WA-17830_17830_CA_RPTS_20170321

ATC Associates of North
Carolina, P.C.

2512 Independence Blvd.
Suite 200-34
Wilmington, NC 28412
USA

Phone: [phone]
Fax: [phone]

www.atcassociates.com

March 13, 2017

Mrs. Sylvia Newsom-Hunneke
North Carolina Department of Environmental Quality
Division of Waste Management - UST Section
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Subject: Groundwater Monitoring Report
Former Craven Oil
1915 Glenburnie Road
New Bern, Craven County, North Carolina
NCDEQ Incident No. 17830
Priority Site Ranking: High

Dear Mrs. Newsom-Hunneke:
ATC Associates of North Carolina, P.C. (ATC), on behalf of Cenama, LLC, is submitting this
Monitoring Report to document the recent groundwater sampling event and summary of
laboratory analytical.
If you have any questions or require additional information, please contact our office at (919)
871-0999
Sincerely,

Maureen A. Jackson, P.G.
Senior Project Manager

Groundwater Monitoring Report
Former Craven Oil
1915 South Glenburnie Road
New Bern, North Carolina
March 13, 2017

TABLE OF CONTENTS

1.0 INTRODUCTION........................................................................................................1
2.0 SITE BACKGROUND ................................................................................................1
3.0 GROUNDWATER MONITORING ..........................................................................2
3.1 Groundwater Elevations .......................................................................................2
3.2 Analytical Results ................................................................................................2
4.0 CONCLUSIONS ..........................................................................................................3

TABLES

Table 1 Monitoring Well Construction Details
Table 2 Historical Groundwater Elevation Data
Table 3 Groundwater Analytical Summary
Table 4 Historical Groundwater Analytical Summary

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Plan
Figure 3 Groundwater Elevation Contour Map
Figure 4 Dissolved Contaminants of Concern Map

APPENDICES

Appendix A Laboratory Analytical Results

Groundwater Monitoring Report March 13, 2017
NCDEQ Incident No. 17830
Page 1

1.0 INTRODUCTION

ATC Associates of North Carolina, P.C. (ATC), on behalf of Cenama, LLC (Worsley), is
submitting this sampling report for the Former Craven Oil facility located at 1915 Glenburnie Road,
New Bern, North Carolina (Incident #17830). A site topographic map is presented as Figure 1 and
site map is presented as Figure 2. Currently, the site operates as an active retail fuel outlet and
convenience store. This report includes the laboratory analytical results for the groundwater
sampling events of February 8, 2017 and February 14, 2017.

2.0 SITE BACKGROUND
Historically, the facility operated as a bulk aboveground storage tank (AST) facility. The former
ASTs were owned by Worsley Companies, Inc. (Worsley) of Wilmington, North Carolina. At an
unknown date, the site’s AST systems were removed.

Site activities conducted to date have included the installation and sampling of seven Type II and
one Type III monitoring wells, soil samples collected during soil assessment activities and
monitoring well construction, and aquifer slug tests. Interim remedial actions have included the
excavation of approximately 1,155 tons of petroleum-impacted soil from the subject facility.

Previous reports submitted include: Comprehensive Site Assessment (CSA) Report, dated
November 1999, Clark Environmental Services, P.C. (CES); CSA Report Addendum, dated June
16, 2000, Delta Environmental Consultants, Inc. (Delta); Corrective Action Plan (CAP) and
addendum, dated December 29, 2000, and October 3, 2001, by Delta; Groundwater Monitoring
Reports submitted between May 2002 and March 2007 by Delta; Groundwater Monitoring
Reports submitted by Environmental Services & Solutions, PLLC (ESS) submitted March 2009
and August 2010.

In August 2010, Worsley awarded an environmental services contract to ATC for continuing
environmental services at the site.

This report describes the groundwater sampling results for the February 8, 2017 and February 14,
2017 sampling events.
Groundwater Monitoring Report March 13, 2017
NCDEQ Incident No. 17830

Page 2
3.0 GROUNDWATER MONITORING
3.1 Groundwater Elevations
On February 8, 2017, ATC collected static water level measurements from monitoring wells
MW-1, MW-2, MW-4A, MW-6, MW-7A, and T-1A. Monitoring wells MW-3A and MW-5A
could not be located on this date. Therefore, on February 14, 2017, ATC installed temporary
monitoring well TW-3A (replacement for well MW-3A) to collect a groundwater sample from
this area. The temporary well was installed to an approximate depth of ten feet below ground
surface. On this date, monitoring well MW-5A was located and measured.

Depths to water measurements were collected using an electronic oil/water interface probe. The
groundwater depths were converted to relative elevations using an assumed datum of 100 feet
relative to an arbitrary on-site benchmark. Monitoring well construction details are included in
Table 1. Current and historical groundwater elevation data are included in Table 2. A groundwater
elevation contour map is included as Figure 3. Groundwater flow appears to be south across the
site, which is consistent with historical groundwater flow.

3.2 Groundwater Analytical Results
On February 8, 2017, groundwater samples were collected from monitoring wells MW-1, MW-2,
MW-4A, MW-6, MW-7A, and T-1A. On February 14, 2017, groundwater samples were
collected from monitoring well MW-5A and temporary well TW-3A. Groundwater samples
were collected into laboratory-approved containers, packed in ice and delivered under
chain-of-custody to Con-Test Analytical Laboratory (Contest), in East Longmeadow,
Massachusetts, for analyses. Groundwater samples were analyzed for volatile organic compounds
(VOCs) via EPA Method 6200B including methyl tertiary-butyl ether (MTBE) and isopropyl
ether (IPE), Massachusetts Department of Environmental Protection (MADEP) volatile
petroleum hydrocarbons (VPH), and MADEP extractable petroleum hydrocarbons (EPH). A
summary of the recent groundwater analytical data is presented in Table 3 and a historical
summary of groundwater analytical data is presented in Table 4.

The laboratory analytical results from the February 2017 sampling event indicates target
compound concentrations were detected above established Title 15A NCAC 2L.0202 (2L)
Groundwater Monitoring Report March 13, 2017
NCDEQ Incident No. 17830

Page 3
standards in the groundwater samples collected from wells MW-1, TW-3A, MW-4A and
MW-7A. Dissolved contaminants of concern are depicted on Figure 4.

It should be noted dissolved target compound concentrations in the groundwater sample collected
from well MW-1 have historically been below laboratory method detection limits; however,
dissolved target compound concentrations were detected above 2L Standard for dissolved
benzene, naphthalene, and C9-C22 aromatics. This well appears to be located hydraulically
downgradient of the currently active gasoline dispensers.

Additionally, monitoring well MW-6 was listed on each laboratory report/chain-of-custody as
being sampled during each sampling event; however, this is in error. Monitoring well MW-6
was sampled on February 8, 2017 and monitoring well MW-5A was not located on this date. On
February 14, 2017, monitoring well MW-5A was located and subsequently sampled; however, it
was incorrectly labeled as well MW-6 on the chain-of-custody and subsequent laboratory report.
The laboratory results have been reported as the results for well MW-5A.

A copy of the laboratory analytical report is included as Appendix A.

