HomeMy WebLinkAboutWA-27528_38681_CA_RPTS_20180918_SCH
Speedway LLC
Speedway Office
500 Speedway Drive
Enon, OH 45323
Telephone 937-864-3000
September 12, 2018
Submitted via electronic mail to anna.edwards@ncdenr.gov
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
Division of Waste Management - UST Section
943 Washington Square Mall
Washington, North Carolina 27889
Re: Site Check Report Addendum
Speedway No. 7956
107 South Wilson Street
Fremont, Wayne County, North Carolina
NCDEQ Facility ID No. 0-035993
Dear Ms. Edwards:
Please find attached the Site Check Report Addendum as requested in the North Carolina
Department of Environmental Quality (NCDEQ) correspondence, dated July 13, 2018. Our
environmental consultant, ATC Associates of North Carolina, P.C. (ATC), completed these
activities as a result of the August 18, 2017, Site Check Report, that reported soil concentrations
of xylenes, naphthalene, and C5-C8 Aliphatics greater than their respective Soil-to-Groundwater
Maximum Contaminant Concentrations (MSCC) in boring SB-01. This boring was installed near
the spill bucket end of the premium unleaded tank due to its spill bucket failing its hydrostatic
test on June 8, 2017.
Upon request from the NCDEQ, ATC oversaw ARM Environmental (ARM) install an additional
boring, identified as SB-02, adjacent to the boring SB-01, in order to collect a groundwater
sample. The location of borings SB-01 and SB-02 is provided in Figure 2. Prior to breaking
ground, the area was investigated for potential underground utilities and then cleared using a
soft-dig (air knife) technology to a depth of six feet bls. After clearing the well location, ARM
installed boring SB-02 using direct push technology to a depth of 15 feet below land surface
(bls). A temporary well was constructed of one-inch diameter schedule-40 polyvinyl chloride
(PVC) riser with 10 feet of 0.010-inch slotted screen. The borehole annulus was backfilled with
No. 2 sand filter pack. The well casing and screen were removed from the ground once the
groundwater samples were obtained.
Using a water level indicator, ATC measured the depth to groundwater to be 6.09 feet bls in boring
SB-02. Subsequently, a groundwater sample was collected from the boring; placed in laboratory-
supplied, preserved containers; entered into chain-of-custody; placed on ice; and shipped via
FedEx to ESC Lab Sciences (ESC) [12065 Lebanon Road, Mt. Juliet, Tennessee 37122, North
Carolina Laboratory Certification Number ENV375/DW21704/BI0041, (615) 758-5858] for
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
Page 2
analysis of volatile organics by EPA Method 6200B, MADEP VPH, Lead by Method 6010B and
low level ethylene dibromide (EDB) by EPA Method 501.4. Laboratory analytical results
detected concentration of benzene, ethylbenzene, total xylenes, naphthalene, lead, and C5-C8
and C9-C12 Aliphatics greater than their respective 2L Groundwater Standards; however, no
analytes were detected greater than their respective gross contaminant levels (GCLs).
Groundwater analytical results are summarized in Table 2, and the groundwater analytical report
is located in Appendix A.
As a result of groundwater concentrations existing greater than their respective 2L Standards, it
is anticipated that a Limited Site Assessment will be required by the NCDEQ to confirm these
groundwater concentrations and determine groundwater receptors. If you have any questions
or require additional information, please contact me at 937-863-6507 or by email at
bmwitt@speedway.com.
