WA-26757_31939_CA_RPTS_20180830_MRP

EXECUTIVE SUMMARY

The Miller’s Country Store site is located at 1706 US Highway 17 N, Merry Hill, Bertie County, North
Carolina. According to available information, a release was discovered during UST closure activities
conducted at the site in September 2008. Three 4,000-gallon gasoline USTs were removed from the site
in September 2008 and one orphan 2,000-gallon UST, whose former contents are unknown, was removed
from the site in April 2009. Municipal water is available to the site and surrounding properties.
Additional petroleum releases (UST Incident Number 11963 – Todd’s Service Center and UST Incident
Number 13592 – Bowen’s Grocery) are located adjacent to the Miller’s Country Store site and are
considered to be commingled with the Miller’s Country Store contaminant plume.

The current risk classification is high due to the presence of water supply wells within a 250-foot radius
of the source area.

A ground water monitoring event was conducted for the Miller’s Country Store site in conjunction with
the ground water monitoring event for the Todd’s Service Center and Bowen’s Grocery sites on July 24,
2018. Concentrations of requested method constituents that exceeded the Maximum Allowable
Concentrations specified in T15A NCAC 2L.0202 were reported in MW-1M and MW-3M. None of the
reported contaminant concentrations exceeded the Gross Contamination Levels.

Upon conclusion of the July 2018 sampling event, Oxygen Releasing Compound (ORC-A) treated socks
were installed in MW-1M, MW-3M and TW-1M.

Based on this information, the effectiveness of the ORC-A socks should be evaluated during the next
semi-annual ground water monitoring event. The next semi-annual ground water monitoring event is
tentatively scheduled for January 2019.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1
3.0 GROUND WATER QUALITY .................................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 3
5.0 LIMITATIONS .............................................................................................................................. 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
Table 2A: Summary of Field Parameters Results

APPENDICES
Appendix A: Todd’s/Bowen’s Ground Water Gauging and Sample Information
Appendix B: Laboratory Report - Ground Water Samples
Appendix C: Notice of Intent to Construct or Operate Injection Wells
Appendix D: Injection Event Record

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Miller’s Country Store site is located at 1706 US Highway 17 N in Merry Hill, Bertie County, North
Carolina (Figure 1). The subject site is a former retail petroleum facility. According to available
information, three 4,000-gallon gasoline USTs were removed from the site on September 9, 2008, and
one orphan 2,000-gallon UST, whose former contents are unknown, was removed from the site on April
30, 2009. An additional UST system consisting of three 3,000-gallon gasoline USTs was removed from
the site on September 1, 1988. A release at the site was discovered when petroleum impacted soil was
encountered during the September 2008 UST closure event.

Three Type II monitoring wells (MW-1M, MW-2M and MW-3M) and one Type III monitoring well
(TW-1M) were installed at the site during past assessment activities. A receptor survey was conducted on
October 1, 2009. Eighteen water supply wells were identified within a 1,500-foot radius of the site.
Three out of service water supply wells (WSW-1, WSW-2 and WSW-3) were identified within a 250-foot
radius of the site. Municipal water is available to the site and surrounding properties.

Additional petroleum releases (UST Incident Number 11963 – Todd’s Service Center and UST Incident
Number 13592 – Bowen’s Grocery) are located adjacent to the Miller’s Country Store site and are
considered to be commingled with the Miller’s Country Store contaminant plume. This sampling event
was conducted in conjunction with the sampling event at the adjacent Todd’s and Bowen’s sites. A Site
Map showing the locations of monitoring wells associated with the Miller’s Country Store, Todd’s
Service Center and Bowen’s Grocery site and structures on-site is included as Figure 2.

Certain information in this report was obtained as a result of assessment activities conducted by past
consultants. Although Geological Resources Inc. (GRI) cannot verify the accuracy of this information,
for the purpose of this report, it is assumed to be correct. Any inferences or interpretations made by GRI
based on data that may be incorrect are not the responsibility of GRI. Please refer to earlier submittals for
additional information regarding past assessment activities.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water sampling activities conducted on July
24, 2018, at the site. The activities were conducted in accordance with GRI proposal number 17-721,
which was submitted to NCDEQ on February 9, 2018 and approved as Task Authorization No. 31939-9
on February 12, 2018. The purpose of the scope of work was to obtain current ground water quality data
for the site, as well as install Oxygen Releasing Compound (ORC-A) treated socks at the site.

2
3.0 GROUND WATER QUALITY
Three Type II monitoring wells (MW-1M, MW-2M and MW-3M) and one Type III monitoring well
(TW-1M) were gauged, purged and sampled on July 24, 2018. Please note, monitoring wells associated
with the Todd’s Service Center and Bowen’s Grocery sites (MW-1A, MW-2, MW-4, MW-5, MW-15,
MW-22, MW-25B, MW-29, MW-36, MW-43, and MW-44) were sampled for those incidents
concurrently with the Miller’s Country Store site. Ground water gauging and sampling information for the
Todd’s/Bowen’s sites are included as Appendix A.

The depths to ground water in the Type II monitoring wells during the July 2018 sampling event ranged
from 18.54 to 19.22 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from
80.46 to 80.89 feet. Based on this information, the direction of ground water flow was generally toward
the southeast. The average horizontal hydraulic gradient across the site was less than 0.01 feet per foot.
The vertical gradient calculated for paired wells MW-1M and TW-1M was approximately 0.03 feet per
foot upward. A Water Table Surface Map for the July 2018 sampling event has been included as Figure
3. Well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the July 2018 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, naphthalene, n-propylbenzene, 1,2,4-trimethylbenzene
and/or 1,3,5-trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) specified
in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1M and MW-
3M. None of the reported contaminant concentrations exceeded the Gross Contamination Levels (GCLs).
A Ground Water Quality Map based on data from the July 24, 2018 sampling event has been included as
Figure 5. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix A.

Field parameter data (dissolved oxygen, temperature, pH, conductivity and oxygen reduction potential)
were collected during the July 2018 sampling for use in the evaluation of the ORC-A sock application.
Field parameter results are tabulate in Table 2A.

Upon conclusion of the July 2018 sampling event, ORC-A socks were installed in MW-1M, MW-3M,
and TW-1M. A copy of the Notice of Intent to Construct or Operate Injection Wells is included as
Appendix C. A copy of the Injection Event Record is included as Appendix D.

3
4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells in July 2018 was 18.80 feet
below the tops of well casings. Ground water flow was generally toward the southeast with an
average horizontal hydraulic gradient of less than 0.01 feet per foot. The average vertical
gradient between paired wells MW-1M and TW-1M was approximately 0.03 feet per foot
upward.
 Concentrations of one or more BTEX constituents, naphthalene, n-propylbenzene, 1,2,4-
trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the
ground water samples collected from MW-1M and MW-3M. None of the reported contaminant
concentrations exceeded the GCLs.
 Upon conclusion of the July 2018 sampling event, ORC-A treated socks were installed in MW-
1M, MW-3M and TW-1M.
 Based on this information, the site should remain high risk. The effectiveness of the ORC-A
socks should be evaluated during the next semi-annual sampling event. The next semi-annual
ground water monitoring event is tentatively scheduled for January 2019.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of Ms. Shirley Miller for the specific application to
the reference site in Bertie County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of environmental practices
in the State of North Carolina, available information, and our professional judgment. No other warranty
is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the times the samples were collected. In addition, the data obtained from the samples
would be interpreted as being meaningful with respect to parameters indicated in the laboratory report.
No additional information can logically be inferred from these data.

