WA-26757_31939_CA_RPTS_20170823_AFVR

EXECUTIVE SUMMARY

The Miller’s Country Store site (Miller’s) is located at 1706 US Highway 17, North, Merry Hill, Bertie
County, North Carolina. According to available information, a release was discovered during UST
closure activities conducted at the site in September 2008. Three 4,000-gallon gasoline USTs were
removed from the site in September 2008 and one orphan 2,000-gallon UST whose former contents are
unknown was removed from the site in April 2009. Municipal water is available to the site and
surrounding properties. Additional petroleum releases (UST Incident Number 11963 – Todd’s Service
Center and UST Incident Number 13592 – Bowen’s Grocery) are located adjacent to the Miller’s site and
are considered to be commingled with the Miller’s contaminant plume. The current risk classification is
high due to the presence of water supply wells within a 250-foot radius of the source area.

On June 6, 2017, an 8-hour Aggressive Fluid-Vapor Recovery (AFVR) event was conducted on
monitoring wells MW-1M and MW-3M in order to reduce the contaminant concentrations at the site. No
free product was measured in either well prior to the start of the event. Approximately 1,094 gallons of
petroleum impacted ground water was removed during the 8-hour AFVR event. No free product was
observed in the tanker at the conclusion of the event. Based on mass-removal calculations, approximately
18.87 pounds or 3.02 gallons of vapor phase hydrocarbons were removed. An average of 0.38 gallons of
vapor phase product was removed per hour. At the conclusion of the event, no free product was measured
in the vacuum wells.

A ground water monitoring event was conducted for the Todd’s, Bowen’s and Miller’s sites on July 12,
2017. On July 12, 2017, fifteen Type II monitoring wells (MW-1A, MW-2, MW-4, MW-11, MW-15,
MW-22, MW-23A, MW-26, MW-29, MW-36, MW-44, MW-46, MW-1M, MW-2M, and MW-3M), one
Type III monitoring well (TW-1M) and one water supply well (WSW-13) were gauged, purged and/or
sampled. No free product was measured in any of the wells sampled. Concentrations of requested
method constituents that exceeded the Maximum Allowable Concentrations (MACs) were reported in
MW-1A, MW-2, MW-4, MW-11, MW-15, MW-22, MW-29, MW-1M, MW-3M and TW-1M. None of
the reported contaminant concentrations exceeded the Gross Contamination Levels.

Based on this information, semi-annual ground water monitoring should continue at the site until the
NTCP can be completed and implemented. Additional AFVR events should be conducted as needed in
order to continue to reduce the contaminant concentrations at the site. The next semi-annual ground
water monitoring event is tentatively scheduled for January 2018.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 AFVR EVENT .......................................................................................................................... 2
4.0 GROUND WATER QUALITY ................................................................................................ 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
6.0 LIMITATIONS ......................................................................................................................... 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results
Table 3: Free Product Recovery Event Information
Table 4: Free Product Recovery Cost Summary
Table 5: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: AFVR Data, Calculations and Disposal Manifest
Appendix B: Laboratory Report - Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Miller’s Country Store site is located at 1706 US Highway 17 N in Merry Hill, Bertie County, North
Carolina (Figure 1). The subject site is a former retail petroleum facility. According to available
information, three 4,000-gallon gasoline USTs were removed from the site on September 9, 2008, and
one orphan 2,000-gallon UST, whose former contents are unknown, was removed from the site on April
30, 2009. An additional UST system consisting of three 3,000-gallon gasoline USTs was removed from
the site on September 1, 1988. A release at the site was discovered when petroleum impacted soil was
encountered during the September 2008 UST closure event.

Three Type II monitoring wells (MW-1M, MW-2M and MW-3M) and one Type III monitoring well
(TW-1M) were installed at the site during past assessment activities. A receptor survey was conducted on
October 1, 2009. Eighteen water supply wells were identified within a 1,500-foot radius of the site.
Three out of service water supply wells (WSW-1, WSW-2 and WSW-3) were identified within a 250-foot
radius of the site. Municipal water is available to the site and surrounding properties. A Site Vicinity
Map showing properties and water supply wells within a 1,500-foot radius of the source area is included
as Figure 2. A Site Map is included as Figure 3. This sampling event was conducted in conjunction
with the sampling event at the adjacent Todd’s and Bowen’s sites. The releases from all three sites are
commingled.

Certain information in this report was obtained as a result of assessment activities conducted by past
consultants. Although Geological Resources Inc. (GRI) cannot verify the accuracy of this information,
for the purpose of this report, it is assumed to be correct. Any inferences or interpretations made by GRI
based on data that may be incorrect are not the responsibility of GRI. Please refer to earlier submittals for
additional information regarding past assessment activities.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of Aggressive Fluid-Vapor Recovery (AFVR) and ground water sampling
activities conducted between June and July 2017 at the Miller’s Country Store site. The subject site is a
former petroleum retail facility. The property is currently vacant. The activities were conducted in
accordance with GRI proposal numbers 16-791 and 17-275, which were submitted to NCDEQ on January
31, 2017 and April 13, 2017, respectively. The proposals were approved as Task Authorization Nos.
31939-07 and 08 on February 1, 2017, and April 27, 2017, respectively. The purpose of the activities was
to reduce contaminant concentrations and obtain current ground water quality data for the site.

2
3.0 AFVR EVENT
On June 6, 2017, an AFVR event was conducted by Greenwood Applied Services, LLC (GAS), under the
supervision of GRI personnel. The AFVR equipment included a vacuum truck, flexible vacuum hoses,
1.5-inch diameter PVC stinger pipes and associated couplings and pipe fittings needed to connect to two
monitoring wells (MW-1M and MW-3M). The vacuum truck had a storage capacity of 3,500 gallons and
was rated at 680 CFM at 18 in/Hg. Prior to the event, the depths to product and ground water were
measured in the vacuum wells. No free product was measured in any of the monitoring wells prior to the
even. During the event, which was conducted for approximately 8 hours (total), measurements of
vacuum, relative humidity, temperature, exhaust air velocity and off-gas concentrations were recorded at
15-minute intervals for the first two hours and every 30 minutes thereafter. No measurable free product
was reported at the conclusion of the event. A summary of well construction information and ground
water gauging data is presented in Table 1. A copy of the AFVR field data sheet has been included as
Appendix A.

The results of the AFVR event indicate that a total of 1,094 gallons of liquid was removed during the 8-
hour event. No free product was observed in the tanker at the conclusion of the event. Based on 8 hours
of operation, the average fluid recovery rate was 136.75 gallons per hour. Based on mass removal
calculations, 18.87 pounds or 3.02 gallons of vapor phase hydrocarbons were removed. Based on 8 hours
of operation, an average of 0.38 gallons of vapor phase free product was removed per hour by the AFVR
event. Based on the June 2017 AFVR event, the cost per gallon of fluids recovered was $2.18/gallon. A
Site Map showing the locations of the monitoring wells and the structures on-site and on surrounding
properties has been included as Figure 2. A summary of the free product recovery results is presented in
Table 2. A summary of information collected during the AFVR event as well as a breakdown of fluids
removed is included in Table 3. A summary of costs associated with free product and total fluids
recovery is included in Table 4. The AFVR data calculations are included as Appendix A. At the
conclusion of the AFVR event, all wastewater was transported to a permitted facility for disposal. A copy
of the disposal manifest has been included as Appendix A.

4.0 GROUND WATER QUALITY
Three Type II monitoring wells (MW-1M, MW-2M, and MW-3M) and one Type III monitoring well
(TW-1M) were gauged, purged and sampled on July 12, 2017. Please note, monitoring wells associated
with the Todd’s Service Center and Bowen’s Grocery sites (MW-1A, MW-2, MW-4, MW-11, MW-15,
MW-22, MW-23A, MW-26, MW-29, MW-36 and MW-44), as well as WSW-3, were gauged, purged

3
and/or sampled for those incidents concurrently with the Miller’s Country Store site and are included in
data collected for the July 2017 sampling event.

The depths to ground water in the Type II monitoring wells during the July 2017 sampling event ranged
from 6.94 to 20.07 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from
75.30 to 80.64 feet. Based on this information, the direction of ground water flow was generally toward
the east. The average horizontal hydraulic gradient across the site was less than 0.01 feet per foot. The
vertical gradient calculated for paired wells MW-1M and TW-1M was approximately 0.02 feet per foot
upward. A Water Table Surface Map for the July 2017 sampling event has been included as Figure 4.
Well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the July 2017 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the
Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-1A, MW-2, MW-4, MW-11, MW-15, MW-29, MW-1M, MW-
3M and TW-1M. None of the reported contaminant concentrations exceeded the Gross Contamination
Levels (GCLs). No detectable contaminant concentrations were reported in the ground water sample
collected from WSW-13. A Ground Water Quality Map based on data from the July 12, 2017, sampling
event has been included as Figure 5. A summary of ground water sample analytical results is presented
in Table 5. A complete laboratory report has been included as Appendix B.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 A total of 1,094 gallons of petroleum contaminated ground water was recovered during the
AFVR event conducted on June 6, 2017. No free product was reported in the extraction wells at
the start of or the conclusion of the event. Based on mass-removal calculations, 3.02 gallons of
vapor phase hydrocarbons were removed during the June 2017 AFVR event.
 The average depth to ground water in the Type II monitoring wells in July 2017 was 18.45 feet
below the tops of well casings. Ground water flow was generally toward the east with an average
horizontal hydraulic gradient of less than 0.01 feet per foot. The average vertical gradient
between paired wells MW-1M and TW-1M was approximately 0.02 feet per foot upward.

4
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the
MACs were reported in the ground water samples collected from MW-1A, MW-2, MW-4, MW-
11, MW-15, MW-29, MW-1M, MW-3M and TW-1M. None of the reported contaminant
concentrations exceeded the GCLs. No detectable contaminant concentrations were reported in
the ground water sample collected from WSW-13.
 Based on this information, the site should remain high risk. Semi-annual ground water
monitoring should continue at the site. Additional MMPE and/or AFVR events should be
conducted as needed in order to continue to reduce the contaminant concentrations at the site.
The next semi-annual ground water monitoring event is tentatively scheduled for January 2018.

6.0 LIMITATIONS
This report has been prepared for the exclusive use of Ms. Shirley Miller for the specific application to
the reference site in Bertie County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of environmental practices
in the State of North Carolina, available information, and our professional judgment. No other warranty
is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the times the samples were collected. In addition, the data obtained from the samples
would be interpreted as being meaningful with respect to parameters indicated in the laboratory report.
No additional information can logically be inferred from these data.

FIGURES
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"J
SITE
U S 1 7 H W Y
NC 45 HWYU S 1 7 H W Y
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-1
WSW-12
WSW-18
WSW-17
WSW-19 WSW-16
WSW-15
WSW-14
WSW-13
WSW-11
WSW-10³
0 300150
Feet
FIGURE 2: SITE VICINITY MAPMILLER'S COUNTRY STORE1706 US HIGHWAY 17 NORTHMERRY HILL,BERTIE COUNTYNORTH CAROLINAINCIDENT NO. 31939GRI PROJECT NO. 2721
PREPARED BYGEOLOGICAL RESOURCES, INC.SEPTEMBER 16, 2009
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
Legend
"J Water Supply Well
River_Line
Centerline
Parcel_Polygon
Pond_Lake_Polygon
6853575623
6853487515 PIN Number