Sincerely,
Speedway LLC
Bryan M. Witt
Environmental Representative
Attachments
cc: ATC Associates of North Carolina, P.C., 7606 Whitehall Executive Center Drive, Suite 800, Charlotte, NC 28273
7606 Whitehall Executive Center Drive
Suite 800
Charlotte, North Carolina 28273
Tel: 704.529.3200
Fax: 704.529.3272
www.atcgroupservices.com
N.C. Engineering License No. C-1598
September 12, 2018
Submitted via electronic mail to anna.edwards@ncdenr.gov
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
Division of Waste Management - UST Section
943 Washington Square Mall
Washington, North Carolina 27889
Re: Site Check Report Addendum
Speedway No. 7956
107 South Wilson Street
Fremont, Wayne County, North Carolina
Facility ID No. 0-035993
Dear Ms. Edwards:
On behalf of Speedway LLC (Speedway), ATC Associates of North Carolina, P.C. (ATC) has
completed a Site Check Report Addendum for the above-referenced facility in response to the
North Carolina Department of Environmental Quality (NCDEQ) request, dated July 13, 2018, for
further information after its review of the Site Check Report, dated August 18, 2017. The Site
Check Report was completed following a spill bucket test failure in accordance with the United
States Environmental Protection Agency (EPA) “Revising Underground Storage Tank
Regulations” dated July 15, 2015.
On June 9, 2017, Speedway LLC (Speedway) submitted NCDEQ Form UST-17A, which
documented a suspected release at the above referenced site due to the premium unleaded
spill bucket failing its hydrostatic test on June 8, 2017. On July 7, 2017, Speedway submitted
NCDEQ Form UST-17B that included the failed hydrostatic test results. On July 20, 2017, the
spill bucket was replaced by TideLand Construction & Petroleum.
On July 24, 2017, ATC Associates of North Carolina, P.C. (ATC), used a hand auger to
complete a soil boring (identified as SB-01) to 13 feet below land surface (bls) near the spill
bucket end of the premium unleaded tank. The soil sample was placed in laboratory-supplied
containers, entered into chain-of-custody control, placed on ice, and shipped via FedEx to ESC
Lab Sciences (ESC) [12065 Lebanon Road, Mt. Juliet, Tennessee 37122, North Carolina
Laboratory Certification Number ENV375/DW21704/BI0041, (615) 758-5858] for benzene,
toluene, ethylbenzene, total xylenes (BTEX), methyl tert-butyl ether (MTBE), and naphthalene
analysis by Environmental Protection Agency (EPA) Method 6200B, and Massachusetts
Department of Environmental Protection (MADEP) Method for volatile petroleum hydrocarbons
(VPH). Laboratory analytical results detected concentrations of xylenes, naphthalene, and C5-
C8 Aliphatics greater than their respective Soil-to-Groundwater Maximum Contaminant
Concentrations (MSCC). The soil sample analytical results from the original site check activities
are provided in Table 1.
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
Speedway submitted the Site Check and the Form UST-61 to the NCDEQ on August 18, 2017.
On July 13, 2018, the NCDEQ requested additional information be gathered regarding the site
groundwater and be presented in a Site Check Report Addendum.
Groundwater Sample Collection
On August 6, 2018, ATC oversaw ARM Environmental (ARM) install an additional soil boring,
identified as SB-02, adjacent to boring SB-01 for groundwater sample collection purposes. The
location of soil borings SB-01 and SB-02 are provided in Figure 2. Prior to breaking ground, the
area was investigated for potential underground utilities and then cleared using a soft-dig (air
knife) technology to a depth of six feet bls. After clearing the well location, ARM installed soil
boring SB-02 using direct push technology to a depth of 15 feet bls. A temporary well was
constructed of one-inch diameter schedule-40 polyvinyl chloride (PVC) riser with 10 feet of
0.010-inch slotted screen. The borehole annulus was backfilled with No. 2 sand filter pack. The
well casing and screen were removed from the ground once the groundwater samples were
obtained.
Using a water level indicator, ATC measured the depth to groundwater to be 6.09 feet bls in boring
SB-02. Subsequently, a groundwater sample was collected from the boring; placed in laboratory-
supplied, preserved containers; entered into chain-of-custody; placed on ice; and shipped via
FedEx to ESC Lab Sciences (ESC) [12065 Lebanon Road, Mt. Juliet, Tennessee 37122, North
Carolina Laboratory Certification Number ENV375/DW21704/BI0041, (615) 758-5858] for
analysis of volatile organics by EPA Method 6200B, MADEP VPH, Lead by Method 6010B, and
low level ethylene dibromide (EDB) by EPA Method 501.4. Laboratory analytical results
detected concentration of benzene, ethylbenzene, total xylenes, naphthalene, lead, and C5-C8
and C9-C12 Aliphatics greater than their respective 2L Groundwater Standards; however, no
analytes were detected greater than their respective gross contaminant levels (GCLs).
