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HomeMy WebLinkAboutWA-26024_31302_CA_MRP_20170403Analytical Report L7C0151 Project Lighthouse Food Mart #110 Project Number 02804 March 23, 2017 Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Mebane, NC 27302 Minority Women Business Enterprise Small Disadvantaged Business Enterprise 1412 Tech Blvd Phone #:813-620-2000 Website:www.ftsanalytical.comTampa, FL 33619 Minority Women Business Enterprise Small Disadvantaged Business Enterprise March 23, 2017 Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Ryan Kerins RE: Lighthouse Food Mart #110 We are reporting the results of the analyses performed on the samples recieved on 3/9/2017 under the project name referenced above and identified as the lab Work Order L7C0151. All results being reported under this Report apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontracted lab, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reporting using all other available quality control methods. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise agreed upon. The samples received, and described as recorded in Work Order L7C0151 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard practices, controlled/regulated substances, etc.) We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions concerning this report, please do not hesitate to contact us at any time. We will be happy to help. Mebane, NC 27302 Sincerely, Chad Bechtold VP of Client Services Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Samples in this Report Sample Lab ID Matrix Date Sampled Date Received MW1A WaterL7C0151-01 09-Mar-2017 09:5008-Mar-2017 12:05 MW2 WaterL7C0151-02 09-Mar-2017 09:5008-Mar-2017 12:08 MW3 WaterL7C0151-03 09-Mar-2017 09:5008-Mar-2017 12:11 MW5 WaterL7C0151-04 09-Mar-2017 09:5008-Mar-2017 12:15 MW7 WaterL7C0151-05 09-Mar-2017 09:5008-Mar-2017 12:20 MW14 WaterL7C0151-06 09-Mar-2017 09:5008-Mar-2017 12:24 MW17 WaterL7C0151-07 09-Mar-2017 09:5008-Mar-2017 12:28 MW18 WaterL7C0151-08 09-Mar-2017 09:5008-Mar-2017 12:33 MW19 WaterL7C0151-09 09-Mar-2017 09:5008-Mar-2017 12:40 MW22 WaterL7C0151-10 09-Mar-2017 09:5008-Mar-2017 12:45 Page 3 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Analysis Case Narrative Method 6200B Batch B7C0234 The precision (RPD) of the Blank Spike and Blank Spike Duplicate exceeded control limits for Chloroethane. The precision (RPD) was within limits for the Matrix Spike and Matrix Spike Duplicate. The precision of the Matrix Spike and Matrix Spike Duplicate exceeded control limits for 1,1,1-Trichloroethane; however, the recoveries were within acceptable limits. The precision (RPD) was within limits for the Blank Spike and Blank Sipke Duplicate. The Matrix Spike and/or Matrix Spike Duplicate recoveries for Vinyl acetate are outside the laboratory control limits . However, the Blank Spike and/or Blank Spike Duplicate recoveries are within acceptable limits. Page 4 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary Sample: MW1A MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-01 12.5 ug/L2.58 252060 3/10/17 18:26 95-63-6 SM 6200B1,2,4-Trimethylbenzene 12.5 ug/L2.18 25440 3/10/17 18:26 108-67-8 SM 6200B1,3,5-trimethylbenzene 12.5 ug/L2.22 2543.0 3/10/17 18:26 99-87-6 SM 6200B4-Isopropyltoluene (p-Cymene) 12.5 ug/L2.98 25528 3/10/17 18:26 71-43-2 SM 6200BBenzene 12.5 ug/L2.30 251350 3/10/17 18:26 100-41-4 SM 6200BEthylbenzene 12.5 ug/L2.45 2587.8 3/10/17 18:26 98-82-8 SM 6200Bisopropylbenzene 50.0 ug/L2.35 25399 3/10/17 18:26 91-20-3 SM 6200BNaphthalene 25.0 ug/L1.62 25221 3/10/17 18:26 103-65-1 SM 6200Bn-Propylbenzene 12.5 ug/L1.42 25678 3/10/17 18:26 108-88-3 SM 6200BToluene 25.0 ug/L4.40 252650 3/10/17 18:26 179601-23-1 SM 6200Bm,p-Xylenes 12.5 ug/L3.05 25921 3/10/17 18:26 95-47-6 SM 6200Bo-Xylene 25.0 ug/L4.50 253570 3/10/17 18:26 1330-20-7 SM 6200BTotal Xylenes Sample: MW2 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-02 25.0 ug/L5.15 503120 3/16/17 19:22 95-63-6 SM 6200B1,2,4-Trimethylbenzene 12.5 ug/L2.18 25972 3/10/17 17:59 108-67-8 SM 6200B1,3,5-trimethylbenzene 12.5 ug/L2.22 2568.8 3/10/17 17:59 99-87-6 SM 6200B4-Isopropyltoluene (p-Cymene) 125 ug/L8.80 25J13.0 3/10/17 17:59 67-64-1 SM 6200BAcetone 12.5 ug/L2.30 25934 3/10/17 17:59 100-41-4 SM 6200BEthylbenzene 12.5 ug/L2.45 2561.0 3/10/17 17:59 98-82-8 SM 6200Bisopropylbenzene 50.0 ug/L2.35 25668 3/10/17 17:59 91-20-3 SM 6200BNaphthalene 25.0 ug/L1.62 25129 3/10/17 17:59 103-65-1 SM 6200Bn-Propylbenzene 12.5 ug/L1.85 2528.2 3/10/17 17:59 100-42-5 SM 6200BStyrene 12.5 ug/L1.42 25724 3/10/17 17:59 108-88-3 SM 6200BToluene 25.0 ug/L4.40 255700 3/10/17 17:59 179601-23-1 SM 6200Bm,p-Xylenes 12.5 ug/L3.05 253390 3/10/17 17:59 95-47-6 SM 6200Bo-Xylene 25.0 ug/L4.50 259090 3/10/17 17:59 1330-20-7 SM 6200BTotal Xylenes Page 5 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary (Continued) Sample: MW3 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-03 5.00 ug/L1.03 10582 3/10/17 17:32 95-63-6 SM 6200B1,2,4-Trimethylbenzene 5.00 ug/L0.870 10137 3/10/17 17:32 108-67-8 SM 6200B1,3,5-trimethylbenzene 5.00 ug/L0.890 1016.0 3/10/17 17:32 99-87-6 SM 6200B4-Isopropyltoluene (p-Cymene) 5.00 ug/L1.19 1023.8 3/10/17 17:32 71-43-2 SM 6200BBenzene 5.00 ug/L0.920 10221 3/10/17 17:32 100-41-4 SM 6200BEthylbenzene 5.00 ug/L0.980 1021.6 3/10/17 17:32 98-82-8 SM 6200Bisopropylbenzene 20.0 ug/L0.940 10132 3/10/17 17:32 91-20-3 SM 6200BNaphthalene 10.0 ug/L0.650 1060.9 3/10/17 17:32 103-65-1 SM 6200Bn-Propylbenzene 5.00 ug/L0.740 1010.6 3/10/17 17:32 100-42-5 SM 6200BStyrene 5.00 ug/L0.570 10144 3/10/17 17:32 108-88-3 SM 6200BToluene 10.0 ug/L1.76 10750 3/10/17 17:32 179601-23-1 SM 6200Bm,p-Xylenes 5.00 ug/L1.22 10365 3/10/17 17:32 95-47-6 SM 6200Bo-Xylene 10.0 ug/L1.80 101120 3/10/17 17:32 1330-20-7 SM 6200BTotal Xylenes Sample: MW7 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-05 2.50 ug/L0.515 5141 3/10/17 17:05 95-63-6 SM 6200B1,2,4-Trimethylbenzene 2.50 ug/L0.435 57.50 3/10/17 17:05 108-67-8 SM 6200B1,3,5-trimethylbenzene 2.50 ug/L0.445 57.05 3/10/17 17:05 99-87-6 SM 6200B4-Isopropyltoluene (p-Cymene) 2.50 ug/L0.595 598.8 3/10/17 17:05 71-43-2 SM 6200BBenzene 2.50 ug/L0.860 5J1.20 3/10/17 17:05 67-66-3 SM 6200BChloroform 2.50 ug/L0.460 5334 3/10/17 17:05 100-41-4 SM 6200BEthylbenzene 2.50 ug/L0.490 520.4 3/10/17 17:05 98-82-8 SM 6200Bisopropylbenzene 5.00 ug/L0.845 5J3.55 3/10/17 17:05 1634-04-4 SM 6200BMethyl tert-butyl ether (MTBE) 10.0 ug/L0.470 5124 3/10/17 17:05 91-20-3 SM 6200BNaphthalene 10.0 ug/L0.300 5J8.85 3/10/17 17:05 104-51-8 SM 6200Bn-Butylbenzene 5.00 ug/L0.325 556.5 3/10/17 17:05 103-65-1 SM 6200Bn-Propylbenzene 2.50 ug/L0.370 55.20 3/10/17 17:05 100-42-5 SM 6200BStyrene 2.50 ug/L0.285 529.5 3/10/17 17:05 108-88-3 SM 6200BToluene 5.00 ug/L0.880 5121 3/10/17 17:05 179601-23-1 SM 6200Bm,p-Xylenes 2.50 ug/L0.610 5152 3/10/17 17:05 95-47-6 SM 6200Bo-Xylene 5.00 ug/L0.900 5273 3/10/17 17:05 1330-20-7 SM 6200BTotal Xylenes Page 6 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary (Continued) Sample: MW14 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-06 0.500 ug/L0.103 111.0 3/10/17 15:24 95-63-6 SM 6200B1,2,4-Trimethylbenzene 0.500 ug/L0.0940 1J0.110 3/10/17 15:24 95-50-1 SM 6200B1,2-Dichlorobenzene 0.500 ug/L0.0900 1J0.190 3/10/17 15:24 106-43-4 SM 6200B4-Chlorotoluene 0.500 ug/L0.0890 11.53 3/10/17 15:24 99-87-6 SM 6200B4-Isopropyltoluene (p-Cymene) 0.500 ug/L0.119 130.9 3/10/17 15:24 71-43-2 SM 6200BBenzene 0.500 ug/L0.172 16.66 3/10/17 15:24 67-66-3 SM 6200BChloroform 0.500 ug/L0.0920 13.14 3/10/17 15:24 100-41-4 SM 6200BEthylbenzene 5.00 ug/L0.0920 1J0.200 3/10/17 15:24 108-20-3 SM 6200BIsopropyl Ether 0.500 ug/L0.0980 11.49 3/10/17 15:24 98-82-8 SM 6200Bisopropylbenzene 1.00 ug/L0.169 14.56 3/10/17 15:24 1634-04-4 SM 6200BMethyl tert-butyl ether (MTBE) 2.00 ug/L0.0940 125.6 3/10/17 15:24 91-20-3 SM 6200BNaphthalene 2.00 ug/L0.0600 1J1.69 3/10/17 15:24 104-51-8 SM 6200Bn-Butylbenzene 1.00 ug/L0.0650 11.20 3/10/17 15:24 103-65-1 SM 6200Bn-Propylbenzene 0.500 ug/L0.0920 10.530 3/10/17 15:24 135-98-8 SM 6200BSec-Butylbenzene 1.00 ug/L0.176 16.08 3/10/17 15:24 179601-23-1 SM 6200Bm,p-Xylenes 0.500 ug/L0.122 13.45 3/10/17 15:24 95-47-6 SM 6200Bo-Xylene 1.00 ug/L0.180 19.53 3/10/17 15:24 1330-20-7 SM 6200BTotal Xylenes Sample: MW17 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-07 0.500 ug/L0.119 1J0.160 3/10/17 16:13 71-43-2 SM 6200BBenzene 0.500 ug/L0.0920 18.40 3/10/17 16:13 100-41-4 SM 6200BEthylbenzene 0.500 ug/L0.0980 12.17 3/10/17 16:13 98-82-8 SM 6200Bisopropylbenzene 1.00 ug/L0.169 13.30 3/10/17 16:13 1634-04-4 SM 6200BMethyl tert-butyl ether (MTBE) 2.00 ug/L0.0940 17.48 3/10/17 16:13 91-20-3 SM 6200BNaphthalene 2.00 ug/L0.0600 1J1.34 3/10/17 16:13 104-51-8 SM 6200Bn-Butylbenzene 1.00 ug/L0.0650 13.49 3/10/17 16:13 103-65-1 SM 6200Bn-Propylbenzene 0.500 ug/L0.0570 1J0.100 3/10/17 16:13 108-88-3 SM 6200BToluene Sample: MW19 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-09 1.00 ug/L0.169 1J0.380 3/10/17 15:48 1634-04-4 SM 6200BMethyl tert-butyl ether (MTBE) 2.00 ug/L0.0940 12.53 3/10/17 15:48 91-20-3 SM 6200BNaphthalene Page 7 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary (Continued) Sample: MW22 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: L7C0151-10 2.00 ug/L0.0600 1J1.18 3/10/17 14:35 104-51-8 SM 6200Bn-Butylbenzene Page 8 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-01 (Water) Client Sample ID: MW1A RL Dil Date Prepared Sampled: 3/8/17 12:05 CAS # VOCs by NC Method 6200B 25.0 ug/L4.50 254.50 U 3/10/17 18:263/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 12.5 ug/L1.90 251.90 U 3/10/17 18:263/10/17 12:25 71-55-61,1,1-Trichloroethane 12.5 ug/L1.75 251.75 U 3/10/17 18:263/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 12.5 ug/L2.82 252.82 U 3/10/17 18:263/10/17 12:25 79-00-51,1,2-Trichloroethane 12.5 ug/L3.02 253.02 U 3/10/17 18:263/10/17 12:25 75-34-31,1-Dichloroethane 12.5 ug/L2.60 252.60 U 3/10/17 18:263/10/17 12:25 75-35-41,1-Dichloroethene 12.5 ug/L1.50 251.50 U 3/10/17 18:263/10/17 12:25 563-58-61,1-Dichloropropene 50.0 ug/L2.95 252.95 U 3/10/17 18:263/10/17 12:25 87-61-61,2,3-Trichlorobenzene 25.0 ug/L3.45 253.45 U 3/10/17 18:263/10/17 12:25 96-18-41,2,3-Trichloropropane 25.0 ug/L1.72 251.72 U 3/10/17 18:263/10/17 12:25 120-82-11,2,4-Trichlorobenzene 12.5 ug/L2.58 252060 3/10/17 18:263/10/17 12:25 95-63-61,2,4-Trimethylbenzene 25.0 ug/L4.50 254.50 U 3/10/17 18:263/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 12.5 ug/L2.35 252.35 U 3/10/17 18:263/10/17 12:25 95-50-11,2-Dichlorobenzene 12.5 ug/L2.25 252.25 U 3/10/17 18:263/10/17 12:25 107-06-21,2-Dichloroethane 12.5 ug/L3.05 253.05 U 3/10/17 18:263/10/17 12:25 78-87-51,2-Dichloropropane 12.5 ug/L2.18 25440 3/10/17 18:263/10/17 12:25 108-67-81,3,5-trimethylbenzene 12.5 ug/L2.45 252.45 U 3/10/17 18:263/10/17 12:25 541-73-11,3-Dichlorobenzene 12.5 ug/L3.32 253.32 U 3/10/17 18:263/10/17 12:25 142-28-91,3-Dichloropropane 12.5 ug/L1.68 251.68 U 3/10/17 18:263/10/17 12:25 106-46-71,4-Dichlorobenzene 5.00 ug/L2.42 252.42 U 3/10/17 18:263/10/17 12:25 590-20-72,2-Dichloropropane 500 ug/L9.45 259.45 U 3/10/17 18:263/10/17 12:25 78-93-32-Butanone (MEK) 5.00 ug/L2.20 252.20 U 3/10/17 18:263/10/17 12:25 95-49-82-Chlorotoluene 125 ug/L8.80 258.80 U 3/10/17 18:263/10/17 12:25 591-78-62-Hexanone 12.5 ug/L2.25 252.25 U 3/10/17 18:263/10/17 12:25 106-43-44-Chlorotoluene 12.5 ug/L2.22 2543.0 3/10/17 18:263/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 125 ug/L6.32 256.32 U 3/10/17 18:263/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 125 ug/L8.80 258.80 U 3/10/17 18:263/10/17 12:25 67-64-1Acetone 12.5 ug/L2.98 25528 3/10/17 18:263/10/17 12:25 71-43-2Benzene 12.5 ug/L3.30 253.30 U 3/10/17 18:263/10/17 12:25 108-86-1Bromobenzene 12.5 ug/L2.80 252.80 U 3/10/17 18:263/10/17 12:25 74-97-5Bromochloromethane 12.5 ug/L3.10 253.10 U 3/10/17 18:263/10/17 12:25 75-27-4Bromodichloromethane 50.0 ug/L3.98 253.98 U 3/10/17 18:263/10/17 12:25 75-25-2Bromoform 25.0 ug/L2.42 252.42 U 3/10/17 18:263/10/17 12:25 74-83-9Bromomethane 12.5 ug/L2.48 252.48 U 3/10/17 18:263/10/17 12:25 56-23-5Carbon Tetrachloride 12.5 ug/L2.62 252.62 U 3/10/17 18:263/10/17 12:25 108-90-7Chlorobenzene 25.0 ug/L4.42 254.42 U 3/10/17 18:263/10/17 12:25 124-48-1Chlorodibromomethane 12.5 ug/L1.05 251.05 U 3/10/17 18:263/10/17 12:25 75-00-3Chloroethane 12.5 ug/L4.30 254.30 U 3/10/17 18:263/10/17 12:25 67-66-3Chloroform 12.5 ug/L2.12 252.12 U 3/10/17 18:263/10/17 12:25 74-87-3Chloromethane 12.5 ug/L2.85 252.85 U 3/10/17 18:263/10/17 12:25 156-59-2cis-1,2-Dichloroethene 25.0 ug/L2.50 252.50 U 3/10/17 18:263/10/17 12:25 10061-01-5cis-1,3-Dichloropropene