FIGURES

TABLES
Date: 08/14/18
09/20/10 19.38 ---80.81
10/27/11 19.19 ---81.00
01/07/13 20.76 ---79.43
07/29/13 19.85 ---80.34
06/23/14 18.92 ---81.27
07/06/15 18.28 ---81.91
01/27/16 18.85 ---81.34
09/07/16 19.25 ---80.94
07/24/18 18.78 ---81.41
09/17/09 21.10 ---79.01
09/20/10 19.38 ---80.73
10/27/11 19.34 ---80.77
01/07/13 20.93 ---79.18
07/29/13 19.66 ---80.45
05/19/14 18.88 ---81.23 Pre-MMPE
05/23/14 19.21 ---80.90 Post-MMPE
06/23/14 19.06 ---81.05
06/01/15 17.75 ---82.36 Pre-MMPE
06/05/15 18.09 ---82.02 Post-MMPE
07/06/15 18.58 ---81.53
01/27/16 19.40 ---80.71
09/07/16 19.63 ---80.48
07/24/18 19.22 ---80.89
09/20/10 18.73 ---80.49
10/27/11 18.73 ---80.49
01/07/13 NM NM NM
07/29/13 19.35 ---79.87
05/19/14 18.26 ---80.96 Pre-MMPE
05/23/14 18.45 ---80.77 Post-MMPE
06/23/14 18.43 ---80.79
07/06/15 17.93 ---81.29
01/27/16 18.83 ---80.39
09/07/16 19.03 ---80.19
07/24/18 18.63 ---80.59
09/20/10 18.60 ---80.40
10/27/11 18.59 ---80.41
01/07/13 20.17 ---78.83
07/29/13 20.17 ---78.83
05/19/14 18.15 ---80.85 Pre-MMPE
05/23/14 18.26 ---80.74 Post-MMPE
06/23/14 18.31 ---80.69
06/01/15 17.07 ---81.93 Pre-MMPE
06/05/15 17.47 ---81.53 Post-MMPE
07/06/15 17.84 ---81.16
01/27/16 18.75 ---80.25
09/07/16 18.91 ---80.09
07/24/18 18.54 ---80.46
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations relative to assumed datum of 100.00 feet.
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TW-1M 09/15/10 40 40-45 45 100.19
MW-1M 09/17/09 10 10-25 25 100.11
MW-2M 09/16/10 10 10-25 25 99.22
MW-3M 09/16/10 10 10-25 25 99.00
• NM: Not Measured.
Page 1 of 1
Date : 08/01/18 Facility ID #: 0-022895
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
09/20/10 4.95 4.15 4.89 18.1 <0.500 <2.00 2.10 <0.280 <0.480 5.78 <0.400 <0.400 4.07 2.60 2.52 3.41 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <3.4 570 <3.0 <8.6 <3.3 <2.4 <2.9 <2.8 <2.8 <2.4 <3.2 <2.4 <3.1 <2.7 <2.7 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 47.9 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/24/18 <0.13 6.0 0.66 1.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.50 0.15 J NR NR NR NR
09/17/09 1,310 36,100 4,070 22,700 211 J 1,060 <90.0 4,200 <120 265 J <100 642 642 4,900 1,170 4.26 12,200 10,700 15,500
09/20/10 1,130 11,900 1,410 6,210 <100 1,640 608 <56.0 <96.0 1,150 792 <80.0 896 2,850 964 45.3 NR NR NR
10/27/11 1,460 24,100 3,970 22,300 244 J 1,000 <100 <100 <100 263 J 226 J <100 763 5,320 1,430 NR NR NR NR
01/07/13 528 16,300 3,830 21,920 45.6 1,000 50.6 27.8 <5.0 186 73.1 18.5 J 589 4,520 1,090 NR NR NR NR
07/30/13 982 23,500 3,030 15,600 208 J 523 <50 <50 <50 110 J 220 J <50 344 2,400 582 NR NR NR NR
06/24/14 1,210 10,600 2,990 21,600 273 1,930 240 128 J <25 296 491 90.4 J 1,140 11,100 3,000 NR NR NR NR
07/06/15 975 17,100 3,150 20,300 <82 1,100 <72 <69 <71 140 J <80 <61 427 4,270 1,040 NR NR NR NR
01/27/16 466 15,200 3,460 22,000 <25 2,280 421 166 <25 373 <25 113 1,400 12,600 3,340 NR NR NR NR
09/07/16 716 22,000 5,560 36,000 <63 2,350 370 167 J <63 415 <63 90.4 J 1,530 12,000 3,570 NR NR NR NR
07/24/18 150 6,550 972 6,560 <31 320 <31 <31 <31 47.5 J <31 <31 137 1490 420 NR NR NR NR
09/20/10 5.49 4.12 4.89 17.7 3.04 2.27 J 15.7 <0.280 <0.480 5.70 3.73 <0.400 4.07 5.24 6.11 33.2 496 <100 380
10/27/11 <0.13 0.37 J 0.26 J 1.4 J <0.13 0.24 J 6.9 2.6 <0.10 1.6 <0.11 0.59 0.13 J 0.95 3.2 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/30/13 <0.10 0.16 J 0.85 1.9 <0.10 0.99 5.8 2.7 <0.10 2.2 <0.10 0.81 0.27 J 5.9 9.6 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.34 J 0.91 0.40 J <0.10 <0.10 <0.10 0.25 J <0.10 0.32 J 0.34 J NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 2.5 0.92 <0.14 <0.12 <0.16 0.50 <0.16 <0.14 0.34 J NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 2.8 0.84 <0.13 <0.13 <0.13 0.27 J <0.13 <0.13 0.35 J NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 5.8 1.9 <0.13 <0.13 <0.13 0.26 J <0.13 <0.13 0.45 J NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 4.0 1.4 <0.13 <0.13 <0.13 0.47 J <0.13 <0.13 0.24 J NR NR NR NR
Analytical Method
EPA Method 6200B
MAC (mg/l)
GCL (mg/l)n-ButylbenzeneNaphthaleneContaminant of
Concern
BenzeneTolueneMADEP Method VPH
1,2-DibromoethaneIsopropylbenzeneIPEp-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticssec-ButylbenzeneEthylbenzeneXylenesMTBEMW-2M
MW-1M
TW-1M
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Page 1 of 2
Date : 08/01/18 Facility ID #: 0-022895
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Analytical Method
EPA Method 6200B
MAC (mg/l)
GCL (mg/l)n-ButylbenzeneNaphthaleneContaminant of
Concern
BenzeneTolueneMADEP Method VPH
1,2-DibromoethaneIsopropylbenzeneIPEp-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticssec-ButylbenzeneEthylbenzeneXylenesMTBE TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
09/20/10 1,090 4,890 1,020 3,150 159 J 601 J 439 <56.0 <96.0 1,150 641 <80.0 829 1,030 606 28.8 25,900 5,280 16,900
10/27/11 1,430 12,300 1,610 6,600 158 352 <25 <26 <26 91.4 J 116 J <25 207 1,360 363 NR NR NR NR
01/07/13 1,120 13,500 1,670 7,150 54.8 312 <10 <10 <10 64.6 131 <10 192 1,390 319 NR NR NR NR
07/30/13 472 6,790 1,080 4,000 <25 171 <25 <25 <25 45.6 J 54.3 J <25 131 811 195 NR NR NR NR
06/24/14 161 2,150 288 1,290 12.6 J 37.2 <5.0 <5.0 <5.0 13.3 J 18.9 J <5.0 29.4 276 78.1 NR NR NR NR
07/06/15 220 4,690 564 2,660 <33 98.1 J <29 <28 <28 25.9 J <32 <24 65.3 J 503 134 NR NR NR NR
01/27/16 659 16,600 1,690 7,720 <25 425 <25 <25 <25 72.4 J 60.0 J <25 203 1,430 340 NR NR NR NR
09/07/16 524 17,500 1,970 9,400 <63 334 <63 <63 <63 82.1 J 81.3 J <63 220 J 1,330 363 NR NR NR NR
07/24/18 246 9,980 1,190 5,130 <25 177 <25 <25 <25 46.6 J <25 <25 125 894 237 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
MW-3M
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
Page 2 of 2
Date: 08/14/18 Facility ID #: 0-022895
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
MW-1M 07/24/18 1.98 5.34 19.92 111 99.8
MW-3M 07/24/18 0.73 5.72 19.32 138 15.8
TW-1M 07/24/18 3.92 7.69 21.34 87 111.1
Notes:
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
1 of 1