TABLES
Date: 07/17/17
11/01/07
09/16/09
09/20/10
10/27/11
01/07/13
11/01/07 99.34 21.00 ---78.34
07/20/09 22.00 0.01 78.01 Pre-MMPE
07/24/09 21.25 ---78.75 Post-MMPE
09/16/09 21.57 ---78.43
09/20/10 19.92 ---80.08
10/27/11 19.90 ---80.10
12/03/12 21.45 ---78.55 Pre-MMPE
12/07/12 20.50 ---79.50 Post-MMPE
01/07/13 21.47 ---78.53
06/24/13 21.09 ---78.91 Pre-MMPE
06/28/13 21.19 ---78.81 Post-MMPE
07/29/13 NM NM NM Not Found
05/19/14 19.54 ---80.46 Pre-MMPE
05/23/14 19.45 ---80.55 Post-MMPE
06/23/14 19.68 ---80.32
07/06/15 NM NM NM Not Found
01/27/16 20.13 ---79.87
08/01/16 19.58 ---80.42 Pre-AFVR
08/01/16 19.91 ---80.09 Post-AFVR
09/07/16 20.29 ---79.71
07/12/17 20.07 ---79.93
11/01/07 99.51 20.92 ---78.59
07/20/09 21.07 ---78.79 Pre-MMPE
07/24/09 21.34 ---78.52 Post-MMPE
09/16/09 21.48 ---78.38
09/20/10 19.83 ---80.03
10/27/11 19.86 ---80.00
12/03/12 21.37 ---78.49 Pre-MMPE
12/07/12 21.42 ---78.44 Post-MMPE
01/07/13 21.40 ---78.46
06/24/13 20.91 ---78.95 Pre-MMPE
06/28/13 21.06 ---78.80 Post-MMPE
07/29/13 20.43 ---79.43
05/19/14 19.49 ---80.37 Pre-MMPE
05/23/14 19.44 ---80.42 Post-MMPE
06/23/14 19.62 ---80.24
06/01/15 18.39 ---81.47 Pre-MMPE
06/05/15 18.51 ---81.35 Post-MMPE
07/06/15 19.13 ---80.73
01/27/16 20.07 ---79.79
09/07/16 20.13 ---79.73
07/12/17 20.00 ---79.86
11/01/07 99.59 20.86 ---78.73
09/16/09 21.40 ---78.56
09/20/10 19.74 ---80.22
10/27/11 19.70 ---80.26
01/07/13 21.27 ---78.69
07/29/13 20.31 ---79.65
05/19/14 19.40 ---80.56 Pre-MMPE
05/23/14 19.29 ---80.67 Post-MMPE
06/03/14 19.47 ---80.49
06/01/15 18.22 ---81.74 Pre-MMPE
06/05/15 18.34 ---81.62 Post-MMPE
07/06/15 18.98 ---80.98
01/27/16 19.89 ---80.07
08/01/16 19.37 ---80.59 Pre-AFVR
08/01/16 19.50 ---80.46 Post-AFVR
MW-1A
99.862515-251504/27/94MW-2
20-302011/16/01
MW-3 04/27/94 15 15-25
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
25 99.96
100.0030
Casing
Collapsed
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
MW-1 04/27/94 15 15-25 25
Page 1 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 99.57 20.60 ---78.99
09/16/09 NM NM NM
09/20/10 19.47 ---80.10
10/27/11 19.40 ---80.17
12/03/12 21.00 ---78.57 Pre-MMPE
12/07/12 21.06 ---78.51 Post-MMPE
01/07/13 21.03 ---78.54
06/24/13 20.55 ---79.02 Pre-MMPE
06/28/13 20.67 ---78.90 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 19.19 ---80.38
07/06/15 18.73 ---80.84
01/27/16 19.64 ---79.93
08/01/16 19.11 ---80.46 Pre-AFVR
08/01/16 19.30 ---80.27 Post-AFVR
09/07/16 19.74 ---79.83
07/12/17 19.60 ---79.97
11/01/07 99.19 20.29 ---78.90
09/16/09 20.85 ---78.72
09/20/10 19.17 ---80.40
10/27/11 19.10 ---80.47
01/07/13 20.70 ---78.87
07/29/13 19.76 ---79.81
05/19/14 18.69 ---80.88 Pre-MMPE
05/23/14 18.58 ---80.99 Post-MMPE
06/23/14 18.83 ---80.74
07/06/15 18.38 ---81.19
01/27/16 19.25 ---80.32
07/12/17 NM NM NM Not Found
11/01/07 99.27 21.20 ---78.07
09/16/09 21.06 ---78.60
09/20/10 19.74 ---79.92
10/27/11 19.48 ---80.18
01/07/13 21.04 ---78.62
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 99.00 20.41 ---78.59
09/16/09 20.96 ---78.44
09/20/10 19.31 ---80.09
10/27/11 19.32 ---80.08
01/07/13 20.84 ---78.56
07/29/13 20.40 ---79.00
06/23/14 19.07 ---80.33
07/06/15 18.59 ---80.81
11/01/07 99.28 20.63 ---78.65
09/16/09 21.20 ---78.47
09/20/10 19.55 ---80.12
10/27/11 19.48 ---80.19
01/07/13 21.07 ---78.60
07/29/13 NM NM NM Not Found
06/23/14 19.25 ---80.42
07/06/15 18.78 ---80.89
11/01/07 99.11 20.45 ---78.66
09/16/09 21.22 ---78.31
09/20/10 19.58 ---79.95
10/27/11 19.55 ---79.98
01/07/13 21.10 ---78.43
07/29/13 20.12 ---79.41
06/23/14 19.30 ---80.23
07/06/15 18.82 ---80.71
11/01/07 98.11 19.73 ---78.38
09/16/09 20.29 ---78.07
09/20/10 18.65 ---79.71
10/27/11 18.68 ---79.68
01/07/13 20.20 ---78.16
07/29/13 19.23 ---79.13
06/23/14 18.36 ---80.00
07/06/15 18.00 ---80.36
01/27/16 18.90 ---79.46
09/07/16 18.47 ---79.89
07/12/17 18.82 ---79.54
98.362818-281812/01/95MW-11
04/27/94MW-5
99.572515-251504/27/94MW-4
99.5725
MW-10A 10/31/07 15 15-25 25 99.53
MW-9A 10/31/07 15 15-25 25 99.67
44 99.66
MW-7 11/24/95 18 18-28 28 99.40
MWD-6 11/22/95 39 39-44
15-2515
Page 2 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 98.28 19.92 ---78.36
07/20/09 20.03 ---78.63 Pre-MMPE
07/24/09 20.21 ---78.45 Post-MMPE
09/16/09 20.48 ---78.18
09/20/10 18.75 ---79.91
10/27/11 18.87 ---79.79
12/03/12 20.39 ---78.27 Pre-MMPE
12/07/12 20.45 ---78.21 Post-MMPE
01/07/13 20.40 ---78.26
06/24/13 19.83 ---78.83 Pre-MMPE
06/28/13 19.95 ---78.71 Post-MMPE
07/29/13 19.46 ---79.20
05/19/14 18.51 ---80.15 Pre-MMPE
05/23/14 18.43 ---80.23 Post-MMPE
06/23/14 NM NM NM Not Found
09/07/16 NM NM NM Destroyed
07/12/17 NM NM NM Destroyed
11/01/07 98.23 19.85 ---78.38
09/16/09 20.40 ---78.20
09/20/10 18.77 ---79.83
10/27/11 18.81 ---79.79
01/07/13 20.30 ---78.30
07/29/13 19.40 ---79.20
06/23/14 NM NM NM Not Found
11/01/07 98.90 20.17 ---78.73
09/16/09 20.71 ---78.61
09/20/10 19.07 ---80.25
10/27/11 19.01 ---80.31
12/03/12 20.59 ---78.73 Pre-MMPE
12/07/12 20.66 ---78.66 Post-MMPE
01/07/13 20.60 ---78.72
06/24/13 20.11 ---79.21 Pre-MMPE
06/28/13 20.23 ---79.09 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
07/06/15 18.30 ---81.02
06/23/14 18.94 ---NM
01/27/16 19.34 ---NM
07/12/17 19.36 ---NM
11/01/07 99.34 20.42 ---78.92
09/16/09 20.97 ---78.76
09/20/10 19.23 ---80.50
10/27/11 19.20 ---80.53
01/07/13 20.51 ---79.22
07/29/13 NM NM NM Not Found
05/19/14 18.80 ---80.93 Pre-MMPE
05/23/14 18.78 ---80.95 Post-MMPE
06/23/14 NM NM NM Not Found
11/01/07 98.66 20.26 ---78.40
09/16/09 20.89 ---78.06
09/20/10 19.22 ---79.73
10/27/11 19.22 ---79.73
01/07/13 20.78 ---78.17
07/29/13 19.84 ---79.11
06/23/14 19.00 ---79.95
07/06/15 18.56 ---80.39
11/01/07 98.08 19.57 ---78.51
09/16/09 20.13 ---78.41
09/20/10 18.50 ---80.04
10/27/11 18.51 ---80.03
01/07/13 20.00 ---78.54
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 98.23 20.12 ---78.11
09/16/09 20.73 ---77.90
09/20/10 19.10 ---79.53
10/27/11 19.14 ---79.49
01/07/13 20.65 ---77.98
07/29/13 19.76 ---78.87
06/23/14 18.98 ---79.25
07/06/15 18.50 ---80.13
98.66
12/08/95MW-15
MW-20 04/22/96 18 18-28 28 98.63
MW-19 04/22/96 18 18-28 28 98.54
MW-17 04/19/96 18 18-28 28 98.95
MW-15A 11/01/07 15 15-25 25 99.73
NM2818-2818
MW-14 11/28/95 15 15-25 25 99.32
MW-13 11/30/95 15 15-25 25 98.60
2812/01/95MW-12 18-2818
Page 3 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 100.03 20.57 ---79.46
09/16/09 21.18 ---79.21
09/20/10 19.41 ---80.98
10/27/11 19.25 ---81.14
01/07/13 20.95 ---79.44
07/29/13 20.84 ---79.55
06/23/14 18.99 ---81.40
11/01/07 99.07 20.10 ---78.97
09/16/09 20.62 ---78.90
09/20/10 18.94 ---80.58
10/27/11 18.91 ---80.61
01/07/13 20.49 ---79.03
07/29/13 19.44 ---80.08
05/19/14 18.41 ---81.11 Pre-MMPE
05/23/14 18.62 ---80.90 Post-MMPE
06/23/14 18.61 ---80.91
06/01/15 17.35 ---82.17 Pre-MMPE
06/05/15 17.65 ---81.87 Post-MMPE
07/06/15 18.14 ---81.38
01/27/16 19.02 ---80.50
07/12/17 19.04 ---80.48
11/01/07 98.90 20.14 ---78.76
09/16/09 20.69 ---78.80
09/20/10 18.95 ---80.54
10/27/11 18.92 ---80.57
01/07/13 20.54 ---78.95
07/29/13 19.46 ---80.03
06/23/14 18.66 ---80.83
07/06/15 18.19 ---81.30
01/27/16 19.05 ---80.44
07/12/17 19.07 ---80.42
11/01/07 99.41 20.10 ---79.31
09/16/09 20.69 ---79.12
09/20/10 NM NM NM
11/01/07 98.43 20.42 ---78.01
09/16/09 21.01 ---77.88
09/20/10 19.38 ---79.51
10/27/11 19.50 ---79.39
01/07/13 20.92 ---77.97
07/29/13 20.07 ---78.82
06/23/14 19.31 ---79.58
07/06/15 18.80 ---80.09
11/01/07 97.29 19.57 ---77.72
09/16/09 20.13 ---77.57
09/20/10 18.58 ---79.12
10/27/11 18.65 ---79.05
01/07/13 20.07 ---77.63
07/29/13 19.30 ---78.40
18.24 ---79.46 Pre-AFVR
18.30 ---79.40 Post-AFVR
06/23/14 18.52 ---79.18
06/01/15 17.40 ---80.30 Pre-AFVR
06/01/15 17.44 ---80.26 Post-AFVR
07/06/15 18.05 ---79.65
01/27/16 18.90 ---78.80
09/07/16 18.98 ---78.72
07/12/17 18.86 ---78.84
11/01/07 98.36 NM NM NM Well Dry
09/16/09 NM NM NM Well Dry
09/20/10 NM NM NM Well Dry
10/27/11 NM NM NM Well Dry
01/07/13 17.25 ---81.53
07/29/13 NM NM NM Well Dry
06/23/14 NM NM NM Well Dry
07/06/15 NM NM NM Well Dry
11/01/07 95.54 18.14 ---77.40
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
10/04/12 20.92 ---74.62 Pre-AFVR
10/04/12 20.93 ---74.61 Post-AFVR
01/07/13 NM NM NM
06/23/14 NM NM NM
28
1809/25/96MW-26
99.493020-302011/01/07MW-23A
99.5218-281809/24/96
100.39
MW-28 10/15/98 22 22-32 32 95.54
MW-27 10/03/96 8 8-18 18 98.78
05/22/14
97.702818-28
MW-25B 11/01/07 15 15-25 25 98.89
MW-24 09/25/96 18 18-28 28 99.81
MW-22
MW-21 09/24/96 18 18-28 28
Page 4 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 97.70 20.25 ---77.45
09/16/09 20.85 ---77.30
09/20/10 19.31 ---78.84
10/27/11 19.47 ---78.68
20.81 ---77.34 Pre-AFVR
20.82 ---77.33 Post-AFVR
01/07/13 20.77 ---77.38
20.52 ---77.63 Pre-AFVR
20.52 ---77.63 Post-AFVR
07/29/13 20.05 ---78.10
18.88 ---79.27 Pre-AFVR
19.05 ---79.10 Post-AFVR
06/23/14 19.32 ---78.83
06/01/15 18.23 ---79.92 Pre-AFVR
06/01/15 18.23 ---79.92 Post-AFVR
07/06/15 19.32 ---78.83
01/27/16 19.67 ---78.48
09/07/16 19.77 ---78.38
07/12/17 19.67 ---78.48
11/01/07 96.32 19.34 ---76.98
09/16/09 19.88 ---76.85
09/20/10 NM NM NM
11/01/07 97.86 20.37 ---77.49
09/16/09 20.96 ---77.28
09/20/10 19.42 ---78.82
10/27/11 19.51 ---78.73
01/07/13 20.83 ---77.41
07/29/13 19.14 ---79.10
06/23/14 19.39 ---78.85
07/06/15 18.97 ---79.27
11/01/07 97.64 19.30 ---78.34
09/16/09 19.87 ---78.47
09/20/10 NM NM NM
11/01/07 94.72 18.32 ---76.40
09/16/09 18.81 ---76.38
09/20/10 17.51 ---77.68
10/27/11 17.68 ---77.51
01/07/13 18.78 ---76.41
07/29/13 18.31 ---76.88
06/23/14 17.68 ---77.51
07/06/15 17.30 ---77.89
01/27/16 17.95 ---77.24
09/07/16 18.07 ---77.12
11/01/07 NA 6.53 ------
09/16/09 7.03 ---75.21
09/20/10 6.40 ---75.84
10/27/11 6.47 ---75.77
01/07/13 7.23 ---75.01
07/29/13 6.95 ---75.29
06/23/14 6.69 ---75.55
07/06/15 6.47 ---75.77
07/12/17 6.94 ---75.30
09/16/09 20.36 ---79.16
09/20/10 NM NM NM
09/16/09 17.58 ---75.75
09/20/10 16.50 ---76.83
10/27/11 16.64 ---76.69
01/07/13 17.67 ---75.66
07/29/13 17.17 ---76.16
06/23/14 16.68 ---76.65
07/06/15 16.35 ---76.98
09/16/09 19.54 ---78.77
09/20/10 NM NM NM
09/16/09 24.24 ---77.82
09/20/10 NM NM NM
09/20/10 19.42 ---81.20
10/27/11 19.19 ---81.43
01/07/13 20.99 ---79.63
06/23/14 18.94 ---81.68
09/20/10 19.74 ---81.01
10/27/11 19.60 ---81.15
01/07/13 21.27 ---79.48
07/29/13 20.13 ---80.62
06/23/14 19.30 ---81.45
07/06/15 18.91 ---81.84
12/04/12
98.153525-352510/15/98MW-29
MW-42 09/16/10 10 10-25 25 100.75
MW-41 09/16/10 10 10-25 25 100.62
MW-40 09/16/09 10 10-25 25 102.06
MW-39 09/16/09 10 10-25 25 98.31
10 10-25 25 99.52
MW-38 09/16/09 10 10-25 25 93.33
82.242510-2510
MW-37 09/01/09
MW-34 11/07/01 20 20-30 30 95.19
98.24
MW-33 11/07/01 20 20-30 30 98.34
03/19/01 19 19-29 29 96.73
MW-31 02/28/01 20 20-30 30
06/26/13
05/22/14
03/10/03MW-36
MW-30A
Page 5 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
09/20/10 19.15 ---79.47
10/27/11 19.27 ---79.35
01/07/13 20.55 ---78.07
07/29/13 19.85 ---78.77
06/23/14 19.09 ---79.53
07/06/15 18.58 ---80.04
07/12/17 NM NM NM Not Sampled
09/20/10 18.81 ---78.38
