WA-27683_38811_CA_RPTS_20201120_LSAII

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

November 20, 2020

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Phase I High Risk Limited Site Assessment Report
Handy Mart 15
2495 US Highway 13 North
Goldsboro, Wayne County
North Carolina
Facility ID Number: 00-0-0000005485
Incident Number: 38811
GRI Project Number: 5415

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Christa Benton
Administrative Assistant

Enclosure

Cc: Mr. Scott Driscoll; E.J. Pope & Son, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Phase I High Risk Limited Site Assessment Report
Handy Mart 15
2495 US Highway 13 North
Goldsboro, Wayne County
North Carolina
Facility ID Number: 00-0-0000005485
Incident Number: 38811
GRI Project Number: 5415

Prepared for:

Scott Driscoll
E.J. Pope & Son, Inc.
1092 N. Breazeale Ave.
Mt. Olive, NC 28365

November 20, 2020

William Regenthal, P.G.
Project Manager
Alex Lin, E.I.T.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
i

EXECUTIVE SUMMARY
The Handy Mart 15 site is located at 2495 US Highway 13 North in Goldsboro, Wayne County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered
by concrete, asphalt, and grass. Two 8,000-gallon gasoline, one 4,000-gallon gasoline, and one 4,000-
gallon kerosene USTs are in use at the site. One 4,000-gallon kerosene UST was permanently closed in
1987. The surrounding properties are commercial and residential.

On January 28, 2020, a Geoenvironmental Phase II Investigation was submitted to North Carolina
Department of Environmental Quality (NCDEQ) documenting that soil samples collected in the DOT right-
of-way indicated a potential release. On June 4, 2020, a Notice of Regulatory Requirements was issued
for a site check by NCDEQ.

On June 18, 2020, eleven soil samples and ten ground water samples were collected adjacent to the tank
basins and dispenser islands during site check activities. Soil samples were analyzed on-site for TPH-GRO
and TPH-DRO using a mobile UVF laboratory. Petroleum contamination was confirmed in soil samples SB-
2-3’ and SB-3-2’. Ground water samples collected from temporary monitoring wells were analyzed on-
site for TPH-GRO and TPH-DRO using a mobile UVF laboratory. The mobile UVF laboratory reported no
contamination. To confirm results, two ground water samples (SB-2 and SB-10) were submitted for
laboratory analyses using EPA 6200B, EPA 504.1, EPA 625.1, and MADEP VPH and EPH. The laboratory
results confirmed that a release to the ground water had occurred.

During the August 13, 2020, receptor survey, seven water supply wells were identified within a 1,500-foot
radius of the site. Two potable water supply wells were identified within a 1,000-foot radius of the site.
No water supply wells were identified within a 250-foot radius of the site. Public water is available to the
subject site and to all surrounding properties. No surface water bodies were identified within a 500-foot
radius of the site.

On October 22, 2020, four Type II monitoring wells (MW-1 through MW-4) were installed at the site, and
subsequently were gauged, purged, and sampled. The depths to ground water ranged from 4.21 to 6.91
feet. Ground water flow was generally toward the north and northwest, with a horizontal gradient of 0.01
feet per foot. Concentrations of benzene, naphthalene, tert-amyl alcohol, tert-butyl alcohol, methyl
chloride, n-propylbenzene, lead, 1-methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C10
aromatics, and/or C11-C22 aromatics that exceeded the MACs were reported in the ground water samples
collected from MW-1 and MW-2. All of the reported contaminant concentrations were less than the GCLs.
No free product was observed at the site.

Based on this information, the site risk should be classified as high. While a Comprehensive Site
Assessment is warranted for this incident, an attempt should be made to connect the property where
MW-5 is located to the municipal water supply. Additional ground water sampling activities should be

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
ii

conducted in order to confirm ground water flow direction and to confirm that WSW-4 is cross-gradient
of the contaminant plume.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415

TABLE OF CONTENTS

1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................4
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................5
4. SITE INVESTIGATION .............................................................................................................6
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................8
6. LIMITATIONS ........................................................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Wayne County Property Cards
Appendix B: Well Permit, Well Construction Records, and Subsurface Logs
Appendix C: State Correspondence
Appendix D: Laboratory Report – Ground Water Samples
Appendix E: June 2020 Site Check Soil Quality Map

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? Unknown

Water supply wells were not sampled to determine contamination concentrations.

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? YES

City water is available to the relevant properties; however, WSW-5 and WSW-7 are currently used
for potable purposes.

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

No water supply wells were identified within 250 feet of the source area.

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and most surrounding properties. A water line has not been
installed along EW Lane, in the vicinity of the site.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
2

On November 11, 2020, GRI personnel accessed the NCDEQ Source Water Assessment and
Protection (SWAP) Program’s website to identify wellhead protection areas in the vicinity of the
subject site. The site is not located within a wellhead protection area.

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? YES

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? NO
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

All contaminant concentrations were below Gross Contamination Levels (GCLs).

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
3
5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility in the near future.
7. What is the zoning status of the property?
According to the City of Goldsboro Official Zoning Map, the site is zoned GB (General-Business).
8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store in the near future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 2457 US 13 Hwy North located approximately 120 feet west of
the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

The closest place of public assembly is Pathway Baptist Church 2436 US 13 Hwy North located
approximately 710 feet southwest of the UST basin.

11. What is the zoning status of properties in the surrounding area?

According to the City of Goldsboro Official Zoning Map, the surrounding areas are zoned General
Business (GB), and Residential (RM-9, R-12, and R-20A).

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
4

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, agricultural and residential properties.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on August 13, 2020. Seven water supply wells were identified
within a 1,500-foot radius of the site. Two of those water supply wells (WSW-4 and WSW-5)
within 1,000 feet are used for potable purposes. No water supply wells were identified within a
250-foot radius of the site. A Site Location Map is provided as Figure 1 and a Site Vicinity Map
showing property boundaries for the site and surrounding properties has been included as Figure
2. Water supply well information has been provided in Table 3.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by the City of Goldsboro. Please note, a water
line has not been installed along E W Lane, to the west of the site.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
No surface water bodies were identified within 1,500 feet.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On November 11, 2020, GRI personnel accessed the NCDEQ Source Water Assessment and
Protection (SWAP) Program’s website to identify wellhead protection areas in the vicinity of the
subject site. The site is not located within a wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along US-13 Highway North and several underground utility

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
5
lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
4. Property boundaries are shown on Figure 2. Property cards for the adjacent property owners
are attached as Appendix A.

3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the undivided Yorktown and
Duplin Formations of the Coastal Plain. The Yorktown Formation consists of bluish gray fossiliferous clay
with varying amounts of fine-grained sand, with shell material commonly concentrated in lenses; mainly
in the area north of Neuse River. The Duplin Formation consists of bluish gray shelly, medium- to coarse-
grained sand, sandy marl, and limestone; mainly in area south of the Neuse River. The surficial aquifer at
the site overlies the Black Creek confining unit and Black Creek aquifer, respectively.

Four Type II monitoring wells (MW-1 through MW-4) were installed at the site on October 22, 2020.
Monitoring wells MW-1, MW-2 and MW-3 were each installed to total depths of 12 feet below grade and
MW-4 was installed to a total depth of 11 feet below grade. Monitoring wells MW-1, MW-2 and MW-3
were each completed with 10-foot screened intervals, and MW-4 was completed with a 9-foot screened
interval. The screened intervals were set to bracket the water table at the time of installation. Top of
casing elevations for MW-1 through MW-4 were measured on October 22, 2020. The soil samples
collected during well installation activities were brown and gray clay and medium sand. The depths to
ground water during the October 2020 gauging event ranged from 4.21 to 6.91 feet below the tops of well
casings. A Site Map showing the locations of the wells and structures onsite is included as Figure 3. Well
construction and gauging information is presented in Table 5. Copies of the well permit, well construction
records and subsurface logs have been included as Appendix B. Photos of the monitoring wells are shown
below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
6

4. SITE INVESTIGATION
On January 28, 2020, the Department of Transportation (DOT) reported a suspected release to the North
Carolina Department of Environmental Quality (NCDEQ) based on soil samples collected in the right-of-
way during assessment activities. On June 4, 2020, a Notice of Regulatory Requirements (NORR) was
issued for a site check by the NCDEQ. A copy of the NORR has been included in Appendix C.

On June 18, 2020, eleven soil borings were advanced adjacent to the tank basins and dispenser islands.
Soil samples were analyzed on-site for gasoline-range and diesel-range total petroleum hydrocarbons
(TPH-GRO and TPH-DRO) using a mobile UVF laboratory. Based on the UVF results, petroleum
contamination was confirmed in soil samples SB-2-3’ and SB-3-2’.

As a part of the June 2020 site check activities ground water samples were collected from temporary wells
and were analyzed on-site for TPH-GRO and TPH-DRO using a mobile UVF laboratory. The mobile UVF
laboratory reported no contamination. To confirm the on-site analyses, two ground water samples (SB-2
and SB-10) were submitted for laboratory analysis of method specific constituents. The laboratory
analytical results confirmed a release to the ground water.

Based on the ground water contaminant concentrations and the presence of potable water supply wells
within a 1,000-foot radius of the source area, MW-1 through MW-4 were installed at the site on October
22, 2020.

Monitoring wells MW-1 through MW-4 were gauged on October 22, 2020. The depths to ground water
ranged from 4.21 to 6.91 feet below the tops of well casings. Ground water elevations ranged from 93.36
to 95.45 during the October 2020 ground water gauging event. Ground water flow was generally toward
the north and northwest with a horizontal gradient of 0.02 feet per foot. A Water Table Surface Map has
been included as Figure 4. Gauging data from the October 2020 gauging event has been included in Table
5. A summary of the current gauging data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
7
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1 2 - 12 12 100.00 4.59 95.41
MW-2 2 - 12 12 99.40 4.21 95.19
MW-3 2 - 12 12 100.35 4.90 95.45
MW-4 2 - 11 11 100.27 6.91 93.36

1. Ground Water Sampling:
On October 22, 2020, MW-1 through MW-4 were purged and sampled in accordance with NCDEQ
guidelines. The ground water samples were submitted for analyses of VOCs + 5 oxygenates by EPA
Method 6200B, EDB by EPA Method 504.1, total lead by EPA Method 6010, semi-VOCs by EPA 625,
and VPH and EPH by the MADEP Methods. Concentrations of benzene, naphthalene, tert-amyl
alcohol, tert-butyl alcohol, methyl chloride, n-propylbenzene, lead, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C10 aromatics, and/or C11-C22 aromatics that exceeded the
Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-1 and MW-2. All of the reported contaminant
concentrations were less than the Gross Contamination Levels (GCLs). No free product was observed
at the site. A Ground Water Quality Map has been included as Figure 5. A summary of the ground
water analytical data has been included in Table 6. A copy of the laboratory report has been included
in Appendix D. A summary of the current ground water sampling data is shown below:

Contaminant of
Concern
 Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 <0.31 3.6 70.7 305 <0.31 47.1
MW-2 637 127 176 479 12.4 69.0
MW-3 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13

2. Soil Sampling
Soil samples were not collected during the October 2020 assessment activities. The Soil Quality Map
from the June 2020 Site Check is included as Appendix E. A summary of the soil sampling data from
the June 2020 Site Check Activities is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
8 Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) 50 100
SB-1-3' 06/18/20 3 <0.5 42.9
SB-2-3' 06/18/20 3 134.7 190
SB-3-2' 06/18/20 2 <1.5 106.8
SB-4-2' 06/18/20 2 <0.6 0.1
SB-5-2' 06/18/20 2 <0.6 2
SB-6-4' 06/18/20 4 <0.6 <0.25
SB-7-2' 06/18/20 2 <0.4 4.9
SB-8-2' 06/18/20 2 <0.5 22.5
SB-9-2' 06/18/20 2 <0.5 0.9
SB-10-2' 06/18/20 2 8.2 3.6
DI-Kerosene-2' 06/18/20 2 <0.6 7.5

3. Quality Control:
The ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the
monitoring wells and new nitrile gloves were worn during soil and ground water sampling. Samples
were logged using proper chain-of-custody procedures. The samples were transported to a North
Carolina certified laboratory for analysis.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, agricultural and residential properties.
 A receptor survey was conducted on August 13, 2020. Seven water supply wells were identified
within a 1,500-foot radius of the site. Two potable water supply wells were identified within a
1,000-foot radius of the site. Public water is available to the subject site and to most surrounding
properties. Municipal water is not available to properties to the east of the site along E W Lane.
 No surface water bodies were identified within a 500-foot radius of the site.
 Monitoring wells MW-1 through MW-4 were gauged on October 22, 2020. The depths to ground
water ranged from 4.21 to 6.91 feet. Ground water flow was generally toward the north and
northwest with a horizontal gradient of 0.02 feet per foot.
 On October 22, 2020, MW-1 through MW-4 were purged, and sampled. Concentrations of
benzene, naphthalene, tert-amyl alcohol, tert-butyl alcohol, methyl chloride, n-propylbenzene,
lead, 1-methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C10 aromatics, and/or

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: November 20, 2020 Handy Mart 15
Project Manager: William Regenthal, P.G. GRI Project No. 5415
9
C11-C22 aromatics that exceeded the MACs were reported in the ground water samples collected
from MW-1 and MW-2. All of the reported contaminant concentrations were less than the GCLs.
No free product was observed at the site.
 Based on the presence of potable water supply wells within 1,000 feet of the site, the site risk
should be classified as high. While a Comprehensive Site Assessment is warranted for this
incident, an attempt should be made to connect the property where MW-5 is located to the
municipal water supply. Additional ground water sampling activities should be conducted in order
to confirm ground water flow direction and to confirm that WSW-4 is cross-gradient of the
contaminant plume.

