WA-27076_38241_CA_RPTS_20181120_MRP

MONITORING REPORT

FOR

GASOLINE DISPENSER LINE RELEASE AT
NCDOT MARTIN COUNTY MAINTENANCE FACILITY
1740 PRISON CAMP ROAD
WILLIAMSTON, MARTIN COUNTY, NC

WBS ELEMENT: 30173.156

FACILITY ID: 0-024673
SITE RISK: H 165 D
INCIDENT NUMBER: 38241
LAND USE CLASSIFICATION: RESIDENTIAL

November 20, 2018

CATLIN PROJECT NO. 211010.10

Prepared By:

220 Old Dairy Road Wilmington, NC 28405 [phone]
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585 CORPORATE GEOLOGY LICENSE NO. C-118
Post Office Box 10279 Wilmington, North Carolina 28404-0279
Telephone: [phone] Fax: [phone] www.catlinusa.com
November 20, 2018
North Carolina Department of Environmental Quality Washington Regional Office
Division of waste Management Underground Storage Tank Section
Attn: Ms. Sylvia Newsome-Hunneke
943 Washington Square Mall Washington, North Carolina 27889

Re: Monitoring Report NCDOT Martin County Maintenance Facility
Gasoline Dispenser Line Release
1740 Prison Camp Road Williamston, North Carolina 27892
WBS Element: 30173.156
NCDEQ Incident No. 38241 CATLIN Project No. 211010.10
Dear Ms. Newsome-Hunneke:
On behalf of the North Carolina Department of Transportation (NCDOT), CATLIN Engineers and Scientists (CATLIN) is pleased to submit the latest Monitoring Report for the above referenced
site in Williamston, North Carolina.
If you should have any questions, concerns or require further actions, please contact Mr. Jeffrey
Walston at [phone] or CATLIN at [phone] at your convenience.
Sincerely,
Sean O’Neil, P.E.
Project Manager
Enclosures

cc: Mr. Jeffrey Walston, NCDOT (Enclosure w/CD) DOT_MartinCntyGAS_Mtr_Ltr_2017

MONITORING REPORT

For

GASOLINE DISPENSER LINE RELEASE AT
NCDOT MARTIN COUNTY MAINTENANCE FACILITY
1740 PRISON CAMP ROAD
WILLIAMSTON, MARTIN COUNTY, NC

WBS ELEMENT: 30173.156

FACILITY ID: 0-024673
SITE RISK: H 165 D
NCDEQ INCIDENT NUMBER: 38241
LAND USE CLASSIFICATION: RESIDENTIAL

November 20, 2018
PREPARED FOR:
NORTH CAROLINA DEPARTMENT OF TRANSPORTATION
ATTN: MR. JEFFREY WALSTON, PE, CPESC, CPSWQ
ROADSIDE ENVIRONMENTAL UNIT
1557 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1557

CATLIN PROJECT NO. 211010

PREPARED BY:

CATLIN ENGINEERS AND SCIENTISTS
P. O. BOX 10279
WILMINGTON, NORTH CAROLINA 28404-0279
[phone]

CORPORATE GEOLOGY LICENSE NO. C-118
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018
TABLE OF CONTENTS PAGE
A. SITE INFORMATION 1
B. SITE HISTORY AND SOURCE CHARACTERIZATION 2
C. RECEPTOR INFORMATION 2
D. SUMMARY OF FIELD ACTIVITIES 4
E. SUMMARY OF FIELD RESULTS 5
F. CONCLUSIONS AND RECOMMENDATIONS 6
G. LIMITATIONS 7

TABLES
TABLE 1 SITE HISTORY – UST OWNER/OPERATOR INFORMATION
TABLE 2 SITE HISTORY – UST SYSTEM INFORMATION
TABLE 3 MONITORING WELL CONSTRUCTION AND GROUNDWATER ELEVATION
INFORMATION
TABLE 4 SUMMARY OF MONITORING WELL GROUNDWATER LABORATORY
RESULTS – STANDARD METHOD 6200B
TABLE 5 SUMMARY OF HISTORICAL MONITORING WELL GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B

FIGURES

FIGURE 1A SITE VICINITY MAP
FIGURE 1B AERIAL PHOTOGRAPH WITH WATER SUPPLY WELLS
FIGURE 2 SITE MAP
FIGURE 3A GROUNDWATER CONTOURS AS OF SEPTEMBER 7, 2017
FIGURE 3B GROUNDWATER CONTOURS AS OF OCTOBER 9, 2018
FIGURE 4 GROUNDWATER SAMPLE LOCATIONS AND SUMMARIZED RESULTS AS
OF OCTOBER 2018

APPENDICES
APPENDIX A LABORATORY REPORT AND CHAIN-OF-CUSTODY DOCUMENTATION
APPENDIX B WELL CONSTRUCTION RECORDS AND MONITORING WELL LOGS
MONITORING REPORT
A. SITE INFORMATION
SITE IDENTIFICATION: Date of Report: November 20, 2018
Facility ID: _o_-_0_24_6_7_3 ______ UST Incident Number (if known): _3_8_2_4_1 __ _
Site Risk: High Site Rank: H 165D Land Use Classification: Residential
Site Name: NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release)
Site Location: 1740 Prison Camp Road (see Figures 1A and 1B)
Nearest City/Town: Williamston County: Martin -----------
CONTACTS: (see Table 1)
North Carolina Department of Transportation (NCDOT) Fleet & Material
UST Owner: Management Unit
Address: 4809 Beryl Road Raleigh, NC 27606 Phone: [phone]
UST Operator: NCDOT Fleet & Material Management Unit
Address: 4809 Beryl Road Raleigh, NC 27606 Phone: [phone]
Property Owner: NCDOT Martin County (Division 1)
Address: 1740 Prison Camp Road Williamston, NC 27892 Phone: [phone]
Property Occupant: NCDOT Martin County (Division 1)
Address: 1740 Prison Camp Road Williamston, NC 27892 Phone: [phone]
Consultant/Contractor: CATLIN Engineers and Scientists (CATLIN)
Address: 220 Old Dairy Road, Wilmington, NC 28405 Phone: [phone]
Analytical Laboratory: Pace Analytical Services, Inc. (Pace} State Cert. No. 12
9800 Kincey Ave. Suite 100
Address: Huntersville, NC 28078 Phone: [phone] -----------
RELEASE INFORMATION:
Date Discovered: _S_e_,p'-t_em_b_e_r 2--'''-2_0_1_0 ________ _
Longitude: W -77.095822822° Latitude: N 35.831615947°
----------------~ Estimated Quantity of Release: Unknown ----------------------Cause of Release: Unknown, possibly resulting from utility work in the area.
Source of Release (e.g. Piping/UST): Gasoline piping (supply line) Sizes and contents of UST system(s) from
which the release occurred: (see Table 2} 15,000 gallon gasoline UST
Criteria Used to No contaminant concentrations above the established Gross Contaminant Classify Risk: Levels (GCLs), potable well(s) within 1,000 feet
I, Sean O'Neil
CATLIN Engineers and Scientists, o c a e information contained in this report is
correct and accurate to the best of my knowledge. \ \ \ \ \ I f / / f 111 ,,,,'(o.~CA R /// ~~,~~ ..... ii; ... ~ ..__ Q • A • • -<7 -........ • ·y , -3 . y. ::
~ : 03747 : =: ::. ·.. ll·to·' l ... 2 -:::.. . ~"' ~~. ...... ~/~~A·.~!~.-:~~\$' //,,NJ 0 ,,, (Please Affix Seal and Signature) 111 / / / l l \ \ \ \
NCDOT; 211010_2018_MR
CATLIN Project No. 211010 1
CATLIN Engineers and Scientists
November 2018

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 2 November 2018
B. SITE HISTORY AND SOURCE CHARACTERIZATION
1. Site Operations and History
Table 1 includes a summary of the underground storage tank (UST)
owner/operator information and Table 2 includes site UST system information.
Figure 2 illustrates the UST dispenser canopy, line layout and approximate
area of excavation. 2. Contaminant Source Inventory
According to NCDOT, a gasoline line leak was discovered in 2010 during a UST system pressure test. Soils around the identified leak were excavated
and the line leak was repaired.

3. Previous Investigations and Initial Abatement
NCDOT submitted a “24-Hour Release and UST Leak Reporting Form (UST
61 Form)” to the North Carolina Department of Environmental Quality (NCDEQ), previously the North Carolina Department of Environment and Natural Resources (NCDENR), on September 2, 2010. CATLIN conducted a
Limited Site Assessment (LSA) investigation and submitted a LSA report
dated August 19, 2011, to NCDEQ. Since the submittal of the LSA, CATLIN
has conducted several groundwater sampling events at this site. Results from these sampling events were submitted to NCDEQ in subsequently prepared reports.

4. Site Characteristics
Currently, potable water is available to the subject site and surrounding
properties (within a 1,000 foot radius) from a public municipal water system.
There are no water supply wells within 250 feet of the source area. Initially,
during the LSA investigation, sixteen water wells were identified as shown on
Figure 1B. Interviews with occupants and subsequent follow-up with the Town of Williamston indicate there are currently three (3) potable wells within the
1,000 foot radius. Water supply well information is summarized in Section C of
this report. Potable wells are identified on the table in Section C of this report
and their locations are illustrated on Figure 1B.
5. Surface Water

The nearest natural surface water body is an intermittent, unnamed stream
approximately 1,200 feet northeast of the site (refer to Figure 1A).

C. RECEPTOR INFORMATION
Currently there are three (3) potable water supply wells within 1,000 feet of the
source area. These wells (numbers 5, 10 and 16) are identified on Figure 1B and
are indicated in bold on the following table.

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 3 November 2018

Owner / Occupant Address Phone # Well Use Well Depth Type of Well
Well
Screen
Interval
Distance
from
Source
Figure 1B
Location
Key
Barbara Rogers 1788 Prison Camp Rd. Unknown Not in Use Unknown Unknown Unknown 400 feet Southwest 1
NC Forest Service
1169 Kekukee
Rd.
252-331-4781 Not in Use Unknown 4-inch galvanized Unknown 850 feet West 2
Garland
Craft
1731 Prison
Camp Rd
252-792-
5393
Not in
Use Unknown Unknown Unknown 263 feet South-Southeast 3
Cecil Bonds
/ Rebecca Thomas
1685 Prison Camp Rd. 252-792-2306 Not In Use Unknown Unknown Unknown
250 feet
East-Southeast 4
Jorge Villigas / David
Williams
1671 Prison
Camp Rd.
252-217-7880 Potable Un-known Unknown Un-known
350 feet East-
Southeast
5
Jeffrey Whitley 1651 Prison Camp Rd. Unknown Not in Use Unknown Unknown Unknown 400 feet East 6
Nathan Mizelle 1797 Prison Camp Rd. 252-792-2861 Not in Use Unknown Unknown Unknown 600 feet South 7
Nathan Mizelle 1829 Prison Camp Rd. Unknown Not in Use Unknown Unknown Unknown
650 feet
South-Southwest 8
Gregory Kay
1710
Kekukee Rd. Unknown Not in Use Unknown Unknown Unknown
950 feet
South-Southwest 9
John
Dunlow
1690
Kekukee
Rd.
252-802-
0499 Potable Un-
known Unknown Un-
known
1,000 feet
West 10
Gordon
Knox
Knox
Mobile Home Park
– Prison Camp Rd.
252-217-
5484
Not in
Use Unknown Unknown Unknown 560 feet
South 11
Jorge Villigas /
David Williams
1677 Prison
Camp Rd.
252-217-
7880
Not in
Use
Un-
known Unknown Un-
known
450feet
Northwest 12
Robert
Warren
1605 Prison
Camp Rd. Unknown Not in
Use Unknown Unknown Unknown 600 feet
East 13
Donnie
Whitley
1210 Pineview Road Unknown Irrigation Unknown Unknown Unknown 550 feet
East 14
Daniel Casey
1250
Pineview Road Unknown Not in Use Unknown Unknown Unknown 500 feet Southeast 15
William
Roberson
1211 Pineview
Road
252-792-
8409 Potable Un-
known Unknown Un-
known
750 feet East-
Southeast
16

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 4 November 2018
The additional supply wells within 1,000 feet of the site were identified to be not in
service or non-potable used for irrigation. Public water is available for surrounding
properties; however, utilization of the water supply system is voluntary at this time.
Based on the distance of well 16 from the project site, the current municipal water
supply line location and the orientation of the well (in a side gradient groundwater
flow direction), it was determined in an email correspondence dated December 31,
2015, that potable well 16 could be left in place and only wells 5 and 10 needed to
be disconnected in order to request the site be re-ranked to a Low Risk Site.
D. SUMMARY OF FIELD ACTIVITIES
CATLIN installed two shallow, Type II, monitoring wells on October 9, 2018, and conducted a groundwater sampling event on October 12, 2018. Field activities
during the sampling event included collection of water-level measurements and
groundwater samples from all accessible monitoring wells. Figure 2 illustrates the
monitoring well locations.
Monitoring Well Installation

Shallow, Type II, monitoring wells MW05 and MW06 were installed on October 9,
2018, by a North Carolina licensed well driller utilizing hollow stem augers. The new
wells were installed upgradient if potable wells 5 and 10. Each well was installed approximately 12 feet below land surface (BLS) with a screened interval from
approximately 2 to 12 feet BLS. Following monitoring well isntallations, the
monitoring wells were developed by over pumping and surging. The locations and
top of casing elevations were surveyed using traditional survey techniques (rod and
level).
Monitoring well construction information is summarized on Table 3 and the well
construction records and monitoring well logs are included in Appendix B. The
monitoring well locations are illustrated on Figure 2.
Groundwater Gauging

CATLIN personnel gauged all monitoring wells for depth to water and potential free-
product thicknesses to determine the groundwater flow direction using an electronic
oil-water interface probe. To prevent cross contamination, the interface probe was decontaminated with a phosphate-free soap and water solution and rinsed with de-
ionized water between each well. Section E discusses the gauging results.