10/27/11 18.92 ---78.27
01/07/13 20.19 ---77.00
07/29/13 19.55 ---77.64
06/23/14 18.86 ---78.33
07/06/15 18.42 ---78.77
07/12/17 19.79 ---77.40
09/20/10 18.10 ---78.15
10/27/11 18.31 ---77.94
01/07/13 19.52 ---76.73
07/29/13 14.48 ---81.77
06/23/14 18.22 ---78.03
07/06/15 17.76 ---78.49
09/20/10 17.59 ---77.88
10/27/11 17.77 ---77.70
01/07/13 18.94 ---76.53
07/29/13 18.41 ---77.06
06/23/14 17.71 ---77.76
07/06/15 17.29 ---78.18
09/20/10 17.62 ---77.47
10/27/11 17.79 ---77.30
01/07/13 18.91 ---76.18
07/29/13 18.38 ---76.71
06/23/14 17.79 ---77.30
07/06/15 17.44 ---77.65
09/20/10 14.57 ---76.59
10/27/11 14.70 ---76.46
01/07/13 15.61 ---75.55
07/29/13 15.24 ---75.92
06/23/14 14.80 ---76.36
07/06/15 14.48 ---76.68
09/20/10 19.38 ---80.81
10/27/11 19.19 ---81.00
01/07/13 20.76 ---79.43
07/29/13 19.85 ---80.34
06/23/14 18.92 ---81.27
07/06/15 18.28 ---81.91
01/27/16 18.85 ---81.34
09/07/16 19.25 ---80.94
07/12/17 19.17 ---81.02
09/17/09 21.10 ---79.01
09/20/10 19.38 ---80.73
10/27/11 19.34 ---80.77
01/07/13 20.93 ---79.18
07/29/13 19.66 ---80.45
05/19/14 18.88 ---81.23 Pre-MMPE
05/23/14 19.21 ---80.90 Post-MMPE
06/23/14 19.06 ---81.05
06/01/15 17.75 ---82.36 Pre-MMPE
06/05/15 18.09 ---82.02 Post-MMPE
07/06/15 18.58 ---81.53
01/27/16 19.40 ---80.71
09/07/16 19.63 ---80.48
06/06/17 18.86 ---81.25 Pre-AFVR
06/06/17 19.10 ---81.01 Post-AFVR
07/12/17 19.47 ---80.64
09/20/10 18.73 ---80.49
10/27/11 18.73 ---80.49
01/07/13 NM NM NM
07/29/13 19.35 ---79.87
05/19/14 18.26 ---80.96 Pre-MMPE
05/23/14 18.45 ---80.77 Post-MMPE
06/23/14 18.43 ---80.79
07/06/15 17.93 ---81.29
01/27/16 18.83 ---80.39
09/07/16 19.03 ---80.19
07/12/17 18.87 ---80.35
MW-48 09/15/10 10 10-25 25 91.16
100.194540-45
MW-47 09/15/10 10 10-25 25 95.09
99.2225
09/15/10 10 10-25 25 96.25
95.472510-2510
2510-2510
10-251009/16/10MW-2M
MW-45
98.622510-2510
100.112510-2510
40
97.19
09/17/09MW-1M
09/15/10TW-1M
09/15/10MW-46
09/15/10MW-43
09/15/10MW-44
Page 6 of 7
Date: 07/17/17
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Top of
Casing
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
09/20/10 18.60 ---80.40
10/27/11 18.59 ---80.41
01/07/13 20.17 ---78.83
07/29/13 20.17 ---78.83
05/19/14 18.15 ---80.85 Pre-MMPE
05/23/14 18.26 ---80.74 Post-MMPE
06/23/14 18.31 ---80.69
06/01/15 17.07 ---81.93 Pre-MMPE
06/05/15 17.47 ---81.53 Post-MMPE
07/06/15 17.84 ---81.16
01/27/16 18.75 ---80.25
09/07/16 18.91 ---80.09
06/06/17 18.17 ---80.83 Pre-AFVR
06/06/17 18.33 ---80.67 Post-AFVR
07/12/17 18.73 ---80.27
11/01/07 NA 20.89 ------
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
01/07/13 NM NM NM
07/29/13 NM NM NM
06/23/14 NM NM NM
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations and well construction information for monitoring wells installed prior to 2007 reproduced from previous assessment
reports prepared by CES Engineering, P. C.
• Monitoring wells MW-9A, MW-10A, MW-15A and MW-25B were resurveyed on August 12, 2008 by GRI personnel.
• Monitoring wells MW-41 through MW-48, TW-1M, MW-1M, MW-2M and MW-3M were surveyed on September 17, 2010 by GRI personnel.
• Monitoring wells MW-1M, MW-2M, MW-3M and TW-1M were installed in order to assess UST Incident No. 31939 (Miller's Country Store).
• NM: Not Measured.
RW-1 07/22/03 10 10-30 30 100.03
99.002510-251009/16/10MW-3M
Page 7 of 7
Date: 06/19/17 Facility ID#: 0-022895
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-1M 2 ----
MW-2M 2 ----
MW-3M 2 ----
MW-22 2 ----
MW-1M 2 ----
MW-3M 2 ----
MW-22 2 ----
MW-1M 2 ----
MW-3M 2 ----
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
Gasoline
05/19/14 -
05/23/14 MMPE 13,479 --
--1,094AFVR06/06/17
TABLE 2
FREE PRODUCT RECOVERY RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Interface probe at top-of-casing
Gasoline 06/01/15 -
06/05/15 MMPE 16,317 --
Gasoline
Page 1 of 1
Date: 06/19/17
MW-1M
MW-2M
MW-3M
MW-22
MW-1M
MW-3M
MW-22
MW-1M
MW-3M
110.92 30,890 0 110.92
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
3.0284.29206.542,600.81AFVR06/06/17
16,317 ---75.68
3.02---1,094
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
1,758.92
Total Amount
of Product
Recovered
(gallons)
32.22 13,479
Amount of
Vaporized
Product
(gallons)
32.22---
94.37 352.09 75.68
Total Product Removed (in gallons)
3,604.79 136.84 391.89
Totals
Average
Effluent
Concentration
(ppm)
05/19/14 -
05/23/14 MMPE
06/01/15 -
06/05/15 MMPE
Facility ID #: 0-022895
Total To Date 31,000.92 110.92
SUMMARY OF FLUID REMOVAL
3.02
Summary Total Fluids Removed (in gallons)
Current Event 1,097.02
Page 1 of 1
Date: 06/19/17
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered (gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total liquids)
MW-1M, MW-2M,
MW-3M and MW-
22
MMPE 05/19/14 -
05/23/14 13,511.22 $11,786.11 $0.87
MW-1M, MW-3M
and MW-22 MMPE 06/01/15 -
06/05/15 16,392.68 $11,409.36 $0.70
MW-1M and MW-
3M AFVR 6/6/2017 1,097.02 $2,396.90 $2.18
31,000.92 $25,592.37 $1.25
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Comments
TOTAL (to date)
Cost per gallon for the event is based on
volume of 13,511.22 gallons of total fluids
recovered.
Cost per gallon for the event is based on
volume of 16,392.68 gallons of total fluids
recovered.
Facility ID #: 0-022895
Cost per gallon for the event is based on
volume of 1,097.02 gallons of total fluids
recovered.
Page 1 of 1
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
10/31/07 10,100 23,700 1,570 9,290 648 286 33.1 16.0 <5.00 71.6 13.0 14.1 166 988 309 39.8 NR NR NR
09/17/09 2,110 8,190 552 2,660 814 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 <44.0 313 73.9 J 10.1 2,510 2,080 2,990
09/20/10 9,050 29,400 2,100 11,000 8,740 <250 <250 <250 <120 111 J <100 <100 221 J 1,530 398 J 31.8 NR NR NR
10/27/11 14,400 39,900 2,940 14,200 3,320 391 J <100 <100 <100 133 J <110 <100 262 J 1,840 439 J NR NR NR NR
01/07/13 4,940 25,700 1,980 10,400 2,710 327 <10 <10 <10 74.1 <10 <10 195 1,390 354 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 9,320 36,700 3,200 16,300 6,320 556 20.4 J 16.8 J <10 143 19.4 J <10 362 2,800 698 NR NR NR NR
07/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/27/16 7,300 37,800 2,610 12,700 5,880 502 <63 <63 <63 103 J <63 <63 274 1,850 449 NS NS NS NS
09/07/16 10,500 56,000 3,740 19,800 5,610 1,420 <130 <130 <130 142 J <130 <130 358 J 2,270 595 NR NR NR NR
07/12/17 2,770 18,900 1,660 8,320 1,350 280 <63 <63 <63 71.5 J <63 <63 173 J 1,360 349 NR NR NR NR
10/31/07 10,600 39,000 2,420 11,300 1,870 439 37.8 <10.0 <10.0 86.0 11.2 <10.0 175 1,230 356 23.0 NR NR NR
09/17/09 5,830 28,800 2,110 10,600 660 376 <45.0 1,080 <60.0 91.6 J <50.0 <50.0 161 J 1,270 289 29.9 5,000 3,150 4,860
09/20/10 4,680 12,000 1,210 5,650 7,310 137 <50.0 <50.0 <24.0 41.3 J <20.0 <20.0 66.8 J 525 140 116 NR NR NR
10/27/11 3,940 15,000 1,170 6,410 897 149 <20 <20 <21 33.0 J <21 <20 74.8 J 634 144 NR NR NR NR
01/07/13 0.67 3.7 0.41 J 1.70 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.16 J <0.10 NR NR NR NR
07/30/13 3,130 22,300 1,620 8,970 952 265 <10 <10 <10 43.4 J <10 <10 93.2 825 179 NR NR NR NR
06/24/14 1,450 8,130 752 4,340 769 157 1.5 J 1.5 J <1.0 24.0 3.6 J <1.0 51.7 434 96.0 NR NR NR NR
07/06/15 2,290 11,100 1,420 7,930 4,540 248 <36 <35 <35 42.6 J <40 <31 98.2 J 900 208 NR NR NR NR
01/27/16 <0.13 0.16 J <0.13 <0.31 2.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 1.9 21.5 3.8 12.7 1.7 0.96 <0.13 <0.13 <0.13 0.16 J <0.13 <0.13 0.56 1.4 0.35 J NR NR NR NR
07/12/17 330 2,790 387 1,670 38.0 J 57.2 <13 <13 <13 13.6 J <13 <13 29.2 J 245 50.1 NR NR NR NR
02/28/07 15.0 <0.500 3.36 1.43 <0.500 15.5 0.880 0.870 <0.500 2.24 <0.500 0.710 1.57 2.38 <0.500 15.9 NR NR NR
10/31/07 59.1 0.930 14.6 7.97 <0.500 16.4 4.10 4.09 <0.500 11.3 <0.500 4.09 9.58 3.22 4.16 29.9 NR NR NR
09/17/09 20.1 <0.190 2.31 <0.220 <0.250 1.58 <0.180 0.970 J <0.240 2.65 <0.200 <0.200 1.39 0.883 J <0.180 7.05 106 <100 <100
09/20/10 13.7 2.15 0.606 J 1.85 J <0.500 3.61 <1.00 <1.00 <0.480 2.69 <0.400 <0.400 0.776 J 0.488 J <0.360 14.3 NR NR NR
10/27/11 8.4 0.22 J 0.89 1.1 J <0.13 1.8 <0.10 0.42 J <0.10 1.6 <0.11 <0.10 0.93 0.19 J <0.10 NR NR NR NR
01/07/13 0.74 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 1.0 <0.10 <0.10 0.55 J <0.10 <0.10 <0.10 0.14 J <0.10 0.22 J 0.11 J <0.10 0.28 J 0.36 J 0.15 J NR NR NR NR
07/06/15 2.9 <0.17 <0.15 0.62 J <0.16 0.98 0.35 J 0.59 <0.14 0.79 <0.16 <0.12 0.63 1.7 0.16 J NR NR NR NR
01/27/16 0.45 J <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-3
Contaminant of
Concern
BenzeneMW-1A
MW-2 p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
Page 1 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 1,500 45,000 9,170 53,400 309 J 2,870 1,830 <500 <240 852 J <200 <200 2,410 21,900 5,330 30.6 NR NR NR
10/27/11 1,700 33,200 6,290 33,500 2,880 1,180 201 J 120 J <100 457 J <110 <100 1,290 8,760 2,370 NR NR NR NR
01/07/13 509 19,500 4,620 24,300 737 960 58.1 43.7 J <10 249 <10 22.7 J 761 4,610 1,340 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 894 19,200 4,580 27,300 1,170 858 471 269 <2.5 725 7.6 J 144 920 6,200 1,730 NR NR NR NR
07/06/15 381 14,200 4,810 28,600 620 1,440 98.9 J 59.1 J <35 264 <40 34.7 J 763 7,110 1,890 NR NR NR NR
01/27/16 349 24,200 12,200 68,400 1,810 3,360 879 465 <63 1,170 <63 240 J 4,190 22,100 7,640 NR NR NR NR
09/07/16 146 J 13,000 5,710 35,100 184 J 1,500 260 159 J <63 388 <63 66.9 J 1,320 9,470 2,940 NR NR NR NR
07/12/17 118 6,410 3,580 19,400 143 830 29.3 J <25 <25 172 <25 <25 477 3,920 1,040 NR NR NR NR
10/31/07 1,120 5,620 1,490 4,130 <5.00 283 36.3 17.0 <5.00 82.5 <5.00 20.2 141 682 287 16.0 NR NR NR
09/17/09 274 2,280 666 1,810 <10.0 168 <7.20 <5.60 <9.60 58.6 <8.00 <8.00 64.8 392 124 12.9 2,770 2,250 1,480
09/20/10 568 1,780 630 2,340 <5.00 95.9 40.7 <10.0 11.5 J 38.0 <4.00 <4.00 52.1 539 160 19.6 NR NR NR
10/27/11 130 456 267 617 <0.13 47.9 3.2 2.4 1.8 26.0 <0.11 3.3 34.0 108 32.8 NR NR NR NR
01/07/13 590 4,770 1,400 5,120 <1.0 391 9.0 8.8 4.9 J 80.0 <1.0 11.9 132 804 248 NR NR NR NR
07/30/13 69.0 705 485 1,670 <2.0 216 6.1 J 5.8 J <2.0 40.2 <2.0 8.0 J 70.3 314 121 NR NR NR NR
06/24/14 14.8 38.1 12.3 79.1 <0.10 8.7 0.29 J 0.26 J 0.30 J 1.8 <0.10 0.39 J 2.2 9.2 4.1 NR NR NR NR
07/06/15 5.3 40.7 9.2 38.4 <0.16 2.0 <0.14 <0.14 <0.14 0.55 <0.16 <0.12 0.86 3.4 1.3 NR NR NR NR
01/27/16 185 1,690 631 2,060 <3.1 187 5.4 J 4.8 J <3.1 40.6 <3.1 6.0 J 63.2 336 111 NR NR NR NR
07/12/17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 2.72 3.43 <0.500 1.17 6.10 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 NR NR NR
09/17/09 0.627 J 0.602 J <0.150 <0.220 0.868 J <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.200 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.700 2.84 J 1.23 J 2.21 J <1.25 <2.50 <2.50 <2.50 <1.20 <0.750 <1.00 <1.00 <1.10 0.756 J <0.900 6.89 NR NR NR
10/27/11 <0.13 0.52 <0.15 0.56 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.38 J 0.46 J <0.10 0.21 J 0.59 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 36.9 <0.500 14.6 <1.00 <0.500 6.30 1.63 2.71 <0.500 7.20 1.53 3.14 6.78 <0.500 <0.500 <5.00 NR NR NR
09/17/09 10.3 0.366 J 179 3.61 <0.250 58.7 <0.180 7.46 <0.240 57.3 1.75 0.588 J 93.3 2.06 0.795 J <1.50 758 489 481
09/20/10 1.91 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 0.485 J <0.200 <0.200 <0.220 <0.150 <0.180 25.0 NR NR NR
10/27/11 3.7 0.30 J <0.15 <0.30 <0.13 0.53 <0.10 0.41 J <0.10 0.77 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 19.1 <0.10 13.1 <0.22 0.33 J 3.0 1.3 2.9 <0.10 12.5 0.90 1.5 19.2 <0.10 <0.10 NR NR NR NR
07/30/13 7.3 <0.10 7.0 <0.22 0.43 J 1.5 0.46 J 0.78 <0.10 4.7 0.78 0.34 J 7.2 <0.10 <0.10 NR NR NR NR
06/24/14 0.16 J <0.10 0.15 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.13 J <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-7
MW-4
MW-5
MWD-6
Page 2 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 0.930 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.79 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 11.3 <100 <100 <100
09/20/10 0.284 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.1 NR NR NR
10/27/11 0.55 0.23 J <0.15 0.46 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 2.9 <0.10 <0.10 <0.22 0.11 J <0.15 <0.10 0.13 J <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 7.29 <100 <100 <100
09/20/10 0.475 J 2.95 0.384 J 1.90 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 0.503 J <0.180 27.9 NR NR NR
10/27/11 <0.13 0.14 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.11 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
10/31/07 617 191 366 652 52.0 132 9.58 4.13 <0.500 28.5 0.640 5.68 43.6 199 81.9 7.17 NR NR NR
09/17/09 1,560 3,120 687 1,920 43.6 J 208 <18.0 <14.0 <24.0 53.3 J <20.0 <20.0 52.5 J 316 88.1 J 12.5 3,150 1,430 1,870
09/20/10 29.2 1.68 0.400 J 13.3 11.1 3.56 <0.500 <0.500 <0.240 1.53 <0.200 <0.200 0.304 J 5.78 <0.180 25.6 NR NR NR
10/27/11 3.4 <0.13 <0.15 <0.30 1.2 0.37 J <0.10 <0.10 <0.10 0.11 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 324 E 97.6 114 188.9 121 44.3 1.2 1.5 0.38 J 12.3 0.83 1.6 18.7 55.5 11.3 NR NR NR NR
07/30/13 276 194 66.4 249 98.8 36.9 0.89 0.97 0.30 J 8.6 0.61 1.1 12.7 39.6 7.7 NR NR NR NR
06/24/14 152 20.5 11.5 89.9 29.3 21.9 0.40 J 0.37 J 0.29 J 3.2 <0.10 0.65 3.6 14.9 1.9 NR NR NR NR
07/06/15 33.8 0.38 J 6.5 12.8 7.6 16.0 0.28 J 0.25 J <0.14 1.7 <0.16 0.55 2.2 4.4 <0.14 NR NR NR NR
01/27/16 225 310 144 467 6.7 68.1 1.4 J <1.3 <1.3 11.0 <1.3 2.1 J 15.8 98.9 23.2 NR NR NR NR
09/07/16 27.7 29.5 16.8 32.3 0.25 J 7.1 <0.13 <0.13 <0.13 1.1 <0.13 <0.13 1.5 3.7 0.73 NR NR NR NR
07/12/17 32.8 1.1 4.3 19.4 0.93 24.3 0.41 J 0.57 <0.13 4.7 <0.13 0.58 1.7 6.1 <0.13 NR NR NR NR
11/01/07 8,470 20,300 2,100 8,390 9,250 449 27.3 8.19 <0.500 76.3 46.0 6.75 154 1,280 420 18.8 NR NR NR
09/17/09 2,560 8,380 778 2,500 330 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 88.1 J 552 141 J 3.22 2,630 1,700 2,360
09/20/10 1,500 517 260 764 845 76.3 7.59 J <5.00 <2.40 17.7 <2.00 <2.00 32.3 174 65.7 74.5 NR NR NR
10/27/11 3,120 9,080 895 4,130 2,990 128 <20 <20 <21 35.1 J <21 <20 83.9 J 613 160 NR NR NR NR
01/07/13 4,010 15,500 1,400 6,790 1,790 235 <10 <10 <10 52.3 <10 <10 146 1,080 241 NR NR NR NR
07/30/13 1,640 6,850 785 3,230 1,140 152 <25 <25 <25 32.5 J <25 <25 89.0 J 503 126 J NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/07/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/12/17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-9A
MW-10A
MW-11
MW-12
Page 3 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 12.9 <0.500 2.65 <1.00 <0.500 <5.00 <0.500 2.06 <0.500 2.57 <0.500 <0.500 2.69 <0.500 <0.500 45.0 NR NR NR
09/17/09 8.77 <0.190 43.7 <0.220 <0.250 3.50 <0.180 3.19 <0.240 20.3 <0.200 0.454 J 26.4 <0.150 0.624 J 12.1 246 179 183
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 42.1 NR NR NR
10/27/11 0.15 J 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 1.2 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 0.20 J <0.10 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.83 0.14 J <0.10 <0.22 <0.10 <0.15 <0.10 0.11 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 199 2.45 88.3 101 14.8 63.7 8.79 4.09 <0.500 26.8 <0.500 6.02 20.5 104 36.3 47.6 NR NR NR
10/31/07 212 11.4 280 185 8.98 144 17.4 6.66 <0.500 46.8 <0.500 10.2 54.8 87.4 90.8 12.4 NR NR NR
09/17/09 153 193 261 200 3.32 J 143 <1.80 <1.40 <2.40 22.5 <2.00 <2.00 20.7 62.4 21.5 13.6 1,100 504 506
09/20/10 64.5 6.39 68.7 41.7 <0.250 66.9 2.58 1.94 <0.240 16.6 <0.200 0.391 J 12.3 24.4 0.665 J 50.2 NR NR NR
10/27/11 183 5.0 148 12.2 12.3 78.6 2.7 3.8 <0.52 32.0 <0.54 3.5 23.3 5.0 0.66 J NR NR NR NR
01/07/13 144 170 228 237.8 9.5 135 3.2 3.4 <0.50 26.5 <0.50 2.8 25.6 50.2 10.5 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/06/15 0.89 0.34 J 2.3 2.1 0.20 J 1.5 <0.14 <0.14 <0.14 0.24 J <0.16 <0.12 0.29 J 0.51 0.16 J NR NR NR NR
06/24/14 38.8 282 213 1,120 <0.10 120 4.9 4.3 <0.10 24.8 <0.10 7.2 31.5 224 74.6 NS NS NS NS
01/27/16 114 535 638 1,840 <3.1 250 9.5 J 8.5 J <3.1 64.4 <3.1 11.7 J 95.3 398 177 NS NS NS NS
07/12/17 143 743 670 2,040 <3.1 230 9.3 J 9.1 J <3.1 69.6 <3.1 12.6 J 113 427 176 NR NR NR NR
11/01/07 358 1,690 1,320 3,240 <0.500 358 36.4 12.0 <0.500 81.5 <0.500 17.1 116 721 333 56.4 NR NR NR
09/17/09 78.6 1,030 513 1,680 <5.00 170 <3.60 <2.80 <4.80 45.4 <4.00 <4.00 44.3 360 112 9.16 2,640 1,100 1,460
09/20/10 551 756 542 1,570 <50.0 343 J <36.0 <28.0 <48.0 576 <40.0 <40.0 413 482 313 64.5 NR NR NR
10/27/11 151 534 458 1,230 <2.6 150 7.1 J 5.5 J <2.1 44.5 <2.1 8.0 J 64.9 287 130 NR NR NR NR
01/07/13 59.0 477 353 885 <2.0 125 5.3 J 5.5 J <2.0 35.9 <2.0 5.1 J 50.7 172 101 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 55.2 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.79 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.83 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 15.5 NR NR NR
10/27/11 <0.13 0.22 J <0.15 0.36 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-14
MW-15
MW-15A
MW-17
MW-13
Page 4 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 6.58 1.13 10.5 3.33 4.88 25.9 6.63 4.30 <0.500 13.2 0.630 2.50 7.16 2.52 <0.500 45.3 NR NR NR
09/17/09 <0.140 <0.190 37.7 22.6 <0.250 66.2 <0.180 3.38 <0.240 34.8 <0.200 <0.200 41.2 116 47.4 14.6 243 394 505
09/20/10 0.917 J <0.190 <0.150 0.270 J 1.51 1.64 2.65 1.35 <0.240 1.15 <0.200 <0.200 <0.220 <0.150 <0.180 49.2 NR NR NR
10/27/11 <0.13 0.24 J <0.15 0.56 J <0.13 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.23 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 7.5 12.5 0.12 J 40.4 2.4 2.6 <0.10 16.7 <0.10 0.87 10.4 47.0 1.0 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.5 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.32 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.3 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 30.6 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.69 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.4 NR NR NR
09/17/09 11.1 0.398 J 1.69 11.3 <0.250 <0.500 <0.180 <0.140 <0.240 0.773 J <0.200 <0.200 0.749 J 3.69 1.81 5.70 429 105 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 1.20 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 8.09 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
02/28/07 291 387 345 1,020 34.5 35.3 19.1 6.00 <0.500 33.2 29.4 4.95 75.2 523 115 18.1 NR NR NR
10/31/07 95.7 1,020 795 2,820 <2.50 155 46.4 16.6 <2.50 79.4 <2.50 13.4 224 1,190 373 <5.00 NR NR NR
09/17/09 78.9 J 2,270 1,900 8,570 <50.0 324 <36.0 <28.0 <48.0 156 J <40.0 <40.0 305 2,430 558 3.75 4,900 5,980 393,000
09/20/10 158 58.2 188 156 16.9 20.8 24.0 15.9 <2.40 30.9 30.5 <2.00 60.6 288 53.9 37.2 NR NR NR
10/27/11 69.3 301 487 1,730 <2.6 78.9 16.6 12.7 <2.1 61.0 4.2 J 9.4 J 190 955 267 NR NR NR NR
01/07/13 90.4 261 1,180 4,820 29.5 240 27.3 24.5 <2.0 172 12.4 16.0 542 3,480 828 NR NR NR NR
07/30/13 91.0 199 648 2,480 9.7 J 115 27.0 22.5 J <5.0 99.2 12.5 J 15.6 J 382 1,680 486 NR NR NR NR
06/23/14 8.6 5.3 34.6 111 <0.10 6.4 4.2 3.3 <0.10 8.5 0.73 2.6 28.5 67.8 20.7 NR NR NR NR
07/06/15 12.6 17.4 97.2 379 <0.82 20.3 7.1 4.9 <0.71 13.1 <0.80 3.7 46.3 211 60.0 NR NR NR NR
01/27/16 37.2 82.2 445 1,710 <3.1 106 22.2 16.4 <3.1 47.2 <3.1 12.0 J 159 878 218 NR NR NR NR
07/12/17 6.0 13.2 152 422 <1.3 38.5 3.6 J 3.5 J <1.3 21.5 <1.3 2.0 J 61.0 337 65.2 NR NR NR NR
MW-21
MW-22
MW-19
MW-20
Page 5 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
02/28/07 7.39 <0.500 4.73 7.21 <0.500 <5.00 <0.500 0.590 <0.500 1.88 <0.500 0.990 2.42 17.4 2.49 16.2 NR NR NR
10/31/07 3.32 <0.500 1.98 2.58 <0.500 <5.00 <0.500 <0.500 <0.500 1.53 <0.500 <0.500 0.810 6.75 1.27 16.4 NR NR NR
09/17/09 3.86 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 0.792 J <0.200 <0.200 0.387 J 3.64 <0.180 18.7 <100 <100 <100
09/20/10 14.2 0.242 J 2.39 9.05 <0.250 6.07 2.53 3.44 <0.240 6.40 <0.200 0.580 J 1.64 20.4 1.69 20.9 NR NR NR
10/27/11 7.0 0.22 J 3.7 3.1 <0.13 2.3 <0.10 0.61 <0.10 2.0 <0.11 0.95 1.8 6.8 <0.10 NR NR NR NR
01/07/13 1.7 <0.10 <0.10 0.28 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.96 <0.10 NR NR NR NR
07/30/13 12.3 0.15 J 4.1 5.5 <0.10 3.5 <0.10 1.4 <0.10 3.6 0.16 J 1.8 4.4 15.8 <0.10 NR NR NR NR
06/24/14 7.4 <0.10 3.1 3.0 <0.10 2.3 <0.10 0.83 <0.10 2.1 <0.10 1.1 2.4 8.6 0.14 J NR NR NR NR
07/06/15 22.0 0.47 J 11.7 19.8 <0.16 12.7 0.14 J 1.4 <0.14 4.7 <0.16 2.6 5.0 36.5 1.0 NR NR NR NR
01/27/16 1.1 <0.13 0.21 J <0.31 <0.13 0.46 J <0.13 <0.13 <0.13 0.18 J <0.13 <0.13 0.19 J 0.19 J <0.13 NR NR NR NR
07/12/17 0.15 J <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.1 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 4.67 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 61.5 95.7 46.1 75.8 5.64 12.2 2.94 2.03 <0.500 3.77 5.95 <0.500 7.17 20.6 7.97 32.3 NR NR NR
09/17/09 11.5 <0.190 <0.150 <0.220 10.7 5.35 <0.180 <0.140 <0.240 0.515 J 12.7 <0.200 <0.220 <0.150 <0.180 8.33 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 26.8 NR NR NR
10/27/11 <0.13 0.15 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.49 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 4,210 2,780 1,120 2,200 2,350 1,690 12.8 4.70 3.71 53.9 11.0 3.30 96.9 594 143 6.94 NR NR NR
11/01/07 4,130 2,880 1,150 2,220 1,720 190 14.9 6.23 1.65 47.7 9.05 4.76 89.0 509 139 21.6 NR NR NR
09/17/09 3,910 6,350 952 2,950 1,730 172 <18.0 <14.0 <24.0 50.3 J <20.0 <20.0 75.4 J 424 117 4.19 1,950 1,670 83,000
09/20/10 25.1 <0.190 0.827 J <0.220 96.2 0.957 J <0.500 <0.500 <0.240 0.313 J <0.200 <0.200 <0.220 <0.150 <0.180 45.3 NR NR NR
10/27/11 4.1 0.22 J 0.54 <0.30 4.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 257 102 77.0 149.9 147 13.3 <1.0 <1.0 <1.0 4.7 J <1.0 <1.0 10.3 47.7 9.2 NR NR NR NR
07/30/13 180 173 40.7 120 188 7.3 <0.10 0.15 J <0.10 2.1 0.44 J <0.10 3.3 10.1 2.2 NR NR NR NR
06/23/14 14.6 1.6 1.5 4.7 86.5 0.46 J <0.10 <0.10 <0.10 0.15 J 0.13 J <0.10 0.13 J 0.73 <0.10 NR NR NR NR
07/06/15 2.4 <0.17 0.22 J <0.43 12.1 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 9.0 8.3 1.6 5.9 26.4 0.50 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.51 <0.13 NR NR NR NR
09/07/16 0.31 J <0.13 <0.13 <0.31 5.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/12/17 <0.13 0.25 J <0.13 1.2 J 4.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-23A
MW-24
MW-25B
MW-26
Page 6 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
02/28/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 2.81 <0.500 <0.500 <0.500 <0.500 9.40 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.6 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 692 90.3 93.4 81.7 120 15.4 3.91 2.96 <0.500 28.0 1.04 1.25 15.0 16.7 5.44 6.88 NR NR NR
11/01/07 3,810 2,110 788 1,580 1,370 148 13.7 6.32 <0.500 40.9 9.59 5.45 67.8 364 92.0 40.5 NR NR NR
09/17/09 2,860 5,780 696 2,320 869 127 <18.0 <14.0 <24.0 37.8 J <20.0 <20.0 61.2 J 370 91.5 J <1.50 1,690 1,280 1,800
09/20/10 1,140 939 266 636 402 <100 <18.0 <14.0 <24.0 28.8 J <20.0 <20.0 37.3 J 156 36.4 J 13.4 NR NR NR
10/28/11 2,130 1,340 487 762 1,060 80.2 6.4 J <5.1 <5.2 32.1 5.9 J <5.0 50.0 236 25.9 NR NR NR NR
01/07/13 2,110 6,130 731 3,300 1,110 150 <5.0 <5.0 <5.0 31.2 <5.0 <5.0 74.5 551 138 NR NR NR NR
07/30/13 1,420 3,280 438 1,590 858 78.8 <10 <10 <10 20.2 J <10 <10 43.0 J 289 69.7 NR NR NR NR
06/23/14 508 2,480 268 1,070 319 67.2 2.6 2.2 <0.10 19.9 1.4 1.4 38.7 206 42.7 NR NR NR NR
07/06/15 525 1,780 317 1,290 157 90.1 <7.2 <6.9 <7.1 21.4 J <8.0 <6.1 35.0 270 65.7 NR NR NR NR
01/27/16 550 1,370 337 1,380 138 106 <3.1 <3.1 <3.1 20.7 <3.1 <3.1 33.0 315 70.5 NR NR NR NR
09/07/16 647 1,330 408 1,920 317 93.4 <6.3 <6.3 <6.3 25.0 <6.3 <6.3 39.5 309 79.9 NR NR NR NR
07/12/17 1,040 606 528 2,080 676 132 4.1 J 4.8 J <3.1 35.9 <3.1 3.4 J 56.9 419 102 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 218 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 28.4 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.2 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0500 <0.500 <0.500 90.3 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 13.9 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 27.6 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-27
MW-28
MW-29
MW-30A
MW-31
Page 7 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 91.1 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 97.3 <0.500 <0.500 <1.00 50.9 <5.00 <0.500 <0.500 <0.500 1.13 <0.500 <0.500 <0.500 <0.500 <0.500 58.8 NR NR NR
11/01/07 146 <0.500 <0.500 <1.00 60.8 <5.00 <0.500 <0.500 <0.500 2.00 <0.500 <0.500 <0.500 <0.500 <0.500 165 NR NR NR
09/17/09 102 <0.190 <0.150 <0.220 32.2 <0.500 <0.180 <0.140 <0.240 1.10 <0.200 <0.200 <0.220 <0.150 0.525 J 12.5 <100 <100 <100
09/20/10 72.4 0.908 J 4.77 4.41 78.0 4.60 0.382 J 0.303 J <0.480 2.50 <0.400 <0.400 1.21 J <0.300 <0.360 40.4 NR NR NR
10/28/11 0.13 J 0.15 J <0.15 <0.30 1.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 11.7 J <10 <10 <22 451 <15 <10 <10 <10 <10 <10 <10 <10 <10 <10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 3.9 <0.17 0.17 J <0.43 5.1 0.45 J <0.14 <0.14 <0.14 0.17 J <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 0.32 J 0.25 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 1.5 <0.13 <0.13 <0.13 <0.13 <0.13 0.43 J <0.13 <0.13 <0.13 <0.13 NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.4 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.75 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.410 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 24.6 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/12/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 20.3 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 <0.190 <0.150 <0.220 3.07 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 39.4 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.794 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 77.4 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-34
MW-36
MW-37
MW-38
MW-33
Page 8 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 25.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 1.82 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.0 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 0.327 J <0.180 100 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/20/10 6.54 1.30 17.4 77.1 <0.250 1.43 J 3.24 0.680 J <0.240 1.85 <0.200 <0.200 4.04 25.8 9.18 80.2 1,450 431 665
10/27/11 10.7 1.3 1.5 11.0 0.15 J 0.12 J 0.14 J <0.10 <0.10 0.21 J <0.11 <0.10 0.29 J 1.6 2.1 NR NR NR NR
01/07/13 18.1 3.1 10.7 39.9 <0.10 <0.15 0.15 J 0.18 J <0.10 1.1 <0.10 0.12 J 2.0 7.7 5.1 NR NR NR NR
07/29/13 5.6 0.31 J 0.27 J 3.5 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.41 J 1.1 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 78.5 <100 <100 <100
10/27/11 <0.13 0.19 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.11 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/12/17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 20.4 0.447 J 4.18 1.01 8.18 <1.00 <0.180 <0.140 <0.240 1.11 <0.200 <0.200 0.961 J <0.150 <0.180 104 <100 <100 <100
10/28/11 11.4 0.22 J <0.15 0.36 J 4.8 <0.10 <0.10 <0.10 <0.10 0.24 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 5.3 <0.10 0.11 J <0.22 4.6 <0.15 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 46.7 0.25 J 2.7 <0.22 11.9 <0.15 0.13 J 0.13 J <0.10 1.1 <0.10 <0.10 0.60 <0.10 <0.10 NR NR NR NR
06/23/14 1.2 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/12/17 0.27 J <0.13 <0.13 <0.25 12.3 <0.13 <0.13 <0.13 <0.13 0.21 J <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-42
MW-43
MW-44
MW-39
MW-40
MW-41
Page 9 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 229 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 1.17 <0.190 <0.150 0.276 J 1.99 <1.00 <0.180 <0.140 <0.240 0.415 J 2.32 <0.200 <0.220 <0.150 <0.180 106 <100 <100 <100
10/28/11 <0.13 0.14 J <0.15 0.48 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.17 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.17 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.25 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.40 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 26.6 <0.190 <0.150 <0.220 12.0 <1.00 0.201 J 0.177 J <0.240 1.43 <0.200 <0.200 <0.220 <0.150 <0.180 116 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 101 <0.50 <0.50 <1.08 11.0 <0.74 <0.50 <0.50 <0.50 1.8 J <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR
07/30/13 12.9 <0.10 <0.10 <0.22 1.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 0.502 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 49.9 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.96 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.18 J <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 9.6 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 4.95 4.15 4.89 18.1 <0.500 <2.00 2.10 <0.280 <0.480 5.78 <0.400 <0.400 4.07 2.60 2.52 3.41 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <3.4 570 <3.0 <8.6 <3.3 <2.4 <2.9 <2.8 <2.8 <2.4 <3.2 <2.4 <3.1 <2.7 <2.7 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 47.9 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/12/17 <3.1 3,190 <3.1 <6.3 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 <3.1 NR NR NR NR
MW-48
MW-45
MW-46
MW-47
TW-1M
Page 10 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/17/09 1,310 36,100 4,070 22,700 211 J 1,060 <90.0 4,200 <120 265 J <100 642 642 4,900 1,170 4.26 12,200 10,700 15,500
09/20/10 1,130 11,900 1,410 6,210 <100 1,640 608 <56.0 <96.0 1,150 792 <80.0 896 2,850 964 45.3 NR NR NR
10/27/11 1,460 24,100 3,970 22,300 244 J 1,000 <100 <100 <100 263 J 226 J <100 763 5,320 1,430 NR NR NR NR
01/07/13 528 16,300 3,830 21,920 45.6 1,000 50.6 27.8 <5.0 186 73.1 18.5 J 589 4,520 1,090 NR NR NR NR
07/30/13 982 23,500 3,030 15,600 208 J 523 <50 <50 <50 110 J 220 J <50 344 2,400 582 NR NR NR NR
06/24/14 1,210 10,600 2,990 21,600 273 1,930 240 128 J <25 296 491 90.4 J 1,140 11,100 3,000 NR NR NR NR
07/06/15 975 17,100 3,150 20,300 <82 1,100 <72 <69 <71 140 J <80 <61 427 4,270 1,040 NR NR NR NR
01/27/16 466 15,200 3,460 22,000 <25 2,280 421 166 <25 373 <25 113 1,400 12,600 3,340 NR NR NR NR
09/07/16 716 22,000 5,560 36,000 <63 2,350 370 167 J <63 415 <63 90.4 J 1,530 12,000 3,570 NR NR NR NR
07/12/17 256 10,500 1,390 9,380 <25 366 <25 <25 <25 49.6 J <25 <25 123 1,550 350 NR NR NR NR
09/20/10 5.49 4.12 4.89 17.7 3.04 2.27 J 15.7 <0.280 <0.480 5.70 3.73 <0.400 4.07 5.24 6.11 33.2 496 <100 380
10/27/11 <0.13 0.37 J 0.26 J 1.4 J <0.13 0.24 J 6.9 2.6 <0.10 1.6 <0.11 0.59 0.13 J 0.95 3.2 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/30/13 <0.10 0.16 J 0.85 1.9 <0.10 0.99 5.8 2.7 <0.10 2.2 <0.10 0.81 0.27 J 5.9 9.6 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.34 J 0.91 0.40 J <0.10 <0.10 <0.10 0.25 J <0.10 0.32 J 0.34 J NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 2.5 0.92 <0.14 <0.12 <0.16 0.50 <0.16 <0.14 0.34 J NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 2.8 0.84 <0.13 <0.13 <0.13 0.27 J <0.13 <0.13 0.35 J NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 5.8 1.9 <0.13 <0.13 <0.13 0.26 J <0.13 <0.13 0.45 J NR NR NR NR
07/12/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.40 J 3.8 1.1 <0.13 <0.13 <0.13 0.18 J <0.13 <0.13 0.20 J NR NR NR NR
09/20/10 1,090 4,890 1,020 3,150 159 J 601 J 439 <56.0 <96.0 1,150 641 <80.0 829 1,030 606 28.8 25,900 5,280 16,900
10/27/11 1,430 12,300 1,610 6,600 158 352 <25 <26 <26 91.4 J 116 J <25 207 1,360 363 NR NR NR NR
01/07/13 1,120 13,500 1,670 7,150 54.8 312 <10 <10 <10 64.6 131 <10 192 1,390 319 NR NR NR NR
07/30/13 472 6,790 1,080 4,000 <25 171 <25 <25 <25 45.6 J 54.3 J <25 131 811 195 NR NR NR NR
06/24/14 161 2,150 288 1,290 12.6 J 37.2 <5.0 <5.0 <5.0 13.3 J 18.9 J <5.0 29.4 276 78.1 NR NR NR NR
07/06/15 220 4,690 564 2,660 <33 98.1 J <29 <28 <28 25.9 J <32 <24 65.3 J 503 134 NR NR NR NR
01/27/16 659 16,600 1,690 7,720 <25 425 <25 <25 <25 72.4 J 60.0 J <25 203 1,430 340 NR NR NR NR
09/07/16 524 17,500 1,970 9,400 <63 334 <63 <63 <63 82.1 J 81.3 J <63 220 J 1,330 363 NR NR NR NR
07/12/17 286 13,000 1,250 5,860 <31 222 <31 <31 <31 45.2 J <31 <31 131 1,040 234 NR NR NR NR
11/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.45 NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
WSW-5
MW-1M
MW-2M
MW-3M
Page 11 of 12
Date : 07/25/17
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Contaminant of
Concern
Benzenep-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneIPENaphthalenen-ButylbenzeneC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)TolueneEthylbenzeneXylenesMTBELeadC5-C8 Aliphaticssec-Butylbenzene1,2-Dibromoethane TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 0.189 J <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.44 J NR NR NR
10/28/11 <0.13 0.14 J <0.15 <0.30 <0.13 0.11 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/12/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• Other reported compounds that exceeded the MACs: 07/12/17: Styrene in MW-1M and MW-3M
WSW-18
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
WSW-13
Page 12 of 12

APPENDICES

APPENDIX A
MMPE Data, Calculations and Disposal Manifest
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET
Site Name :Miller's Country Store
Incident Number :31939
Average Depth to Ground Water :18.52 ft
Well Name:MW-1M and MW-3M Inner Dia. of Well (inches):2
Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg) :680 cfm @ 18" of Hg
Diameter of Exhaust Stack (inches) :6
Start Time :6:30 Date :06/06/17
End Time :14:30
Note: Take all the readings listed below every 15 minutes for the first 2 hours of the test and every
30 minutes thereafter.
Test Conducted By (AFVR Contractor):Greenwood Applied Services, LLC
Test Supervised By (Consultant):Geological Resources, Inc.
Frequency Time Vacuum Exhaust Velocity Temperature Rel. Humidity OVA
(min)(in. of Hg)(ft/min)(°F)(%)(ppm)
0 6:30 25 2,376 101.0 60.0 114.0
15 6:45 25 1,471 140.1 40.3 132.6
30 7:00 25 2,604 180.1 29.9 115.5
45 7:15 25 2,896 214.0 19.1 84.7
60 7:30 25 2,872 212.1 9.9 83.6
75 7:45 25 3,140 213.8 9.1 82.5
90 8:00 25 3,138 215.8 8.5 83.7
105 8:15 25 2,868 217.4 8.0 85.9
120 8:30 25 2,867 218.9 7.2 88.3
150 9:00 25 3,031 216.0 7.9 79.1
180 9:30 25 2,891 217.3 7.7 80.6
210 10:00 25 3,093 215.1 7.9 60.9
240 10:30 25 2,481 209.8 8.7 58.1
270 11:00 25 2,888 216.5 7.1 73.2
300 11:30 25 2,976 220.9 6.8 82.6
330 12:00 25 2,608 220.7 6.8 81.2
360 12:30 25 1,060 227.3 5.0 78.7
390 13:00 25 2,957 221.6 6.0 78.5
420 13:30 25 2,731 223.2 5.7 78.4
450 14:00 25 2,160 224.7 5.0 74.3
480 14:30 25 1,509 211.1 5.9 73.6
Total Fluids Recovered (in gallons) :1,094
Total Product Recovered (in gallons) :0
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET (Cont'd.)
Site Name :Miller's Country Store
Incident Number :31939
Well Name:MW-1M and MW-3M Inner Dia. of Well (inches):2
Start Time :6:30 Date :6/6/2017
End Time :14:30
Note: Record water levels in Vacuum Well at start and end of Test. Record Water Levels in a few
Observation Wells periodically (hourly during event) and at end of event.
Test Conducted By (AFVR Contractor):Greenwood Applied Services
Test Supervised By (Consultant):Geological Resources, Inc.
Parameters AFVR Well AFVR Well Obs. Well 1 Obs. Well 2 Obs. Well 3
Well Name MW-1M MW-3M
Diameter (in.)2 2
Distance from
AFVR Well (ft)
Depth to Water Measurements (in feet)
Frequency Time MW-1A MW-4
(min)
(Vac. Well)
(ft.)
(Vac. Well)
(ft.)(Obs. Well)(Obs. Well)(Obs. Well)
0 (Before Start)6:30 18.86 18.17
60 7:30 ------
120 8:30 ------
180 9:30 ------
240 10:30 ------
300 11:30 ------
360 12:30 ------
420 13:30 ------
480 14:30 ------
End of Event 14:35 19.10 18.33
00
AGGRESSIVE FLUID VAPOR RECOVERY EVENT
SITE NAME:Miller's Country Store Date: 06/06/17
INCIDENT NUMBER:31939
AVERAGE DEPTH TO GROUNDWATER:18.52 ft.
DESCRIBE SOIL IN THE SATURATED ZONE:
INDICATE AVERAGE HYDRAULIC CONDUCTIVITY unknown
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR AFVR:MW-1M and MW-3M
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg):680 cfm @ 18 in./Hg
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Rel Humid Water Qstd
(inches of Hg)(ft/min)(in)(°F)(%)Vapor (%)(flow)
06/06/17 6:30 25 2,376 6 101.0 60.0 0.0259 428
06/06/17 6:45 25 1,471 6 140.1 40.3 0.0537 240
06/06/17 7:00 25 2,604 6 180.1 29.9 0.1126 374
06/06/17 7:15 25 2,896 6 214.0 19.1 0.1544 377
06/06/17 7:30 25 2,872 6 212.1 9.9 0.0686 413
06/06/17 7:45 25 3,140 6 213.8 9.1 0.0648 452
06/06/17 8:00 25 3,138 6 215.8 8.5 0.0628 451
06/06/17 8:15 25 2,868 6 217.4 8.0 0.0608 412
06/06/17 8:30 25 2,867 6 218.9 7.2 0.0559 413
06/06/17 9:00 25 3,031 6 216.0 7.9 0.0582 438
06/06/17 9:30 25 2,891 6 217.3 7.7 0.0582 417
06/06/17 10:00 25 3,093 6 215.1 7.9 0.0571 448
06/06/17 10:30 25 2,481 6 209.8 8.7 0.0566 362
06/06/17 11:00 25 2,888 6 216.5 7.1 0.0524 419
06/06/17 11:30 25 2,976 6 220.9 6.8 0.0548 428
06/06/17 12:00 25 2,608 6 220.7 6.8 0.0546 376
06/06/17 12:30 25 1,060 6 227.3 5.0 0.0449 153
06/06/17 13:00 25 2,957 6 221.6 6.0 0.0486 428
06/06/17 13:30 25 2,731 6 223.2 5.7 0.0475 395
06/06/17 14:00 25 2,160 6 224.7 5.0 0.0426 313
06/06/17 14:30 25 1,509 6 211.1 5.9 0.0383 224
Averages NA 25.00 2,600.81 6.00 206.54 12.98 0.06063 379.09
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart
(temp Vs relative humidity)
EQUATION
Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)^2) * (528°R/(Temp + 460))
Date Time
EMISSION CALCULATIONS
0 428 114.0 4 456.0 2,425 0.000151388 3.89 0.00
15 240 132.6 4 530.4 2,821 0.000176088 2.54 0.64
30 374 115.5 4 462.0 2,457 0.000153380 3.44 0.86
45 377 84.7 4 338.8 1,801.68 0.000112479 2.54 0.64
60 413 83.6 4 334.4 1,778.28 0.000111018 2.75 0.69
75 452 82.5 4 330.0 1,754.88 0.000109557 2.97 0.74
90 451 83.7 4 334.8 1,780.41 0.000111151 3.01 0.75
105 412 85.9 4 343.6 1,827.20 0.000114072 2.82 0.71
120 413 88.3 4 353.2 1,878.26 0.000117259 2.91 0.73
150 438 79.1 4 316.4 1,682.56 0.000105042 2.76 1.38
180 417 80.6 4 322.4 1,714.47 0.000107034 2.68 1.34
210 448 60.9 4 243.6 1295.42 0.000080873 2.17 1.09
240 362 58.1 4 232.4 1235.86 0.000077155 1.68 0.84
270 419 73.2 4 292.8 1557.06 0.000097207 2.45 1.22
300 428 82.6 4 330.4 1757.01 0.000109690 2.82 1.41
330 376 81.2 4 324.8 1727.23 0.000107831 2.43 1.21
360 153 78.7 4 314.8 1674.05 0.000104511 0.96 0.48
390 428 78.5 4 314.0 1669.80 0.000104245 2.68 1.34
420 395 78.4 4 313.6 1667.67 0.000104113 2.47 1.23
450 313 74.3 4 297.2 1580.46 0.000098668 1.85 0.93
480 224 73.6 4 294.4 1565.57 0.000097738 1.31 0.66
Averages 379.09 84.29 4.00 337.14 1,792.87 0.000111929 2.53 0.90
Total emissions in pounds 18.87
NOTES
PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cg:m = mg/dsm3, mass concentration of gasoline emission
Mg = 128 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant)
K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP
Cg = lb/dcsf, mass concentration of gasoline emission, dry basis at STP
PMRg = lb/hr, pollutant mass removal rate of gasoline emission
PMR = pollutant mass removal of gasoline emission over time
EQUATIONS
PPMg = PPM measured * K
Cg:m = PPMg * (Mg / K3)
Cg = Cg:m * 62.43E-09 lb-m^3/mg-ft^3
PMRg = Cg * Qstd * 60 min/hr
PMR = PMRg * ((T2 - T1) / 60)
Cg
(lb/dscf)
PMRg
(lb/hr)
Elapsed
Time
(min)
Flow
(DSCFM)
PMR
(lb)
PPM
measured
(ppm)
K
(#C-gas)PPMg Cg:m
(mg/dsm^3)