6. LIMITATIONS
This report has been prepared for the exclusive use of E. J. Pope & Son, Inc. for specific application to the
referenced site in Wayne County, North Carolina. The assessment was conducted based on the scope of
work and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site LocationHandy Mart 152495 US Highway 13 Goldsboro, Wayne County, NCIncident No. 38811GRI Project No. 5415500 M2000 FTDate: 07/09/2020Location: 35.404222° N -77.898599° W Dad
"J
"J
"J
!H
!H
!H
!H
SITE
3620920776
3620834499362074304536208318773620834930362074337336207398873620842496
3620831715
3620842187
362083868636207421513620842032
3620749004
WSW-6
WSW-3
WSW-2
WSW-1
WSW-7
WSW-5
WSW-4
Ut
U
t
Ut
E W LN
N US 13 HWYH O O D SW A M P RDTWIN DR
DURWOOD DR
DARYL DR
CENTRAL HEIGHTS RDMOORING LN
FIGURE 2: SITE VICINITY MAPHANDY MART #152495 US HIGHWAY 13 NORTHGOLDSBORO, WAYNE COUNTYNORTH CAROLINAINCIDENT NO. 38811GRI PROJECT NO. 5415
PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 11, 2020
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS 250-FOOT RADIUS
500-FOOT RADIUS
LEGEND
!H Water Supply Well (Non-Potable)
"J Water Supply Well (Potable)
Wayne_County_Centerlines
All_Ditches_Streams_Rivers
Adjacent Properties and Well Owners
Wayne_County_Parcels

TABLES
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 5 Facility ID Number
Owner or Operator?
Owner/Operator
00-0-0000005485
TABLE 1
UST OWNER/OPERATOR INFORMATION
HANDY MART 15 (INCIDENT NO. 38811)
PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566
Name of Owner or Operator Dates of Ownership / Operation
E. J. Pope & Son, Inc.04/01/1982 - Current
Address Telephone Number
00-0-0000005484
Name of Owner or Operator Dates of Ownership / Operation
E. J. Pope & Son, Inc.03/31/1986 - 03/01/1987
Address Telephone Number
PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566
00-0-0000005484
PO Box 649 Mount Olive, North Caorlina 28365 919-658-6566
Name of Owner or Operator Dates of Ownership / Operation
E. J. Pope & Son, Inc.03/31/1987 - Current
Address Telephone Number
Page 1 of 1
Date: 07/06/20
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 8,000 4/1/1982 Single Wall Steel 8' x 21' 4"Single Wall FRP Current Yes
2 Gasoline 8,000 4/1/1982 Single Wall Steel 8' x 21' 4"Single Wall FRP Current Yes
3 Gasoline 4,000 4/1/1982 Single Wall Steel 64" x 24'Single Wall FRP Current Yes
4 Kerosene 4,000 3/31/1986 Single Wall Steel 64" x 24'Single Wall FRP Removed No
5 Kerosene 4,000 3/31/1987 Single Wall Steel 64" x 24'Single Wall FRP Current Yes
TABLE 2
UST SYSTEM INFORMATION
HANDY MART 15 (INCIDENT NO. 38811)
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 00-0-0000005485
Page 1 of 1
Date: 11/11/20 Facility ID # : 00-0-0000005485
Well ID Parcel ID No.Well Owner Mailing Address Well Location Address
Well Use
(Potable/
Agriculture, etc.)
Public Water
Connected
Distance from
source area of
release
(ft.)
WSW-1 3620743373 Knox Charles Atlas & Wife 102 Daryl Drive
Goldsboro, NC 27534
102 Daryl Drive
Goldsboro, NC 27534 Not in Use Yes ~920 NW
WSW-2 3620743045 Smith Craig 3009 US Highway 13 N
Goldsboro, NC 27530
101 Daryl Drive
Goldsboro, NC 27534 Not in Use Yes ~850 W
WSW-3 3620742151 Bledsoe Richard 103 Daryl Drive
Goldsboro, NC 27534
103 Daryl Drive
Goldsboro, NC 27534 Not in Use Yes ~970 W
WSW-4 3620838686 Gurley Emily C.142 EW Lane
Goldsboro, NC 27534
142 EW Lane
Goldsboro, NC 27534 Potable No ~720 E
WSW-5 3620842496 Ambriz Filiberto 109 Shady Meadow Lane
Clayton, NC 27520
2545 N. US 13 Highway
Goldsboro, NC 27534 Potable No, available ~600 N
WSW-6 3620842187 Peele Marie P.2521 US 13 North
Goldsboro, NC 27534
2521 US 13 North
Goldsboro, NC 27534 Not in Use Yes ~280 N
WSW-7 3620920776 Smith Earl W Heirs 126 EW Lane
Goldsboro, NC 27534
180 EW Lane
Goldsboro, NC 27534 Potable No ~1,110 SE
Notes:
• Water supply wells are shown on Figure 2
• Ft. BGS : Feet below ground surface
TABLE 3
WATER SUPPLY WELL INFORMATION
HANDY MART 15 (INCIDENT NO. 38811)
Page 1 of 1
Date: 11/11/20 Facility ID # : 00-0-0000005485
PIN Number Property Owner Name Owner Mailing Address
3620831877 (site)Peele, Marie P.2521 US 13 North
Goldsboro, NC 27534
3620831715 Boyette, Kenneth Ray Jr.2457 US 13 Hwy North
Goldsboro, NC 27534
3620739887 Fields, Stanley P.105 Durwood Drive
Goldsboro, NC 27534
3620842032 Peele, Durwood Lee and Heirs 112 Durwood Drive
Goldsboro, NC 27534
3620834930 JCTB LLC 126 EW Lane
Goldsboro, NC 27534
3620834499 Smith, Carolyn S.126 E W Lane
Goldsboro, NC 27534
3620749004 Peele, Marie P.2521 US 13 North
Goldsboro, NC 27534
Note:
• Properties are keyed to Figure 2.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
HANDY MART 15 (INCIDENT NO. 38811)
Page 1 of 1
Date: 11/11/20
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
MW-1 10/22/20 10/22/20 2 2 - 12 12 100.00 4.59 ---95.41
MW-2 10/22/20 10/22/20 2 2 - 12 12 99.40 4.21 ---95.19
MW-3 10/22/20 10/22/20 2 2 - 12 12 100.35 4.90 ---95.45
MW-4 10/22/20 10/22/20 2 2 - 11 11 100.27 6.91 ---93.36
Notes:
• Elevation relative to mean sea level.
• ft BGS : feet below ground surface.
• NM : Not measured.
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY MART 15 (INCIDENT NO. 38811)
Facility ID # : 00-0-0000005485
Page 1 of 1
Date: 11/11/20 Facility ID # : 00-0-0000005485
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 40 10 3 70 0.02 15 1 30 400 700 200 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 40,000 10,000 3,000 30,000 50 15,000 1,000 12,500 NE NE NE NE NE NE
MW-1 10/22/20 <0.31 3.6 70.7 305 <0.31 47.1 12.0 J <5.0 <0.50 21.4 <0.0037 <5.0 7.3 13.0 513 <35 1,060 <49 <49 278
MW-2 10/22/20 637 127 176 479 12.4 69.0 146 J 134 J 4.6 J 174 <0.0037 6.8 32.6 44.2 1,130 <35 2,920 <99 <99 259 J
MW-3 10/22/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.0037 22.9 <0.54 <0.61 <35 <35 <35 <51 <51 98.7 J
MW-4 10/22/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.20 <0.13 <0.0038 1,130 <0.50 <0.57 <35 <35 <35 <51 <51 <82
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• J: Estimated value.
• NE: Not established.
• NR: Not requested.
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
• NR: Not requested.
Analytical Method

TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY MART 15 (INCIDENT NO. 38811)
MAC (μg/l)
EPA 625.1 MADEP VPH MADEP EPH
C11-C22 AromaticsC9-C12 AliphaticsNaphthaleneMTBEC19-C36 AliphaticsC5-C8 Aliphatics2-MethylnaphthaleneLeadC9-C18 AliphaticsC9-C10 AromaticsGCL (μg/l)
Contaminant of Concern
XylenesEthylbenzeneTolueneBenzene1,2-Dibromoethane(EDB)1-MethylnaphthaleneEPA 6200B
tert-Amyl alcohol(TAA)tert-Butyl alcohol(TBA)Methyl chloride(Chloromethane)n-PropylbenzenePage 1 of 1

APPENDICES

APPENDIX A
Wayne County Property Cards
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OBJECTID
58819
PIN
3620831877
Owner Name
PEELE MARIE P
Co-Owner Name

Owner Address 1
2521 US 13 NORTH
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7319
Unit or Apt

Deed Date
1/1/1901 12:00:00 AM
REID
0024971
Deed Book
0084E
Deed Page
616
Sale Month
1
Sale Year
1901
Sale Price
0
Previous Deed Book
0084E
Previous Deed Page
0616
Previous Sale Month
1
Previous Sales Year
1901
Previous Sale Price
0
Property Use
10 - COMMERCIAL
Record Source
Owner
Property Address
2495 N US 13 HWY
Legal Description
2495 N US 13 HY
Acres
0.61
Neighborhood
05906
Account Number
51393700
Township Code
05
Building Value
70370
Outbuilding Value
10350
Land Value
54900
Total Market Value
135620
Total Assessed Value
135620
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
14085
PIN
3620831715
Owner Name
BOYETTE KENNETH RAY JR
Co-Owner Name

Owner Address 1
2457 US 13 HWY NORTH
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7317
Unit or Apt

Deed Date
12/1/2002 12:00:00 AM
REID
0024970
Deed Book
2018
Deed Page
834
Sale Month
12
Sale Year
2002
Sale Price
37500
Previous Deed Book
01081
Previous Deed Page
0125
Previous Sale Month
1
Previous Sales Year
1984
Previous Sale Price
6000
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
2487 N US 13 HWY
Legal Description
2487 N US 13 HY
Acres
0.61
Neighborhood
05906
Account Number
244610
Township Code
05
Building Value
0
Outbuilding Value
4360
Land Value
16200
Total Market Value
20560
Total Assessed Value
20560
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
10504
PIN
3620739887
Owner Name
FIELDS STANLEY P
Co-Owner Name

Owner Address 1
105 DURWOOD DR
Owner Address 2

Owner Address 3

Owner City
GOLDBSORO
Owner State
NC
Owner Zip
27534-9121
Unit or Apt

Deed Date
1/1/2003 12:00:00 AM
REID
0024915
Deed Book
2021
Deed Page
749
Sale Month
1
Sale Year
2003
Sale Price
74500
Previous Deed Book
01753
Previous Deed Page
0821
Previous Sale Month
12
Previous Sales Year
1999
Previous Sale Price
0
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
105 DURWOOD DR
Legal Description
N US 13 HY REAR
Acres
0.54
Neighborhood
05906
Account Number
504680
Township Code
05
Building Value
54270
Outbuilding Value
5930
Land Value
6910
Total Market Value
67110
Total Assessed Value
67110
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
52357
PIN
3620842032
Owner Name
PEELE DURWOOD LEE & HEIRS
Co-Owner Name

Owner Address 1
%LINDA STEVENS
Owner Address 2
112 DURWOOD DR
Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-9191
Unit or Apt

Deed Date
1/1/1974 12:00:00 AM
REID
0024977
Deed Book
860
Deed Page
886
Sale Month
1
Sale Year
1974
Sale Price
0
Previous Deed Book
00860
Previous Deed Page
0086
Previous Sale Month
1
Previous Sales Year
1901
Previous Sale Price
0
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
112 DURWOOD DR
Legal Description
112 DURWOOD DR
Acres
0.44
Neighborhood
05906
Account Number
51337120
Township Code
05
Building Value
22620
Outbuilding Value
7430
Land Value
12600
Total Market Value
42650
Total Assessed Value
42650
Vacant Or Improved
I
Vacant or Improved 2
V
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
30456
PIN
3620834930
Owner Name
JCTB LLC
Co-Owner Name

Owner Address 1
126 EW LN
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7944
Unit or Apt

Deed Date
7/6/2015 12:00:00 AM
REID
0024973
Deed Book
3166
Deed Page
502
Sale Month
7
Sale Year
2015
Sale Price
0
Previous Deed Book
01765
Previous Deed Page
0167
Previous Sale Month
3
Previous Sales Year
2000
Previous Sale Price
65000
Property Use
49 - STEEL FRAME WAREHOUSE
Record Source
Owner
Property Address
2502 N US 13 HWY
Legal Description
2502 N US 13 HY
Acres
1
Neighborhood
05906
Account Number
75342692
Township Code
05
Building Value
131740
Outbuilding Value
6590
Land Value
90000
Total Market Value
228330
Total Assessed Value
228330
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
1722
PIN
3620834499
Owner Name
SMITH CAROLYN S
Co-Owner Name

Owner Address 1
126 E W LANE
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7944
Unit or Apt

Deed Date
1/1/1983 12:00:00 AM
REID
0024972
Deed Book
1059
Deed Page
671
Sale Month
1
Sale Year
1983
Sale Price
0
Previous Deed Book
01059
Previous Deed Page
0671
Previous Sale Month
1
Previous Sales Year
1983
Previous Sale Price
0
Property Use
50 - RURAL SINGLE FAMILY
RESIDENCE
Record Source
Owner
Property Address
126 E W LN
Legal Description
126 E W LN
Acres
14.11
Neighborhood
05906
Account Number
59627820
Township Code
05
Building Value
74390
Outbuilding Value
42700
Land Value
95870
Total Market Value
212960
Total Assessed Value
150820
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats andother public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data containedin this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By acceptingthis disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
43451
PIN
3620749004
Owner Name
PEELE MARIE P
Co-Owner Name

Owner Address 1
2521 US 13 NORTH
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7319
Unit or Apt

Deed Date
1/1/1901 12:00:00 AM
REID
0024939
Deed Book
0084E
Deed Page
616
Sale Month
1
Sale Year
1901
Sale Price
0
Previous Deed Book
0084E
Previous Deed Page
0616
Previous Sale Month
1
Previous Sales Year
1901
Previous Sale Price
0
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
N US 13 HWY
Legal Description
N US 13 HY REAR
Acres
2.08
Neighborhood
05906
Account Number
51393700
Township Code
05
Building Value
0
Outbuilding Value
0
Land Value
29330
Total Market Value
29330
Total Assessed Value
29330
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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OBJECTID
53211
PIN
3620743373
Owner Name
KNOX CHARLES ATLAS & WIFE
Co-Owner Name

Owner Address 1
102 DARYL DR
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-9190
Unit or Apt

