Loading...
HomeMy WebLinkAboutWA-27119_38285_CA_RPTS_20140801_MRP Environment Prepared for 7-Eleven Dallas, Texas Prepared by AECOM Raleigh, NC 60263455 August 2014 Groundwater Monitoring Report and Closure Request 7-Eleven Store No. 19847 1610 S. Croatan Highway Kill Devil Hills, North Carolina Incident # 38285 AECOM Environment i 60263455 August 2014 Executive Summary ............................................................................................................................................................. ES-1  1 Introduction ......................................................................................................................................................................... 1-1  2 Site Information ................................................................................................................................................................... 2-1  2.1 Site Identification .......................................................................................................................................................... 2-1  2.2 Contact Information ...................................................................................................................................................... 2-1  2.3 Information about the Release ..................................................................................................................................... 2-1  3 Site History and Characterization ...................................................................................................................................... 3-1  3.1 Underground Storage Tank Systems ........................................................................................................................... 3-1  3.2 Aboveground Storage Tank Systems ........................................................................................................................... 3-1  3.3 Historical Release Information ...................................................................................................................................... 3-1  3.4 Site Characteristics and Land Use ............................................................................................................................... 3-1  3.5 Site Geology and Hydrogeology ................................................................................................................................... 3-2  3.6 Current Status of Remediation ..................................................................................................................................... 3-2  4 Field Activities ..................................................................................................................................................................... 4-1  4.1 Groundwater Sampling ................................................................................................................................................. 4-1  4.2 Water Supply Well Sampling ........................................................................................................................................ 4-1  5 Results ................................................................................................................................................................................. 5-1  5.1 Gauging Results ........................................................................................................................................................... 5-1  5.2 Groundwater Sampling Results .................................................................................................................................... 5-1  5.3 Private Water Well Sampling Results ........................................................................................................................... 5-1  5.4 Soil Sampling Results .................................................................................................................................................. 5-1  6 Discussion and Conclusions ............................................................................................................................................. 6-1  7 References ........................................................................................................................................................................... 7-1  List of Appendices Appendix A. Notice of Regulatory Requirements Appendix B. Laboratory Analytical Results Table of Contents AECOM Environment ii 60263455 August 2014 List of Tables Table 3-1. (Reporting Table B-2) Site History – UST Owner/Operator and Other Responsible party Information Table 3-2. (Reporting Table B-1) Site History – UST/AST System and Other Release Information Table 3-3. (Reporting Table B-5) Public and Private Water Supply Wells and Other Receptor Information Table 4-1. (Reporting Table B-7) Monitoring and Remediation Well Construction Information Table 5-1. (Reporting Table B-4) Summary of Groundwater Sampling Results Table 5-2. (Reporting Table B-3) Summary of Soil Sampling Results List of Figures Figure 1-1. Site Location Map Figure 1-2. Site Map Figure 3-1. Private Well Location Map Figure 3-2. Utility Location Map Figure 5-1. Groundwater Elevation Map, August 5, 2014 Figure 5-2. Dissolved Benzene Isoconcentration Map, August 5, 2014 Figure 5-3. Dissolved Ethylbenzene Isoconcentration Map, August 5, 2014 Figure 5-4. Dissolved Toluene Isoconcentration Map, August 5, 2014 Figure 5-5. Dissolved Xylene Isoconcentration Map, August 5, 2014 Figure 5-6. Dissolved Naphthalene Isoconcentration Map, August 5, 2014 Figure 5-7. VPH Distribution Map, August 5, 2014 AECOM Environment iii 60263455 August 2014 List of Acronyms 2L Standard Title 15A North Carolina Administrative Code 2L Groundwater Standard AECOM AECOM North Carolina, Inc. AST aboveground storage tanks bgs below ground surface CSA Comprehensive Site Assessment ESC ESC Lab Sciences ft/ft feet per foot GPS global positioning system NC North Carolina NCDENR North Carolina Department of Environment and Natural Resources Site 7-Eleven Store No. 19847 TX Texas USCS Unified Soil Classification System UST underground storage tank VOCs volatile organic compounds VPH volatile petroleum hydrocarbon µg/L micrograms per liter AECOM Environment ES-1 60263455 August 2014 As required by the North Carolina Department of Environment and Natural Resources in correspondence dated June 5, 2014, AECOM North Carolina, Inc. (AECOM) prepared this Groundwater Monitoring Report for activities conducted at the 7-Eleven Store No. 19847 (Site), located at 1610 S. Croatan Highway, Kill Devil Hills, North Carolina. The Site has been classified as high risk due to the presence of nearby irrigation wells. The site is currently used as a 7-Eleven convenience store only; site underground storage tanks (USTs) were removed in February 2013. During the current investigation, the nine (MW-2R, MW-3R, MW-4 to MW-9, and DW-1) on- and off-site monitoring wells were sampled. Groundwater samples were analyzed for volatile organic compounds (VOCs), Massachusetts Department of Environmental Protection volatile petroleum hydrocarbons (VPH), and lead. During sampling, eight VOC or VPH compounds were detected above their respective Title 15A North Carolina