APPENDIX B
Laboratory Report – Ground Water Samples
07/22/17
Technical Report for
GRI (Geological Resources Inc.)
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
31939/2721
SGS Accutest Job Number: FA45820
Sampling Date: 07/12/17
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Michael Senglaub
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Southeast 07/22/17
e-Hardcopy 2.0
Automated Report
31
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
1 of 31
FA45820
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA45820-1: MW-1M ....................................................................................................6
3.2: FA45820-2: MW-2M ....................................................................................................8
3.3: FA45820-3: MW-3M ....................................................................................................10
3.4: FA45820-4: TW-1M .....................................................................................................12
Section 4: Misc. Forms ............................................................................................................15
4.1: Chain of Custody ...........................................................................................................16
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................19
5.1: Method Blank Summary ................................................................................................20
5.2: Blank Spike Summary ...................................................................................................24
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................28 123452 of 31
FA45820
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA45820
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Project No: 31939/2721
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA45820-1 07/12/17 11:29 JW 07/14/17 AQ Ground Water MW-1M
FA45820-2 07/12/17 11:45 JW 07/14/17 AQ Ground Water MW-2M
FA45820-3 07/12/17 11:54 JW 07/14/17 AQ Ground Water MW-3M
FA45820-4 07/12/17 11:37 JW 07/14/17 AQ Ground Water TW-1M
3 of 31
FA458201
Summary of Hits Page 1 of 1
Job Number:FA45820
Account:GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Collected:07/12/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA45820-1 MW-1M
Benzene 256 100 25 ug/l SM 6200B
o-Chlorotoluene 49.3 J 100 25 ug/l SM 6200B
Ethylbenzene 1390 100 25 ug/l SM 6200B
Isopropylbenzene 49.6 J 100 25 ug/l SM 6200B
Naphthalene 366 100 25 ug/l SM 6200B
n-Propylbenzene 123 100 25 ug/l SM 6200B
Styrene 90.3 J 100 25 ug/l SM 6200B
Toluene 10500 130 31 ug/l SM 6200B
1,2,4-Trimethylbenzene 1550 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 350 100 25 ug/l SM 6200B
m,p-Xylene 6180 200 25 ug/l SM 6200B
o-Xylene 3210 100 25 ug/l SM 6200B
Xylene (total)9380 300 50 ug/l SM 6200B
FA45820-2 MW-2M
n-Butylbenzene 3.8 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.1 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.18 J 0.50 0.13 ug/l SM 6200B
Methyl Chloride 0.25 J 0.50 0.20 ug/l SM 6200B
Naphthalene 0.40 J 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.20 J 0.50 0.13 ug/l SM 6200B
FA45820-3 MW-3M
Benzene 286 130 31 ug/l SM 6200B
Ethylbenzene 1250 130 31 ug/l SM 6200B
Isopropylbenzene 45.2 J 130 31 ug/l SM 6200B
Naphthalene 222 130 31 ug/l SM 6200B
n-Propylbenzene 131 130 31 ug/l SM 6200B
Styrene 81.1 J 130 31 ug/l SM 6200B
Toluene 13000 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 1040 130 31 ug/l SM 6200B
1,3,5-Trimethylbenzene 234 130 31 ug/l SM 6200B
m,p-Xylene 3820 250 31 ug/l SM 6200B
o-Xylene 2040 130 31 ug/l SM 6200B
Xylene (total)5860 380 63 ug/l SM 6200B
FA45820-4 TW-1M
Toluene a 3190 50 13 ug/l SM 6200B
(a) Internal standard areas outside method criteria. Confirmed by reanalysis.
4 of 31
FA458202
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
5 of 31
FA458203
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA45820-1 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E053979.D 200 07/19/17 12:59 TD n/a n/a VE1804
Run #2 E053982.D 250 07/19/17 14:06 TD n/a n/a VE1804
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 256 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene ND 100 25 ug/l
135-98-8 sec-Butylbenzene ND 100 25 ug/l
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene 49.3 100 25 ug/l J
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 31
FA4582033.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA45820-1 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 100 25 ug/l
100-41-4 Ethylbenzene 1390 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 49.6 100 25 ug/l J
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 100 25 ug/l
91-20-3 Naphthalene 366 100 25 ug/l
103-65-1 n-Propylbenzene 123 100 25 ug/l
100-42-5 Styrene 90.3 100 25 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 10500 a 130 31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 1550 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 350 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 6180 200 25 ug/l
95-47-6 o-Xylene 3210 100 25 ug/l
1330-20-7 Xylene (total)9380 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%94%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%98%70-130%
2037-26-5 Toluene-D8 105%106%70-130%
460-00-4 4-Bromofluorobenzene 103%104%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.1
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Report of Analysis Page 1 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA45820-2 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E053980.D 1 07/19/17 13:22 TD n/a n/a VE1804
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 3.8 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.1 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.2
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Report of Analysis Page 2 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA45820-2 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.18 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride 0.25 0.50 0.20 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.40 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.20 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.2
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Report of Analysis Page 1 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA45820-3 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E053981.D 250 07/19/17 13:44 TD n/a n/a VE1804
Run #2 E053983.D 500 07/19/17 14:28 TD n/a n/a VE1804
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 286 130 31 ug/l
108-86-1 Bromobenzene ND 130 31 ug/l
74-97-5 Bromochloromethane ND 130 31 ug/l
75-27-4 Bromodichloromethane ND 130 31 ug/l
75-25-2 Bromoform ND 130 31 ug/l
104-51-8 n-Butylbenzene ND 130 31 ug/l
135-98-8 sec-Butylbenzene ND 130 31 ug/l
98-06-6 tert-Butylbenzene ND 130 31 ug/l
56-23-5 Carbon Tetrachloride ND 130 31 ug/l
108-90-7 Chlorobenzene ND 130 31 ug/l
75-00-3 Chloroethane ND 130 50 ug/l
67-66-3 Chloroform ND 130 31 ug/l
95-49-8 o-Chlorotoluene ND 130 31 ug/l
106-43-4 p-Chlorotoluene ND 130 31 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 62 ug/l
106-93-4 1,2-Dibromoethane ND 130 31 ug/l
75-71-8 Dichlorodifluoromethane ND 130 50 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l
75-34-3 1,1-Dichloroethane ND 130 31 ug/l
107-06-2 1,2-Dichloroethane ND 130 31 ug/l
75-35-4 1,1-Dichloroethylene ND 130 31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l
78-87-5 1,2-Dichloropropane ND 130 31 ug/l
142-28-9 1,3-Dichloropropane ND 130 31 ug/l
594-20-7 2,2-Dichloropropane ND 130 31 ug/l
563-58-6 1,1-Dichloropropene ND 130 31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.3
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Report of Analysis Page 2 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA45820-3 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 31 ug/l
100-41-4 Ethylbenzene 1250 130 31 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 45.2 130 31 ug/l J
99-87-6 p-Isopropyltoluene ND 130 31 ug/l
74-83-9 Methyl Bromide ND 130 50 ug/l
74-87-3 Methyl Chloride ND 130 50 ug/l
74-95-3 Methylene Bromide ND 130 31 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 130 31 ug/l
91-20-3 Naphthalene 222 130 31 ug/l
103-65-1 n-Propylbenzene 131 130 31 ug/l
100-42-5 Styrene 81.1 130 31 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l
127-18-4 Tetrachloroethylene ND 130 31 ug/l
108-88-3 Toluene 13000 a 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l
79-01-6 Trichloroethylene ND 130 31 ug/l
75-69-4 Trichlorofluoromethane ND 130 50 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 31 ug/l
95-63-6 1,2,4-Trimethylbenzene 1040 130 31 ug/l
108-67-8 1,3,5-Trimethylbenzene 234 130 31 ug/l
75-01-4 Vinyl Chloride ND 130 31 ug/l
m,p-Xylene 3820 250 31 ug/l
95-47-6 o-Xylene 2040 130 31 ug/l
1330-20-7 Xylene (total)5860 380 63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%99%70-130%
2037-26-5 Toluene-D8 106%106%70-130%
460-00-4 4-Bromofluorobenzene 106%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.3
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Report of Analysis Page 1 of 3
Client Sample ID:TW-1M
Lab Sample ID:FA45820-4 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0208230.D 25 07/18/17 13:27 TD n/a n/a VA2193
Run #2 b A0208239.D 100 07/18/17 17:17 TD n/a n/a VA2193
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 13 3.1 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
104-51-8 n-Butylbenzene ND 13 3.1 ug/l
135-98-8 sec-Butylbenzene ND 13 3.1 ug/l
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene ND 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane ND 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.4
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Report of Analysis Page 2 of 3
Client Sample ID:TW-1M
Lab Sample ID:FA45820-4 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 3.1 ug/l
100-41-4 Ethylbenzene ND 13 3.1 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene ND 13 3.1 ug/l
99-87-6 p-Isopropyltoluene ND 13 3.1 ug/l
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride ND 13 5.0 ug/l
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 3.1 ug/l
91-20-3 Naphthalene ND 13 3.1 ug/l
103-65-1 n-Propylbenzene ND 13 3.1 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene 3190 c 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene ND 25 3.1 ug/l
95-47-6 o-Xylene ND 13 3.1 ug/l
1330-20-7 Xylene (total)ND 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 93%94%70-130%
2037-26-5 Toluene-D8 93%93%70-130%
460-00-4 4-Bromofluorobenzene 101%100%70-130%
(a) Sample was not preserved to a pH < 2.
(b) Internal standard areas outside method criteria. Confirmed by reanalysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.4
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Report of Analysis Page 3 of 3
Client Sample ID:TW-1M
Lab Sample ID:FA45820-4 Date Sampled:07/12/17
Matrix:AQ - Ground Water Date Received:07/14/17
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4582033.4
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
15 of 31
FA458204
FA45820: Chain of Custody
Page 1 of 3
16 of 31
FA4582044.1
Job Number:FA45820 Client:GRI
Date / Time Received:7/14/2017 9:30:00 AM Delivery Method:FED EX
Project:2721
Airbill #'s:8110 6225 4036
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments SAMPLE #4 VIALS ALL HAVE HEADSPACE.
SM001Rev. Date 05/24/17
SGS Accutest Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.8);
Cooler 1: (3.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP P.H Date:7/15/2017Date:7/14/2017 9:30:00 AM
FA45820: Chain of Custody
Page 2 of 3
17 of 31
FA4582044.1
Response:
Per client proceed with analysis.
Responded to by: Muna Mohammed Response Date: 7/17/17
FA45820: Chain of Custody
Page 3 of 3
18 of 31
FA4582044.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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FA458205
Method Blank Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2193-MB A0208224.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
20 of 31
FA4582055.1.1
Method Blank Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2193-MB A0208224.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
21 of 31
FA4582055.1.1
Method Blank Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1804-MB E053991.D 1 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 1.4 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
22 of 31
FA4582055.1.2
Method Blank Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1804-MB E053991.D 1 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
23 of 31
FA4582055.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2193-BS A0208223.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.3 93 70-130
108-86-1 Bromobenzene 10 9.6 96 70-130
74-97-5 Bromochloromethane 10 9.3 93 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 8.6 86 70-130
104-51-8 n-Butylbenzene 10 9.3 93 70-130
135-98-8 sec-Butylbenzene 10 9.8 98 70-130
98-06-6 tert-Butylbenzene 10 9.2 92 70-130
56-23-5 Carbon Tetrachloride 10 11.2 112 70-130
108-90-7 Chlorobenzene 10 9.5 95 70-130
75-00-3 Chloroethane 10 8.7 87 60-140
67-66-3 Chloroform 10 9.1 91 70-130
95-49-8 o-Chlorotoluene 10 9.4 94 70-130
106-43-4 p-Chlorotoluene 10 9.3 93 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.6 76 70-130
106-93-4 1,2-Dibromoethane 10 9.5 95 70-130
75-71-8 Dichlorodifluoromethane 10 9.7 97 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.4 94 70-130
106-46-7 1,4-Dichlorobenzene 10 9.4 94 70-130
75-34-3 1,1-Dichloroethane 10 9.4 94 70-130
107-06-2 1,2-Dichloroethane 10 9.3 93 70-130
75-35-4 1,1-Dichloroethylene 10 9.4 94 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.0 100 70-130
78-87-5 1,2-Dichloropropane 10 9.2 92 70-130
142-28-9 1,3-Dichloropropane 10 8.7 87 70-130
594-20-7 2,2-Dichloropropane 10 9.9 99 70-130
563-58-6 1,1-Dichloropropene 10 9.4 94 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
108-20-3 Di-Isopropyl Ether 10 8.5 85 70-130
100-41-4 Ethylbenzene 10 9.1 91 70-130
87-68-3 Hexachlorobutadiene 10 9.3 93 70-130
98-82-8 Isopropylbenzene 10 9.5 95 70-130
* = Outside of Control Limits.