Groundwater Sampling
CATLIN personnel collected groundwater samples from all monitoring wells via new
disposable bailers and string. To prevent cross contamination, a new disposal
bailer and string were used for each monitoring well. Prior to collecting a
groundwater sample, a minimum of three well volumes (or a minimum of one well
volume if the well was bailed dry due to minimal recharge rates) were removed.

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 5 November 2018
Once CATLIN removed the required volume of groundwater from the well, a
groundwater sample was collected directly from the bailer into the appropriate
laboratory provided glassware for laboratory analysis.
The groundwater samples were collected in general accordance with the following
procedures:

 Chemical preservatives, where applicable were added to sample bottles by the laboratory;
 Sample bottles were labeled prior to sample collection with date and time of
sample collection;
 Caps were secured on bottles;
 Sample containers were kept of ice (<4oC) during transportation to the
laboratory.

All groundwater samples were transported, under appropriate Chain-of-Custody (CoC) documentation, to Pace Anaytical Services, Inc (Pace). The groundwater
samples were analyzed per Standard Method (SM) 6200B. Section E discusses
the laboratory analytical results.

E. SUMMARY OF FIELD RESULTS

Groundwater Gauging
Table 3 summarizes current and historical groundwater gauging data. Groundwater
contours were computer generated in AutoCAD.

The depths to groundwater in the shallow (Type II) aquifer monitoring ranged from 1.51 feet to 4.86 feet below top of casing. Surficial groundwater contours for the
previous sampling event (September 2017) and current sampling event (October
2018) are illustrated on Figures 3A and 3B, respectively. The October 2018 surficial
groundwater migration trend is primarily towards the east. Historically, the
groundwater migration trend has been to the west.
No free-phase product was detected during the October 2018 sampling event or any
prior sampling events.

Groundwater Sampling
Pace analyzed the groundwater samples per SM 6200B. Table 4 summarizes the
current laboratory analytical data, while Table 5 summarizes the historical laboratory
analytical data. Figure 4 illustrates the most recent analytical results. The complete
laboratory analytical report is provided in Appendix A.
Laboratory results per SM 6200 revealed dissolved Benzene concentrations in the
groundwater samples collected from MW01 (344 micrograms per liter [ug/L]) and
MW05 (1.6 ug/L) above the North Carolina Administrative Code Title 15A 2L
Groundwater Quality Standards (2L GWQS) of 1 ug/L. In addition, MW01

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 6 November 2018
contained a dissolved Naphthalene concentration (26.7 ug/L) above the 2L GWQS
of 6 ug/L. No other contaminant concentrations were detected above their
respective 2L GWQS.
Historically, groundwater contaminant concentrations above the 2L GWQS have
been detected in the groundwater samples collected from MW01, MW02 and
MW04. Concentrations in these wells have generally decreased since the initial
sampling event in May 2011. Monitoring well MW05 was sampled for the first time in
October 2018 and contained a Benzene concentration slightly above the 2L GWQS.
F. CONCLUSIONS AND RECOMMENDATIONS
1. Conclusions
Based on the findings of this monitoring report, the following conclusions are
made:
 Historically, no free-phase product has ever been detected when gauging
or sampling the site.
 Groundwater volatile contaminant concentrations were detected above corresponding 2L GWQS in the groundwater sample collected from
MW01 and MW05 (Benzene and/or Naphthalene).
 Laboratory analytical results did not reveal any groundwater contaminant
concentrations above the GCLs. Historically, no GCL exceedances have been reported at this site.
 Groundwater volatile compound concentrations have clearly decreased
over time.
 The groundwater migration trend was towards the east in October 2018,
which is generally in the opposite direction as the historical groundwater trend.

2. Recommendations

CATLIN recommends continuing with annual groundwater sampling until water supply wells 5 and 10 are disconnected/abandoned. In addition,
based on the slightly elevated Benzene concentration in newly installed
monitoring well MW05, CATLIN recommends collecting an additional
groundwater sample in January 2019. If a Benzene concentration is
detected above the 2L GWQS in the January 2019 sample, CATLIN recommends collecting a sample from potable well 5 (see Figure 1B).

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 7 November 2018
G. LIMITATIONS
The field and groundwater data evaluated as part of this investigation only provides
isolated data points and may not represent conditions at every location in the project
area. Analyses and conclusions of this report, being based on interpolation
between data points at the project area, may not be completely representative of all site conditions. Conclusions and recommendations of this investigation and report
are based on the best available data in an effort to comply with current regulatory
requirements.

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018

TABLES

Page 1 of 1
NCDOT; TABLE1OwnerOperator CATLIN Engineers and Scientists
CATLIN Project No.: 211010 November 2018
TABLE 1
SITE HISTORY UST OWNER/OPERATOR INFORMATION
Incident Number and Name: Facility ID#: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release) 0-024673

UST ID Numbers: 160-101 160-102
160-103
Facility ID Number: 0-024673
Name of Owner Dates of Operation
NCDOT Fleet & Material Management Unit 4/30/1990 to Present
Street Address
4809 Beryl Road
City State Zip Telephone Number
Raleigh NC 27606 [phone]
Name of Operator Dates of Operation
NCDOT Martin County Maintenance 4/30/1990 to Present
Street Address
1740 Prison Camp Road
City State Zip Telephone Number
Williamston NC 27892 (252)-792-2503
Incident Number: 38241
Name of Other Responsible Party Dates of Release(s)
None Unknown – Discovered September 2, 2010
Street Address
Not Applicable
City State Zip Telephone Number
Not Applicable Not
Applicable
Not
Applicable
Not Applicable

Page 1 of 1
SITE HISTORY - UST SYSTEM INFORMATION*
UST ID
Number
Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description
of Associated
Piping
Date
Installed Status of UST
Was Release
Associated With
UST System?
1 Gasoline Unknown 6,300 Unknown Unknown Unknown 8/29/1973 Removed
4/30/1990 No
2 Kerosene Unknown 1,000 Unknown Unknown Unknown 8/29/1974 Removed
4/30/1990 No
3 Waste Oil Unknown 3,000 Unknown Unknown Unknown 8/29/1972 Removed
4/30/1990 No
4 Gasoline Unknown 10,000 Unknown Unknown Unknown 8/29/1974 Removed
4/30/1990 No
5 Diesel Unknown 10,000 Unknown Unknown Unknown 8/29/1975 Removed
4/30/1990 No
6 Waste OIl Unknown 3,500 Unknown Unknown Unknown 1/1/1964 Removed
10/31/1994 No
160-101 Gasoline None 15,000 Unknown Unknown Unknown 4/30/1990 Active Yes - Piping Only
160-102 Diesel None 15,000 Unknown Unknown Unknown 4/30/1990 Active No
160-103 Waste Oil Unknown 2,000 Unknown Unknown Unknown 4/30/1990 Active No
* = UST System information reported by MACTEC as obtained from NCDEQ online UST registry
TABLE 2
Incident Number and Name: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release)
Facility ID#:
0-024673
NCDOT; TABLE2SystemInfo
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018
Page 1 of 1
MONITORING WELL CONSTRUCTION AND GROUNDWATER ELEVATION INFORMATION
Facility ID#:
0-024673
Well ID Date
Installed
Date Water
Level
Measured
Well Casing
Depth
(ft. BLS)
Screened
Interval
(x to y ft.
BLS)
Bottom of
Well
(ft. BLS)
Top of
Casing
Elevation*
(ft.)
Depth to
Ground-
water
(ft.)
Groundwater
Elevation
(ft.)
5/13/11 4.43 70.66
12/8/11 4.92 70.17
6/17/13 5.04 70.05
12/5/13 7.67 67.42
8/28/14 4.92 70.17
9/17/15 5.63 69.46
2/9/17 4.98 70.11
9/7/2017 4.72 70.37
10/12/2018 4.86 70.23
5/13/11 3.43 70.97
12/8/11 2.47 71.93
6/17/13 3.01 71.39
12/5/13 2.51 71.89
8/28/14 2.38 72.02
9/17/15 3.49 70.91
2/9/17 2.10 72.30
9/7/2017 1.93 72.47
10/12/2018 2.27 72.13
5/13/11 4.05 70.87
12/8/11 3.55 71.37
6/17/13 4.07 70.85
12/5/13 3.83 71.09
8/28/14 3.39 71.53
9/17/15 4.85 70.07
2/9/17 3.65 71.27
9/7/2017 3.69 71.23
10/12/2018 2.77 72.15
5/13/11 2.90 72.22
12/8/11 3.15 71.97
6/17/13 3.35 71.77
12/5/13 3.00 72.12
8/28/14 3.20 71.92
9/17/15 4.72 70.40
2/9/17 2.79 72.33
9/7/2017 2.91 72.21
10/12/2018 3.13 71.99
MW05 10/9/2018 10/12/2018 2 2 - 12 12 73.90 1.51 72.39
MW06 10/9/2018 10/12/2018 2 2 - 12 12 77.31 3.54 73.77
No free-phase product has been measured at the site.
ft. BLS = Feet Below Land Surface
75.12
MW02 5/12/11 2 2 - 12
MW04 5/12/11 2 2 - 12 12
12 74.40
MW03 5/12/11
12 75.09
Incident Number and Name:
38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release)
12 74.9222 - 12
TABLE 3
MW01 5/12/11 2 2 - 12
NCDOT; TABLE3Wellcon-Grndwtr
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018
Page 1 of 1
TABLE 4
SUMMARY OF MONITORING WELL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
Incident Number and Name: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release) Facility ID: 0-024673
Sample
ID
Date
Collected
MW01 MW-01 10/12/2018 82.6 <0.62 344 139 16.9 26.7 213 <0.62 325 1.7 2.6
MW02 MW-02 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW03 MW-03 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34J ND
MW04 MW-04 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW05 MW-05 10/12/2018 <0.25 <0.25 1.6 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW06 MW-06 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34J ND
All results in micrograms per liter (mg/L).
< = Less than Method Detection Limit
ND= Not detected at or above the adjusted reporting limit or method detection limit
GCL = Gross Contaminant Level
2L GWQS = North Carolina Adminstrative Code Title 15A 2L Groundwater Quality Standards
Bold results indicate concentrations above 2L GWQS.
J = Estimated concentration above the adjusted Method Detection Limit and below the adjusted Reporting Limit Methyl-tert-butyl ether (MTBE)All Other 6200B Parametersn-PropylbenzeneTotal XylenesIsopropylbenzene (Cumene)NaphthaleneTolueneEthylbenzeneBenzene1,3,5-Trimethylbenzene1,2,4-TrimethylbenzeneWell ID
Contaminant
of Concern
GCL (mg/L)
2L GWQS (mg/L)
28,500
400
25,000
400
5,000
1
84,500
600
25,000
70
6,000
6
20,000
20
Varies
Varies
260,000
600
30,000
70
85,500
500
NCDOT;TABLE4WELLS6200B
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018
Page 1 of 3
TABLE 5
SUMMARY OF HISTORICAL MONITORING WELL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
Incident Number and Name: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release) Facility ID: 0-024673
Sample
ID
Date
Collected
MW01 5/13/2011 518 138 3,030 540 33.3 162 3,690 76.6 2,744 <0.576 BMDL
MW-01 12/8/2011 58.8 16.8 650 20.2 7.22 11.9 76 6.82 163.5 <0.144 10.28
MW-01 6/17/2013 163 26.9 900 96.2 18.7 34.2 166 20.4 383.2 1.6 BMDL
MW-01 12/5/2013 165 23.6 902 81.5 25.9 32.7 80.0 21.0 257.3 <0.50 ND
MW-01 8/28/2014 187 34.5 785 129 29.7 45.1 203 28.1 386 1.7 ND
MW-01 9/17/2015 79.5 23.4 665 81.2 16.4 27.3 141 15.9 187.1 <2.5 2.6
MW-01 2/9/2017 111 40.9 520 146 20.2 38.6 283 25.7 375 4.2 1.6 J
MW-01 9/7/2017 119 <1.0 474 171 21 38.5 334 <1.0 443 1.5 J 3.2
MW-01 10/12/2018 82.6 <0.62 344 139 16.9 26.7 213 <0.62 325 1.7 2.6
MW02 5/13/2011 202 45.9 1,320 188 7.78 62.0 1,620 21.4 990 3.32 BMDL
MW-02 7/27/2011 76.0 20.8 740 74.4 <20.0 <20.0 54.6 <20.0 249 <20.0 BMDL
MW-02 12/8/2011 28.6 6.14 259 17.9 3.05 12.5 2.75 5.00 73.3 <0.144 5.77
MW-02 6/17/2013 2.4 0.74 247 1.7 0.45 J 2.5 0.25 J 0.49 J 2.6 1.1 BMDL
MW-02 12/5/2013 2.1 <0.50 182 0.60 0.75 2.6 <0.50 <0.50 2.9 0.84 ND
MW-02 8/28/2014 0.58 0.57 59.8 0.82 <0.50 <2.0 <0.50 <0.50 <1.50 <0.50 ND
MW-02 9/17/2015 <0.50 <0.50 4.2 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 <0.50 ND
MW-02 2/9/2017 6.30 2.4 2.8 3.50 0.45 J 1.7 J 1.3 1.3 8.6 <0.25 ND
MW-02 9/7/2017 0.93 0.33 J 0.36 J 0.42 J <0.25 <1.0 <0.25 <0.25 <0.94 J <0.25 ND
MW-02 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW01
MW02
GCL (mg/L)
2L GWQS (mg/L)
Contaminant
of Concern
Well ID
1,2,4-Trimethylbenzene28,500
400 1,3,5-Trimethylbenzene25,000
400 Benzene5,000
1 NaphthaleneEthylbenzeneIsopropylbenzene (Cumene)84,500
600
25,000
70
6,000
6 Toluene30,000
70
85,500
500
20,000
20
Varies
VariesAll Other SM 6200B Parametersn-PropylbenzeneMethyl-tert-butyl ether (MTBE)Total Xylenes260,000
600
NCDOT; TABLE5Historical
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018
Page 2 of 3
TABLE 5
SUMMARY OF HISTORICAL MONITORING WELL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
Incident Number and Name: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release) Facility ID: 0-024673
Sample
ID
Date
Collected
MW01
GCL (mg/L)
2L GWQS (mg/L)
Contaminant
of Concern
Well ID
1,2,4-Trimethylbenzene28,500
400 1,3,5-Trimethylbenzene25,000
400 Benzene5,000
1 NaphthaleneEthylbenzeneIsopropylbenzene (Cumene)84,500
600
25,000
70
6,000
6 Toluene30,000
70
85,500
500
20,000
20
Varies
VariesAll Other SM 6200B Parametersn-PropylbenzeneMethyl-tert-butyl ether (MTBE)Total Xylenes260,000
600
MW03 5/13/2011 <0.0961 <0.113 <0.113 <0.0877 <0.0869 <0.0855 0.140 J <0.113 <0.2694 0.760 BMDL
MW-03 12/8/2011 <0.0961 <0.113 <0.113 <0.0877 <0.0869 <0.0855 <0.133 <0.113 <0.2694 <0.144 BMDL
MW-03 6/17/2013 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 1.2 BMDL
MW-03 12/5/2013 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 1.5 ND
MW-03 8/28/2014 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 <0.50 ND
MW-03 9/17/2015 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 2.7 ND
MW-03 2/9/2017 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.66 ND
MW-03 9/7/2017 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.55 ND
MW-03 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34J ND
MW04 5/13/2011 <0.0961 <0.113 1.16 <0.0877 <0.0869 <0.0855 0.640 <0.113 <0.352 J <0.144 BMDL
MW-04 12/8/2011 <0.0961 <0.113 <0.113 <0.0877 <0.0869 <0.0855 <0.133 <0.113 <0.2694 <0.144 BMDL
MW-04 6/17/2013 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 BMDL
MW-04 12/5/2013 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 <0.50 ND
MW-04 8/28/2014 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 1.0 ND
MW-04 9/17/2015 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <1.50 <0.50 ND
MW-04 2/9/2017 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW-04 9/7/2017 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW-04 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW03
MW04
NCDOT; TABLE5Historical
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018
Page 3 of 3
TABLE 5
SUMMARY OF HISTORICAL MONITORING WELL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
Incident Number and Name: 38241 - NCDOT Martin County Maintenance Facility (Gasoline Dispenser Line Release) Facility ID: 0-024673
Sample
ID
Date
Collected
MW01
GCL (mg/L)
2L GWQS (mg/L)
Contaminant
of Concern
Well ID
1,2,4-Trimethylbenzene28,500
400 1,3,5-Trimethylbenzene25,000
400 Benzene5,000
1 NaphthaleneEthylbenzeneIsopropylbenzene (Cumene)84,500
600
25,000
70
6,000
6 Toluene30,000
70
85,500
500
20,000
20
Varies
VariesAll Other SM 6200B Parametersn-PropylbenzeneMethyl-tert-butyl ether (MTBE)Total Xylenes260,000
600
MW05 MW-05 10/12/2018 <0.25 <0.25 1.6 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 ND
MW06 MW-06 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34J ND
All results in micrograms per liter (mg/L).
< = Less than method detection limit or reporting limit
BMDL = Below Method Detection Limit
GCL = Gross Contaminant Level
2L GWQS = North Carolina Administrative Code Title 15A 2L Groundwater Quality Standards
J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Bold results indicate concentrations above 2L GWQS.
ND= Not detected at or above the adjusted reporting limit.
NCDOT; TABLE5Historical
CATLIN Project No. 211010
CATLIN Engineers and Scientists
November 2018