Groundwater analytical results are summarized in Table 2, and the groundwater analytical report
is located in Appendix A.
As a result of groundwater concentrations existing greater than their respective 2L Standards, it
is anticipated that a Limited Site Assessment will be required by the NCDEQ to confirm these
groundwater concentrations and determine groundwater receptors. Should you have any
questions or require additional information, please contact me or Bob Bolton. I can be reached
at 757-467-2100 and by email at donald.hurdle@atcgs.com, and Bob may be reached at 803-
753-0003 or by email at bob.bolton@atcgs.com.
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
Sincerely,
ATC ASSOCIATES OF NORTH CAROLINA, P.C.
Attachments
Bob Bolton Donald T. Hurdle, P.G.
Senior Project Manager Project Manager
for ATC Group Services LLC for ATC Group Services LLC
Direct Line +1 803.223.0793 Direct Line +1 757.467.2100
Email: bob.bolton@atcgs.com Email: donald.hurdle@atcgs.com
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
TABLES
BenzeneTolueneEthylbenzeneTotal XylenesTotal BTEXNaphthaleneMethyl tert-butyl ether (MTBE)C5-C-8 AliphanticsC9-C12 AliphanticsC9-C-19 Aliphantics0.0056 4.3 4.9 4.6 ---0.16 0.091 68 540 31
18 1,200 1,560 3,129 ---313 350 939 1,500 469
164 32,000 40,000 81,760 ---8,176 3,100 24,528 40,000 12,268
SB-01 13 7/24/17 1726.0 <0.209 <1.05 3.5500 12.5 16.0500 1.55 <0.209 346 177 85.9
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. The MADEP VPH values were obtained from Table 10 in the "Guidelines for Assessment and corrective Action for UST Releases, dated July 15, 2008, updated October 2012.
3. MSCCs = Maximum Soil Contaminant Concentration
4. Italics type denotes concentration equals or exceeds Soil-to-Groundwater MSCCs.
5. BOLD type denotes concentration equals or exceeds Residential MSCCs.
6. BOLD/Underline denotes concentration equals or exceeds Industrial/Commercial MSCCs.
7. "<" denotes compound not detected above laboratory method detection limit.
8. NA = Not Analyzed
9. J value denotes estimated concentration by the laboratory.
NCDEQ FACILITY ID NO. 0-035993
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP795602
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
SPEEDWAY NO. 7956
103 SOUTH WILSON STREET
FREMONT, WAYNE COUNTY, NORTH CAROLINA
MADEP Method for VPH (mg/kg)
Soil-to-Groundwater MSCCs
Residential MSCCs
Industrial/Commercial MSCCs
Soil Sample ID Sample
Depth (feet)
Sampling
Date
PID Reading
Parts Per Million
(ppm)
EPA Method 8260
EPA
Method
504.1
EPA
Method
6010B
BenzeneTolueneEthylbenzeneTotal XylenesTotal BTEXNaphthaleneMethyl tert-butyl ether (MTBE)1, 2-Dichloroethane (DCA)Di-Isopropyl Ether1,2-DibromoethaneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AliphaticsTotal VPH1 600 600 500 ---6 20 0.4 70 0.02 15.00 400 700 200 ---
5,000 260,000 84,500 85,500 ---6,000 20,000 400 70,000 50 15,000 NE NE NE NE
SB-02 8/6/18 60.9 512 1,030 3,560 5,162.9 413 <50 <50 <50 <0.01 360 12,300 10,800 <5,000 28,000
Notes:
1. Concentrations reported in micrograms per liter (ug/L).
2. Italics type denotes concentration equals or exceeds - 2L Standard
3. BOLD/Underline denotes concentration equals or exceeds - GCL = Gross Contaminant Level
4. "<" denotes compound not detected above laboratory method detection limit.