Administrative Code 2L Groundwater Standards (2L Standards) in well MW-3 and/or MW-5: benzene, naphthalene, n-propylbenzene, 1,2,4- trimethylbenzene, total xylenes, C5-C8 aliphatics, C9-C12 aliphatics, and C9-C10 aromatics. No other compounds exceeded the 2L Standards during the August 5, 2014 sampling event. Groundwater concentrations of VOC and VPH compounds in well MW-3 and MW-5 have decreased since the February 2014 sampling event, with most detected compounds in MW-3 decreasing by more than 50 percent. Since August 2012, prior to the removal of the Site USTs, concentrations of benzene, naphthalene, toluene, 1,2,4-trimethylbenzene, total xylenes, and VPH compounds in MW-3 have decreased by more than an order of magnitude. The groundwater flow direction during the August 5, 2014 event was to the east, with a gradient of approximately 0.003 feet per foot. This is consistent with historical observations of site groundwater flow. AECOM attempted to contact two nearby property owners to sample their irrigation wells. The property owner at 1617 Wrightsville Avenue refused access. AECOM was unable to successfully contact the property owner at 1620 S. Memorial Boulevard. Based on the delineation of the plume, declining concentrations in MW-3 and MW-5, removal of the source of petroleum, and the location of the nearest irrigation well 250 feet or more from the Site, AECOM, on behalf of 7-Eleven, requests closure. Executive Summary AECOM Environment 1-1 60263455 August 2014 As required by the North Carolina Department of Environment and Natural Resources (NCDENR) in correspondence dated June 5, 2014 (also included in Appendix A), AECOM North Carolina, Inc. (AECOM) conducted a site-wide groundwater monitoring event at the 7-Eleven Store No. 19847 (Site), located at 1610 S. Croatan Highway, Kill Devil Hills, North Carolina (NC) (Figure 1-1 and Figure 1-2). A release was discovered during the in-place abandonment of underground storage tank (UST) #2 on April 10, 2012 (AECOM, 2012a). An Initial Abatement Action Report (AECOM, 2012b), a Limited Site Assessment (AECOM, 2012c), a UST closure report (AECOM, 2013a), and a Comprehensive Site Assessment (CSA) (AECOM, 2013b) have been completed at the Site. 1 Introduction AECOM Environment 2-1 60263455 August 2014 The following sections provide site background and contact information. 2.1 Site Identification  Date of Incident Report: April 11, 2012  Facility ID: 0-011788 Incident Number: 38285 Site Risk Classification: High  Site Rank: H 162 D  Site Name: 7-Eleven Store No. 19847  Site Street Address: 1610 S. Croatan Highway (Note: the Site is identified as 1601 S. Croatan Highway in the Dare County geographic information system mapper, available online at http://daregis.darenc.com/website/dare/viewer.htm.)  City/Town: Kill Devil Hills Zip Code: 27948 County: Dare  Description of Geographical Data Point (e.g., dispenser): UST fill port  Location Method (global positioning system [GPS], topographical map, other): GPS  Latitude (decimal degrees): 35.9986°, Longitude (decimal degrees): 75.6513° 2.2 Contact Information  UST Owner: 7-Eleven, Inc., Address: 1722 Routh Street, Dallas, Texas (TX), Telephone: (972) 828-0711  UST Operator: 7-Eleven, Inc., Address: 1610 S. Croatan Highway, Kill Devil Hills, NC, Telephone: (252) 441-4549  Property Owner: 7-Eleven, Inc. Employees’ Trust, c/o Evercore Trust Company, Address: 601 South Figueroa Street, 44th Floor, Los Angeles, California 90017, Telephone: (213) 443-2626  Property Occupant: 7-Eleven,Inc., Address: 1722 Routh Street, Dallas, TX, Telephone: (972) 828-0711  Consultant/Contractor: AECOM North Carolina, Inc., Address: 701 Corporate Center Drive, Suite 475, Raleigh NC 27607, Telephone: (919) 854-6200  Analytical Laboratory: ESC Lab Sciences (ESC), State Certification No. ENV375/DW21704, Address: 12065 Lebanon Pike, Mount Juliet, Tennessee (TN) 37122, Telephone: (615) 758-5858 2.3 Information about the Release After removing the UST #2 from service in May 2011 due to false leak detection warnings, 7-Eleven decided to abandon the #2 gasoline UST tank in place. On April 10, 2012, strong petroleum odors were observed during the installation of two soil borings, one of which was converted into a groundwater monitoring well. A suspected release was reported to NCDENR on April 11, 2012. The release was confirmed with the receipt of analytical data, received April 18, 2012. In February 2013, the three USTs were removed, including UST #2. Petroleum odors and soil staining were observed, and a sheen of non-aqueous phase liquid was observed in the tank field following the removal of the USTs. Pinhole leaks were observed in the walls of the fiberglass USTs. 2 Site Information AECOM Environment 3-1 60263455 August 2014 The following sections provide information on the USTs operated at the Site and follows the general outline established in Guidelines for Assessment and Corrective Action for UST Releases. 3.1 Underground Storage Tank Systems UST owner operator and other responsible party information are provided in Table 3-1. A summary of current and former USTs maintained at the Site is provided below and summarized in Table 3-2. Three 10,000-gallon USTs were installed on-site in 1985. UST #2 was removed from service in May 2011 due to false leak detection warnings, and was abandoned in place on April 10, 2012. A suspected release was reported to NCDENR on April 11, 2012. The three USTs were removed from the Site on February 6, 2013. The USTs were single-walled fiberglass, with single-walled fiberglass piping and under dispenser containment. Since installation, the USTs contained gasoline. At the time of removal, pinhole leaks were observed in the side of the USTs. Based on observations made during the February 2013 tank removal, all three of the USTs may have contributed to the release. AECOM has not conducted previous (pre-2012) investigations at this site. No reports of previous site investigations (pre-2012) are known. 3.2 Aboveground Storage Tank Systems No aboveground storage tank systems (ASTs) are currently present on-site. Based on available information, no ASTs have historically been present at the Site. 3.3 Historical Release Information No historical releases, prior to the release discovered during the 2012 UST abandonment activities, are known. 3.4 Site Characteristics and Land Use The location of the Site is shown on a portion of the United States Geological Survey 7.5-minute topographic map of the Kill Devil Hills, NC (1984) Quadrangle (Figure 1-1). The layout of the Site is found on Figure 1-2. The layout of the Site is found on Figure 1-2. The Site is currently an active 7-Eleven convenience store located on the east side of South Croatan Highway (US-158). The majority of the Site is occupied by the 7-Eleven building and paved parking area, with some grassy area along the southern side of the Site. A drainage ditch is located along the west side of the Site. The Site and surrounding properties are located within the Town of Kill Devil Hills and Dare County. Use of the Site and surrounding properties is consistent with business and residential areas in an urban setting. The Site and properties located within the Town of Kill Devil Hills generally receive municipal water from the Town of Kill Devil Hills, which receives its water from Dare County Water Department. Properties located within Dare County receive municipal water from Dare County or private wells. No potable wells have been identified within 1,500 feet of the Site (AECOM, 2012b), and municipal water (from the Town of Kill Devil Hills) is available to properties within 1,500 feet of the Site. Two irrigation wells have been identified within 500 feet of the Site: 3 Site History and Characterization AECOM Environment 3-2 60263455 August 2014  1617 Wrightsville Avenue (approximately 250 feet southeast of the tank field) – The well was installed in 2000 to a depth of 75 feet below ground surface (bgs) and is used for irrigation. Based on site reconnaissance, the well may be located in a small structure adjacent to the residence; however, the well location could not be confirmed as the resident was not at home during the site reconnaissance. The approximate location of the structure is shown on Figure 3-1.  