4.0 CONCLUSIONS
ATC has performed a groundwater sampling event at the former Craven Oil facility in New Bern,
North Carolina. Based on field activities, observations, and groundwater analytical results, ATC
concludes the following:

· Depth to groundwater measurements in the shallow aquifer ranged from 1.41 feet to 3.36 feet
below ground surface in MW-6 and MW-1, respectively. The inferred shallow groundwater
flow direction across the site is to the south.
· Free product has not been associated with the release.
· The site is not located within a designated wellhead protection area.
· The site is connected to the public water supply system. The surrounding properties have the
option of being connected to the public water supply system.
Groundwater Monitoring Report March 13, 2017
NCDEQ Incident No. 17830

Page 4
· Target compound concentrations were detected above established 2L standards in the
groundwater samples collected from wells MW-1, TW-3A, MW-4A, and MW-7A.
· Dissolved target compound concentrations appear to be decreasing at the facility through time.
· It appears an off-site release may be impacted the monitoring wells associated with the Craven
Oil release.

Based on the above information, ATC recommends NCDEQ look into the possibility of an off-site
source impacting the groundwater at the site (based on the groundwater analytical data obtained
from well MW-1). NCDEQ should consider issuing a Notice of No Further Action for Incident
Number 17830.

TABLES
TABLE 1
MONITORING WELL CONSTRUCTION DETAILS
FORMER CRAVEN OIL
1915 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Depth of
Water (feet)
Elevation
(feet)
MW-1 Unknown 2 1.5-11.5 11.5 96.15 3.36 92.79
MW-2 Unknown 2 1.5-11.5 11.5 96.99 1.70 95.29
MW-3A Unknown 2 1.5-11.5 11.5 96.07
TW-3A 2/14/2017 2 3.20 --
MW-4A Unknown 2 2.0-12.0 12 96.68 2.17 94.51
MW-5A Unknown 2 2.0-12.0 12 96.14 1.40 94.74
MW-6 Unknown 2 2.0-12.0 12 96.94 1.41 95.53
MW-7A Unknown 2 2.0-12.0 12 96.87 2.44 94.43
T-1A Unknown 2 26.0-31.0 31 97.07 6.68 90.39
Notes:
1. Elevations are referenced to an arbitrary on-site benchmark of 100.00 feet.
2. Total well depths measured from top of casing.
Temporary Well
Monitoring
Well ID Date Installed
Well Casing
Diameter
(Inches)
Screened
Interval
(feet)
Unable To Locate
Depth of Well
(feet)
Top of Casing
(feet)
Date Measured: 2/8/17
TABLE 2
HISTORICAL GROUNDWATER ELEVATION DATA
FORMER CRAVEN OIL
1915 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well
No.Date Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation
(Feet)
8/21/2007 3.95 --92.20
2/6/2008 3.44 --92.71
8/19/2008 4.21 --91.94
2/19/2009 3.38 --92.77
8/11/2009 3.11 --93.04
2/17/2010 2.67 --93.48
8/9/2010 3.58 --92.57
2/8/2011 2.52 --93.63
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 3.36 --92.79
8/21/2007 2.91 --94.08
2/6/2008 2.27 --94.72
8/19/2008 3.06 --93.93
2/19/2009 2.24 --94.75
8/11/2009 2.08 --94.91
2/17/2010 1.68 --95.31
8/9/2010 2.51 --94.48
2/8/2011 1.66 --95.33
11/7/2011 2.65 --94.34
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 1.70 --95.29
8/21/2007 3.23 --92.84
2/6/2008 2.37 --93.70
8/19/2008 3.28 --92.79
2/19/2009 2.13 --93.94
8/11/2009 2.45 --93.62
2/17/2010 1.91 --94.16
8/9/2010 2.89 --93.18
2/8/2011 1.84 --94.23
10/9/2012
7/1/2013
4/7/2014 2.29 --93.78
1/7/2015
6/29/2016
2/8/2017
8/21/2007 3.37 --93.31
2/6/2008 2.63 --94.05
8/19/2008 3.32 --93.36
2/19/2009 2.48 --94.20
8/11/2009 2.60 --94.08
2/17/2010 2.13 --94.55
8/9/2010 2.97 --93.71
2/8/2011 1.91 --94.77
11/7/2011 2.95 --93.73
10/9/2012 2.58 --94.10
7/1/2013 2.04 --94.64
4/7/2014 2.43 --94.25
1/7/2015 2.49 --94.19
6/29/2016 2.27 --94.41
2/8/2017 2.17 --94.51
Not Measured
Not Measured
Not Measured
Not Measured
Unable to Locate
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
MW-1 96.15
MW-4A 96.68
MW-3A 96.07
MW-2 96.99
Page 1 of 2
TABLE 2
HISTORICAL GROUNDWATER ELEVATION DATA
FORMER CRAVEN OIL
1915 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well
No.Date Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation
(Feet)
8/21/2007 3.63 --92.51
2/6/2008 1.21 --94.93
8/19/2008 3.86 --92.28
2/19/2009 0.96 --95.18
8/11/2009
2/17/2010 0.86 --95.28
8/9/2010 0.99 --95.15
2/8/2011
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017
2/14/2017 1.40 --94.74
8/21/2007 3.22 --93.72
2/6/2008 1.56 --95.38
8/19/2008 3.22 --93.72
2/19/2009 1.73 --95.21
8/11/2009 1.97 --94.97
2/17/2010 1.35 --95.59
8/9/2010 2.50 --94.44
2/8/2011
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 1.41 --95.53
8/21/2007 3.38 --93.49
2/6/2008 2.76 --94.11
8/19/2008 3.55 --93.32
2/19/2009 2.95 --93.92
8/11/2009 2.63 --94.24
2/17/2010 2.04 --94.83
8/9/2010 3.13 --93.74
2/8/2011 2.19 --94.68
11/7/2011 3.14 --93.73
10/9/2012 2.74 --94.13
7/1/2013 2.31 --94.56
4/7/2014 2.51 --94.36
1/7/2015 2.57 --94.30
6/29/2016 2.36 --94.51
2/8/2017 2.44 --94.43
8/21/2007 8.66 --88.41
2/6/2008 9.56 --87.51
8/19/2008 10.25 --86.82
2/19/2009 9.11 --87.96
8/11/2009 9.13 --87.94
2/17/2010 5.65 --91.42
8/9/2010 9.17 --87.90
2/8/2011 6.54 --90.53
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 6.68 --90.39
Well Not Accessible
Not Measured
Not Measured
Not Measured
Not Measured
MW-5A 96.14
Unable to Locate
Not Measured
Not Measured
Not Measured
Not Measured
Unable to Locate
Not Measured
Unable to Access - Car Parked Over
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
T-1A 97.07
MW-7A 96.87
MW-6 96.94
Page 2 of 2
TABLE 3
GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
MW-1 2/8/2017 150 6.0 56 345 557 3.7 0.64J 49 230 58 8.1 2.8 1.3 1.6 <1.0 16 210 570 1,190 480
MW-2 2/8/2017 0.93 <0.50 <0.50 <1.5 0.93 2.7 0.32J <0.50 <0.50 0.25J 0.20J <0.50 <0.50 <0.50 <0.50 <0.50 <100 1,400 1,900 210
TW-3A 2/14/2017 3.8 2.8 12 201 219.6 1.6J <2.5 100 130 38 7.1 12 8.9 6.6 1.2J 11 <500 16,000 14,990 62,000
MW-4A 2/8/2017 0.18J <0.50 0.18J 1.96J 2.32J <0.50 <0.50 24 5.6 0.75 5.9 2.9 1.0 6.8 1.1 8.1 <100 200 1,110 1,700
MW-5A 2/14/2017 <0.50 <0.50 <0.50 <1.5 <3.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <100 160 170 320
MW-6 2/8/2017 <0.50 <0.50 <0.50 <1.5 <3.0 0.26J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <100 480 160 <200
MW-7A 2/8/2017 1.5 0.35J 170 1.51J 173.36J <0.50 <0.50 110 0.23J <0.50 15 5.4 <0.50 3.5 0.51 37 <100 <100 800 270
T-1A 2/8/2017 <0.50 <0.50 <0.50 <1.5 <3.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <100 <100 120 <200
1 600 600 500 NE 20 70 6 400 400 70 70 NE 70 70 70 400 10,000 200 700
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000 28,500 25,000 25,000 6,900 NE 8,500 15,000 30,000 NE NE NE NE
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (mg/l) = parts per billion.
3. NCDENR = North Carolina Department of Environment and Natural Resources.
4. GCL = Gross Contaminant Level.
5. NE = Not Established.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contaminant Levels for Groundwater are referenced in the Guidelines for Assessment
and Corrective Action, November 2008, updated January 2010.
8. BTEX = Benzene, Toluene, Ethylbenzene, Total Xylenes
9. J denotes estimated value by the laboratory.
Analytical Method
Contaminant of
Concern
BenzeneTolueneEthylbenzeneMTBEStandard Method 6200B
Total Xylenes2L Standard (mg/l)
GCL (mg/l)n-PropylbenzeneC5-C8 AliphaticsC9-C22 AromaticsTotal BTEXNaphthaleneIsopropyl etherMADEP Method EPH and VPH
C19-C36 Aliphaticstert-Butylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Butylbenzenep-Isopropyltoluenesec-ButylbenzeneC9-C18 Aliphatics
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 3.5 1.0 <5.0
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 4.31 <1.00 <1.00
2/8/2011 <1 <1 <1 <1 <4 <1 <1 <10
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 150 6.0 56 345 557 3.7 0.64J 49
4/24/2002 <0.5 <0.5 <0.5 <0.5 <2.0 <10 ----
7/24/2002 <1.0 <1.0 <1.0 <4.0 <7.0 5.0 <1.0 --
11/21/2002 <2.0 <2.0 <2.0 <2.0 <8.0 234 <10 --
1/28/2003 <0.5 <0.5 <0.5 <0.5 <2.0 31 <5 --
5/28/2003 <1.0 <1.0 <1.0 <4.0 <7.0 170 <1.0 --
11/11/2003 <0.5 <0.5 <0.5 <0.5 <2.0 188 <5.0 --
6/22/2004 <5.0 <5.0 <5.0 <5.0 <20.0 148 <50.0 --
1/17/2005 <0.5 <0.5 <0.5 <0.5 <2.0 101 <5.0 --
9/1/2005 <1.0 <1.0 <1.0 <2.0 <5.0 39 <1.0 --
2/1/2006 <1.0 <1.0 <1.0 <2.0 <5.0 46.0 <5.0 --
6/15/2006 <1.0 <1.0 <1.0 <2.0 <5.0 39 <1.0 --
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 41 <1.0 <5.0
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 26.5 <1.00 <1.00
2/8/2011 <1 <1 <1 <1 <4 9.6 <1 <10
11/7/2011 <1 <1 <1 <1 <4 9.0 <1 <10
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 0.93 <0.50 <0.50 <1.5 0.93 2.7 0.32J <0.50
4/24/2002 <0.5 <0.5 1.2 25 26.2 <10 ----
7/24/2002 <1.0 <1.0 <1.0 <4.0 <7.0 3.0 <1.0 --
11/21/2002 <1.0 <1.0 <1.0 <1.0 <4.0 <5.0 <5.0 --
1/28/2003 <0.5 <0.5 <0.5 <0.5 <2.0 <5.0 <5.0 --
5/28/2003 <1.0 <1.0 <1.0 <4.0 <7.0 <2.0 <1.0 --
11/11/2003 <0.5 <0.5 <0.5 <0.5 <2.0 5.4 <5.0 --
6/22/2004 <0.5 <0.5 <0.5 <0.5 <2.0 5.4 <5.0 --
1/17/2005 <0.5 <0.5 <0.5 <0.5 <2.0 5.0 <5.0 --
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 5.0 <1.0 <5.0
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 9.15 <1.00 1.96
2/8/2011
10/9/2012
7/1/2013
4/7/2014 <0.50 <0.50 <0.50 <1.50 <3.0 2.5 <0.50 <2.0
1/7/2015
6/29/2016
2/8/2017
TW-3A 2/14/2017 3.8 2.8 12 201 219.6 1.6 J <2.5 100
1 600 600 500 NE 20 70 6
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (mg/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
2L Standard (mg/l)
GCL (mg/l)
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEXNot Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Could Not Sample - Bent or Broken Casing
Not Sampled
Unable To Locate
Not Sampled
MW-3A
MW-1
MW-2
Not Sampled
Not Sampled
Not Sampled
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEX8. Gross Contamination Levels for Groundwater are referenced in the Guidelines for Assessment
and Corrective Action, November 2008, updated January 2010.
9. BTEX = Benzene, Toluene, Ethylbenzene, Total Xylenes
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEX4/24/2002 5.1 <0.5 21 10 36.1 13.0 ----
7/24/2002 5.0 1.00 16 8 30.0 11.0 <1.0 --
11/21/2002 1.5 <1.0 24 3.7 29.2 <5 <5 --
1/28/2003 2.3 <0.5 29 1.5 32.8 <5 <5 --
5/28/2003 1.3 <1.0 12 <4.0 13.3 <2.0 <1.0 --
11/11/2003 0.8 <0.5 7.9 0.8 9.5 <5.0 <5.0 --
6/22/2004 0.8 <0.5 2.6 <0.5 3.4 <5.0 <5.0 --
1/17/2005 <0.5 <0.5 3.1 0.5 3.6 <5.0 <5.0 --
9/1/2005 <1.0 <1.0 4.9 <2.0 4.9 <2.0 <1.0 --
2/1/2006 <0.5 <1.0 3.8 <3.0 3.8 <5.0 <5.0 --
6/15/2006 <0.5 <1.0 6.3 <3.0 6.3 <5.0 <1.0 --
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 <1.0 <1.0 27.00
2/6/2008 <1.0 <1.0 <1.0 <4.0 <7.0 <2.0 <1.0 19.5
8/19/2008 <4.00 <4.00 <4.00 <16.00 <28.00 <8.00 <4.00 42.1
2/19/2009 <1.00 1.17 <1.00 <3.00 1.17 <1.00 <1.00 34.9
8/11/2009 <1.00 <1.00 <1.00 <4.00 <7.00 <2.00 <1.00 67.1
2/17/2010 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 27.3
8/9/2010 <4.00 <4.00 <4.00 <16.00 <28.00 <8.00 <4.00 46.9