Page 9 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-01 (Water) Client Sample ID: MW1A (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:05 CAS # VOCs by NC Method 6200B (Continued) 12.5 ug/L1.68 251.68 U 3/10/17 18:263/10/17 12:25 75-71-8Dichlorodifluoromethane 1250 ug/L75.0 2575.0 U 3/10/17 18:263/10/17 12:25 64-17-5Ethanol 12.5 ug/L2.30 251350 3/10/17 18:263/10/17 12:25 100-41-4Ethylbenzene 125 ug/L2.30 252.30 U 3/10/17 18:263/10/17 12:25 108-20-3Isopropyl Ether 12.5 ug/L2.45 2587.8 3/10/17 18:263/10/17 12:25 98-82-8isopropylbenzene 25.0 ug/L4.22 254.22 U 3/10/17 18:263/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 12.5 ug/L4.75 254.75 U 3/10/17 18:263/10/17 12:25 75-09-2Methylene Chloride 50.0 ug/L2.35 25399 3/10/17 18:263/10/17 12:25 91-20-3Naphthalene 50.0 ug/L1.50 251.50 U 3/10/17 18:263/10/17 12:25 104-51-8n-Butylbenzene 25.0 ug/L1.62 25221 3/10/17 18:263/10/17 12:25 103-65-1n-Propylbenzene 12.5 ug/L2.30 252.30 U 3/10/17 18:263/10/17 12:25 135-98-8Sec-Butylbenzene 12.5 ug/L1.85 251.85 U 3/10/17 18:263/10/17 12:25 100-42-5Styrene 12.5 ug/L2.22 252.22 U 3/10/17 18:263/10/17 12:25 98-06-6tert-Butylbenzene 12.5 ug/L1.35 251.35 U 3/10/17 18:263/10/17 12:25 127-18-4Tetrachloroethene 12.5 ug/L1.42 25678 3/10/17 18:263/10/17 12:25 108-88-3Toluene 12.5 ug/L4.70 254.70 U 3/10/17 18:263/10/17 12:25 156-60-5trans-1,2-dichloroethene 25.0 ug/L2.75 252.75 U 3/10/17 18:263/10/17 12:25 1006-10-26trans-1,3-dichloropropene 12.5 ug/L3.48 253.48 U 3/10/17 18:263/10/17 12:25 79-01-6Trichloroethene 12.5 ug/L1.35 251.35 U 3/10/17 18:263/10/17 12:25 75-69-4Trichlorofluoromethane 25.0 ug/L18.0 2518.0 U 3/10/17 18:263/10/17 12:25 108-05-4Vinyl Acetate 12.5 ug/L2.02 252.02 U 3/10/17 18:263/10/17 12:25 75-01-4Vinyl Chloride 25.0 ug/L4.40 252650 3/10/17 18:263/10/17 12:25 179601-23-1m,p-Xylenes 12.5 ug/L3.05 25921 3/10/17 18:263/10/17 12:25 95-47-6o-Xylene 25.0 ug/L4.50 253570 3/10/17 18:263/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13087%3/10/17 18:26 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13090%3/10/17 18:26 460-00-4 Surrogate: Toluene-D8 (SUR)70-13097%3/10/17 18:26 2037-26-5 Page 10 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-02 (Water) Client Sample ID: MW2 RL Dil Date Prepared Sampled: 3/8/17 12:08 CAS # VOCs by NC Method 6200B 25.0 ug/L4.50 254.50 U 3/10/17 17:593/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 12.5 ug/L1.90 251.90 U 3/10/17 17:593/10/17 12:25 71-55-61,1,1-Trichloroethane 12.5 ug/L1.75 251.75 U 3/10/17 17:593/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 12.5 ug/L2.82 252.82 U 3/10/17 17:593/10/17 12:25 79-00-51,1,2-Trichloroethane 12.5 ug/L3.02 253.02 U 3/10/17 17:593/10/17 12:25 75-34-31,1-Dichloroethane 12.5 ug/L2.60 252.60 U 3/10/17 17:593/10/17 12:25 75-35-41,1-Dichloroethene 12.5 ug/L1.50 251.50 U 3/10/17 17:593/10/17 12:25 563-58-61,1-Dichloropropene 50.0 ug/L2.95 252.95 U 3/10/17 17:593/10/17 12:25 87-61-61,2,3-Trichlorobenzene 25.0 ug/L3.45 253.45 U 3/10/17 17:593/10/17 12:25 96-18-41,2,3-Trichloropropane 25.0 ug/L1.72 251.72 U 3/10/17 17:593/10/17 12:25 120-82-11,2,4-Trichlorobenzene 25.0 ug/L5.15 503120 3/16/17 19:223/16/17 8:33 95-63-61,2,4-Trimethylbenzene 25.0 ug/L4.50 254.50 U 3/10/17 17:593/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 12.5 ug/L2.35 252.35 U 3/10/17 17:593/10/17 12:25 95-50-11,2-Dichlorobenzene 12.5 ug/L2.25 252.25 U 3/10/17 17:593/10/17 12:25 107-06-21,2-Dichloroethane 12.5 ug/L3.05 253.05 U 3/10/17 17:593/10/17 12:25 78-87-51,2-Dichloropropane 12.5 ug/L2.18 25972 3/10/17 17:593/10/17 12:25 108-67-81,3,5-trimethylbenzene 12.5 ug/L2.45 252.45 U 3/10/17 17:593/10/17 12:25 541-73-11,3-Dichlorobenzene 12.5 ug/L3.32 253.32 U 3/10/17 17:593/10/17 12:25 142-28-91,3-Dichloropropane 12.5 ug/L1.68 251.68 U 3/10/17 17:593/10/17 12:25 106-46-71,4-Dichlorobenzene 5.00 ug/L2.42 252.42 U 3/10/17 17:593/10/17 12:25 590-20-72,2-Dichloropropane 500 ug/L9.45 259.45 U 3/10/17 17:593/10/17 12:25 78-93-32-Butanone (MEK) 5.00 ug/L2.20 252.20 U 3/10/17 17:593/10/17 12:25 95-49-82-Chlorotoluene 125 ug/L8.80 258.80 U 3/10/17 17:593/10/17 12:25 591-78-62-Hexanone 12.5 ug/L2.25 252.25 U 3/10/17 17:593/10/17 12:25 106-43-44-Chlorotoluene 12.5 ug/L2.22 2568.8 3/10/17 17:593/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 125 ug/L6.32 256.32 U 3/10/17 17:593/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 125 ug/L8.80 2513.0 J 3/10/17 17:593/10/17 12:25 67-64-1Acetone 12.5 ug/L2.98 252.98 U 3/10/17 17:593/10/17 12:25 71-43-2Benzene 12.5 ug/L3.30 253.30 U 3/10/17 17:593/10/17 12:25 108-86-1Bromobenzene 12.5 ug/L2.80 252.80 U 3/10/17 17:593/10/17 12:25 74-97-5Bromochloromethane 12.5 ug/L3.10 253.10 U 3/10/17 17:593/10/17 12:25 75-27-4Bromodichloromethane 50.0 ug/L3.98 253.98 U 3/10/17 17:593/10/17 12:25 75-25-2Bromoform 25.0 ug/L2.42 252.42 U 3/10/17 17:593/10/17 12:25 74-83-9Bromomethane 12.5 ug/L2.48 252.48 U 3/10/17 17:593/10/17 12:25 56-23-5Carbon Tetrachloride 12.5 ug/L2.62 252.62 U 3/10/17 17:593/10/17 12:25 108-90-7Chlorobenzene 25.0 ug/L4.42 254.42 U 3/10/17 17:593/10/17 12:25 124-48-1Chlorodibromomethane 12.5 ug/L1.05 251.05 U 3/10/17 17:593/10/17 12:25 75-00-3Chloroethane 12.5 ug/L4.30 254.30 U 3/10/17 17:593/10/17 12:25 67-66-3Chloroform 12.5 ug/L2.12 252.12 U 3/10/17 17:593/10/17 12:25 74-87-3Chloromethane 12.5 ug/L2.85 252.85 U 3/10/17 17:593/10/17 12:25 156-59-2cis-1,2-Dichloroethene 25.0 ug/L2.50 252.50 U 3/10/17 17:593/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 12.5 ug/L1.68 251.68 U 3/10/17 17:593/10/17 12:25 75-71-8Dichlorodifluoromethane Page 11 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-02 (Water) Client Sample ID: MW2 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:08 CAS # VOCs by NC Method 6200B (Continued) 1250 ug/L75.0 2575.0 U 3/10/17 17:593/10/17 12:25 64-17-5Ethanol 12.5 ug/L2.30 25934 3/10/17 17:593/10/17 12:25 100-41-4Ethylbenzene 125 ug/L2.30 252.30 U 3/10/17 17:593/10/17 12:25 108-20-3Isopropyl Ether 12.5 ug/L2.45 2561.0 3/10/17 17:593/10/17 12:25 98-82-8isopropylbenzene 25.0 ug/L4.22 254.22 U 3/10/17 17:593/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 12.5 ug/L4.75 254.75 U 3/10/17 17:593/10/17 12:25 75-09-2Methylene Chloride 50.0 ug/L2.35 25668 3/10/17 17:593/10/17 12:25 91-20-3Naphthalene 50.0 ug/L1.50 251.50 U 3/10/17 17:593/10/17 12:25 104-51-8n-Butylbenzene 25.0 ug/L1.62 25129 3/10/17 17:593/10/17 12:25 103-65-1n-Propylbenzene 12.5 ug/L2.30 252.30 U 3/10/17 17:593/10/17 12:25 135-98-8Sec-Butylbenzene 12.5 ug/L1.85 2528.2 3/10/17 17:593/10/17 12:25 100-42-5Styrene 12.5 ug/L2.22 252.22 U 3/10/17 17:593/10/17 12:25 98-06-6tert-Butylbenzene 12.5 ug/L1.35 251.35 U 3/10/17 17:593/10/17 12:25 127-18-4Tetrachloroethene 12.5 ug/L1.42 25724 3/10/17 17:593/10/17 12:25 108-88-3Toluene 12.5 ug/L4.70 254.70 U 3/10/17 17:593/10/17 12:25 156-60-5trans-1,2-dichloroethene 25.0 ug/L2.75 252.75 U 3/10/17 17:593/10/17 12:25 1006-10-26trans-1,3-dichloropropene 12.5 ug/L3.48 253.48 U 3/10/17 17:593/10/17 12:25 79-01-6Trichloroethene 12.5 ug/L1.35 251.35 U 3/10/17 17:593/10/17 12:25 75-69-4Trichlorofluoromethane 25.0 ug/L18.0 2518.0 U 3/10/17 17:593/10/17 12:25 108-05-4Vinyl Acetate 12.5 ug/L2.02 252.02 U 3/10/17 17:593/10/17 12:25 75-01-4Vinyl Chloride 25.0 ug/L4.40 255700 3/10/17 17:593/10/17 12:25 179601-23-1m,p-Xylenes 12.5 ug/L3.05 253390 3/10/17 17:593/10/17 12:25 95-47-6o-Xylene 25.0 ug/L4.50 259090 3/10/17 17:593/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13091%3/10/17 17:59 10706-07-0 Surrogate: 1,2-Dichloroethane-D4 (SUR) (Reshot)70-130104%3/16/17 19:22 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13090%3/10/17 17:59 460-00-4 Surrogate: 4-Bromofluorobenzene (SUR) (Reshot)70-13086%3/16/17 19:22 460-00-4 Surrogate: Toluene-D8 (SUR)70-13096%3/10/17 17:59 2037-26-5 Surrogate: Toluene-D8 (SUR) (Reshot)70-13093%3/16/17 19:22 2037-26-5 Page 12 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-03 (Water) Client Sample ID: MW3 RL Dil Date Prepared Sampled: 3/8/17 12:11 CAS # VOCs by NC Method 6200B 10.0 ug/L1.80 101.80 U 3/10/17 17:323/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 5.00 ug/L0.760 100.760 U 3/10/17 17:323/10/17 12:25 71-55-61,1,1-Trichloroethane 5.00 ug/L0.700 100.700 U 3/10/17 17:323/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 5.00 ug/L1.13 101.13 U 3/10/17 17:323/10/17 12:25 79-00-51,1,2-Trichloroethane 5.00 ug/L1.21 101.21 U 3/10/17 17:323/10/17 12:25 75-34-31,1-Dichloroethane 5.00 ug/L1.04 101.04 U 3/10/17 17:323/10/17 12:25 75-35-41,1-Dichloroethene 5.00 ug/L0.600 100.600 U 3/10/17 17:323/10/17 12:25 563-58-61,1-Dichloropropene 20.0 ug/L1.18 101.18 U 3/10/17 17:323/10/17 12:25 87-61-61,2,3-Trichlorobenzene 10.0 ug/L1.38 101.38 U 3/10/17 17:323/10/17 12:25 96-18-41,2,3-Trichloropropane 10.0 ug/L0.690 100.690 U 3/10/17 17:323/10/17 12:25 120-82-11,2,4-Trichlorobenzene 5.00 ug/L1.03 10582 3/10/17 17:323/10/17 12:25 95-63-61,2,4-Trimethylbenzene 10.0 ug/L1.80 101.80 U 3/10/17 17:323/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 5.00 ug/L0.940 100.940 U 3/10/17 17:323/10/17 12:25 95-50-11,2-Dichlorobenzene 5.00 ug/L0.900 100.900 U 3/10/17 17:323/10/17 12:25 107-06-21,2-Dichloroethane 5.00 ug/L1.22 101.22 U 3/10/17 17:323/10/17 12:25 78-87-51,2-Dichloropropane 5.00 ug/L0.870 10137 3/10/17 17:323/10/17 12:25 108-67-81,3,5-trimethylbenzene 5.00 ug/L0.980 100.980 U 3/10/17 17:323/10/17 12:25 541-73-11,3-Dichlorobenzene 5.00 ug/L1.33 101.33 U 3/10/17 17:323/10/17 12:25 142-28-91,3-Dichloropropane 5.00 ug/L0.670 100.670 U 3/10/17 17:323/10/17 12:25 106-46-71,4-Dichlorobenzene 2.00 ug/L0.970 100.970 U 3/10/17 17:323/10/17 12:25 590-20-72,2-Dichloropropane 200 ug/L3.78 103.78 U 3/10/17 17:323/10/17 12:25 78-93-32-Butanone (MEK) 2.00 ug/L0.880 100.880 U 3/10/17 17:323/10/17 12:25 95-49-82-Chlorotoluene 50.0 ug/L3.52 103.52 U 3/10/17 17:323/10/17 12:25 591-78-62-Hexanone 5.00 ug/L0.900 100.900 U 3/10/17 17:323/10/17 12:25 106-43-44-Chlorotoluene 5.00 ug/L0.890 1016.0 3/10/17 17:323/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 50.0 ug/L2.53 102.53 U 3/10/17 17:323/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 50.0 ug/L3.52 103.52 U 3/10/17 17:323/10/17 12:25 67-64-1Acetone 5.00 ug/L1.19 1023.8 3/10/17 17:323/10/17 12:25 71-43-2Benzene 5.00 ug/L1.32 101.32 U 3/10/17 17:323/10/17 12:25 108-86-1Bromobenzene 5.00 ug/L1.12 101.12 U 3/10/17 17:323/10/17 12:25 74-97-5Bromochloromethane 5.00 ug/L1.24 101.24 U 3/10/17 17:323/10/17 12:25 75-27-4Bromodichloromethane 20.0 ug/L1.59 101.59 U 3/10/17 17:323/10/17 12:25 75-25-2Bromoform 10.0 ug/L0.970 100.970 U 3/10/17 17:323/10/17 12:25 74-83-9Bromomethane 5.00 ug/L0.990 100.990 U 3/10/17 17:323/10/17 12:25 56-23-5Carbon Tetrachloride 5.00 ug/L1.05 101.05 U 3/10/17 17:323/10/17 12:25 108-90-7Chlorobenzene 10.0 ug/L1.77 101.77 U 3/10/17 17:323/10/17 12:25 124-48-1Chlorodibromomethane 5.00 ug/L0.420 100.420 U 3/10/17 17:323/10/17 12:25 75-00-3Chloroethane 5.00 ug/L1.72 101.72 U 3/10/17 17:323/10/17 12:25 67-66-3Chloroform 5.00 ug/L0.850 100.850 U 3/10/17 17:323/10/17 12:25 74-87-3Chloromethane 5.00 ug/L1.14 101.14 U 3/10/17 17:323/10/17 12:25 156-59-2cis-1,2-Dichloroethene 10.0 ug/L1.00 101.00 U 3/10/17 17:323/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 5.00 ug/L0.670 100.670 U 3/10/17 17:323/10/17 12:25 75-71-8Dichlorodifluoromethane Page 13 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-03 (Water) Client Sample ID: MW3 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:11 CAS # VOCs by NC Method 6200B (Continued) 500 ug/L30.0 1030.0 U 3/10/17 17:323/10/17 12:25 64-17-5Ethanol 5.00 ug/L0.920 10221 3/10/17 17:323/10/17 12:25 100-41-4Ethylbenzene 50.0 ug/L0.920 100.920 U 3/10/17 17:323/10/17 12:25 108-20-3Isopropyl Ether 5.00 ug/L0.980 1021.6 3/10/17 17:323/10/17 12:25 98-82-8isopropylbenzene 10.0 ug/L1.69 101.69 U 3/10/17 17:323/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 5.00 ug/L1.90 101.90 U 3/10/17 17:323/10/17 12:25 75-09-2Methylene Chloride 20.0 ug/L0.940 10132 3/10/17 17:323/10/17 12:25 91-20-3Naphthalene 20.0 ug/L0.600 100.600 U 3/10/17 17:323/10/17 12:25 104-51-8n-Butylbenzene 10.0 ug/L0.650 1060.9 3/10/17 17:323/10/17 12:25 103-65-1n-Propylbenzene 5.00 ug/L0.920 100.920 U 3/10/17 17:323/10/17 12:25 135-98-8Sec-Butylbenzene 5.00 ug/L0.740 1010.6 3/10/17 17:323/10/17 12:25 100-42-5Styrene 5.00 ug/L0.890 100.890 U 3/10/17 17:323/10/17 12:25 98-06-6tert-Butylbenzene 5.00 ug/L0.540 100.540 U 3/10/17 17:323/10/17 12:25 127-18-4Tetrachloroethene 5.00 ug/L0.570 10144 3/10/17 17:323/10/17 12:25 108-88-3Toluene 5.00 ug/L1.88 101.88 U 3/10/17 17:323/10/17 12:25 156-60-5trans-1,2-dichloroethene 10.0 ug/L1.10 101.10 U 3/10/17 17:323/10/17 12:25 