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HomeMy WebLinkAboutWA-27683_38811_CA_RPTS_20210722_MRP 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 July 22, 2021 Mr. Jared Edwards North Carolina Department of Environmental Quality Washington Regional Office 943 Washington Square Mall Washington, North Carolina 27889 Re: UST Closure Report June 2021 Handy Mart 15 2495 US Highway 13 North Goldsboro, Wayne County North Carolina Facility ID Number: 00-0-0000005485 Incident Number: 38811 GRI Project Number: 5415 Dear Mr. Edwards, Please find enclosed the referenced report, for the above mentioned site. If you have any questions, please contact William Regenthal at 704-845-4010. Sincerely, Geological Resources, Inc. Leslie Maxtone-Graham Administrative Assistant Enclosure Cc: Mr. Scott Driscoll; E.J. Pope & Son, Inc., file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Engineering Certification: C-2727 • Geology Certification: C-127 Ground Water Monitoring Report June 2021 Handy Mart 15 2495 US Highway 13 North Goldsboro, Wayne County North Carolina Facility ID Number: 00-0-0000005485 Incident Number: 38811 GRI Project Number: 5415 Prepared for: Mr. Scott Driscoll E.J. Pope & Son, Inc. Post Office Box 649 Mount Olive, North Carolina 28365 July 22, 2021 William Regenthal, P.G. Project Manager Tyler Frazier Staff Scientist ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 i SITE INFORMATION 1. Site Identification  Handy Mart 15 (Facility ID 00-0-0000005485)  Incident Number 38811 – High Risk (H190A)  Location of Source Area: 2495 US Highway 13 North Goldsboro, NC 28365 Wayne County 35.404222°N, 77.898599°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner E.J. Pope & Son, Inc. P.O. Box 649 Mount Olive, NC 28365 scott_driscoll@ejpope.com 919-658-6566 UST Operator E.J. Pope & Son, Inc. P.O. Box 649 Mount Olive, NC 28365 scott_driscoll@ejpope.com 919-658-6566 Property Owner Marie P. Peele 2521 US 13 North Goldsboro, NC 27534 Email Unknown Phone No. Unknown Property Occupant Handy Mart 15 2495 US Highway 13 North Goldsboro, NC 27530 Email Unknown 919-778-1468 Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 wlr@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS North America, Inc. 4405 Vineland Road, suite C-15 Orlando, FL 32811 State Certification No. 573 407-425-6700 3. Information about Release  Release was reported on January 28, 2020  An unknown amount of product was released from the leaking UST System  Two 8,000-gallon gasoline, one 4,000-gallon gasoline and one 4,000-gallon kerosene USTs are in use at the site. One 4,000-gallon kerosene UST was permanently closed in 1987. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 ii EXECUTIVE SUMMARY Handy Mart 15 is located at 2495 US Highway 13 North in Goldsboro, Wayne County, North Carolina. The site is currently owned by Ms. Marie Peele and is operated by E.J. Pope & Son, Inc. as a petroleum retail facility and convenience store. The site is covered by concrete, asphalt, and grass. Two 8,000-gallon gasoline, one 4,000-gallon gasoline, and one 4,000-gallon kerosene USTs are in use at the site. One 4,000- gallon kerosene UST was permanently closed in 1987. The surrounding properties are commercial and residential. On January 28, 2020, a Geoenvironmental Phase II Investigation was submitted to NCDEQ documenting that soil samples collected in the DOT right-of-way indicated a potential release. On June 4, 2020, a NORR was issued for a site check by NCDEQ. Laboratory results from the Site Check activities confirmed that a release had occurred at the site. During the August 13, 2020, receptor survey, seven possible water supply wells were identified within a 1,500-foot radius of the site. Two possible potable water supply wells were identified within a 1,000-foot radius of the site. No water supply wells were identified within a 250-foot radius of the site. Public water is available to the subject site and to most surrounding properties. No surface water bodies were identified within a 500-foot radius of the site. Receptor information was updated in February 2021 when it was confirmed that WSW-5 does not exist. Additionally, an inactive water supply well (WSW-8) was observed at 126 E W Lane. The property owner of 126 E W Lane confirmed that her property is connected to municipal water and that the municipal line stops at her residence. The owners of WSW-4 and WSW- 7 have agreed to connect their properties to the municipal water line. Currently, bids are being solicited from local plumbers to connect the properties containing WSW-4 and WSW-7 to the municipal water supply. Four Type II monitoring wells were installed at the site during past assessment activities. On June 29, 2021, four monitoring wells were gauged, purged and sampled. No free product was observed in any of the monitoring wells. Concentrations of benzene, toluene, xylenes, naphthalene, n- propylbenzene, isopropylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-1 and MW-2. All of the reported contaminant concentrations were less than the GCLs. Contaminant mass at the site has increased by 185% since October 2020. Based on this information, the risk classification for the site should remain high risk until public water connections can be made to the properties associated with WSW-4 and WSW-7. Additional monitoring well installations would be unnecessary if the municipal water connections are completed. In the interim, semi-annual ground water monitoring should continue at the site with the next sampling event tentatively scheduled for January 2022. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 iii ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment RAL: Regulatory Action Level SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocar ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii ACRONYMS ....................................................................................................................................... iii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................2 3.0 FREE PRODUCT REMOVAL ........................................................................................................4 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4 5.0 CONCLUSIONS .........................................................................................................................4 6.0 LIMITATIONS ...........................................................................................................................4 7.0 STATEMENTS AND CERTIFICATION ...........................................................................................4 FIGURES Figure 1: Site Location Map Figure 2: Site Map Figure 3: Site Vicinity Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map Figure 6: Benzene Isoconcentration Map Figure 7: Naphthalene Isoconcentration Map Figure 8: Contaminant Mass Area Map TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Water Supply Well Information Table 4: Adjacent Property Owner Information Table 5: Well Construction and Gauging Information Table 6: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: State Correspondence Appendix B: Laboratory Report – Ground Water Samples Appendix C: Contaminant Mass Calculations ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 1 1.0 SITE HISTORY AND CHARACTERIZATION GRI) presents the results of June 2021 ground water sampling event at the Handy Mart 15 site; located at 2495 US Highway 13 North in Goldsboro, Wayne County, North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 21-370, which was submitted to NCDEQ on June 7, 2021, and was approved as Task Authorization No. 38811-4 on June 8, 2021. State correspondence has been included as Appendix A. The site is currently owned by Ms. Marie Peele and is operated by E.J. Pope & Son, Inc. as a petroleum retail facility and convenience store. A site check was conducted at the site in June 2020 following a Geoenvironmental Phase II Investigation that confirmed the presence of a release. Currently, two 8,000- gallon gasoline, one 4,000-gallon gasoline and one 4,000-gallon kerosene USTs are active at the site. One 4,000-gallon kerosene UST was permanently closed in 1987. UST owner/operator information and UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below: The site and surrounding area are a mixture residential and commercial properties. The site contains one building (the convenience store) and is primarily capped with concrete and asphalt. The overall topography at the site is relatively flat. No surface water bodies were identified within a 500-foot radius of the site. Four Type II monitoring wells (MW-1 through MW-4) were installed at the site during previous ground water assessment activities. A Site Map showing the locations of the monitoring wells and the structures on-site has been included as Figure 2. On August 13, 2020, GRI personnel conducted a receptor survey at the site. Seven possible water supply wells were identified within a 1,500-foot radius of the site. Two possible potable water supply wells were identified within a 1,000-foot radius of the site. No water supply wells were identified with-in a 250-foot ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 2 radius of the site. Please note that it was later determined that the water supply well previously identified as WSW-5 does not exist. Receptor information was updated in February 2021 when an inactive water supply well (WSW-8) was observed at 126 E W Lane. The property owner of 126 E W Lane confirmed that her property is connected to municipal water and that the municipal line stops at her residence. One potable water supply well (WSW-4) is located within 1,000-feet of the site and one potable water supply well (WSW-7) is located just beyond the 1,000-foot radius of the site. The owners of WSW-4 and WSW-7 have agreed to connect their properties to the municipal water line. Currently, bids are being solicited to local plumbers to connect the properties associated with WSW-4 and WSW-7 to the municipal water supply. Public water is available to the site and to most surrounding properties. Water supply well information and adjacent property owner information are presented in Table 3 and Table 4, respectively. A Site Vicinity Map showing the adjacent properties has been included as Figure 3. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION On June 29, 2021, four Type II monitoring wells (MW-1 through MW-4) were gauged, purged and sampled in accordance with NCDEQ guidelines. No free product was observed at the site. Depths to ground water in the Type II monitoring wells ranged from 2.90 feet to 3.64 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells ranged from 96.50 feet to 96.88 feet. Ground water flow was generally to the southeast with a horizontal gradient of less than 0.01 feet per foot. Well construction and gauging information is presented in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-1 2 - 12 12 100.00 3.28 --- 96.72 MW-2 2 - 12 12 99.40 2.90 --- 96.50 MW-3 2 - 12 12 100.35 3.64 --- 96.71 MW-4 2 – 11 11 100.27 3.39 --- 96.88 Ground water samples collected from the monitoring wells were submitted for laboratory analyses of VOCs using EPA Method 6200B. Concentrations of benzene, toluene, xylenes, naphthalene, isopropylbenzene n-propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-1 and MW-2. All of the reported contaminant concentrations were less than the GCLs. A summary of the analytical results for ground water samples collected on June 29, 2021, is presented in Table 6. A Ground Water Quality Map based on the June 2021 data is included as Figure 5. Contaminant specific isoconcentration maps for benzene and naphthalene are included as Figures 6 and 7, respectively. A complete report of laboratory analyses for the June 2021 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 3 sampling event has been included as Appendix C. A summary of the current ground water analytical data is shown below: Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000 MW-1 0.91 J 5.4 104 444 <0.63 84.4 MW-2 929 695 568 1,670 <6.3 190 MW-3 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and naphthalene concentrations from the October 2020 ground water sampling event as well as the maximum historical water column height observed in each area. The contaminant plume was based on the naphthalene concentrations during the October 2020 ground water sampling event. The contaminant mass has increased by 185% since October 2020 and has decreased 76.6% since February 2021. Contaminant mass calculations have been included as Appendix C. A map of the contaminant mass area has been included as Figure 8. A chart depicting the overall trend in contaminant mass is shown below: The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a seasonal high depth to water of approximately 2.90 to 3.64 feet below ground surface (bgs). ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: July 22, 2021 Handy Mart 15 Project Manager: William Regenthal, P.G. GRI Project No. 5415 4 3.0 FREE PRODUCT REMOVAL No free product has been detected at the site to date. 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS No natural attenuation monitoring plan is currently in place at the site. 5.0 CONCLUSIONS  The site is an active petroleum retail facility and convenience store. Land use in the area consists of commercial and residential properties.  Currently, bids are being solicited in order to connect the properties associated with WSW-4 and WSW-7 to the municipal water supply.  During the June 2021 gauging event, ground water flow was generally toward the southeast with a horizontal gradient of less than 0.01 feet per foot.  Concentrations of benzene, toluene, xylenes, naphthalene, isporppylbenzene, n-propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-1 and MW-2. All the reported contaminant concentrations were less than the GCLs. No free product was observed at the site.  Contaminant mass has increased by 185% since October 2020, but has decreased by 76.6% since February 2021.  Based on this information, the risk classification for the site should remain high risk until public water connections can be made to the properties associated with WSW-4 and WSW-7. Additional monitoring well installations would be unnecessary if the municipal water connections are completed. In the interim, semi-annual ground water monitoring should continue at the site with the next sampling event tentatively scheduled for January 2022. 6.0 LIMITATIONS This report has been prepared for the exclusive use of E.J. Pope & Son, Inc. for specific application to the referenced site in Wayne County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. 7.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. n/a Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO FIGURES SITE LOCATIONFigure 1 Site LocationHandy Mart 152495 US Highway 13 Goldsboro, Wayne County, NCIncident No. 38811GRI Project No. 5415500 M2000 FTDate: 07/09/2020Location: 35.404222° N -77.898599° W Dad 2 "J "J !H !H !H !H S DJ SITE WSW-5 WSW-8 3620920776 3620834499362074304536208318773620834930362074337336207398873620831715 3620842187 362083868636207421513620842032 3620749004 3620842496 WSW-6 WSW-3 WSW-2 WSW-1 WSW-7 Ut U t Ut E W LN N US 13 HWYH O O D SW A M P RDTWIN DR DURWOOD DR DARYL DR CENTRAL HEIGHTS RDMOORING LN WSW-4 FIGURE 3: SITE VICINITY MAPHANDY MART #152495 US HIGHWAY 13 NORTHGOLDSBORO, WAYNE COUNTYNORTH CAROLINAINCIDENT NO. 38811GRI PROJECT NO. 5415 PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 11, 2020 ³ 0 300150Feet 1 inch = 300 feet 1,500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS 500-FOOT RADIUS LEGEND DJ Water Supply Well (Does Not Exist) S Water Supply Well (Inactive) !H Water Supply Well (Non-Potable) "J Water Supply Well (Potable) Wayne_County_Centerlines All_Ditches_Streams_Rivers Adjacent Properties and Well Owners Wayne_County_Parcels TABLES UST ID Number 1-3 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 4 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 5 Facility ID Number Owner or Operator? Owner/Operator 00-0-0000005485 TABLE 1 UST OWNER/OPERATOR INFORMATION HANDY MART 15 (INCIDENT NO. 38811) PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566 Name of Owner or Operator Dates of Ownership / Operation E. J. Pope & Son, Inc.04/01/1982 - Current Address Telephone Number 00-0-0000005484 Name of Owner or Operator Dates of Ownership / Operation E. J. Pope & Son, Inc.03/31/1986 - 03/01/1987 Address Telephone Number PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566 00-0-0000005484 PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566 Name of Owner or Operator Dates of Ownership / Operation E. J. Pope & Son, Inc.03/31/1987 - Current Address Telephone Number Page 1 of 1 Date: 07/06/20 Was Release Associated with UST System? (Yes / No) 1 Gasoline 8,000 4/1/1982 Single Wall Steel 8' x 21' 4"Single Wall FRP Current Yes 2 Gasoline 8,000 4/1/1982 Single Wall Steel 8' x 21' 4"Single Wall FRP Current Yes 3 Gasoline 4,000 4/1/1982 Single Wall Steel 64" x 24'Single Wall FRP Current Yes 4 Kerosene 4,000 3/31/1986 Single Wall Steel 64" x 24'Single Wall FRP Removed No 5 Kerosene 4,000 3/31/1987 Single Wall Steel 64" x 24'Single Wall FRP Current Yes TABLE 2 UST SYSTEM INFORMATION HANDY MART 15 (INCIDENT NO. 38811) UST ID No. Current or Most Recent Contents Capacity (gallons) Date Installed Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Status of UST Facility ID #: 00-0-0000005485 Page 1 of 1 Date: 02/23/2021 Facility ID # : 00-0-0000005485 Well ID Parcel ID No.Well Owner Mailing Address Well Location Address Well Use (Potable/ Agriculture, etc.) Public Water Connected Distance from source area of release (ft.) WSW-1 3620743373 Knox Charles Atlas & Wife 102 Daryl Drive Goldsboro, NC 27534 102 Daryl Drive Goldsboro, NC 27534 Not in Use Yes ~920 NW WSW-2 3620743045 Smith Craig 3009 US Highway 13 N Goldsboro, NC 27530 101 Daryl Drive Goldsboro, NC 27534 Not in Use Yes ~850 W WSW-3 3620742151 Bledsoe Richard 103 Daryl Drive Goldsboro, NC 27534 103 Daryl Drive Goldsboro, NC 27534 Not in Use Yes ~970 W WSW-4 3620838686 Gurley Emily C.142 EW Lane Goldsboro, NC 27534 142 EW Lane Goldsboro, NC 27534 Potable No ~720 E WSW-5 3620842496 Ambriz Filiberto 109 Shady Meadow Lane Clayton, NC 27520 2545 N. US 13 Highway Goldsboro, NC 27534 Does Not Exist Yes, house vacant NA WSW-6 3620842187 Peele Marie P.2521 US 13 North Goldsboro, NC 27534 2521 US 13 North Goldsboro, NC 27534 Not in Use Yes ~280 N WSW-7 3620920776 Earl W. Smith Heirs 126 EW Lane Goldsboro, NC 27534 180 EW Lane Goldsboro, NC 27534 Potable No ~1,110 SE WSW-8 3620834499 Carolyn Smith Heirs 126 EW Lane Goldsboro, NC 27534 126 EW Lane Goldsboro, NC 27534 Not in Use Yes ~630 SE Notes: • Water supply wells are shown on Figure 3 • Ft. BGS : Feet below ground surface TABLE 3 WATER SUPPLY WELL INFORMATION HANDY MART 15 (INCIDENT NO. 38811) Page 1 of 1 Date: 11/11/20 Facility ID # : 00-0-0000005485 PIN Number Property Owner Name Owner Mailing Address 3620831877 (site)Peele, Marie P.2521 US 13 North Goldsboro, NC 27534 3620831715 Boyette, Kenneth Ray Jr.2457 US 13 Hwy North