84 136 76.8 1 32.0-149 J3 55.5 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1573085
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1281079-01
L1280740-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1280740-01 11/08/20 13:26 • (MS) R3590854-3 11/08/20 20:06 • (MSD) R3590854-4 11/08/20 20:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
1,3,5-Trimethylbenzene 5.00 ND 6.80 3.83 136 76.6 1 28.0-153 J3 55.9 27
Vinyl chloride 5.00 ND 5.59 3.61 112 72.2 1 10.0-160 J3 43.0 27
Xylenes, Total 15.0 ND 20.6 12.1 137 80.7 1 29.0-154 J3 52.0 28
(S) Toluene-d8 103 102 80.0-120
(S) 4-Bromofluorobenzene 93.2 97.3 77.0-126
(S) 1,2-Dichloroethane-d4 102 102 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 1

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210008211 Facility ID 0-021716
Address:1602 Martin L King Jr Pkwy Se
City:Wilson State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:200281 Work Order #:1104801136

COC ID # 00054145
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Ethan Rogerson
Shipped:FedExp
Tracking #:100963782192
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-A 10/30/2020 01:21pm W 1 VOA HCL BTEX by 6200B NC task code 2726200B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/1 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 54145 Printed: 12/26/2020
Analysis Name: BTEX by 6200B NC task code 272 ( Water )
Analysis Description / Method:6200B / 6200B
Container Type / Preservative:VOA / HCL
Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethylene ug/L, 1,1-Dichloropropene ug/L,
1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,3-Trimethylbenzene ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L,
1,2-Dichlorobenzene ug/L, 1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethylbenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L,
Benzene ug/L, Bromobenzene ug/L, Bromochloromethane ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chloroethane ug/L, Chloroform ug/L,
Dibromochloromethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Hexachlorobutadiene ug/L, Isopropylbenzene ug/L, Methyl bromide ug/L, Methyl chloride ug/L, Methyl tert butyl
ether ug/L, Methylene bromide ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethyllene ug/L, Toluene ug/L, Trichloroethylene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, Xylene
ug/L, cis-1,2-Dichloroethylene ug/L, cis-1,3-Dichloropropene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Chlorotoluene ug/L, p-Isopropyltoluene ug/L, p-chlorotoluene ug/L, sec-Butylbenzene ug/L,
tert-Butylbenzene ug/L, trans-1,2-Dichloroethylene ug/L, trans-1,3-Dichloropropene ug/L

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