1006-10-26trans-1,3-dichloropropene 5.00 ug/L1.39 101.39 U 3/10/17 17:323/10/17 12:25 79-01-6Trichloroethene 5.00 ug/L0.540 100.540 U 3/10/17 17:323/10/17 12:25 75-69-4Trichlorofluoromethane 10.0 ug/L7.20 107.20 U 3/10/17 17:323/10/17 12:25 108-05-4Vinyl Acetate 5.00 ug/L0.810 100.810 U 3/10/17 17:323/10/17 12:25 75-01-4Vinyl Chloride 10.0 ug/L1.76 10750 3/10/17 17:323/10/17 12:25 179601-23-1m,p-Xylenes 5.00 ug/L1.22 10365 3/10/17 17:323/10/17 12:25 95-47-6o-Xylene 10.0 ug/L1.80 101120 3/10/17 17:323/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13096%3/10/17 17:32 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13089%3/10/17 17:32 460-00-4 Surrogate: Toluene-D8 (SUR)70-13095%3/10/17 17:32 2037-26-5 Page 14 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-04 (Water) Client Sample ID: MW5 RL Dil Date Prepared Sampled: 3/8/17 12:15 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 14:593/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 U 3/10/17 14:593/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 14:593/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 14:593/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 14:593/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 14:593/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 14:593/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 14:593/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 14:593/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 14:593/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 10.103 U 3/10/17 14:593/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 14:593/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.0940 U 3/10/17 14:593/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 14:593/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 14:593/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 14:593/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 14:593/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 14:593/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 14:593/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 14:593/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 14:593/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 14:593/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 14:593/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.0900 U 3/10/17 14:593/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 10.0890 U 3/10/17 14:593/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 14:593/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 14:593/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 10.119 U 3/10/17 14:593/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 14:593/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 14:593/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 14:593/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 14:593/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 14:593/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 14:593/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 14:593/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 14:593/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 14:593/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 10.172 U 3/10/17 14:593/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 14:593/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 14:593/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 14:593/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 14:593/10/17 12:25 75-71-8Dichlorodifluoromethane Page 15 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-04 (Water) Client Sample ID: MW5 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:15 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 14:593/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 10.0920 U 3/10/17 14:593/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.0920 U 3/10/17 14:593/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 10.0980 U 3/10/17 14:593/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 10.169 U 3/10/17 14:593/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 14:593/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 10.0940 U 3/10/17 14:593/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 10.0600 U 3/10/17 14:593/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 10.0650 U 3/10/17 14:593/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.0920 U 3/10/17 14:593/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 14:593/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 14:593/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 14:593/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.0570 U 3/10/17 14:593/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 14:593/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 14:593/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 14:593/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 14:593/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 U 3/10/17 14:593/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 14:593/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 10.176 U 3/10/17 14:593/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 10.122 U 3/10/17 14:593/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 10.180 U 3/10/17 14:593/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13099%3/10/17 14:59 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13094%3/10/17 14:59 460-00-4 Surrogate: Toluene-D8 (SUR)70-13096%3/10/17 14:59 2037-26-5 Page 16 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-05 (Water) Client Sample ID: MW7 RL Dil Date Prepared Sampled: 3/8/17 12:20 CAS # VOCs by NC Method 6200B 5.00 ug/L0.900 50.900 U 3/10/17 17:053/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 2.50 ug/L0.380 50.380 U 3/10/17 17:053/10/17 12:25 71-55-61,1,1-Trichloroethane 2.50 ug/L0.350 50.350 U 3/10/17 17:053/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 2.50 ug/L0.565 50.565 U 3/10/17 17:053/10/17 12:25 79-00-51,1,2-Trichloroethane 2.50 ug/L0.605 50.605 U 3/10/17 17:053/10/17 12:25 75-34-31,1-Dichloroethane 2.50 ug/L0.520 50.520 U 3/10/17 17:053/10/17 12:25 75-35-41,1-Dichloroethene 2.50 ug/L0.300 50.300 U 3/10/17 17:053/10/17 12:25 563-58-61,1-Dichloropropene 10.0 ug/L0.590 50.590 U 3/10/17 17:053/10/17 12:25 87-61-61,2,3-Trichlorobenzene 5.00 ug/L0.690 50.690 U 3/10/17 17:053/10/17 12:25 96-18-41,2,3-Trichloropropane 5.00 ug/L0.345 50.345 U 3/10/17 17:053/10/17 12:25 120-82-11,2,4-Trichlorobenzene 2.50 ug/L0.515 5141 3/10/17 17:053/10/17 12:25 95-63-61,2,4-Trimethylbenzene 5.00 ug/L0.900 50.900 U 3/10/17 17:053/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 2.50 ug/L0.470 50.470 U 3/10/17 17:053/10/17 12:25 95-50-11,2-Dichlorobenzene 2.50 ug/L0.450 50.450 U 3/10/17 17:053/10/17 12:25 107-06-21,2-Dichloroethane 2.50 ug/L0.610 50.610 U 3/10/17 17:053/10/17 12:25 78-87-51,2-Dichloropropane 2.50 ug/L0.435 57.50 3/10/17 17:053/10/17 12:25 108-67-81,3,5-trimethylbenzene 2.50 ug/L0.490 50.490 U 3/10/17 17:053/10/17 12:25 541-73-11,3-Dichlorobenzene 2.50 ug/L0.665 50.665 U 3/10/17 17:053/10/17 12:25 142-28-91,3-Dichloropropane 2.50 ug/L0.335 50.335 U 3/10/17 17:053/10/17 12:25 106-46-71,4-Dichlorobenzene 1.00 ug/L0.485 50.485 U 3/10/17 17:053/10/17 12:25 590-20-72,2-Dichloropropane 100 ug/L1.89 51.89 U 3/10/17 17:053/10/17 12:25 78-93-32-Butanone (MEK) 1.00 ug/L0.440 50.440 U 3/10/17 17:053/10/17 12:25 95-49-82-Chlorotoluene 25.0 ug/L1.76 51.76 U 3/10/17 17:053/10/17 12:25 591-78-62-Hexanone 2.50 ug/L0.450 50.450 U 3/10/17 17:053/10/17 12:25 106-43-44-Chlorotoluene 2.50 ug/L0.445 57.05 3/10/17 17:053/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 25.0 ug/L1.26 51.26 U 3/10/17 17:053/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 25.0 ug/L1.76 51.76 U 3/10/17 17:053/10/17 12:25 67-64-1Acetone 2.50 ug/L0.595 598.8 3/10/17 17:053/10/17 12:25 71-43-2Benzene 2.50 ug/L0.660 50.660 U 3/10/17 17:053/10/17 12:25 108-86-1Bromobenzene 2.50 ug/L0.560 50.560 U 3/10/17 17:053/10/17 12:25 74-97-5Bromochloromethane 2.50 ug/L0.620 50.620 U 3/10/17 17:053/10/17 12:25 75-27-4Bromodichloromethane 10.0 ug/L0.795 50.795 U 3/10/17 17:053/10/17 12:25 75-25-2Bromoform 5.00 ug/L0.485 50.485 U 3/10/17 17:053/10/17 12:25 74-83-9Bromomethane 2.50 ug/L0.495 50.495 U 3/10/17 17:053/10/17 12:25 56-23-5Carbon Tetrachloride 2.50 ug/L0.525 50.525 U 3/10/17 17:053/10/17 12:25 108-90-7Chlorobenzene 5.00 ug/L0.885 50.885 U 3/10/17 17:053/10/17 12:25 124-48-1Chlorodibromomethane 2.50 ug/L0.210 50.210 U 3/10/17 17:053/10/17 12:25 75-00-3Chloroethane 2.50 ug/L0.860 51.20 J 3/10/17 17:053/10/17 12:25 67-66-3Chloroform 2.50 ug/L0.425 50.425 U 3/10/17 17:053/10/17 12:25 74-87-3Chloromethane 2.50 ug/L0.570 50.570 U 3/10/17 17:053/10/17 12:25 156-59-2cis-1,2-Dichloroethene 5.00 ug/L0.500 50.500 U 3/10/17 17:053/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 2.50 ug/L0.335 50.335 U 3/10/17 17:053/10/17 12:25 75-71-8Dichlorodifluoromethane Page 17 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-05 (Water) Client Sample ID: MW7 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:20 CAS # VOCs by NC Method 6200B (Continued) 250 ug/L15.0 515.0 U 3/10/17 17:053/10/17 12:25 64-17-5Ethanol 2.50 ug/L0.460 5334 3/10/17 17:053/10/17 12:25 100-41-4Ethylbenzene 25.0 ug/L0.460 50.460 U 3/10/17 17:053/10/17 12:25 108-20-3Isopropyl Ether 2.50 ug/L0.490 520.4 3/10/17 17:053/10/17 12:25 98-82-8isopropylbenzene 5.00 ug/L0.845 53.55 J 3/10/17 17:053/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 2.50 ug/L0.950 50.950 U 3/10/17 17:053/10/17 12:25 75-09-2Methylene Chloride 10.0 ug/L0.470 5124 3/10/17 17:053/10/17 12:25 91-20-3Naphthalene 10.0 ug/L0.300 58.85 J 3/10/17 17:053/10/17 12:25 104-51-8n-Butylbenzene 5.00 ug/L0.325 556.5 3/10/17 17:053/10/17 12:25 103-65-1n-Propylbenzene 2.50 ug/L0.460 50.460 U 3/10/17 17:053/10/17 12:25 135-98-8Sec-Butylbenzene 2.50 ug/L0.370 55.20 3/10/17 17:053/10/17 12:25 100-42-5Styrene 2.50 ug/L0.445 50.445 U 3/10/17 17:053/10/17 12:25 98-06-6tert-Butylbenzene 2.50 ug/L0.270 50.270 U 3/10/17 17:053/10/17 12:25 127-18-4Tetrachloroethene 2.50 ug/L0.285 529.5 3/10/17 17:053/10/17 12:25 108-88-3Toluene 2.50 ug/L0.940 50.940 U 3/10/17 17:053/10/17 12:25 156-60-5trans-1,2-dichloroethene 5.00 ug/L0.550 50.550 U 3/10/17 17:053/10/17 12:25 1006-10-26trans-1,3-dichloropropene 2.50 ug/L0.695 50.695 U 3/10/17 17:053/10/17 12:25 79-01-6Trichloroethene 2.50 ug/L0.270 50.270 U 3/10/17 17:053/10/17 12:25 75-69-4Trichlorofluoromethane 5.00 ug/L3.60 53.60 U 3/10/17 17:053/10/17 12:25 108-05-4Vinyl Acetate 2.50 ug/L0.405 50.405 U 3/10/17 17:053/10/17 12:25 75-01-4Vinyl Chloride 5.00 ug/L0.880 5121 3/10/17 17:053/10/17 12:25 179601-23-1m,p-Xylenes 2.50 ug/L0.610 5152 3/10/17 17:053/10/17 12:25 95-47-6o-Xylene 5.00 ug/L0.900 5273 3/10/17 17:053/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13098%3/10/17 17:05 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13091%3/10/17 17:05 460-00-4 Surrogate: Toluene-D8 (SUR)70-13094%3/10/17 17:05 2037-26-5 Page 18 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-06 (Water) Client Sample ID: MW14 RL Dil Date Prepared Sampled: 3/8/17 12:24 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 15:243/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 U 3/10/17 15:243/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 15:243/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 15:243/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 15:243/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 15:243/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 15:243/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 15:243/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 15:243/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 15:243/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 111.0 3/10/17 15:243/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 15:243/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.110 J 3/10/17 15:243/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 15:243/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 15:243/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 15:243/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 15:243/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 15:243/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 15:243/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 15:243/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 15:243/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 15:243/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 15:243/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.190 