Goldsboro, NC 27534 3620739887 Fields, Stanley P.105 Durwood Drive Goldsboro, NC 27534 3620842032 Peele, Durwood Lee and Heirs 112 Durwood Drive Goldsboro, NC 27534 3620834930 JCTB LLC 126 EW Lane Goldsboro, NC 27534 3620834499 Smith, Carolyn S.126 E W Lane Goldsboro, NC 27534 3620749004 Peele, Marie P.2521 US 13 North Goldsboro, NC 27534 Note: • Properties are keyed to Figure 2. TABLE 4 ADJACENT PROPERTY OWNER INFORMATION HANDY MART 15 (INCIDENT NO. 38811) Page 1 of 1 Date: 07/15/21 Well ID Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 10/22/20 4.59 ---95.41 02/04/21 2.10 ---97.90 06/29/21 3.28 ---96.72 10/22/20 4.21 ---95.19 02/04/21 1.75 ---97.65 06/29/21 2.90 ---96.50 10/22/20 4.90 ---95.45 02/04/21 2.32 ---98.03 06/29/21 3.64 ---96.71 10/22/20 6.91 ---93.36 02/04/21 2.36 ---97.91 06/29/21 3.39 ---96.88 Notes: 10/22/20MW-1 2 - 12 2 2 2 2 10/22/20MW-4 10/22/20MW-3 10/22/20MW-2 • Elevation relative to mean sea level. • ft BGS : feet below ground surface. • NM : Not measured. TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION HANDY MART 15 (INCIDENT NO. 38811) Facility ID # : 00-0-0000005485 100.27 100.35 99.40 100.00 11 12 12 12 2 - 11 2 - 12 2 - 12 Page 1 of 1 Date: 07/15/21 Facility ID # : 00-0-0000005485 EPA 504.1 EPA 6010 Well ID Date Sampled (mm/dd/yy) MAC (μg/l)1 600 600 500 20 6 40 10 3 70 70 400 400 0.02 15 1 30 400 700 200 700 10,000 200 GCL (μg/l)5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 3,000 25,000 30,000 28,500 #####50 15,000 1,000 12,500 NE NE NE NE NE NE 10/22/20 <0.31 3.6 70.7 305 <0.31 47.1 12.0 J <5.0 <0.50 6.3 21.4 151 37.2 <0.0037 <5.0 7.3 13.0 513 <35 1,060 <49 <49 278 02/04/21 0.77 J 4.3 76.3 429 <0.63 70.6 <10 <10 <1.0 11.5 32.6 208 42.8 NR NR NR NR NR NR NR NR NR NR 06/29/21 0.91 J 5.4 104 444 <0.63 84.4 NR NR <1.0 10.9 35.3 243 52.3 NR NR NR NR NR NR NR NR NR NR 10/22/20 637 127 176 479 12.4 69.0 146 J 134 J 4.6 J 56.4 174 241 52.5 <0.0037 6.8 32.6 44.2 1,130 <35 2,920 <99 <99 259 J 02/04/21 2,760 4,560 2,090 7,250 <13 489 760 J <200 <20.0 152 382 1,750 401 NR NR NR NR NR NR NR NR NR NR 06/29/21 929 695 568 1,670 <6.3 190 NR NR <10 72.2 227 671 141 NR NR NR NR NR NR NR NR NR NR 10/22/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.13 <0.13 <0.13 <0.0037 22.9 <0.54 <0.61 <35 <35 <35 <51 <51 98.7 J 02/04/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR 06/29/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR 10/22/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.13 <0.13 <0.13 <0.0038 1,130 <0.50 <0.57 <35 <35 <35 <51 <51 <82 02/04/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR 06/29/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR WSW-7 02/04/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR Notes: • Results reported in micrograms per liter (µg/l). • MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202. • < : Less than the method detection limit specified in the laboratory report. • GCL: Gross contamination level. • Concentrations in bold face type indicate the MAC was below the reported concentration. • J: Estimated value. • NE: Not established. • NR: Not requested. • Refer to laboratory report for other detectable concentrations which did not exceed the MACs. TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS HANDY MART 15 (INCIDENT NO. 38811) EPA 625.1 MADEP VPH MADEP EPHEPA 6200B 1,2-Dibromoethane(EDB)1-Methylnaphthalenetert-Amyl alcohol(TAA)tert-Butyl alcohol(TBA)Analytical Method n-PropylbenzeneXylenesEthylbenzeneTolueneC11-C22 AromaticsC9-C12 AliphaticsNaphthaleneMTBEC19-C36 AliphaticsC5-C8 Aliphatics2-MethylnaphthaleneLeadC9-C18 AliphaticsC9-C10 Aromatics1,3,5- Trimethylbenzene1,2,4-TrimethylbenzeneBenzeneIsopropylbenzeneContaminant of Concern  MW-4 MW-3 MW-2 MW-1 Methyl chloride(Chloromethane)Page 1 of 1 APPENDICES APPENDIX A State Correspondence ROY COOPER Governor MICHAEL S. REGAN Secretary MICHAEL SCOTT Director State of North Carolina | Environmental Quality | Waste Management Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 February 25, 2021 Scott Driscoll E.J. Pope & Son, Inc. PO Drawer 649 Mount Olive, NC 28365 Re: Notice of Regulatory Requirements 15A NCAC 2L .0407(c) [High Risk] Risk-based Assessment and Corrective Action For Petroleum Underground Storage Tanks Handy Mart 15 / Peele Property UST Facility ID: 00-0-0000005485 2495 US Highway 13 North, Goldsboro, NC Wayne County Incident Number: 38811 Risk Classification: High Ranking: H 185 A Dear Mr. Driscoll: The Underground Storage Tank (UST) Section, Division of Waste Management, Department of Environmental Quality (Department) has received and reviewed the February 23, 2021 Ground Water Monitoring Report for the subject site submitted in lieu of a Comprehensive Site Assessment (CSA) Report. This report documents groundwater sampling efforts performed on February 4, 2021 and includes updated receptor information along with copies of signed agreements to connect two potentially at-risk drinking water supply well owners to public water available in the area. With while any potentially at-risk well remains present, under the definitions provided in Title 15A of the North Carolina Administrative Code (NCAC) Subchapter 2L Section .0406, the risk posed by the discharge or release at this site remains classified as High. Once the public water connections have been completed, or the plume onsite is modeled as stable with no apparent migration towards the potential receptors, the site risk classification may be reevaluated. Please note that contaminant source definition and abatement efforts are necessary for any risk reclassification and/or risk-based closure strategy, as is confirmation that the site meets the allowable maximum soil contaminant concentrations (MSCCs) as described in Title 15A NCAC 2L .0408(3) and gross contaminant levels (GCLs) for groundwater contamination in the Intermediate Risk Classification definition under Title 15A NCAC 2L .0406(2). Any request for reclassification must present one or more potential sources for the contamination detected during the Department of Transportation’s Environmental Site Assessment at soil boring 2495DPT-3, during the Site Check at soil boring SB-3-2’, and during the Phase II Limited Site Assessment at MW-1 and MW-2. The request must document any subsequent abatement efforts undertaken to address those sources and stop any ongoing releases to the environment. Until the site has been