APPENDICES

APPENDIX A
Todd’s/Bowen’s Ground Water Gauging and Sample Information
Date: 08/14/18
11/01/07
09/16/09
09/20/10
10/27/11
01/07/13
11/01/07 99.34 21.00 ---78.34
07/20/09 22.00 0.01 78.01 Pre-MMPE
07/24/09 21.25 ---78.75 Post-MMPE
09/16/09 21.57 ---78.43
09/20/10 19.92 ---80.08
10/27/11 19.90 ---80.10
12/03/12 21.45 ---78.55 Pre-MMPE
12/07/12 20.50 ---79.50 Post-MMPE
01/07/13 21.47 ---78.53
06/24/13 21.09 ---78.91 Pre-MMPE
06/28/13 21.19 ---78.81 Post-MMPE
07/29/13 NM NM NM Not Found
05/19/14 19.54 ---80.46 Pre-MMPE
05/23/14 19.45 ---80.55 Post-MMPE
06/23/14 19.68 ---80.32
07/06/15 NM NM NM Not Found
01/27/16 20.13 ---79.87
08/01/16 19.58 ---80.42 Pre-AFVR
08/01/16 19.91 ---80.09 Post-AFVR
09/07/16 20.29 ---79.71
07/24/18 19.91 ---80.09
11/01/07 99.51 20.92 ---78.59
07/20/09 21.07 ---78.79 Pre-MMPE
07/24/09 21.34 ---78.52 Post-MMPE
09/16/09 21.48 ---78.38
09/20/10 19.83 ---80.03
10/27/11 19.86 ---80.00
12/03/12 21.37 ---78.49 Pre-MMPE
12/07/12 21.42 ---78.44 Post-MMPE
01/07/13 21.40 ---78.46
06/24/13 20.91 ---78.95 Pre-MMPE
06/28/13 21.06 ---78.80 Post-MMPE
07/29/13 20.43 ---79.43
05/19/14 19.49 ---80.37 Pre-MMPE
05/23/14 19.44 ---80.42 Post-MMPE
06/23/14 19.62 ---80.24
06/01/15 18.39 ---81.47 Pre-MMPE
06/05/15 18.51 ---81.35 Post-MMPE
07/06/15 19.13 ---80.73
01/27/16 20.07 ---79.79
09/07/16 20.13 ---79.73
07/24/18 19.80 ---80.06
11/01/07 99.59 20.86 ---78.73
09/16/09 21.40 ---78.56
09/20/10 19.74 ---80.22
10/27/11 19.70 ---80.26
01/07/13 21.27 ---78.69
07/29/13 20.31 ---79.65
05/19/14 19.40 ---80.56 Pre-MMPE
05/23/14 19.29 ---80.67 Post-MMPE
06/03/14 19.47 ---80.49
06/01/15 18.22 ---81.74 Pre-MMPE
06/05/15 18.34 ---81.62 Post-MMPE
07/06/15 18.98 ---80.98
01/27/16 19.89 ---80.07
11/01/07 99.57 20.60 ---78.99
09/16/09 NM NM NM
09/20/10 19.47 ---80.10
10/27/11 19.40 ---80.17
12/03/12 21.00 ---78.57 Pre-MMPE
12/07/12 21.06 ---78.51 Post-MMPE
01/07/13 21.03 ---78.54
06/24/13 20.55 ---79.02 Pre-MMPE
06/28/13 20.67 ---78.90 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 19.19 ---80.38
07/06/15 18.73 ---80.84
01/27/16 19.64 ---79.93
08/01/16 19.11 ---80.46 Pre-AFVR
08/01/16 19.30 ---80.27 Post-AFVR
09/07/16 19.74 ---79.83
07/24/18 19.42 ---80.15
99.572515-251504/27/94MW-4
Bottom
of Well
(ft. BGS)
MW-1 04/27/94 15 15-25
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed Casing Collapsed Casing
Collapsed25
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
99.862515-2515
100.0020-3020 30
25 99.96
11/16/01MW-1A
MW-3 04/27/94 15 15-25
04/27/94MW-2
Page 1 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 99.19 20.29 ---78.90
09/16/09 20.85 ---78.72
09/20/10 19.17 ---80.40
10/27/11 19.10 ---80.47
01/07/13 20.70 ---78.87
07/29/13 19.76 ---79.81
05/19/14 18.69 ---80.88 Pre-MMPE
05/23/14 18.58 ---80.99 Post-MMPE
06/23/14 18.83 ---80.74
07/06/15 18.38 ---81.19
01/27/16 19.25 ---80.32
07/24/18 19.07 ---80.50
11/01/07 99.27 21.20 ---78.07
09/16/09 21.06 ---78.60
09/20/10 19.74 ---79.92
10/27/11 19.48 ---80.18
01/07/13 21.04 ---78.62
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 99.00 20.41 ---78.59
09/16/09 20.96 ---78.44
09/20/10 19.31 ---80.09
10/27/11 19.32 ---80.08
01/07/13 20.84 ---78.56
07/29/13 20.40 ---79.00
06/23/14 19.07 ---80.33
07/06/15 18.59 ---80.81
11/01/07 99.28 20.63 ---78.65
09/16/09 21.20 ---78.47
09/20/10 19.55 ---80.12
10/27/11 19.48 ---80.19
01/07/13 21.07 ---78.60
07/29/13 NM NM NM Not Found
06/23/14 19.25 ---80.42
07/06/15 18.78 ---80.89
11/01/07 99.11 20.45 ---78.66
09/16/09 21.22 ---78.31
09/20/10 19.58 ---79.95
10/27/11 19.55 ---79.98
01/07/13 21.10 ---78.43
07/29/13 20.12 ---79.41
06/23/14 19.30 ---80.23
07/06/15 18.82 ---80.71
11/01/07 98.11 19.73 ---78.38
09/16/09 20.29 ---78.07
09/20/10 18.65 ---79.71
10/27/11 18.68 ---79.68
01/07/13 20.20 ---78.16
07/29/13 19.23 ---79.13
06/23/14 18.36 ---80.00
07/06/15 18.00 ---80.36
01/27/16 18.90 ---79.46
09/07/16 18.47 ---79.89
11/01/07 98.28 19.92 ---78.36
07/20/09 20.03 ---78.63 Pre-MMPE
07/24/09 20.21 ---78.45 Post-MMPE
09/16/09 20.48 ---78.18
09/20/10 18.75 ---79.91
10/27/11 18.87 ---79.79
12/03/12 20.39 ---78.27 Pre-MMPE
12/07/12 20.45 ---78.21 Post-MMPE
01/07/13 20.40 ---78.26
06/24/13 19.83 ---78.83 Pre-MMPE
06/28/13 19.95 ---78.71 Post-MMPE
07/29/13 19.46 ---79.20
05/19/14 18.51 ---80.15 Pre-MMPE
05/23/14 18.43 ---80.23 Post-MMPE
06/23/14 NM NM NM Not Found
09/07/16 NM NM NM Destroyed
11/01/07 98.23 19.85 ---78.38
09/16/09 20.40 ---78.20
09/20/10 18.77 ---79.83
10/27/11 18.81 ---79.79
01/07/13 20.30 ---78.30
07/29/13 19.40 ---79.20
06/23/14 NM NM NM Not Found
11/01/07 98.90 20.17 ---78.73
09/16/09 20.71 ---78.61
09/20/10 19.07 ---80.25
10/27/11 19.01 ---80.31
12/03/12 20.59 ---78.73 Pre-MMPE
12/07/12 20.66 ---78.66 Post-MMPE
01/07/13 20.60 ---78.72
06/24/13 20.11 ---79.21 Pre-MMPE
06/28/13 20.23 ---79.09 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
07/06/15 18.30 ---81.02
04/27/94MW-5
39
MW-13 11/30/95
MWD-6 11/22/95 39-44 44 99.66
MW-7 11/24/95 18 18-28 28 99.40
15 15-25
MW-10A 10/31/07 15 15-25
MW-12 12/01/95 18 18-28
25 99.53
98.60
MW-14 11/28/95 15 15-25 25 99.32
15 15-25 25
28 98.66
99.572515-2515
MW-11 12/01/95 18 18-28
25 99.67
28 98.36
MW-9A 10/31/07
Page 2 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
06/23/14 18.94 ---NM
01/27/16 19.34 ---NM
07/24/18 19.46 ---NM
11/01/07 99.34 20.42 ---78.92
09/16/09 20.97 ---78.76
09/20/10 19.23 ---80.50
10/27/11 19.20 ---80.53
01/07/13 20.51 ---79.22
07/29/13 NM NM NM Not Found
05/19/14 18.80 ---80.93 Pre-MMPE
05/23/14 18.78 ---80.95 Post-MMPE
06/23/14 NM NM NM Not Found
11/01/07 98.66 20.26 ---78.40
09/16/09 20.89 ---78.06
09/20/10 19.22 ---79.73
10/27/11 19.22 ---79.73
01/07/13 20.78 ---78.17
07/29/13 19.84 ---79.11
06/23/14 19.00 ---79.95
07/06/15 18.56 ---80.39
11/01/07 98.08 19.57 ---78.51
09/16/09 20.13 ---78.41
09/20/10 18.50 ---80.04
10/27/11 18.51 ---80.03
01/07/13 20.00 ---78.54
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 98.23 20.12 ---78.11
09/16/09 20.73 ---77.90
09/20/10 19.10 ---79.53
10/27/11 19.14 ---79.49
01/07/13 20.65 ---77.98
07/29/13 19.76 ---78.87
06/23/14 18.98 ---79.25
07/06/15 18.50 ---80.13
11/01/07 100.03 20.57 ---79.46
09/16/09 21.18 ---79.21
09/20/10 19.41 ---80.98
10/27/11 19.25 ---81.14
01/07/13 20.95 ---79.44
07/29/13 20.84 ---79.55
06/23/14 18.99 ---81.40
11/01/07 99.07 20.10 ---78.97
09/16/09 20.62 ---78.90
09/20/10 18.94 ---80.58
10/27/11 18.91 ---80.61
01/07/13 20.49 ---79.03
07/29/13 19.44 ---80.08
05/19/14 18.41 ---81.11 Pre-MMPE
05/23/14 18.62 ---80.90 Post-MMPE
06/23/14 18.61 ---80.91
06/01/15 17.35 ---82.17 Pre-MMPE
06/05/15 17.65 ---81.87 Post-MMPE
07/06/15 18.14 ---81.38
01/27/16 19.02 ---80.50
07/24/18 17.78 ---81.74
11/01/07 98.90 20.14 ---78.76
09/16/09 20.69 ---78.80
09/20/10 18.95 ---80.54
10/27/11 18.92 ---80.57
01/07/13 20.54 ---78.95
07/29/13 19.46 ---80.03
06/23/14 18.66 ---80.83
07/06/15 18.19 ---81.30
01/27/16 19.05 ---80.44
11/01/07 99.41 20.10 ---79.31
09/16/09 20.69 ---79.12
09/20/10 NM NM NM
11/01/07 98.43 20.42 ---78.01
09/16/09 21.01 ---77.88
09/20/10 19.38 ---79.51
10/27/11 19.50 ---79.39
01/07/13 20.92 ---77.97
07/29/13 20.07 ---78.82
06/23/14 19.31 ---79.58
07/06/15 18.80 ---80.09
07/24/18 19.54 ---79.35
98.892515-251511/01/07MW-25B
99.522818-281809/24/96MW-22
18 18-28
11/01/07
NM2818-281812/08/95MW-15
99.493020-3020
MW-15A 11/01/07 15 15-25 25 99.73
MW-17 04/19/96 18 18-28 28 98.95
MW-19 04/22/96 18 18-28 28 98.54
100.39
MW-20 04/22/96 18 18-28 28 98.63
MW-23A
MW-21 09/24/96 18 18-28
28
28
99.81MW-24 09/25/96
Page 3 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 97.29 19.57 ---77.72
09/16/09 20.13 ---77.57
09/20/10 18.58 ---79.12
10/27/11 18.65 ---79.05
01/07/13 20.07 ---77.63
07/29/13 19.30 ---78.40
18.24 ---79.46 Pre-AFVR
18.30 ---79.40 Post-AFVR
06/23/14 18.52 ---79.18
06/01/15 17.40 ---80.30 Pre-AFVR
06/01/15 17.44 ---80.26 Post-AFVR
07/06/15 18.05 ---79.65
01/27/16 18.90 ---78.80
09/07/16 18.98 ---78.72
11/01/07 98.36 NM NM NM Well Dry
09/16/09 NM NM NM Well Dry
09/20/10 NM NM NM Well Dry
10/27/11 NM NM NM Well Dry
01/07/13 17.25 ---81.53
07/29/13 NM NM NM Well Dry
06/23/14 NM NM NM Well Dry
07/06/15 NM NM NM Well Dry
11/01/07 95.54 18.14 ---77.40
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
10/04/12 20.92 ---74.62 Pre-AFVR
10/04/12 20.93 ---74.61 Post-AFVR
01/07/13 NM NM NM
06/23/14 NM NM NM
11/01/07 97.70 20.25 ---77.45
09/16/09 20.85 ---77.30
09/20/10 19.31 ---78.84
10/27/11 19.47 ---78.68
20.81 ---77.34 Pre-AFVR
20.82 ---77.33 Post-AFVR
01/07/13 20.77 ---77.38
20.52 ---77.63 Pre-AFVR
20.52 ---77.63 Post-AFVR
07/29/13 20.05 ---78.10
18.88 ---79.27 Pre-AFVR
19.05 ---79.10 Post-AFVR
06/23/14 19.32 ---78.83
06/01/15 18.23 ---79.92 Pre-AFVR
06/01/15 18.23 ---79.92 Post-AFVR
07/06/15 19.32 ---78.83
01/27/16 19.67 ---78.48
09/07/16 19.77 ---78.38
07/24/18 19.50 ---78.65
11/01/07 96.32 19.34 ---76.98
09/16/09 19.88 ---76.85
09/20/10 NM NM NM
11/01/07 97.86 20.37 ---77.49
09/16/09 20.96 ---77.28
09/20/10 19.42 ---78.82
10/27/11 19.51 ---78.73
01/07/13 20.83 ---77.41
07/29/13 19.14 ---79.10
06/23/14 19.39 ---78.85
07/06/15 18.97 ---79.27
11/01/07 97.64 19.30 ---78.34