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018

FIGURES

2,000 0 2,000 4,0001,000 Feet
SOIL STOCKPILEAREA(NCDOT YARD)PRISON CAMP ROADT
Y
N
E
R

R
O
A
DKEKUKEE PARK ROADUS HWY 64
SCALE
Source: Terrain Navigator Pro Quadrangle, (Williamston, NC 1982)/
SITE LOCATION
DESCRIPTION:
PREPARED BY:SCALE:TITLE:COUNTY:
FA No:
ST PROJ:WBS ELEM:FIGURE No:NCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELEASE SITE
SITE VICINITYMAPAS SHOWN
MARTINN/AN/A30173.156 1A
211010
ENGLISH
400 0 400 800200Feet1000FOOTRADIUS
SITE LOCATION
PRISON CAMP ROADT
Y
N
E
R
R
O
A
DKEKUKEE PARK ROAD2
9
1
4
6
13
1178
1431215
5
10 16
SCALE
Source: Terrain Navigator Pro Orthophotos, (Williamston, NC 2009) Parcels provided by Martin County GIS, 2011./
DESCRIPTION:
PREPARED BY:SCALE:TITLE:COUNTY:FA No:
ST PROJ:WBS ELEM:FIGURE No:
NCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELASE SITE
AERIAL PHOTOGRAPH WITH WATER SUPPLY WELLSAS SHOWN
MARTINN/AN/A30173.156 1B
211010
ENGLISH
LEGEND
WATER SUPPLY WELL LOCATION!(W
NOTE: Water Supply Well numbers correspond to LSA Report Section D.1 (Water Supply Well Table)
ENGLISHNCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELEASE SITE211010SITE MAPDESCRIPTION:FIGURE NO.230173.156N/AMARTINCOUNTY:T.I.P. NO.:WBS:TITLE:S:\WPMKTG\PROJECT\2011\211010 NCDOT WILLIAMSTON MARTIN CNTY GAS\MONITORING\2018\OCT 2018\FIGS\FIGURE2.DWGPROJECT NO.:MW06MW03MW02MW01MW05MW04APPROXIMATE AREA OF PREVIOUSEXCAVATION AROUND FUEL LINERELEASE4020 040SCALE IN FEETLEGENDSYMBOL DESCRIPTIONSOIL BORING/SAMPLEMONITORING WELL (TYPE II)FIRE HYDRANTNOTES:1. MAP ADAPTED FROM GPS DATA COLLECTED BYCATLIN AND FROM GOOGLE EARTH
ENGLISH0SCALE IN FEET201020NCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELEASE SITEGROUNDWATER CONTOURSAS OF SEPTEMBER 7, 2017DESCRIPTION:FIGURE NO.3A30173.156N/AMARTINCOUNTY:T.I.P. NO.:WBS:TITLE:LEGENDEXISTING DESCRIPTIONMONITORING WELL (TYPE II)NOTES:1. MAP ADAPTED FROM GPS DATA COLLECTED BY CATLIN.2. ELEVATION BASED ON MEAN SEA LEVEL.3. * - MW01 GROUNDWATER ELEVATION CONSIDERED ANOMALOUS, LIKELYEFFECTED BY ADJACENT UTILITIES AND WAS NOT USED FOR CONTOURING.MW03MW04ROADGRASSGRASSP
R
I
S
O
N

C
AM
P

RO
A
D FUEL L
INESELECTRIC WATERLINESEWER LINEGAS LINES
EW
E
R

L
I
N
EWATERLINE GATEFIRE HYDRANTDISPENSERISLANDCANOPYAPPROXIMATE AREA OF PREVIOUSEXCAVATION AROUND FUEL LINE RELEASE(72.21)(71.23)GROUNDWATER FLOW DIRECTIONGROUNDWATER CONTOUR (0.25 FT. INTERVAL)MW01*(70.37)MW02(72.47)S:\WPMKTG\PROJECT\2011\211010 NCDOT WILLIAMSTON MARTIN CNTY GAS\MONITORING\2018\OCT 2018\FIGS\FIGURE3A.DWG(71.25)211010PROJECT NO.:( )GROUNDWATER ELEVATION (FEET)(71.50)(71.75)(72.00)(72.25)
ENGLISHNCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELEASE SITE211010GROUNDWATER CONTOURSAS OF OCTOBER 9, 2018DESCRIPTION:FIGURE NO.3B30173.156N/AMARTINCOUNTY:T.I.P. NO.:WBS:TITLE:S:\WPMKTG\PROJECT\2011\211010 NCDOT WILLIAMSTON MARTIN CNTY GAS\MONITORING\2018\OCT 2018\FIGS\FIGURE3B.DWGPROJECT NO.:MW06(73.77)MW03(72.15)MW02(72.13)MW01(70.23)MW05(72.39)MW04(71.99)APPROXIMATE AREA OF PREVIOUSEXCAVATION AROUND FUEL LINERELEASE4020 040SCALE IN FEETNOTES:1. MAP ADAPTED FROM GPS DATA COLLECTED BY CATLIN ANDFROM GOOGLE EARTH.2. GROUNDWATER ELEVATIONS BASED ON MEAN SEA LEVEL.3. * - MW01 GROUNDWATER ELEVATION CONSIDERED ANOMALOUS,LIKELY EFFECTED BY ADJACENT UTILITIES AND WAS NOT USEDFOR CONTOURING.73.5073.2573.0072.7572.5072.2572.00LEGENDSYMBOLDESCRIPTIONSOIL BORING/SAMPLEMONITORING WELL (TYPE II)FIRE HYDRANTGROUNDWATER FLOW DIRECTIONGROUNDWATER CONTOUR (0.25 FT. INTERVAL)( )GROUNDWATER ELEVATION (FEET)
ENGLISHNCDOT MARTIN COUNTYMAINTENANCE FACILITYGASOLINE RELEASE SITE211010GROUNDWATER SAMPLELOCATIONS AND SUMMARIZEDRESULTSAS OF OCTOBER 2018DESCRIPTION:FIGURE NO.230173.156N/AMARTINCOUNTY:T.I.P. NO.:WBS:TITLE:S:\WPMKTG\PROJECT\2011\211010 NCDOT WILLIAMSTON MARTIN CNTY GAS\MONITORING\2018\OCT 2018\FIGS\FIGURE4.DWGPROJECT NO.:MW06MW03MW02MW01MW05MW04APPROXIMATE AREA OF PREVIOUSEXCAVATION AROUND FUEL LINERELEASE4020 040SCALE IN FEETLEGENDSYMBOL DESCRIPTIONSOIL BORING/SAMPLEMONITORING WELL (TYPE II)FIRE HYDRANTNOTES:1. MAP ADAPTED FROM GPS DATA COLLECTED BYCATLIN AND FROM GOOGLE EARTHSUMMARY OF MONITORING WELL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200BWell IDContaminantof Concern 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Benzene Ethylbenzene
Isopropylbenzene
(Cumene)
Naphthalene
Toluene
n-Propylbenzene
Total Xylenes
Methyl-tert-butyl ether
(MTBE)
All Other
6200B ParametersSampleIDDateCollectedGCL (mg/L)2L GWQS (mg/L)28,50040025,0004005,000184,50060025,000706,0006260,00060030,0007085,50050020,00020VariesVariesMW01 MW-01 10/12/2018 82.6 <0.62344139 16.926.7213 <0.62 325 1.7 2.6MW02 MW-02 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 NDMW03 MW-03 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34 J NDMW04 MW-04 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 NDMW05 MW-05 10/12/2018 <0.25 <0.251.6<0.25 <0.25 <1.0 <0.25 <0.25 <0.75 <0.25 NDMW06 MW-06 10/12/2018 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <0.75 0.34 J ND All results in micrograms per liter (mg/L). < = Less than Method Detection Limit ND= Not detected at or above the adjusted reporting limit or method detection limit GCL = Gross Contaminant Level 2L GWQS = North Carolina Adminstrative Code Title 15A 2L Groundwater Quality Standards Bold results indicate concentrations above 2L GWQS. J = Estimated concentration above the adjusted Method Detection Limit and below the adjusted Reporting LimitESTIMATED EXTENT OFIMPACTED GROUNDWATERABOVE 2L GWQS??