reclassified, Title 15A NCAC 2L .0407(c) [High Risk] continues to require you to comply with the assessment and cleanup requirements of Title 15A NCAC 2N .0706 and Title15A NCAC 2L .0106(c) and 2L .0106(g), as described in the most recent version of the Guidelines for Assessment for UST Releases. Based on the information provided in this most recent monitoring report, the prior deadline for preparing and submitting a report in accordance with these requirements has been rescinded. A new deadline for completion of the CSA and submittal of a report documenting the findings is set at 90 days from the date of this notice. In accordance with Title 15A NCAC 2L .0114, a summary of the CSA Report must also be submitted to the local Health Director and the local Chief Administrative Officer, no later than five working days after submittal of the CSA Report to this office. Failure to comply in the manner and time specified may result in the assessment of civil penalties and/or the use of other enforcement mechanisms. Within the CSA Report conclusions and recommendations, a general description of a proposed plausible strategy to remediate the contamination onsite should be included as a preliminary step in moving towards any formal corrective action plan. If not included in the CSA Report, this information must be provided separately prior to the authorization of any corrective action feasibility study tasks. Further extension to the CSA deadline may be obtained through the completion and submittal of an Accelerated Site Characterization (ASC) Report prior to the completion of the CSA, as described in the Department’s December 2, 2020 Notice of Regulatory Requirements (NORR). Also as noted in that NORR, Title 15A NCAC 2L .0407(a) presents a continuing obligation to notify the Department of any changes that might affect the risk or land use classifications that have been assigned. Additionally, the requirements to submit a Preapproval/Claim Authorization Form if you intend to seek reimbursement from the State Trust Fund for any eligible costs incurred at this site remain as described in that NORR. Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to the Department in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b). If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking Petroleum Underground Storage Tank Cleanup Fund, please contact the UST Section Trust Fund Branch at (919) 707-8171. If you have questions regarding the information contained in this letter, please contact me at the physical address, telephone number, or email address listed below. Sincerely, Jared M. Edwards Hydrogeologist - Washington Regional Office UST Section, Division of Waste Management, NCDEQ (252) 948-3949 / jared.edwards@ncdenr.gov cc: E.J. Pope & Son, Inc., Scott Driscoll (electronic copy) Geological Resources, Inc., William Regenthal (electronic copy) APPENDIX B Laboratory Report – Ground Water Samples 07/09/21 Technical Report for GRI (Geological Resources Inc.) Handy Mart 15; 2495 US 13, Goldsboro, NC 5415 SGS Job Number: FA86866 Sampling Date: 06/29/21 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 wlr@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com; nml@geologicalresourcesinc.com ATTN: William Regenthall Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 07/09/21 e-Hardcopy 2.0 Automated Report 23 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 23 FA86866 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA86866-1: MW-1 ........................................................................................................6 3.2: FA86866-2: MW-2 ........................................................................................................8 3.3: FA86866-3: MW-3 ........................................................................................................10 3.4: FA86866-4: MW-4 ........................................................................................................12 Section 4: Misc. Forms ............................................................................................................14 4.1: Chain of Custody ...........................................................................................................15 Section 5: MS Volatiles - QC Data Summaries .....................................................................17 5.1: Method Blank Summary ................................................................................................18 5.2: Blank Spike Summary ...................................................................................................20 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................22 123452 of 23 FA86866 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA86866 Handy Mart 15; 2495 US 13, Goldsboro, NC Project No: 5415 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA86866-1 06/29/21 12:30 TF 06/30/21 AQ Ground Water MW-1 FA86866-2 06/29/21 12:45 TF 06/30/21 AQ Ground Water MW-2 FA86866-3 06/29/21 12:59 TF 06/30/21 AQ Ground Water MW-3 FA86866-4 06/29/21 13:11 TF 06/30/21 AQ Ground Water MW-4 3 of 23 FA868661 Summary of Hits Page 1 of 1 Job Number:FA86866 Account:GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Collected:06/29/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA86866-1 MW-1 Benzene 0.91 J 2.5 0.63 ug/l SM 6200B n-Butylbenzene 5.2 2.5 0.63 ug/l SM 6200B sec-Butylbenzene 3.9 2.5 0.63 ug/l SM 6200B Ethylbenzene 104 2.5 0.63 ug/l SM 6200B Isopropylbenzene 10.9 2.5 0.63 ug/l SM 6200B p-Isopropyltoluene 1.4 J 2.5 0.63 ug/l SM 6200B Naphthalene 84.4 2.5 0.63 ug/l SM 6200B n-Propylbenzene 35.3 2.5 0.63 ug/l SM 6200B Toluene 5.4 2.5 0.63 ug/l SM 6200B 1,2,4-Trimethylbenzene 243 2.5 0.63 ug/l SM 6200B 1,3,5-Trimethylbenzene 52.3 2.5 0.63 ug/l SM 6200B m,p-Xylene 259 5.0 0.63 ug/l SM 6200B o-Xylene 185 2.5 0.63 ug/l SM 6200B Xylene (total)444 7.5 1.3 ug/l SM 6200B FA86866-2 MW-2 Benzene 929 25 6.3 ug/l SM 6200B n-Butylbenzene 16.6 J 25 6.3 ug/l SM 6200B sec-Butylbenzene 16.1 J 25 6.3 ug/l SM 6200B Ethylbenzene 568 25 6.3 ug/l SM 6200B Isopropylbenzene 72.2 25 6.3 ug/l SM 6200B Naphthalene 190 25 6.3 ug/l SM 6200B n-Propylbenzene 227 25 6.3 ug/l SM 6200B Toluene 695 25 6.3 ug/l SM 6200B 1,2,4-Trimethylbenzene 671 25 6.3 ug/l SM 6200B 1,3,5-Trimethylbenzene 141 25 6.3 ug/l SM 6200B m,p-Xylene 1480 50 6.3 ug/l SM 6200B o-Xylene 187 25 6.3 ug/l SM 6200B Xylene (total)1670 75 13 ug/l SM 6200B FA86866-3 MW-3 No hits reported in this sample. FA86866-4 MW-4 No hits reported in this sample. 