1620 South Memorial Boulevard (approximately 400 feet southeast of the tank field) – The well was installed in 2001 to a depth of 50 feet bgs and is used for irrigation. No well-related structures were identified during the February 2013 reconnaissance; a presumed location of the well is shown on Figure 3-1. Two additional irrigation wells were identified within 1,000 feet of the Site based on information provided by Mr. Charles Spry (owner of 1617 Wrightsville Avenue) and confirmed by discussions with representatives of the property owners. One irrigation well is present at Nags Head Hammocks, located at 1801 Croatan Highway and approximately 750 feet cross-gradient from the Site, and one irrigation well is present at Wings, located at 1405 S. Croatan Highway and approximately 650 feet cross- gradient of the Site. The information on private wells is summarized on Table 3-3. 3.5 Site Geology and Hydrogeology The Site is located within the Coastal Plain physiographic province. Based on observations made during the installation of the six site monitoring wells, subsurface soils consist predominantly of brown to gray fine sand (Unified Soil Classification System [USCS] symbol SP) to 20 feet bgs. A layer of poorly sorted sand (USCS symbol SW) was observed at deep well DW-1 from a depth of 20-25 feet, below which brown-gray fine sand continued to a depth of 53 feet. A gray clay layer containing shell material (USCS symbol CL) was encountered from 53-54 feet. Below the clay layer, the brown-gray fine sand continued until the monitoring well boring was terminated at 70 feet bgs. Petroleum odors and elevated photo ionization detector readings were noted during the installation of MW-5 and DW-1. No odor, staining, or other evidence of petroleum contamination was observed during the installation of wells MW-2R and MW-6, located north and west of the tank field, respectively. The Site topography is generally flat. Historically, groundwater has been encountered between roughly 1.5 feet bgs and 4.5 feet bgs. Aquifer testing was attempted in August 2013 during the CSA phase, but was not completed due to the quick recharge of the Site monitoring wells. Based on Site lithology and literature values, the hydraulic conductivity of the surficial aquifer was estimated to be approximately 0.0032 centimeters per second or 9 feet per day (AECOM, 2013b). Assuming the shallow wells to be fully penetrating (aquifer thickness of 12 feet) and using aforementioned literature value for hydraulic conductivity, the calculated transmissivity is 1.17 centimeters squared per second or 108 square feet per day. Groundwater flow was determined to be eastward toward the Atlantic Ocean. The hydraulic gradient was approximately 0.003 feet per foot (ft/ft) in August 2014. Based on liquid level data, it appears that the gradient flattens out across the former tank field, which is likely related to the presence of fill material. 3.6 Current Status of Remediation To address the subsurface contamination, 102,617 gallons of petroleum-impacted water was removed from the tank field wells and well MW-3 and 351.69 tons of petroleum-impacted soils were removed from the subsurface. These initial abatement measures were conducted with approval from NCDENR during UST removal. The following post-excavation activities have been conducted at the Site as part of the groundwater monitoring investigation:  In October 2012, monitoring well MW-3 was over-drilled and replaced with a 4-inch diameter well.  In July 2013, monitoring wells MW-2R and MW-6 were installed to replace monitoring wells MW-1 and MW-2, which were destroyed during the UST removal.  In July 2013, monitoring wells MW-5 and DW-1 were installed to further characterize site groundwater conditions.  In May 2014, monitoring wells MW-7 to MW-9 were installed off-site. AECOM Environment 4-1 60263455 August 2014 Site activities were conducted in accordance with the Region 4 United States Environmental Protection Agency (EPA) Environmental Investigations Standard Operating Procedures and Quality Manual. 4.1 Groundwater Sampling A groundwater sample was collected from each of the nine site groundwater monitoring wells (MW-2R to MW-9 and DW-1) on August 5, 2014. Prior to sampling, each well was gauged using an oil/water interface probe. Figure 1-2 shows the monitoring well locations. The elevation summary for the wells is provided in Table 4-1. Dedicated disposable bailers were used to purge and sample monitoring wells MW-2R to MW-6. Due to the depth of monitoring well DW-1, a monsoon pump was used to purge the well, and a dedicated disposable bailer was used to sample the well. Three well volumes were purged from each monitoring well prior to sample collection. The purging was performed on all wells prior to any sampling activities. Sampling occurred in the same order as purging to allow groundwater turbidity in each well to reduce prior to sample collection. Groundwater samples were analyzed for volatile organic compounds (VOCs) via EPA Method SM 6200B and Massachusetts Department of Environmental Protection volatile petroleum hydrocarbon (VPH). Samples were sent to ESC of Mt. Juliet, TN for analysis. 4.2 Water Supply Well Sampling NCDENR correspondence dated June 5, 2014 required the sampling of the two water supply wells identified within 500 feet of the Site (1617 Wrightsville Avenue and 1620 South Memorial Boulevard). As previously documented, the property owner at 1617 Wrightsville Avenue has refused access to sample the well. Prior to the February 2014 sampling event, the property owner at 1620 South Memorial Boulevard indicated willingness to allow the well to be sampled, but stated that the well was off due to winterization of the house. The property owner at 1620 South Memorial Boulevard could not be reached prior to the August 2014 groundwater sampling event to confirm the well’s operational status and permission to sample the well. No private wells were sampled during the August 2014 sampling event. 4 Field Activities AECOM Environment 5-1 60263455 August 2014 5.1 Gauging Results On August 5, 2014, groundwater was encountered between 1.33 feet bgs (MW-9) to 3.27 feet bgs (DW-1). Groundwater flow was estimated to be toward the east, with a gradient of approximately 0.003 ft/ft (Figure 5-1). Groundwater gauging data and monitoring well details are summarized on Table 4-1. 