09/16/09 19.87 ---78.47
09/20/10 NM NM NM
11/01/07 94.72 18.32 ---76.40
09/16/09 18.81 ---76.38
09/20/10 17.51 ---77.68
10/27/11 17.68 ---77.51
01/07/13 18.78 ---76.41
07/29/13 18.31 ---76.88
06/23/14 17.68 ---77.51
07/06/15 17.30 ---77.89
01/27/16 17.95 ---77.24
09/07/16 18.07 ---77.12
11/01/07 NA 6.53 ------
09/16/09 7.03 ---75.21
09/20/10 6.40 ---75.84
10/27/11 6.47 ---75.77
01/07/13 7.23 ---75.01
07/29/13 6.95 ---75.29
06/23/14 6.69 ---75.55
07/06/15 6.47 ---75.77
07/24/18 6.39 ---75.85
09/16/09 20.36 ---79.16
09/20/10 NM NM NM
3525-352510/15/98MW-29
12/04/12
95.54
18-2818
8 8-18 18 98.78
06/26/13
98.15
MW-28 10/15/98 22 22-32 32
97.7028
MW-31 02/28/01 20 20-30
29 96.73
30 98.24
MW-30A 03/19/01
MW-33 11/07/01 20 30
MW-34
MW-37 09/01/09 10 10-25 25 99.52
10-251003/10/03MW-36
05/22/1409/25/96MW-26
82.2425
19-29
20-30
05/22/14
MW-27 10/03/96
95.193020-302011/07/01
98.34
19
Page 4 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
09/16/09 17.58 ---75.75
09/20/10 16.50 ---76.83
10/27/11 16.64 ---76.69
01/07/13 17.67 ---75.66
07/29/13 17.17 ---76.16
06/23/14 16.68 ---76.65
07/06/15 16.35 ---76.98
09/16/09 19.54 ---78.77
09/20/10 NM NM NM
09/16/09 24.24 ---77.82
09/20/10 NM NM NM
09/20/10 19.42 ---81.20
10/27/11 19.19 ---81.43
01/07/13 20.99 ---79.63
06/23/14 18.94 ---81.68
09/20/10 19.74 ---81.01
10/27/11 19.60 ---81.15
01/07/13 21.27 ---79.48
07/29/13 20.13 ---80.62
06/23/14 19.30 ---81.45
07/06/15 18.91 ---81.84
09/20/10 19.15 ---79.47
10/27/11 19.27 ---79.35
01/07/13 20.55 ---78.07
07/29/13 19.85 ---78.77
06/23/14 19.09 ---79.53
07/06/15 18.58 ---80.04
07/24/18 19.23 ---79.39
09/20/10 18.81 ---78.38
10/27/11 18.92 ---78.27
01/07/13 20.19 ---77.00
07/29/13 19.55 ---77.64
06/23/14 18.86 ---78.33
07/06/15 18.42 ---78.77
07/24/18 19.11 ---78.08
09/20/10 18.10 ---78.15
10/27/11 18.31 ---77.94
01/07/13 19.52 ---76.73
07/29/13 14.48 ---81.77
06/23/14 18.22 ---78.03
07/06/15 17.76 ---78.49
09/20/10 17.59 ---77.88
10/27/11 17.77 ---77.70
01/07/13 18.94 ---76.53
07/29/13 18.41 ---77.06
06/23/14 17.71 ---77.76
07/06/15 17.29 ---78.18
09/20/10 17.62 ---77.47
10/27/11 17.79 ---77.30
01/07/13 18.91 ---76.18
07/29/13 18.38 ---76.71
06/23/14 17.79 ---77.30
07/06/15 17.44 ---77.65
09/20/10 14.57 ---76.59
10/27/11 14.70 ---76.46
01/07/13 15.61 ---75.55
07/29/13 15.24 ---75.92
06/23/14 14.80 ---76.36
07/06/15 14.48 ---76.68
11/01/07 NA 20.89 ------
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
01/07/13 NM NM NM
07/29/13 NM NM NM
06/23/14 NM NM NM
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations and well construction information for monitoring wells installed prior to 2007 reproduced from previous assessment
reports prepared by CES Engineering, P. C.
• Monitoring wells MW-9A, MW-10A, MW-15A and MW-25B were resurveyed on August 12, 2008 by GRI personnel.
• Monitoring wells MW-41 through MW-48, TW-1M, MW-1M, MW-2M and MW-3M were surveyed on September 17, 2010 by GRI personnel.
MW-43 25
MW-38 09/16/09 10 10-25 25 93.33
MW-39 09/16/09 10 10-25 25 98.31
MW-40 09/16/09 10 10-25 25 102.06
MW-41 09/16/10 10 10-25 25 100.62
MW-42 09/16/10 10 10-25 25 100.75
98.6210-25
1009/15/10
25 95.47
2510-25
1009/15/10
MW-45 09/15/10 10 10-25 25 96.25
95.09
91.16
MW-47
MW-48
09/15/10
09/15/10
10
10
• NM: Not Measured.
10-25
10-25
25
25
MW-46 09/15/10 10 10-25
97.19MW-44
100.033010-301007/22/03RW-1
Page 5 of 5
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
10/31/07 10,100 23,700 1,570 9,290 648 286 33.1 16.0 <5.00 71.6 13.0 14.1 166 988 309 39.8 NR NR NR
09/17/09 2,110 8,190 552 2,660 814 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 <44.0 313 73.9 J 10.1 2,510 2,080 2,990
09/20/10 9,050 29,400 2,100 11,000 8,740 <250 <250 <250 <120 111 J <100 <100 221 J 1,530 398 J 31.8 NR NR NR
10/27/11 14,400 39,900 2,940 14,200 3,320 391 J <100 <100 <100 133 J <110 <100 262 J 1,840 439 J NR NR NR NR
01/07/13 4,940 25,700 1,980 10,400 2,710 327 <10 <10 <10 74.1 <10 <10 195 1,390 354 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 9,320 36,700 3,200 16,300 6,320 556 20.4 J 16.8 J <10 143 19.4 J <10 362 2,800 698 NR NR NR NR
07/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/27/16 7,300 37,800 2,610 12,700 5,880 502 <63 <63 <63 103 J <63 <63 274 1,850 449 NS NS NS NS
09/07/16 10,500 56,000 3,740 19,800 5,610 1,420 <130 <130 <130 142 J <130 <130 358 J 2,270 595 NR NR NR NR
07/24/18 3,460 28,200 2,360 11,600 1,520 483 <63 <63 <63 103 J <63 <63 239 J 1730 455 NR NR NR NR
10/31/07 10,600 39,000 2,420 11,300 1,870 439 37.8 <10.0 <10.0 86.0 11.2 <10.0 175 1,230 356 23.0 NR NR NR
09/17/09 5,830 28,800 2,110 10,600 660 376 <45.0 1,080 <60.0 91.6 J <50.0 <50.0 161 J 1,270 289 29.9 5,000 3,150 4,860
09/20/10 4,680 12,000 1,210 5,650 7,310 137 <50.0 <50.0 <24.0 41.3 J <20.0 <20.0 66.8 J 525 140 116 NR NR NR
10/27/11 3,940 15,000 1,170 6,410 897 149 <20 <20 <21 33.0 J <21 <20 74.8 J 634 144 NR NR NR NR
01/07/13 0.67 3.7 0.41 J 1.70 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.16 J <0.10 NR NR NR NR
07/30/13 3,130 22,300 1,620 8,970 952 265 <10 <10 <10 43.4 J <10 <10 93.2 825 179 NR NR NR NR
06/24/14 1,450 8,130 752 4,340 769 157 1.5 J 1.5 J <1.0 24.0 3.6 J <1.0 51.7 434 96.0 NR NR NR NR
07/06/15 2,290 11,100 1,420 7,930 4,540 248 <36 <35 <35 42.6 J <40 <31 98.2 J 900 208 NR NR NR NR
01/27/16 <0.13 0.16 J <0.13 <0.31 2.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 1.9 21.5 3.8 12.7 1.7 0.96 <0.13 <0.13 <0.13 0.16 J <0.13 <0.13 0.56 1.4 0.35 J NR NR NR NR
07/24/18 135 2,150 230 1,050 27.8 37.2 <6.3 <6.3 <6.3 9.9 J <6.3 <6.3 23.1 J 173 45.1 NR NR NR NR
02/28/07 15.0 <0.500 3.36 1.43 <0.500 15.5 0.880 0.870 <0.500 2.24 <0.500 0.710 1.57 2.38 <0.500 15.9 NR NR NR
10/31/07 59.1 0.930 14.6 7.97 <0.500 16.4 4.10 4.09 <0.500 11.3 <0.500 4.09 9.58 3.22 4.16 29.9 NR NR NR
09/17/09 20.1 <0.190 2.31 <0.220 <0.250 1.58 <0.180 0.970 J <0.240 2.65 <0.200 <0.200 1.39 0.883 J <0.180 7.05 106 <100 <100
09/20/10 13.7 2.15 0.606 J 1.85 J <0.500 3.61 <1.00 <1.00 <0.480 2.69 <0.400 <0.400 0.776 J 0.488 J <0.360 14.3 NR NR NR
10/27/11 8.4 0.22 J 0.89 1.1 J <0.13 1.8 <0.10 0.42 J <0.10 1.6 <0.11 <0.10 0.93 0.19 J <0.10 NR NR NR NR
01/07/13 0.74 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 1.0 <0.10 <0.10 0.55 J <0.10 <0.10 <0.10 0.14 J <0.10 0.22 J 0.11 J <0.10 0.28 J 0.36 J 0.15 J NR NR NR NR
07/06/15 2.9 <0.17 <0.15 0.62 J <0.16 0.98 0.35 J 0.59 <0.14 0.79 <0.16 <0.12 0.63 1.7 0.16 J NR NR NR NR
01/27/16 0.45 J <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
Facility ID #s: 0-022807 & 0-022804
MW-3 1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-ButylbenzeneMW-1A
MW-2
Page 1 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/20/10 1,500 45,000 9,170 53,400 309 J 2,870 1,830 <500 <240 852 J <200 <200 2,410 21,900 5,330 30.6 NR NR NR
10/27/11 1,700 33,200 6,290 33,500 2,880 1,180 201 J 120 J <100 457 J <110 <100 1,290 8,760 2,370 NR NR NR NR
01/07/13 509 19,500 4,620 24,300 737 960 58.1 43.7 J <10 249 <10 22.7 J 761 4,610 1,340 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 894 19,200 4,580 27,300 1,170 858 471 269 <2.5 725 7.6 J 144 920 6,200 1,730 NR NR NR NR
07/06/15 381 14,200 4,810 28,600 620 1,440 98.9 J 59.1 J <35 264 <40 34.7 J 763 7,110 1,890 NR NR NR NR
01/27/16 349 24,200 12,200 68,400 1,810 3,360 879 465 <63 1,170 <63 240 J 4,190 22,100 7,640 NR NR NR NR
09/07/16 146 J 13,000 5,710 35,100 184 J 1,500 260 159 J <63 388 <63 66.9 J 1,320 9,470 2,940 NR NR NR NR
07/24/18 115 4,380 2,900 16,100 <25 628 58.8 J 43.1 J <25 195 <25 <25 550 4,250 1,200 NR NR NR NR
10/31/07 1,120 5,620 1,490 4,130 <5.00 283 36.3 17.0 <5.00 82.5 <5.00 20.2 141 682 287 16.0 NR NR NR
09/17/09 274 2,280 666 1,810 <10.0 168 <7.20 <5.60 <9.60 58.6 <8.00 <8.00 64.8 392 124 12.9 2,770 2,250 1,480
09/20/10 568 1,780 630 2,340 <5.00 95.9 40.7 <10.0 11.5 J 38.0 <4.00 <4.00 52.1 539 160 19.6 NR NR NR
10/27/11 130 456 267 617 <0.13 47.9 3.2 2.4 1.8 26.0 <0.11 3.3 34.0 108 32.8 NR NR NR NR
01/07/13 590 4,770 1,400 5,120 <1.0 391 9.0 8.8 4.9 J 80.0 <1.0 11.9 132 804 248 NR NR NR NR
07/30/13 69.0 705 485 1,670 <2.0 216 6.1 J 5.8 J <2.0 40.2 <2.0 8.0 J 70.3 314 121 NR NR NR NR
06/24/14 14.8 38.1 12.3 79.1 <0.10 8.7 0.29 J 0.26 J 0.30 J 1.8 <0.10 0.39 J 2.2 9.2 4.1 NR NR NR NR
07/06/15 5.3 40.7 9.2 38.4 <0.16 2.0 <0.14 <0.14 <0.14 0.55 <0.16 <0.12 0.86 3.4 1.3 NR NR NR NR
01/27/16 185 1,690 631 2,060 <3.1 187 5.4 J 4.8 J <3.1 40.6 <3.1 6.0 J 63.2 336 111 NR NR NR NR
07/24/18 168 1,860 553 1,930 <6.3 92.2 <6.3 <6.3 <6.3 37.0 <6.3 <6.3 55.1 239 85.3 NR NR NR NR
10/31/07 2.72 3.43 <0.500 1.17 6.10 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 NR NR NR
09/17/09 0.627 J 0.602 J <0.150 <0.220 0.868 J <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.200 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.700 2.84 J 1.23 J 2.21 J <1.25 <2.50 <2.50 <2.50 <1.20 <0.750 <1.00 <1.00 <1.10 0.756 J <0.900 6.89 NR NR NR
10/27/11 <0.13 0.52 <0.15 0.56 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.38 J 0.46 J <0.10 0.21 J 0.59 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 36.9 <0.500 14.6 <1.00 <0.500 6.30 1.63 2.71 <0.500 7.20 1.53 3.14 6.78 <0.500 <0.500 <5.00 NR NR NR
09/17/09 10.3 0.366 J 179 3.61 <0.250 58.7 <0.180 7.46 <0.240 57.3 1.75 0.588 J 93.3 2.06 0.795 J <1.50 758 489 481
09/20/10 1.91 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 0.485 J <0.200 <0.200 <0.220 <0.150 <0.180 25.0 NR NR NR
10/27/11 3.7 0.30 J <0.15 <0.30 <0.13 0.53 <0.10 0.41 J <0.10 0.77 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 19.1 <0.10 13.1 <0.22 0.33 J 3.0 1.3 2.9 <0.10 12.5 0.90 1.5 19.2 <0.10 <0.10 NR NR NR NR
07/30/13 7.3 <0.10 7.0 <0.22 0.43 J 1.5 0.46 J 0.78 <0.10 4.7 0.78 0.34 J 7.2 <0.10 <0.10 NR NR NR NR
06/24/14 0.16 J <0.10 0.15 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.13 J <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-7
MWD-6
MW-5
MW-4
Page 2 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 0.930 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.79 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 11.3 <100 <100 <100
09/20/10 0.284 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.1 NR NR NR
10/27/11 0.55 0.23 J <0.15 0.46 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 2.9 <0.10 <0.10 <0.22 0.11 J <0.15 <0.10 0.13 J <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 7.29 <100 <100 <100
09/20/10 0.475 J 2.95 0.384 J 1.90 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 0.503 J <0.180 27.9 NR NR NR
10/27/11 <0.13 0.14 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.11 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
10/31/07 617 191 366 652 52.0 132 9.58 4.13 <0.500 28.5 0.640 5.68 43.6 199 81.9 7.17 NR NR NR
09/17/09 1,560 3,120 687 1,920 43.6 J 208 <18.0 <14.0 <24.0 53.3 J <20.0 <20.0 52.5 J 316 88.1 J 12.5 3,150 1,430 1,870
09/20/10 29.2 1.68 0.400 J 13.3 11.1 3.56 <0.500 <0.500 <0.240 1.53 <0.200 <0.200 0.304 J 5.78 <0.180 25.6 NR NR NR
10/27/11 3.4 <0.13 <0.15 <0.30 1.2 0.37 J <0.10 <0.10 <0.10 0.11 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 324 E 97.6 114 188.9 121 44.3 1.2 1.5 0.38 J 12.3 0.83 1.6 18.7 55.5 11.3 NR NR NR NR
07/30/13 276 194 66.4 249 98.8 36.9 0.89 0.97 0.30 J 8.6 0.61 1.1 12.7 39.6 7.7 NR NR NR NR
06/24/14 152 20.5 11.5 89.9 29.3 21.9 0.40 J 0.37 J 0.29 J 3.2 <0.10 0.65 3.6 14.9 1.9 NR NR NR NR
07/06/15 33.8 0.38 J 6.5 12.8 7.6 16.0 0.28 J 0.25 J <0.14 1.7 <0.16 0.55 2.2 4.4 <0.14 NR NR NR NR
01/27/16 225 310 144 467 6.7 68.1 1.4 J <1.3 <1.3 11.0 <1.3 2.1 J 15.8 98.9 23.2 NR NR NR NR
09/07/16 27.7 29.5 16.8 32.3 0.25 J 7.1 <0.13 <0.13 <0.13 1.1 <0.13 <0.13 1.5 3.7 0.73 NR NR NR NR
11/01/07 8,470 20,300 2,100 8,390 9,250 449 27.3 8.19 <0.500 76.3 46.0 6.75 154 1,280 420 18.8 NR NR NR
09/17/09 2,560 8,380 778 2,500 330 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 88.1 J 552 141 J 3.22 2,630 1,700 2,360
09/20/10 1,500 517 260 764 845 76.3 7.59 J <5.00 <2.40 17.7 <2.00 <2.00 32.3 174 65.7 74.5 NR NR NR
10/27/11 3,120 9,080 895 4,130 2,990 128 <20 <20 <21 35.1 J <21 <20 83.9 J 613 160 NR NR NR NR
01/07/13 4,010 15,500 1,400 6,790 1,790 235 <10 <10 <10 52.3 <10 <10 146 1,080 241 NR NR NR NR
07/30/13 1,640 6,850 785 3,230 1,140 152 <25 <25 <25 32.5 J <25 <25 89.0 J 503 126 J NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/07/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-10A
MW-9A
MW-11
MW-12
Page 3 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 12.9 <0.500 2.65 <1.00 <0.500 <5.00 <0.500 2.06 <0.500 2.57 <0.500 <0.500 2.69 <0.500 <0.500 45.0 NR NR NR
09/17/09 8.77 <0.190 43.7 <0.220 <0.250 3.50 <0.180 3.19 <0.240 20.3 <0.200 0.454 J 26.4 <0.150 0.624 J 12.1 246 179 183
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 42.1 NR NR NR
10/27/11 0.15 J 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 1.2 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 0.20 J <0.10 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.83 0.14 J <0.10 <0.22 <0.10 <0.15 <0.10 0.11 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 199 2.45 88.3 101 14.8 63.7 8.79 4.09 <0.500 26.8 <0.500 6.02 20.5 104 36.3 47.6 NR NR NR
10/31/07 212 11.4 280 185 8.98 144 17.4 6.66 <0.500 46.8 <0.500 10.2 54.8 87.4 90.8 12.4 NR NR NR
09/17/09 153 193 261 200 3.32 J 143 <1.80 <1.40 <2.40 22.5 <2.00 <2.00 20.7 62.4 21.5 13.6 1,100 504 506
09/20/10 64.5 6.39 68.7 41.7 <0.250 66.9 2.58 1.94 <0.240 16.6 <0.200 0.391 J 12.3 24.4 0.665 J 50.2 NR NR NR
10/27/11 183 5.0 148 12.2 12.3 78.6 2.7 3.8 <0.52 32.0 <0.54 3.5 23.3 5.0 0.66 J NR NR NR NR
01/07/13 144 170 228 237.8 9.5 135 3.2 3.4 <0.50 26.5 <0.50 2.8 25.6 50.2 10.5 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/06/15 0.89 0.34 J 2.3 2.1 0.20 J 1.5 <0.14 <0.14 <0.14 0.24 J <0.16 <0.12 0.29 J 0.51 0.16 J NR NR NR NR
06/24/14 38.8 282 213 1,120 <0.10 120 4.9 4.3 <0.10 24.8 <0.10 7.2 31.5 224 74.6 NS NS NS NS
01/27/16 114 535 638 1,840 <3.1 250 9.5 J 8.5 J <3.1 64.4 <3.1 11.7 J 95.3 398 177 NS NS NS NS
07/24/18 41.8 249 229 808 <1.3 81.3 5.2 5.0 <1.3 26.5 <1.3 6.0 41.9 201 73.5 NR NR NR NR
11/01/07 358 1,690 1,320 3,240 <0.500 358 36.4 12.0 <0.500 81.5 <0.500 17.1 116 721 333 56.4 NR NR NR
09/17/09 78.6 1,030 513 1,680 <5.00 170 <3.60 <2.80 <4.80 45.4 <4.00 <4.00 44.3 360 112 9.16 2,640 1,100 1,460
09/20/10 551 756 542 1,570 <50.0 343 J <36.0 <28.0 <48.0 576 <40.0 <40.0 413 482 313 64.5 NR NR NR
10/27/11 151 534 458 1,230 <2.6 150 7.1 J 5.5 J <2.1 44.5 <2.1 8.0 J 64.9 287 130 NR NR NR NR
01/07/13 59.0 477 353 885 <2.0 125 5.3 J 5.5 J <2.0 35.9 <2.0 5.1 J 50.7 172 101 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 55.2 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.79 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.83 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 15.5 NR NR NR
10/27/11 <0.13 0.22 J <0.15 0.36 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-15
MW-14
MW-17
MW-15A
MW-13
Page 4 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 6.58 1.13 10.5 3.33 4.88 25.9 6.63 4.30 <0.500 13.2 0.630 2.50 7.16 2.52 <0.500 45.3 NR NR NR
09/17/09 <0.140 <0.190 37.7 22.6 <0.250 66.2 <0.180 3.38 <0.240 34.8 <0.200 <0.200 41.2 116 47.4 14.6 243 394 505
09/20/10 0.917 J <0.190 <0.150 0.270 J 1.51 1.64 2.65 1.35 <0.240 1.15 <0.200 <0.200 <0.220 <0.150 <0.180 49.2 NR NR NR
10/27/11 <0.13 0.24 J <0.15 0.56 J <0.13 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.23 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 7.5 12.5 0.12 J 40.4 2.4 2.6 <0.10 16.7 <0.10 0.87 10.4 47.0 1.0 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.5 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.32 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.3 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 30.6 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.69 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.4 NR NR NR
09/17/09 11.1 0.398 J 1.69 11.3 <0.250 <0.500 <0.180 <0.140 <0.240 0.773 J <0.200 <0.200 0.749 J 3.69 1.81 5.70 429 105 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 1.20 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 8.09 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
02/28/07 291 387 345 1,020 34.5 35.3 19.1 6.00 <0.500 33.2 29.4 4.95 75.2 523 115 18.1 NR NR NR
10/31/07 95.7 1,020 795 2,820 <2.50 155 46.4 16.6 <2.50 79.4 <2.50 13.4 224 1,190 373 <5.00 NR NR NR
09/17/09 78.9 J 2,270 1,900 8,570 <50.0 324 <36.0 <28.0 <48.0 156 J <40.0 <40.0 305 2,430 558 3.75 4,900 5,980 393,000
09/20/10 158 58.2 188 156 16.9 20.8 24.0 15.9 <2.40 30.9 30.5 <2.00 60.6 288 53.9 37.2 NR NR NR
10/27/11 69.3 301 487 1,730 <2.6 78.9 16.6 12.7 <2.1 61.0 4.2 J 9.4 J 190 955 267 NR NR NR NR
01/07/13 90.4 261 1,180 4,820 29.5 240 27.3 24.5 <2.0 172 12.4 16.0 542 3,480 828 NR NR NR NR
07/30/13 91.0 199 648 2,480 9.7 J 115 27.0 22.5 J <5.0 99.2 12.5 J 15.6 J 382 1,680 486 NR NR NR NR
06/23/14 8.6 5.3 34.6 111 <0.10 6.4 4.2 3.3 <0.10 8.5 0.73 2.6 28.5 67.8 20.7 NR NR NR NR
07/06/15 12.6 17.4 97.2 379 <0.82 20.3 7.1 4.9 <0.71 13.1 <0.80 3.7 46.3 211 60.0 NR NR NR NR
01/27/16 37.2 82.2 445 1,710 <3.1 106 22.2 16.4 <3.1 47.2 <3.1 12.0 J 159 878 218 NR NR NR NR
07/24/18 5.4 26.0 421 1,390 <1.3 90.6 16.6 12.7 <1.3 58.6 <1.3 8.5 165 954 241 NR NR NR NR
MW-19
MW-22
MW-20
MW-21
Page 5 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene02/28/07 7.39 <0.500 4.73 7.21 <0.500 <5.00 <0.500 0.590 <0.500 1.88 <0.500 0.990 2.42 17.4 2.49 16.2 NR NR NR
10/31/07 3.32 <0.500 1.98 2.58 <0.500 <5.00 <0.500 <0.500 <0.500 1.53 <0.500 <0.500 0.810 6.75 1.27 16.4 NR NR NR
09/17/09 3.86 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 0.792 J <0.200 <0.200 0.387 J 3.64 <0.180 18.7 <100 <100 <100
09/20/10 14.2 0.242 J 2.39 9.05 <0.250 6.07 2.53 3.44 <0.240 6.40 <0.200 0.580 J 1.64 20.4 1.69 20.9 NR NR NR
10/27/11 7.0 0.22 J 3.7 3.1 <0.13 2.3 <0.10 0.61 <0.10 2.0 <0.11 0.95 1.8 6.8 <0.10 NR NR NR NR
01/07/13 1.7 <0.10 <0.10 0.28 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.96 <0.10 NR NR NR NR
07/30/13 12.3 0.15 J 4.1 5.5 <0.10 3.5 <0.10 1.4 <0.10 3.6 0.16 J 1.8 4.4 15.8 <0.10 NR NR NR NR
06/24/14 7.4 <0.10 3.1 3.0 <0.10 2.3 <0.10 0.83 <0.10 2.1 <0.10 1.1 2.4 8.6 0.14 J NR NR NR NR
07/06/15 22.0 0.47 J 11.7 19.8 <0.16 12.7 0.14 J 1.4 <0.14 4.7 <0.16 2.6 5.0 36.5 1.0 NR NR NR NR
01/27/16 1.1 <0.13 0.21 J <0.31 <0.13 0.46 J <0.13 <0.13 <0.13 0.18 J <0.13 <0.13 0.19 J 0.19 J <0.13 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.1 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 4.67 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 61.5 95.7 46.1 75.8 5.64 12.2 2.94 2.03 <0.500 3.77 5.95 <0.500 7.17 20.6 7.97 32.3 NR NR NR
09/17/09 11.5 <0.190 <0.150 <0.220 10.7 5.35 <0.180 <0.140 <0.240 0.515 J 12.7 <0.200 <0.220 <0.150 <0.180 8.33 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 26.8 NR NR NR
10/27/11 <0.13 0.15 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.49 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/28/07 4,210 2,780 1,120 2,200 2,350 1,690 12.8 4.70 3.71 53.9 11.0 3.30 96.9 594 143 6.94 NR NR NR
11/01/07 4,130 2,880 1,150 2,220 1,720 190 14.9 6.23 1.65 47.7 9.05 4.76 89.0 509 139 21.6 NR NR NR
09/17/09 3,910 6,350 952 2,950 1,730 172 <18.0 <14.0 <24.0 50.3 J <20.0 <20.0 75.4 J 424 117 4.19 1,950 1,670 83,000
09/20/10 25.1 <0.190 0.827 J <0.220 96.2 0.957 J <0.500 <0.500 <0.240 0.313 J <0.200 <0.200 <0.220 <0.150 <0.180 45.3 NR NR NR
10/27/11 4.1 0.22 J 0.54 <0.30 4.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 257 102 77.0 149.9 147 13.3 <1.0 <1.0 <1.0 4.7 J <1.0 <1.0 10.3 47.7 9.2 NR NR NR NR
07/30/13 180 173 40.7 120 188 7.3 <0.10 0.15 J <0.10 2.1 0.44 J <0.10 3.3 10.1 2.2 NR NR NR NR
06/23/14 14.6 1.6 1.5 4.7 86.5 0.46 J <0.10 <0.10 <0.10 0.15 J 0.13 J <0.10 0.13 J 0.73 <0.10 NR NR NR NR
07/06/15 2.4 <0.17 0.22 J <0.43 12.1 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 9.0 8.3 1.6 5.9 26.4 0.50 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.51 <0.13 NR NR NR NR
09/07/16 0.31 J <0.13 <0.13 <0.31 5.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-26
MW-25B
MW-24
MW-23A
Page 6 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene02/28/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 2.81 <0.500 <0.500 <0.500 <0.500 9.40 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.6 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 692 90.3 93.4 81.7 120 15.4 3.91 2.96 <0.500 28.0 1.04 1.25 15.0 16.7 5.44 6.88 NR NR NR
11/01/07 3,810 2,110 788 1,580 1,370 148 13.7 6.32 <0.500 40.9 9.59 5.45 67.8 364 92.0 40.5 NR NR NR
09/17/09 2,860 5,780 696 2,320 869 127 <18.0 <14.0 <24.0 37.8 J <20.0 <20.0 61.2 J 370 91.5 J <1.50 1,690 1,280 1,800
09/20/10 1,140 939 266 636 402 <100 <18.0 <14.0 <24.0 28.8 J <20.0 <20.0 37.3 J 156 36.4 J 13.4 NR NR NR
10/28/11 2,130 1,340 487 762 1,060 80.2 6.4 J <5.1 <5.2 32.1 5.9 J <5.0 50.0 236 25.9 NR NR NR NR
01/07/13 2,110 6,130 731 3,300 1,110 150 <5.0 <5.0 <5.0 31.2 <5.0 <5.0 74.5 551 138 NR NR NR NR
07/30/13 1,420 3,280 438 1,590 858 78.8 <10 <10 <10 20.2 J <10 <10 43.0 J 289 69.7 NR NR NR NR
06/23/14 508 2,480 268 1,070 319 67.2 2.6 2.2 <0.10 19.9 1.4 1.4 38.7 206 42.7 NR NR NR NR
07/06/15 525 1,780 317 1,290 157 90.1 <7.2 <6.9 <7.1 21.4 J <8.0 <6.1 35.0 270 65.7 NR NR NR NR
01/27/16 550 1,370 337 1,380 138 106 <3.1 <3.1 <3.1 20.7 <3.1 <3.1 33.0 315 70.5 NR NR NR NR
09/07/16 647 1,330 408 1,920 317 93.4 <6.3 <6.3 <6.3 25.0 <6.3 <6.3 39.5 309 79.9 NR NR NR NR
07/24/18 677 291 409 1,800 627 81.7 <3.1 <3.1 <3.1 20.3 <3.1 <3.1 39.3 312 75.5 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 218 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 28.4 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.2 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0500 <0.500 <0.500 90.3 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 13.9 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 27.6 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-29
MW-31
MW-30A
MW-27
MW-28
Page 7 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 91.1 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 97.3 <0.500 <0.500 <1.00 50.9 <5.00 <0.500 <0.500 <0.500 1.13 <0.500 <0.500 <0.500 <0.500 <0.500 58.8 NR NR NR
11/01/07 146 <0.500 <0.500 <1.00 60.8 <5.00 <0.500 <0.500 <0.500 2.00 <0.500 <0.500 <0.500 <0.500 <0.500 165 NR NR NR
09/17/09 102 <0.190 <0.150 <0.220 32.2 <0.500 <0.180 <0.140 <0.240 1.10 <0.200 <0.200 <0.220 <0.150 0.525 J 12.5 <100 <100 <100
09/20/10 72.4 0.908 J 4.77 4.41 78.0 4.60 0.382 J 0.303 J <0.480 2.50 <0.400 <0.400 1.21 J <0.300 <0.360 40.4 NR NR NR
10/28/11 0.13 J 0.15 J <0.15 <0.30 1.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 11.7 J <10 <10 <22 451 <15 <10 <10 <10 <10 <10 <10 <10 <10 <10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 3.9 <0.17 0.17 J <0.43 5.1 0.45 J <0.14 <0.14 <0.14 0.17 J <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 0.32 J 0.25 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 1.5 <0.13 <0.13 <0.13 <0.13 <0.13 0.43 J <0.13 <0.13 <0.13 <0.13 NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.4 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.75 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.410 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 24.6 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 1.0 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 20.3 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 <0.190 <0.150 <0.220 3.07 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 39.4 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.794 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 77.4 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-37
MW-33
MW-34
MW-36
MW-38
Page 8 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 25.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 1.82 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.0 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 0.327 J <0.180 100 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/20/10 6.54 1.30 17.4 77.1 <0.250 1.43 J 3.24 0.680 J <0.240 1.85 <0.200 <0.200 4.04 25.8 9.18 80.2 1,450 431 665
10/27/11 10.7 1.3 1.5 11.0 0.15 J 0.12 J 0.14 J <0.10 <0.10 0.21 J <0.11 <0.10 0.29 J 1.6 2.1 NR NR NR NR
01/07/13 18.1 3.1 10.7 39.9 <0.10 <0.15 0.15 J 0.18 J <0.10 1.1 <0.10 0.12 J 2.0 7.7 5.1 NR NR NR NR
07/29/13 5.6 0.31 J 0.27 J 3.5 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.41 J 1.1 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 78.5 <100 <100 <100
10/27/11 <0.13 0.19 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.11 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/20/10 20.4 0.447 J 4.18 1.01 8.18 <1.00 <0.180 <0.140 <0.240 1.11 <0.200 <0.200 0.961 J <0.150 <0.180 104 <100 <100 <100
10/28/11 11.4 0.22 J <0.15 0.36 J 4.8 <0.10 <0.10 <0.10 <0.10 0.24 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 5.3 <0.10 0.11 J <0.22 4.6 <0.15 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 46.7 0.25 J 2.7 <0.22 11.9 <0.15 0.13 J 0.13 J <0.10 1.1 <0.10 <0.10 0.60 <0.10 <0.10 NR NR NR NR
06/23/14 1.2 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-39
MW-43
MW-40
MW-42
MW-41
MW-44
Page 9 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 229 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 1.17 <0.190 <0.150 0.276 J 1.99 <1.00 <0.180 <0.140 <0.240 0.415 J 2.32 <0.200 <0.220 <0.150 <0.180 106 <100 <100 <100
10/28/11 <0.13 0.14 J <0.15 0.48 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.17 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.17 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.25 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.40 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 26.6 <0.190 <0.150 <0.220 12.0 <1.00 0.201 J 0.177 J <0.240 1.43 <0.200 <0.200 <0.220 <0.150 <0.180 116 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 101 <0.50 <0.50 <1.08 11.0 <0.74 <0.50 <0.50 <0.50 1.8 J <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR
07/30/13 12.9 <0.10 <0.10 <0.22 1.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 0.502 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 49.9 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.96 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.18 J <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 9.6 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.45 NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 0.189 J <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.44 J NR NR NR
10/28/11 <0.13 0.14 J <0.15 <0.30 <0.13 0.11 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-45
MW-46
MW-47
MW-48
WSW-5
WSW-13
Page 10 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• A concentration of o-chlorotoluene (140 µg/l) that exceeded the MAC was reported in the ground water sample collected from MW-4 on July 24, 2018.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
WSW-18
Page 11 of 11
Date: 08/14/18 Facility ID #: 0-022807 & 0-022804
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
MW-1A 07/24/18 1.16 5.51 19.80 125 30.0
MW-2 07/24/18 2.06 5.82 19.94 195 106.0
MW-4 07/24/18 0.46 4.70 19.82 59 97.8
MW-15 07/24/18 0.50 5.51 20.04 98 45.2
MW-22 07/24/18 1.85 5.44 20.41 91 69.6
MW-29 07/24/18 1.08 6.03 22.00 189 35.9
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)
1 of 1

APPENDIX B
Laboratory Report – Ground Water Samples
07/31/18
Technical Report for
GRI (Geological Resources Inc.)
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
31939/2721
SGS Job Number: FA56100
Sampling Date: 07/24/18
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Holden McClenney
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 07/31/18
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FA56100
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA56100-1: MW-1M ....................................................................................................7
3.2: FA56100-2: MW-2M ....................................................................................................9
3.3: FA56100-3: MW-3M ....................................................................................................11
3.4: FA56100-4: TW-1M .....................................................................................................13
Section 4: Misc. Forms ............................................................................................................15
4.1: Chain of Custody ...........................................................................................................16
Section 5: MS Volatiles - QC Data Summaries .....................................................................18
5.1: Method Blank Summary ................................................................................................19
5.2: Blank Spike Summary ...................................................................................................23
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................27 123452 of 30
FA56100
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA56100
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Project No: 31939/2721
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA56100-1 07/24/18 00:00 WR 07/25/18 AQ Water MW-1M
FA56100-2 07/24/18 00:00 WR 07/25/18 AQ Water MW-2M
FA56100-3 07/24/18 00:00 WR 07/25/18 AQ Water MW-3M
FA56100-4 07/24/18 00:00 WR 07/25/18 AQ Water TW-1M
3 of 30
FA561001
Summary of Hits Page 1 of 2
Job Number:FA56100
Account:GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Collected:07/24/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA56100-1 MW-1M
Benzene 150 130 31 ug/l SM 6200B
o-Chlorotoluene 49.9 J 130 31 ug/l SM 6200B
Ethylbenzene 972 130 31 ug/l SM 6200B
Isopropylbenzene 47.5 J 130 31 ug/l SM 6200B
Naphthalene 320 130 31 ug/l SM 6200B
n-Propylbenzene 137 130 31 ug/l SM 6200B
Styrene 57.7 J 130 31 ug/l SM 6200B
Toluene 6550 130 31 ug/l SM 6200B
1,2,4-Trimethylbenzene 1490 130 31 ug/l SM 6200B
1,3,5-Trimethylbenzene 420 130 31 ug/l SM 6200B
m,p-Xylene 4360 250 31 ug/l SM 6200B
o-Xylene 2200 130 31 ug/l SM 6200B
Xylene (total)6560 380 63 ug/l SM 6200B
FA56100-2 MW-2M
n-Butylbenzene 4.0 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.4 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.47 J 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.24 J 0.50 0.13 ug/l SM 6200B
FA56100-3 MW-3M
Benzene 246 100 25 ug/l SM 6200B
o-Chlorotoluene 28.7 J 100 25 ug/l SM 6200B
Ethylbenzene 1190 100 25 ug/l SM 6200B
Isopropylbenzene 46.6 J 100 25 ug/l SM 6200B
Naphthalene 177 100 25 ug/l SM 6200B
n-Propylbenzene 125 100 25 ug/l SM 6200B
Styrene 69.4 J 100 25 ug/l SM 6200B
Toluene 9980 100 25 ug/l SM 6200B
1,2,4-Trimethylbenzene 894 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 237 100 25 ug/l SM 6200B
m,p-Xylene 3520 200 25 ug/l SM 6200B
o-Xylene 1600 100 25 ug/l SM 6200B
Xylene (total)5130 300 50 ug/l SM 6200B
FA56100-4 TW-1M
Ethylbenzene 0.66 0.50 0.13 ug/l SM 6200B
Toluene 6.0 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.50 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.15 J 0.50 0.13 ug/l SM 6200B
4 of 30
FA561002
Summary of Hits Page 2 of 2
Job Number:FA56100
Account:GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Collected:07/24/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
m,p-Xylene 1.1 1.0 0.13 ug/l SM 6200B
o-Xylene 0.58 0.50 0.13 ug/l SM 6200B
Xylene (total)1.7 1.5 0.25 ug/l SM 6200B
5 of 30
FA561002
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 30
FA561003
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA56100-1 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214772.D 250 07/27/18 17:58 AB n/a n/a VA2433
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 150 130 31 ug/l
108-86-1 Bromobenzene ND 130 31 ug/l
74-97-5 Bromochloromethane ND 130 31 ug/l
75-27-4 Bromodichloromethane ND 130 31 ug/l
75-25-2 Bromoform ND 130 31 ug/l
104-51-8 n-Butylbenzene ND 130 31 ug/l
135-98-8 sec-Butylbenzene ND 130 31 ug/l
98-06-6 tert-Butylbenzene ND 130 31 ug/l
56-23-5 Carbon Tetrachloride ND 130 31 ug/l
108-90-7 Chlorobenzene ND 130 31 ug/l
75-00-3 Chloroethane ND 130 50 ug/l
67-66-3 Chloroform ND 130 31 ug/l
95-49-8 o-Chlorotoluene 49.9 130 31 ug/l J
106-43-4 p-Chlorotoluene ND 130 31 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 62 ug/l
106-93-4 1,2-Dibromoethane ND 130 31 ug/l
75-71-8 Dichlorodifluoromethane ND 130 50 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l
75-34-3 1,1-Dichloroethane ND 130 31 ug/l
107-06-2 1,2-Dichloroethane ND 130 31 ug/l
75-35-4 1,1-Dichloroethylene ND 130 31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l
78-87-5 1,2-Dichloropropane ND 130 31 ug/l
142-28-9 1,3-Dichloropropane ND 130 31 ug/l
594-20-7 2,2-Dichloropropane ND 130 31 ug/l
563-58-6 1,1-Dichloropropene ND 130 31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 30
FA5610033.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA56100-1 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 31 ug/l
100-41-4 Ethylbenzene 972 130 31 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 47.5 130 31 ug/l J
99-87-6 p-Isopropyltoluene ND 130 31 ug/l
74-83-9 Methyl Bromide ND 130 50 ug/l
74-87-3 Methyl Chloride ND 130 50 ug/l
74-95-3 Methylene Bromide ND 130 31 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 130 31 ug/l
91-20-3 Naphthalene 320 130 31 ug/l
103-65-1 n-Propylbenzene 137 130 31 ug/l
100-42-5 Styrene 57.7 130 31 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l
127-18-4 Tetrachloroethylene ND 130 31 ug/l
108-88-3 Toluene 6550 130 31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l
79-01-6 Trichloroethylene ND 130 31 ug/l
75-69-4 Trichlorofluoromethane ND 130 50 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 31 ug/l
95-63-6 1,2,4-Trimethylbenzene 1490 130 31 ug/l
108-67-8 1,3,5-Trimethylbenzene 420 130 31 ug/l
75-01-4 Vinyl Chloride ND 130 31 ug/l
m,p-Xylene 4360 250 31 ug/l
95-47-6 o-Xylene 2200 130 31 ug/l
1330-20-7 Xylene (total)6560 380 63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 30
FA5610033.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA56100-2 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214773.D 1 07/27/18 18:22 AB n/a n/a VA2433
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 4.0 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.4 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 30
FA5610033.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA56100-2 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.47 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.24 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 30
FA5610033.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA56100-3 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214787.D 200 07/30/18 11:35 AB n/a n/a VA2434
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 246 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene ND 100 25 ug/l
135-98-8 sec-Butylbenzene ND 100 25 ug/l
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene 28.7 100 25 ug/l J
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 30
FA5610033.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA56100-3 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 100 25 ug/l
100-41-4 Ethylbenzene 1190 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 46.6 100 25 ug/l J
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 100 25 ug/l
91-20-3 Naphthalene 177 100 25 ug/l
103-65-1 n-Propylbenzene 125 100 25 ug/l
100-42-5 Styrene 69.4 100 25 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 9980 100 25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 894 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 237 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 3520 200 25 ug/l
95-47-6 o-Xylene 1600 100 25 ug/l
1330-20-7 Xylene (total)5130 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 30
FA5610033.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:TW-1M
Lab Sample ID:FA56100-4 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214786.D 1 07/30/18 11:12 AB n/a n/a VA2434
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 30
FA5610033.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:TW-1M
Lab Sample ID:FA56100-4 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.66 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 6.0 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.50 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.15 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.1 1.0 0.13 ug/l
95-47-6 o-Xylene 0.58 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.7 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 30
FA5610033.4
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
15 of 30
FA561004
FA56100: Chain of Custody
Page 1 of 2
16 of 30
FA5610044.1
Job Number:FA56100 Client:GRI
Date / Time Received:7/25/2018 9:00:00 AM Delivery Method:FED EX
Project:2721
Airbill #'s:1015899923610003281100812565568268
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (4.1);
Cooler 1: (4.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP SP Date:7/25/2018Date:7/25/2018 9:00:00 AM
FA56100: Chain of Custody
Page 2 of 2
17 of 30
FA5610044.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
18 of 30
FA561005
Method Blank Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2433-MB A0214754.D 1 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
19 of 30
FA5610055.1.1
Method Blank Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2433-MB A0214754.D 1 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
20 of 30
FA5610055.1.1
Method Blank Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-MB A0214784.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
21 of 30
FA5610055.1.2
Method Blank Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-MB A0214784.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
22 of 30
FA5610055.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2433-BS A0214752.D 1 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.4 94 70-130
108-86-1 Bromobenzene 10 8.3 83 70-130
74-97-5 Bromochloromethane 10 8.2 82 70-130
75-27-4 Bromodichloromethane 10 8.9 89 70-130
75-25-2 Bromoform 10 7.7 77 70-130
104-51-8 n-Butylbenzene 10 9.3 93 70-130
135-98-8 sec-Butylbenzene 10 9.8 98 70-130
98-06-6 tert-Butylbenzene 10 9.4 94 70-130
56-23-5 Carbon Tetrachloride 10 9.6 96 70-130
108-90-7 Chlorobenzene 10 9.2 92 70-130
75-00-3 Chloroethane 10 10.8 108 60-140
67-66-3 Chloroform 10 9.3 93 70-130
95-49-8 o-Chlorotoluene 10 9.5 95 70-130
106-43-4 p-Chlorotoluene 10 8.7 87 70-130
124-48-1 Dibromochloromethane 10 8.2 82 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.0 80 70-130
106-93-4 1,2-Dibromoethane 10 7.9 79 70-130
75-71-8 Dichlorodifluoromethane 10 8.5 85 60-140
95-50-1 1,2-Dichlorobenzene 10 8.3 83 70-130
541-73-1 1,3-Dichlorobenzene 10 9.0 90 70-130
106-46-7 1,4-Dichlorobenzene 10 8.8 88 70-130
75-34-3 1,1-Dichloroethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.7 97 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.0 90 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 8.4 84 70-130
594-20-7 2,2-Dichloropropane 10 9.3 93 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.2 82 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.6 86 70-130
108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130
100-41-4 Ethylbenzene 10 9.4 94 70-130
87-68-3 Hexachlorobutadiene 10 8.7 87 70-130
98-82-8 Isopropylbenzene 10 9.8 98 70-130
* = Outside of Control Limits.
23 of 30
FA5610055.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2433-BS A0214752.D 1 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 10.9 109 60-140
74-87-3 Methyl Chloride 10 10.6 106 60-140
74-95-3 Methylene Bromide 10 9.2 92 70-130
75-09-2 Methylene Chloride 10 9.8 98 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.9 89 70-130
91-20-3 Naphthalene 10 7.6 76 70-130
103-65-1 n-Propylbenzene 10 9.5 95 70-130
100-42-5 Styrene 10 8.3 83 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.5 85 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.5 85 70-130
127-18-4 Tetrachloroethylene 10 9.2 92 70-130
108-88-3 Toluene 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.1 81 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.1 81 70-130
71-55-6 1,1,1-Trichloroethane 10 9.3 93 70-130
79-00-5 1,1,2-Trichloroethane 10 8.4 84 70-130
79-01-6 Trichloroethylene 10 9.4 94 70-130
75-69-4 Trichlorofluoromethane 10 11.2 112 60-140
96-18-4 1,2,3-Trichloropropane 10 8.1 81 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.6 86 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130
75-01-4 Vinyl Chloride 10 9.7 97 60-140
m,p-Xylene 20 19.0 95 70-130
95-47-6 o-Xylene 10 9.1 91 70-130