4 of 23 FA868662 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 5 of 23 FA868663 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-1 Lab Sample ID:FA86866-1 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E107734.D 5 07/02/21 19:43 LR n/a n/a VE2501 Run #2 a E107820.D 5 07/08/21 20:56 LR n/a n/a VE2504 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 0.91 2.5 0.63 ug/l J 108-86-1 Bromobenzene ND 2.5 0.63 ug/l 74-97-5 Bromochloromethane ND 2.5 0.63 ug/l 75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l 75-25-2 Bromoform ND 2.5 0.63 ug/l 104-51-8 n-Butylbenzene 5.2 2.5 0.63 ug/l 135-98-8 sec-Butylbenzene 3.9 2.5 0.63 ug/l 98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l 56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l 108-90-7 Chlorobenzene ND 2.5 0.63 ug/l 75-00-3 Chloroethane ND 2.5 1.0 ug/l 67-66-3 Chloroform ND 2.5 0.63 ug/l 95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l 106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l 124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l 106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l 75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l 541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l 106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l 75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l 107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l 75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l 78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l 142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l 594-20-7 2,2-Dichloropropane b ND 2.5 0.63 ug/l 563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 23 FA8686633.1 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-1 Lab Sample ID:FA86866-1 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 2.5 0.63 ug/l 100-41-4 Ethylbenzene 104 2.5 0.63 ug/l 87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l 98-82-8 Isopropylbenzene 10.9 2.5 0.63 ug/l 99-87-6 p-Isopropyltoluene 1.4 2.5 0.63 ug/l J 74-83-9 Methyl Bromide ND 2.5 1.0 ug/l 74-87-3 Methyl Chloride ND 2.5 1.0 ug/l 74-95-3 Methylene Bromide ND 2.5 0.63 ug/l 75-09-2 Methylene Chloride ND 10 5.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.63 ug/l 91-20-3 Naphthalene 84.4 2.5 0.63 ug/l 103-65-1 n-Propylbenzene 35.3 2.5 0.63 ug/l 100-42-5 Styrene ND 2.5 0.63 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l 127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l 108-88-3 Toluene 5.4 2.5 0.63 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l 71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l 79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l 79-01-6 Trichloroethylene ND 2.5 0.63 ug/l 75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l 95-63-6 1,2,4-Trimethylbenzene 243 2.5 0.63 ug/l 108-67-8 1,3,5-Trimethylbenzene 52.3 2.5 0.63 ug/l 75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l m,p-Xylene 259 5.0 0.63 ug/l 95-47-6 o-Xylene 185 2.5 0.63 ug/l 1330-20-7 Xylene (total)444 7.5 1.3 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%104%70-130% 17060-07-0 1,2-Dichloroethane-D4 96%110%70-130% 2037-26-5 Toluene-D8 103%103%70-130% 460-00-4 4-Bromofluorobenzene 103%102%70-130% (a) Confirmation run. (b) Associated ECC outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 23 FA8686633.1 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-2 Lab Sample ID:FA86866-2 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E107735.D 50 07/02/21 20:05 LR n/a n/a VE2501 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 929 25 6.3 ug/l 108-86-1 Bromobenzene ND 25 6.3 ug/l 74-97-5 Bromochloromethane ND 25 6.3 ug/l 75-27-4 Bromodichloromethane ND 25 6.3 ug/l 75-25-2 Bromoform ND 25 6.3 ug/l 104-51-8 n-Butylbenzene 16.6 25 6.3 ug/l J 135-98-8 sec-Butylbenzene 16.1 25 6.3 ug/l J 98-06-6 tert-Butylbenzene ND 25 6.3 ug/l 56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l 108-90-7 Chlorobenzene ND 25 6.3 ug/l 75-00-3 Chloroethane ND 25 10 ug/l 67-66-3 Chloroform ND 25 6.3 ug/l 95-49-8 o-Chlorotoluene ND 25 6.3 ug/l 106-43-4 p-Chlorotoluene ND 25 6.3 ug/l 124-48-1 Dibromochloromethane ND 25 6.3 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l 106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l 75-71-8 Dichlorodifluoromethane ND 25 10 ug/l 95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l 541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l 106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l 75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l 107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l 75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l 78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l 142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l 594-20-7 2,2-Dichloropropane a ND 25 6.3 ug/l 563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 23 FA8686633.2 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-2 Lab Sample ID:FA86866-2 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l 100-41-4 Ethylbenzene 568 25 6.3 ug/l 87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l 98-82-8 Isopropylbenzene 72.2 25 6.3 ug/l 99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l 74-83-9 Methyl Bromide ND 25 10 ug/l 74-87-3 Methyl Chloride ND 25 10 ug/l 74-95-3 Methylene Bromide ND 25 6.3 ug/l 75-09-2 Methylene Chloride ND 100 50 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 25 6.3 ug/l 91-20-3 Naphthalene 190 25 6.3 ug/l 103-65-1 n-Propylbenzene 227 25 6.3 ug/l 100-42-5 Styrene ND 25 6.3 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l 127-18-4 Tetrachloroethylene ND 25 6.3 ug/l 108-88-3 Toluene 695 25 6.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l 71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l 79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l 79-01-6 Trichloroethylene ND 25 6.3 ug/l 75-69-4 Trichlorofluoromethane ND 25 10 ug/l 96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l 95-63-6 1,2,4-Trimethylbenzene 671 25 6.3 ug/l 108-67-8 1,3,5-Trimethylbenzene 141 25 6.3 ug/l 75-01-4 Vinyl Chloride ND 25 6.3 ug/l m,p-Xylene 1480 50 6.3 ug/l 95-47-6 o-Xylene 187 25 6.3 ug/l 1330-20-7 Xylene (total)1670 75 13 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 93%70-130% 17060-07-0 1,2-Dichloroethane-D4 93%70-130% 2037-26-5 Toluene-D8 106%70-130% 460-00-4 4-Bromofluorobenzene 104%70-130% (a) Associated ECC outside control limits low; no sample available for re-analysis. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 23 FA8686633.2 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-3 Lab Sample ID:FA86866-3 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E107725.D 1 07/02/21 16:25 LR n/a n/a VE2501 Run #2 a E107817.D 1 07/08/21 19:50 LR n/a n/a VE2504 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane b ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 23 FA8686633.3 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-3 Lab Sample ID:FA86866-3 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101%108%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%112%70-130% 2037-26-5 Toluene-D8 106%104%70-130% 460-00-4 4-Bromofluorobenzene 104%99%70-130% (a) Confirmation run. (b) Associated ECC outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 23 FA8686633.3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-4 Lab Sample ID:FA86866-4 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E107726.D 1 07/02/21 16:47 LR n/a n/a VE2501 Run #2 a E107818.D 1 07/08/21 20:12 LR n/a n/a VE2504 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane b ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 23 FA8686633.4 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-4 Lab Sample ID:FA86866-4 Date Sampled:06/29/21 Matrix:AQ - Ground Water Date Received:06/30/21 Method:SM 6200B Percent Solids:n/a Project:Handy Mart 15; 2495 US 13, Goldsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%108%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%112%70-130% 2037-26-5 Toluene-D8 106%104%70-130% 460-00-4 4-Bromofluorobenzene 103%99%70-130% (a) Confirmation run. (b) Associated ECC outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 23 FA8686633.4 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 14 of 23 FA868664 FA86866: Chain of Custody Page 1 of 2 15 of 23 FA8686644.1 Job Number:FA86866 Client:GEOLOGICAL RESOURCES Date / Time Received:6/30/2021 9:50:00 AM Delivery Method:FX Project:HANDY MART #15 Airbill #'s:1009 6379 0433 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (5.3); Cooler 1: (4.5); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR4; Therm CF:-0.8; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:PETERH Date:Date:6/30/2021 9:50:00 AM FA86866: Chain of Custody Page 2 of 2 16 of 23 FA8686644.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 17 of 23 FA868665 Method Blank Summary Page 1 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2501-MB E107716.D 1 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 18 of 23 FA8686655.1.1 Method Blank Summary Page 2 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2501-MB E107716.D 1 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 93%70-130% 17060-07-0 1,2-Dichloroethane-D4 94%70-130% 2037-26-5 Toluene-D8 105%70-130% 460-00-4 4-Bromofluorobenzene 106%70-130% 19 of 23 FA8686655.1.1 Blank Spike Summary Page 1 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2501-BS E107714.D 1 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.1 91 70-130 108-86-1 Bromobenzene 10 9.9 99 70-130 74-97-5 Bromochloromethane 10 9.2 92 70-130 75-27-4 Bromodichloromethane 10 9.3 93 70-130 75-25-2 Bromoform 10 9.1 91 70-130 104-51-8 n-Butylbenzene 10 9.6 96 70-130 135-98-8 sec-Butylbenzene 10 10.6 106 70-130 98-06-6 tert-Butylbenzene 10 9.9 99 70-130 56-23-5 Carbon Tetrachloride 10 9.0 90 70-130 108-90-7 Chlorobenzene 10 10.4 104 70-130 75-00-3 Chloroethane 10 13.5 135 60-140 67-66-3 Chloroform 10 9.1 91 70-130 95-49-8 o-Chlorotoluene 10 9.9 99 70-130 106-43-4 p-Chlorotoluene 10 10.1 101 70-130 124-48-1 Dibromochloromethane 10 9.0 90 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.1 91 70-130 106-93-4 1,2-Dibromoethane 10 9.7 97 70-130 75-71-8 Dichlorodifluoromethane 10 8.1 81 60-140 95-50-1 1,2-Dichlorobenzene 10 10.0 100 70-130 541-73-1 1,3-Dichlorobenzene 10 10.2 102 70-130 106-46-7 1,4-Dichlorobenzene 10 10.4 104 70-130 75-34-3 1,1-Dichloroethane 10 9.1 91 70-130 107-06-2 1,2-Dichloroethane 10 8.9 89 70-130 75-35-4 1,1-Dichloroethylene 10 8.5 85 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.3 93 70-130 156-60-5 trans-1,2-Dichloroethylene 10 8.6 86 70-130 78-87-5 1,2-Dichloropropane 10 9.2 92 70-130 142-28-9 1,3-Dichloropropane 10 9.9 99 70-130 594-20-7 2,2-Dichloropropane 10 8.9 89 70-130 563-58-6 1,1-Dichloropropene 10 9.0 90 70-130 10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130 108-20-3 Di-Isopropyl Ether 10 8.2 82 70-130 100-41-4 Ethylbenzene 10 9.7 97 70-130 87-68-3 Hexachlorobutadiene 10 10.2 102 70-130 98-82-8 Isopropylbenzene 10 10.2 102 70-130 * = Outside of Control Limits. 20 of 23 FA8686655.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2501-BS E107714.D 1 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.3 103 70-130 74-83-9 Methyl Bromide 10 8.4 84 60-140 74-87-3 Methyl Chloride 10 9.0 90 60-140 74-95-3 Methylene Bromide 10 8.9 89 70-130 75-09-2 Methylene Chloride 10 7.1 71 70-130 1634-04-4 Methyl Tert Butyl Ether 10 8.5 85 70-130 91-20-3 Naphthalene 10 9.1 91 70-130 103-65-1 n-Propylbenzene 10 10.3 103 70-130 100-42-5 Styrene 10 9.4 94 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.2 92 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130 127-18-4 Tetrachloroethylene 10 10 100 70-130 108-88-3 Toluene 10 10.1 101 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.2 92 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.1 91 70-130 71-55-6 1,1,1-Trichloroethane 10 8.9 89 70-130 79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130 79-01-6 Trichloroethylene 10 9.7 97 70-130 75-69-4 Trichlorofluoromethane 10 9.0 90 60-140 96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.9 99 70-130 75-01-4 Vinyl Chloride 10 9.7 97 60-140 m,p-Xylene 20 19.7 99 70-130 95-47-6 o-Xylene 10 9.8 98 70-130 1330-20-7 Xylene (total)30 29.4 98 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 95%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% * = Outside of Control Limits. 21 of 23 FA8686655.2.