5.2 Groundwater Sampling Results The following compounds were detected above their Title 15A North Carolina Administrative Code 2L Groundwater Standard (2L Standard) in one or more wells:  Benzene exceeded its 2L Standard of 1 microgram per liter (µg/L) in well MW-3 (120 µg/L) and MW-5 (230 µg/L)  Naphthalene exceeded its 2L Standard of 6 µg/L in well MW-3 (110 µg/L) and MW-5 (240 µg/L)  n-Propylbenzene exceeded its 2L Standard of 70 µg/L in wells MW-3 (82 µg/L) and MW-5 (86 µg/L)  1,2,4-Trimethylbenzene exceeded its 2L Standard of 400 µg/L in well MW-5 (590 µg/L)  Total xylenes exceeded its 2L Standard of 500 µg/L in well MW-5 (1,300 µg/L)  C5-C8 aliphatics exceeded its 2L Standard of 400 µg/L in wells MW-3 (1,500 µg/L) and MW-5 (1,100 µg/L)  C9-C12 aliphatics exceeded its 2L Standard of 700 µg/L in wells MW-3 (2,300 µg/L) and MW-5 (4,100 µg/L)  C9-C10 aromatics exceeded its 2L Standard of 200 µg/L in well MW-5 (1,600 µg/L) Five compounds were only detected below 2L Standards in one or more wells: ethylbenzene, n-butylbenzene, sec- butylbenzene, isoprorylbenzene, and 1,3,5-trimethylbenzene. No VOC or VPH compounds were detected in the samples collected from monitoring wells MW-2R, MW-4, MW-6, MW-7, MW- 8, MW-9, and DW-1 during the August 2014 monitoring event. Groundwater concentrations of VOC and VPH compounds in well MW-3 and MW-5 have decreased since the February 2014 sampling event, with most detected compounds in MW-3 decreasing by more than 50 percent. Since August 2012, prior to the removal of the Site USTs, concentrations of benzene, naphthalene, toluene, 1,2,4-trimethylbenzene, total xylenes, and VPH compounds in MW-3 have decreased by more than an order of magnitude. Analytical results are summarized in Table 5-1. Figures 5-2 to 5-6 include isoconcentration maps for benzene, ethylbenzene, toluene, xylene, and naphthalene, respectively, and Figure 5-7 is a VPH distribution map. Laboratory analytical reports are included in Appendix B. 5.3 Private Water Well Sampling Results As discussed in Section 4.2, no private wells were sampled during the February 2014 sampling event. 5.4 Soil Sampling Results Historical soil sampling results are included on Table 5-2. 5 Results AECOM Environment 6-1 60263455 August 2014 No compounds were detected above the 2L Standard in the deep well (DW-1) or the on-site wells located north (MW-2R), west (MW-4), or south (MW-6) of the UST field. In addition, no compounds were detected in the three off-site, downgradient wells (MW-7 to MW-9). Since August 2012, prior to the removal of the Site USTs, groundwater concentrations of several compounds in well MW-3 have decreased by more than an order of magnitude, including benzene, naphthalene, toluene, 1,2,4-trimethylbenzene, total xylenes, and VPH compounds. Groundwater concentrations in well MW-3 and MW-5 have decreased in both sampling events since August 2013 (the first sampling event following the UST removal). The two nearby irrigation wells were not available for sampling during this event. The property owner at 1617 Wrightsville Avenue refused access. AECOM was unable to successfully contact the property owner at 1620 S. Memorial Boulevard. Though several VOC and VPH compounds are still present on-site at concentrations above 2L Standards, the plume has been fully delineated. Based on the delineation of the plume, declining concentrations in MW-3 and MW-5, and the location of the nearest irrigation well approximately 250 feet from the Site, AECOM, on behalf of 7-Eleven, requests closure. 6 Discussion and Conclusions AECOM Environment 7-1 60263455 August 2014 AECOM, 2012a. 20-Day Report, 7-Eleven Store No. 19847, 1610 S. Croatan Highway, Kill Devil Hills, NC. May 2012. AECOM, 2012b. Initial Abatement Action Report, 7-Eleven Store No. 19847, 1610 S. Croatan Highway, Kill Devil Hills, NC. July 2012. AECOM, 2012c. Limited Site Assessment Report, 7-Eleven Store No. 19847, 1610 S. Croatan Highway, Kill Devil Hills, NC. August 2012. AECOM, 2013a. Pre-Corrective Action Plan Groundwater Monitoring and Underground Storage Tank Closure Report, 7- Eleven Store No. 19847, 1610 S. Croatan Highway, Kill Devil Hills, NC. March 2013. AECOM, 2013b Comprehensive Site Assessment Report, 7-Eleven Store No. 19847, 1610 S. Croatan Highway, Kill Devil Hills, NC. September 2013. 7 References AECOM Environment 60263455 August 2014 Tables Table 3-1Site History - UST Owner/Operator and Other Responsible Party Information7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 09/19/2013UST ID Number1,2,3 (All removed February 2013)Facility ID Number0-011788City State Zip Telephone NumberDallas TX 75201 978-828-0711City State Zip Telephone NumberKill Devil Hills NC 27948 252-441-4549Address1601 South Croatan Highway7-Eleven, Inc. 1985 to Present7-Eleven, Inc. 1985 to PresentName of UST Owner Date of OperationAddress1722 Routh Street, Suite 1000Name of UST Operator Date of OperationAECOM Table 3-2Site History - UST/AST System and Other Release Information7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 09/19/2013UST ID NumberCurrent / Last ContentsPrevious ContentsCapacity (gallons)Construction DetailsTank Dimensions (feet)Associated Piping and PumpsDate Installed Current StatusWas release associated with UST System?1Regular Unleaded GasolineGasoline 10,000Single-walled fiberglass8 x 27Single-walled fiberglassApr-85 Removed 2/2013 Yes2Regular Unleaded GasolineGasoline 10,000Single-walled fiberglass8 x 27Single-walled fiberglassApr-85Abandoned in Place 4/2012; removed 2/2013Yes3Premium Unleaded GasolineGasoline 10,000Single-walled fiberglass8 x 27Single-walled fiberglassApr-85 Removed 2/2013 YesIncident Number Material Released Date of Release38285 Gasoline 4/10/2012Description of ReleasePetroleum odors observed during installation of soil borings. Analytical results, received 4/18/12, confirmed presence of petroleum in soil and groundwater.AECOM Table 3-3Public and Private Water Supply Wells and Other Receptor Information7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 02/25/2014Map ID 1PINWell Owner 2Property Address Mailing Address Phone Number Well UseWell Depth (ft bgs)Type of WellWell Casing Depth (ft bgs)Well Screen Interval (ft bgs)Distance from source area of release 3(ft)Up or Downgradient41989309058019Scruggs and Simmons1620 S. Memorial BoulevardKill Devil Hills, NC 2794814441 Makenzie Lee Road Disputanta, VA 23842804-861-1761 Irrigation 50 N/A N/A N/A 400 Cross-gradient2989309056085Charles and Kim Spry1617 Wrightsville Avenue Kill Devil Hills, NC 27948 1617 Wrightsville Avenue Kill Devil Hills, NC 27948 252-480-0794 Irrigation 75 N/A N/A N/A 250 Cross-gradient989313046470Nags Head Hammocks1801 Croatan HighwayKill Devil Hills, NC1801 Croatan HighwayKill Devil Hills, NCBill252-441-6115Irrigation N/A N/A N/A N/A 750 Cross-gradient988312959785Wings1405 S. Croatan HighwayKill Devil Hills, NC1405 S. Croatan HighwayKill Devil Hills, NCWendy252-480-0009x21Irrigation N/A N/A N/A N/A 650 Cross-gradientContact Phone NumberDistance from source area of release (ft)Up or Downgradient2N/A N/A 1,200 Up-GradientN/A N/A 1,500 Up-GradientNotes:1 - Map ID refers to Figure 3-1.2-Well Owner information based on results of the well survey.3-Exact location of well unknown; distance from source area calculated based on the nearest property boundar4-Groundwater gradient is expected to be toward the northwest based on gauging data collected on August 12, 201ft bgs ‐ feet below ground surfaceN/A - not availablePIN - Parcel Identification NumberWell Survey (within 500 feet)Other ReceptorsReceptor IDDescriptionUsagePWS 0428030 Dare County Water System Wellhead Protection Area (NW of Site) Wellhead Protection AreaPWS 0428030 Dare County Water System Wellhead Protection Area (SW of Site) Wellhead Protection AreaAECOM Table 4-1Monitoring and Remediation Well Construction Information7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 02/24/2014Well ID Date InstalledDate Water Level MeasuredWell Casing Diameter (in.)Well Casing Depth (ft bgs)Screened Interval (ft bgs)Depth of well (ft bgs)Top of Casing Elevation (msl)Depth to Water from TOC (ft)Free Product Thickness (ft)Groundwater Elevation (ft)Comments4/9/2012 44/9/2012 N/A N/A 8.53 3.18 0 5.748/9/2012 N/A N/A 8.53 1.90 0 7.024/9/2012 N/A N/A 8.26 3.53 0 5.388/9/2012 N/A N/A 8.26 1.85 0 7.064/9/2012 44/10/20123.75 05.628/12/20122.47 06.908/12/201220 - 2.5 2.5 - 15 15 8.56 1.67 06.898/12/201220 - 2.5 2.5 - 15 15 9.43 2.60 06.838/2/20133.12 05.402/7/20142.42 06.108/5/20142.05 06.478/2/20134.10 05.232/7/20143.39 05.948/5/20143.01 06.328/2/20133.31 05.582/7/20142.64 06.258/5/20142.31 06.588/2/20134.17 05.192/7/20143.47 05.898/5/20143.10 06.268/2/20133.93 05.382/7/20143.27 06.048/5/20142.91 06.48/5/20142.22 05.938/5/20141.94 05.878/5/20141.33 06.008/2/20134.37 04.902/7/20143.68 05.598/5/20143.27 06.00Notes:ft - feetft bgs - feet below ground surfacein - inchesmsl - mean sea levelN/A - not availableTOC - top of casingSite wells constructed as a flush-mount wells. NS - not surveyedNM - not measured2 0-60 60 - 70 70 9.272 0-2 2 - 12 12 7.3312 8.152 0-2 2 - 12 12 7.810-222 0-2 2 - 12MW-8MW-9DW-1 7/31/20135/12/20145/12/201415 8.89MW-5MW-6MW-7 5/12/20147/30/20137/30/2013 2 0-2 2 - 12 12 9.369.31122 - 12MW-4 8/9/2012 2 0 - 2.5 2.5 - 1512 8.52MW-3R 10/26/2012 4 0 - 2.5 2.5 - 15 15 9.33MW-2R 7/30/2013 2 0-2 2 - 120 - 2.5 2.5 - 15MW-1 4/10/2012unable to remove well cap - could not gaugeunable to remove well cap - could not gauge448.928.91TF-1 N/ATF-4 N/AN/ATF-3MW-3 8/9/2012Well destroyed during February 2012 UST removal activitiesWell destroyed during February 2012 UST removal activitiesWell destroyed during February 2012 UST removal activitiesWell destroyed during February 2012 UST removal activitiesWell Abandoned 10/26/2012Well Abandoned 10/26/2012Well over-drilled and replaced with a 4-inch well (MW-3R) on 10/26/2012TF-2 N/AMW-2 8/9/201215 9.372AECOM Table 5-1Summary of Groundwater Sampling Results7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 02/25/2014504.16010BWellDate CollectedSource Area Sample IDIncident Phase 4/10/2012 MW-1 UST Closure860<100 <100 <1001,200<100 <100 <100 <500190 6,300 760 200 4,800<0.0114,000 9,700 6,600 1,800<5.08/12/2012 MW-1 LSA690<100 <100 <1001,000 70<50 <50640 150 6,200 1,200 300 6,800NA19,000 12,000 10,000 3,000<5.08/12/2012 MW-2 LSA560<100 <100 <1002,300 93<25 <25570 220 13,000 1,800 460 12,700NA36,000 23,000 17,000 3,700<5.0MW-2R 8/2/2013 North of TFMW-2R CSA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.02/7/2014MW-2R Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014MW-2R Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NA8/12/2012 MW-3 LSA2,700<100 <100 <1001,500 76<50 <501,100 170 13,000 2,300 620 12,800NA38,000 25,000 19,000 5,200<5.02/5/2013 MW 3 Dewater*430 10<10 <10630 48<10 <10280 140 1,700 550 200 2,380NA9,500 5,600 5,700 1,700NA2/11/2013 MW 3 Dewater*330 11<10 <10460 42<10 <10260 120 1,400 530 180 1,890NA7,800 4,600 4,800 1,600NA2/11/2013 MW-3 UST Closure91 9.4 5<1.054 34<1.0 <1.0170 97 58 56 40 178NA2,300 1,600 1,400 760<5.08/2/2013 MW-3 CSA1,100<50 <50 <501,800 110<50 <50540 280 1,700 2,400 600 4,700NA18,000 8,200 14,000 4,400<5.02/7/2014 MW-3 Monitoring400<50 <50 <50770 57<50 <50 <250160<250890 260 1,030NA5,300 3,000 4,600 2,300<5.08/5/2014MW-3 Monitoring120<255.3<5360 21<5 <5110 82<25210 65 481NA3,900 1,500 2,300<1,000NA8/12/2012 MW-4 LSA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/2/2013 MW-4 CSA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <1008.82/7/2014 MW-4 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014MW-4 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NAMW-5 8/2/2013MW-5 CSA550<25 <25 <25720 66<25 <25330 200 580 860 230 2,930NA7,800 3,200 6,300 1,8007.52/7/2014MW-5 Monitoring520 16 7.9<1.0700 36 2.2<1.0290 92 42 1,000 160 3,054NA7,100 2,900 7,000 2,800<5.08/5/2014MW-5 Monitoring230 12 6.8<5440 31<5 <5240 86<25590 160 1,300NA3,500 1,100 4,100 1,600NAMW-6 8/2/2013MW-6 CSA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.02/7/2014MW-6 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.01.5<3.0 NA <100 <100 <100 <100<5.08/5/2014MW-6 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NA5/12/2014MW-7 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014MW-7 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NA5/12/2014MW-8 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014MW-8 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NA5/12/2014MW-9 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014MW-9 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NADW-1 8/2/2013DW-1 CSA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <1005.22/7/2014DW-1 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.3<5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100<5.08/5/2014DW-1 Monitoring <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <1.0 <1.0 <3.0 NA <100 <100 <100 <100NA1 70 70 70 600 70 -- 20 6 70 600 400 400 500 0.02-- 400 700 200 15-- -- -- -- -- -- 25 -- -- -- -- -- -- -- ------ -- ----5,000 6,900 8,500 70,000 84,500 25,000 11,700 20,000 6,000 30,000 260,000 28,500 25,000 85,500 50-- 400,000 700,000 200,000 15,000Notes:2L Standard - NCAC 2L Groundwater StandardIMAC - NCAC Interim Maximum Allowable ConcentrationBold - detected valueEPA - Environmental Protection AgencyGCL = gross contamination levelLSA - Limited Site AssessmentMADEP VPH - Massachusetts Department of Environmental Protection Volatile Petroleum HydrocarbonsNA - not analyzedShaded - value exceeds the 2L StandardTF - tank fieldVOC ‐ volatile organic compound*MW 3 Dewater samples collected from the piping to the tank field. The UST Closure sample collected from MW-3 was collected via bailer after dewatering activities had ceasedSoutheast of TFDewateringGCL (µg/L)2L Standard (µg/L)IMAC (µg/L)MW-7MW-8MW-9 Southeast of TFEast of TFEast of TFEast of TFWest of TFSoutheast of TFSouth of TFNorth of TFMW-2MW-3MW-4MW-1Ethylene Dibromide1,3,5-TrimethylbenzeneXylenes, totalVolatile Petroleum HydrocarbonsSouth of TFNaphthalenen-PropylbenzeneDi-isopropyl etherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethyl tert-butyl ether (MTBE)Analytical Method (e.g. VOCs by EPA 8260)Contaminant of ConcernWell Abandoned 10/26/2012Well Abandoned 10/26/2012C9-C12 AliphaticsC9-C10 AromaticsVOCs by EPA Method 6200BMADEP VPHn-Butylbenzenesec-ButylbenzeneLeadBenzeneToluene1,2,4-TrimethylbenzeneC5-C8 AliphaticsAECOM Table 5-2Summary of Soil Sampling Results7-Eleven Store No. 19847Kill Devil Hills, NCIncident Number: 38285 Facility ID #: 0-011788 Revision Date: 09/19/2013Sample ID Date Collected Source AreaSample Depth (ft bgs)Incident Phase TPH-GROSB-01 (3.5-4) 4/10/2012 South of Tank 2 3.5-40.37<0.241.2<0.2412 2.3 0.96<2.411 6.2<0.2419 73 16 24 100NA NA NA NA1,000SB-02 (3-3.5) 4/10/2012 North of Tank 