J 3/10/17 15:243/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 11.53 3/10/17 15:243/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 15:243/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 15:243/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 130.9 3/10/17 15:243/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 15:243/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 15:243/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 15:243/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 15:243/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 15:243/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 15:243/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 15:243/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 15:243/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 15:243/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 16.66 3/10/17 15:243/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 15:243/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 15:243/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 15:243/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 15:243/10/17 12:25 75-71-8Dichlorodifluoromethane Page 19 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-06 (Water) Client Sample ID: MW14 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:24 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 15:243/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 13.14 3/10/17 15:243/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.200 J 3/10/17 15:243/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 11.49 3/10/17 15:243/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 14.56 3/10/17 15:243/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 15:243/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 125.6 3/10/17 15:243/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 11.69 J 3/10/17 15:243/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 11.20 3/10/17 15:243/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.530 3/10/17 15:243/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 15:243/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 15:243/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 15:243/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.0570 U 3/10/17 15:243/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 15:243/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 15:243/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 15:243/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 15:243/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 U 3/10/17 15:243/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 15:243/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 16.08 3/10/17 15:243/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 13.45 3/10/17 15:243/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 19.53 3/10/17 15:243/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-130100%3/10/17 15:24 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13087%3/10/17 15:24 460-00-4 Surrogate: Toluene-D8 (SUR)70-13095%3/10/17 15:24 2037-26-5 Page 20 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-07 (Water) Client Sample ID: MW17 RL Dil Date Prepared Sampled: 3/8/17 12:28 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 16:133/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 U 3/10/17 16:133/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 16:133/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 16:133/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 16:133/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 16:133/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 16:133/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 16:133/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 16:133/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 16:133/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 10.103 U 3/10/17 16:133/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 16:133/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.0940 U 3/10/17 16:133/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 16:133/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 16:133/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 16:133/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 16:133/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 16:133/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 16:133/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 16:133/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 16:133/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 16:133/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 16:133/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.0900 U 3/10/17 16:133/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 10.0890 U 3/10/17 16:133/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 16:133/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 16:133/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 10.160 J 3/10/17 16:133/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 16:133/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 16:133/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 16:133/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 16:133/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 16:133/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 16:133/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 16:133/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 16:133/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 16:133/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 10.172 U 3/10/17 16:133/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 16:133/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 16:133/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 16:133/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 16:133/10/17 12:25 75-71-8Dichlorodifluoromethane Page 21 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-07 (Water) Client Sample ID: MW17 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:28 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 16:133/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 18.40 3/10/17 16:133/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.0920 U 3/10/17 16:133/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 12.17 3/10/17 16:133/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 13.30 3/10/17 16:133/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 16:133/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 17.48 3/10/17 16:133/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 11.34 J 3/10/17 16:133/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 13.49 3/10/17 16:133/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.0920 U 3/10/17 16:133/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 16:133/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 16:133/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 16:133/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.100 J 3/10/17 16:133/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 16:133/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 16:133/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 16:133/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 16:133/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 U 3/10/17 16:133/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 16:133/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 10.176 U 3/10/17 16:133/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 10.122 U 3/10/17 16:133/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 10.180 U 3/10/17 16:133/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13095%3/10/17 16:13 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13095%3/10/17 16:13 460-00-4 Surrogate: Toluene-D8 (SUR)70-13096%3/10/17 16:13 2037-26-5 Page 22 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-08 (Water) Client Sample ID: MW18 RL Dil Date Prepared Sampled: 3/8/17 12:33 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 16:373/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 U 3/10/17 16:373/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 16:373/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 16:373/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 16:373/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 16:373/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 16:373/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 16:373/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 16:373/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 16:373/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 10.103 U 3/10/17 16:373/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 16:373/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.0940 U 3/10/17 16:373/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 16:373/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 16:373/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 16:373/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 16:373/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 16:373/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 16:373/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 16:373/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 16:373/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 16:373/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 16:373/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.0900 U 3/10/17 16:373/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 10.0890 U 3/10/17 16:373/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 16:373/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 16:373/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 10.119 U 3/10/17 16:373/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 16:373/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 16:373/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 16:373/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 16:373/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 16:373/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 16:373/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 16:373/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 16:373/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 16:373/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 10.172 U 3/10/17 16:373/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 16:373/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 16:373/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 16:373/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 16:373/10/17 12:25 75-71-8Dichlorodifluoromethane Page 23 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-08 (Water) Client Sample ID: MW18 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:33 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 16:373/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 10.0920 U 3/10/17 16:373/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.0920 U 3/10/17 16:373/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 10.0980 U 3/10/17 16:373/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 10.169 U 3/10/17 16:373/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 16:373/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 10.0940 U 3/10/17 16:373/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 10.0600 U 3/10/17 16:373/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 10.0650 U 3/10/17 16:373/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.0920 U 3/10/17 16:373/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 16:373/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 16:373/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 16:373/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.0570 U 3/10/17 16:373/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 16:373/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 16:373/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 16:373/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 16:373/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 U 3/10/17 16:373/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 16:373/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 10.176 U 3/10/17 16:373/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 10.122 U 3/10/17 16:373/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 10.180 U 3/10/17 16:373/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13099%3/10/17 16:37 