1330-20-7 Xylene (total)30 28.1 94 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
24 of 30
FA5610055.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-BS A0214782.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 8.3 83 70-130
74-97-5 Bromochloromethane 10 8.2 82 70-130
75-27-4 Bromodichloromethane 10 9.1 91 70-130
75-25-2 Bromoform 10 8.0 80 70-130
104-51-8 n-Butylbenzene 10 9.0 90 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 9.0 90 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 11.2 112 60-140
67-66-3 Chloroform 10 9.3 93 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 8.5 85 70-130
124-48-1 Dibromochloromethane 10 8.2 82 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.9 79 70-130
106-93-4 1,2-Dibromoethane 10 7.9 79 70-130
75-71-8 Dichlorodifluoromethane 10 8.2 82 60-140
95-50-1 1,2-Dichlorobenzene 10 8.2 82 70-130
541-73-1 1,3-Dichlorobenzene 10 8.9 89 70-130
106-46-7 1,4-Dichlorobenzene 10 8.6 86 70-130
75-34-3 1,1-Dichloroethane 10 9.9 99 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 10.2 102 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 8.2 82 70-130
594-20-7 2,2-Dichloropropane 10 9.4 94 70-130
563-58-6 1,1-Dichloropropene 10 9.9 99 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.4 84 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.5 85 70-130
108-20-3 Di-Isopropyl Ether 10 9.0 90 70-130
100-41-4 Ethylbenzene 10 9.2 92 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 9.6 96 70-130
* = Outside of Control Limits.
25 of 30
FA5610055.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-BS A0214782.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.0 90 70-130
74-83-9 Methyl Bromide 10 11.3 113 60-140
74-87-3 Methyl Chloride 10 10.3 103 60-140
74-95-3 Methylene Bromide 10 9.4 94 70-130
75-09-2 Methylene Chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130
91-20-3 Naphthalene 10 7.5 75 70-130
103-65-1 n-Propylbenzene 10 9.2 92 70-130
100-42-5 Styrene 10 8.2 82 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 9.3 93 70-130
108-88-3 Toluene 10 9.1 91 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.9 79 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.9 79 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 8.2 82 70-130
79-01-6 Trichloroethylene 10 9.4 94 70-130
75-69-4 Trichlorofluoromethane 10 11.2 112 60-140
96-18-4 1,2,3-Trichloropropane 10 8.0 80 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.4 84 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.3 93 70-130
75-01-4 Vinyl Chloride 10 9.5 95 60-140
m,p-Xylene 20 18.6 93 70-130
95-47-6 o-Xylene 10 9.0 90 70-130
1330-20-7 Xylene (total)30 27.6 92 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
26 of 30
FA5610055.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56090-2MS A0214763.D 50 07/27/18 AB n/a n/a VA2433
FA56090-2MSD A0214764.D 50 07/27/18 AB n/a n/a VA2433
FA56090-2 A0214776.D 50 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
FA56090-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 500 409 82 500 434 87 6 70-130/20
108-86-1 Bromobenzene ND 500 362 72 500 397 79 9 70-130/20
74-97-5 Bromochloromethane ND 500 361 72 500 384 77 6 70-130/20
75-27-4 Bromodichloromethane ND 500 373 75 500 400 80 7 70-130/20
75-25-2 Bromoform ND 500 282 56*500 304 61*8 70-130/20
104-51-8 n-Butylbenzene 20.8 J 500 504 82 500 540 89 7 70-130/20
135-98-8 sec-Butylbenzene 11.2 J 500 472 86 500 507 93 7 70-130/20
98-06-6 tert-Butylbenzene ND 500 435 87 500 467 93 7 70-130/20
56-23-5 Carbon Tetrachloride ND 500 421 84 500 453 91 7 70-130/20
108-90-7 Chlorobenzene ND 500 410 82 500 437 87 6 70-130/20
75-00-3 Chloroethane ND 500 506 101 500 563 113 11 60-140/20
67-66-3 Chloroform ND 500 450 80 500 477 85 6 70-130/20
95-49-8 o-Chlorotoluene 51.4 500 517 103 500 550 110 6 70-130/20
106-43-4 p-Chlorotoluene ND 500 377 75 500 410 82 8 70-130/20
124-48-1 Dibromochloromethane ND 500 322 64*500 349 70 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 599 120 500 628 126 5 70-130/20
106-93-4 1,2-Dibromoethane ND 500 349 70 500 372 74 6 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 385 77 500 435 87 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 500 368 74 500 396 79 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 500 399 80 500 432 86 8 70-130/20
106-46-7 1,4-Dichlorobenzene ND 500 385 77 500 417 83 8 70-130/20
75-34-3 1,1-Dichloroethane ND 500 429 86 500 459 92 7 70-130/20
107-06-2 1,2-Dichloroethane ND 500 410 82 500 428 86 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 432 86 500 454 91 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 500 394 79 500 428 86 8 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 424 85 500 450 90 6 70-130/20
78-87-5 1,2-Dichloropropane ND 500 417 83 500 447 89 7 70-130/20
142-28-9 1,3-Dichloropropane ND 500 371 74 500 391 78 5 70-130/20
594-20-7 2,2-Dichloropropane ND 500 385 77 500 409 82 6 70-130/20
563-58-6 1,1-Dichloropropene ND 500 429 86 500 458 92 7 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 348 70 500 371 74 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 363 73 500 382 76 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 500 405 81 500 435 87 7 70-130/20
100-41-4 Ethylbenzene 403 500 932 73 500 964 79 3 70-130/20
87-68-3 Hexachlorobutadiene ND 500 422 84 500 453 91 7 70-130/20
98-82-8 Isopropylbenzene 35.1 500 516 88 500 551 95 7 70-130/20
* = Outside of Control Limits.
27 of 30
FA5610055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56090-2MS A0214763.D 50 07/27/18 AB n/a n/a VA2433
FA56090-2MSD A0214764.D 50 07/27/18 AB n/a n/a VA2433
FA56090-2 A0214776.D 50 07/27/18 AB n/a n/a VA2433
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-1, FA56100-2
FA56090-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 12.2 J 500 464 84 500 499 91 7 70-130/20
74-83-9 Methyl Bromide ND 500 507 101 500 551 110 8 60-140/20
74-87-3 Methyl Chloride ND 500 513 103 500 538 108 5 60-140/20
74-95-3 Methylene Bromide ND 500 407 81 500 427 85 5 70-130/20
75-09-2 Methylene Chloride ND 500 418 84 500 447 89 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 500 385 77 500 402 80 4 70-130/20
91-20-3 Naphthalene 173 500 727 67*500 750 71 3 70-130/20
103-65-1 n-Propylbenzene 100 500 636 80 500 679 89 7 70-130/20
100-42-5 Styrene ND 500 377 75 500 406 81 7 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 382 76 500 418 84 9 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 374 75 500 396 79 6 70-130/20
127-18-4 Tetrachloroethylene ND 500 411 82 500 453 91 10 70-130/20
108-88-3 Toluene 135 500 552 80 500 579 85 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 375 75 500 400 80 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 379 76 500 408 82 7 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 407 81 500 435 87 7 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 599 120 500 641 128 7 70-130/20
79-01-6 Trichloroethylene ND 500 423 85 500 449 90 6 70-130/20
75-69-4 Trichlorofluoromethane ND 500 502 100 500 545 109 8 60-140/20
96-18-4 1,2,3-Trichloropropane ND 500 356 71 500 371 74 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1220 500 3040 20* a 500 3190 50* a 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 456 500 1380 62* a 500 1460 78 6 70-130/20
75-01-4 Vinyl Chloride ND 500 442 88 500 480 96 8 60-140/20
m,p-Xylene 1890 1000 3240 51* a 1000 3320 59* a 2 70-130/20
95-47-6 o-Xylene 612 500 1220 64*500 1260 72 3 70-130/20
1330-20-7 Xylene (total)2500 1500 4460 55* a 1500 4580 63* a 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA56090-2 Limits
1868-53-7 Dibromofluoromethane 102%102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%106%107%70-130%
2037-26-5 Toluene-D8 101%100%100%70-130%
460-00-4 4-Bromofluorobenzene 98%98%97%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
28 of 30
FA5610055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56100-3MS A0214797.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3MSD A0214798.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3 A0214787.D 200 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
FA56100-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 246 2000 2160 96 2000 2230 99 3 70-130/20
108-86-1 Bromobenzene ND 2000 1680 84 2000 1730 87 3 70-130/20
74-97-5 Bromochloromethane ND 2000 1630 82 2000 1690 85 4 70-130/20
75-27-4 Bromodichloromethane ND 2000 1710 86 2000 1830 92 7 70-130/20
75-25-2 Bromoform ND 2000 1210 61*2000 1450 73 18 70-130/20
104-51-8 n-Butylbenzene ND 2000 1830 92 2000 1880 94 3 70-130/20
135-98-8 sec-Butylbenzene ND 2000 1910 96 2000 1970 99 3 70-130/20
98-06-6 tert-Butylbenzene ND 2000 1860 93 2000 1900 95 2 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 1940 97 2000 2020 101 4 70-130/20
108-90-7 Chlorobenzene ND 2000 1860 93 2000 1920 96 3 70-130/20
75-00-3 Chloroethane ND 2000 2160 108 2000 2290 115 6 60-140/20
67-66-3 Chloroform ND 2000 1910 96 2000 1950 98 2 70-130/20
95-49-8 o-Chlorotoluene 28.7 J 2000 1900 94 2000 1960 97 3 70-130/20
106-43-4 p-Chlorotoluene ND 2000 1720 86 2000 1770 89 3 70-130/20
124-48-1 Dibromochloromethane ND 2000 1430 72 2000 1580 79 10 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 1500 75 2000 1590 80 6 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 1540 77 2000 1620 81 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1540 77 2000 1680 84 9 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 1640 82 2000 1720 86 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 1790 90 2000 1870 94 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 1760 88 2000 1810 91 3 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2010 101 2000 2060 103 2 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1890 95 2000 1960 98 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2080 104 2000 2130 107 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 1830 92 2000 1920 96 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2010 101 2000 2060 103 2 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 1900 95 2000 1980 99 4 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 1650 83 2000 1700 85 3 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 1900 95 2000 1880 94 1 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 2000 100 2000 2090 105 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1610 81 2000 1680 84 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1640 82 2000 1690 85 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 1850 93 2000 1910 96 3 70-130/20
100-41-4 Ethylbenzene 1190 2000 3110 96 2000 3140 98 1 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 1740 87 2000 1790 90 3 70-130/20
98-82-8 Isopropylbenzene 46.6 J 2000 2010 98 2000 2080 102 3 70-130/20
* = Outside of Control Limits.
29 of 30
FA5610055.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA56100
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56100-3MS A0214797.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3MSD A0214798.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3 A0214787.D 200 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56100-3, FA56100-4
FA56100-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 2000 1830 92 2000 1900 95 4 70-130/20
74-83-9 Methyl Bromide ND 2000 2110 106 2000 2270 114 7 60-140/20
74-87-3 Methyl Chloride ND 2000 2090 105 2000 2150 108 3 60-140/20
74-95-3 Methylene Bromide ND 2000 1850 93 2000 1900 95 3 70-130/20
75-09-2 Methylene Chloride ND 2000 2000 100 2000 2060 103 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 2000 1730 87 2000 1780 89 3 70-130/20
91-20-3 Naphthalene 177 2000 1700 76 2000 1740 78 2 70-130/20
103-65-1 n-Propylbenzene 125 2000 2010 94 2000 2070 97 3 70-130/20
100-42-5 Styrene 69.4 J 2000 1750 84 2000 1830 88 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 1660 83 2000 1740 87 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 1620 81 2000 1670 84 3 70-130/20
127-18-4 Tetrachloroethylene ND 2000 1880 94 2000 1950 98 4 70-130/20
108-88-3 Toluene 9980 2000 11600 81 2000 11400 71 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 1580 79 2000 1620 81 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 1600 80 2000 1650 83 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 1900 95 2000 1950 98 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 1650 83 2000 1700 85 3 70-130/20
79-01-6 Trichloroethylene ND 2000 1870 94 2000 1970 99 5 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 2080 104 2000 2250 113 8 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1530 77 2000 1630 82 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene 894 2000 2690 90 2000 2740 92 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 237 2000 2160 96 2000 2210 99 2 70-130/20
75-01-4 Vinyl Chloride ND 2000 1800 90 2000 1920 96 6 60-140/20
m,p-Xylene 3520 4000 7360 96 4000 7410 97 1 70-130/20
95-47-6 o-Xylene 1600 2000 3470 94 2000 3510 96 1 70-130/20
1330-20-7 Xylene (total)5130 6000 10800 95 6000 10900 96 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA56100-3 Limits
1868-53-7 Dibromofluoromethane 102%102%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%107%109%70-130%
2037-26-5 Toluene-D8 99%98%99%70-130%
460-00-4 4-Bromofluorobenzene 97%97%99%70-130%
* = Outside of Control Limits.
30 of 30
FA5610055.3.2

APPENDIX C
Notice of Intent to Construct or Operate Injection Wells

APPENDIX D:
Injection Event Record