5. J value denotes estimated concentration by the laboratory.
6. NA - Not Analyzed.
7. BDL - Below Laboratory Detection Limits.
2L Standard
GCL
EPA Method 6200B
Groundwater
Sample ID
Sampling
Date
MADEP Method for VPH
TABLE 2
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
SPEEDWAY NO. 7956
103 SOUTH WILSON STREET
FREMONT, WAYNE COUNTY, NORTH CAROLINA
NCDEQ FACILITY ID NO. 0-035993
ATC GROUP SERVICES OF NORTH CAROLINA, P.C. PROJECT NO. SWDP795602
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
FIGURES
N
SITE
LOCATION
SITE LOCATION MAP
DATE:PROJECT NO.:
SCALE:
FIGURE 1
DRAWN BY:
REVIEWED BY:CHARLOTTE, NORTH CAROLINA 28217
PHONE: (704) 529-3200 FAX: (704) 529-3272
ASSOCIATES OF NORTH CAROLINA, P.C.
SOUTH WILSON STREETEAS
T
W
A
Y
N
E
S
T
R
E
E
T
FIGURE 2
PROJECT NO.:
DRAWN BY:
REVIEWED BY:
DATE:
SCALE:
SITE MAP
N
CHARLOTTE, NORTH CAROLINA 28217
PHONE: (704) 529-3200 FAX: (704) 529-3272
ASSOCIATES OF NORTH CAROLINA, P.C.
Ms. Anna Edwards
North Carolina Department of Environmental Quality
Washington Regional Office
September 12, 2018
APPENDIX A
ANALYTICAL REPORT
August 20, 2018
ATC Group Services - NC Speedway
Sample Delivery Group:L1015573
Samples Received:08/08/2018
Project Number:SW-7956
Description:SW 7956 107 S. Wilson Street
Site:0007956
Report To:Bob Bolton
7606 Whitehall Executive Ctr Ste 800
Charlotte, NC 28273
Entire Report Reviewed By:
August 20, 2018
[Preliminary Report]
John Hawkins
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
August 20, 2018
John Hawkins
Project Manager
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SB-02 L1015573-01 5
Qc: Quality Control Summary 6
Metals (ICP) by Method 6010D 6
Volatile Petroleum Hydrocarbons by Method MADEPV 7
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 8
EDB / DBCP by Method 8011 9
Gl: Glossary of Terms 10
Al: Accreditations & Locations 11
Sc: Sample Chain of Custody 12
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-02 L1015573-01 GW Frank Beecher 08/06/18 18:30 08/08/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010D WG1152355 1 08/15/18 08:25 08/15/18 11:11 TRB
Volatile Petroleum Hydrocarbons by Method MADEPV WG1149591 50 08/08/18 20:20 08/08/18 20:20 LRL
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG1149932 50 08/09/18 13:03 08/09/18 13:03 AB
EDB / DBCP by Method 8011 WG1149116 1 08/09/18 14:33 08/09/18 20:39 HMH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
John Hawkins
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SW-7956 L1015573 08/20/18 15:42 4 of 14
John Hawkins
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Speedway SW-7956 L1015573 08/20/18 17:18 4 of 14
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1015573
SB-02
Collected date/time: 08/06/18 18:30
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead 360 5.00 1 08/15/2018 11:11 WG1152355
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 12300 5000 50 08/08/2018 20:20 WG1149591
Unadjusted C9-C12 Aliphatics 10800 5000 50 08/08/2018 20:20 WG1149591
Unadjusted C9-C10 Aromatics ND 5000 50 08/08/2018 20:20 WG1149591
Total VPH 28000 5000 50 08/08/2018 20:20 WG1149591
(S) 2,5-Dibromotoluene(FID)110 70.0-130 08/08/2018 20:20 WG1149591
(S) 2,5-Dibromotoluene(PID)85.5 70.0-130 08/08/2018 20:20 WG1149591
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzene 60.9 50.0 50 08/09/2018 13:03 WG1149932
1,2-Dichloroethane ND 50.0 50 08/09/2018 13:03 WG1149932
Di-isopropyl ether ND 50.0 50 08/09/2018 13:03 WG1149932