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13090%3/10/17 16:37 460-00-4 Surrogate: Toluene-D8 (SUR)70-13093%3/10/17 16:37 2037-26-5 Page 24 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-09 (Water) Client Sample ID: MW19 RL Dil Date Prepared Sampled: 3/8/17 12:40 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 15:483/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 U 3/10/17 15:483/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 15:483/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 15:483/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 15:483/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 15:483/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 15:483/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 15:483/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 15:483/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 15:483/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 10.103 U 3/10/17 15:483/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 15:483/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.0940 U 3/10/17 15:483/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 15:483/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 15:483/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 15:483/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 15:483/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 15:483/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 15:483/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 15:483/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 15:483/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 15:483/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 15:483/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.0900 U 3/10/17 15:483/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 10.0890 U 3/10/17 15:483/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 15:483/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 15:483/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 10.119 U 3/10/17 15:483/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 15:483/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 15:483/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 15:483/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 15:483/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 15:483/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 15:483/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 15:483/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 15:483/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 15:483/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 10.172 U 3/10/17 15:483/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 15:483/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 15:483/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 15:483/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 15:483/10/17 12:25 75-71-8Dichlorodifluoromethane Page 25 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-09 (Water) Client Sample ID: MW19 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:40 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 15:483/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 10.0920 U 3/10/17 15:483/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.0920 U 3/10/17 15:483/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 10.0980 U 3/10/17 15:483/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 10.380 J 3/10/17 15:483/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 15:483/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 12.53 3/10/17 15:483/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 10.0600 U 3/10/17 15:483/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 10.0650 U 3/10/17 15:483/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.0920 U 3/10/17 15:483/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 15:483/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 15:483/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 15:483/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.0570 U 3/10/17 15:483/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 15:483/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 15:483/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 15:483/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 15:483/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 U 3/10/17 15:483/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 15:483/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 10.176 U 3/10/17 15:483/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 10.122 U 3/10/17 15:483/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 10.180 U 3/10/17 15:483/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-13096%3/10/17 15:48 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13089%3/10/17 15:48 460-00-4 Surrogate: Toluene-D8 (SUR)70-13095%3/10/17 15:48 2037-26-5 Page 26 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-10 (Water) Client Sample ID: MW22 RL Dil Date Prepared Sampled: 3/8/17 12:45 CAS # VOCs by NC Method 6200B 1.00 ug/L0.180 10.180 U 3/10/17 14:353/10/17 12:25 630-20-61,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 10.0760 XU 3/10/17 14:353/10/17 12:25 71-55-61,1,1-Trichloroethane 0.500 ug/L0.0700 10.0700 U 3/10/17 14:353/10/17 12:25 79-34-51,1,2,2-Tetrachloroethane 0.500 ug/L0.113 10.113 U 3/10/17 14:353/10/17 12:25 79-00-51,1,2-Trichloroethane 0.500 ug/L0.121 10.121 U 3/10/17 14:353/10/17 12:25 75-34-31,1-Dichloroethane 0.500 ug/L0.104 10.104 U 3/10/17 14:353/10/17 12:25 75-35-41,1-Dichloroethene 0.500 ug/L0.0600 10.0600 U 3/10/17 14:353/10/17 12:25 563-58-61,1-Dichloropropene 2.00 ug/L0.118 10.118 U 3/10/17 14:353/10/17 12:25 87-61-61,2,3-Trichlorobenzene 1.00 ug/L0.138 10.138 U 3/10/17 14:353/10/17 12:25 96-18-41,2,3-Trichloropropane 1.00 ug/L0.0690 10.0690 U 3/10/17 14:353/10/17 12:25 120-82-11,2,4-Trichlorobenzene 0.500 ug/L0.103 10.103 U 3/10/17 14:353/10/17 12:25 95-63-61,2,4-Trimethylbenzene 1.00 ug/L0.180 10.180 U 3/10/17 14:353/10/17 12:25 106-93-41,2-Dibromoethane (EDB) 0.500 ug/L0.0940 10.0940 U 3/10/17 14:353/10/17 12:25 95-50-11,2-Dichlorobenzene 0.500 ug/L0.0900 10.0900 U 3/10/17 14:353/10/17 12:25 107-06-21,2-Dichloroethane 0.500 ug/L0.122 10.122 U 3/10/17 14:353/10/17 12:25 78-87-51,2-Dichloropropane 0.500 ug/L0.0870 10.0870 U 3/10/17 14:353/10/17 12:25 108-67-81,3,5-trimethylbenzene 0.500 ug/L0.0980 10.0980 U 3/10/17 14:353/10/17 12:25 541-73-11,3-Dichlorobenzene 0.500 ug/L0.133 10.133 U 3/10/17 14:353/10/17 12:25 142-28-91,3-Dichloropropane 0.500 ug/L0.0670 10.0670 U 3/10/17 14:353/10/17 12:25 106-46-71,4-Dichlorobenzene 0.200 ug/L0.0970 10.0970 U 3/10/17 14:353/10/17 12:25 590-20-72,2-Dichloropropane 20.0 ug/L0.378 10.378 U 3/10/17 14:353/10/17 12:25 78-93-32-Butanone (MEK) 0.200 ug/L0.0880 10.0880 U 3/10/17 14:353/10/17 12:25 95-49-82-Chlorotoluene 5.00 ug/L0.352 10.352 U 3/10/17 14:353/10/17 12:25 591-78-62-Hexanone 0.500 ug/L0.0900 10.0900 U 3/10/17 14:353/10/17 12:25 106-43-44-Chlorotoluene 0.500 ug/L0.0890 10.0890 U 3/10/17 14:353/10/17 12:25 99-87-64-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 10.253 U 3/10/17 14:353/10/17 12:25 108-10-14-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 10.352 U 3/10/17 14:353/10/17 12:25 67-64-1Acetone 0.500 ug/L0.119 10.119 U 3/10/17 14:353/10/17 12:25 71-43-2Benzene 0.500 ug/L0.132 10.132 U 3/10/17 14:353/10/17 12:25 108-86-1Bromobenzene 0.500 ug/L0.112 10.112 U 3/10/17 14:353/10/17 12:25 74-97-5Bromochloromethane 0.500 ug/L0.124 10.124 U 3/10/17 14:353/10/17 12:25 75-27-4Bromodichloromethane 2.00 ug/L0.159 10.159 U 3/10/17 14:353/10/17 12:25 75-25-2Bromoform 1.00 ug/L0.0970 10.0970 U 3/10/17 14:353/10/17 12:25 74-83-9Bromomethane 0.500 ug/L0.0990 10.0990 U 3/10/17 14:353/10/17 12:25 56-23-5Carbon Tetrachloride 0.500 ug/L0.105 10.105 U 3/10/17 14:353/10/17 12:25 108-90-7Chlorobenzene 1.00 ug/L0.177 10.177 U 3/10/17 14:353/10/17 12:25 124-48-1Chlorodibromomethane 0.500 ug/L0.0420 10.0420 U 3/10/17 14:353/10/17 12:25 75-00-3Chloroethane 0.500 ug/L0.172 10.172 U 3/10/17 14:353/10/17 12:25 67-66-3Chloroform 0.500 ug/L0.0850 10.0850 U 3/10/17 14:353/10/17 12:25 74-87-3Chloromethane 0.500 ug/L0.114 10.114 U 3/10/17 14:353/10/17 12:25 156-59-2cis-1,2-Dichloroethene 1.00 ug/L0.100 10.100 U 3/10/17 14:353/10/17 12:25 10061-01-5cis-1,3-Dichloropropene 0.500 ug/L0.0670 10.0670 U 3/10/17 14:353/10/17 12:25 75-71-8Dichlorodifluoromethane Page 27 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: L7C0151-10 (Water) Client Sample ID: MW22 (Continued) RL Dil Date Prepared Sampled: 3/8/17 12:45 CAS # VOCs by NC Method 6200B (Continued) 50.0 ug/L3.00 13.00 U 3/10/17 14:353/10/17 12:25 64-17-5Ethanol 0.500 ug/L0.0920 10.0920 U 3/10/17 14:353/10/17 12:25 100-41-4Ethylbenzene 5.00 ug/L0.0920 10.0920 U 3/10/17 14:353/10/17 12:25 108-20-3Isopropyl Ether 0.500 ug/L0.0980 10.0980 U 3/10/17 14:353/10/17 12:25 98-82-8isopropylbenzene 1.00 ug/L0.169 10.169 U 3/10/17 14:353/10/17 12:25 1634-04-4Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 10.190 U 3/10/17 14:353/10/17 12:25 75-09-2Methylene Chloride 2.00 ug/L0.0940 10.0940 U 3/10/17 14:353/10/17 12:25 91-20-3Naphthalene 2.00 ug/L0.0600 11.18 J 3/10/17 14:353/10/17 12:25 104-51-8n-Butylbenzene 1.00 ug/L0.0650 10.0650 U 3/10/17 14:353/10/17 12:25 103-65-1n-Propylbenzene 0.500 ug/L0.0920 10.0920 U 3/10/17 14:353/10/17 12:25 135-98-8Sec-Butylbenzene 0.500 ug/L0.0740 10.0740 U 3/10/17 14:353/10/17 12:25 100-42-5Styrene 0.500 ug/L0.0890 10.0890 U 3/10/17 14:353/10/17 12:25 98-06-6tert-Butylbenzene 0.500 ug/L0.0540 10.0540 U 3/10/17 14:353/10/17 12:25 127-18-4Tetrachloroethene 0.500 ug/L0.0570 10.0570 U 3/10/17 14:353/10/17 12:25 108-88-3Toluene 0.500 ug/L0.188 10.188 U 3/10/17 14:353/10/17 12:25 156-60-5trans-1,2-dichloroethene 1.00 ug/L0.110 10.110 U 3/10/17 14:353/10/17 12:25 1006-10-26trans-1,3-dichloropropene 0.500 ug/L0.139 10.139 U 3/10/17 14:353/10/17 12:25 79-01-6Trichloroethene 0.500 ug/L0.0540 10.0540 U 3/10/17 14:353/10/17 12:25 75-69-4Trichlorofluoromethane 1.00 ug/L0.720 10.720 XU 3/10/17 14:353/10/17 12:25 108-05-4Vinyl Acetate 0.500 ug/L0.0810 10.0810 U 3/10/17 14:353/10/17 12:25 75-01-4Vinyl Chloride 1.00 ug/L0.176 10.176 U 3/10/17 14:353/10/17 12:25 179601-23-1m,p-Xylenes 0.500 ug/L0.122 10.122 U 3/10/17 14:353/10/17 12:25 95-47-6o-Xylene 1.00 ug/L0.180 10.180 U 3/10/17 14:353/10/17 12:25 1330-20-7Total Xylenes Surrogate: 1,2-Dichloroethane-D4 (SUR)70-130100%3/10/17 14:35 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)70-13092%3/10/17 14:35 460-00-4 Surrogate: Toluene-D8 (SUR)70-13096%3/10/17 14:35 2037-26-5 Page 28 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control VOCs by NC Method 6200B MDL Batch: B7C0234 Prepared & Analyzed: 3/10/2017Blank (B7C0234-BLK1) 1.00 ug/L0.180 U 0.1801,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 U 0.07601,1,1-Trichloroethane 0.500 ug/L0.0700 U 0.07001,1,2,2-Tetrachloroethane 0.500 ug/L0.113 U 0.1131,1,2-Trichloroethane 0.500 ug/L0.121 U 0.1211,1-Dichloroethane 0.500 ug/L0.104 U 0.1041,1-Dichloroethene 0.500 ug/L0.0600 U 0.06001,1-Dichloropropene 2.00 ug/L0.118 U 0.1181,2,3-Trichlorobenzene 1.00 ug/L0.138 U 0.1381,2,3-Trichloropropane 1.00 ug/L0.0690 U 0.06901,2,4-Trichlorobenzene 0.500 ug/L0.103 U 0.1031,2,4-Trimethylbenzene 1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB) 0.500 ug/L0.0940 U 0.09401,2-Dichlorobenzene 0.500 ug/L0.0900 U 0.09001,2-Dichloroethane 0.500 ug/L0.122 U 0.1221,2-Dichloropropane 0.500 ug/L0.0870 U 0.08701,3,5-trimethylbenzene 0.500 ug/L0.0980 U 0.09801,3-Dichlorobenzene 0.500 ug/L0.133 U 0.1331,3-Dichloropropane 0.500 ug/L0.0670 U 0.06701,4-Dichlorobenzene 0.200 ug/L0.0970 U 0.09702,2-Dichloropropane 20.0 ug/L0.378 U 0.3782-Butanone (MEK) 0.200 ug/L0.0880 U 0.08802-Chlorotoluene 5.00 ug/L0.352 U 0.3522-Hexanone 0.500 ug/L0.0900 U 0.09004-Chlorotoluene 0.500 ug/L0.0890 U 0.08904-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 U 0.2534-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 U 0.352Acetone 0.500 ug/L0.119 U 0.119Benzene 0.500 ug/L0.132 U 0.132Bromobenzene 0.500 ug/L0.112 U 0.112Bromochloromethane 0.500 ug/L0.124 U 0.124Bromodichloromethane 2.00 ug/L0.159 U 0.159Bromoform 1.00 ug/L0.0970 U 0.0970Bromomethane 0.500 ug/L0.0990 U 0.0990Carbon Tetrachloride 0.500 ug/L0.105 U 0.105Chlorobenzene 1.00 ug/L0.177 U 0.177Chlorodibromomethane 0.500 ug/L0.0420 U 0.0420Chloroethane 0.500 ug/L0.172 U 0.172Chloroform 0.500 ug/L0.0850 U 0.0850Chloromethane 0.500 ug/L0.114 U 0.114cis-1,2-Dichloroethene 1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene Page 29 