Deed Date
2/1/1987 12:00:00 AM
REID
0024927
Deed Book
1156
Deed Page
115
Sale Month
2
Sale Year
1987
Sale Price
10500
Previous Deed Book
01138
Previous Deed Page
0817
Previous Sale Month
1
Previous Sales Year
1986
Previous Sale Price
4500
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
102 DARYL DR
Legal Description
102 DARYL DR
Acres
0.61
Neighborhood
05018
Account Number
38846190
Township Code
05
Building Value
16530
Outbuilding Value
3880
Land Value
15000
Total Market Value
35410
Total Assessed Value
35410
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
66931
PIN
3620743045
Owner Name
SMITH CRAIG
Co-Owner Name

Owner Address 1
3009 US HIGHWAY 13 N
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27530-8984
Unit or Apt

Deed Date
5/1/2006 12:00:00 AM
REID
0024926
Deed Book
2428
Deed Page
229
Sale Month
5
Sale Year
2006
Sale Price
15000
Previous Deed Book
01712
Previous Deed Page
0003
Previous Sale Month
4
Previous Sales Year
1999
Previous Sale Price
0
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
101 DARYL DR
Legal Description
101 DARYL DR
Acres
0.77
Neighborhood
05018
Account Number
599120
Township Code
05
Building Value
0
Outbuilding Value
2160
Land Value
15000
Total Market Value
17160
Total Assessed Value
17160
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
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OBJECTID
56075
PIN
3620742151
Owner Name
BLEDSOE RICHARD
Co-Owner Name
BLEDSOE BONNIE WIFE
Owner Address 1
103 DARYL DR
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-9190
Unit or Apt

Deed Date
11/22/2017 12:00:00 AM
REID
0024923
Deed Book
3339
Deed Page
48
Sale Month
11
Sale Year
2017
Sale Price
15000
Previous Deed Book
01177
Previous Deed Page
0565
Previous Sale Month
9
Previous Sales Year
1987
Previous Sale Price
0
Property Use
02 - MOBILE HOME
Record Source
Owner
Property Address
103 DARYL DR
Legal Description
103 DARYL DR
Acres
1
Neighborhood
05018
Account Number
747410
Township Code
05
Building Value
0
Outbuilding Value
2820
Land Value
15000
Total Market Value
17820
Total Assessed Value
17820
Vacant Or Improved
V
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats and
other public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data contained
in this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By accepting
this disclaimer you agree and understand the disclaimer.
11/12/2020 ConnectGIS Feature Report
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Wayne
Printed November 12, 2020
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OBJECTID
64085
PIN
3620838686
Owner Name
GURLEY EMILY C
Co-Owner Name
GURLEY MICHAEL R HUSBAND
Owner Address 1
142 EW LN
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7944
Unit or Apt

Deed Date
5/17/2018 12:00:00 AM
REID
0024974
Deed Book
3372
Deed Page
300
Sale Month
5
Sale Year
2018
Sale Price
145000
Previous Deed Book
00957
Previous Deed Page
0461
Previous Sale Month
1
Previous Sales Year
1979
Previous Sale Price
0
Property Use
50 - RURAL SINGLE FAMILY
RESIDENCE
Record Source
Owner
Property Address
142 E W LN
Legal Description
142 E W LN
Acres
0.49
Neighborhood
05906
Account Number
748769
Township Code
05
Building Value
104630
Outbuilding Value
0
Land Value
12800
Total Market Value
117430
Total Assessed Value
117430
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats andother public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data containedin this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By acceptingthis disclaimer you agree and understand the disclaimer.
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Printed November 12, 2020
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OBJECTID
60957
PIN
3620842496
Owner Name
AMBRIZ FILIBERTO
Co-Owner Name
AMBRIZ ANGELA WIFE
Owner Address 1
109 SHADY MEADOW LN
Owner Address 2

Owner Address 3

Owner City
CLAYTON
Owner State
NC
Owner Zip
27520-6449
Unit or Apt

Deed Date
12/1/2004 12:00:00 AM
REID
0024981
Deed Book
2267
Deed Page
810
Sale Month
12
Sale Year
2004
Sale Price
0
Previous Deed Book
01621
Previous Deed Page
0167
Previous Sale Month
9
Previous Sales Year
1997
Previous Sale Price
57000
Property Use
50 - RURAL SINGLE FAMILY
RESIDENCE
Record Source
Owner
Property Address
2545 N US 13 HWY
Legal Description
2545 N US 13 HY DB 1141-714
Acres
0.59
Neighborhood
05906
Account Number
558060
Township Code
05
Building Value
59220
Outbuilding Value
1540
Land Value
14400
Total Market Value
75160
Total Assessed Value
75160
Vacant Or Improved
I
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats andother public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data containedin this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By acceptingthis disclaimer you agree and understand the disclaimer.
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Wayne
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OBJECTID
29084
PIN
3620842187
Owner Name
PEELE MARIE P
Co-Owner Name

Owner Address 1
2521 US 13 NORTH
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7319
Unit or Apt

Deed Date
1/1/1901 12:00:00 AM
REID
0024979
Deed Book
084 E
Deed Page
616
Sale Month
1
Sale Year
1901
Sale Price
0
Previous Deed Book
0084E
Previous Deed Page
0616
Previous Sale Month
1
Previous Sales Year
1901
Previous Sale Price
0
Property Use
50 - RURAL SINGLE FAMILY
RESIDENCE
Record Source
Owner
Property Address
2521 N US 13 HWY
Legal Description
2521 N US 13 HY
Acres
1
Neighborhood
05906
Account Number
51393700
Township Code
05
Building Value
60180
Outbuilding Value
0
Land Value
16200
Total Market Value
76380
Total Assessed Value
76380
Vacant Or Improved
V
Vacant or Improved 2
I
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats andother public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data containedin this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By acceptingthis disclaimer you agree and understand the disclaimer.
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Printed November 12, 2020
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OBJECTID
6503
PIN
3620920776
Owner Name
SMITH EARL W HEIRS
Co-Owner Name

Owner Address 1
126 E W LANE
Owner Address 2

Owner Address 3

Owner City
GOLDSBORO
Owner State
NC
Owner Zip
27534-7944
Unit or Apt

Deed Date
1/1/1968 12:00:00 AM
REID
0025020
Deed Book
726
Deed Page
419
Sale Month
1
Sale Year
1968
Sale Price
0
Previous Deed Book
00726
Previous Deed Page
0019
Previous Sale Month
1
Previous Sales Year
1901
Previous Sale Price
0
Property Use
50 - RURAL SINGLE FAMILY
RESIDENCE
Record Source
Owner
Property Address
180 E W LN
Legal Description
180 E W LN REAR
Acres
21.87
Neighborhood
05906
Account Number
59818500
Township Code
05
Building Value
33450
Outbuilding Value
1830
Land Value
115000
Total Market Value
150280
Total Assessed Value
74310
Vacant Or Improved
I
Vacant or Improved 2
V
Users of the GIS information/data contained in this web mapping application are hereby notified that the information was compiled from recorded deeds, plats andother public records and data. Users are notified that the aforementioned public primary information sources should be consulted for verification of the data containedin this information. The County of Wayne and the mapping companies or other entities assume no legal responsibility for the information contained herein. By acceptingthis disclaimer you agree and understand the disclaimer.

APPENDIX B
Well Permit, Well Construction Records and Subsurface Logs

Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Handy Mart 15
Address 2495 US Highway 13, Goldsboro, Wayne County, NC
Boring Number MW-1 Date Drilled
Sample Method NA Drilling Method 6" SFA
Completion DetailsWell completed to a total depth of 12 feet with a 10 foot screened interval
Driller Justin Radford (GRI)Log By Ethan Rogerson (GRI)
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
34

36
10/22/20
0' - 0.5' Concrete
0.5' - 3' Dark Gray Clay w/ med. Sand
3' - 12' Brown and gray clay
Total Depth = 12 feet
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Handy Mart 15
Address 2495 US Highway 13, Goldsboro, Wayne County, NC
Boring Number MW-2 Date Drilled
Sample Method NA Drilling Method 6" SFA
Completion DetailsWell completed to a total depth of 12 feet with a 10 foot screened interval
Driller Justin Radford (GRI)Log By Ethan Rogerson (GRI)
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
34

36
3' - 12' Brown and gray clay
10/22/20
0' - 0.5' Asphalt
0.5' - 3' Dark Gray Clay w/ med. Sand
Total Depth = 12 feet
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Handy Mart 15
Address 2495 US Highway 13, Goldsboro, Wayne County, NC
Boring Number MW-3 Date Drilled
Sample Method NA Drilling Method 6" SFA
Completion DetailsWell completed to a total depth of 12 feet with a 10 foot screened interval
Driller Justin Radford (GRI)Log By Ethan Rogerson (GRI)
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
34

36
0.5' - 12' Brown and Gray Clay w/med. sand
10/22/20
0' - 0.5' Grass/Topsoil
Total Depth = 12 feet
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Handy Mart 15
Address 2495 US Highway 13, Goldsboro, Wayne County, NC
Boring Number MW-4 Date Drilled
Sample Method NA Drilling Method 6" SFA
Completion DetailsWell completed to a total depth of 11 feet with a 9 foot screened interval
Driller Justin Radford (GRI)Log By Ethan Rogerson (GRI)
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
34

36
0.5' - 11' Brown and Gray Clay w/med. sand
10/22/20
0' - 0.5' Grass/Topsoil
Total Depth = 11 feet