2 3-3.56.4<2.46.8<2.4170 23 4.9<2453 74<2.4270 420 82 140 820NA NA NA NA10,000D-1 2/5/2013 Dispenser 1 2.5 ft <0.00100.0013<0.0010 <0.00100.011 0.0022<0.0010 <0.00100.024 0.0059 0.0029 0.0087 0.047 0.014 0.013 0.082NA NA NA NA < 5D-2 2/5/2013 Dispenser 2 2.5 ft <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0050 <0.0010 <0.0010 <0.0050 <0.0010 <0.0010 <0.0010 <0.0030 NA NA NA NA < 4.3PL-1 2/7/2013 Product Line 2.5 ft <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.010 <0.0050 <0.0010 <0.0010 <0.0050 <0.0010 <0.0010<0.0010 <0.0030 NA NA NA NA <4.6PL-2 2/7/2013 Product Line 2.5 ft <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.010 <0.0050 <0.0010 <0.0010 <0.0050 <0.0010 <0.0010<0.0010 <0.0030 NA NA NA NA <4.9PL-3 2/7/2013 Product Line 2.5 ft <0.480.91<0.48 <0.481.6 0.53<0.48 <4.84.4 2.3<0.48 <2.418 4.1 5.5 8.9NA NA NA NA180PRSW-1 2/6/2013 2.5 ft <1.79.3 3.9<1.770 10 2.4 21 38 37<1.757 240 52 73 400NA NA NA NA3,400PRSW-2 2/6/2013 2.5 ft <0.8911 4.1<0.8952 12 2.1 31 29 43<0.89 <4.4360 60 78 260NA NA NA NA4,200PRSW-3 2/6/2013 2.5 ft <2.314 6.2<2.396 18 3.6 35 54 65<2.3 <11370 78 110 480NA NA NA NA5,800PRSW-4 2/6/2013 2.5 ft <2.06.9 3<2.05.8 6.1<2.0 <20 <1025<2.0 <10140 25 45 21NA NA NA NA4,000PRSE-1 2/6/2013 2.5 ft <2.210 6.1<2.232 10 3.3<2266 26<2.230 400 91 130 430NA NA NA NA4,300PRSE-2 2/6/2013 2.5 ft <9.516<9.5 <9.555 14<9.5 <9571 45<9.5 <48430 92 130 510NA NA NA NA4,600PRSE-3 2/6/2013 2.5 ft <8.89.2<8.8 <8.845 9.1<8.8 <88 <4433<8.8 <44220 46 70 280NA NA NA NA2,900PRSE-4 2/6/2013 2.5 ft <9.617<9.6 <9.6110 19<9.6 <9662 69<9.6100 440 88 140 650NA NA NA NA4,900PRSN-1 2/6/2013 2.5 ft <0.048 <0.048 <0.048 <0.048 <0.048 <0.048 <0.048 <0.480.25<0.048 <0.048 <0.240.16 0.065 0.051<0.14 NA NA NA NA <4.8PRSN-2 2/6/2013 2.5 ft <4.68.2<4.629 44 8.2<4.6 <4632 30<4.642 200 41 60 260NA NA NA NA2,600PRSN-3 2/6/2013 2.5 ft <0.471.3 0.51<0.472.2 0.76<0.47 <4.76.2 2.8<0.47 <2.425 5.6 7.6 16NA NA NA NA1,800PRSN-4 2/6/2013 2.5 ft <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.010 <0.0050 <0.0010 <0.0010 <0.00500.002<0.0010 <0.0010 <0.0030 NA NA NA NA <4.8PRSS-1 2/6/2013 2.5 ft <0.046 <0.046 <0.046 <0.046 <0.046 <0.046 <0.046 <0.460.55<0.046 <0.046 <0.230.28 0.16 0.12<0.14 NA NA NA NA <4.6PRSS-2 2/6/2013 2.5 ft <4.812 4.8<4.850 10<4.8 <4841 35<4.842 280 58 89 360NA NA NA NA4,000PRSS-3 2/6/2013 2.5 ft <2.26 2.4<2.226 4.8<2.2 <2220 18<2.225 140 31 42 190NA NA NA NA2,300PRSS-4 2/6/2013 2.5 ft6.6 16 5.8 56 140 18 3.6<9.255 64<0.92310 430 88 120 920NA NA NA NA8,800OEN 2/7/2013North of Tank Field2.5 ft <1.09.2 3.6<1.026 6.8 2.5<106.8 2.5<1.0 <5.127 44 62 160 920 2001500 840NAOES 2/7/2013South of Tank Field2.5 ft <0.100.63 0.18<0.100.39 0.19 0.12<1.04.7 0.83<0.10 <0.509.2 2.6 2.6 3.3 35<5.087 52NAOEW 2/7/2013West of Tank Field2.5 ft <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.010 <0.0051 <0.0010 <0.0010 <0.0051 <0.0010 <0.0010 <0.0010 <0.0031 <4.8 <4.8 <4.8 <4.8 NAOEE 2/12/2012East of Tank Field2.57.4 21 9.1<4.8120 21 18<4873 75<4.8280 600 120 190 1000 28001300 2700 1200NAMW-2R 7/30/2013North of Tank Field3-3.5 ft CSA <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.012 <0.0062 <0.0012 <0.0012 <0.0062 <0.0012 <0.0012 <0.0012 <0.0037 <4.2 <4.2 <4.2 <4.2 NAMW-5 7/30/2013Southeast of Tank Field3-3.5 ft CSA <0.0013 <0.0013 <0.0013 <0.0013 <0.0013 <0.0013 <0.0013 <0.013 <0.0064 <0.0013 <0.0013 <0.0064 <0.0013 <0.0013 <0.0013 <0.0038 <6.4 <6.4 <6.4 <6.4 NAMW-6 7/30/2013South of Tank Field3-3.5 ft CSA <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.012 <0.0060 <0.0012 <0.0012 <0.0060 <0.0012 <0.0012 <0.0012 <0.0036 <5.9 <5.9 <5.9 <5.9 NA0.0056 4.3 3.3 3.4 4.9 1.7 0.12 16 0.16 1.7 1.5 4.3 8.5 -- 8.3 4.6 -- 68 540 31 --18 626 626 626 1,560 1,560 100 9,385 313 626 3128 1,200 782 -- 782 3,129 -- 939 1,500 469 --164 16,350 16,350 16,350 40,000 40,000 4,000 245,280 8,176 16,350 81,760 32,000 20,440 -- 20,440 81,760 -- 24,528 40,000 12,264 --Notes:Bold - detected valueShaded - value exceeds Soil to Groundwater MSCCRed - value exceeds the residential MSCC EPA - Environmental Protection Agencyft bgs - feet below ground surfaceGRO - Gasoline Range Organicsmg/kg - milligrams per kilogramMSCC - maximum soil contaminant concentrationTPH - Total Petroleum HydrocarbonsVOC - volatile organic compoundResults reported in milligrams-per-kilogram (mg/kg)MADEP VPHGRO by 8015IsopropylbenzeneTolueneVOCs by EPA Method 8260Analytical Method (e.g. VOCs by EPA 8260)Contaminant of ConcernBenzeneEthylbenzeneNaphthaleneResidential MSCC (mg/kg)Industrial/Commercial MSCC (mg/kg)1,3,5-TrimethylbenzeneXylenes, totalVolatile Petroleum Hydrocarbons1,2,4-Trimethylbenzene2-Butanone (MEK)North of Tank FieldSouth of Tank FieldOver-excavationSoil to Groundwater MSCC (mg/kg)C5-C8 AliphaticsC9-C12 Aliphatics* C9-C10 Aromatics **n-Butylbenzenesec-Butylbenzenep-Isopropyltoluenen-Propylbenzene1,2,3-TrimethylbenzeneStyrenetert-ButylbenzeneUST Closure: In-place abandonment of UST #2UST Closure: Removal of site USTsWest of Tank FieldEast of Tank FieldAECOM AECOM Environment 60263455 August 2014 Figures Site Location Map Location September 9, 2013 60263455.20.521 Site Location Map1601 S. Croatan HighwayKill Devil Hills, NC 27948 Figure 1-1 AECOM North Carolina, Inc.8540 Colonnade Center Drive, Suite 306Raleigh, NC 27615Phone: (919) 872-6600Fax: (919) 872-7996Web: http://www.aecom.com 0 2,000 4,000Feet NC VA SCGA KY TN WV MD Kill Devil Hills, NC USGS Topographic Quadrangle (1984) #3#2#17-Eleven#19847GrassPARKINGLOT(ADJACENTPROPERTY)Grass(AdjacentProperty)GARBAGEBI NSNEPTUNEDRI VEParkingParkingFormerCanopyGrassGrass VENTPIPESTF-2TF-1MW-4TF-3TF-4MW-2MW-1MW-3MW-6MW-2RMW-5DW-1WRIGHTSVILLEBOULEVARDRESIDENTIALTREESTREESGrassGrassGrassMW-9MW-8MW-7#2#3#1LEGENDMONITORINGWELLLOCATIONFORMERMONITORINGWELLLOCATION(REMOVED2/2013)FORMERTANKFIELDWELLSFORMERREGULARUNLEADEDGRADEUSTFORMERREGULARUNLEADEDGRADEUSTFORMERPREMIUMUNLEADEDGRADEUSTFORMERPRODUCTLINESAREAOFEXCAVATIONEDGEOFPAVEMENTEDGEOFCONCRETECURBANDGUTTERWOODFENCESOURCES:1.SURVEYEDLOCATIONSPROVIDEDBYTAYLORWISEMAN&TAYLOR;PROJECT70534.6033.00;AUGUST14,2012.2.TANKFIELDANDCANOPYLOCATIONSAREBASEDONAERIALPHOTOGRAPHYPROVIDEDBY7-ELEVEN,INC.7-11 Store No. 19847 1610 S. Croatan Highway Kill Devil Hills, North Carolina Project No.: 60263455.20-5.21 ANSI B 11" x 17"Last saved by: DESKINSL(2014-05-19) Last Plotted: 2014-05-20 Project Management Initials:Designer:Checked:Approved:Filename: \\USGNA2FP001\DATA\USERS\DESKINSL\BASKET\INTEROFFICE WORK\7-11\7-11 CROATAN HWY.DWG SITE MAP Figure: 1-2 Date: May 19, 2014 C.J.C. AECOM Environment 60263455 August 2014 Appendix A. Notice of Regulatory Requirements AECOM Environment 60263455 August 2014 Appendix B. Laboratory Analytical Results 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Ms. Michelle Friedman AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 Report Summary Wednesday August 13, 2014 Report Number: L714144 Samples Received: 08/06/14 Client Project: 60263455 Description: 7-Eleven Store 19847 - 1601S. Croatan Hwy The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: ____________________________________ Terrie Fudge , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-01 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-2R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:40 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/08/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/08/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 85.6 % Rec. MADEPV 08/08/14 1 2,5-Dibromotoluene(PID) 80.1 % Rec. MADEPV 08/08/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 2 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-01 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-2R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:40 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 96.