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018

APPENDICES

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018

APPENDIX A

LABORATORY REPORT AND CHAIN-OF-CUSTODY DOCUMENTATION

#=CL#
October 22, 2018
LIMS USE: FR - CHEMICAL
LIMS OBJECT ID: 92403459
92403459
Project:
Pace Project No.:
RE:
Chemical Testing EngineerNCDOTMaterials & Tests Unit1801 Blue Ridge RoadRaleigh, NC 27607
WBS 30173.156
Dear Chemical Engineer:
Enclosed are the analytical results for sample(s) received by the laboratory on October 15, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager(704)875-9092
Enclosures
cc: Ben Ashba, CATLIN Engineers & Scientists, Inc.
Sean O'Neil, CATLIN Engineers and Scientists
Theodore Triantafillopoulos, Catlin Engineers and Scientst
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92403459
WBS 30173.156
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92403459
WBS 30173.156
Lab ID Sample ID Matrix Date Collected Date Received
92403459001 MW-01 Water 10/12/18 10:50 10/15/18 13:20
92403459002 MW-02 Water 10/12/18 10:45 10/15/18 13:20
92403459003 MW-03 Water 10/12/18 10:40 10/15/18 13:20
92403459004 MW-04 Water 10/12/18 10:25 10/15/18 13:20
92403459005 MW-05 Water 10/12/18 10:30 10/15/18 13:20
92403459006 MW-06 Water 10/12/18 11:45 10/15/18 13:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92403459
WBS 30173.156
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92403459001 MW-01 SM 6200B 63 PASI-CGAW
92403459002 MW-02 SM 6200B 63 PASI-CGAW
92403459003 MW-03 SM 6200B 63 PASI-CGAW
92403459004 MW-04 SM 6200B 63 PASI-CGAW
92403459005 MW-05 SM 6200B 63 PASI-CGAW
92403459006 MW-06 SM 6200B 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-01 Lab ID: 92403459001 Collected: 10/12/18 10:50 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 344 ug/L 10/20/18 15:22 71-43-21.2 0.62 2.5
Bromobenzene ND ug/L 10/20/18 15:22 108-86-11.2 0.62 2.5
Bromochloromethane ND ug/L 10/20/18 15:22 74-97-51.2 0.62 2.5
Bromodichloromethane ND ug/L 10/20/18 15:22 75-27-41.2 0.62 2.5
Bromoform ND ug/L 10/20/18 15:22 75-25-21.2 0.62 2.5
Bromomethane ND ug/L 10/20/18 15:22 74-83-912.5 6.2 2.5
n-Butylbenzene 2.6 ug/L 10/20/18 15:22 104-51-81.2 0.62 2.5
sec-Butylbenzene ND ug/L 10/20/18 15:22 135-98-81.2 0.62 2.5
tert-Butylbenzene ND ug/L 10/20/18 15:22 98-06-61.2 0.62 2.5
Carbon tetrachloride ND ug/L 10/20/18 15:22 56-23-51.2 0.62 2.5
Chlorobenzene ND ug/L 10/20/18 15:22 108-90-71.2 0.62 2.5
Chloroethane ND ug/L 10/20/18 15:22 75-00-32.5 1.2 2.5
Chloroform ND ug/L 10/20/18 15:22 67-66-31.2 0.62 2.5
Chloromethane ND ug/L 10/20/18 15:22 74-87-32.5 1.2 2.5
2-Chlorotoluene ND ug/L 10/20/18 15:22 95-49-81.2 0.62 2.5
4-Chlorotoluene ND ug/L 10/20/18 15:22 106-43-41.2 0.62 2.5
1,2-Dibromo-3-chloropropane ND ug/L 10/20/18 15:22 96-12-82.5 1.2 2.5
Dibromochloromethane ND ug/L 10/20/18 15:22 124-48-11.2 0.62 2.5
1,2-Dibromoethane (EDB)ND ug/L 10/20/18 15:22 106-93-41.2 0.62 2.5
Dibromomethane ND ug/L 10/20/18 15:22 74-95-31.2 0.62 2.5
1,2-Dichlorobenzene ND ug/L 10/20/18 15:22 95-50-11.2 0.62 2.5
1,3-Dichlorobenzene ND ug/L 10/20/18 15:22 541-73-11.2 0.62 2.5
1,4-Dichlorobenzene ND ug/L 10/20/18 15:22 106-46-71.2 0.62 2.5
Dichlorodifluoromethane ND ug/L 10/20/18 15:22 75-71-81.2 0.62 2.5
1,1-Dichloroethane ND ug/L 10/20/18 15:22 75-34-31.2 0.62 2.5
1,2-Dichloroethane ND ug/L 10/20/18 15:22 107-06-21.2 0.62 2.5
1,1-Dichloroethene ND ug/L 10/20/18 15:22 75-35-41.2 0.62 2.5
cis-1,2-Dichloroethene ND ug/L 10/20/18 15:22 156-59-21.2 0.62 2.5
trans-1,2-Dichloroethene ND ug/L 10/20/18 15:22 156-60-51.2 0.62 2.5
1,2-Dichloropropane ND ug/L 10/20/18 15:22 78-87-51.2 0.62 2.5
1,3-Dichloropropane ND ug/L 10/20/18 15:22 142-28-91.2 0.62 2.5
2,2-Dichloropropane ND ug/L 10/20/18 15:22 594-20-71.2 0.62 2.5
1,1-Dichloropropene ND ug/L 10/20/18 15:22 563-58-61.2 0.62 2.5
cis-1,3-Dichloropropene ND ug/L 10/20/18 15:22 10061-01-51.2 0.62 2.5
trans-1,3-Dichloropropene ND ug/L 10/20/18 15:22 10061-02-61.2 0.62 2.5
Diisopropyl ether ND ug/L 10/20/18 15:22 108-20-31.2 0.62 2.5
Ethylbenzene 139 ug/L 10/20/18 15:22 100-41-41.2 0.62 2.5
Hexachloro-1,3-butadiene ND ug/L 10/20/18 15:22 87-68-35.0 2.5 2.5
Isopropylbenzene (Cumene)16.9 ug/L 10/20/18 15:22 98-82-81.2 0.62 2.5
Methylene Chloride ND ug/L 10/20/18 15:22 75-09-25.0 2.5 2.5
Methyl-tert-butyl ether 1.7 ug/L 10/20/18 15:22 1634-04-41.2 0.62 2.5
Naphthalene 26.7 ug/L 10/20/18 15:22 91-20-35.0 2.5 2.5
n-Propylbenzene ND ug/L 10/20/18 15:22 103-65-11.2 0.62 2.5
Styrene ND ug/L 10/20/18 15:22 100-42-51.2 0.62 2.5
1,1,1,2-Tetrachloroethane ND ug/L 10/20/18 15:22 630-20-61.2 0.62 2.5
1,1,2,2-Tetrachloroethane ND ug/L 10/20/18 15:22 79-34-51.2 0.62 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-01 Lab ID: 92403459001 Collected: 10/12/18 10:50 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 10/20/18 15:22 127-18-41.2 0.62 2.5
Toluene 213 ug/L 10/20/18 15:22 108-88-31.2 0.62 2.5
1,2,3-Trichlorobenzene ND ug/L 10/20/18 15:22 87-61-65.0 2.5 2.5
1,2,4-Trichlorobenzene ND ug/L 10/20/18 15:22 120-82-15.0 2.5 2.5
1,1,1-Trichloroethane ND ug/L 10/20/18 15:22 71-55-61.2 0.62 2.5
1,1,2-Trichloroethane ND ug/L 10/20/18 15:22 79-00-51.2 0.62 2.5
Trichloroethene ND ug/L 10/20/18 15:22 79-01-61.2 0.62 2.5
Trichlorofluoromethane ND ug/L 10/20/18 15:22 75-69-42.5 1.2 2.5
1,2,3-Trichloropropane ND ug/L 10/20/18 15:22 96-18-41.2 0.62 2.5
1,2,4-Trimethylbenzene 82.6 ug/L 10/20/18 15:22 95-63-61.2 0.62 2.5
1,3,5-Trimethylbenzene ND ug/L 10/20/18 15:22 108-67-81.2 0.62 2.5
Vinyl chloride ND ug/L 10/20/18 15:22 75-01-42.5 1.2 2.5
m&p-Xylene 209 ug/L 10/20/18 15:22 179601-23-12.5 1.2 2.5
o-Xylene 116 ug/L 10/20/18 15:22 95-47-61.2 0.62 2.5
Surrogates
1,2-Dichloroethane-d4 (S)94 %10/20/18 15:22 17060-07-070-130 2.5
4-Bromofluorobenzene (S)96 %10/20/18 15:22 460-00-470-130 2.5
Toluene-d8 (S)98 %10/20/18 15:22 2037-26-570-130 2.5
Sample: MW-02 Lab ID: 92403459002 Collected: 10/12/18 10:45 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/19/18 21:52 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/19/18 21:52 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/19/18 21:52 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/19/18 21:52 75-27-40.50 0.25 1
Bromoform ND ug/L 10/19/18 21:52 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/19/18 21:52 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/19/18 21:52 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/19/18 21:52 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/19/18 21:52 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/19/18 21:52 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/19/18 21:52 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/19/18 21:52 75-00-31.0 0.50 1
Chloroform ND ug/L 10/19/18 21:52 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/19/18 21:52 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/19/18 21:52 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/19/18 21:52 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/18 21:52 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/19/18 21:52 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/18 21:52 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/19/18 21:52 74-95-30.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-02 Lab ID: 92403459002 Collected: 10/12/18 10:45 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,2-Dichlorobenzene ND ug/L 10/19/18 21:52 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/19/18 21:52 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/19/18 21:52 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/19/18 21:52 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/19/18 21:52 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/19/18 21:52 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/19/18 21:52 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/19/18 21:52 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/19/18 21:52 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/19/18 21:52 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/19/18 21:52 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/19/18 21:52 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/19/18 21:52 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/19/18 21:52 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/19/18 21:52 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/19/18 21:52 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/19/18 21:52 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/19/18 21:52 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/19/18 21:52 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/19/18 21:52 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/19/18 21:52 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/19/18 21:52 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/19/18 21:52 103-65-10.50 0.25 1
Styrene ND ug/L 10/19/18 21:52 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/18 21:52 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/18 21:52 79-34-50.50 0.25 1
Tetrachloroethene ND ug/L 10/19/18 21:52 127-18-40.50 0.25 1
Toluene ND ug/L 10/19/18 21:52 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/19/18 21:52 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/19/18 21:52 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/19/18 21:52 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/19/18 21:52 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/19/18 21:52 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/19/18 21:52 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/19/18 21:52 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/19/18 21:52 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/19/18 21:52 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/19/18 21:52 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/19/18 21:52 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/19/18 21:52 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %10/19/18 21:52 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %10/19/18 21:52 460-00-470-130 1
Toluene-d8 (S)100 %10/19/18 21:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-03 Lab ID: 92403459003 Collected: 10/12/18 10:40 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/19/18 21:35 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/19/18 21:35 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/19/18 21:35 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/19/18 21:35 75-27-40.50 0.25 1
Bromoform ND ug/L 10/19/18 21:35 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/19/18 21:35 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/19/18 21:35 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/19/18 21:35 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/19/18 21:35 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/19/18 21:35 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/19/18 21:35 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/19/18 21:35 75-00-31.0 0.50 1
Chloroform ND ug/L 10/19/18 21:35 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/19/18 21:35 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/19/18 21:35 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/19/18 21:35 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/18 21:35 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/19/18 21:35 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/18 21:35 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/19/18 21:35 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 10/19/18 21:35 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/19/18 21:35 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/19/18 21:35 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/19/18 21:35 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/19/18 21:35 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/19/18 21:35 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/19/18 21:35 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/19/18 21:35 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/19/18 21:35 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/19/18 21:35 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/19/18 21:35 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/19/18 21:35 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/19/18 21:35 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/19/18 21:35 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/19/18 21:35 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/19/18 21:35 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/19/18 21:35 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/19/18 21:35 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/19/18 21:35 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/19/18 21:35 75-09-22.0 1.0 1
Methyl-tert-butyl ether 0.34J ug/L 10/19/18 21:35 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/19/18 21:35 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/19/18 21:35 103-65-10.50 0.25 1
Styrene ND ug/L 10/19/18 21:35 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/18 21:35 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/18 21:35 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-03 Lab ID: 92403459003 Collected: 10/12/18 10:40 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 10/19/18 21:35 127-18-40.50 0.25 1
Toluene ND ug/L 10/19/18 21:35 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/19/18 21:35 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/19/18 21:35 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/19/18 21:35 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/19/18 21:35 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/19/18 21:35 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/19/18 21:35 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/19/18 21:35 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/19/18 21:35 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/19/18 21:35 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/19/18 21:35 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/19/18 21:35 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/19/18 21:35 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %10/19/18 21:35 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %10/19/18 21:35 460-00-470-130 1