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA86866-2MS E107736.D 50 07/02/21 LR n/a n/a VE2501 FA86866-2MSD E107737.D 50 07/02/21 LR n/a n/a VE2501 FA86866-2 E107735.D 50 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 FA86866-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 929 500 1460 106 500 1400 94 4 70-130/20 108-86-1 Bromobenzene ND 500 552 110 500 502 100 9 70-130/20 74-97-5 Bromochloromethane ND 500 507 101 500 453 91 11 70-130/20 75-27-4 Bromodichloromethane ND 500 529 106 500 460 92 14 70-130/20 75-25-2 Bromoform ND 500 516 103 500 459 92 12 70-130/20 104-51-8 n-Butylbenzene 16.6 J 500 550 107 500 500 97 10 70-130/20 135-98-8 sec-Butylbenzene 16.1 J 500 606 118 500 551 107 10 70-130/20 98-06-6 tert-Butylbenzene ND 500 554 111 500 499 100 10 70-130/20 56-23-5 Carbon Tetrachloride ND 500 491 98 500 436 87 12 70-130/20 108-90-7 Chlorobenzene ND 500 572 114 500 515 103 10 70-130/20 75-00-3 Chloroethane ND 500 526 105 500 561 112 6 60-140/20 67-66-3 Chloroform ND 500 503 101 500 453 91 10 70-130/20 95-49-8 o-Chlorotoluene ND 500 575 115 500 521 104 10 70-130/20 106-43-4 p-Chlorotoluene ND 500 550 110 500 493 99 11 70-130/20 124-48-1 Dibromochloromethane ND 500 506 101 500 450 90 12 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 500 528 106 500 472 94 11 70-130/20 106-93-4 1,2-Dibromoethane ND 500 546 109 500 485 97 12 70-130/20 75-71-8 Dichlorodifluoromethane ND 500 375 75 500 399 80 6 60-140/20 95-50-1 1,2-Dichlorobenzene ND 500 545 109 500 492 98 10 70-130/20 541-73-1 1,3-Dichlorobenzene ND 500 557 111 500 504 101 10 70-130/20 106-46-7 1,4-Dichlorobenzene ND 500 559 112 500 511 102 9 70-130/20 75-34-3 1,1-Dichloroethane ND 500 502 100 500 449 90 11 70-130/20 107-06-2 1,2-Dichloroethane ND 500 494 99 500 436 87 12 70-130/20 75-35-4 1,1-Dichloroethylene ND 500 461 92 500 406 81 13 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 500 513 103 500 450 90 13 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 500 470 94 500 421 84 11 70-130/20 78-87-5 1,2-Dichloropropane ND 500 527 105 500 471 94 11 70-130/20 142-28-9 1,3-Dichloropropane ND 500 557 111 500 499 100 11 70-130/20 594-20-7 2,2-Dichloropropane ND 500 401 80 500 361 72 10 70-130/20 563-58-6 1,1-Dichloropropene ND 500 496 99 500 441 88 12 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 500 489 98 500 431 86 13 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 500 521 104 500 465 93 11 70-130/20 108-20-3 Di-Isopropyl Ether ND 500 471 94 500 419 84 12 70-130/20 100-41-4 Ethylbenzene 568 500 1110 108 500 1050 96 6 70-130/20 87-68-3 Hexachlorobutadiene ND 500 555 111 500 500 100 10 70-130/20 98-82-8 Isopropylbenzene 72.2 500 652 116 500 595 105 9 70-130/20 * = Outside of Control Limits. 22 of 23 FA8686655.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA86866 Account:GRINCC GRI (Geological Resources Inc.) Project:Handy Mart 15; 2495 US 13, Goldsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA86866-2MS E107736.D 50 07/02/21 LR n/a n/a VE2501 FA86866-2MSD E107737.D 50 07/02/21 LR n/a n/a VE2501 FA86866-2 E107735.D 50 07/02/21 LR n/a n/a VE2501 The QC reported here applies to the following samples:Method: SM 6200B FA86866-1, FA86866-2, FA86866-3, FA86866-4 FA86866-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 500 569 114 500 512 102 11 70-130/20 74-83-9 Methyl Bromide ND 500 385 77 500 423 85 9 60-140/20 74-87-3 Methyl Chloride ND 500 438 88 500 443 89 1 60-140/20 74-95-3 Methylene Bromide ND 500 503 101 500 448 90 12 70-130/20 75-09-2 Methylene Chloride ND 500 413 83 500 369 74 11 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 500 479 96 500 431 86 11 70-130/20 91-20-3 Naphthalene 190 500 739 110 500 682 98 8 70-130/20 103-65-1 n-Propylbenzene 227 500 820 119 500 761 107 7 70-130/20 100-42-5 Styrene ND 500 532 106 500 476 95 11 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 500 500 100 500 456 91 9 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 500 554 111 500 491 98 12 70-130/20 127-18-4 Tetrachloroethylene ND 500 537 107 500 487 97 10 70-130/20 108-88-3 Toluene 695 500 1240 109 500 1180 97 5 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 500 502 100 500 457 91 9 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 500 523 105 500 468 94 11 70-130/20 71-55-6 1,1,1-Trichloroethane ND 500 485 97 500 439 88 10 70-130/20 79-00-5 1,1,2-Trichloroethane ND 500 569 114 500 497 99 14 70-130/20 79-01-6 Trichloroethylene ND 500 539 108 500 487 97 10 70-130/20 75-69-4 Trichlorofluoromethane ND 500 405 81 500 434 87 7 60-140/20 96-18-4 1,2,3-Trichloropropane ND 500 562 112 500 495 99 13 70-130/20 95-63-6 1,2,4-Trimethylbenzene 671 500 1230 112 500 1190 104 3 70-130/20 108-67-8 1,3,5-Trimethylbenzene 141 500 710 114 500 656 103 8 70-130/20 75-01-4 Vinyl Chloride ND 500 455 91 500 480 96 5 60-140/20 m,p-Xylene 1480 1000 2530 105 1000 2420 94 4 70-130/20 95-47-6 o-Xylene 187 500 754 113 500 702 103 7 70-130/20 1330-20-7 Xylene (total)1670 1500 3280 107 1500 3130 97 5 70-130/20 CAS No.Surrogate Recoveries MS MSD FA86866-2 Limits 1868-53-7 Dibromofluoromethane 95%94%93%70-130% 17060-07-0 1,2-Dichloroethane-D4 95%93%93%70-130% 2037-26-5 Toluene-D8 101%102%106%70-130% 460-00-4 4-Bromofluorobenzene 104%103%104%70-130% * = Outside of Control Limits. 23 of 23 FA8686655.3.1 APPENDIX C Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-1 MW-2 Area Date Well Benzene (μ/L) Toluene (μ/L) Ethylbenzene (μ/L) Xylenes (μ/L) MTBE (μ/L) Naphthalene (μ/L) Total (μ/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red.To Date Red. MW-1 0 3.6 70.7 305 0 47.1 426.40 4.59 MW-2 637 127 176 479 12.4 69.0 1500.40 4.21 Avg.318.50 65.30 123.35 392.00 6.20 58.05 963.40 4.40 MW-1 0.77 4.3 76.3 429 0 70.6 580.97 2.10 MW-2 2,760 4,560 2,090 7,250 <13 489 17149.00 1.75 Avg.1,380.39 2,282.15 1,083.15 3,839.50 0.00 279.80 8864.99 1.93 MW-1 0.91 5.4 104 444 0.63 84.4 639.34 3.28 MW-2 929 695 568 1,670 6.3 190 4052.00 2.90 Avg.464.96 350.20 336.00 1,057.00 0.63 137.20 2345.67 3.09 Date Average Water Column Height (ft.) 10/22/20 7.60 02/04/21 10.08 06/29/21 8.91 Notes: • Area of the contaminant plume is calculated from Figure 8 • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event. • When areas couldn’t be sampled, the last known concentrations were used in the calculations. 16,167 457,811 68,672 APPENDIX C CONTAMINANT MASS CALCULATIONS HANDY MART #15 (INCIDENT NO. 38811) Baseline Event 0.1512,127.3 12 4.4 7.6 Area 4 ------ 02/04/21 10.08 807.03 -1119.8%-1119.8% 10/22/20 7.60 66.16 06/29/21 8.91 188.85 76.6%-185.4% 188.85 76.6%-185% Total Contaminant Mass (g) Percent Reduction Compared to Previous Event Percent Reduction To Date 66 ------ 807.03 -1119.8%-1120%