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017Blank (B7C0234-BLK1) 0.500 ug/L0.0670 U 0.0670Dichlorodifluoromethane 50.0 ug/L3.00 U 3.00Ethanol 0.500 ug/L0.0920 U 0.0920Ethylbenzene 5.00 ug/L0.0920 U 0.0920Isopropyl Ether 0.500 ug/L0.0980 U 0.0980isopropylbenzene 1.00 ug/L0.169 U 0.169Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 U 0.190Methylene Chloride 2.00 ug/L0.0940 U 0.0940Naphthalene 2.00 ug/L0.0600 U 0.0600n-Butylbenzene 1.00 ug/L0.0650 U 0.0650n-Propylbenzene 0.500 ug/L0.0920 U 0.0920Sec-Butylbenzene 0.500 ug/L0.0740 U 0.0740Styrene 0.500 ug/L0.0890 U 0.0890tert-Butylbenzene 0.500 ug/L0.0540 U 0.0540Tetrachloroethene 0.500 ug/L0.0570 U 0.0570Toluene 0.500 ug/L0.188 U 0.188trans-1,2-dichloroethene 1.00 ug/L0.110 U 0.110trans-1,3-dichloropropene 0.500 ug/L0.139 U 0.139Trichloroethene 0.500 ug/L0.0540 U 0.0540Trichlorofluoromethane 1.00 ug/L0.720 U 0.720Vinyl Acetate 0.500 ug/L0.0810 U 0.0810Vinyl Chloride 1.00 ug/L0.176 U 0.176m,p-Xylenes 0.500 ug/L0.122 U 0.122o-Xylene 1.00 ug/L0.180 U 0.180Total Xylenes 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)10025.0 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)8922.2 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9523.8 ug/L Page 30 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017LCS (B7C0234-BS1) 1.00 25.0 70-13093ug/L23.3 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 70-130114ug/L28.6 0.07601,1,1-Trichloroethane 0.500 25.0 70-13080ug/L20.0 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 70-13091ug/L22.8 0.1131,1,2-Trichloroethane 0.500 25.0 70-13093ug/L23.2 0.1211,1-Dichloroethane 0.500 25.0 70-130103ug/L25.7 0.1041,1-Dichloroethene 0.500 25.0 70-130104ug/L26.0 0.06001,1-Dichloropropene 2.00 25.0 70-13086ug/L21.4 0.1181,2,3-Trichlorobenzene 1.00 25.0 70-13075ug/L18.9 0.1381,2,3-Trichloropropane 1.00 25.0 70-13090ug/L22.5 0.06901,2,4-Trichlorobenzene 0.500 25.0 70-130102ug/L25.5 0.1031,2,4-Trimethylbenzene 1.00 25.0 70-13092ug/L22.9 0.1801,2-Dibromoethane (EDB) 0.500 25.0 70-13095ug/L23.7 0.09401,2-Dichlorobenzene 0.500 25.0 70-13080ug/L20.0 0.09001,2-Dichloroethane 0.500 25.0 70-13091ug/L22.7 0.1221,2-Dichloropropane 0.500 25.0 70-130105ug/L26.1 0.08701,3,5-trimethylbenzene 0.500 25.0 70-13098ug/L24.4 0.09801,3-Dichlorobenzene 0.500 25.0 70-13090ug/L22.6 0.1331,3-Dichloropropane 0.500 25.0 70-130100ug/L24.9 0.06701,4-Dichlorobenzene 0.200 25.0 70-130122ug/L30.4 0.09702,2-Dichloropropane 20.0 50.0 70-13072ug/L36.0 0.3782-Butanone (MEK) 0.200 25.0 70-13093ug/L23.3 0.08802-Chlorotoluene 5.00 50.0 70-13076ug/L38.2 0.3522-Hexanone 0.500 25.0 70-13095ug/L23.8 0.09004-Chlorotoluene 0.500 25.0 70-13098ug/L24.4 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 70-13070ug/L35.1 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 70-13077ug/L38.4 0.352Acetone 0.500 25.0 70-130100ug/L25.0 0.119Benzene 0.500 25.0 70-13085ug/L21.4 0.132Bromobenzene 0.500 25.0 70-13095ug/L23.8 0.112Bromochloromethane 0.500 25.0 70-130102ug/L25.5 0.124Bromodichloromethane 2.00 25.0 70-13073ug/L18.2 0.159Bromoform 1.00 25.0 60-140108ug/L26.9 0.0970Bromomethane 0.500 25.0 70-130122ug/L30.6 0.0990Carbon Tetrachloride 0.500 25.0 70-13098ug/L24.4 0.105Chlorobenzene 1.00 25.0 70-13087ug/L21.7 0.177Chlorodibromomethane 0.500 25.0 60-14095ug/L23.7 0.0420Chloroethane 0.500 25.0 70-13097ug/L24.2 0.172Chloroform 0.500 25.0 60-14082ug/L20.5 0.0850Chloromethane 0.500 25.0 70-13098ug/L24.4 0.114cis-1,2-Dichloroethene 1.00 25.0 70-13092ug/L22.9 0.100cis-1,3-Dichloropropene Page 31 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017LCS (B7C0234-BS1) 0.500 25.0 60-140106ug/L26.6 0.0670Dichlorodifluoromethane 50.0 1000 70-13092ug/L9193.00Ethanol 0.500 25.0 70-130105ug/L26.2 0.0920Ethylbenzene 5.00 25.0 70-13086ug/L21.6 0.0920Isopropyl Ether 0.500 25.0 70-13099ug/L24.8 0.0980isopropylbenzene 1.00 50.0 70-13078ug/L39.0 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 70-13099ug/L24.6 0.190Methylene Chloride 2.00 25.0 70-13073ug/L18.2 0.0940Naphthalene 2.00 25.0 70-13098ug/L24.6 0.0600n-Butylbenzene 1.00 25.0 70-130101ug/L25.2 0.0650n-Propylbenzene 0.500 25.0 70-130112ug/L27.9 0.0920Sec-Butylbenzene 0.500 25.0 70-13099ug/L24.8 0.0740Styrene 0.500 25.0 70-13097ug/L24.2 0.0890tert-Butylbenzene 0.500 25.0 70-130115ug/L28.8 0.0540Tetrachloroethene 0.500 25.0 70-13097ug/L24.1 0.0570Toluene 0.500 25.0 70-13098ug/L24.4 0.188trans-1,2-dichloroethene 1.00 25.0 70-13087ug/L21.8 0.110trans-1,3-dichloropropene 0.500 25.0 70-13090ug/L22.6 0.139Trichloroethene 0.500 25.0 60-140106ug/L26.4 0.0540Trichlorofluoromethane 1.00 25.0 70-13076ug/L19.1 0.720Vinyl Acetate 0.500 25.0 60-140100ug/L25.1 0.0810Vinyl Chloride 1.00 50.0 70-130111ug/L55.4 0.176m,p-Xylenes 0.500 25.0 70-130101ug/L25.2 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8320.9 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9122.7 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9523.8 ug/L Prepared & Analyzed: 3/10/2017LCS Dup (B7C0234-BSD1) 1.00 25.0 2070-13099 5ug/L24.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 2070-130108 6ug/L26.9 0.07601,1,1-Trichloroethane 0.500 25.0 2070-13096 18ug/L23.9 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 2070-13098 7ug/L24.5 0.1131,1,2-Trichloroethane 0.500 25.0 2070-13099 7ug/L24.8 0.1211,1-Dichloroethane 0.500 25.0 2070-130108 5ug/L27.1 0.1041,1-Dichloroethene 0.500 25.0 2070-130110 6ug/L27.5 0.06001,1-Dichloropropene 2.00 25.0 2070-13099 14ug/L24.7 0.1181,2,3-Trichlorobenzene 1.00 25.0 2070-13090 18ug/L22.6 0.1381,2,3-Trichloropropane 1.00 25.0 2070-130100 11ug/L25.0 0.06901,2,4-Trichlorobenzene 0.500 25.0 2070-130114 12ug/L28.6 0.1031,2,4-Trimethylbenzene 1.00 25.0 2070-130103 12ug/L25.8 0.1801,2-Dibromoethane (EDB) Page 32 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017LCS Dup (B7C0234-BSD1) 0.500 25.0 2070-130108 13ug/L26.9 0.09401,2-Dichlorobenzene 0.500 25.0 2070-13085 6ug/L21.2 0.09001,2-Dichloroethane 0.500 25.0 2070-13097 7ug/L24.3 0.1221,2-Dichloropropane 0.500 25.0 2070-130114 9ug/L28.6 0.08701,3,5-trimethylbenzene 0.500 25.0 2070-130109 11ug/L27.3 0.09801,3-Dichlorobenzene 0.500 25.0 2070-130101 11ug/L25.2 0.1331,3-Dichloropropane 0.500 25.0 2070-130112 11ug/L27.9 0.06701,4-Dichlorobenzene 0.200 25.0 2070-130129 6ug/L32.3 0.09702,2-Dichloropropane 20.0 50.0 2070-13080 11ug/L40.2 0.3782-Butanone (MEK) 0.200 25.0 2070-130105 12ug/L26.2 0.08802-Chlorotoluene 5.00 50.0 2070-13076 0.7ug/L38.0 0.3522-Hexanone 0.500 25.0 2070-130106 10ug/L26.4 0.09004-Chlorotoluene 0.500 25.0 2070-130108 10ug/L27.0 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 2070-13081 15ug/L40.7 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 2070-13078 2ug/L39.1 0.352Acetone 0.500 25.0 2070-130107 7ug/L26.7 0.119Benzene 0.500 25.0 2070-13098 14ug/L24.5 0.132Bromobenzene 0.500 25.0 2070-130102 7ug/L25.6 0.112Bromochloromethane 0.500 25.0 2070-130108 6ug/L27.1 0.124Bromodichloromethane 2.00 25.0 2070-13085 16ug/L21.3 0.159Bromoform 1.00 25.0 2060-140116 7ug/L28.9 0.0970Bromomethane 0.500 25.0 2070-130114 7ug/L28.6 0.0990Carbon Tetrachloride 0.500 25.0 2070-130105 7ug/L26.3 0.105Chlorobenzene 1.00 25.0 2070-13094 8ug/L23.5 0.177Chlorodibromomethane 0.500 25.0 2060-140118 22ug/L29.6 X 0.0420Chloroethane 0.500 25.0 2070-130104 7ug/L25.9 0.172Chloroform 0.500 25.0 2060-14086 5ug/L21.4 0.0850Chloromethane 0.500 25.0 2070-130106 8ug/L26.4 0.114cis-1,2-Dichloroethene 1.00 25.0 2070-13099 8ug/L24.8 0.100cis-1,3-Dichloropropene 0.500 25.0 2060-140109 2ug/L27.1 0.0670Dichlorodifluoromethane 50.0 1000 2070-13091 0.5ug/L9143.00Ethanol 0.500 25.0 2070-130112 6ug/L28.0 0.0920Ethylbenzene 5.00 25.0 2070-13093 7ug/L23.2 0.0920Isopropyl Ether 0.500 25.0 2070-130109 9ug/L27.3 0.0980isopropylbenzene 1.00 50.0 2070-13088 12ug/L43.8 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 2070-130106 7ug/L26.6 0.190Methylene Chloride 2.00 25.0 2070-13086 16ug/L21.4 0.0940Naphthalene 2.00 25.0 2070-130109 10ug/L27.2 0.0600n-Butylbenzene 1.00 25.0 2070-130114 12ug/L28.4 0.0650n-Propylbenzene 0.500 25.0 2070-130124 10ug/L30.9 0.0920Sec-Butylbenzene 0.500 25.0 2070-130106 7ug/L26.6 0.0740Styrene Page 33 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017LCS Dup (B7C0234-BSD1) 0.500 25.0 2070-130109 12ug/L27.3 0.0890tert-Butylbenzene 0.500 25.0 2070-130121 5ug/L30.3 0.0540Tetrachloroethene 0.500 25.0 2070-130103 7ug/L25.8 0.0570Toluene 0.500 25.0 2070-130103 5ug/L25.7 0.188trans-1,2-dichloroethene 1.00 25.0 2070-13094 7ug/L23.5 0.110trans-1,3-dichloropropene 0.500 25.0 2070-13096 6ug/L24.0 0.139Trichloroethene 0.500 25.0 2060-140112 5ug/L27.9 0.0540Trichlorofluoromethane 1.00 25.0 2070-13083 9ug/L20.9 0.720Vinyl Acetate 0.500 25.0 2060-140103 2ug/L25.7 0.0810Vinyl Chloride 1.00 50.0 2070-130119 7ug/L59.3 0.176m,p-Xylenes 0.500 25.0 2070-130108 7ug/L26.9 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8421.0 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9122.7 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9323.3 ug/L Prepared & Analyzed: 3/10/2017Source: L7C0151-10Matrix Spike (B7C0234-MS1) 1.00 25.0 ND 70-13094ug/L23.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 70-130117ug/L29.2 0.07601,1,1-Trichloroethane 0.500 25.0 ND 70-13098ug/L24.5 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 70-13098ug/L24.4 0.1131,1,2-Trichloroethane 0.500 25.0 ND 70-13099ug/L24.7 0.1211,1-Dichloroethane 0.500 25.0 ND 70-130107ug/L26.8 0.1041,1-Dichloroethene 0.500 25.0 ND 70-130107ug/L26.7 0.06001,1-Dichloropropene 2.00 25.0 ND 70-13097ug/L24.3 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 70-13091ug/L22.8 0.1381,2,3-Trichloropropane 1.00 25.0 ND 70-13099ug/L24.9 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 70-130124ug/L31.0 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 70-130101ug/L25.2 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 70-130105ug/L26.3 0.09401,2-Dichlorobenzene 0.500 25.0 ND 70-13083ug/L20.8 0.09001,2-Dichloroethane 0.500 25.0 ND 70-13095ug/L23.8 0.1221,2-Dichloropropane 0.500 25.0 ND 70-130115ug/L28.6 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 70-130106ug/L26.5 0.09801,3-Dichlorobenzene 0.500 25.0 ND 70-13099ug/L24.8 0.1331,3-Dichloropropane 0.500 25.0 ND 70-130108ug/L27.1 0.06701,4-Dichlorobenzene 0.200 25.0 ND 70-130111ug/L27.8 0.09702,2-Dichloropropane 20.0 50.0 ND 70-13081ug/L40.5 0.3782-Butanone (MEK) 0.200 25.0 ND 70-130106ug/L26.4 0.08802-Chlorotoluene 5.00 50.0 ND 70-13077ug/L38.4 0.3522-Hexanone 0.500 25.0 ND 70-130103ug/L25.8 0.09004-Chlorotoluene Page 34 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017Source: L7C0151-10Matrix Spike (B7C0234-MS1) 0.500 25.0 ND 70-130105ug/L26.3 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 70-13082ug/L40.8 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 70-13082ug/L41.2 0.352Acetone 0.500 25.0 ND 70-130103ug/L25.7 0.119Benzene 0.500 25.0 ND 70-13095ug/L23.8 0.132Bromobenzene 0.500 25.0 ND 70-130104ug/L25.9 0.112Bromochloromethane 0.500 25.0 ND 70-130103ug/L25.7 0.124Bromodichloromethane 2.00 25.0 ND 70-13079ug/L19.7 0.159Bromoform 1.00 25.0 ND 60-140106ug/L26.4 0.0970Bromomethane 0.500 25.0 ND 70-130109ug/L27.2 0.0990Carbon Tetrachloride 0.500 25.0 ND 70-130101ug/L25.2 0.105Chlorobenzene 1.00 25.0 ND 70-13086ug/L21.5 0.177Chlorodibromomethane 0.500 25.0 ND 60-140137ug/L34.3 0.0420Chloroethane 0.500 25.0 ND 70-130101ug/L25.3 0.172Chloroform 0.500 25.0 ND 60-14085ug/L21.2 0.0850Chloromethane 0.500 25.0 ND 70-130103ug/L25.7 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 70-13091ug/L22.8 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 60-140110ug/L27.6 0.0670Dichlorodifluoromethane 50.0 1000 ND 70-13083ug/L8263.00Ethanol 0.500 25.0 ND 70-130113ug/L28.2 0.0920Ethylbenzene 5.00 25.0 ND 70-13093ug/L23.3 0.0920Isopropyl Ether 0.500 25.0 ND 70-130110ug/L27.5 0.0980isopropylbenzene 1.00 50.0 ND 70-13088ug/L43.9 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 70-130104ug/L26.1 0.190Methylene Chloride 2.00 25.0 ND 70-13092ug/L23.0 0.0940Naphthalene 2.00 25.0 1.18 70-13099ug/L25.9 0.0600n-Butylbenzene 1.00 25.0 ND 70-130112ug/L28.1 0.0650n-Propylbenzene 0.500 25.0 ND 70-130120ug/L30.1 0.0920Sec-Butylbenzene 0.500 25.0 ND 70-130100ug/L25.1 0.0740Styrene 0.500 25.0 ND 70-130108ug/L27.0 0.0890tert-Butylbenzene 0.500 25.0 ND 70-130108ug/L27.0 0.0540Tetrachloroethene 0.500 25.0 ND 70-130102ug/L25.4 0.0570Toluene 0.500 25.0 ND 70-130103ug/L25.8 0.188trans-1,2-dichloroethene 1.00 25.0 ND 70-13088ug/L21.9 0.110trans-1,3-dichloropropene 0.500 25.0 ND 70-13092ug/L23.0 0.139Trichloroethene 0.500 25.0 ND 60-140112ug/L28.1 0.0540Trichlorofluoromethane 1.00 25.0 ND 70-13074ug/L18.5 0.720Vinyl Acetate 0.500 25.0 ND 60-140105ug/L26.2 0.0810Vinyl Chloride 1.00 50.0 ND 