Toluene-d8 (S)99 %10/19/18 21:35 2037-26-570-130 1
Sample: MW-04 Lab ID: 92403459004 Collected: 10/12/18 10:25 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/19/18 20:15 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/19/18 20:15 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/19/18 20:15 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/19/18 20:15 75-27-40.50 0.25 1
Bromoform ND ug/L 10/19/18 20:15 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/19/18 20:15 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/19/18 20:15 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/19/18 20:15 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/19/18 20:15 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/19/18 20:15 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/19/18 20:15 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/19/18 20:15 75-00-31.0 0.50 1
Chloroform ND ug/L 10/19/18 20:15 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/19/18 20:15 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/19/18 20:15 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/19/18 20:15 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/18 20:15 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/19/18 20:15 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/18 20:15 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/19/18 20:15 74-95-30.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-04 Lab ID: 92403459004 Collected: 10/12/18 10:25 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,2-Dichlorobenzene ND ug/L 10/19/18 20:15 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/19/18 20:15 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/19/18 20:15 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/19/18 20:15 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/19/18 20:15 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/19/18 20:15 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/19/18 20:15 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/19/18 20:15 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/19/18 20:15 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/19/18 20:15 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/19/18 20:15 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/19/18 20:15 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/19/18 20:15 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/19/18 20:15 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/19/18 20:15 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/19/18 20:15 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/19/18 20:15 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/19/18 20:15 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/19/18 20:15 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/19/18 20:15 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/19/18 20:15 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/19/18 20:15 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/19/18 20:15 103-65-10.50 0.25 1
Styrene ND ug/L 10/19/18 20:15 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/18 20:15 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/18 20:15 79-34-50.50 0.25 1
Tetrachloroethene ND ug/L 10/19/18 20:15 127-18-40.50 0.25 1
Toluene ND ug/L 10/19/18 20:15 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/19/18 20:15 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/19/18 20:15 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/19/18 20:15 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/19/18 20:15 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/19/18 20:15 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/19/18 20:15 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/19/18 20:15 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/19/18 20:15 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/19/18 20:15 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/19/18 20:15 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/19/18 20:15 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/19/18 20:15 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)90 %10/19/18 20:15 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %10/19/18 20:15 460-00-470-130 1
Toluene-d8 (S)102 %10/19/18 20:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-05 Lab ID: 92403459005 Collected: 10/12/18 10:30 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 1.6 ug/L 10/19/18 23:12 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/19/18 23:12 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/19/18 23:12 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/19/18 23:12 75-27-40.50 0.25 1
Bromoform ND ug/L 10/19/18 23:12 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/19/18 23:12 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/19/18 23:12 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/19/18 23:12 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/19/18 23:12 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/19/18 23:12 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/19/18 23:12 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/19/18 23:12 75-00-31.0 0.50 1
Chloroform ND ug/L 10/19/18 23:12 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/19/18 23:12 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/19/18 23:12 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/19/18 23:12 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/18 23:12 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/19/18 23:12 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/18 23:12 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/19/18 23:12 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 10/19/18 23:12 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/19/18 23:12 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/19/18 23:12 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/19/18 23:12 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/19/18 23:12 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/19/18 23:12 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/19/18 23:12 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/19/18 23:12 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/19/18 23:12 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/19/18 23:12 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/19/18 23:12 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/19/18 23:12 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/19/18 23:12 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/19/18 23:12 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/19/18 23:12 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/19/18 23:12 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/19/18 23:12 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/19/18 23:12 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/19/18 23:12 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/19/18 23:12 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 10/19/18 23:12 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/19/18 23:12 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/19/18 23:12 103-65-10.50 0.25 1
Styrene ND ug/L 10/19/18 23:12 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/18 23:12 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/18 23:12 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
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Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-05 Lab ID: 92403459005 Collected: 10/12/18 10:30 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 10/19/18 23:12 127-18-40.50 0.25 1
Toluene ND ug/L 10/19/18 23:12 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/19/18 23:12 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/19/18 23:12 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/19/18 23:12 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/19/18 23:12 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/19/18 23:12 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/19/18 23:12 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/19/18 23:12 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/19/18 23:12 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/19/18 23:12 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/19/18 23:12 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/19/18 23:12 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/19/18 23:12 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)91 %10/19/18 23:12 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %10/19/18 23:12 460-00-470-130 1
Toluene-d8 (S)99 %10/19/18 23:12 2037-26-570-130 1
Sample: MW-06 Lab ID: 92403459006 Collected: 10/12/18 11:45 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 10/19/18 23:28 71-43-20.50 0.25 1
Bromobenzene ND ug/L 10/19/18 23:28 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 10/19/18 23:28 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 10/19/18 23:28 75-27-40.50 0.25 1
Bromoform ND ug/L 10/19/18 23:28 75-25-20.50 0.25 1
Bromomethane ND ug/L 10/19/18 23:28 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 10/19/18 23:28 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 10/19/18 23:28 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 10/19/18 23:28 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 10/19/18 23:28 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 10/19/18 23:28 108-90-70.50 0.25 1
Chloroethane ND ug/L 10/19/18 23:28 75-00-31.0 0.50 1
Chloroform ND ug/L 10/19/18 23:28 67-66-30.50 0.25 1
Chloromethane ND ug/L 10/19/18 23:28 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 10/19/18 23:28 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 10/19/18 23:28 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/18 23:28 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 10/19/18 23:28 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/18 23:28 106-93-40.50 0.25 1
Dibromomethane ND ug/L 10/19/18 23:28 74-95-30.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
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Huntersville, NC 28078
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Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92403459
WBS 30173.156
Sample: MW-06 Lab ID: 92403459006 Collected: 10/12/18 11:45 Received: 10/15/18 13:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,2-Dichlorobenzene ND ug/L 10/19/18 23:28 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 10/19/18 23:28 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 10/19/18 23:28 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 10/19/18 23:28 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 10/19/18 23:28 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 10/19/18 23:28 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 10/19/18 23:28 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 10/19/18 23:28 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 10/19/18 23:28 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 10/19/18 23:28 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 10/19/18 23:28 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 10/19/18 23:28 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 10/19/18 23:28 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 10/19/18 23:28 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 10/19/18 23:28 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 10/19/18 23:28 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 10/19/18 23:28 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 10/19/18 23:28 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 10/19/18 23:28 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 10/19/18 23:28 75-09-22.0 1.0 1
Methyl-tert-butyl ether 0.34J ug/L 10/19/18 23:28 1634-04-40.50 0.25 1
Naphthalene ND ug/L 10/19/18 23:28 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 10/19/18 23:28 103-65-10.50 0.25 1
Styrene ND ug/L 10/19/18 23:28 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/18 23:28 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/18 23:28 79-34-50.50 0.25 1
Tetrachloroethene ND ug/L 10/19/18 23:28 127-18-40.50 0.25 1
Toluene ND ug/L 10/19/18 23:28 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 10/19/18 23:28 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 10/19/18 23:28 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 10/19/18 23:28 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 10/19/18 23:28 79-00-50.50 0.25 1
Trichloroethene ND ug/L 10/19/18 23:28 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 10/19/18 23:28 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 10/19/18 23:28 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 10/19/18 23:28 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 10/19/18 23:28 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 10/19/18 23:28 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 10/19/18 23:28 179601-23-11.0 0.50 1
o-Xylene ND ug/L 10/19/18 23:28 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %10/19/18 23:28 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %10/19/18 23:28 460-00-470-130 1
Toluene-d8 (S)101 %10/19/18 23:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
437261
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92403459002, 92403459003, 92403459004, 92403459005, 92403459006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2405009