Ethylbenzene 1030 50.0 50 08/09/2018 13:03 WG1149932
Methyl tert-butyl ether ND 50.0 50 08/09/2018 13:03 WG1149932
Naphthalene 413 250 50 08/09/2018 13:03 WG1149932
Toluene 512 50.0 50 08/09/2018 13:03 WG1149932
Total Xylenes 3560 150 50 08/09/2018 13:03 WG1149932
(S) Toluene-d8 99.5 80.0-120 08/09/2018 13:03 WG1149932
(S) Dibromofluoromethane 94.3 76.0-123 08/09/2018 13:03 WG1149932
(S) a,a,a-Trifluorotoluene 98.3 80.0-120 08/09/2018 13:03 WG1149932
(S) 4-Bromofluorobenzene 97.4 80.0-120 08/09/2018 13:03 WG1149932
EDB / DBCP by Method 8011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide ND 0.0100 1 08/09/2018 20:39 WG1149116
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1152355
Metals (ICP) by Method 6010D L1015573-01
Method Blank (MB)
(MB) R3333835-1 08/15/18 10:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead U 1.90 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3333835-2 08/15/18 10:27 • (LCSD) R3333835-3 08/15/18 10:29
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Lead 1000 992 989 99.2 98.9 80.0-120 0.355 20
L1017463-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1017463-04 08/15/18 10:32 • (MS) R3333835-5 08/15/18 10:37 • (MSD) R3333835-6 08/15/18 10:39
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Lead 1000 ND 976 984 97.6 98.4 1 75.0-125 0.797 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1149591
Volatile Petroleum Hydrocarbons by Method MADEPV L1015573-01
Method Blank (MB)
(MB) R3332214-3 08/08/18 12:23
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID)106 70.0-130
(S) 2,5-Dibromotoluene(PID)83.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3332214-1 08/08/18 10:26 • (LCSD) R3332214-2 08/08/18 11:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1450 1440 121 120 70.0-130 0.850 25
Unadjusted C9-C12 Aliphatics 1400 1710 1710 122 122 70.0-130 0.0584 25
Unadjusted C9-C10 Aromatics 200 198 189 99.1 94.4 70.0-130 4.79 25
Total VPH 2800 3360 3340 120 119 70.0-130 0.567 25
(S) 2,5-Dibromotoluene(FID) 110 110 70.0-130
(S) 2,5-Dibromotoluene(PID) 88.3 86.3 70.0-130
L1015573-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1015573-01 08/08/18 20:20 • (MS) R3332214-4 08/08/18 20:59 • (MSD) R3332214-5 08/08/18 21:37
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 12300 76100 75300 106 105 50 70.0-130 1.06 25
Unadjusted C9-C12 Aliphatics 1400 10800 91700 93400 116 118 50 70.0-130 1.84 25
Unadjusted C9-C10 Aromatics 200 ND 12300 12600 73.8 77.1 50 70.0-130 2.71 25
Total VPH 2800 28000 180000 181000 109 109 50 70.0-130 0.664 25
(S) 2,5-Dibromotoluene(FID) 109 111 70.0-130
(S) 2,5-Dibromotoluene(PID) 84.8 86.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1149932
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L1015573-01
Method Blank (MB)
(MB) R3332440-3 08/09/18 10:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
1,2-Dichloroethane U 0.361 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
Toluene U 0.412 1.00
Xylenes, Total U 1.06 3.00
(S) a,a,a-Trifluorotoluene 99.5 80.0-120
(S) Toluene-d8 101 80.0-120
(S) Dibromofluoromethane 93.0 76.0-123
(S) 4-Bromofluorobenzene 98.1 80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3332440-1 08/09/18 09:07 • (LCSD) R3332440-4 08/09/18 10:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 24.0 23.6 96.1 94.2 69.0-123 2.02 20
1,2-Dichloroethane 25.0 22.8 22.2 91.3 88.7 67.0-126 2.85 20
Di-isopropyl ether 25.0 25.6 24.9 102 99.5 59.0-133 2.74 20