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 104. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 96.6 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 85.0 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:06 Page 3 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-02 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-3R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:15 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons 3900 1000 ug/l MADEPV 08/08/14 10 C5-C8 Aliphatics 1500 1000 ug/l MADEPV 08/08/14 10 C9-C12 Aliphatics 2300 1000 ug/l MADEPV 08/08/14 10 C9-C10 Aromatics BDL 1000 ug/l MADEPV 08/08/14 10 Surrogate Recovery 2,5-Dibromotoluene(FID) 80.4 % Rec. MADEPV 08/08/14 10 2,5-Dibromotoluene(PID) 77.0 % Rec. MADEPV 08/08/14 10 Volatile Organics Acetone 260 250 ug/l 6200B-1997 08/07/14 5 Acrolein BDL 250 ug/l 6200B-1997 08/07/14 5 Acrylonitrile BDL 50. ug/l 6200B-1997 08/07/14 5 Benzene 120 5.0 ug/l 6200B-1997 08/07/14 5 Bromobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromodichloromethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromoform BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromomethane BDL 25. ug/l 6200B-1997 08/07/14 5 n-Butylbenzene 10. 5.0 ug/l 6200B-1997 08/07/14 5 sec-Butylbenzene 5.3 5.0 ug/l 6200B-1997 08/07/14 5 tert-Butylbenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Carbon tetrachloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorodibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chloroethane BDL 25. ug/l 6200B-1997 08/07/14 5 Chloroform BDL 25. ug/l 6200B-1997 08/07/14 5 Chloromethane BDL 12. ug/l 6200B-1997 08/07/14 5 2-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 4-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dibromo-3-Chloropropane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2-Dibromoethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,4-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dichlorodifluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 cis-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 trans-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 4 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-02 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-3R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:15 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloropropene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 2,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Di-isopropyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Ethylbenzene 360 5.0 ug/l 6200B-1997 08/07/14 5 Hexachloro-1,3-butadiene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Isopropylbenzene 21. 5.0 ug/l 6200B-1997 08/07/14 5 p-Isopropyltoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 2-Butanone (MEK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methylene Chloride BDL 25. ug/l 6200B-1997 08/07/14 5 4-Methyl-2-pentanone (MIBK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methyl tert-butyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Naphthalene 110 25. ug/l 6200B-1997 08/07/14 5 n-Propylbenzene 82. 5.0 ug/l 6200B-1997 08/07/14 5 Styrene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Tetrachloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Toluene BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2,4-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichlorofluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichloropropane BDL 12. ug/l 6200B-1997 08/07/14 5 1,2,4-Trimethylbenzene 210 5.0 ug/l 6200B-1997 08/07/14 5 1,3,5-Trimethylbenzene 65. 5.0 ug/l 6200B-1997 08/07/14 5 Vinyl chloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 o-Xylene 11. 5.0 ug/l 6200B-1997 08/07/14 5 m&p-Xylenes 470 10. ug/l 6200B-1997 08/07/14 5 Surrogate Recovery Toluene-d8 96.2 % Rec. 6200B-1997 08/07/14 5 Dibromofluoromethane 101. % Rec. 6200B-1997 08/07/14 5 a,a,a-Trifluorotoluene 96.1 % Rec. 6200B-1997 08/07/14 5 4-Bromofluorobenzene 87.1 % Rec. 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:06 Page 5 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-03 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-4 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:20 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/08/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/08/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 78.7 % Rec. MADEPV 08/08/14 1 2,5-Dibromotoluene(PID) 79.0 % Rec. MADEPV 08/08/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 6 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-03 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-4 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:20 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 97.5 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 102. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 97.7 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.8 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 7 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-04 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-5 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons 3500 500 ug/l MADEPV 08/13/14 5 C5-C8 Aliphatics 1100 500 ug/l MADEPV 08/13/14 5 C9-C12 Aliphatics 4100 500 ug/l MADEPV 08/13/14 5 C9-C10 Aromatics 1600 500 ug/l MADEPV 08/13/14 5 Surrogate Recovery 2,5-Dibromotoluene(FID) 74.7 % Rec. MADEPV 08/13/14 5 2,5-Dibromotoluene(PID) 76.4 % Rec. MADEPV 08/13/14 5 Volatile Organics Acetone BDL 250 ug/l 6200B-1997 08/07/14 5 Acrolein BDL 250 ug/l 6200B-1997 08/07/14 5 Acrylonitrile BDL 50. ug/l 6200B-1997 08/07/14 5 Benzene 230 5.0 ug/l 6200B-1997 08/07/14 5 Bromobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromodichloromethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromoform BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromomethane BDL 25. ug/l 6200B-1997 08/07/14 5 n-Butylbenzene 12. 5.0 ug/l 6200B-1997 08/07/14 5 sec-Butylbenzene 6.8 5.0 ug/l 6200B-1997 08/07/14 5 tert-Butylbenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Carbon tetrachloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorodibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chloroethane BDL 25. ug/l 6200B-1997 08/07/14 5 Chloroform BDL 25. ug/l 6200B-1997 08/07/14 5 Chloromethane BDL 12. ug/l 6200B-1997 08/07/14 5 2-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 4-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dibromo-3-Chloropropane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2-Dibromoethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,4-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dichlorodifluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 cis-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 trans-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 8 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-04 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-5 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloropropene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 2,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Di-isopropyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Ethylbenzene 440 5.0 ug/l 6200B-1997 08/07/14 5 Hexachloro-1,3-butadiene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Isopropylbenzene 31. 5.0 ug/l 6200B-1997 08/07/14 5 p-Isopropyltoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 2-Butanone (MEK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methylene Chloride BDL 25. ug/l 6200B-1997 08/07/14 5 4-Methyl-2-pentanone (MIBK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methyl tert-butyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Naphthalene 240 25. ug/l 6200B-1997 08/07/14 5 n-Propylbenzene 86. 5.0 ug/l 6200B-1997 08/07/14 5 Styrene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Tetrachloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Toluene BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2,4-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichlorofluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichloropropane BDL 12. ug/l 6200B-1997 08/07/14 5 1,2,4-Trimethylbenzene 590 5.0 ug/l 6200B-1997 08/07/14 5 1,3,5-Trimethylbenzene 160 5.0 ug/l 6200B-1997 08/07/14 5 Vinyl chloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 o-Xylene BDL 5.0 ug/l 6200B-1997 08/07/14 5 m&p-Xylenes 1300 10. ug/l 6200B-1997 08/07/14 5 Surrogate Recovery Toluene-d8 98.0 % Rec. 6200B-1997 08/07/14 5 Dibromofluoromethane 99.7 % Rec. 6200B-1997 08/07/14 5 a,a,a-Trifluorotoluene 95.9 % Rec. 6200B-1997 08/07/14 5 4-Bromofluorobenzene 87.9 % Rec. 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 9 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-05 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-6 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 81.6 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 77.9 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 10 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-05 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-6 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 96.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 103. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 95.2 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.8 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 11 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-06 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-7 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:55 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 84.1 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 78.5 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 12 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-06 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-7 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:55 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 97.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 103. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 96.9 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.4 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 13 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-07 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-8 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:00 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 84.8 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 81.5 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 14 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-07 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-8 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:00 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 95.3 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 106. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 95.5 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 88.0 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 15 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-08 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-9 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:05 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 91.2 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 84.6 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/08/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/08/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/08/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/08/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 16 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-08 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-9 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:05 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/08/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/08/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/08/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/08/14 1 Surrogate Recovery Toluene-d8 103. % Rec. 6200B-1997 08/08/14 1 Dibromofluoromethane 95.9 % Rec. 6200B-1997 08/08/14 1 a,a,a-Trifluorotoluene 103. % Rec. 6200B-1997 08/08/14 1 4-Bromofluorobenzene 96.7 % Rec. 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 17 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-09 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : DW-1 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:45 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 86.4 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 82.1 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/08/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/08/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/08/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/08/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 18 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-09 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : DW-1 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:45 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/08/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/08/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/08/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/08/14 1 Surrogate Recovery Toluene-d8 103. % Rec. 6200B-1997 08/08/14 1 Dibromofluoromethane 95.3 % Rec. 6200B-1997 08/08/14 1 a,a,a-Trifluorotoluene 96.2 % Rec. 6200B-1997 08/08/14 1 4-Bromofluorobenzene 97.7 % Rec. 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 19 of 19 About AECOM AECOM (NYSE: ACM) is a global provider of professional technical and management support services to a broad range of markets, including transportation, facilities, environmental, energy, water and government. With approximately 45,000 employees around the world, AECOM is a leader in all of the key markets that it serves. AECOM provides a blend of global reach, local knowledge, innovation, and collaborative technical excellence in delivering solutions that enhance and sustain the world’s built, natural, and social environments. A Fortune 500 company, AECOM serves clients in more than 130 countries and has annual revenue in excess of $8.0 billion. More information on AECOM and its services can be found at www.aecom.com. AECOM 701 Corporate Center Drive, Suite 475 Raleigh, North Carolina 27607 T: +1.919.854.6200 F: +1.919.854.6259