Associated Lab Samples:92403459002, 92403459003, 92403459004, 92403459005, 92403459006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/19/18 19:590.25
1,1,1-Trichloroethane ug/L ND 0.50 10/19/18 19:590.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/19/18 19:590.25
1,1,2-Trichloroethane ug/L ND 0.50 10/19/18 19:590.25
1,1-Dichloroethane ug/L ND 0.50 10/19/18 19:590.25
1,1-Dichloroethene ug/L ND 0.50 10/19/18 19:590.25
1,1-Dichloropropene ug/L ND 0.50 10/19/18 19:590.25
1,2,3-Trichlorobenzene ug/L ND 2.0 10/19/18 19:591.0
1,2,3-Trichloropropane ug/L ND 0.50 10/19/18 19:590.25
1,2,4-Trichlorobenzene ug/L ND 2.0 10/19/18 19:591.0
1,2,4-Trimethylbenzene ug/L ND 0.50 10/19/18 19:590.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/19/18 19:590.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/19/18 19:590.25
1,2-Dichlorobenzene ug/L ND 0.50 10/19/18 19:590.25
1,2-Dichloroethane ug/L ND 0.50 10/19/18 19:590.25
1,2-Dichloropropane ug/L ND 0.50 10/19/18 19:590.25
1,3,5-Trimethylbenzene ug/L ND 0.50 10/19/18 19:590.25
1,3-Dichlorobenzene ug/L ND 0.50 10/19/18 19:590.25
1,3-Dichloropropane ug/L ND 0.50 10/19/18 19:590.25
1,4-Dichlorobenzene ug/L ND 0.50 10/19/18 19:590.25
2,2-Dichloropropane ug/L ND 0.50 10/19/18 19:590.25
2-Chlorotoluene ug/L ND 0.50 10/19/18 19:590.25
4-Chlorotoluene ug/L ND 0.50 10/19/18 19:590.25
Benzene ug/L ND 0.50 10/19/18 19:590.25
Bromobenzene ug/L ND 0.50 10/19/18 19:590.25
Bromochloromethane ug/L ND 0.50 10/19/18 19:590.25
Bromodichloromethane ug/L ND 0.50 10/19/18 19:590.25
Bromoform ug/L ND 0.50 10/19/18 19:590.25
Bromomethane ug/L ND 5.0 10/19/18 19:592.5
Carbon tetrachloride ug/L ND 0.50 10/19/18 19:590.25
Chlorobenzene ug/L ND 0.50 10/19/18 19:590.25
Chloroethane ug/L ND 1.0 10/19/18 19:590.50
Chloroform ug/L ND 0.50 10/19/18 19:590.25
Chloromethane ug/L ND 1.0 10/19/18 19:590.50
cis-1,2-Dichloroethene ug/L ND 0.50 10/19/18 19:590.25
cis-1,3-Dichloropropene ug/L ND 0.50 10/19/18 19:590.25
Dibromochloromethane ug/L ND 0.50 10/19/18 19:590.25
Dibromomethane ug/L ND 0.50 10/19/18 19:590.25
Dichlorodifluoromethane ug/L ND 0.50 10/19/18 19:590.25
Diisopropyl ether ug/L ND 0.50 10/19/18 19:590.25
Ethylbenzene ug/L ND 0.50 10/19/18 19:590.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2405009
Associated Lab Samples:92403459002, 92403459003, 92403459004, 92403459005, 92403459006
Matrix: Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 10/19/18 19:591.0
Isopropylbenzene (Cumene)ug/L ND 0.50 10/19/18 19:590.25
m&p-Xylene ug/L ND 1.0 10/19/18 19:590.50
Methyl-tert-butyl ether ug/L ND 0.50 10/19/18 19:590.25
Methylene Chloride ug/L ND 2.0 10/19/18 19:591.0
n-Butylbenzene ug/L ND 0.50 10/19/18 19:590.25
n-Propylbenzene ug/L ND 0.50 10/19/18 19:590.25
Naphthalene ug/L ND 2.0 10/19/18 19:591.0
o-Xylene ug/L ND 0.50 10/19/18 19:590.25
sec-Butylbenzene ug/L ND 0.50 10/19/18 19:590.25
Styrene ug/L ND 0.50 10/19/18 19:590.25
tert-Butylbenzene ug/L ND 0.50 10/19/18 19:590.25
Tetrachloroethene ug/L ND 0.50 10/19/18 19:590.25
Toluene ug/L ND 0.50 10/19/18 19:590.25
trans-1,2-Dichloroethene ug/L ND 0.50 10/19/18 19:590.25
trans-1,3-Dichloropropene ug/L ND 0.50 10/19/18 19:590.25
Trichloroethene ug/L ND 0.50 10/19/18 19:590.25
Trichlorofluoromethane ug/L ND 1.0 10/19/18 19:590.50
Vinyl chloride ug/L ND 1.0 10/19/18 19:590.50
1,2-Dichloroethane-d4 (S)%95 70-130 10/19/18 19:59
4-Bromofluorobenzene (S)%94 70-130 10/19/18 19:59
Toluene-d8 (S)%100 70-130 10/19/18 19:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2405010LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.550 93 60-140
1,1,1-Trichloroethane ug/L 42.950 86 60-140
1,1,2,2-Tetrachloroethane ug/L 46.150 92 60-140
1,1,2-Trichloroethane ug/L 46.950 94 60-140
1,1-Dichloroethane ug/L 42.650 85 60-140
1,1-Dichloroethene ug/L 45.250 90 60-140
1,1-Dichloropropene ug/L 46.950 94 60-140
1,2,3-Trichlorobenzene ug/L 45.550 91 60-140
1,2,3-Trichloropropane ug/L 49.550 99 60-140
1,2,4-Trichlorobenzene ug/L 48.150 96 60-140
1,2,4-Trimethylbenzene ug/L 44.750 89 60-140
1,2-Dibromo-3-chloropropane ug/L 44.550 89 60-140
1,2-Dibromoethane (EDB)ug/L 48.850 98 60-140
1,2-Dichlorobenzene ug/L 48.350 97 60-140
1,2-Dichloroethane ug/L 44.550 89 60-140
1,2-Dichloropropane ug/L 46.250 92 60-140
1,3,5-Trimethylbenzene ug/L 44.650 89 60-140
1,3-Dichlorobenzene ug/L 46.850 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2405010LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 50.250 100 60-140
1,4-Dichlorobenzene ug/L 47.450 95 60-140
2,2-Dichloropropane ug/L 44.550 89 60-140
2-Chlorotoluene ug/L 44.350 89 60-140
4-Chlorotoluene ug/L 44.550 89 60-140
Benzene ug/L 46.250 92 60-140
Bromobenzene ug/L 48.250 96 60-140
Bromochloromethane ug/L 51.250 102 60-140
Bromodichloromethane ug/L 44.750 89 60-140
Bromoform ug/L 46.250 92 60-140
Bromomethane ug/L 38.150 76 60-140
Carbon tetrachloride ug/L 45.950 92 60-140
Chlorobenzene ug/L 47.850 96 60-140
Chloroethane ug/L 39.050 78 60-140
Chloroform ug/L 48.250 96 60-140
Chloromethane ug/L 38.150 76 60-140
cis-1,2-Dichloroethene ug/L 43.150 86 60-140
cis-1,3-Dichloropropene ug/L 47.850 96 60-140
Dibromochloromethane ug/L 48.050 96 60-140
Dibromomethane ug/L 51.150 102 60-140
Dichlorodifluoromethane ug/L 47.250 94 60-140
Diisopropyl ether ug/L 42.050 84 60-140
Ethylbenzene ug/L 45.350 91 60-140
Hexachloro-1,3-butadiene ug/L 43.850 88 60-140
Isopropylbenzene (Cumene)ug/L 47.450 95 60-140
m&p-Xylene ug/L 91.7100 92 60-140
Methyl-tert-butyl ether ug/L 45.150 90 60-140
Methylene Chloride ug/L 44.550 89 60-140
n-Butylbenzene ug/L 46.450 93 60-140
n-Propylbenzene ug/L 45.250 90 60-140
Naphthalene ug/L 46.550 93 60-140
o-Xylene ug/L 47.350 95 60-140
sec-Butylbenzene ug/L 46.250 92 60-140
Styrene ug/L 46.050 92 60-140
tert-Butylbenzene ug/L 40.150 80 60-140
Tetrachloroethene ug/L 45.250 90 60-140
Toluene ug/L 43.050 86 60-140
trans-1,2-Dichloroethene ug/L 44.850 90 60-140
trans-1,3-Dichloropropene ug/L 44.950 90 60-140
Trichloroethene ug/L 47.850 96 60-140
Trichlorofluoromethane ug/L 45.150 90 60-140
Vinyl chloride ug/L 48.050 96 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2405814MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403459006
2405815
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 60-140103 1 3020ND20.5 20.7
1,1,1-Trichloroethane ug/L 20 95 60-140102 7 3020ND19.0 20.5
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140102 2 3020ND20.1 20.5
1,1,2-Trichloroethane ug/L 20 102 60-140107 5 3020ND20.5 21.5
1,1-Dichloroethane ug/L 20 93 60-14098 5 3020ND18.7 19.6
1,1-Dichloroethene ug/L 20 99 60-140101 3 3020ND19.7 20.2
1,1-Dichloropropene ug/L 20 106 60-140107 1 3020ND21.2 21.4
1,2,3-Trichlorobenzene ug/L 20 98 60-14099 1 3020ND19.6 19.8
1,2,3-Trichloropropane ug/L 20 104 60-140107 3 3020ND20.9 21.4
1,2,4-Trichlorobenzene ug/L 20 106 60-140104 1 3020ND21.1 20.9
1,2,4-Trimethylbenzene ug/L 20 102 60-140101 2 3020ND20.4 20.1
1,2-Dibromo-3-chloropropane ug/L 20 99 60-14098 1 3020ND19.8 19.6
1,2-Dibromoethane (EDB) ug/L 20 107 60-140110 3 3020ND21.3 22.0
1,2-Dichlorobenzene ug/L 20 108 60-140108 0 3020ND21.7 21.6
1,2-Dichloroethane ug/L 20 95 60-140102 7 3020ND18.9 20.4
1,2-Dichloropropane ug/L 20 104 60-140109 5 3020ND20.8 21.9
1,3,5-Trimethylbenzene ug/L 20 104 60-140102 2 3020ND20.9 20.5
1,3-Dichlorobenzene ug/L 20 105 60-140104 1 3020ND21.0 20.8
1,3-Dichloropropane ug/L 20 111 60-140114 3 3020ND22.3 22.9
1,4-Dichlorobenzene ug/L 20 107 60-140106 1 3020ND21.4 21.2
2,2-Dichloropropane ug/L 20 89 60-14095 7 3020ND17.8 19.0
2-Chlorotoluene ug/L 20 102 60-14099 3 3020ND20.4 19.9
4-Chlorotoluene ug/L 20 103 60-140102 1 3020ND20.6 20.4
Benzene ug/L 20 103 60-140110 7 3020ND20.5 22.0
Bromobenzene ug/L 20 110 60-140109 1 3020ND22.0 21.8
Bromochloromethane ug/L 20 113 60-140118 4 3020ND22.6 23.5
Bromodichloromethane ug/L 20 95 60-140104 9 3020ND19.0 20.8
Bromoform ug/L 20 99 60-140100 1 3020ND19.9 20.1
Bromomethane ug/L 20 68 60-14070 2 3020ND13.6 13.9
Carbon tetrachloride ug/L 20 103 60-140113 10 3020ND20.6 22.7
Chlorobenzene ug/L 20 108 60-140109 1 3020ND21.6 21.8
Chloroethane ug/L 20 81 60-14081 0 3020ND16.2 16.2
Chloroform ug/L 20 102 60-140107 4 3020ND20.5 21.3
Chloromethane ug/L 20 67 60-14069 3 3020ND13.3 13.8
cis-1,2-Dichloroethene ug/L 20 96 60-140101 4 3020ND19.3 20.1
cis-1,3-Dichloropropene ug/L 20 101 60-140111 9 3020ND20.2 22.2
Dibromochloromethane ug/L 20 106 60-140106 0 3020ND21.3 21.2
Dibromomethane ug/L 20 110 60-140119 7 3020ND22.1 23.7
Dichlorodifluoromethane ug/L 20 68 60-14063 8 3020ND13.7 12.6
Diisopropyl ether ug/L 20 90 60-14094 5 3020ND18.0 18.9
Ethylbenzene ug/L 20 104 60-140105 1 3020ND20.7 20.9
Hexachloro-1,3-butadiene ug/L 20 96 60-140100 4 3020ND19.2 20.0
Isopropylbenzene (Cumene) ug/L 20 107 60-140109 1 3020ND21.5 21.8
m&p-Xylene ug/L 40 104 60-140104 0 3040ND41.6 41.6
Methyl-tert-butyl ether ug/L 20 96 60-140101 4 30200.34J 19.6 20.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
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Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2405814MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403459006
2405815
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 85 60-14087 2 3020ND17.0 17.3
n-Butylbenzene ug/L 20 104 60-140104 0 3020ND20.9 20.8
n-Propylbenzene ug/L 20 104 60-140103 1 3020ND20.7 20.5
Naphthalene ug/L 20 101 60-14099 1 3020ND20.1 19.9
o-Xylene ug/L 20 104 60-140110 6 3020ND20.8 22.1
sec-Butylbenzene ug/L 20 106 60-140106 0 3020ND21.3 21.2
Styrene ug/L 20 103 60-140103 0 3020ND20.6 20.7
tert-Butylbenzene ug/L 20 94 60-14093 1 3020ND18.8 18.6
Tetrachloroethene ug/L 20 101 60-140103 2 3020ND20.3 20.7
Toluene ug/L 20 98 60-140104 6 3020ND19.6 20.8
trans-1,2-Dichloroethene ug/L 20 97 60-140102 4 3020ND19.5 20.4
trans-1,3-Dichloropropene ug/L 20 93 60-140103 10 3020ND18.6 20.6
Trichloroethene ug/L 20 106 60-140115 8 3020ND21.2 22.9
Trichlorofluoromethane ug/L 20 99 60-14097 2 3020ND19.7 19.4
Vinyl chloride ug/L 20 93 60-14090 3 3020ND18.5 17.9
1,2-Dichloroethane-d4 (S)%92 70-13091
4-Bromofluorobenzene (S) %94 70-13094
Toluene-d8 (S)%96 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
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Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
437453
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92403459001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2405880
Associated Lab Samples:92403459001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/20/18 13:130.25
1,1,1-Trichloroethane ug/L ND 0.50 10/20/18 13:130.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/20/18 13:130.25
1,1,2-Trichloroethane ug/L ND 0.50 10/20/18 13:130.25
1,1-Dichloroethane ug/L ND 0.50 10/20/18 13:130.25
1,1-Dichloroethene ug/L ND 0.50 10/20/18 13:130.25
1,1-Dichloropropene ug/L ND 0.50 10/20/18 13:130.25
1,2,3-Trichlorobenzene ug/L ND 2.0 10/20/18 13:131.0
1,2,3-Trichloropropane ug/L ND 0.50 10/20/18 13:130.25
1,2,4-Trichlorobenzene ug/L ND 2.0 10/20/18 13:131.0
1,2,4-Trimethylbenzene ug/L ND 0.50 10/20/18 13:130.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/20/18 13:130.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/20/18 13:130.25
1,2-Dichlorobenzene ug/L ND 0.50 10/20/18 13:130.25
1,2-Dichloroethane ug/L ND 0.50 10/20/18 13:130.25
1,2-Dichloropropane ug/L ND 0.50 10/20/18 13:130.25
1,3,5-Trimethylbenzene ug/L ND 0.50 10/20/18 13:130.25
1,3-Dichlorobenzene ug/L ND 0.50 10/20/18 13:130.25
1,3-Dichloropropane ug/L ND 0.50 10/20/18 13:130.25
1,4-Dichlorobenzene ug/L ND 0.50 10/20/18 13:130.25
2,2-Dichloropropane ug/L ND 0.50 10/20/18 13:130.25
2-Chlorotoluene ug/L ND 0.50 10/20/18 13:130.25
4-Chlorotoluene ug/L ND 0.50 10/20/18 13:130.25
Benzene ug/L ND 0.50 10/20/18 13:130.25
Bromobenzene ug/L ND 0.50 10/20/18 13:130.25
Bromochloromethane ug/L ND 0.50 10/20/18 13:130.25
Bromodichloromethane ug/L ND 0.50 10/20/18 13:130.25
Bromoform ug/L ND 0.50 10/20/18 13:130.25
Bromomethane ug/L ND 5.0 10/20/18 13:132.5
Carbon tetrachloride ug/L ND 0.50 10/20/18 13:130.25
Chlorobenzene ug/L ND 0.50 10/20/18 13:130.25
Chloroethane ug/L ND 1.0 10/20/18 13:130.50
Chloroform ug/L ND 0.50 10/20/18 13:130.25
Chloromethane ug/L ND 1.0 10/20/18 13:130.50
cis-1,2-Dichloroethene ug/L ND 0.50 10/20/18 13:130.25
cis-1,3-Dichloropropene ug/L ND 0.50 10/20/18 13:130.25
Dibromochloromethane ug/L ND 0.50 10/20/18 13:130.25
Dibromomethane ug/L ND 0.50 10/20/18 13:130.25
Dichlorodifluoromethane ug/L ND 0.50 10/20/18 13:130.25
Diisopropyl ether ug/L ND 0.50 10/20/18 13:130.25
Ethylbenzene ug/L ND 0.50 10/20/18 13:130.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2405880
Associated Lab Samples:92403459001
Matrix: Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 10/20/18 13:131.0
Isopropylbenzene (Cumene)ug/L ND 0.50 10/20/18 13:130.25
m&p-Xylene ug/L ND 1.0 10/20/18 13:130.50
Methyl-tert-butyl ether ug/L ND 0.50 10/20/18 13:130.25
Methylene Chloride ug/L ND 2.0 10/20/18 13:131.0
n-Butylbenzene ug/L ND 0.50 10/20/18 13:130.25
n-Propylbenzene ug/L ND 0.50 10/20/18 13:130.25
Naphthalene ug/L ND 2.0 10/20/18 13:131.0
o-Xylene ug/L ND 0.50 10/20/18 13:130.25
sec-Butylbenzene ug/L ND 0.50 10/20/18 13:130.25
Styrene ug/L ND 0.50 10/20/18 13:130.25
tert-Butylbenzene ug/L ND 0.50 10/20/18 13:130.25
Tetrachloroethene ug/L ND 0.50 10/20/18 13:130.25
Toluene ug/L ND 0.50 10/20/18 13:130.25
trans-1,2-Dichloroethene ug/L ND 0.50 10/20/18 13:130.25
trans-1,3-Dichloropropene ug/L ND 0.50 10/20/18 13:130.25
Trichloroethene ug/L ND 0.50 10/20/18 13:130.25
Trichlorofluoromethane ug/L ND 1.0 10/20/18 13:130.50
Vinyl chloride ug/L ND 1.0 10/20/18 13:130.50
1,2-Dichloroethane-d4 (S)%93 70-130 10/20/18 13:13
4-Bromofluorobenzene (S)%94 70-130 10/20/18 13:13
Toluene-d8 (S)%100 70-130 10/20/18 13:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2405881LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.150 98 60-140
1,1,1-Trichloroethane ug/L 45.350 91 60-140
1,1,2,2-Tetrachloroethane ug/L 47.650 95 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 43.550 87 60-140