24 of 31
FA4582055.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2193-BS A0208223.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.5 95 70-130
74-83-9 Methyl Bromide 10 9.1 91 60-140
74-87-3 Methyl Chloride 10 8.9 89 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130
91-20-3 Naphthalene 10 9.7 97 70-130
103-65-1 n-Propylbenzene 10 9.6 96 70-130
100-42-5 Styrene 10 9.3 93 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.7 87 70-130
127-18-4 Tetrachloroethylene 10 10 100 70-130
108-88-3 Toluene 10 9.0 90 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.3 93 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.1 91 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 9.1 91 70-130
79-01-6 Trichloroethylene 10 9.8 98 70-130
75-69-4 Trichlorofluoromethane 10 11.9 119 60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.2 92 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.1 91 70-130
75-01-4 Vinyl Chloride 10 9.0 90 60-140
m,p-Xylene 20 18.4 92 70-130
95-47-6 o-Xylene 10 9.0 90 70-130
1330-20-7 Xylene (total)30 27.4 91 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
25 of 31
FA4582055.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1804-BS E053977.D 1 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 8.8 88 70-130
74-97-5 Bromochloromethane 10 9.4 94 70-130
75-27-4 Bromodichloromethane 10 9.4 94 70-130
75-25-2 Bromoform 10 8.4 84 70-130
104-51-8 n-Butylbenzene 10 9.1 91 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 9.1 91 70-130
56-23-5 Carbon Tetrachloride 10 9.6 96 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 10.1 101 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 9.0 90 70-130
106-43-4 p-Chlorotoluene 10 9.1 91 70-130
124-48-1 Dibromochloromethane 10 9.2 92 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 9.4 94 70-130
75-71-8 Dichlorodifluoromethane 10 7.0 70 60-140
95-50-1 1,2-Dichlorobenzene 10 9.3 93 70-130
541-73-1 1,3-Dichlorobenzene 10 9.5 95 70-130
106-46-7 1,4-Dichlorobenzene 10 9.3 93 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 10.4 104 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.0 110 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 8.9 89 70-130
594-20-7 2,2-Dichloropropane 10 9.9 99 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.5 85 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.3 93 70-130
108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130
100-41-4 Ethylbenzene 10 9.4 94 70-130
87-68-3 Hexachlorobutadiene 10 10.1 101 70-130
98-82-8 Isopropylbenzene 10 9.4 94 70-130
* = Outside of Control Limits.
26 of 31
FA4582055.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1804-BS E053977.D 1 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.3 93 70-130
74-83-9 Methyl Bromide 10 9.3 93 60-140
74-87-3 Methyl Chloride 10 8.4 84 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 9.6 96 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130
91-20-3 Naphthalene 10 10.1 101 70-130
103-65-1 n-Propylbenzene 10 9.2 92 70-130
100-42-5 Styrene 10 8.8 88 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.6 96 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.1 91 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 9.3 93 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.7 97 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.5 95 70-130
71-55-6 1,1,1-Trichloroethane 10 9.1 91 70-130
79-00-5 1,1,2-Trichloroethane 10 9.5 95 70-130
79-01-6 Trichloroethylene 10 9.5 95 70-130
75-69-4 Trichlorofluoromethane 10 9.8 98 60-140
96-18-4 1,2,3-Trichloropropane 10 9.2 92 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.9 89 70-130
75-01-4 Vinyl Chloride 10 8.7 87 60-140
m,p-Xylene 20 18.3 92 70-130
95-47-6 o-Xylene 10 9.1 91 70-130
1330-20-7 Xylene (total)30 27.4 91 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
27 of 31
FA4582055.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA45821-8MS A0208246.D 1 07/18/17 TD n/a n/a VA2193
FA45821-8MSD A0208247.D 1 07/18/17 TD n/a n/a VA2193
FA45821-8 A0208240.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
FA45821-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 8.9 89 10 8.7 87 2 70-130/20
108-86-1 Bromobenzene ND 10 8.9 89 10 9.1 91 2 70-130/20
74-97-5 Bromochloromethane ND 10 9.3 93 10 9.0 90 3 70-130/20
75-27-4 Bromodichloromethane ND 10 9.1 91 10 8.8 88 3 70-130/20
75-25-2 Bromoform ND 10 7.4 74 10 7.0 70 6 70-130/20
104-51-8 n-Butylbenzene ND 10 8.2 82 10 8.1 81 1 70-130/20
135-98-8 sec-Butylbenzene ND 10 8.9 89 10 8.7 87 2 70-130/20
98-06-6 tert-Butylbenzene ND 10 8.4 84 10 8.4 84 0 70-130/20
56-23-5 Carbon Tetrachloride ND 10 11.2 112 10 10.1 101 10 70-130/20
108-90-7 Chlorobenzene ND 10 8.9 89 10 8.9 89 0 70-130/20
75-00-3 Chloroethane ND 10 9.4 94 10 8.7 87 8 60-140/20
67-66-3 Chloroform ND 10 9.1 91 10 8.7 87 4 70-130/20
95-49-8 o-Chlorotoluene ND 10 8.7 87 10 8.7 87 0 70-130/20
106-43-4 p-Chlorotoluene ND 10 8.5 85 10 8.5 85 0 70-130/20
124-48-1 Dibromochloromethane ND 10 8.3 83 10 8.0 80 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 6.8 68*10 6.7 67*1 70-130/20
106-93-4 1,2-Dibromoethane ND 10 8.6 86 10 8.9 89 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 10.1 101 10 9.3 93 8 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 8.8 88 10 8.8 88 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 9.0 90 10 8.9 89 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 8.8 88 10 8.7 87 1 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.3 93 10 8.8 88 6 70-130/20
107-06-2 1,2-Dichloroethane ND 10 8.8 88 10 8.9 89 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 9.5 95 10 8.7 87 9 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.1 91 10 8.7 87 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.0 100 10 9.3 93 7 70-130/20
78-87-5 1,2-Dichloropropane ND 10 8.4 84 10 8.3 83 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 8.0 80 10 8.2 82 2 70-130/20
594-20-7 2,2-Dichloropropane ND 10 9.2 92 10 8.6 86 7 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.1 91 10 8.7 87 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 7.3 73 10 7.5 75 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 7.8 78 10 8.0 80 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 7.8 78 10 7.7 77 1 70-130/20
100-41-4 Ethylbenzene ND 10 8.5 85 10 8.4 84 1 70-130/20
87-68-3 Hexachlorobutadiene ND 10 7.1 71 10 7.5 75 5 70-130/20
98-82-8 Isopropylbenzene ND 10 9.0 90 10 8.6 86 5 70-130/20
* = Outside of Control Limits.
28 of 31
FA4582055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA45821-8MS A0208246.D 1 07/18/17 TD n/a n/a VA2193
FA45821-8MSD A0208247.D 1 07/18/17 TD n/a n/a VA2193
FA45821-8 A0208240.D 1 07/18/17 TD n/a n/a VA2193
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-4
FA45821-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 8.7 87 10 8.6 86 1 70-130/20
74-83-9 Methyl Bromide ND 10 9.7 97 10 8.8 88 10 60-140/20
74-87-3 Methyl Chloride ND 10 9.1 91 10 8.4 84 8 60-140/20
74-95-3 Methylene Bromide ND 10 9.1 91 10 9.4 94 3 70-130/20
75-09-2 Methylene Chloride ND 10 8.3 83 10 7.8 78 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether 4.5 10 13.3 88 10 12.7 82 5 70-130/20
91-20-3 Naphthalene ND 10 9.0 90 10 9.2 92 2 70-130/20
103-65-1 n-Propylbenzene ND 10 8.7 87 10 8.6 86 1 70-130/20
100-42-5 Styrene ND 10 8.6 86 10 8.2 82 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.4 94 10 9.0 90 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 8.1 81 10 8.3 83 2 70-130/20
127-18-4 Tetrachloroethylene ND 10 9.4 94 10 8.9 89 5 70-130/20
108-88-3 Toluene 0.25 J 10 8.5 83 10 8.4 82 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 8.3 83 10 8.6 86 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.2 82 10 8.3 83 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.6 96 10 8.9 89 8 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 8.3 83 10 8.7 87 5 70-130/20
79-01-6 Trichloroethylene ND 10 9.2 92 10 9.1 91 1 70-130/20
75-69-4 Trichlorofluoromethane ND 10 12.9 129 10 11.5 115 11 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 8.7 87 10 8.9 89 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 8.7 87 10 8.5 85 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 8.4 84 10 8.3 83 1 70-130/20
75-01-4 Vinyl Chloride ND 10 9.1 91 10 8.3 83 9 60-140/20
m,p-Xylene 0.55 J 20 18.1 88 20 17.4 84 4 70-130/20
95-47-6 o-Xylene 0.60 10 9.2 86 10 8.9 83 3 70-130/20
1330-20-7 Xylene (total)1.2 J 30 27.3 87 30 26.4 84 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA45821-8 Limits
1868-53-7 Dibromofluoromethane 108%104%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%101%95%70-130%
2037-26-5 Toluene-D8 91%91%91%70-130%
460-00-4 4-Bromofluorobenzene 96%98%101%70-130%
* = Outside of Control Limits.
29 of 31
FA4582055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA45889-10MS E053999.D 100 07/19/17 TD n/a n/a VE1804
FA45889-10MSD E054000.D 100 07/19/17 TD n/a n/a VE1804
FA45889-10 E053988.D 100 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
FA45889-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 182 1000 1200 102 1000 1040 86 14 70-130/20
108-86-1 Bromobenzene ND 1000 945 95 1000 773 77 20 70-130/20
74-97-5 Bromochloromethane ND 1000 969 97 1000 796 80 20 70-130/20
75-27-4 Bromodichloromethane ND 1000 955 96 1000 807 81 17 70-130/20
75-25-2 Bromoform ND 1000 810 81 1000 693 69*16 70-130/20
104-51-8 n-Butylbenzene 34.5 J 1000 1030 100 1000 854 82 19 70-130/20
135-98-8 sec-Butylbenzene 22.0 J 1000 1040 102 1000 867 85 18 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1010 101 1000 848 85 17 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 971 97 1000 810 81 18 70-130/20
108-90-7 Chlorobenzene ND 1000 1040 104 1000 865 87 18 70-130/20
75-00-3 Chloroethane ND 1000 991 99 1000 1010 101 2 60-140/20
67-66-3 Chloroform ND 1000 975 98 1000 825 83 17 70-130/20
95-49-8 o-Chlorotoluene 94.9 1000 1110 102 1000 933 84 17 70-130/20
106-43-4 p-Chlorotoluene ND 1000 988 99 1000 822 82 18 70-130/20
124-48-1 Dibromochloromethane ND 1000 926 93 1000 777 78 17 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 987 99 1000 811 81 20 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 1010 101 1000 827 83 20 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 775 78 1000 797 80 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 1010 101 1000 821 82 21*70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 1010 101 1000 830 83 20 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 1020 102 1000 839 84 19 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1060 106 1000 896 90 17 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 990 99 1000 809 81 20 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1070 107 1000 897 90 18 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 960 96 1000 815 82 16 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1130 113 1000 963 96 16 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 975 98 1000 820 82 17 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 969 97 1000 776 78 22*70-130/20
594-20-7 2,2-Dichloropropane ND 1000 932 93 1000 790 79 16 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1000 100 1000 836 84 18 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 919 92 1000 760 76 19 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 978 98 1000 797 80 20 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 1010 101 1000 840 84 18 70-130/20
100-41-4 Ethylbenzene 2520 1000 3620 110 1000 3490 97 4 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 1020 102 1000 870 87 16 70-130/20
98-82-8 Isopropylbenzene 109 1000 1120 101 1000 959 85 15 70-130/20
* = Outside of Control Limits.
30 of 31
FA4582055.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA45820
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA45889-10MS E053999.D 100 07/19/17 TD n/a n/a VE1804
FA45889-10MSD E054000.D 100 07/19/17 TD n/a n/a VE1804
FA45889-10 E053988.D 100 07/19/17 TD n/a n/a VE1804
The QC reported here applies to the following samples:Method: SM 6200B
FA45820-1, FA45820-2, FA45820-3
FA45889-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 15.8 J 1000 1020 100 1000 838 82 20 70-130/20
74-83-9 Methyl Bromide ND 1000 908 91 1000 897 90 1 60-140/20
74-87-3 Methyl Chloride ND 1000 943 94 1000 927 93 2 60-140/20
74-95-3 Methylene Bromide ND 1000 967 97 1000 813 81 17 70-130/20
75-09-2 Methylene Chloride ND 1000 940 94 1000 798 80 16 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 1000 986 99 1000 830 83 17 70-130/20
91-20-3 Naphthalene 1370 1000 2960 159*1000 2210 84 29*70-130/20
103-65-1 n-Propylbenzene 335 1000 1350 102 1000 1180 85 13 70-130/20
100-42-5 Styrene 15.7 J 1000 995 98 1000 839 82 17 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 997 100 1000 830 83 18 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 981 98 1000 801 80 20 70-130/20
127-18-4 Tetrachloroethylene ND 1000 996 100 1000 815 82 20 70-130/20
108-88-3 Toluene 2670 1000 3710 104 1000 3550 88 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 837 84 1000 767 77 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 957 96 1000 819 82 16 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 956 96 1000 795 80 18 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 1010 101 1000 833 83 19 70-130/20
79-01-6 Trichloroethylene ND 1000 987 99 1000 830 83 17 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 971 97 1000 999 100 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 989 99 1000 820 82 19 70-130/20
95-63-6 1,2,4-Trimethylbenzene 3010 1000 4070 106 1000 3870 86 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 741 1000 1750 101 1000 1560 82 11 70-130/20
75-01-4 Vinyl Chloride ND 1000 920 92 1000 905 91 2 60-140/20
m,p-Xylene 10100 E 2000 11500 70 2000 11300 60* a 2 70-130/20
95-47-6 o-Xylene 5130 E 1000 5930 80 1000 5870 74 1 70-130/20
1330-20-7 Xylene (total)15300 E 3000 17400 70 3000 17200 63* a 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA45889-10 Limits
1868-53-7 Dibromofluoromethane 97%98%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%103%99%70-130%
2037-26-5 Toluene-D8 103%103%106%70-130%
460-00-4 4-Bromofluorobenzene 105%106%105%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
31 of 31
FA4582055.3.2