70-130120ug/L60.2 0.176m,p-Xylenes 0.500 25.0 ND 70-130108ug/L27.0 0.122o-Xylene Page 35 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017Source: L7C0151-10Matrix Spike (B7C0234-MS1) 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8320.8 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9223.0 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9122.8 ug/L Prepared & Analyzed: 3/10/2017Source: L7C0151-10Matrix Spike Dup (B7C0234-MSD1) 1.00 25.0 ND 2070-13086 9ug/L21.5 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 2070-13092 24ug/L23.0 X 0.07601,1,1-Trichloroethane 0.500 25.0 ND 2070-13093 6ug/L23.1 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 2070-13091 7ug/L22.6 0.1131,1,2-Trichloroethane 0.500 25.0 ND 2070-13085 14ug/L21.4 0.1211,1-Dichloroethane 0.500 25.0 ND 2070-13090 17ug/L22.6 0.1041,1-Dichloroethene 0.500 25.0 ND 2070-13096 11ug/L24.0 0.06001,1-Dichloropropene 2.00 25.0 ND 2070-13091 7ug/L22.7 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 2070-13086 6ug/L21.4 0.1381,2,3-Trichloropropane 1.00 25.0 ND 2070-13092 7ug/L23.1 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 2070-130107 15ug/L26.6 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 2070-13092 9ug/L23.0 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 2070-13097 8ug/L24.2 0.09401,2-Dichlorobenzene 0.500 25.0 ND 2070-13076 9ug/L19.0 0.09001,2-Dichloroethane 0.500 25.0 ND 2070-13089 7ug/L22.2 0.1221,2-Dichloropropane 0.500 25.0 ND 2070-130102 12ug/L25.5 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 2070-13096 10ug/L24.0 0.09801,3-Dichlorobenzene 0.500 25.0 ND 2070-13091 8ug/L22.8 0.1331,3-Dichloropropane 0.500 25.0 ND 2070-13099 9ug/L24.8 0.06701,4-Dichlorobenzene 0.200 25.0 ND 2070-13097 13ug/L24.4 0.09702,2-Dichloropropane 20.0 50.0 ND 2070-13075 8ug/L37.5 0.3782-Butanone (MEK) 0.200 25.0 ND 2070-13094 11ug/L23.6 0.08802-Chlorotoluene 5.00 50.0 ND 2070-13074 4ug/L36.8 0.3522-Hexanone 0.500 25.0 ND 2070-13094 9ug/L23.6 0.09004-Chlorotoluene 0.500 25.0 ND 2070-13095 10ug/L23.8 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 2070-13078 4ug/L39.1 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 2070-13077 7ug/L38.3 0.352Acetone 0.500 25.0 ND 2070-13092 11ug/L22.9 0.119Benzene 0.500 25.0 ND 2070-13089 7ug/L22.3 0.132Bromobenzene 0.500 25.0 ND 2070-13091 12ug/L22.9 0.112Bromochloromethane 0.500 25.0 ND 2070-13094 9ug/L23.6 0.124Bromodichloromethane 2.00 25.0 ND 2070-13075 5ug/L18.8 0.159Bromoform 1.00 25.0 ND 2060-14098 7ug/L24.5 0.0970Bromomethane 0.500 25.0 ND 2070-13096 13ug/L23.9 0.0990Carbon Tetrachloride 0.500 25.0 ND 2070-13091 11ug/L22.7 0.105Chlorobenzene Page 36 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0234 (Continued) Prepared & Analyzed: 3/10/2017Source: L7C0151-10Matrix Spike Dup (B7C0234-MSD1) 1.00 25.0 ND 2070-13083 4ug/L20.6 0.177Chlorodibromomethane 0.500 25.0 ND 2060-140114 18ug/L28.5 0.0420Chloroethane 0.500 25.0 ND 2070-13090 11ug/L22.6 0.172Chloroform 0.500 25.0 ND 2060-14074 14ug/L18.5 0.0850Chloromethane 0.500 25.0 ND 2070-13091 12ug/L22.8 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 2070-13083 9ug/L20.8 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 2060-14093 18ug/L23.2 0.0670Dichlorodifluoromethane 50.0 1000 ND 2070-13074 11ug/L7393.00Ethanol 0.500 25.0 ND 2070-13099 13ug/L24.8 0.0920Ethylbenzene 5.00 25.0 ND 2070-13082 13ug/L20.6 0.0920Isopropyl Ether 0.500 25.0 ND 2070-13098 12ug/L24.4 0.0980isopropylbenzene 1.00 50.0 ND 2070-13080 9ug/L40.1 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 2070-13092 13ug/L23.0 0.190Methylene Chloride 2.00 25.0 ND 2070-13085 7ug/L21.4 0.0940Naphthalene 2.00 25.0 1.18 2070-13088 11ug/L23.2 0.0600n-Butylbenzene 1.00 25.0 ND 2070-130100 11ug/L25.0 0.0650n-Propylbenzene 0.500 25.0 ND 2070-130108 11ug/L27.0 0.0920Sec-Butylbenzene 0.500 25.0 ND 2070-13090 11ug/L22.6 0.0740Styrene 0.500 25.0 ND 2070-13097 11ug/L24.2 0.0890tert-Butylbenzene 0.500 25.0 ND 2070-13096 12ug/L24.0 0.0540Tetrachloroethene 0.500 25.0 ND 2070-13091 11ug/L22.8 0.0570Toluene 0.500 25.0 ND 2070-13091 12ug/L22.9 0.188trans-1,2-dichloroethene 1.00 25.0 ND 2070-13081 8ug/L20.1 0.110trans-1,3-dichloropropene 0.500 25.0 ND 2070-13083 11ug/L20.7 0.139Trichloroethene 0.500 25.0 ND 2060-14096 15ug/L24.0 0.0540Trichlorofluoromethane 1.00 25.0 ND 2070-13066 11ug/L16.6 X 0.720Vinyl Acetate 0.500 25.0 ND 2060-14091 14ug/L22.7 0.0810Vinyl Chloride 1.00 50.0 ND 2070-130105 14ug/L52.4 0.176m,p-Xylenes 0.500 25.0 ND 2070-13095 13ug/L23.7 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8320.6 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9323.1 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9122.8 ug/L Page 37 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 Prepared & Analyzed: 3/16/2017Blank (B7C0316-BLK1) 1.00 ug/L0.180 U 0.1801,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 U 0.07601,1,1-Trichloroethane 0.500 ug/L0.0700 U 0.07001,1,2,2-Tetrachloroethane 0.500 ug/L0.113 U 0.1131,1,2-Trichloroethane 0.500 ug/L0.121 U 0.1211,1-Dichloroethane 0.500 ug/L0.104 U 0.1041,1-Dichloroethene 0.500 ug/L0.0600 U 0.06001,1-Dichloropropene 2.00 ug/L0.118 U 0.1181,2,3-Trichlorobenzene 1.00 ug/L0.138 U 0.1381,2,3-Trichloropropane 1.00 ug/L0.0690 U 0.06901,2,4-Trichlorobenzene 0.500 ug/L0.103 U 0.1031,2,4-Trimethylbenzene 1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB) 0.500 ug/L0.0940 U 0.09401,2-Dichlorobenzene 0.500 ug/L0.0900 U 0.09001,2-Dichloroethane 0.500 ug/L0.122 U 0.1221,2-Dichloropropane 0.500 ug/L0.0870 U 0.08701,3,5-trimethylbenzene 0.500 ug/L0.0980 U 0.09801,3-Dichlorobenzene 0.500 ug/L0.133 U 0.1331,3-Dichloropropane 0.500 ug/L0.0670 U 0.06701,4-Dichlorobenzene 0.200 ug/L0.0970 U 0.09702,2-Dichloropropane 20.0 ug/L0.378 U 0.3782-Butanone (MEK) 0.200 ug/L0.0880 U 0.08802-Chlorotoluene 5.00 ug/L0.352 U 0.3522-Hexanone 0.500 ug/L0.0900 U 0.09004-Chlorotoluene 0.500 ug/L0.0890 U 0.08904-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 U 0.2534-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 U 0.352Acetone 0.500 ug/L0.119 U 0.119Benzene 0.500 ug/L0.132 U 0.132Bromobenzene 0.500 ug/L0.112 U 0.112Bromochloromethane 0.500 ug/L0.124 U 0.124Bromodichloromethane 2.00 ug/L0.159 U 0.159Bromoform 1.00 ug/L0.0970 U 0.0970Bromomethane 0.500 ug/L0.0990 U 0.0990Carbon Tetrachloride 0.500 ug/L0.105 U 0.105Chlorobenzene 1.00 ug/L0.177 U 0.177Chlorodibromomethane 0.500 ug/L0.0420 U 0.0420Chloroethane 0.500 ug/L0.172 U 0.172Chloroform 0.500 ug/L0.0850 U 0.0850Chloromethane 0.500 ug/L0.114 U 0.114cis-1,2-Dichloroethene 1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene Page 38 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017Blank (B7C0316-BLK1) 0.500 ug/L0.0670 U 0.0670Dichlorodifluoromethane 50.0 ug/L3.00 U 3.00Ethanol 0.500 ug/L0.0920 U 0.0920Ethylbenzene 5.00 ug/L0.0920 U 0.0920Isopropyl Ether 0.500 ug/L0.0980 U 0.0980isopropylbenzene 1.00 ug/L0.169 U 0.169Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 U 0.190Methylene Chloride 2.00 ug/L0.0940 U 0.0940Naphthalene 2.00 ug/L0.0600 U 0.0600n-Butylbenzene 1.00 ug/L0.0650 U 0.0650n-Propylbenzene 0.500 ug/L0.0920 U 0.0920Sec-Butylbenzene 0.500 ug/L0.0740 U 0.0740Styrene 0.500 ug/L0.0890 U 0.0890tert-Butylbenzene 0.500 ug/L0.0540 U 0.0540Tetrachloroethene 0.500 ug/L0.0570 U 0.0570Toluene 0.500 ug/L0.188 U 0.188trans-1,2-dichloroethene 1.00 ug/L0.110 U 0.110trans-1,3-dichloropropene 0.500 ug/L0.139 U 0.139Trichloroethene 0.500 ug/L0.0540 U 0.0540Trichlorofluoromethane 1.00 ug/L0.720 U 0.720Vinyl Acetate 0.500 ug/L0.0810 U 0.0810Vinyl Chloride 1.00 ug/L0.176 U 0.176m,p-Xylenes 0.500 ug/L0.122 U 0.122o-Xylene 1.00 ug/L0.180 U 0.180Total Xylenes 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)9824.5 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9223.0 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9423.6 ug/L Page 39 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017LCS (B7C0316-BS1) 1.00 25.0 70-130102ug/L25.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 70-130107ug/L26.6 0.07601,1,1-Trichloroethane 0.500 25.0 70-13099ug/L24.8 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 70-13098ug/L24.5 0.1131,1,2-Trichloroethane 0.500 25.0 70-130109ug/L27.3 0.1211,1-Dichloroethane 0.500 25.0 70-130118ug/L29.6 0.1041,1-Dichloroethene 0.500 25.0 70-13096ug/L24.0 0.06001,1-Dichloropropene 2.00 25.0 70-13097ug/L24.2 0.1181,2,3-Trichlorobenzene 1.00 25.0 70-13093ug/L23.3 0.1381,2,3-Trichloropropane 1.00 25.0 70-13096ug/L24.1 0.06901,2,4-Trichlorobenzene 0.500 25.0 70-130111ug/L27.7 0.1031,2,4-Trimethylbenzene 1.00 25.0 70-130104ug/L25.9 0.1801,2-Dibromoethane (EDB) 0.500 25.0 70-130106ug/L26.5 0.09401,2-Dichlorobenzene 0.500 25.0 70-13084ug/L21.0 0.09001,2-Dichloroethane 0.500 25.0 70-13093ug/L23.3 0.1221,2-Dichloropropane 0.500 25.0 70-130111ug/L27.7 0.08701,3,5-trimethylbenzene 0.500 25.0 70-130105ug/L26.4 0.09801,3-Dichlorobenzene 0.500 25.0 70-13099ug/L24.8 0.1331,3-Dichloropropane 0.500 25.0 70-130109ug/L27.4 0.06701,4-Dichlorobenzene 0.200 25.0 70-130137ug/L34.3 X 0.09702,2-Dichloropropane 20.0 50.0 70-13084ug/L42.1 0.3782-Butanone (MEK) 0.200 25.0 70-130102ug/L25.4 0.08802-Chlorotoluene 5.00 50.0 70-13078ug/L39.0 0.3522-Hexanone 0.500 25.0 70-130104ug/L26.0 0.09004-Chlorotoluene 0.500 25.0 70-130103ug/L25.7 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 70-13083ug/L41.7 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 70-13095ug/L47.5 0.352Acetone 0.500 25.0 70-13099ug/L24.6 0.119Benzene 0.500 25.0 70-13096ug/L24.0 0.132Bromobenzene 0.500 25.0 70-130106ug/L26.4 0.112Bromochloromethane 0.500 25.0 70-130111ug/L27.8 0.124Bromodichloromethane 2.00 25.0 70-13090ug/L22.6 0.159Bromoform 1.00 25.0 60-14078ug/L19.4 0.0970Bromomethane 0.500 25.0 70-130117ug/L29.4 0.0990Carbon Tetrachloride 0.500 25.0 70-130102ug/L25.6 0.105Chlorobenzene 1.00 25.0 70-13099ug/L24.8 0.177Chlorodibromomethane 0.500 25.0 60-140113ug/L28.4 0.0420Chloroethane 0.500 25.0 70-130106ug/L26.4 0.172Chloroform 0.500 25.0 60-14064ug/L16.0 0.0850Chloromethane 0.500 25.0 70-130108ug/L27.0 0.114cis-1,2-Dichloroethene 1.00 25.0 70-13097ug/L24.4 0.100cis-1,3-Dichloropropene Page 40 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017LCS (B7C0316-BS1) 0.500 25.0 60-14093ug/L23.2 0.0670Dichlorodifluoromethane 50.0 1000 70-130130ug/L13003.00Ethanol 0.500 25.0 70-130107ug/L26.8 0.0920Ethylbenzene 5.00 25.0 70-130105ug/L26.2 0.0920Isopropyl Ether 0.500 25.0 70-130103ug/L25.8 0.0980isopropylbenzene 1.00 50.0 70-13097ug/L48.6 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 70-130127ug/L31.7 0.190Methylene Chloride 2.00 25.0 70-13086ug/L21.4 0.0940Naphthalene 2.00 25.0 70-130103ug/L25.9 0.0600n-Butylbenzene 1.00 25.0 70-130109ug/L27.1 0.0650n-Propylbenzene 0.500 25.0 70-130119ug/L29.7 0.0920Sec-Butylbenzene 0.500 25.0 70-130103ug/L25.8 0.0740Styrene 0.500 25.0 70-130105ug/L26.3 0.0890tert-Butylbenzene 0.500 25.0 70-130104ug/L25.9 0.0540Tetrachloroethene 0.500 25.0 70-13097ug/L24.2 0.0570Toluene 0.500 25.0 70-130108ug/L27.0 0.188trans-1,2-dichloroethene 1.00 25.0 70-13098ug/L24.5 0.110trans-1,3-dichloropropene 0.500 25.0 70-13088ug/L21.9 0.139Trichloroethene 0.500 25.0 60-140118ug/L29.6 0.0540Trichlorofluoromethane 1.00 25.0 70-13098ug/L24.6 0.720Vinyl Acetate 0.500 25.0 60-14086ug/L21.5 0.0810Vinyl Chloride 1.00 50.0 70-130114ug/L57.2 0.176m,p-Xylenes 0.500 25.0 70-130102ug/L25.6 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8822.0 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)8822.1 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9122.8 ug/L Prepared & Analyzed: 3/16/2017LCS Dup (B7C0316-BSD1) 1.00 25.0 2070-130106 4ug/L26.