APPENDIX C
State Correspondence

APPENDIX D
Laboratory Reports

11/11/20
Technical Report for
GRI (Geological Resources Inc.)
Handy Mart 15; 2495 US 13, Goldsboro, NC
SGS Job Number: FA80098
Sampling Date: 10/22/20
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 11/11/20
e-Hardcopy 2.0
Automated Report
101
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 101
FA80098
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA80098-1: MW-1 ........................................................................................................8
3.2: FA80098-2: MW-2 ........................................................................................................18
3.3: FA80098-3: MW-3 ........................................................................................................28
3.4: FA80098-4: MW-4 ........................................................................................................38
Section 4: Misc. Forms ............................................................................................................48
4.1: Chain of Custody ...........................................................................................................49
Section 5: MS Volatiles - QC Data Summaries .....................................................................52
5.1: Method Blank Summary ................................................................................................53
5.2: Blank Spike Summary ...................................................................................................59
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................65
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................71
6.1: Method Blank Summary ................................................................................................72
6.2: Blank Spike Summary ...................................................................................................74
Section 7: GC Volatiles - QC Data Summaries .....................................................................76
7.1: Method Blank Summary ................................................................................................77
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................78
7.3: Matrix Spike Summary ..................................................................................................79
7.4: Duplicate Summary .......................................................................................................80
Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................81
8.1: Method Blank Summary ................................................................................................82
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................84
8.3: Duplicate Summary .......................................................................................................86
Section 9: Metals Analysis - QC Data Summaries ................................................................87
9.1: Prep QC MP38048: Pb ..................................................................................................88
Section 10: Misc. Forms (SGS Scott, LA) ..............................................................................95
10.1: Chain of Custody .........................................................................................................96
Section 11: GC Volatiles - QC Data (SGS Scott, LA) ...........................................................99
11.1: Method Blank Summary ..............................................................................................100
11.2: Blank Spike/Blank Spike Duplicate Summary ............................................................101 12345678910112 of 101
FA80098
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA80098
Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA80098-1 10/22/20 14:00 ER 10/23/20 AQ Ground Water MW-1
FA80098-2 10/22/20 14:05 ER 10/23/20 AQ Ground Water MW-2
FA80098-3 10/22/20 14:09 ER 10/23/20 AQ Ground Water MW-3
FA80098-4 10/22/20 13:55 ER 10/23/20 AQ Ground Water MW-4
3 of 101
FA800981
Summary of Hits Page 1 of 3
Job Number:FA80098
Account:GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Collected:10/22/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA80098-1 MW-1
n-Butylbenzene 3.4 1.3 0.31 ug/l SM 6200B
sec-Butylbenzene 2.1 1.3 0.31 ug/l SM 6200B
Chloroform 0.92 J 1.3 0.31 ug/l SM 6200B
Ethylbenzene 70.7 1.3 0.31 ug/l SM 6200B
Isopropylbenzene 6.3 1.3 0.31 ug/l SM 6200B
p-Isopropyltoluene 0.95 J 1.3 0.31 ug/l SM 6200B
Methylene Chloride 4.4 J 5.0 2.5 ug/l SM 6200B
Naphthalene 47.1 1.3 0.31 ug/l SM 6200B
n-Propylbenzene 21.4 1.3 0.31 ug/l SM 6200B
Tert-Amyl Alcohol 12.0 J 25 5.0 ug/l SM 6200B
Toluene 3.6 1.3 0.31 ug/l SM 6200B
1,2,4-Trimethylbenzene 151 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 37.2 1.3 0.31 ug/l SM 6200B
m,p-Xylene 186 2.5 0.31 ug/l SM 6200B
o-Xylene 111 1.3 0.31 ug/l SM 6200B
Xylene (total)305 7.5 1.3 ug/l SM 6200B
1-Methylnaphthalene 7.3 4.8 0.50 ug/l EPA 625.1
2-Methylnaphthalene 13.0 4.8 0.57 ug/l EPA 625.1
Naphthalene 23.7 4.8 0.48 ug/l EPA 625.1
Total TIC, Semi-Volatile 478 J ug/l
Benzene 1.9 1.0 1.0 ug/l MADEP VPH REV 2.1
Ethylbenzene 69.7 2.0 1.0 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether 2.5 2.0 1.0 ug/l MADEP VPH REV 2.1
Naphthalene 40.1 5.0 3.0 ug/l MADEP VPH REV 2.1
Toluene 4.8 2.0 1.0 ug/l MADEP VPH REV 2.1
m,p-Xylene 172 4.0 2.0 ug/l MADEP VPH REV 2.1
o-Xylene 97.8 2.0 1.0 ug/l MADEP VPH REV 2.1
Xylenes (total)270 6.0 3.0 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)522 100 35 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)1060 500 180 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics 513 100 35 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics 1060 500 180 ug/l MADEP VPH REV 2.1
2-Methylnaphthalene a 25.2 3.9 1.9 ug/l MADEP EPH REV 2.1
Naphthalene a 51.5 3.9 1.9 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.) a 355 190 78 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics a 278 190 78 ug/l MADEP EPH REV 2.1
FA80098-2 MW-2
Benzene 637 10 2.5 ug/l SM 6200B
n-Butylbenzene 13.2 10 2.5 ug/l SM 6200B
sec-Butylbenzene 11.3 10 2.5 ug/l SM 6200B
Di-Isopropyl Ether 3.0 J 10 2.5 ug/l SM 6200B
4 of 101
FA800982
Summary of Hits Page 2 of 3
Job Number:FA80098
Account:GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Collected:10/22/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Ethylbenzene 176 10 2.5 ug/l SM 6200B
Isopropylbenzene 56.4 10 2.5 ug/l SM 6200B
Methyl Chloride 4.6 J 10 4.0 ug/l SM 6200B
Methyl Tert Butyl Ether 12.4 10 2.5 ug/l SM 6200B
Naphthalene 69.0 10 2.5 ug/l SM 6200B
n-Propylbenzene 174 10 2.5 ug/l SM 6200B
Tert-Amyl Alcohol 146 J 200 40 ug/l SM 6200B
Tert-Butyl Alcohol 134 J 200 40 ug/l SM 6200B
Toluene 127 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 241 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 52.5 10 2.5 ug/l SM 6200B
m,p-Xylene 415 20 2.5 ug/l SM 6200B
o-Xylene 64.6 10 2.5 ug/l SM 6200B
Xylene (total)479 30 5.0 ug/l SM 6200B
2,4-Dimethylphenol 2.4 J 5.1 0.75 ug/l EPA 625.1
2-Methylphenol 0.61 J 5.1 0.57 ug/l EPA 625.1
Phenol 2.1 J 5.1 0.51 ug/l EPA 625.1
1-Methylnaphthalene 32.6 5.1 0.54 ug/l EPA 625.1
2-Methylnaphthalene 44.2 5.1 0.61 ug/l EPA 625.1
Naphthalene 40.8 5.1 0.51 ug/l EPA 625.1
Total TIC, Semi-Volatile 936 J ug/l
Benzene 624 10 10 ug/l MADEP VPH REV 2.1
Ethylbenzene 160 2.0 1.0 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether 10.3 2.0 1.0 ug/l MADEP VPH REV 2.1
Naphthalene 64.6 5.0 3.0 ug/l MADEP VPH REV 2.1
Toluene 114 2.0 1.0 ug/l MADEP VPH REV 2.1
m,p-Xylene 360 4.0 2.0 ug/l MADEP VPH REV 2.1
o-Xylene 67.4 2.0 1.0 ug/l MADEP VPH REV 2.1
Xylenes (total)427 6.0 3.0 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)1890 1000 350 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)2920 1000 350 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics 1130 1000 350 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics 2920 1000 350 ug/l MADEP VPH REV 2.1
2-Methylnaphthalene a 52.3 7.9 4.0 ug/l MADEP EPH REV 2.1
Naphthalene a 57.7 7.9 4.0 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.) a 369 J 400 160 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics a 259 J 400 160 ug/l MADEP EPH REV 2.1
Lead 6.8 5.0 ug/l SW846 6010D
FA80098-3 MW-3
Chloroform 0.21 J 0.50 0.13 ug/l SM 6200B
Total TIC, Semi-Volatile 5.3 J ug/l
C11-C22 Aromatics (Unadj.) a 98.7 J 200 82 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics a 98.7 J 200 82 ug/l MADEP EPH REV 2.1
5 of 101
FA800982
Summary of Hits Page 3 of 3
Job Number:FA80098
Account:GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Collected:10/22/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Lead 22.9 5.0 ug/l SW846 6010D
FA80098-4 MW-4
Lead 1130 5.0 ug/l SW846 6010D
(a) Associated MB surrogate recovery outside control limits. Insufficient sample for reextraction.
6 of 101
FA800982
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 101
FA800983
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E104598.D 2.5 10/26/20 18:07 CV n/a n/a VE2367
Run #2 E104655.D 5 10/28/20 13:07 LR n/a n/a VE2369
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.3 0.31 ug/l
108-86-1 Bromobenzene ND 1.3 0.31 ug/l
74-97-5 Bromochloromethane ND 1.3 0.31 ug/l
75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l
75-25-2 Bromoform ND 1.3 0.31 ug/l
104-51-8 n-Butylbenzene 3.4 1.3 0.31 ug/l
135-98-8 sec-Butylbenzene 2.1 1.3 0.31 ug/l
98-06-6 tert-Butylbenzene ND 1.3 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l
108-90-7 Chlorobenzene ND 1.3 0.31 ug/l
75-00-3 Chloroethane ND 1.3 0.50 ug/l
67-66-3 Chloroform 0.92 1.3 0.31 ug/l J
95-49-8 o-Chlorotoluene ND 1.3 0.31 ug/l
106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l
106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l
75-71-8 Dichlorodifluoromethane ND 1.3 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l
107-06-2 1,2-Dichloroethane ND 1.3 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l
78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l
142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l
563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether a ND 1.3 0.31 ug/l
100-41-4 Ethylbenzene 70.7 1.3 0.31 ug/l
637-92-3 Ethyl Tert Butyl Ether a ND 1.3 0.31 ug/l
87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l
98-82-8 Isopropylbenzene 6.3 1.3 0.31 ug/l
99-87-6 p-Isopropyltoluene 0.95 1.3 0.31 ug/l J
74-83-9 Methyl Bromide ND 1.3 0.50 ug/l
74-87-3 Methyl Chloride ND 1.3 0.50 ug/l
74-95-3 Methylene Bromide ND 1.3 0.31 ug/l
75-09-2 Methylene Chloride 4.4 5.0 2.5 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 1.3 0.31 ug/l
91-20-3 Naphthalene 47.1 1.3 0.31 ug/l
103-65-1 n-Propylbenzene 21.4 1.3 0.31 ug/l
100-42-5 Styrene ND 1.3 0.31 ug/l
75-85-4 Tert-Amyl Alcohol 12.0 25 5.0 ug/l J
994-05-8 Tert-Amyl Methyl Ether ND 2.5 0.50 ug/l
75-65-0 Tert-Butyl Alcohol ND 25 5.0 ug/l
762-75-4 Tert-Butyl Formate b ND 25 5.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l
127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l
108-88-3 Toluene 3.6 1.3 0.31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l
79-01-6 Trichloroethylene ND 1.3 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l
95-63-6 1,2,4-Trimethylbenzene 151 c 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 37.2 1.3 0.31 ug/l
75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l
m,p-Xylene 186 2.5 0.31 ug/l
95-47-6 o-Xylene 111 1.3 0.31 ug/l
1330-20-7 Xylene (total)305 c 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 87%83%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%100%70-130%
460-00-4 4-Bromofluorobenzene 95%100%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Associated CCV & ECC outside of control limits high, sample was ND.
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F06947.D 1 10/29/20 12:11 MV 10/28/20 11:00 OP82706 S6F269
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol a ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane) bND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
121-14-2 2,4-Dinitrotoluene ND 4.8 0.77 ug/l
606-20-2 2,6-Dinitrotoluene ND 4.8 0.68 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene c ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene 7.3 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene 13.0 4.8 0.57 ug/l
91-20-3 Naphthalene 23.7 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine a ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 20%14-67%
4165-62-2 Phenol-d5 14%10-50%
118-79-6 2,4,6-Tribromophenol 73%33-118%
4165-60-0 Nitrobenzene-d5 52%42-108%
321-60-8 2-Fluorobiphenyl 59%40-106%
1718-51-0 Terphenyl-d14 64%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
597-96-6 3-Hexanol, 3-methyl-4.13 10 ug/l JN
100-41-4 Ethylbenzene 4.32 43 ug/l JN
95-47-6 o-Xylene 4.66 62 ug/l JN
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
98-82-8 Benzene, (1-methylethyl)-4.97 6.1 ug/l JN
103-65-1 Benzene, propyl-5.26 16 ug/l JN
620-14-4 Benzene, 1-ethyl-3-methyl-5.33 54 ug/l JN
611-14-3 Benzene, 1-ethyl-2-methyl-5.36 27 ug/l JN
526-73-8 Benzene, 1,2,3-trimethyl-5.64 110 ug/l JN
108-67-8 Benzene, 1,3,5-trimethyl-5.89 31 ug/l JN
496-11-7 Indane 6.02 25 ug/l JN
1074-43-7 Benzene, 1-methyl-3-propyl-6.14 11 ug/l JN
105-05-5 Benzene, 1,4-diethyl-6.18 28 ug/l JN
1074-17-5 Benzene, 1-methyl-2-propyl-6.27 5.3 ug/l JN
1758-88-9 Benzene, 2-ethyl-1,4-dimethyl-6.35 14 ug/l JN
934-80-5 Benzene, 4-ethyl-1,2-dimethyl-6.37 8.6 ug/l JN
488-23-3 Benzene, 1,2,3,4-tetramethyl-6.72 10 ug/l JN
2039-89-6 Benzene, 2-ethenyl-1,4-dimethyl-6.97 17 ug/l JN
Total TIC, Semi-Volatile 478 ug/l J
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
(c) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S4218.D 1 10/28/20 02:20 EG n/a n/a G1S108
Run #2 1S4217.D 5 10/28/20 01:52 EG n/a n/a G1S108
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.9 1.0 1.0 ug/l
100-41-4 Ethylbenzene 69.7 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.5 2.0 1.0 ug/l
91-20-3 Naphthalene 40.1 5.0 3.0 ug/l
108-88-3 Toluene 4.8 2.0 1.0 ug/l
m,p-Xylene 172 4.0 2.0 ug/l
95-47-6 o-Xylene 97.8 2.0 1.0 ug/l
1330-20-7 Xylenes (total)270 6.0 3.0 ug/l
C5- C8 Aliphatics (Unadj.)522 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)1060 a 500 180 ug/l
C5- C8 Aliphatics 513 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics 1060 a 500 180 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 102%100%70-130%
460-00-4 BFB 99%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 504.1 EPA 504 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LI130901.D 1 10/30/20 16:51 ALA 10/30/20 06:30 L:OP17582 L:GLI1037
Run #2
Initial Volume Final Volume
Run #1 35.7 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.0037 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
348-51-6 1-Chloro-2-fluorobenzene 107%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN030652.D 1 11/07/20 02:34 JA 10/27/20 10:00 OP82688 GNN1492
Run #2 b NN030457.D 1 10/30/20 16:32 NJ 10/27/20 10:00 OP82688 GNN1486
Initial Volume Final Volume
Run #1 1030 ml 2.0 ml
Run #2 1030 ml 1.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 3.9 1.9 ug/l
208-96-8 Acenaphthylene ND 3.9 1.9 ug/l
120-12-7 Anthracene ND 3.9 1.9 ug/l
56-55-3 Benzo(a)anthracene ND 3.9 1.9 ug/l
50-32-8 Benzo(a)pyrene ND 3.9 1.9 ug/l
205-99-2 Benzo(b)fluoranthene ND 3.9 1.9 ug/l
191-24-2 Benzo(g,h,i)perylene ND 3.9 1.9 ug/l
207-08-9 Benzo(k)fluoranthene ND 3.9 1.9 ug/l
218-01-9 Chrysene ND 3.9 1.9 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 3.9 1.9 ug/l
206-44-0 Fluoranthene ND 3.9 1.9 ug/l
86-73-7 Fluorene ND 3.9 1.9 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 3.9 1.9 ug/l
91-57-6 2-Methylnaphthalene 25.2 3.9 1.9 ug/l
91-20-3 Naphthalene 51.5 3.9 1.9 ug/l
85-01-8 Phenanthrene ND 3.9 1.9 ug/l
129-00-0 Pyrene ND 3.9 1.9 ug/l
C11-C22 Aromatics (Unadj.)355 190 78 ug/l
C11-C22 Aromatics 278 190 78 ug/l
C9-C18 Aliphatics ND 190 49 ug/l
C19-C36 Aliphatics ND 190 49 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 28% c 44%40-140%
580-13-2 2-Bromonaphthalene 123%40-140%
84-15-1 o-Terphenyl 45%36% c 40-140%
321-60-8 2-Fluorobiphenyl 122%40-140%
(a) Associated MB surrogate recovery outside control limits. Insufficient sample for reextraction.
(b) Confirmation run.
(c) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA80098-1 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <5.0 5.0 ug/l 1 10/29/20 10/29/20 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA17189
(2) Prep QC Batch: MP38048
RL = Reporting Limit
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Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E104656.D 20 10/28/20 13:30 LR n/a n/a VE2369
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 637 10 2.5 ug/l
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 13.2 10 2.5 ug/l
135-98-8 sec-Butylbenzene 11.3 10 2.5 ug/l
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene ND 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 101
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Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 3.0 10 2.5 ug/l J
100-41-4 Ethylbenzene 176 10 2.5 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 56.4 10 2.5 ug/l
99-87-6 p-Isopropyltoluene ND 10 2.5 ug/l
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride 4.6 10 4.0 ug/l J
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether 12.4 10 2.5 ug/l
91-20-3 Naphthalene 69.0 10 2.5 ug/l
103-65-1 n-Propylbenzene 174 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
75-85-4 Tert-Amyl Alcohol 146 200 40 ug/l J
994-05-8 Tert-Amyl Methyl Ether ND 20 4.0 ug/l
75-65-0 Tert-Butyl Alcohol 134 200 40 ug/l J
762-75-4 Tert-Butyl Formate a ND 200 40 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 127 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 241 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 52.5 10 2.5 ug/l
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 415 20 2.5 ug/l
95-47-6 o-Xylene 64.6 10 2.5 ug/l
1330-20-7 Xylene (total)479 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 82%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated CCV and ECC outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F06948.D 1 10/29/20 12:37 MV 10/28/20 11:00 OP82706 S6F269
Run #2
Initial Volume Final Volume
Run #1 980 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 51 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.1 0.61 ug/l
95-57-8 2-Chlorophenol ND 5.1 0.64 ug/l
120-83-2 2,4-Dichlorophenol ND 5.1 0.85 ug/l
105-67-9 2,4-Dimethylphenol 2.4 5.1 0.75 ug/l J
51-28-5 2,4-Dinitrophenol ND 26 5.1 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol 0.61 5.1 0.57 ug/l J
3&4-Methylphenol ND 5.1 1.0 ug/l
88-75-5 2-Nitrophenol ND 5.1 0.87 ug/l
100-02-7 4-Nitrophenol ND 26 5.1 ug/l
87-86-5 Pentachlorophenol a ND 26 5.1 ug/l
108-95-2 Phenol 2.1 5.1 0.51 ug/l J
88-06-2 2,4,6-Trichlorophenol ND 5.1 0.77 ug/l
83-32-9 Acenaphthene ND 5.1 0.64 ug/l
208-96-8 Acenaphthylene ND 5.1 0.65 ug/l
120-12-7 Anthracene ND 5.1 0.81 ug/l
56-55-3 Benzo(a)anthracene ND 5.1 0.78 ug/l
50-32-8 Benzo(a)pyrene ND 5.1 0.80 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.1 0.79 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.1 0.84 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.1 0.88 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.1 0.86 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.1 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.1 0.64 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.1 0.83 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.1 0.75 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane) bND 5.1 0.77 ug/l
91-58-7 2-Chloronaphthalene ND 5.1 0.51 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.1 0.55 ug/l
218-01-9 Chrysene ND 5.1 0.87 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.1 0.82 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 5.1 0.61 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.1 0.66 ug/l
84-66-2 Diethyl Phthalate ND 5.1 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.1 1.0 ug/l
84-74-2 Di-n-butyl Phthalate ND 5.1 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.1 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.1 0.83 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.1 0.73 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.1 1.0 ug/l
206-44-0 Fluoranthene ND 5.1 0.56 ug/l
86-73-7 Fluorene ND 5.1 0.72 ug/l
118-74-1 Hexachlorobenzene ND 5.1 0.71 ug/l
87-68-3 Hexachlorobutadiene ND 5.1 0.51 ug/l
77-47-4 Hexachlorocyclopentadiene c ND 5.1 1.8 ug/l
67-72-1 Hexachloroethane ND 5.1 1.7 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.1 0.73 ug/l
78-59-1 Isophorone ND 5.1 0.79 ug/l
90-12-0 1-Methylnaphthalene 32.6 5.1 0.54 ug/l
91-57-6 2-Methylnaphthalene 44.2 5.1 0.61 ug/l
91-20-3 Naphthalene 40.8 5.1 0.51 ug/l
98-95-3 Nitrobenzene ND 5.1 0.95 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.1 0.68 ug/l
86-30-6 N-Nitrosodiphenylamine a ND 5.1 0.82 ug/l
85-01-8 Phenanthrene ND 5.1 0.88 ug/l
129-00-0 Pyrene ND 5.1 0.70 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 23%14-67%
4165-62-2 Phenol-d5 18%10-50%
118-79-6 2,4,6-Tribromophenol 70%33-118%
4165-60-0 Nitrobenzene-d5 52%42-108%
321-60-8 2-Fluorobiphenyl 59%40-106%
1718-51-0 Terphenyl-d14 62%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
108-88-3 Toluene 3.28 58 ug/l JN
597-96-6 3-Hexanol, 3-methyl-4.13 6.6 ug/l JN
100-41-4 Ethylbenzene 4.32 100 ug/l JN
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
95-47-6 o-Xylene 4.65 47 ug/l JN
98-82-8 Benzene, (1-methylethyl)-4.97 39 ug/l JN
103-65-1 Benzene, propyl-5.26 98 ug/l JN
620-14-4 Benzene, 1-ethyl-3-methyl-5.33 65 ug/l JN
611-14-3 Benzene, 1-ethyl-2-methyl-5.36 41 ug/l JN
108-67-8 Benzene, 1,3,5-trimethyl-5.41 40 ug/l JN
526-73-8 Benzene, 1,2,3-trimethyl-5.65 190 ug/l JN
496-11-7 Indane 6.02 110 ug/l JN
1074-55-1 Benzene, 1-methyl-4-propyl-6.26 8.7 ug/l JN
756-81-0 Silane, diethyldimethyl-6.55 11 ug/l JN
95-93-2 Benzene, 1,2,4,5-tetramethyl-6.69 32 ug/l JN
488-23-3 Benzene, 1,2,3,4-tetramethyl-6.72 10 ug/l JN
3454-07-7 Benzene, 1-ethenyl-4-ethyl-6.97 57 ug/l JN
6682-71-9 1H-Indene, 2,3-dihydro-4,7-dimethy 7.72 6.3 ug/l JN
581-42-0 Naphthalene, 2,6-dimethyl-8.83 7.3 ug/l JN
78-51-3 Ethanol, 2-butoxy-, phosphate (3:1 13.82 9.1 ug/l JN
Total TIC, Semi-Volatile 936 ug/l J
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
(c) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S4221.D 1 10/28/20 03:44 EG n/a n/a G1S108
Run #2 1S4220.D 10 10/28/20 03:16 EG n/a n/a G1S108
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 624 a 10 10 ug/l
100-41-4 Ethylbenzene 160 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 10.3 2.0 1.0 ug/l
91-20-3 Naphthalene 64.6 5.0 3.0 ug/l
108-88-3 Toluene 114 2.0 1.0 ug/l
m,p-Xylene 360 4.0 2.0 ug/l
95-47-6 o-Xylene 67.4 2.0 1.0 ug/l
1330-20-7 Xylenes (total)427 6.0 3.0 ug/l
C5- C8 Aliphatics (Unadj.)1890 a 1000 350 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)2920 a 1000 350 ug/l
C5- C8 Aliphatics 1130 a 1000 350 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics 2920 a 1000 350 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 103%99%70-130%
460-00-4 BFB 103%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 504.1 EPA 504 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LI130902.D 1 10/30/20 17:10 ALA 10/30/20 06:30 L:OP17582 L:GLI1037
Run #2
Initial Volume Final Volume
Run #1 36.3 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.019 0.0037 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
348-51-6 1-Chloro-2-fluorobenzene 102%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN030653.D 2 11/07/20 03:03 JA 10/27/20 10:00 OP82688 GNN1492
Run #2 b NN030458.D 1 10/30/20 17:02 NJ 10/27/20 10:00 OP82688 GNN1486
Initial Volume Final Volume
Run #1 1010 ml 2.0 ml
Run #2 1010 ml 1.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 7.9 4.0 ug/l
208-96-8 Acenaphthylene ND 7.9 4.0 ug/l
120-12-7 Anthracene ND 7.9 4.0 ug/l
56-55-3 Benzo(a)anthracene ND 7.9 4.0 ug/l
50-32-8 Benzo(a)pyrene ND 7.9 4.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 7.9 4.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 7.9 4.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 7.9 4.0 ug/l
218-01-9 Chrysene ND 7.9 4.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 7.9 4.0 ug/l
206-44-0 Fluoranthene ND 7.9 4.0 ug/l
86-73-7 Fluorene ND 7.9 4.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 7.9 4.0 ug/l
91-57-6 2-Methylnaphthalene 52.3 7.9 4.0 ug/l
91-20-3 Naphthalene 57.7 7.9 4.0 ug/l
85-01-8 Phenanthrene ND 7.9 4.0 ug/l
129-00-0 Pyrene ND 7.9 4.0 ug/l
C11-C22 Aromatics (Unadj.)369 400 160 ug/l J
C11-C22 Aromatics 259 400 160 ug/l J
C9-C18 Aliphatics ND 400 99 ug/l
C19-C36 Aliphatics ND 400 99 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 25% c 39% c 40-140%
580-13-2 2-Bromonaphthalene 104%40-140%
84-15-1 o-Terphenyl 35% c 32% c 40-140%
321-60-8 2-Fluorobiphenyl 106%40-140%
(a) Associated MB surrogate recovery outside control limits. Insufficient sample for reextraction.
(b) Confirmation run.
(c) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA80098-2 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 6.8 5.0 ug/l 1 10/29/20 10/29/20 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA17189
(2) Prep QC Batch: MP38048
RL = Reporting Limit
27 of 101
FA8009833.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E104604.D 1 10/26/20 20:26 CV n/a n/a VE2367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.21 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 101
FA8009833.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether a ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether a ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate b ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 86%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 101
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SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Associated CCV & ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 101
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SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F06949.D 1 10/29/20 13:02 MV 10/28/20 11:00 OP82706 S6F269
Run #2
Initial Volume Final Volume
Run #1 980 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 51 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.1 0.61 ug/l
95-57-8 2-Chlorophenol ND 5.1 0.64 ug/l
120-83-2 2,4-Dichlorophenol ND 5.1 0.85 ug/l
105-67-9 2,4-Dimethylphenol ND 5.1 0.75 ug/l
51-28-5 2,4-Dinitrophenol ND 26 5.1 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.1 0.57 ug/l
3&4-Methylphenol ND 5.1 1.0 ug/l
88-75-5 2-Nitrophenol ND 5.1 0.87 ug/l
100-02-7 4-Nitrophenol ND 26 5.1 ug/l
87-86-5 Pentachlorophenol a ND 26 5.1 ug/l
108-95-2 Phenol ND 5.1 0.51 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.1 0.77 ug/l
83-32-9 Acenaphthene ND 5.1 0.64 ug/l
208-96-8 Acenaphthylene ND 5.1 0.65 ug/l
120-12-7 Anthracene ND 5.1 0.81 ug/l
56-55-3 Benzo(a)anthracene ND 5.1 0.78 ug/l
50-32-8 Benzo(a)pyrene ND 5.1 0.80 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.1 0.79 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.1 0.84 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.1 0.88 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.1 0.86 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.1 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.1 0.64 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.1 0.83 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.1 0.75 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane) bND 5.1 0.77 ug/l
91-58-7 2-Chloronaphthalene ND 5.1 0.51 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.1 0.55 ug/l
218-01-9 Chrysene ND 5.1 0.87 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.1 0.82 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 101
FA8009833.3
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Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 5.1 0.61 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.1 0.66 ug/l
84-66-2 Diethyl Phthalate ND 5.1 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.1 1.0 ug/l
84-74-2 Di-n-butyl Phthalate ND 5.1 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.1 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.1 0.83 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.1 0.73 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.1 1.0 ug/l
206-44-0 Fluoranthene ND 5.1 0.56 ug/l
86-73-7 Fluorene ND 5.1 0.72 ug/l
118-74-1 Hexachlorobenzene ND 5.1 0.71 ug/l
87-68-3 Hexachlorobutadiene ND 5.1 0.51 ug/l
77-47-4 Hexachlorocyclopentadiene c ND 5.1 1.8 ug/l
67-72-1 Hexachloroethane ND 5.1 1.7 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.1 0.73 ug/l
78-59-1 Isophorone ND 5.1 0.79 ug/l
90-12-0 1-Methylnaphthalene ND 5.1 0.54 ug/l
91-57-6 2-Methylnaphthalene ND 5.1 0.61 ug/l
91-20-3 Naphthalene ND 5.1 0.51 ug/l
98-95-3 Nitrobenzene ND 5.1 0.95 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.1 0.68 ug/l
86-30-6 N-Nitrosodiphenylamine a ND 5.1 0.82 ug/l
85-01-8 Phenanthrene ND 5.1 0.88 ug/l
129-00-0 Pyrene ND 5.1 0.70 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 23%14-67%
4165-62-2 Phenol-d5 17%10-50%
118-79-6 2,4,6-Tribromophenol 71%33-118%
4165-60-0 Nitrobenzene-d5 54%42-108%
321-60-8 2-Fluorobiphenyl 62%40-106%
1718-51-0 Terphenyl-d14 67%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
6863-58-7 Di-sec-butyl ether 5.77 5.3 ug/l JN
Total TIC, Semi-Volatile 5.3 ug/l J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
(c) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 101
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S4215.D 1 10/28/20 00:57 EG n/a n/a G1S108
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
1330-20-7 Xylenes (total)ND 6.0 3.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 99%70-130%
460-00-4 BFB 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 101
FA8009833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 504.1 EPA 504 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LI130903.D 1 10/30/20 17:28 ALA 10/30/20 06:30 L:OP17582 L:GLI1037
Run #2
Initial Volume Final Volume
Run #1 35.9 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.0037 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
348-51-6 1-Chloro-2-fluorobenzene 98%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 101
FA8009833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN030654.D 1 11/07/20 03:32 JA 10/27/20 10:00 OP82688 GNN1492
Run #2 b NN030459.D 1 10/30/20 17:31 NJ 10/27/20 10:00 OP82688 GNN1486
Initial Volume Final Volume
Run #1 980 ml 2.0 ml
Run #2 980 ml 1.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.1 2.0 ug/l
208-96-8 Acenaphthylene ND 4.1 2.0 ug/l
120-12-7 Anthracene ND 4.1 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.1 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.1 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.1 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.1 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.1 2.0 ug/l
218-01-9 Chrysene ND 4.1 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.1 2.0 ug/l
206-44-0 Fluoranthene ND 4.1 2.0 ug/l
86-73-7 Fluorene ND 4.1 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.1 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.1 2.0 ug/l
91-20-3 Naphthalene ND 4.1 2.0 ug/l
85-01-8 Phenanthrene ND 4.1 2.0 ug/l
129-00-0 Pyrene ND 4.1 2.0 ug/l
C11-C22 Aromatics (Unadj.)98.7 200 82 ug/l J
C11-C22 Aromatics 98.7 200 82 ug/l J
C9-C18 Aliphatics ND 200 51 ug/l
C19-C36 Aliphatics ND 200 51 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 30% c 44%40-140%
580-13-2 2-Bromonaphthalene 99%40-140%
84-15-1 o-Terphenyl 37% c 36% c 40-140%
321-60-8 2-Fluorobiphenyl 103%40-140%
(a) Associated MB surrogate recovery outside control limits. Insufficient sample for reextraction.
(b) Confirmation run.
(c) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 101
FA8009833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA80098-3 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 22.9 5.0 ug/l 1 10/29/20 10/29/20 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA17189
(2) Prep QC Batch: MP38048
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E104605.D 1 10/26/20 20:49 CV n/a n/a VE2367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether a ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether a ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate b ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 86%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:SM 6200B Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Associated CCV & ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 101
FA8009833.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F06950.D 1 10/29/20 13:28 MV 10/28/20 11:00 OP82706 S6F269
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol a ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane) bND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
121-14-2 2,4-Dinitrotoluene ND 4.8 0.77 ug/l
606-20-2 2,6-Dinitrotoluene ND 4.8 0.68 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene c ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine a ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 24%14-67%
4165-62-2 Phenol-d5 22%10-50%
118-79-6 2,4,6-Tribromophenol 60%33-118%
4165-60-0 Nitrobenzene-d5 47%42-108%
321-60-8 2-Fluorobiphenyl 53%40-106%
1718-51-0 Terphenyl-d14 54%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
(b) Associated CCV outside of control limits low.
(c) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S4216.D 1 10/28/20 01:25 EG n/a n/a G1S108
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
1330-20-7 Xylenes (total)ND 6.0 3.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 100%70-130%
460-00-4 BFB 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:EPA 504.1 EPA 504 Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LI130904.D 1 10/30/20 17:46 ALA 10/30/20 06:30 L:OP17582 L:GLI1037
Run #2
Initial Volume Final Volume
Run #1 34.6 ml 2.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.0038 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
348-51-6 1-Chloro-2-fluorobenzene 96%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN030655.D 1 11/07/20 04:01 JA 10/27/20 10:00 OP82688 GNN1492
Run #2 b NN030728.D 1 11/10/20 14:04 JA 10/27/20 10:00 OP82688 GNN1494
Initial Volume Final Volume
Run #1 980 ml 2.0 ml
Run #2 980 ml 2.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.1 2.0 ug/l
208-96-8 Acenaphthylene ND 4.1 2.0 ug/l
120-12-7 Anthracene ND 4.1 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.1 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.1 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.1 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.1 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.1 2.0 ug/l
218-01-9 Chrysene ND 4.1 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.1 2.0 ug/l
206-44-0 Fluoranthene ND 4.1 2.0 ug/l
86-73-7 Fluorene ND 4.1 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.1 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.1 2.0 ug/l
91-20-3 Naphthalene ND 4.1 2.0 ug/l
85-01-8 Phenanthrene ND 4.1 2.0 ug/l
129-00-0 Pyrene ND 4.1 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 82 ug/l
C11-C22 Aromatics ND 200 82 ug/l
C9-C18 Aliphatics ND 200 51 ug/l
C19-C36 Aliphatics ND 200 51 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 33% c 32%40-140%
580-13-2 2-Bromonaphthalene 94%69%40-140%
84-15-1 o-Terphenyl 46%29%40-140%
321-60-8 2-Fluorobiphenyl 104%68%40-140%
(a) Associated MB surrogate recovery outside control limits. Insufficient sample for reextraction.
(b) Confirmation run.
(c) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:FA80098-4 Date Sampled:10/22/20
Matrix:AQ - Ground Water Date Received:10/23/20
Percent Solids:n/a
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 1130 5.0 ug/l 1 10/29/20 10/29/20 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA17189
(2) Prep QC Batch: MP38048
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
48 of 101
FA800984
FA80098: Chain of Custody
Page 1 of 3
49 of 101
FA8009844.1
Job Number:FA80098 Client:GEOLOGICAL RESOURCES INC
Date / Time Received:10/23/2020 9:15:00 AM Delivery Method:FED EX
Project:HASTY MART#15
Airbill #'s:100963784508
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.4);
Cooler 1: (1.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:CARLOSD Date:Date:10/23/2020 9:15:00 A
FA80098: Chain of Custody
Page 2 of 3
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FA8009844.1
TAT (Days):7
Received Date:10/23/2020
Due Date:10/30/2020
Project Description:Handy Mart #15; 2495 US 13, Goldsboro, NC
Account Name:GRI (Geological Resources Inc.)
Deliverable:COMMB
CSR:MM
Requested Date:11/11/2020
Job Change Order:FA80098
Sample #:FA80098-ALL Change:
Per client project name should be Handy Mart #15.Dept:
====================================================================================================================
====================================================================================================================
TAT:7
Above Changes Per:
To Client: This Change Order is confirmation of the revisions, previously discussed with the Client Service Representative.
Date/Time:11/11/2020 11:01:03 AM
Page 1 of 1
William Regenthal
FA80098: Chain of Custody
Page 3 of 3
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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Method Blank Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-MB E104589.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-MB E104589.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 85%70-130%
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Method Blank Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-MB E104589.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
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Method Blank Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-MB E104651.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
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Method Blank Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-MB E104651.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 85%70-130%
57 of 101
FA8009855.1.2
Method Blank Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-MB E104651.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
58 of 101
FA8009855.1.2
Blank Spike Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-BS E104587.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.3 113 70-130
108-86-1 Bromobenzene 10 10.0 100 70-130
74-97-5 Bromochloromethane 10 10.5 105 70-130
75-27-4 Bromodichloromethane 10 11.1 111 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 11.0 110 70-130
98-06-6 tert-Butylbenzene 10 11.1 111 70-130
56-23-5 Carbon Tetrachloride 10 11.8 118 70-130
108-90-7 Chlorobenzene 10 10.5 105 70-130
75-00-3 Chloroethane 10 8.8 88 60-140
67-66-3 Chloroform 10 11.0 110 70-130
95-49-8 o-Chlorotoluene 10 10.7 107 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 10.4 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.1 101 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 7.4 74 60-140
95-50-1 1,2-Dichlorobenzene 10 10.3 103 70-130
541-73-1 1,3-Dichlorobenzene 10 10.6 106 70-130
106-46-7 1,4-Dichlorobenzene 10 10.1 101 70-130
75-34-3 1,1-Dichloroethane 10 11.5 115 70-130
107-06-2 1,2-Dichloroethane 10 11.0 110 70-130
75-35-4 1,1-Dichloroethylene 10 12.6 126 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.4 114 70-130
78-87-5 1,2-Dichloropropane 10 11.4 114 70-130
142-28-9 1,3-Dichloropropane 10 10.0 100 70-130
594-20-7 2,2-Dichloropropane 10 12.4 124 70-130
563-58-6 1,1-Dichloropropene 10 12.4 124 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.5 105 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.2 102 70-130
108-20-3 Di-Isopropyl Ether 10 11.6 116 70-130
100-41-4 Ethylbenzene 10 10.9 109 70-130
637-92-3 Ethyl Tert Butyl Ether 10 10.5 105 70-130
87-68-3 Hexachlorobutadiene 10 11.8 118 70-130
* = Outside of Control Limits.
59 of 101
FA8009855.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-BS E104587.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 11.0 110 70-130
99-87-6 p-Isopropyltoluene 10 10.7 107 70-130
74-83-9 Methyl Bromide 10 9.8 98 60-140
74-87-3 Methyl Chloride 10 9.5 95 60-140
74-95-3 Methylene Bromide 10 10.4 104 70-130
75-09-2 Methylene Chloride 10 11.4 114 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.1 111 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
103-65-1 n-Propylbenzene 10 11.0 110 70-130
100-42-5 Styrene 10 9.3 93 70-130
75-85-4 Tert-Amyl Alcohol 100 100 100 70-130
994-05-8 Tert-Amyl Methyl Ether 10 10.8 108 70-130
75-65-0 Tert-Butyl Alcohol 100 112 112 70-130
762-75-4 Tert-Butyl Formate 100 118 118 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.0 110 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.9 109 70-130
127-18-4 Tetrachloroethylene 10 11.0 110 70-130
108-88-3 Toluene 10 10.7 107 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.5 105 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.6 106 70-130
71-55-6 1,1,1-Trichloroethane 10 11.3 113 70-130
79-00-5 1,1,2-Trichloroethane 10 10.6 106 70-130
79-01-6 Trichloroethylene 10 10.9 109 70-130
75-69-4 Trichlorofluoromethane 10 11.3 113 60-140
96-18-4 1,2,3-Trichloropropane 10 10.1 101 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.5 105 70-130
75-01-4 Vinyl Chloride 10 9.6 96 60-140
m,p-Xylene 20 21.9 110 70-130
95-47-6 o-Xylene 10 10.5 105 70-130
1330-20-7 Xylene (total)30 32.4 108 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 87%70-130%
* = Outside of Control Limits.
60 of 101
FA8009855.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2367-BS E104587.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
61 of 101
FA8009855.2.1
Blank Spike Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-BS E104649.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 9.7 97 70-130
74-97-5 Bromochloromethane 10 10.1 101 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 8.8 88 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10.7 107 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 10 100 70-130
75-00-3 Chloroethane 10 10.0 100 60-140
67-66-3 Chloroform 10 10.6 106 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 9.7 97 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.7 97 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
75-71-8 Dichlorodifluoromethane 10 10.8 108 60-140
95-50-1 1,2-Dichlorobenzene 10 9.9 99 70-130
541-73-1 1,3-Dichlorobenzene 10 10.2 102 70-130
106-46-7 1,4-Dichlorobenzene 10 9.7 97 70-130
75-34-3 1,1-Dichloroethane 10 11.1 111 70-130
107-06-2 1,2-Dichloroethane 10 10.6 106 70-130
75-35-4 1,1-Dichloroethylene 10 12.1 121 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.5 105 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.2 112 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 9.9 99 70-130
594-20-7 2,2-Dichloropropane 10 12.2 122 70-130
563-58-6 1,1-Dichloropropene 10 12.0 120 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.1 101 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
108-20-3 Di-Isopropyl Ether 10 11.4 114 70-130
100-41-4 Ethylbenzene 10 10.6 106 70-130
637-92-3 Ethyl Tert Butyl Ether 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 11.3 113 70-130
* = Outside of Control Limits.
62 of 101
FA8009855.2.2
Blank Spike Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-BS E104649.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 10.8 108 70-130
99-87-6 p-Isopropyltoluene 10 10.4 104 70-130
74-83-9 Methyl Bromide 10 10.8 108 60-140
74-87-3 Methyl Chloride 10 11.3 113 60-140
74-95-3 Methylene Bromide 10 9.9 99 70-130
75-09-2 Methylene Chloride 10 10.8 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.9 109 70-130
91-20-3 Naphthalene 10 9.3 93 70-130
103-65-1 n-Propylbenzene 10 10.8 108 70-130
100-42-5 Styrene 10 9.2 92 70-130
75-85-4 Tert-Amyl Alcohol 100 106 106 70-130
994-05-8 Tert-Amyl Methyl Ether 10 10.9 109 70-130
75-65-0 Tert-Butyl Alcohol 100 120 120 70-130
762-75-4 Tert-Butyl Formate 100 127 127 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.5 105 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.5 105 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 10.3 103 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.3 103 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 11.0 110 70-130
79-00-5 1,1,2-Trichloroethane 10 10.3 103 70-130
79-01-6 Trichloroethylene 10 10.6 106 70-130
75-69-4 Trichlorofluoromethane 10 11.8 118 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130
75-01-4 Vinyl Chloride 10 11.2 112 60-140
m,p-Xylene 20 21.2 106 70-130
95-47-6 o-Xylene 10 10.5 105 70-130
1330-20-7 Xylene (total)30 31.6 105 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 85%70-130%