Ethylbenzene 25.0 25.9 24.7 103 98.8 77.0-120 4.58 20
Methyl tert-butyl ether 25.0 25.3 24.0 101 96.0 64.0-123 5.26 20
Naphthalene 25.0 20.1 18.8 80.4 75.3 62.0-128 6.58 20
Toluene 25.0 24.8 24.3 99.0 97.2 77.0-120 1.87 20
Xylenes, Total 75.0 76.2 75.0 102 100 77.0-120 1.59 20
(S) a,a,a-Trifluorotoluene 98.8 99.1 80.0-120
(S) Toluene-d8 99.3 99.6 80.0-120
(S) Dibromofluoromethane 94.4 95.0 76.0-123
(S) 4-Bromofluorobenzene 98.0 97.8 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1149116
EDB / DBCP by Method 8011 L1015573-01
Method Blank (MB)
(MB) R3332670-1 08/09/18 18:22
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ethylene Dibromide U 0.00240 0.0100
L1014947-07 Original Sample (OS) • Duplicate (DUP)
(OS) L1014947-07 08/09/18 19:12 • (DUP) R3332670-3 08/09/18 18:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Ethylene Dibromide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3332670-4 08/09/18 21:15 • (LCSD) R3332670-5 08/09/18 23:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ethylene Dibromide 0.250 0.247 0.248 98.8 99.2 60.0-140 0.404 20
L1014947-08 Original Sample (OS) • Matrix Spike (MS)
(OS) L1014947-08 08/09/18 18:47 • (MS) R3332670-2 08/09/18 18:34
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ethylene Dibromide 0.100 ND 0.113 113 1 72.0-146
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T 104704245-17-14
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS
¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 1
TURN AROUND TIME
STANDARD
Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210007956 Facility ID 0-035993
Address:Po Box 666
City:Fremont State:NC
Phone #:O:937-863-3000 x6507 Fax #:Fax: 937-863-6078
Speedway Proj. Mgr: Mr Bryan Matthew Witt **INVOICE TO SPEEDWAY**
AFE #:170124 Work Order #:1102366210
COC ID # 00049498
Lab Information
Lab:Environmental Science Corporation
Consultant:ATC Group Services - Columbia, SC
Project Mgr: Mr Bob Bolton
Address:7499 Parklane Road Suite 112 Columbia, South Carolina 29223
Phone #:O:803-735-0003 x Fax #:Fax: 803-735-0443
Sampler:Frank Beecher
Shipped:FedExp
Tracking #:449262207360
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
SB-02 08/06/2018 06:30pm W 5 40 MIL AMBER VIAL HCL EDB 504.1
40 MIL AMBER VIAL HCL 6200B 6200B
40 ML AMBER VOA MEOH/NAHSO4MADEP VPH MADEP VPH
250 ML HNO3 EPA Method 6010B - LEAD 6010B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/1 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 49498 Printed: 10/05/2018
Analysis Name: 6200B ( Water )
Analysis Description / Method:BTEX, MTBE, Naphthalene, IPE, 1,2-DCA / 6200B
Container Type / Preservative:40 MIL AMBER VIAL / HCL
Analytes: 1,2-Dichloroethane ug/L, Benzene ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Methyl tert butyl ether ug/L, Naphthalene ug/L, Toluene ug/L, Total Xylenes ug/L
Analysis Name: EDB ( Water )
Analysis Description / Method:EDB 504.1 / 504.1
Container Type / Preservative:40 MIL AMBER VIAL / HCL
Analytes: Dibromoethane ug/L
Analysis Name: EPA Method 6010B - LEAD ( Water )
Analysis Description / Method:EPA Method 6010B - LEAD / 6010B
Container Type / Preservative:250 ML / HNO3
Analytes: Lead ug/L
Analysis Name: MADEP VPH ( Water )
Analysis Description / Method:MADEP VPH / MADEP VPH
Container Type / Preservative:40 ML AMBER VOA / MEOH/NAHSO4
Analytes: C5-C8 aliphatics (unadjusted) ug/L, C9-C10 Aromatics ug/L, C9-C12 Aliphatics ug/L
Speedway LLC.1/1 https://www.speedway-ids.com