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 2070-130108 2ug/L27.1 0.07601,1,1-Trichloroethane 0.500 25.0 2070-130108 8ug/L26.9 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 2070-130108 10ug/L27.1 0.1131,1,2-Trichloroethane 0.500 25.0 2070-130104 5ug/L25.9 0.1211,1-Dichloroethane 0.500 25.0 2070-130121 2ug/L30.2 0.1041,1-Dichloroethene 0.500 25.0 2070-130104 8ug/L26.1 0.06001,1-Dichloropropene 2.00 25.0 2070-130105 8ug/L26.3 0.1181,2,3-Trichlorobenzene 1.00 25.0 2070-130101 8ug/L25.2 0.1381,2,3-Trichloropropane 1.00 25.0 2070-130102 6ug/L25.5 0.06901,2,4-Trichlorobenzene 0.500 25.0 2070-130117 5ug/L29.2 0.1031,2,4-Trimethylbenzene 1.00 25.0 2070-130108 4ug/L27.1 0.1801,2-Dibromoethane (EDB) Page 41 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017LCS Dup (B7C0316-BSD1) 0.500 25.0 2070-130113 6ug/L28.1 0.09401,2-Dichlorobenzene 0.500 25.0 2070-13088 5ug/L22.1 0.09001,2-Dichloroethane 0.500 25.0 2070-13097 4ug/L24.2 0.1221,2-Dichloropropane 0.500 25.0 2070-130119 7ug/L29.7 0.08701,3,5-trimethylbenzene 0.500 25.0 2070-130115 8ug/L28.7 0.09801,3-Dichlorobenzene 0.500 25.0 2070-130104 5ug/L26.1 0.1331,3-Dichloropropane 0.500 25.0 2070-130116 6ug/L29.0 0.06701,4-Dichlorobenzene 0.200 25.0 2070-130136 1ug/L34.0 X 0.09702,2-Dichloropropane 20.0 50.0 2070-13090 7ug/L45.1 0.3782-Butanone (MEK) 0.200 25.0 2070-130109 7ug/L27.2 0.08802-Chlorotoluene 5.00 50.0 2070-13082 6ug/L41.2 0.3522-Hexanone 0.500 25.0 2070-130111 6ug/L27.7 0.09004-Chlorotoluene 0.500 25.0 2070-130110 7ug/L27.4 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 2070-13089 7ug/L44.7 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 2070-130109 13ug/L54.4 0.352Acetone 0.500 25.0 2070-130103 4ug/L25.7 0.119Benzene 0.500 25.0 2070-130103 7ug/L25.7 0.132Bromobenzene 0.500 25.0 2070-130107 2ug/L26.8 0.112Bromochloromethane 0.500 25.0 2070-130116 4ug/L29.1 0.124Bromodichloromethane 2.00 25.0 2070-13096 6ug/L24.0 0.159Bromoform 1.00 25.0 2060-14088 12ug/L21.9 0.0970Bromomethane 0.500 25.0 2070-130122 4ug/L30.5 0.0990Carbon Tetrachloride 0.500 25.0 2070-130106 4ug/L26.6 0.105Chlorobenzene 1.00 25.0 2070-130102 3ug/L25.5 0.177Chlorodibromomethane 0.500 25.0 2060-140124 9ug/L31.0 0.0420Chloroethane 0.500 25.0 2070-130109 3ug/L27.2 0.172Chloroform 0.500 25.0 2060-14069 8ug/L17.3 0.0850Chloromethane 0.500 25.0 2070-130110 2ug/L27.6 0.114cis-1,2-Dichloroethene 1.00 25.0 2070-130102 5ug/L25.6 0.100cis-1,3-Dichloropropene 0.500 25.0 2060-140100 7ug/L25.0 0.0670Dichlorodifluoromethane 50.0 1000 2070-130119 8ug/L11903.00Ethanol 0.500 25.0 2070-130113 5ug/L28.3 0.0920Ethylbenzene 5.00 25.0 2070-13097 8ug/L24.2 0.0920Isopropyl Ether 0.500 25.0 2070-130112 8ug/L27.9 0.0980isopropylbenzene 1.00 50.0 2070-130106 9ug/L53.1 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 2070-130136 7ug/L34.0 X 0.190Methylene Chloride 2.00 25.0 2070-13091 6ug/L22.8 0.0940Naphthalene 2.00 25.0 2070-130110 6ug/L27.4 0.0600n-Butylbenzene 1.00 25.0 2070-130116 6ug/L28.9 0.0650n-Propylbenzene 0.500 25.0 2070-130128 7ug/L31.9 0.0920Sec-Butylbenzene 0.500 25.0 2070-130108 5ug/L27.1 0.0740Styrene Page 42 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017LCS Dup (B7C0316-BSD1) 0.500 25.0 2070-130113 7ug/L28.2 0.0890tert-Butylbenzene 0.500 25.0 2070-130113 9ug/L28.3 0.0540Tetrachloroethene 0.500 25.0 2070-130102 5ug/L25.5 0.0570Toluene 0.500 25.0 2070-130118 9ug/L29.4 0.188trans-1,2-dichloroethene 1.00 25.0 2070-130103 5ug/L25.7 0.110trans-1,3-dichloropropene 0.500 25.0 2070-13092 5ug/L22.9 0.139Trichloroethene 0.500 25.0 2060-140123 4ug/L30.8 0.0540Trichlorofluoromethane 1.00 25.0 2070-13098 0.2ug/L24.5 0.720Vinyl Acetate 0.500 25.0 2060-14093 7ug/L23.1 0.0810Vinyl Chloride 1.00 50.0 2070-130121 5ug/L60.4 0.176m,p-Xylenes 0.500 25.0 2070-130109 7ug/L27.4 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8721.8 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)9122.7 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)9122.8 ug/L Prepared & Analyzed: 3/16/2017Source: L7C0217-04Matrix Spike (B7C0316-MS1) 1.00 25.0 ND 70-130102ug/L25.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 70-130106ug/L26.4 0.07601,1,1-Trichloroethane 0.500 25.0 ND 70-130100ug/L24.9 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 70-130102ug/L25.6 0.1131,1,2-Trichloroethane 0.500 25.0 ND 70-130106ug/L26.4 0.1211,1-Dichloroethane 0.500 25.0 ND 70-130123ug/L30.8 0.1041,1-Dichloroethene 0.500 25.0 ND 70-13098ug/L24.6 0.06001,1-Dichloropropene 2.00 25.0 ND 70-13095ug/L23.8 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 70-13091ug/L22.9 0.1381,2,3-Trichloropropane 1.00 25.0 ND 70-13093ug/L23.3 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 70-130111ug/L27.7 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 70-130103ug/L25.8 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 70-130107ug/L26.8 0.09401,2-Dichlorobenzene 0.500 25.0 ND 70-13087ug/L21.7 0.09001,2-Dichloroethane 0.500 25.0 ND 70-13092ug/L22.9 0.1221,2-Dichloropropane 0.500 25.0 ND 70-130112ug/L28.0 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 70-130108ug/L26.9 0.09801,3-Dichlorobenzene 0.500 25.0 ND 70-13098ug/L24.6 0.1331,3-Dichloropropane 0.500 25.0 ND 70-130111ug/L27.8 0.06701,4-Dichlorobenzene 0.200 25.0 ND 70-13099ug/L24.8 0.09702,2-Dichloropropane 20.0 50.0 ND 70-13080ug/L40.2 0.3782-Butanone (MEK) 0.200 25.0 ND 70-130102ug/L25.6 0.08802-Chlorotoluene 5.00 50.0 ND 70-13073ug/L36.4 0.3522-Hexanone 0.500 25.0 ND 70-130105ug/L26.1 0.09004-Chlorotoluene Page 43 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017Source: L7C0217-04Matrix Spike (B7C0316-MS1) 0.500 25.0 ND 70-130103ug/L25.7 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 70-13080ug/L40.1 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 70-130114ug/L57.0 0.352Acetone 0.500 25.0 ND 70-13097ug/L24.2 0.119Benzene 0.500 25.0 ND 70-13096ug/L24.1 0.132Bromobenzene 0.500 25.0 ND 70-130108ug/L26.9 0.112Bromochloromethane 0.500 25.0 0.240 70-130110ug/L27.8 0.124Bromodichloromethane 2.00 25.0 ND 70-13083ug/L20.9 0.159Bromoform 1.00 25.0 ND 60-140101ug/L25.4 0.0970Bromomethane 0.500 25.0 ND 70-130116ug/L28.9 0.0990Carbon Tetrachloride 0.500 25.0 ND 70-130103ug/L25.8 0.105Chlorobenzene 1.00 25.0 ND 70-13095ug/L23.8 0.177Chlorodibromomethane 0.500 25.0 ND 60-140126ug/L31.4 0.0420Chloroethane 0.500 25.0 1.98 70-130105ug/L28.2 0.172Chloroform 0.500 25.0 ND 60-14067ug/L16.6 0.0850Chloromethane 0.500 25.0 ND 70-130111ug/L27.7 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 70-13083ug/L20.8 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 60-140103ug/L25.8 0.0670Dichlorodifluoromethane 50.0 1000 ND 70-130143ug/L1430X3.00Ethanol 0.500 25.0 ND 70-130110ug/L27.6 0.0920Ethylbenzene 5.00 25.0 ND 70-13095ug/L23.7 0.0920Isopropyl Ether 0.500 25.0 ND 70-130106ug/L26.4 0.0980isopropylbenzene 1.00 50.0 ND 70-13098ug/L49.2 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 70-130133ug/L33.2 X 0.190Methylene Chloride 2.00 25.0 ND 70-13083ug/L20.6 0.0940Naphthalene 2.00 25.0 ND 70-130101ug/L25.3 0.0600n-Butylbenzene 1.00 25.0 ND 70-130111ug/L27.7 0.0650n-Propylbenzene 0.500 25.0 ND 70-130120ug/L30.0 0.0920Sec-Butylbenzene 0.500 25.0 ND 70-130104ug/L25.9 0.0740Styrene 0.500 25.0 ND 70-130106ug/L26.5 0.0890tert-Butylbenzene 0.500 25.0 ND 70-130110ug/L27.4 0.0540Tetrachloroethene 0.500 25.0 ND 70-13099ug/L24.7 0.0570Toluene 0.500 25.0 ND 70-130119ug/L29.6 0.188trans-1,2-dichloroethene 1.00 25.0 ND 70-13087ug/L21.8 0.110trans-1,3-dichloropropene 0.500 25.0 ND 70-13091ug/L22.8 0.139Trichloroethene 0.500 25.0 ND 60-140132ug/L32.9 0.0540Trichlorofluoromethane 1.00 25.0 ND 70-13060ug/L15.1 X 0.720Vinyl Acetate 0.500 25.0 ND 60-14093ug/L23.4 0.0810Vinyl Chloride 1.00 50.0 ND 70-130117ug/L58.7 0.176m,p-Xylenes 0.500 25.0 ND 70-130105ug/L26.3 0.122o-Xylene Page 44 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017Source: L7C0217-04Matrix Spike (B7C0316-MS1) 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8922.3 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)8822.0 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)8822.0 ug/L Prepared & Analyzed: 3/16/2017Source: L7C0217-04Matrix Spike Dup (B7C0316-MSD1) 1.00 25.0 ND 2070-13098 4ug/L24.6 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 2070-13099 6ug/L24.8 0.07601,1,1-Trichloroethane 0.500 25.0 ND 2070-130102 2ug/L25.4 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 2070-13099 3ug/L24.8 0.1131,1,2-Trichloroethane 0.500 25.0 ND 2070-130100 6ug/L25.0 0.1211,1-Dichloroethane 0.500 25.0 ND 2070-130112 9ug/L28.0 0.1041,1-Dichloroethene 0.500 25.0 ND 2070-13093 5ug/L23.3 0.06001,1-Dichloropropene 2.00 25.0 ND 2070-13098 3ug/L24.6 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 2070-13094 3ug/L23.6 0.1381,2,3-Trichloropropane 1.00 25.0 ND 2070-13095 2ug/L23.8 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 2070-130105 6ug/L26.1 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 2070-130103 0.2ug/L25.8 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 2070-130106 1ug/L26.4 0.09401,2-Dichlorobenzene 0.500 25.0 ND 2070-13084 3ug/L21.0 0.09001,2-Dichloroethane 0.500 25.0 ND 2070-13090 1ug/L22.6 0.1221,2-Dichloropropane 0.500 25.0 ND 2070-130107 5ug/L26.8 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 2070-130105 2ug/L26.4 0.09801,3-Dichlorobenzene 0.500 25.0 ND 2070-130100 2ug/L25.0 0.1331,3-Dichloropropane 0.500 25.0 ND 2070-130109 2ug/L27.2 0.06701,4-Dichlorobenzene 0.200 25.0 ND 2070-13094 6ug/L23.4 0.09702,2-Dichloropropane 20.0 50.0 ND 2070-13084 4ug/L42.0 0.3782-Butanone (MEK) 0.200 25.0 ND 2070-130100 2ug/L25.1 0.08802-Chlorotoluene 5.00 50.0 ND 2070-13076 4ug/L37.9 0.3522-Hexanone 0.500 25.0 ND 2070-130102 2ug/L25.6 0.09004-Chlorotoluene 0.500 25.0 ND 2070-130100 2ug/L25.1 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 2070-13080 0.07ug/L40.1 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 2070-130111 3ug/L55.3 0.352Acetone 0.500 25.0 ND 2070-13093 4ug/L23.2 0.119Benzene 0.500 25.0 ND 2070-13095 1ug/L23.8 0.132Bromobenzene 0.500 25.0 ND 2070-130105 3ug/L26.2 0.112Bromochloromethane 0.500 25.0 0.240 2070-130108 2ug/L27.2 0.124Bromodichloromethane 2.00 25.0 ND 2070-13086 3ug/L21.5 0.159Bromoform 1.00 25.0 ND 2060-14099 2ug/L24.8 0.0970Bromomethane 0.500 25.0 ND 2070-130109 6ug/L27.2 0.0990Carbon Tetrachloride 0.500 25.0 ND 2070-130100 3ug/L25.0 0.105Chlorobenzene Page 45 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B7C0316 (Continued) Prepared & Analyzed: 3/16/2017Source: L7C0217-04Matrix Spike Dup (B7C0316-MSD1) 1.00 25.0 ND 2070-13094 2ug/L23.5 0.177Chlorodibromomethane 0.500 25.0 ND 2060-140117 7ug/L29.3 0.0420Chloroethane 0.500 25.0 1.98 2070-130100 4ug/L27.0 0.172Chloroform 0.500 25.0 ND 2060-14064 4ug/L16.0 0.0850Chloromethane 0.500 25.0 ND 2070-130104 7ug/L25.9 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 2070-13082 1ug/L20.5 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 2060-14095 8ug/L23.7 0.0670Dichlorodifluoromethane 50.0 1000 ND 2070-130138 4ug/L1380X3.00Ethanol 0.500 25.0 ND 2070-130105 5ug/L26.3 0.0920Ethylbenzene 5.00 25.0 ND 2070-13092 3ug/L23.1 0.0920Isopropyl Ether 0.500 25.0 ND 2070-130102 4ug/L25.4 0.0980isopropylbenzene 1.00 50.0 ND 2070-13092 6ug/L46.1 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 2070-130120 10ug/L30.0 0.190Methylene Chloride 2.00 25.0 ND 2070-13085 3ug/L21.2 0.0940Naphthalene 2.00 25.0 ND 2070-13098 4ug/L24.4 0.0600n-Butylbenzene 1.00 25.0 ND 2070-130106 4ug/L26.5 0.0650n-Propylbenzene 0.500 25.0 ND 2070-130116 3ug/L29.1 0.0920Sec-Butylbenzene 0.500 25.0 ND 2070-13097 7ug/L24.1 0.0740Styrene 0.500 25.0 ND 2070-130104 2ug/L25.9 0.0890tert-Butylbenzene 0.500 25.0 ND 2070-130104 5ug/L26.1 0.0540Tetrachloroethene 0.500 25.0 ND 2070-13096 3ug/L24.0 0.0570Toluene 0.500 25.0 ND 2070-130109 8ug/L27.2 0.188trans-1,2-dichloroethene 1.00 25.0 ND 2070-13085 2ug/L21.3 0.110trans-1,3-dichloropropene 0.500 25.0 ND 2070-13085 7ug/L21.4 0.139Trichloroethene 0.500 25.0 ND 2060-140122 8ug/L30.4 0.0540Trichlorofluoromethane 1.00 25.0 ND 2070-13059 3ug/L14.7 X 0.720Vinyl Acetate 0.500 25.0 ND 2060-14087 7ug/L21.8 0.0810Vinyl Chloride 1.00 50.0 ND 2070-130112 5ug/L55.9 0.176m,p-Xylenes 0.500 25.0 ND 2070-130100 5ug/L25.0 0.122o-Xylene 25.0 70-130Surrogate: 1,2-Dichloroethane-D4 (SUR)8822.1 ug/L 25.0 70-130Surrogate: 4-Bromofluorobenzene (SUR)8822.1 ug/L 25.0 70-130Surrogate: Toluene-D8 (SUR)8822.0 ug/L Page 46 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Lighthouse Food Mart #110 02804 Ryan Kerins 3/23/17 18:53 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 List of Certifications for FTS - Florida CodeDescriptionNumber ExpiresFacility LANELAC04176LA CERTIFICATE 12/31/2017FTSA ANC483NC CERTIFICATE 12/31/2017FTSL KENTUKY85KENTUKY CERTIFICATE FTSA LFLNELACE84098FL NELAC CERTIFICATE 06/30/2017FTSL AFLNELACE87429FL NELAC CERTIFICATE 06/30/2017FTSA DODLI0-135 DoD CERTIFICATE Renewal in Process 11/30/2016FTSL USDAP330-07-00105 USDA CERTIFICATE FTSA Notes and Definitions Item Definition Dry Sample results reported on a dry weight basis. U Analyte NOT DETECTED at or above the reporting limit. A Suspected adol-condensation product. B Analyte detected in the method blank. C Confirmed by GC/MS analysis. E Concentration exceeds calibration range. K Hold Time exceeded. N Tentatively Identified Compound. P >25% difference between primary and secondary columns. S Quantitation based on single-point calibration. X General QC Failure see Case Narrative. J The target analyte was positively identified below the Reporting Limit and above the Method Detection Limit. RPD Relative Percent Difference %REC Percent Recovery Source Sample that was matrix spiked or duplicated. Page 47 of 48 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety.