Loading...
HomeMy WebLinkAboutWA-27119_38285_CA_LAB_2014081312065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Ms. Michelle Friedman AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 Report Summary Wednesday August 13, 2014 Report Number: L714144 Samples Received: 08/06/14 Client Project: 60263455 Description: 7-Eleven Store 19847 - 1601S. Croatan Hwy The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: ____________________________________ Terrie Fudge , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-01 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-2R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:40 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/08/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/08/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 85.6 % Rec. MADEPV 08/08/14 1 2,5-Dibromotoluene(PID) 80.1 % Rec. MADEPV 08/08/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 2 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-01 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-2R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:40 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 96.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 104. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 96.6 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 85.0 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:06 Page 3 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-02 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-3R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:15 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons 3900 1000 ug/l MADEPV 08/08/14 10 C5-C8 Aliphatics 1500 1000 ug/l MADEPV 08/08/14 10 C9-C12 Aliphatics 2300 1000 ug/l MADEPV 08/08/14 10 C9-C10 Aromatics BDL 1000 ug/l MADEPV 08/08/14 10 Surrogate Recovery 2,5-Dibromotoluene(FID) 80.4 % Rec. MADEPV 08/08/14 10 2,5-Dibromotoluene(PID) 77.0 % Rec. MADEPV 08/08/14 10 Volatile Organics Acetone 260 250 ug/l 6200B-1997 08/07/14 5 Acrolein BDL 250 ug/l 6200B-1997 08/07/14 5 Acrylonitrile BDL 50. ug/l 6200B-1997 08/07/14 5 Benzene 120 5.0 ug/l 6200B-1997 08/07/14 5 Bromobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromodichloromethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromoform BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromomethane BDL 25. ug/l 6200B-1997 08/07/14 5 n-Butylbenzene 10. 5.0 ug/l 6200B-1997 08/07/14 5 sec-Butylbenzene 5.3 5.0 ug/l 6200B-1997 08/07/14 5 tert-Butylbenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Carbon tetrachloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorodibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chloroethane BDL 25. ug/l 6200B-1997 08/07/14 5 Chloroform BDL 25. ug/l 6200B-1997 08/07/14 5 Chloromethane BDL 12. ug/l 6200B-1997 08/07/14 5 2-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 4-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dibromo-3-Chloropropane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2-Dibromoethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,4-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dichlorodifluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 cis-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 trans-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 4 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-02 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-3R Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:15 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloropropene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 2,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Di-isopropyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Ethylbenzene 360 5.0 ug/l 6200B-1997 08/07/14 5 Hexachloro-1,3-butadiene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Isopropylbenzene 21. 5.0 ug/l 6200B-1997 08/07/14 5 p-Isopropyltoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 2-Butanone (MEK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methylene Chloride BDL 25. ug/l 6200B-1997 08/07/14 5 4-Methyl-2-pentanone (MIBK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methyl tert-butyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Naphthalene 110 25. ug/l 6200B-1997 08/07/14 5 n-Propylbenzene 82. 5.0 ug/l 6200B-1997 08/07/14 5 Styrene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Tetrachloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Toluene BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2,4-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichlorofluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichloropropane BDL 12. ug/l 6200B-1997 08/07/14 5 1,2,4-Trimethylbenzene 210 5.0 ug/l 6200B-1997 08/07/14 5 1,3,5-Trimethylbenzene 65. 5.0 ug/l 6200B-1997 08/07/14 5 Vinyl chloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 o-Xylene 11. 5.0 ug/l 6200B-1997 08/07/14 5 m&p-Xylenes 470 10. ug/l 6200B-1997 08/07/14 5 Surrogate Recovery Toluene-d8 96.2 % Rec. 6200B-1997 08/07/14 5 Dibromofluoromethane 101. % Rec. 6200B-1997 08/07/14 5 a,a,a-Trifluorotoluene 96.1 % Rec. 6200B-1997 08/07/14 5 4-Bromofluorobenzene 87.1 % Rec. 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:06 Page 5 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-03 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-4 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:20 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/08/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/08/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/08/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 78.7 % Rec. MADEPV 08/08/14 1 2,5-Dibromotoluene(PID) 79.0 % Rec. MADEPV 08/08/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 6 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-03 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-4 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:20 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 97.5 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 102. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 97.7 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.8 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 7 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-04 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-5 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons 3500 500 ug/l MADEPV 08/13/14 5 C5-C8 Aliphatics 1100 500 ug/l MADEPV 08/13/14 5 C9-C12 Aliphatics 4100 500 ug/l MADEPV 08/13/14 5 C9-C10 Aromatics 1600 500 ug/l MADEPV 08/13/14 5 Surrogate Recovery 2,5-Dibromotoluene(FID) 74.7 % Rec. MADEPV 08/13/14 5 2,5-Dibromotoluene(PID) 76.4 % Rec. MADEPV 08/13/14 5 Volatile Organics Acetone BDL 250 ug/l 6200B-1997 08/07/14 5 Acrolein BDL 250 ug/l 6200B-1997 08/07/14 5 Acrylonitrile BDL 50. ug/l 6200B-1997 08/07/14 5 Benzene 230 5.0 ug/l 6200B-1997 08/07/14 5 Bromobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromodichloromethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromoform BDL 5.0 ug/l 6200B-1997 08/07/14 5 Bromomethane BDL 25. ug/l 6200B-1997 08/07/14 5 n-Butylbenzene 12. 5.0 ug/l 6200B-1997 08/07/14 5 sec-Butylbenzene 6.8 5.0 ug/l 6200B-1997 08/07/14 5 tert-Butylbenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Carbon tetrachloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chlorodibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Chloroethane BDL 25. ug/l 6200B-1997 08/07/14 5 Chloroform BDL 25. ug/l 6200B-1997 08/07/14 5 Chloromethane BDL 12. ug/l 6200B-1997 08/07/14 5 2-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 4-Chlorotoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dibromo-3-Chloropropane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2-Dibromoethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dibromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,4-Dichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Dichlorodifluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2-Dichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 cis-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 trans-1,2-Dichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 8 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-04 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-5 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1-Dichloropropene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,3-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 2,2-Dichloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Di-isopropyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Ethylbenzene 440 5.0 ug/l 6200B-1997 08/07/14 5 Hexachloro-1,3-butadiene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Isopropylbenzene 31. 5.0 ug/l 6200B-1997 08/07/14 5 p-Isopropyltoluene BDL 5.0 ug/l 6200B-1997 08/07/14 5 2-Butanone (MEK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methylene Chloride BDL 25. ug/l 6200B-1997 08/07/14 5 4-Methyl-2-pentanone (MIBK) BDL 50. ug/l 6200B-1997 08/07/14 5 Methyl tert-butyl ether BDL 5.0 ug/l 6200B-1997 08/07/14 5 Naphthalene 240 25. ug/l 6200B-1997 08/07/14 5 n-Propylbenzene 86. 5.0 ug/l 6200B-1997 08/07/14 5 Styrene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2,2-Tetrachloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Tetrachloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Toluene BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,2,4-Trichlorobenzene BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,1-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 1,1,2-Trichloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichloroethene BDL 5.0 ug/l 6200B-1997 08/07/14 5 Trichlorofluoromethane BDL 25. ug/l 6200B-1997 08/07/14 5 1,2,3-Trichloropropane BDL 12. ug/l 6200B-1997 08/07/14 5 1,2,4-Trimethylbenzene 590 5.0 ug/l 6200B-1997 08/07/14 5 1,3,5-Trimethylbenzene 160 5.0 ug/l 6200B-1997 08/07/14 5 Vinyl chloride BDL 5.0 ug/l 6200B-1997 08/07/14 5 o-Xylene BDL 5.0 ug/l 6200B-1997 08/07/14 5 m&p-Xylenes 1300 10. ug/l 6200B-1997 08/07/14 5 Surrogate Recovery Toluene-d8 98.0 % Rec. 6200B-1997 08/07/14 5 Dibromofluoromethane 99.7 % Rec. 6200B-1997 08/07/14 5 a,a,a-Trifluorotoluene 95.9 % Rec. 6200B-1997 08/07/14 5 4-Bromofluorobenzene 87.9 % Rec. 6200B-1997 08/07/14 5 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 9 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-05 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-6 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 81.6 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 77.9 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 10 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-05 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-6 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:30 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 96.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 103. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 95.2 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.8 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 11 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-06 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-7 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:55 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 84.1 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 78.5 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 12 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-06 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-7 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:55 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 97.4 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 103. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 96.9 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 87.4 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 13 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-07 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-8 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:00 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 84.8 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 81.5 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/07/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/07/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/07/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/07/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/07/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/07/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 14 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-07 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-8 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:00 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/07/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/07/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/07/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/07/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/07/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/07/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/07/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/07/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/07/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/07/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/07/14 1 Surrogate Recovery Toluene-d8 95.3 % Rec. 6200B-1997 08/07/14 1 Dibromofluoromethane 106. % Rec. 6200B-1997 08/07/14 1 a,a,a-Trifluorotoluene 95.5 % Rec. 6200B-1997 08/07/14 1 4-Bromofluorobenzene 88.0 % Rec. 6200B-1997 08/07/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 15 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-08 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-9 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:05 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 91.2 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 84.6 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/08/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/08/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/08/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/08/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 16 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-08 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : MW-9 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 11:05 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/08/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/08/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/08/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/08/14 1 Surrogate Recovery Toluene-d8 103. % Rec. 6200B-1997 08/08/14 1 Dibromofluoromethane 95.9 % Rec. 6200B-1997 08/08/14 1 a,a,a-Trifluorotoluene 103. % Rec. 6200B-1997 08/08/14 1 4-Bromofluorobenzene 96.7 % Rec. 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 17 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-09 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : DW-1 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:45 Parameter Result Det. Limit Units Qualifier Method Date Dil. Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 08/09/14 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 08/09/14 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 08/09/14 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 86.4 % Rec. MADEPV 08/09/14 1 2,5-Dibromotoluene(PID) 82.1 % Rec. MADEPV 08/09/14 1 Volatile Organics Acetone BDL 50. ug/l 6200B-1997 08/08/14 1 Acrolein BDL 50. ug/l 6200B-1997 08/08/14 1 Acrylonitrile BDL 10. ug/l 6200B-1997 08/08/14 1 Benzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromodichloromethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromoform BDL 1.0 ug/l 6200B-1997 08/08/14 1 Bromomethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 sec-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 tert-Butylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Carbon tetrachloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chlorodibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Chloroethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloroform BDL 5.0 ug/l 6200B-1997 08/08/14 1 Chloromethane BDL 2.5 ug/l 6200B-1997 08/08/14 1 2-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 4-Chlorotoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2-Dibromoethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dibromomethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Dichlorodifluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2-Dichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Page 18 of 19 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Michelle Friedman August 13,2014 AECOM Inc - Raleigh 701 Corporate Center Drive; Ste 475 Raleigh, NC 27607 ESC Sample # : L714144-09 Date Received : August 06, 2014 Description : 7-Eleven Store 19847 - 1601S. Croatan Hwy Site ID : KILL DEVIL HILLS, NC Sample ID : DW-1 Project # : 60263455 Collected By : DA/NP Collection Date : 08/05/14 10:45 Parameter Result Det. Limit Units Qualifier Method Date Dil. 1,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1-Dichloropropene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 2,2-Dichloropropane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Di-isopropyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Ethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Isopropylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 p-Isopropyltoluene BDL 1.0 ug/l 6200B-1997 08/08/14 1 2-Butanone (MEK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methylene Chloride BDL 5.0 ug/l 6200B-1997 08/08/14 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 6200B-1997 08/08/14 1 Methyl tert-butyl ether BDL 1.0 ug/l 6200B-1997 08/08/14 1 Naphthalene BDL 5.0 ug/l 6200B-1997 08/08/14 1 n-Propylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Styrene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Tetrachloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Toluene BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,1-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,1,2-Trichloroethane BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichloroethene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Trichlorofluoromethane BDL 5.0 ug/l 6200B-1997 08/08/14 1 1,2,3-Trichloropropane BDL 2.5 ug/l 6200B-1997 08/08/14 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 6200B-1997 08/08/14 1 Vinyl chloride BDL 1.0 ug/l 6200B-1997 08/08/14 1 o-Xylene BDL 1.0 ug/l 6200B-1997 08/08/14 1 m&p-Xylenes BDL 2.0 ug/l 6200B-1997 08/08/14 1 Surrogate Recovery Toluene-d8 103. % Rec. 6200B-1997 08/08/14 1 Dibromofluoromethane 95.3 % Rec. 6200B-1997 08/08/14 1 a,a,a-Trifluorotoluene 96.2 % Rec. 6200B-1997 08/08/14 1 4-Bromofluorobenzene 97.7 % Rec. 6200B-1997 08/08/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Laboratory Certification Numbers: AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ -0612, MN - 047-999-395, NY - 11742, NJ - TN002, WI - 998093910 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 08/13/14 11:11 Printed: 08/13/14 12:07 Page 19 of 19