* = Outside of Control Limits.
63 of 101
FA8009855.2.2
Blank Spike Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2369-BS E104649.D 1 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
64 of 101
FA8009855.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA79894-1MS E104600.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1MSD E104601.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1 E104595.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
FA79894-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.4 104 10 10.6 106 2 70-130/20
108-86-1 Bromobenzene ND 10 9.4 94 10 9.4 94 0 70-130/20
74-97-5 Bromochloromethane ND 10 9.7 97 10 9.9 99 2 70-130/20
75-27-4 Bromodichloromethane ND 10 9.9 99 10 10.0 100 1 70-130/20
75-25-2 Bromoform ND 10 7.5 75 10 7.9 79 5 70-130/20
104-51-8 n-Butylbenzene ND 10 9.8 98 10 10.2 102 4 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.2 102 10 10.6 106 4 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.1 101 10 10.5 105 4 70-130/20
56-23-5 Carbon Tetrachloride ND 10 10.8 108 10 11.3 113 5 70-130/20
108-90-7 Chlorobenzene ND 10 9.6 96 10 9.9 99 3 70-130/20
75-00-3 Chloroethane ND 10 11.8 118 10 11.8 118 0 60-140/20
67-66-3 Chloroform ND 10 10.4 104 10 10.6 106 2 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.9 99 10 10.2 102 3 70-130/20
106-43-4 p-Chlorotoluene ND 10 9.8 98 10 10.0 100 2 70-130/20
124-48-1 Dibromochloromethane ND 10 8.7 87 10 9.0 90 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.8 98 10 10.0 100 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.3 93 10 9.4 94 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.9 89 10 9.0 90 1 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 9.5 95 10 9.8 98 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 9.9 99 10 10.0 100 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.5 95 10 9.7 97 2 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.7 107 10 11.0 110 3 70-130/20
107-06-2 1,2-Dichloroethane ND 10 10.1 101 10 10.2 102 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.6 116 10 12.2 122 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.0 100 10 10.2 102 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.6 106 10 11.0 110 4 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.6 106 10 10.5 105 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.2 92 10 9.3 93 1 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.9 109 10 10.9 109 0 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.3 113 10 11.6 116 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 7.8 78 10 7.9 79 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 8.4 84 10 8.5 85 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 11.1 111 10 11.3 113 2 70-130/20
100-41-4 Ethylbenzene ND 10 10.2 102 10 10.5 105 3 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 10 10 100 10 10.1 101 1 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.5 105 10 11.1 111 6 70-130/20
* = Outside of Control Limits.
65 of 101
FA8009855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA79894-1MS E104600.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1MSD E104601.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1 E104595.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
FA79894-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 10 10.1 101 10 10.5 105 4 70-130/20
99-87-6 p-Isopropyltoluene ND 10 9.8 98 10 10.2 102 4 70-130/20
74-83-9 Methyl Bromide ND 10 13.7 137 10 13.4 134 2 60-140/20
74-87-3 Methyl Chloride ND 10 11.2 112 10 11.2 112 0 60-140/20
74-95-3 Methylene Bromide ND 10 9.7 97 10 9.6 96 1 70-130/20
75-09-2 Methylene Chloride ND 10 10.7 107 10 11.0 110 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.4 104 10 10.4 104 0 70-130/20
91-20-3 Naphthalene ND 10 8.4 84 10 8.9 89 6 70-130/20
103-65-1 n-Propylbenzene ND 10 10.3 103 10 10.5 105 2 70-130/20
100-42-5 Styrene ND 10 8.4 84 10 8.7 87 4 70-130/20
75-85-4 Tert-Amyl Alcohol ND 100 92.3 92 100 90.6 91 2 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 10 10 100 10 10.0 100 0 70-130/20
75-65-0 Tert-Butyl Alcohol ND 100 147 147*100 151 151*3 70-130/20
762-75-4 Tert-Butyl Formate ND 100 12.2 12*100 9.0 9*30*70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.0 100 10 10.5 105 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.6 106 10 10.4 104 2 70-130/20
127-18-4 Tetrachloroethylene ND 10 10 100 10 10.3 103 3 70-130/20
108-88-3 Toluene ND 10 9.9 99 10 10.2 102 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.4 94 10 10.2 102 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 9.3 93 10 9.8 98 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 10.6 106 10 10.8 108 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.8 98 10 9.9 99 1 70-130/20
79-01-6 Trichloroethylene ND 10 10.1 101 10 10.3 103 2 70-130/20
75-69-4 Trichlorofluoromethane ND 10 13.7 137 10 13.6 136 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 9.3 93 10 9.4 94 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.2 92 10 9.5 95 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.7 97 10 10 100 3 70-130/20
75-01-4 Vinyl Chloride ND 10 11.8 118 10 11.8 118 0 60-140/20
m,p-Xylene ND 20 20.2 101 20 20.8 104 3 70-130/20
95-47-6 o-Xylene ND 10 9.8 98 10 10.1 101 3 70-130/20
1330-20-7 Xylene (total)ND 30 29.9 100 30 30.9 103 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA79894-1 Limits
1868-53-7 Dibromofluoromethane 88%88%89%70-130%
* = Outside of Control Limits.
66 of 101
FA8009855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA79894-1MS E104600.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1MSD E104601.D 1 10/26/20 CV n/a n/a VE2367
FA79894-1 E104595.D 1 10/26/20 CV n/a n/a VE2367
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-3, FA80098-4
CAS No.Surrogate Recoveries MS MSD FA79894-1 Limits
17060-07-0 1,2-Dichloroethane-D4 110%109%108%70-130%
2037-26-5 Toluene-D8 98%99%101%70-130%
460-00-4 4-Bromofluorobenzene 97%97%97%70-130%
* = Outside of Control Limits.
67 of 101
FA8009855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA80098-1MS E104662.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1MSD E104663.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1 E104655.D 5 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
FA80098-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 100 107 107 100 106 106 1 70-130/20
108-86-1 Bromobenzene ND 100 95.5 96 100 94.9 95 1 70-130/20
74-97-5 Bromochloromethane ND 100 97.2 97 100 95.9 96 1 70-130/20
75-27-4 Bromodichloromethane ND 100 98.9 99 100 98.1 98 1 70-130/20
75-25-2 Bromoform ND 100 65.7 66*100 66.3 66*1 70-130/20
104-51-8 n-Butylbenzene 3.6 100 110 106 100 107 103 3 70-130/20
135-98-8 sec-Butylbenzene 2.3 J 100 109 107 100 107 105 2 70-130/20
98-06-6 tert-Butylbenzene ND 100 107 107 100 106 106 1 70-130/20
56-23-5 Carbon Tetrachloride ND 100 109 109 100 106 106 3 70-130/20
108-90-7 Chlorobenzene ND 100 98.7 99 100 98.3 98 0 70-130/20
75-00-3 Chloroethane ND 100 89.3 89 100 106 106 17 60-140/20
67-66-3 Chloroform 1.1 J 100 104 103 100 103 102 1 70-130/20
95-49-8 o-Chlorotoluene ND 100 109 109 100 107 107 2 70-130/20
106-43-4 p-Chlorotoluene ND 100 102 102 100 102 102 0 70-130/20
124-48-1 Dibromochloromethane ND 100 82.6 83 100 82.5 83 0 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 99.7 100 100 93.3 93 7 70-130/20
106-93-4 1,2-Dibromoethane ND 100 95.3 95 100 95.5 96 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 102 102 100 118 118 15 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 97.5 98 100 95.2 95 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 99.9 100 100 98.1 98 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 94.6 95 100 93.8 94 1 70-130/20
75-34-3 1,1-Dichloroethane ND 100 108 108 100 107 107 1 70-130/20
107-06-2 1,2-Dichloroethane ND 100 104 104 100 104 104 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 117 117 100 115 115 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 99.5 100 100 98.7 99 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 107 107 100 108 108 1 70-130/20
78-87-5 1,2-Dichloropropane ND 100 110 110 100 109 109 1 70-130/20
142-28-9 1,3-Dichloropropane ND 100 96.8 97 100 96.3 96 1 70-130/20
594-20-7 2,2-Dichloropropane ND 100 110 110 100 107 107 3 70-130/20
563-58-6 1,1-Dichloropropene ND 100 117 117 100 115 115 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 95.1 95 100 92.9 93 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 91.7 92 100 90.6 91 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 114 114 100 112 112 2 70-130/20
100-41-4 Ethylbenzene 73.9 100 170 96 100 169 95 1 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 100 102 102 100 101 101 1 70-130/20
87-68-3 Hexachlorobutadiene ND 100 113 113 100 110 110 3 70-130/20
* = Outside of Control Limits.
68 of 101
FA8009855.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA80098-1MS E104662.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1MSD E104663.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1 E104655.D 5 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
FA80098-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene 6.4 100 111 105 100 111 105 0 70-130/20
99-87-6 p-Isopropyltoluene 0.97 J 100 104 103 100 103 102 1 70-130/20
74-83-9 Methyl Bromide ND 100 103 103 100 123 123 18 60-140/20
74-87-3 Methyl Chloride ND 100 112 112 100 127 127 13 60-140/20
74-95-3 Methylene Bromide ND 100 100 100 100 97.6 98 2 70-130/20
75-09-2 Methylene Chloride ND 100 108 108 100 106 106 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 104 104 100 103 103 1 70-130/20
91-20-3 Naphthalene 44.8 100 144 99 100 137 92 5 70-130/20
103-65-1 n-Propylbenzene 22.3 100 129 107 100 127 105 2 70-130/20
100-42-5 Styrene ND 100 88.5 89 100 89.5 90 1 70-130/20
75-85-4 Tert-Amyl Alcohol ND 1000 1010 101 1000 980 98 3 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 100 105 105 100 104 104 1 70-130/20
75-65-0 Tert-Butyl Alcohol ND 1000 1120 112 1000 1100 110 2 70-130/20
762-75-4 Tert-Butyl Formate ND 1000 1170 117 a 1000 1180 118 a 1 a 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 99.6 100 100 100 100 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 104 104 100 103 103 1 70-130/20
127-18-4 Tetrachloroethylene ND 100 100 100 100 100 100 0 70-130/20
108-88-3 Toluene 4.4 100 105 101 100 105 101 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 105 105 100 100 100 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 106 106 100 101 101 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 105 105 100 105 105 0 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 97.5 98 100 97.9 98 0 70-130/20
79-01-6 Trichloroethylene ND 100 102 102 100 102 102 0 70-130/20
75-69-4 Trichlorofluoromethane ND 100 114 114 100 130 130 13 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 95.8 96 100 92.6 93 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 151 100 245 94 100 238 87 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 39.4 100 142 103 100 139 100 2 70-130/20
75-01-4 Vinyl Chloride ND 100 104 104 100 121 121 15 60-140/20
m,p-Xylene 192 200 381 95 200 379 94 1 70-130/20
95-47-6 o-Xylene 114 100 207 93 100 205 91 1 70-130/20
1330-20-7 Xylene (total)305 300 588 94 300 584 93 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA80098-1 Limits
1868-53-7 Dibromofluoromethane 84%84%83%70-130%
* = Outside of Control Limits.
69 of 101
FA8009855.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA80098-1MS E104662.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1MSD E104663.D 10 10/28/20 LR n/a n/a VE2369
FA80098-1 E104655.D 5 10/28/20 LR n/a n/a VE2369
The QC reported here applies to the following samples:Method: SM 6200B
FA80098-1, FA80098-2
CAS No.Surrogate Recoveries MS MSD FA80098-1 Limits
17060-07-0 1,2-Dichloroethane-D4 110%109%107%70-130%
2037-26-5 Toluene-D8 99%99%100%70-130%
460-00-4 4-Bromofluorobenzene 102%103%100%70-130%
(a) Associated CCV and ECC outside control limits high.
* = Outside of Control Limits.
70 of 101
FA8009855.3.2
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
71 of 101
FA800986
Method Blank Summary Page 1 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82706-MB 6F06946.D 1 10/29/20 MV 10/28/20 OP82706 S6F269
The QC reported here applies to the following samples:Method: EPA 625.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
72 of 101
FA8009866.1.1
Method Blank Summary Page 2 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82706-MB 6F06946.D 1 10/29/20 MV 10/28/20 OP82706 S6F269
The QC reported here applies to the following samples:Method: EPA 625.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 32%14-67%
4165-62-2 Phenol-d5 22%10-50%
118-79-6 2,4,6-Tribromophenol 89%33-118%
4165-60-0 Nitrobenzene-d5 65%42-108%
321-60-8 2-Fluorobiphenyl 74%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
73 of 101
FA8009866.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82706-BS a 6F06945.D 1 10/29/20 MV 10/28/20 OP82706 S6F269
The QC reported here applies to the following samples:Method: EPA 625.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 15.7 16 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 32.0 64 54-103
95-57-8 2-Chlorophenol 50 31.4 63 52-98
120-83-2 2,4-Dichlorophenol 50 39.9 80 53-103
105-67-9 2,4-Dimethylphenol 50 34.1 68 43-90
51-28-5 2,4-Dinitrophenol 100 75.9 76 44-112
534-52-1 4,6-Dinitro-o-cresol 100 88.0 88 66-121
95-48-7 2-Methylphenol 50 24.9 50 43-90
3&4-Methylphenol 100 44.4 44 36-88
88-75-5 2-Nitrophenol 50 39.9 80 53-102
100-02-7 4-Nitrophenol 100 27.4 27 18-62
87-86-5 Pentachlorophenol 100 100 100 61-115
108-95-2 Phenol 50 13.7 27 19-56
88-06-2 2,4,6-Trichlorophenol 50 42.1 84 59-107
83-32-9 Acenaphthene 50 41.2 82 61-107
208-96-8 Acenaphthylene 50 44.5 89 60-104
120-12-7 Anthracene 50 40.3 81 65-108
56-55-3 Benzo(a)anthracene 50 42.7 85 66-111
50-32-8 Benzo(a)pyrene 50 44.1 88 62-107
205-99-2 Benzo(b)fluoranthene 50 45.4 91 65-114
191-24-2 Benzo(g,h,i)perylene 50 47.1 94 66-116
207-08-9 Benzo(k)fluoranthene 50 46.1 92 65-114
101-55-3 4-Bromophenyl Phenyl Ether 50 45.5 91 65-109
85-68-7 Butyl Benzyl Phthalate 50 39.2 78 65-112
106-47-8 4-Chloroaniline 50 37.2 74 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 35.6 71 51-102
111-44-4 bis(2-Chloroethyl)ether 50 34.5 69 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 30.4 61 45-106
91-58-7 2-Chloronaphthalene 50 40.1 80 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 40.8 82 62-105
218-01-9 Chrysene 50 43.7 87 66-111
53-70-3 Dibenzo(a,h)anthracene 50 46.0 92 66-119
132-64-9 Dibenzofuran 50 40.8 82 61-106
91-94-1 3,3'-Dichlorobenzidine 50 36.6 73 46-117
84-66-2 Diethyl Phthalate 50 37.4 75 64-108
131-11-3 Dimethyl Phthalate 50 40.4 81 63-106
* = Outside of Control Limits.
74 of 101
FA8009866.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82706-BS a 6F06945.D 1 10/29/20 MV 10/28/20 OP82706 S6F269
The QC reported here applies to the following samples:Method: EPA 625.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
84-74-2 Di-n-butyl Phthalate 50 38.8 78 65-107
117-84-0 Di-n-octyl Phthalate 50 39.3 79 62-118
121-14-2 2,4-Dinitrotoluene 50 42.0 84 61-110
606-20-2 2,6-Dinitrotoluene 50 41.2 82 63-108
117-81-7 bis(2-Ethylhexyl)phthalate 50 39.9 80 61-117
206-44-0 Fluoranthene 50 37.5 75 63-106
86-73-7 Fluorene 50 41.0 82 62-108
118-74-1 Hexachlorobenzene 50 45.3 91 63-108
87-68-3 Hexachlorobutadiene 50 42.1 84 42-102
77-47-4 Hexachlorocyclopentadiene 50 53.8 108*39-102
67-72-1 Hexachloroethane 50 32.8 66 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 44.6 89 64-119
78-59-1 Isophorone 50 36.9 74 43-87
90-12-0 1-Methylnaphthalene 50 37.4 75 53-102
91-57-6 2-Methylnaphthalene 50 39.3 79 51-102
91-20-3 Naphthalene 50 39.5 79 47-100
98-95-3 Nitrobenzene 50 36.3 73 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 32.5 65 52-104
86-30-6 N-Nitrosodiphenylamine 50 40.0 80 64-108
85-01-8 Phenanthrene 50 41.5 83 66-110
129-00-0 Pyrene 50 41.7 83 64-113
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 37%14-67%
4165-62-2 Phenol-d5 24%10-50%
118-79-6 2,4,6-Tribromophenol 97%33-118%
4165-60-0 Nitrobenzene-d5 74%42-108%
321-60-8 2-Fluorobiphenyl 84%40-106%
1718-51-0 Terphenyl-d14 89%39-121%
(a) Insufficient sample for MS/MSD.
* = Outside of Control Limits.
75 of 101
FA8009866.2.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
76 of 101
FA800987
Method Blank Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S108-MB 1S4207.D 1 10/27/20 EG n/a n/a G1S108
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
1330-20-7 Xylenes (total)ND 6.0 3.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 96%70-130%
460-00-4 BFB 94%70-130%
77 of 101
FA8009877.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S108-BS 1S4202.D 1 10/27/20 EG n/a n/a G1S108
G1S108-BSD 1S4203.D 1 10/27/20 EG n/a n/a G1S108
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 80 81.0 101 81.4 102 0 70-130/25
100-41-4 Ethylbenzene 80 80.0 100 80.5 101 1 70-130/25
1634-04-4 Methyl Tert Butyl Ether 80 81.5 102 81.7 102 0 70-130/25
91-20-3 Naphthalene 80 77.7 97 76.7 96 1 70-130/25
108-88-3 Toluene 80 81.9 102 82.5 103 1 70-130/25
m,p-Xylene 160 165 103 166 104 1 70-130/25
95-47-6 o-Xylene 80 79.2 99 79.6 100 1 70-130/25
1330-20-7 Xylenes (total)240 245 102 246 103 0 70-130/25
C5- C8 Aliphatics (Unadj.)240 264 110 266 111 1 70-130/25
C9- C12 Aliphatics (Unadj.)160 143 89 141 88 1 70-130/25
C9- C10 Aromatics (Unadj.)80 76.2 95 78.1 98 2 70-130/25
C9- C10 Aromatics 80 76.2 95 78.1 98 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 98%97%70-130%
460-00-4 BFB 95%95%70-130%
* = Outside of Control Limits.
78 of 101
FA8009877.2.1
Matrix Spike Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA80134-1MS 1S4211.D 1 10/27/20 EG n/a n/a G1S108
FA80134-1 1S4209.D 1 10/27/20 EG n/a n/a G1S108
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
FA80134-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 1.0 U 80 83.6 105 70-130
100-41-4 Ethylbenzene 2.0 U 80 81.4 102 70-130
1634-04-4 Methyl Tert Butyl Ether 2.0 U 80 81.7 102 70-130
91-20-3 Naphthalene 5.0 U 80 75.7 95 70-130
108-88-3 Toluene 1.0 J 80 83.1 103 70-130
m,p-Xylene 4.0 U 160 168 105 70-130
95-47-6 o-Xylene 2.0 U 80 80.8 101 70-130
1330-20-7 Xylenes (total)6.0 U 240 249 104 70-130
C5- C8 Aliphatics (Unadj.)100 U 480 563 117 70-130
C9- C12 Aliphatics (Unadj.)100 U 400 335 84 70-130
C9- C10 Aromatics (Unadj.)100 U 240 224 93 70-130
C9- C10 Aromatics 100 U 240 224 93 70-130
CAS No.Surrogate Recoveries MS FA80134-1 Limits
460-00-4 BFB 93%101%70-130%
460-00-4 BFB 91%98%70-130%
* = Outside of Control Limits.
79 of 101
FA8009877.3.1
Duplicate Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA80134-1DUP 1S4210.D 1 10/27/20 EG n/a n/a G1S108
FA80134-1 1S4209.D 1 10/27/20 EG n/a n/a G1S108
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
FA80134-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 1.0 U ND nc 50
100-41-4 Ethylbenzene 2.0 U ND nc 50
1634-04-4 Methyl Tert Butyl Ether 2.0 U ND nc 50
91-20-3 Naphthalene 5.0 U ND nc 50
108-88-3 Toluene 1.0 J 1.2 J 18 50
m,p-Xylene 4.0 U ND nc 50
95-47-6 o-Xylene 2.0 U ND nc 50
1330-20-7 Xylenes (total)6.0 U ND nc 50
C5- C8 Aliphatics (Unadj.)100 U ND nc 50
C9- C12 Aliphatics (Unadj.)100 U ND nc 50
C9- C10 Aromatics (Unadj.)100 U ND nc 50
C5- C8 Aliphatics 100 U ND nc 50
C9- C12 Aliphatics 100 U ND nc 50
C9- C10 Aromatics 100 U ND nc 50
CAS No.Surrogate Recoveries DUP FA80134-1 Limits
460-00-4 BFB 100%101%70-130%
460-00-4 BFB 98%98%70-130%
* = Outside of Control Limits.
80 of 101
FA8009877.4.1
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 8
81 of 101
FA800988
Method Blank Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82688-MB a NN030453.D 1 10/30/20 NJ 10/27/20 OP82688 GNN1486
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 2.0 1.0 ug/l
208-96-8 Acenaphthylene ND 2.0 1.0 ug/l
120-12-7 Anthracene ND 2.0 1.0 ug/l
56-55-3 Benzo(a)anthracene ND 2.0 1.0 ug/l
50-32-8 Benzo(a)pyrene ND 2.0 1.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 2.0 1.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 2.0 1.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 2.0 1.0 ug/l
218-01-9 Chrysene ND 2.0 1.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 2.0 1.0 ug/l
206-44-0 Fluoranthene ND 2.0 1.0 ug/l
86-73-7 Fluorene ND 2.0 1.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 2.0 1.0 ug/l
91-57-6 2-Methylnaphthalene ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 2.0 1.0 ug/l
85-01-8 Phenanthrene ND 2.0 1.0 ug/l
129-00-0 Pyrene ND 2.0 1.0 ug/l
C11-C22 Aromatics (Unadj.)ND 100 40 ug/l
C11-C22 Aromatics ND 100 40 ug/l
C9-C18 Aliphatics ND 100 25 ug/l
C19-C36 Aliphatics ND 100 25 ug/l
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 47%40-140%
84-15-1 o-Terphenyl 41%40-140%
(a) Results from non-fractionated extract.
82 of 101
FA8009888.1.1
Method Blank Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82688-MB NN030634.D 1 11/06/20 JA 10/27/20 OP82688 GNN1492
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C11-C22 Aromatics ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 38%* a 40-140%
580-13-2 2-Bromonaphthalene 131%40-140%
84-15-1 o-Terphenyl 48%40-140%
321-60-8 2-Fluorobiphenyl 134%40-140%
(a) Outside control limits.
83 of 101
FA8009888.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82688-BS NN030635.D 1 11/06/20 JA 10/27/20 OP82688 GNN1492
OP82688-BSD NN030636.D 1 11/06/20 JA 10/27/20 OP82688 GNN1492
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
83-32-9 Acenaphthene 100 94.3 94 78.5 79 18 40-140/30
208-96-8 Acenaphthylene 100 90.5 91 74.6 75 19 40-140/30
120-12-7 Anthracene 100 104 104 91.3 91 13 40-140/30
56-55-3 Benzo(a)anthracene 100 113 113 100 100 12 40-140/30
50-32-8 Benzo(a)pyrene 100 113 113 101 101 11 40-140/30
205-99-2 Benzo(b)fluoranthene 100 111 111 98.9 99 12 40-140/30
191-24-2 Benzo(g,h,i)perylene 100 113 113 101 101 11 40-140/30
207-08-9 Benzo(k)fluoranthene 100 115 115 102 102 12 40-140/30
218-01-9 Chrysene 100 115 115 102 102 12 40-140/30
53-70-3 Dibenzo(a,h)anthracene 100 131 131 117 117 11 40-140/30
206-44-0 Fluoranthene 100 108 108 95.8 96 12 40-140/30
86-73-7 Fluorene 100 99.4 99 84.5 85 16 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 100 123 123 110 110 11 40-140/30
91-57-6 2-Methylnaphthalene 100 80.8 81 65.8 66 20 40-140/30
91-20-3 Naphthalene 100 75.2 75 60.5 61 22 40-140/30
85-01-8 Phenanthrene 100 101 101 87.8 88 14 40-140/30
129-00-0 Pyrene 100 110 110 98.3 98 11 40-140/30
C11-C22 Aromatics (Unadj.)1700 1830 108 1600 94 13 40-140/30
C9-C18 Aliphatics 600 412 69 386 64 7 40-140/30
C19-C36 Aliphatics 800 689 86 681 85 1 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 35%* a 34%* a 40-140%
580-13-2 2-Bromonaphthalene 102%95%40-140%
84-15-1 o-Terphenyl 44%39%* a 40-140%
321-60-8 2-Fluorobiphenyl 102%95%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP82688-BS 2-Methylnaphthalene 80.8 ND 0.0%5.0
OP82688-BS Naphthalene 75.2 ND 0.0%5.0
OP82688-BSD 2-Methylnaphthalene 65.8 ND 0.0%5.0
OP82688-BSD Naphthalene 60.5 ND 0.0%5.0
* = Outside of Control Limits.
84 of 101
FA8009888.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82688-BS NN030635.D 1 11/06/20 JA 10/27/20 OP82688 GNN1492
OP82688-BSD NN030636.D 1 11/06/20 JA 10/27/20 OP82688 GNN1492
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
(a) Outside control limits.
* = Outside of Control Limits.
85 of 101
FA8009888.2.1
Duplicate Summary Page 1 of 1
Job Number:FA80098
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP82688-DUP a NN030638.D 10 11/06/20 JA 10/27/20 OP82688 GNN1492
FA79765-43 b NN030637.D 10 11/06/20 JA 10/27/20 OP82688 GNN1492
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
FA79765-43 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 c
208-96-8 Acenaphthylene ND ND nc 30 c
120-12-7 Anthracene ND ND nc 30 c
56-55-3 Benzo(a)anthracene ND ND nc 30 c
50-32-8 Benzo(a)pyrene ND ND nc 30 c
205-99-2 Benzo(b)fluoranthene ND ND nc 30 c
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 c
207-08-9 Benzo(k)fluoranthene ND ND nc 30 c
218-01-9 Chrysene ND ND nc 30 c
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 c
206-44-0 Fluoranthene ND ND nc 30 c
86-73-7 Fluorene ND ND nc 30 c
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 c
91-57-6 2-Methylnaphthalene 92.2 93.0 1 30 c
91-20-3 Naphthalene 323 330 2 30 c
85-01-8 Phenanthrene ND ND nc 30 c
129-00-0 Pyrene ND ND nc 30 c
C11-C22 Aromatics (Unadj.)1400 J 1610 J 14 30 c
C11-C22 Aromatics 987 J 1190 J 19 30 c
C9-C18 Aliphatics 1360 J 1670 J 20 30 c
C19-C36 Aliphatics ND ND nc 30 c
CAS No.Surrogate Recoveries DUP FA79765-43 Limits
3386-33-2 1-Chlorooctadecane 25%* e 24%* d 40-140%
580-13-2 2-Bromonaphthalene 146%* e 144%* d 40-140%
84-15-1 o-Terphenyl 47%45%40-140%
321-60-8 2-Fluorobiphenyl 121%124%40-140%
(a) Dilution required prior to fractionation due to matrix.
(b) Dilution required prior to fractionation due to matrix. Associated MB surrogate recovery outside control
limits. Insufficient sample for reextraction.
(c) Advisory control limits.
(d) Outside control limits due to matrix interference. Confirmed by batch duplicate.
(e) Outside control limits due to dilution.
* = Outside of Control Limits.
86 of 101
FA8009888.3.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 9
87 of 101
FA800989
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20 10/29/20
MB MB
Metal RL IDL MDL raw final raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3
Barium 200 1 1
Beryllium 4.0 .2 .2
Cadmium 5.0 .2 .2
Calcium 1000 50 50
Chromium 10 1 1
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 17 17
Lead 5.0 1 1.1 0.70 <5.0 -0.40 <5.0
Magnesium 5000 35 35
Manganese 15 .5 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 200 200
Selenium 10 2.4 2.9
Silver 10 .7 .7
Sodium 10000 500 500
Strontium 10 .5 .5
Thallium 10 1.1 1.4
Tin 50 .9 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
88 of 101
FA8009899.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20 10/29/20
FA79765-11F QC FA79765-11F Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Cadmium anr
Calcium
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 0.0 0.0 NC 0-20 0.0 466 500 93.2 80-120
Magnesium
Manganese anr
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
89 of 101
FA8009899.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20
FA79765-11F Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Cadmium anr
Calcium
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 0.0 458 500 91.6 1.7 20
Magnesium
Manganese anr
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
90 of 101
FA8009899.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Cadmium anr
Calcium
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 457 500 91.4 80-120
Magnesium
Manganese anr
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
91 of 101
FA8009899.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20 10/29/20
FA79765-11F QC FA79894-1 QC
Metal Original SDL 1:5 %DIF Limits Original SDL 1:5 %DIF Limits
Aluminum
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Cadmium anr
Calcium
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 0.00 0.00 NC 0-10 0.00 0.00 NC 0-10
Magnesium
Manganese anr
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
92 of 101
FA8009899.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20
Sample Final FA79765-11F PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 9.8 10 45.6 0.2 2.5 50 91.2 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
93 of 101
FA8009899.1.5
POST DIGESTATE SPIKE SUMMARY
Login Number: FA80098
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Handy Mart 15; 2495 US 13, Goldsboro, NC
QC Batch ID: MP38048 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/29/20
Sample Final FA79894-1 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 9.8 10 44.8 0.2 2.5 50 89.6 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP38048: FA80098-1, FA80098-2, FA80098-3, FA80098-4
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
94 of 101
FA8009899.1.5
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Scott, LA)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 10
95 of 101
FA8009810
FA80098: Chain of Custody
Page 1 of 3
SGS Scott, LA
96 of 101
FA800981010.1
FA80098: Chain of Custody
Page 2 of 3
97 of 101
FA800981010.1
SGS Sample Receipt Summary
Job Number:FA80098 Client:SGS NORTH AMERICA (FL)
Date / Time Received:10/28/2020 8:40:00 AM Delivery Method:FedEx
Project:HASTY MART
4. No. Coolers:1
Airbill #'s:9231 5381 2730
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
DV441;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (2.9/2.9); DV441
FA80098: Chain of Custody
Page 3 of 3
98 of 101
FA800981010.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
(SGS Scott, LA)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 11
99 of 101
FA8009811
Method Blank Summary Page 1 of 1
Job Number:FA80098
Account:ALSE SGS Orlando, FL
Project:GRINCC: Hasty Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP17582-MB LI130886.D 1 10/30/20 LL 10/30/20 OP17582 GLI1037
The QC reported here applies to the following samples:Method: EPA 504.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.020 0.0038 ug/l
CAS No.Surrogate Recoveries Limits
348-51-6 1-Chloro-2-fluorobenzene 98%70-130%
100 of 101
FA800981111.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA80098
Account:ALSE SGS Orlando, FL
Project:GRINCC: Hasty Mart 15; 2495 US 13, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP17582-BS LI130887.D 1 10/30/20 LL 10/30/20 OP17582 GLI1037
OP17582-BSD LI130888.D 1 10/30/20 LL 10/30/20 OP17582 GLI1037
The QC reported here applies to the following samples:Method: EPA 504.1
FA80098-1, FA80098-2, FA80098-3, FA80098-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
106-93-4 1,2-Dibromoethane 0.251 0.24 95 0.27 107 12 70-130/20
CAS No.Surrogate Recoveries BSP BSD Limits
348-51-6 1-Chloro-2-fluorobenzene 98%99%70-130%
* = Outside of Control Limits.
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FA800981111.2.1

APPENDIX E
June 2020 Site Check Soil Quality Map