1,1-Dichloroethene ug/L 46.250 92 60-140
1,1-Dichloropropene ug/L 48.250 96 60-140
1,2,3-Trichlorobenzene ug/L 49.150 98 60-140
1,2,3-Trichloropropane ug/L 50.650 101 60-140
1,2,4-Trichlorobenzene ug/L 51.450 103 60-140
1,2,4-Trimethylbenzene ug/L 47.150 94 60-140
1,2-Dibromo-3-chloropropane ug/L 46.950 94 60-140
1,2-Dibromoethane (EDB)ug/L 50.350 101 60-140
1,2-Dichlorobenzene ug/L 50.650 101 60-140
1,2-Dichloroethane ug/L 45.350 91 60-140
1,2-Dichloropropane ug/L 48.050 96 60-140
1,3,5-Trimethylbenzene ug/L 47.250 94 60-140
1,3-Dichlorobenzene ug/L 49.850 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2405881LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.850 104 60-140
1,4-Dichlorobenzene ug/L 50.350 101 60-140
2,2-Dichloropropane ug/L 46.050 92 60-140
2-Chlorotoluene ug/L 46.250 92 60-140
4-Chlorotoluene ug/L 47.350 95 60-140
Benzene ug/L 48.050 96 60-140
Bromobenzene ug/L 50.650 101 60-140
Bromochloromethane ug/L 52.050 104 60-140
Bromodichloromethane ug/L 47.350 95 60-140
Bromoform ug/L 48.850 98 60-140
Bromomethane ug/L 38.450 77 60-140
Carbon tetrachloride ug/L 48.650 97 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 39.950 80 60-140
Chloroform ug/L 50.550 101 60-140
Chloromethane ug/L 37.950 76 60-140
cis-1,2-Dichloroethene ug/L 44.850 90 60-140
cis-1,3-Dichloropropene ug/L 49.950 100 60-140
Dibromochloromethane ug/L 52.450 105 60-140
Dibromomethane ug/L 52.650 105 60-140
Dichlorodifluoromethane ug/L 45.550 91 60-140
Diisopropyl ether ug/L 44.150 88 60-140
Ethylbenzene ug/L 47.250 94 60-140
Hexachloro-1,3-butadiene ug/L 46.850 94 60-140
Isopropylbenzene (Cumene)ug/L 50.250 100 60-140
m&p-Xylene ug/L 95.2100 95 60-140
Methyl-tert-butyl ether ug/L 45.650 91 60-140
Methylene Chloride ug/L 44.850 90 60-140
n-Butylbenzene ug/L 49.350 99 60-140
n-Propylbenzene ug/L 47.250 94 60-140
Naphthalene ug/L 49.950 100 60-140
o-Xylene ug/L 50.050 100 60-140
sec-Butylbenzene ug/L 48.650 97 60-140
Styrene ug/L 49.050 98 60-140
tert-Butylbenzene ug/L 42.350 85 60-140
Tetrachloroethene ug/L 48.350 97 60-140
Toluene ug/L 45.750 91 60-140
trans-1,2-Dichloroethene ug/L 45.950 92 60-140
trans-1,3-Dichloropropene ug/L 47.850 96 60-140
Trichloroethene ug/L 49.650 99 60-140
Trichlorofluoromethane ug/L 46.050 92 60-140
Vinyl chloride ug/L 48.950 98 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2405882MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403580004
2405883
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 500 101 60-140105 4 30500ND507 527
1,1,1-Trichloroethane ug/L 500 95 60-14098 3 30500ND474 489
1,1,2,2-Tetrachloroethane ug/L 500 100 60-140102 2 30500ND500 511
1,1,2-Trichloroethane ug/L 500 100 60-140103 3 30500ND498 515
1,1-Dichloroethane ug/L 500 92 60-14096 4 30500ND460 478
1,1-Dichloroethene ug/L 500 101 60-140100 1 30500ND506 500
1,1-Dichloropropene ug/L 500 102 60-140107 5 30500ND510 537
1,2,3-Trichlorobenzene ug/L 500 94 60-140101 6 30500ND472 503
1,2,3-Trichloropropane ug/L 500 106 60-140104 2 30500ND531 522
1,2,4-Trichlorobenzene ug/L 500 100 60-140104 5 30500ND498 522
1,2,4-Trimethylbenzene ug/L 500 98 60-14096 1 30500278767 760
1,2-Dibromo-3-chloropropane ug/L 500 95 60-14096 2 30500ND475 482
1,2-Dibromoethane (EDB) ug/L 500 107 60-140106 1 30500ND533 529
1,2-Dichlorobenzene ug/L 500 103 60-140108 5 30500ND515 539
1,2-Dichloroethane ug/L 500 94 60-14099 4 30500151623 646
1,2-Dichloropropane ug/L 500 101 60-140102 1 30500ND505 510
1,3,5-Trimethylbenzene ug/L 500 111 60-140114 2 30500ND557 570
1,3-Dichlorobenzene ug/L 500 101 60-140104 3 30500ND507 520
1,3-Dichloropropane ug/L 500 107 60-140112 5 30500ND533 560
1,4-Dichlorobenzene ug/L 500 104 60-140104 1 30500ND519 522
2,2-Dichloropropane ug/L 500 90 60-14091 1 30500ND449 453
2-Chlorotoluene ug/L 500 102 60-140104 2 30500ND510 519
4-Chlorotoluene ug/L 500 99 60-140100 2 30500ND493 502
Benzene ug/L 500 71 60-14074 1 3050031403490 3510
Bromobenzene ug/L 500 107 60-140106 0 30500ND534 532
Bromochloromethane ug/L 500 112 60-140113 1 30500ND559 567
Bromodichloromethane ug/L 500 96 60-140100 4 30500ND482 499
Bromoform ug/L 500 95 60-14098 3 30500ND473 489
Bromomethane ug/L 500 62 60-14066 7 30500ND310 332
Carbon tetrachloride ug/L 500 103 60-140106 3 30500ND515 532
Chlorobenzene ug/L 500 104 60-140107 2 30500ND522 533
Chloroethane ug/L 500 82 60-14081 1 30500ND409 405
Chloroform ug/L 500 106 60-140108 2 30500ND529 539
Chloromethane ug/L 500 74 60-14073 1 30500ND369 365
cis-1,2-Dichloroethene ug/L 500 93 60-14098 5 30500ND467 492
cis-1,3-Dichloropropene ug/L 500 97 60-140100 3 30500ND487 500
Dibromochloromethane ug/L 500 105 60-140105 0 30500ND526 525
Dibromomethane ug/L 500 108 60-140112 4 30500ND539 562
Dichlorodifluoromethane ug/L 500 82 60-14072 12 30500ND408 360
Diisopropyl ether ug/L 500 89 60-14093 4 30500103550 570
Ethylbenzene ug/L 500 101 60-140102 0 30500280786 789
Hexachloro-1,3-butadiene ug/L 500 94 60-14095 2 30500ND468 476
Isopropylbenzene (Cumene) ug/L 500 109 60-140110 0 30500ND546 548
m&p-Xylene ug/L 1000 102 60-140102 0 3010007491770 1770
Methyl-tert-butyl ether ug/L 500 89 60-14095 2 305009181360 1390
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
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Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92403459
WBS 30173.156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2405882MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403580004
2405883
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 500 88 60-14091 4 30500ND438 457
n-Butylbenzene ug/L 500 102 60-140103 1 30500ND510 516
n-Propylbenzene ug/L 500 105 60-140107 1 30500ND525 533
Naphthalene ug/L 500 97 60-140100 2 3050093.3 580 593
o-Xylene ug/L 500 105 60-140110 3 30500297820 846
sec-Butylbenzene ug/L 500 104 60-140104 0 30500ND518 518
Styrene ug/L 500 103 60-140103 0 30500ND513 513
tert-Butylbenzene ug/L 500 89 60-14092 3 30500ND444 459
Tetrachloroethene ug/L 500 103 60-140102 1 30500ND515 512
Toluene ug/L 500 90 60-14091 0 3050013201770 1770
trans-1,2-Dichloroethene ug/L 500 97 60-140100 3 30500ND485 499
trans-1,3-Dichloropropene ug/L 500 93 60-14097 4 30500ND466 486
Trichloroethene ug/L 500 107 60-140108 1 30500ND534 538
Trichlorofluoromethane ug/L 500 100 60-14099 1 30500ND502 495
Vinyl chloride ug/L 500 97 60-14094 3 30500ND484 470
1,2-Dichloroethane-d4 (S)%92 70-13093
4-Bromofluorobenzene (S) %98 70-13095
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92403459
WBS 30173.156
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92403459
WBS 30173.156
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92403459001 437453MW-01 SM 6200B
92403459002 437261MW-02 SM 6200B
92403459003 437261MW-03 SM 6200B
92403459004 437261MW-04 SM 6200B
92403459005 437261MW-05 SM 6200B
92403459006 437261MW-06 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/22/2018 11:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 28
Page 26 of 28
Document Name: Document Revised: February 7, 2018
;aeAnalyticat° Sample Condition Upon Receipt(SCUR) Page 1of2
Document No.: Issuing Authority:
F~CAR·C-S-033-·Rev.o:; Pac-~-Garollna-s-Quality--Gffi€:
Laboratory receiving samples:
Asheville D EdenO Greenwood D Huntersvllle,12f Ralelgh0 MechanlcsvilleO
Sample Condition
Upon Receipt
Client Name: , I
/ (1~1LJjv Project I LJO# · 924Cl3459
1111111111111111111111 Courier: v[]Fed Ex
OP ace
OuPs OusPs 0Client
0 Commercial
Custody Seal Present? Oves ~o
Packing Material: 0Bubble Wrap
Thermo me~: '-lZJ IR Gun ID: 92T045
Oather: __
Seals Intact? Oves
/ \[21Bubble Bags 0None 0 Other
Type of Ice: v DWet 0Blue
Cooler Temp ('Cl: 7._ -(J Correction Factor: Add/Subtract ("Cl -0 l \ 'C\ Cooler Temp Corrected ('Cl:-----
USDA Regulated Soll (q/~'/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NV, or SC (check maps)?
Oves 0No
Chain of Custody Present? ~ 0No ON/A 1.
Samples Arrived within Hold nme? ie:{ves 0No ON/A 2.
Short Hold Time Analysis (<72 hr.)? Ove.s n 1' ON/A 3.
Rush Turn Around Time Requested? Oves \.eJNo ON/A 4.
Sufficient Volume 7 \~ 0No O N/A 5.
,r Correct Containers Used? \12'.Jves 0No ON/A 6.
-Pace containers Used? 10ves 0 No ON/A
Containers Intact? ,_efves 0No ON/A 7 .
Dissolved analysis: Samples Field Filtered? Oves 0 No .Qt1/A 8,
Sample Labels Match COC? C3ves v' 0No ON/A 9.
·Includes Date/Time/ID/ Analysis Matrix: \,/\
Headspace in VOA Vials (>S-6mm)? O ves ~ OrJ/A 10.
Trip Blank Present? O ves QNo \£JN/A ll.
Trip Blank Custody Seals Present? Oves 0No '~A
COMMENTS/SAMPLE DISCREPANCY
92403459
v-"p I c_, ( S ,-l ( Date/lnitl!ls Person Examining Contenu:, ___ _
ON one
Blologlcal Tissue y ozen?
Oves 0No 1'.'.'.]N/A
Temp should be above freezing to 6°C
Osamples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? Oves 0 No
Comments/Discrepancy:
Fleld Data Required7 O ves 0No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:------------------Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: 19~ Date: ----'-'/(o"------
Page 27 of 28
~eAnatytica( Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recelpt(SCUR) Page 1of2
Document No.: Issuing Authority:
'"·CAR·'S·033-Rev.o: PaGe-Caroli11aS-Quality-Offic::
Project# rlJO# · 92403459 *Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples. PH: PTE Due Dale : 10/22/18
Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
! "'O g g ... ' (! g ~ < < ::c g ., ~ g 0 "' < ...... ...... < :!! £ ~ ~ "' ...... ~ ...... N" N' z ;:;:; Q. ~ 'N "C "'O "2 £ ~ .... c "O 'N :::> "' v "' QI "O v v I\ "'O (! v (! (! (! ::c ~ "' 'N ::c QI ::c ::c .~ (! "' :c .e ~ "' :!( (! .e .e ro .e v "' "' .e ~ ~ ~ QI ... Qi "' :!( ::c ., .. "' "' "' Ci. 0 Q. Q. Q. QI 0 0 u ::c .. ~ .e ... c c c Ci. "' <C. 0 15 Q. c 0 ~ :::> :::> :::> N z z "' c u :::> "' c :c ::c z "'O N :c N :::> ::c -~ u u :::> u ., ~ :c --~ ~ u .,
-~ -~ ·~ t: t: .:::. cu (U .t:I -., :; ., ·..o "' "' "' "' .. .. .)! "' 0 J:I J:I E J:I E c:: c:: ii: "' ii: Q. c:: E E <C. E c:: a.. E <C. <C. <C. ... ... .... ..... ... ..... ..... < ..... E E E ~ E E "E E .;, ~ E ~ E "'O ~ ~ VI 0 0 "' 0 "' Ill ~ 0 0 N "' 0 "' "' N N V'I Ill .... N "' .... .... N .... .... .... .... "l' ... N .. ::; ::; ::::, ::; .;, z ,.:. v :> :::, ± ::I ~ :Ii e ... ... "' N ... ... "' ~ ... l:l ... .. "' ~ a.. c.. c.. c.. c.. c.. a.. 3 l:l l:l ~ ~ l:l m m m CD CD co CD IQ < < <
1 I~ I\ I\ I\ ~ I'\ '\ ~
2 ~ ~ ~ I\ ~ I'\ I'\ ~
3 I\ ~ I\ I\ I\ I\ I\ I\
4 I\ I\ I\ I~ ~ I'\ I\ I\
s I'\ I\ I\ I\ I\ I\ I\ I\
6 I\ ~ I\ I\ I\ ~ I\ I\
7 ~ ~ '\ I\ I\ ~ I\ I\
8 I~ ~ I\ I\ I\ ~ I\ '\
9 I~ ·~ I\ I~ I'\ ~ I~ I'\
10 I~ ~ ~ I~ I\ ~ I\ I'\
11 i\ \ '\ I'\ I\ \ I\ I\
12 ~ ~ ~ I~ I\ ~ I\ I'\
CLIENT : 92-NCDOTNE
g
~ ;:: < :0 ~ ~ ~ ...... ~ ~ ~ .!l! "' u I !l!. ~ I ... ~ ~ ;;; <f ::c <C. ~ a z ~ .>::: "' ..._
~ .. ~ .... "' cu < ~ ~ \!) -~ ~ "' "' ...... u .t:I ...... 0 ,... ::c ~ E ~ ~ .. 0 0.. "' ::c
<C. N 0 ~ > "' .. ~ "' Q. 0.. ii: ii: N '.'e' -t: ... u "' c ,.., u .!! E ::c z :::> ::c .... :¥ ~ ·;:; ·;::: ·;: "' 0 <C. < <f < ;; Ci ~ e .. "' 0 0 0 0 a. c:: "l' > > > a. VI VI > .. ..... ..... < e e ..... e ~ JD ..... E E "' E .!! E
8 > > ti\ 0 0 0 0 0 0 ~ N "' "' ., ., "i ., !!. .... N N ~ ::c Iii :::> c.. ¥ ¥ t;:; ~ < < OI en en l:l N "' l:l l:l l:l l:l l:l 0 '>' c.. c.. c.. < c > > c > "' Ill m
~ t ( I~ I~ I'\ 'i I~ I~ I\ \' I\ \ I'\ ~1 I'\ !\
I'\ l I\ \ I'\ \ 1 ~ \
~ I\ '\
~ ~ '\
I~ ~ '\
i~ ~ '\
1\ .\ I'\
~ ~ '\
pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative
adjusted added
< < ...... ~ ...... ~ "' "' iii iii > ~ ·:; "'O "'O ., ~ (! QI (! ., .!a "' ., ., .. "' ·:; ~ Q. c c Q. :::> .g c :::> cu ~ cu J:I .E J:I E E <C. ·;:; "' <C. ... E e ... E 8 ~ 0 .... N :::, ::, :::, c l;t OI l:l l:l < > c
lot#
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Cert1flcat1on Office 11.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 28 of 28
Section A Required Client Information: Company: CATLIN Enoineers and Scientists Address: 1044 Washington Streel Raleigh, NC 27605 Email: sean.oneilt!l!callinusa.com Phone: [phone] s I Fax Requested Due Date: "'::.~ ''·"'-'\ 1,,.. .\ SAMPLE ID One Character per box. 'II: (A.Z, 0-9 I , ·) ~ Sample Ids must be unique w !:: 1 f"\ "'-.YO ' 2 MW·0'L 3 ('I\ 1 .. \.1"\ ~ 4 tl\.w-04-5 ("\-...j-0:; 6 l'J\,~ \ -() L, 7 8 9 10 11 12 AODtTIONAL COMMENTS ~;:. .......... r-\. M~\..-S \ CHAIN-OF-CUSTODY I Analytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Required Project Information: Invoice Information: Paae : 1 Of Report To: Sean O'Neil Attention: .,., 1 , • • • •. _ Copy To: Company Name: .l,.>, \\ \ ~ L lJ...) \ Address: Purchase Order II: Pace Quote: Project Name: Williamston Gas Site • WBS: 30173. 156 Pace Project Manager: tavlor.ezell@.pacelabs.com. Project#: Pace Profile #: 5838 R8Quested Analvsla Fiitered (YIN) ~ 0:-z 0 ::; Preservatives ):: 0 COLLECTED MATR~ CODE u z Orlnklr gWa1er ow m " 0 8 u ;:: W111te1 WT Ill u W H I Water WN :!! ~ ~ p, .. ,, p ~ -" 0 .., SoollS "" SL m ~ u GI m START END "' I-°" Ol. .... a:: Wipe WP < w .., w w Q, z GI 8 Ai• AR c 0.. ::; ~ ,, "' ., Other OT 0 ~ w ~ "' >. "' u .... z 0 U> Trssu TS x ~ ~ 0 il: ... 0 c: ii ... "' ii: 0.. 0.. u I!! 0 "' :i: (/) .. :;; c D 0 s= c( u .... ::; ::; ... 0. (/) C3 0 "' ;;; s= < < < 0 c: "' z .. .. 0 0 ::; "' DATE TIME DATE TIME "' .. :::> :i: :i: :i: z z ::;: > l<!1 l:; iOiiL \())C 4-x '{., I I io4S j t ~ I 161-0 I. i \ l6lS x x· I ) 10;0 x ~ I " y J-114·S , I 'A ll"\. r AFFtutTION REU~ISHEO BY 1 DATE TIME /'\ACCI PfeD 'y _}1Ftl.IA TtON DATE TIME ~~ ..-"./ IA ...... 1 ) IC>/ /'l. {377 'M Lt 'f0 /JcvCC-i0/1;./fi I ;"L'f.. rt/r)/]J. l/M ~-/()/1.dtt ~#1,J. / .df) #~ ~ 9.1~d -ob ~.,4~.,y .A ~_l"°'_,, j/ ~QI p /:l..-fl 'i!> -1<--.<Y it /flJ { lL/ Z£. fl-/<J#( /v..'/r" I// ,,,.t~~~-A ~;/.> l 1-., Jo; '<7~r2 _/ /1 t · l t...,-1} P":..u , SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: ~ n ~<._ 1 \ SIGNATURE ofSAMPLE'Z::Z ~~ 1' DATE Signed: \b { \ l. I£:. Regulatorv Aaencv State I Location NC ~ .. .!: 0 :c u (ii ~i4a-slf :> ,, ~ ·;;; .. a: ( '\. u .s a. ::;: w ,... I)~\ <J1z_, 6d3 mil oJ( Ii ( t, SAMPLE CONDITIONS ~ t"-'

NCDOT; 211010_2018_MR CATLIN Engineers and Scientists
CATLIN Project No. 211010 November 2018

APPENDIX B

WELL CONSTRUCTION RECORDS
AND
MONITORING WELL LOGS

D.T. Chalmers, Jr.
10/09/18
HSA
35.831585001 77.095530000
4146A
1.51
MW05
Bent. Pellets1
0.5
0.5
0
2 12 PVC
2
Sch. 40
Surface Pour
0 Sch. 40 PVC2
Portland Cement
N/A
1 12
Martin
1
X
11/13/2018
Surface Pour
CATLIN Engineers and Scientists
X
12
2 Slot .010
1740 Prison Camp Rd. 27892, Williamston, NC
#2 Medium Sand Torpedo Sand
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy ofthis record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.
SEE
ATTAC
H
E
D
0.0
5.0
10.0
12.0
4
1
Hand
1
WOH
3
WOH
Auguer
1
WOH
0.5
1.0
12.02" Sch. 40 PVC2" Slot .010Sch. 40 PVC2.0
12.012.0
0.0
72.4
61.9
72.41.51.5
12.0
(SP) - Brown, gravely SAND with ABC stone.
(CL-SW) - Tan & orange, marbled sandy CLAY with
mod-low plasticity.
*Becomes gray color around 4'
BORING TERMINATED AT ELEVATION 61.9 ft
D
D
Sat.
END DATE:10/9/18
OF1
BORING LOCATION:Near road along parking lot
BLOW COUNT
0.5ft
LOCATION:Williamston
START DATE:10/9/18
PROJECT NAME:
0.5ft
WELL ID:
STATE:
MW05
Shawn McGuire
D.T. Chalmers, Jr.
Eddie SwaineEASTING:
DRILL MACHINE:CME 45B METHOD:HSA
COUNTY:Martin
2564483 763008
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
DEPTH
NORTHING:
1
PROJECT NO.:211010
SHEET
3.2
1.5
LOGGED BY:
DRILLER:
CREW:
DOT Martin County GasolineRelease
0.5ft0.5ft
73.90
12.0
12.0
0 HOUR DTW:
24 HOUR DTW:
SYSTEM:NCSP NAD 83 (USft)CATLIN BORING LOG 211010_DOT_MARTIN_CO_GASOLINE_RELEASE.GPJ CATLIN.GDT 11/13/180.0
WELL LOG
Portland Cement Bentonite Pellets #2 Medium Sand
WELL
DETAIL
73.9
ELEVATION
OVA
(ppm)DEPTH
M
OIS
0.0
LAB.
LAND SURFACE
SOIL AND ROCK
DESCRIPTION
LOG
Wilmington, NC211010
D.T. Chalmers, Jr.
10/09/18
HSA
35.831191000 77.097036998
4146A
3.54
MW06
Bent. Pellets1
0.5
0.5
0
2 12 PVC
2
Sch. 40
Surface Pour
0 Sch. 40 PVC2
Portland Cement
N/A
1 12
Martin
1
X
11/13/2018
Surface Pour
CATLIN Engineers and Scientists
X
12
2 Slot .010
1740 Prison Camp Rd. 27892, Williamston, NC
#2 Medium Sand Torpedo Sand
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy ofthis record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.
SEE
ATTAC
H
E
D
0.0
5.0
10.0
12.0
8
2
1
10
WOH
1
9
2
1
9
2
1
0.5
1.0
12.02" Sch. 40 PVC2" Slot .010Sch. 40 PVC2.0
12.012.0
0.0
75.3
67.3
65.3
75.8
67.3
1.5
10.0
2.0
10.0
12.0
(SP) - Brown, gravely SAND with ABC stone.
(CL-SW) - Dark brown, marbled sandy CLAY with
mod-low plasticity.
*Becomes light brown color around 3-4'
(SP) - Tan, fn. SAND.
BORING TERMINATED AT ELEVATION 65.3 ft
D
D
Sat.
END DATE:10/9/18
OF1
BORING LOCATION:Corner toward road by boat awning.
BLOW COUNT
0.5ft
LOCATION:Williamston
START DATE:10/9/18
PROJECT NAME:
0.5ft
WELL ID:
STATE:
MW06
Shawn McGuire
D.T. Chalmers, Jr.
Eddie SwaineEASTING:
DRILL MACHINE:CME 45B METHOD:HSA
COUNTY:Martin
2564039 762856
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
DEPTH
NORTHING:
1
PROJECT NO.:211010
SHEET
5.3
3.5
LOGGED BY:
DRILLER:
CREW:
DOT Martin County GasolineRelease
0.5ft0.5ft
77.31
12.0
12.0
0 HOUR DTW:
24 HOUR DTW:
SYSTEM:NCSP NAD 83 (USft)CATLIN BORING LOG 211010_DOT_MARTIN_CO_GASOLINE_RELEASE.GPJ CATLIN.GDT 11/13/180.0
WELL LOG
Portland Cement Bentonite Pellets #2 Medium Sand
WELL
DETAIL
77.3
ELEVATION
OVA
(ppm)DEPTH
M
OIS
0.0
LAB.
LAND SURFACE
SOIL AND ROCK
DESCRIPTION
LOG
Wilmington, NC211010