2/8/2011 <1 <1 <1 <1 <4 <1 <1 48
11/7/2011 <1 <1 <1 <1 <4 <8 <1 43
10/9/2012 <1 <1 <1 <1 <4 <8 <1 56
7/1/2013 <1 <1 <1 <1 <4 <8 <1 95
4/7/2014 <0.50 <0.50 <0.50 <1.50 <3.0 <0.50 <0.50 11.0
1/7/2015 <0.25 <0.25 <0.25 1.4 1.4 <0.25 <0.25 37.3
6/29/2016 <2.5 <2.5 <2.5 <7.5 ND <2.5 <2.5 4.9
2/8/2017 0.18J <0.50 0.18J 1.96J 2.32J <0.50 <0.50 24
4/24/2002 <0.5 <0.5 <0.5 <0.5 <2.0 91 ----
7/24/2002 <1.0 <1.0 <1.0 <4.0 <7.0 53 <1.0 --
11/21/2002 <1.0 <1.0 <1.0 <1.0 <4.0 61 <5.0 --
1/28/2003 <0.5 <0.5 <0.5 <0.5 <2.0 48 <5.0 --
5/28/2003 <1.0 <1.0 <1.0 <4.0 <7.0 24 <1.0 --
11/11/2003 <0.5 <0.5 <0.5 <0.5 <2.0 24.7 <5.0 --
6/22/2004 <0.5 <0.5 <0.5 <0.5 <2.0 16.7 <5.0 --
1/17/2005 <0.5 <0.5 <0.5 <0.5 <2.0 209 <5.0 --
9/1/2005 <1.0 <1.0 <1.0 <2.0 <5.0 6.2 <1.0 --
2/1/2006 <0.5 <0.5 <0.5 <3.0 <4.5 12 <5.0 --
6/15/2006 <1.0 <1.0 <1.0 <3.0 <6.0 11 <5.0 --
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 16 <1.0 <5.0
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 10.2 <1.00 <1.00
2/8/2011
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017
2/14/2017 <0.50 <0.50 <0.50 <1.5 <3.0 <0.50 <0.50 <0.50
1 600 600 500 NE 20 70 6
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (mg/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
8. Gross Contamination Levels for Groundwater are referenced in the Guidelines for Assessment
GCL (mg/l)
Not Sampled
2L Standard (mg/l)
Not Sampled
Well Not Accessible - Vehicle Parked Over
Not Sampled
Not Sampled
Unable To Locate
MW-4A
MW-5A
Not Sampled
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEX and Corrective Action, November 2008, updated January 2010.
9. BTEX = Benzene, Toluene, Ethylbenzene, Total Xylenes
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEX4/24/2002 <0.5 <0.5 <0.5 <0.5 <2.0 337 ----
7/24/2002 <1.0 <1.0 <1.0 <4.0 <7.0 190 <1.0 --
11/21/2002 <1.0 <1.0 <1.0 <1.0 <4.0 93 <5.0 --
1/28/2003 <0.5 <0.5 <0.5 <0.5 <2.0 260 <5.0 --
5/28/2003 <1.0 <1.0 <1.0 <4.0 <7.0 130 <1.0 --
11/11/2003 <0.5 <0.5 <0.5 <0.5 <2.0 250 <5.0 --
6/22/2004 <0.5 <0.5 <0.5 <0.5 <2.0 177 <5.0 --
1/17/2005 <0.5 <0.5 <0.5 <0.5 <2.0 129 <5.0 --
9/1/2005 <1.0 <1.0 <1.0 <2.0 <5.0 31 <1.0 --
6/15/2006 <1.0 <1.0 <1.0 <3.0 <6.0 22 <1.0 --
8/21/2007 <1.0 <5.0 <1.0 <3.0 <10.0 9.7 <1.0 <5.0
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 4.50 <1.00 <1.00
2/8/2011
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 <0.50 <0.50 <0.50 <1.5 <3.0 0.26J <0.50 <0.50
4/24/2002 149 279 289 1,810 2,527 <100 ----
7/24/2002 290 570 430 2,650 3,940 81 <40 --
11/21/2002 119 115 325 1,270 1,829 <50 <50 --
1/28/2003 80 16 366 177 639 <25 <25 --
5/28/2003 34 3 240 54 331 4.7 <1.0 --
11/11/2003 23.3 <0.5 214 59 296.3 <5.0 <5.0 --
6/22/2004 14.8 <5.0 1,789 19.5 1,823.8 <50.0 <50 --
1/17/2005 23.4 6.3 233 159 421.7 <50.0 <50 --
9/1/2005 <1.0 <1.0 8 <2.0 8 <2.0 <1.0 --
8/21/2007 11 <5.0 140 100 251 4.2 <1.0 140
2/6/2008 3.36 <2.0 64.4 21.1 88.9 <4.0 <2.0 56.1
8/19/2008 <16.0 <16.0 270 184 454 <32.0 <16.0 274
2/19/2009 <10.0 <10.0 149 84 233 <10.0 <10.0 148
8/11/2009 7.67 <1.00 <1.00 <4.00 7.67 <2.00 <1.00 142
2/17/2010 4.2 <2.0 85.9 <4.0 90.1 <2.0 <2.0 87.4
8/9/2010 1.12 <1.00 <1.00 <4.00 1.12 <2.00 <1.00 3.53
2/8/2011 1.3 <1 5.8 <1 7.1 <8 <1 <10
11/7/2011 1.6 <1 22 1.6 25.2 <8 <1 22
10/9/2012 <1 <1 28 <1 28 <8 <1 21
7/1/2013 1.2 <1 59 <1 60.2 <8 <1 47
4/7/2014 0.76 <0.50 61.7 1.84 64.30 <0.50 <0.50 7.8
1/7/2015 1.2 0.63 146 4.10 151.93 1 <0.25 55.1
6/29/2016 <2.5 <2.5 <2.5 <7.5 ND <2.5 <2.5 <2.5
2/8/2017 1.5 0.35J 170 1.51J 173.36J <0.50 <0.50 110
1 600 600 500 NE 20 70 6
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (mg/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
8. Gross Contamination Levels for Groundwater are referenced in the Guidelines for Assessment
and Corrective Action, November 2008, updated January 2010.
9. BTEX = Benzene, Toluene, Ethylbenzene, Total Xylenes
GCL (mg/l)
MW-7A
2L Standard (mg/l)
Not Sampled
Not Sampled
MW-6
Not Sampled
Not Sampled
Not Sampled
Well Not Accessible - Vehicle Parked Over
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL SUMMARY
FORMER CRAVEN OIL
1915 GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 17830
Well ID
Date
Collected
Analytical Method
Contaminant of Concern
BenzeneTolueneStandard Method 6200B
Isopropyl etherNaphthaleneMTBEEthylbenzeneTotal XylenesTotal BTEX4/24/2002 <0.5 <0.5 <0.5 <0.5 <2.0 <10 ----
7/24/2002 <1.0 <1.0 <1.0 <4.0 <7.0 <2.0 <1.0 --
11/21/2002 <1.0 <1.0 <1.0 <1.0 <4.0 <5.0 <5.0 --
1/28/2003 <0.5 <0.5 <0.5 <0.5 <2.0 <5.0 <5.0 --
5/28/2003 <1.0 <1.0 <1.0 <4.0 <7.0 <2.0 <1.0 --
11/11/2003 <0.5 <0.5 <0.5 <0.5 <2.0 <5.0 <5.0 --
6/22/2004 <0.5 <0.5 <0.5 <0.5 <2.0 <5.0 <5.0 --
1/17/2005 <0.5 <0.5 <0.5 <0.5 <2.0 <5.0 <5.0 --
9/1/2005 <1.0 <1.0 <1.0 <2.0 <5.0 <2.0 <1.0 --
2/1/2006 <1.0 <1.0 <1.0 <3.0 <6.0 <5.0 <5.0 --
2/19/2009 <1.00 <1.00 <1.00 <3.00 <6.00 <1.00 <1.00 <1.00
2/8/2011 <1 <1 <1 <1 <4 <8 <1 <10
10/9/2012
7/1/2013
4/7/2014
1/7/2015
6/29/2016
2/8/2017 <0.50 <0.50 <0.50 <1.5 <3.0 <0.50 <0.50 <0.50
1 600 600 500 NE 20 70 6
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (mg/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
8. Gross Contamination Levels for Groundwater are referenced in the Guidelines for Assessment
and Corrective Action, November 2008, updated January 2010.
9. BTEX = Benzene, Toluene, Ethylbenzene, Total Xylenes
GCL (mg/l)
2L Standard (mg/l)
T-1A
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled

FIGURES
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: WFH006
DATE: 3/2011 REVIEWED BY: EAA
FORMER CRAVEN OIL
1915 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY,
NORTH CAROLINA
SOURCE: 1994 TOPOGRAPHIC MAP - MSRMAPS.COM.
SCALE: SEE ABOVE
SITE
FIGURE 1: SITE TOPOGRAPHIC MAP

APPENDIX A

LABORATORY ANALYTICAL RESULTS

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
February 16, 2017
Maureen Jackson
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: New Bern, NC
Client Job Number:
Project Number: Craven Oil
Laboratory Work Order Number: 17B0473
Enclosed are results of analyses for samples received by the laboratory on February 9, 2017. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 54
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
17B0473-01 8
17B0473-02 12
17B0473-03 16
17B0473-04 20
17B0473-05 24
17B0473-06 28
Sample Preparation Information 32
QC Data 33
Volatile Organic Compounds by GC/MS 33
B170298 33
B170372 37
Petroleum Hydrocarbons Analyses - EPH 41
B170179 41
Petroleum Hydrocarbons Analyses - VPH 44
B170421 44
Flag/Qualifier Summary 46
Certifications 47
Chain of Custody/Sample Receipt 50
Page 2 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
2/16/2017
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Maureen Jackson
Craven Oil
17B0473
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
New Bern, NC
MW-1 17B0473-01 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
MW-2 17B0473-02 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
MW-4A 17B0473-03 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
MW-6 17B0473-04 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
MW-7A 17B0473-05 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
T-1A 17B0473-06 Ground Water MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-01MW-1
DL
1,2,4-Trimethylbenzene 230 1.0 g/L SM21-22 6200B0.36
1,3,5-Trimethylbenzene 58 1.0 g/L SM21-22 6200B0.26
Benzene 150 1.0 g/L SM21-22 6200B0.24
Diisopropyl Ether (DIPE)0.64 1.0 g/L SM21-22 6200BJ0.36
Ethylbenzene 56 1.0 g/L SM21-22 6200B0.26
Isopropylbenzene (Cumene)8.1 1.0 g/L SM21-22 6200B0.24
m+p Xylene 270 2.0 g/L SM21-22 6200B0.51
Methyl tert-Butyl Ether (MTBE)3.7 1.0 g/L SM21-22 6200B0.18
Naphthalene 49 1.0 g/L SM21-22 6200B0.24
n-Butylbenzene 2.8 1.0 g/L SM21-22 6200B0.30
n-Propylbenzene 16 1.0 g/L SM21-22 6200B0.26
o-Xylene 75 1.0 g/L SM21-22 6200B0.26
p-Isopropyltoluene (p-Cymene)1.3 1.0 g/L SM21-22 6200B0.30
sec-Butylbenzene 1.6 1.0 g/L SM21-22 6200B0.26
Toluene 6.0 1.0 g/L SM21-22 6200B0.34
C11-C22 Aromatics 330 100 g/L MADEP-EPH-04-1.1
C19-C36 Aliphatics 570 100 g/L MADEP-EPH-04-1.1
C9-C18 Aliphatics 290 100 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 460 100 g/L MADEP-EPH-04-1.1
C5-C8 Aliphatics 210 100 g/L MADEP-VPH-04-1.1
C9-C10 Aromatics 860 100 g/L MADEP-VPH-04-1.1
C9-C12 Aliphatics 190 100 g/L MADEP-VPH-04-1.1
Unadjusted C5-C8 Aliphatics 310 100 g/L MADEP-VPH-04-1.1
Unadjusted C9-C12 Aliphatics 1300 100 g/L MADEP-VPH-04-1.1
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-02MW-2
DL
1,3,5-Trimethylbenzene 0.25 0.50 g/L SM21-22 6200BJ0.13
Benzene 0.93 0.50 g/L SM21-22 6200B0.12
Diisopropyl Ether (DIPE)0.32 0.50 g/L SM21-22 6200BJ0.18
Isopropylbenzene (Cumene)0.20 0.50 g/L SM21-22 6200BJ0.12
Methyl tert-Butyl Ether (MTBE)2.7 0.50 g/L SM21-22 6200B0.090
C11-C22 Aromatics 1900 97 g/L MADEP-EPH-04-1.1
C19-C36 Aliphatics 1400 97 g/L MADEP-EPH-04-1.1
C9-C18 Aliphatics 210 97 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 3200 97 g/L MADEP-EPH-04-1.1
Page 4 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-03MW-4A
DL
1,2,4-Trimethylbenzene 5.6 0.50 g/L SM21-22 6200B0.18
1,3,5-Trimethylbenzene 0.75 0.50 g/L SM21-22 6200B0.13
Benzene 0.18 0.50 g/L SM21-22 6200BJ0.12
Ethylbenzene 0.18 0.50 g/L SM21-22 6200BJ0.13
Isopropylbenzene (Cumene)5.9 0.50 g/L SM21-22 6200B0.12
m+p Xylene 1.7 1.0 g/L SM21-22 6200B0.26
Naphthalene 24 0.50 g/L SM21-22 6200B0.12
n-Butylbenzene 2.9 0.50 g/L SM21-22 6200B0.15
n-Propylbenzene 8.1 0.50 g/L SM21-22 6200B0.13
o-Xylene 0.26 0.50 g/L SM21-22 6200BJ0.13
p-Isopropyltoluene (p-Cymene)1.0 0.50 g/L SM21-22 6200B0.15
sec-Butylbenzene 6.8 0.50 g/L SM21-22 6200B0.13
tert-Butylbenzene 1.1 0.50 g/L SM21-22 6200B0.12
C11-C22 Aromatics 930 100 g/L MADEP-EPH-04-1.1
C19-C36 Aliphatics 200 100 g/L MADEP-EPH-04-1.1
C9-C18 Aliphatics 1700 100 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 1200 100 g/L MADEP-EPH-04-1.1
C9-C10 Aromatics 180 100 g/L MADEP-VPH-04-1.1
Unadjusted C9-C12 Aliphatics 260 100 g/L MADEP-VPH-04-1.1
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-04MW-6
DL
Methyl tert-Butyl Ether (MTBE)0.26 0.50 g/L SM21-22 6200BJ0.090
C11-C22 Aromatics 160 100 g/L MADEP-EPH-04-1.1
C19-C36 Aliphatics 480 100 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 160 100 g/L MADEP-EPH-04-1.1
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-05MW-7A
DL
1,2,4-Trimethylbenzene 0.23 0.50 g/L SM21-22 6200BJ0.18
Benzene 1.5 0.50 g/L SM21-22 6200B0.12
Ethylbenzene 170 0.50 g/L SM21-22 6200B0.13
Isopropylbenzene (Cumene)15 0.50 g/L SM21-22 6200B0.12
m+p Xylene 0.58 1.0 g/L SM21-22 6200BJ0.26
Naphthalene 110 0.50 g/L SM21-22 6200B0.12
n-Butylbenzene 5.4 0.50 g/L SM21-22 6200B0.15
n-Propylbenzene 37 0.50 g/L SM21-22 6200B0.13
o-Xylene 0.93 0.50 g/L SM21-22 6200B0.13
sec-Butylbenzene 3.5 0.50 g/L SM21-22 6200B0.13
tert-Butylbenzene 0.51 0.50 g/L SM21-22 6200B0.12
Toluene 0.35 0.50 g/L SM21-22 6200BJ0.17
C11-C22 Aromatics 340 100 g/L MADEP-EPH-04-1.1
C9-C18 Aliphatics 130 100 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 390 100 g/L MADEP-EPH-04-1.1
C9-C10 Aromatics 460 100 g/L MADEP-VPH-04-1.1
C9-C12 Aliphatics 140 100 g/L MADEP-VPH-04-1.1
Unadjusted C9-C12 Aliphatics 750 100 g/L MADEP-VPH-04-1.1
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
17B0473-06T-1A
DL
C11-C22 Aromatics 120 100 g/L MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 120 100 g/L MADEP-EPH-04-1.1
Page 5 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH, only hydrocarbon ranges were requested and reported.
For method 6200B,elevated reporting limit for sample17B0473-01 due to the high concentration of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Chloromethane
17B0473-01[MW-1], 17B0473-02[MW-2], 17B0473-03[MW-4A], 17B0473-04[MW-6], 17B0473-05[MW-7A], B170298-BLK1, B170298-BS1, B170298-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
17B0473-01[MW-1]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-04-1.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 7 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/8/2017 14:45
[TOC_2]17B0473-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 2/14/17 4:17 EEHg/L9.7 2/13/17SM21-22 6200B2Acetone
150 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B2Benzene
ND 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B2Bromobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.45 2/13/17SM21-22 6200B2Bromochloromethane
ND 1.0 2/14/17 4:17 EEHg/L0.59 2/13/17SM21-22 6200B2Bromodichloromethane
ND 4.0 2/14/17 4:17 EEHg/L0.42 2/13/17SM21-22 6200B2Bromoform
ND 4.0 2/14/17 4:17 EEHg/L1.9 2/13/17SM21-22 6200B2Bromomethane
ND 10 2/14/17 4:17 EEHg/L4.7 2/13/17SM21-22 6200B22-Butanone (MEK)
2.8 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B2n-Butylbenzene
1.6 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B2sec-Butylbenzene
ND 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B2tert-Butylbenzene
ND 2.0 2/14/17 4:17 EEHg/L0.49 2/13/17SM21-22 6200B2Carbon Tetrachloride
ND 1.0 2/14/17 4:17 EEHg/L0.32 2/13/17SM21-22 6200B2Chlorobenzene
ND 100 2/14/17 4:17 EEHg/L90 2/13/17SM21-22 6200B2Ethanol
ND 1.0 2/14/17 4:17 EEHg/L0.21 2/13/17SM21-22 6200B2Chlorodibromomethane
ND 2.0 2/14/17 4:17 EEHg/L0.56 2/13/17SM21-22 6200B2Chloroethane
ND 1.0 2/14/17 4:17 EEHg/L0.44 2/13/17SM21-22 6200B2Chloroform
ND 4.0 2/14/17 4:17 EEHg/L1.1 2/13/17SM21-22 6200B2L-04Chloromethane
ND 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B22-Chlorotoluene
ND 1.0 2/14/17 4:17 EEHg/L0.28 2/13/17SM21-22 6200B24-Chlorotoluene
ND 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 2/14/17 4:17 EEHg/L0.34 2/13/17SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.34 2/13/17SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.57 2/13/17SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 2/14/17 4:17 EEHg/L0.32 2/13/17SM21-22 6200B21,1-Dichloroethane
ND 2.0 2/14/17 4:17 EEHg/L0.39 2/13/17SM21-22 6200B21,2-Dichloroethane
ND 1.0 2/14/17 4:17 EEHg/L0.42 2/13/17SM21-22 6200B21,1-Dichloroethylene
ND 1.0 2/14/17 4:17 EEHg/L0.29 2/13/17SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B21,2-Dichloropropane
ND 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B21,3-Dichloropropane
ND 1.0 2/14/17 4:17 EEHg/L0.43 2/13/17SM21-22 6200B22,2-Dichloropropane
ND 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B21,1-Dichloropropene
ND 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 2/14/17 4:17 EEHg/L0.22 2/13/17SM21-22 6200B2trans-1,3-Dichloropropene
0.64 1.0 2/14/17 4:17 EEHg/L0.36 2/13/17SM21-22 6200B2JDiisopropyl Ether (DIPE)
56 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B2Ethylbenzene
ND 10 2/14/17 4:17 EEHg/L3.0 2/13/17SM21-22 6200B22-Hexanone (MBK)
8.1 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B2Isopropylbenzene (Cumene)
1.3 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B2p-Isopropyltoluene (p-Cymene)
3.7 1.0 2/14/17 4:17 EEHg/L0.18 2/13/17SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 2/14/17 4:17 EEHg/L6.4 2/13/17SM21-22 6200B2Methylene Chloride
ND 10 2/14/17 4:17 EEHg/L2.9 2/13/17SM21-22 6200B24-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 8 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/8/2017 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
49 1.0 2/14/17 4:17 EEHg/L0.24 2/13/17SM21-22 6200B2Naphthalene
16 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B2n-Propylbenzene
ND 1.0 2/14/17 4:17 EEHg/L0.30 2/13/17SM21-22 6200B2Styrene
ND 1.0 2/14/17 4:17 EEHg/L0.32 2/13/17SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 2/14/17 4:17 EEHg/L0.54 2/13/17SM21-22 6200B2Tetrachloroethylene
6.0 1.0 2/14/17 4:17 EEHg/L0.34 2/13/17SM21-22 6200B2Toluene
ND 1.0 2/14/17 4:17 EEHg/L0.28 2/13/17SM21-22 6200B21,2,3-Trichlorobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.38 2/13/17SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 2/14/17 4:17 EEHg/L0.47 2/13/17SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 2/14/17 4:17 EEHg/L0.40 2/13/17SM21-22 6200B2Trichloroethylene
ND 1.0 2/14/17 4:17 EEHg/L0.29 2/13/17SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 2/14/17 4:17 EEHg/L0.43 2/13/17SM21-22 6200B21,2,3-Trichloropropane
230 1.0 2/14/17 4:17 EEHg/L0.36 2/13/17SM21-22 6200B21,2,4-Trimethylbenzene
58 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B21,3,5-Trimethylbenzene
ND 10 2/14/17 4:17 EEHg/L2.9 2/13/17SM21-22 6200B2Vinyl Acetate
ND 1.0 2/14/17 4:17 EEHg/L0.27 2/13/17SM21-22 6200B2Vinyl Chloride
270 2.0 2/14/17 4:17 EEHg/L0.51 2/13/17SM21-22 6200B2m+p Xylene
75 1.0 2/14/17 4:17 EEHg/L0.26 2/13/17SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 2/14/17 4:1770-130
Toluene-d8 99.5 2/14/17 4:1770-130
4-Bromofluorobenzene 97.1 2/14/17 4:1770-130
Page 9 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/8/2017 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
290 100 2/15/17 2:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
570 100 2/15/17 2:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
460 100 2/15/17 2:52 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
330 100 2/15/17 2:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)42.1 2/15/17 2:5240-140
o-Terphenyl (OTP)57.0 2/15/17 2:5240-140
2-Bromonaphthalene 78.4 2/15/17 2:5240-140
2-Fluorobiphenyl 92.1 2/15/17 2:5240-140
Page 10 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/8/2017 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
310 100 2/14/17 2:48 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
210 100 2/14/17 2:48 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
1300 100 2/14/17 2:48 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
190 100 2/14/17 2:48 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
860 100 2/14/17 2:48 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)118 2/14/17 2:4870-130
2,5-Dibromotoluene (PID)116 2/14/17 2:4870-130
Page 11 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/8/2017 15:45
[TOC_2]17B0473-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/14/17 2:02 EEHg/L4.9 2/13/17SM21-22 6200B1Acetone
0.93 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B1Benzene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1Bromobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.22 2/13/17SM21-22 6200B1Bromochloromethane
ND 0.50 2/14/17 2:02 EEHg/L0.30 2/13/17SM21-22 6200B1Bromodichloromethane
ND 2.0 2/14/17 2:02 EEHg/L0.21 2/13/17SM21-22 6200B1Bromoform
ND 2.0 2/14/17 2:02 EEHg/L0.94 2/13/17SM21-22 6200B1Bromomethane
ND 5.0 2/14/17 2:02 EEHg/L2.4 2/13/17SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1n-Butylbenzene
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B1tert-Butylbenzene
ND 1.0 2/14/17 2:02 EEHg/L0.25 2/13/17SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/14/17 2:02 EEHg/L0.16 2/13/17SM21-22 6200B1Chlorobenzene
ND 50 2/14/17 2:02 EEHg/L45 2/13/17SM21-22 6200B1Ethanol
ND 0.50 2/14/17 2:02 EEHg/L0.10 2/13/17SM21-22 6200B1Chlorodibromomethane
ND 1.0 2/14/17 2:02 EEHg/L0.28 2/13/17SM21-22 6200B1Chloroethane
ND 0.50 2/14/17 2:02 EEHg/L0.22 2/13/17SM21-22 6200B1Chloroform
ND 2.0 2/14/17 2:02 EEHg/L0.55 2/13/17SM21-22 6200B1L-04Chloromethane
ND 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B12-Chlorotoluene
ND 0.50 2/14/17 2:02 EEHg/L0.14 2/13/17SM21-22 6200B14-Chlorotoluene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/14/17 2:02 EEHg/L0.17 2/13/17SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.17 2/13/17SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.28 2/13/17SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/14/17 2:02 EEHg/L0.16 2/13/17SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/14/17 2:02 EEHg/L0.19 2/13/17SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/14/17 2:02 EEHg/L0.21 2/13/17SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/14/17 2:02 EEHg/L0.21 2/13/17SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/14/17 2:02 EEHg/L0.11 2/13/17SM21-22 6200B1trans-1,3-Dichloropropene
0.32 0.50 2/14/17 2:02 EEHg/L0.18 2/13/17SM21-22 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1Ethylbenzene
ND 5.0 2/14/17 2:02 EEHg/L1.5 2/13/17SM21-22 6200B12-Hexanone (MBK)
0.20 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B1JIsopropylbenzene (Cumene)
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
2.7 0.50 2/14/17 2:02 EEHg/L0.090 2/13/17SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/14/17 2:02 EEHg/L3.2 2/13/17SM21-22 6200B1Methylene Chloride
ND 5.0 2/14/17 2:02 EEHg/L1.5 2/13/17SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 12 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/8/2017 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 2/14/17 2:02 EEHg/L0.12 2/13/17SM21-22 6200B1Naphthalene
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1n-Propylbenzene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1Styrene
ND 0.50 2/14/17 2:02 EEHg/L0.16 2/13/17SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/14/17 2:02 EEHg/L0.27 2/13/17SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/14/17 2:02 EEHg/L0.17 2/13/17SM21-22 6200B1Toluene
ND 0.50 2/14/17 2:02 EEHg/L0.14 2/13/17SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.19 2/13/17SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/14/17 2:02 EEHg/L0.24 2/13/17SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/14/17 2:02 EEHg/L0.20 2/13/17SM21-22 6200B1Trichloroethylene
ND 0.50 2/14/17 2:02 EEHg/L0.15 2/13/17SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/14/17 2:02 EEHg/L0.22 2/13/17SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/14/17 2:02 EEHg/L0.18 2/13/17SM21-22 6200B11,2,4-Trimethylbenzene
0.25 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1J1,3,5-Trimethylbenzene
ND 5.0 2/14/17 2:02 EEHg/L1.4 2/13/17SM21-22 6200B1Vinyl Acetate
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1Vinyl Chloride
ND 1.0 2/14/17 2:02 EEHg/L0.26 2/13/17SM21-22 6200B1m+p Xylene
ND 0.50 2/14/17 2:02 EEHg/L0.13 2/13/17SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 2/14/17 2:0270-130
Toluene-d8 99.4 2/14/17 2:0270-130
4-Bromofluorobenzene 91.5 2/14/17 2:0270-130
Page 13 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/8/2017 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
210 97 2/15/17 3:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
1400 97 2/15/17 3:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
3200 97 2/15/17 3:12 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
1900 97 2/15/17 3:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)71.8 2/15/17 3:1240-140
o-Terphenyl (OTP)81.2 2/15/17 3:1240-140
2-Bromonaphthalene 76.2 2/15/17 3:1240-140
2-Fluorobiphenyl 96.6 2/15/17 3:1240-140
Page 14 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/8/2017 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/13/17 18:28 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 2/13/17 18:28 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 100 2/13/17 18:28 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 100 2/13/17 18:28 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 100 2/13/17 18:28 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)95.8 2/13/17 18:2870-130
2,5-Dibromotoluene (PID)97.0 2/13/17 18:2870-130
Page 15 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-03
Field Sample #: MW-4A
Sample Matrix: Ground Water
Sampled: 2/8/2017 11:15
[TOC_2]17B0473-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/14/17 3:50 EEHg/L4.9 2/13/17SM21-22 6200B1Acetone
0.18 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B1JBenzene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1Bromobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.22 2/13/17SM21-22 6200B1Bromochloromethane
ND 0.50 2/14/17 3:50 EEHg/L0.30 2/13/17SM21-22 6200B1Bromodichloromethane
ND 2.0 2/14/17 3:50 EEHg/L0.21 2/13/17SM21-22 6200B1Bromoform
ND 2.0 2/14/17 3:50 EEHg/L0.94 2/13/17SM21-22 6200B1Bromomethane
ND 5.0 2/14/17 3:50 EEHg/L2.4 2/13/17SM21-22 6200B12-Butanone (MEK)
2.9 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1n-Butylbenzene
6.8 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B1sec-Butylbenzene
1.1 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B1tert-Butylbenzene
ND 1.0 2/14/17 3:50 EEHg/L0.25 2/13/17SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/14/17 3:50 EEHg/L0.16 2/13/17SM21-22 6200B1Chlorobenzene
ND 50 2/14/17 3:50 EEHg/L45 2/13/17SM21-22 6200B1Ethanol
ND 0.50 2/14/17 3:50 EEHg/L0.10 2/13/17SM21-22 6200B1Chlorodibromomethane
ND 1.0 2/14/17 3:50 EEHg/L0.28 2/13/17SM21-22 6200B1Chloroethane
ND 0.50 2/14/17 3:50 EEHg/L0.22 2/13/17SM21-22 6200B1Chloroform
ND 2.0 2/14/17 3:50 EEHg/L0.55 2/13/17SM21-22 6200B1L-04Chloromethane
ND 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B12-Chlorotoluene
ND 0.50 2/14/17 3:50 EEHg/L0.14 2/13/17SM21-22 6200B14-Chlorotoluene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/14/17 3:50 EEHg/L0.17 2/13/17SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.17 2/13/17SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.28 2/13/17SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/14/17 3:50 EEHg/L0.16 2/13/17SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/14/17 3:50 EEHg/L0.19 2/13/17SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/14/17 3:50 EEHg/L0.21 2/13/17SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/14/17 3:50 EEHg/L0.21 2/13/17SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/14/17 3:50 EEHg/L0.11 2/13/17SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/14/17 3:50 EEHg/L0.18 2/13/17SM21-22 6200B1Diisopropyl Ether (DIPE)
0.18 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B1JEthylbenzene
ND 5.0 2/14/17 3:50 EEHg/L1.5 2/13/17SM21-22 6200B12-Hexanone (MBK)
5.9 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B1Isopropylbenzene (Cumene)
1.0 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/14/17 3:50 EEHg/L0.090 2/13/17SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/14/17 3:50 EEHg/L3.2 2/13/17SM21-22 6200B1Methylene Chloride
ND 5.0 2/14/17 3:50 EEHg/L1.5 2/13/17SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-03
Field Sample #: MW-4A
Sample Matrix: Ground Water
Sampled: 2/8/2017 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
24 0.50 2/14/17 3:50 EEHg/L0.12 2/13/17SM21-22 6200B1Naphthalene
8.1 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B1n-Propylbenzene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1Styrene
ND 0.50 2/14/17 3:50 EEHg/L0.16 2/13/17SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/14/17 3:50 EEHg/L0.27 2/13/17SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/14/17 3:50 EEHg/L0.17 2/13/17SM21-22 6200B1Toluene
ND 0.50 2/14/17 3:50 EEHg/L0.14 2/13/17SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.19 2/13/17SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/14/17 3:50 EEHg/L0.24 2/13/17SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/14/17 3:50 EEHg/L0.20 2/13/17SM21-22 6200B1Trichloroethylene
ND 0.50 2/14/17 3:50 EEHg/L0.15 2/13/17SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/14/17 3:50 EEHg/L0.22 2/13/17SM21-22 6200B11,2,3-Trichloropropane
5.6 0.50 2/14/17 3:50 EEHg/L0.18 2/13/17SM21-22 6200B11,2,4-Trimethylbenzene
0.75 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 2/14/17 3:50 EEHg/L1.4 2/13/17SM21-22 6200B1Vinyl Acetate
ND 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B1Vinyl Chloride
1.7 1.0 2/14/17 3:50 EEHg/L0.26 2/13/17SM21-22 6200B1m+p Xylene
0.26 0.50 2/14/17 3:50 EEHg/L0.13 2/13/17SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 102 2/14/17 3:5070-130
Toluene-d8 99.0 2/14/17 3:5070-130
4-Bromofluorobenzene 96.8 2/14/17 3:5070-130
Page 17 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-03
Field Sample #: MW-4A
Sample Matrix: Ground Water
Sampled: 2/8/2017 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
1700 100 2/15/17 3:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
200 100 2/15/17 3:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
1200 100 2/15/17 3:32 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
930 100 2/15/17 3:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)64.1 2/15/17 3:3240-140
o-Terphenyl (OTP)79.7 2/15/17 3:3240-140
2-Bromonaphthalene 70.3 2/15/17 3:3240-140
2-Fluorobiphenyl 90.4 2/15/17 3:3240-140
Page 18 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-03
Field Sample #: MW-4A
Sample Matrix: Ground Water
Sampled: 2/8/2017 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/13/17 18:57 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 2/13/17 18:57 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
260 100 2/13/17 18:57 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 100 2/13/17 18:57 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
180 100 2/13/17 18:57 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)120 2/13/17 18:5770-130
2,5-Dibromotoluene (PID)117 2/13/17 18:5770-130
Page 19 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-04
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/8/2017 12:05
[TOC_2]17B0473-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/14/17 2:29 EEHg/L4.9 2/13/17SM21-22 6200B1Acetone
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B1Benzene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1Bromobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.22 2/13/17SM21-22 6200B1Bromochloromethane
ND 0.50 2/14/17 2:29 EEHg/L0.30 2/13/17SM21-22 6200B1Bromodichloromethane
ND 2.0 2/14/17 2:29 EEHg/L0.21 2/13/17SM21-22 6200B1Bromoform
ND 2.0 2/14/17 2:29 EEHg/L0.94 2/13/17SM21-22 6200B1Bromomethane
ND 5.0 2/14/17 2:29 EEHg/L2.4 2/13/17SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1n-Butylbenzene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B1tert-Butylbenzene
ND 1.0 2/14/17 2:29 EEHg/L0.25 2/13/17SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/14/17 2:29 EEHg/L0.16 2/13/17SM21-22 6200B1Chlorobenzene
ND 50 2/14/17 2:29 EEHg/L45 2/13/17SM21-22 6200B1Ethanol
ND 0.50 2/14/17 2:29 EEHg/L0.10 2/13/17SM21-22 6200B1Chlorodibromomethane
ND 1.0 2/14/17 2:29 EEHg/L0.28 2/13/17SM21-22 6200B1Chloroethane
ND 0.50 2/14/17 2:29 EEHg/L0.22 2/13/17SM21-22 6200B1Chloroform
ND 2.0 2/14/17 2:29 EEHg/L0.55 2/13/17SM21-22 6200B1L-04Chloromethane
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B12-Chlorotoluene
ND 0.50 2/14/17 2:29 EEHg/L0.14 2/13/17SM21-22 6200B14-Chlorotoluene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/14/17 2:29 EEHg/L0.17 2/13/17SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.17 2/13/17SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.28 2/13/17SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/14/17 2:29 EEHg/L0.16 2/13/17SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/14/17 2:29 EEHg/L0.19 2/13/17SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/14/17 2:29 EEHg/L0.21 2/13/17SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/14/17 2:29 EEHg/L0.21 2/13/17SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/14/17 2:29 EEHg/L0.11 2/13/17SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/14/17 2:29 EEHg/L0.18 2/13/17SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B1Ethylbenzene
ND 5.0 2/14/17 2:29 EEHg/L1.5 2/13/17SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.26 0.50 2/14/17 2:29 EEHg/L0.090 2/13/17SM21-22 6200B1JMethyl tert-Butyl Ether (MTBE)
ND 5.0 2/14/17 2:29 EEHg/L3.2 2/13/17SM21-22 6200B1Methylene Chloride
ND 5.0 2/14/17 2:29 EEHg/L1.5 2/13/17SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 20 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-04
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/8/2017 12:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 2/14/17 2:29 EEHg/L0.12 2/13/17SM21-22 6200B1Naphthalene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B1n-Propylbenzene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1Styrene
ND 0.50 2/14/17 2:29 EEHg/L0.16 2/13/17SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/14/17 2:29 EEHg/L0.27 2/13/17SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/14/17 2:29 EEHg/L0.17 2/13/17SM21-22 6200B1Toluene
ND 0.50 2/14/17 2:29 EEHg/L0.14 2/13/17SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.19 2/13/17SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/14/17 2:29 EEHg/L0.24 2/13/17SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/14/17 2:29 EEHg/L0.20 2/13/17SM21-22 6200B1Trichloroethylene
ND 0.50 2/14/17 2:29 EEHg/L0.15 2/13/17SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/14/17 2:29 EEHg/L0.22 2/13/17SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/14/17 2:29 EEHg/L0.18 2/13/17SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 2/14/17 2:29 EEHg/L1.4 2/13/17SM21-22 6200B1Vinyl Acetate
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B1Vinyl Chloride
ND 1.0 2/14/17 2:29 EEHg/L0.26 2/13/17SM21-22 6200B1m+p Xylene
ND 0.50 2/14/17 2:29 EEHg/L0.13 2/13/17SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 102 2/14/17 2:2970-130
Toluene-d8 101 2/14/17 2:2970-130
4-Bromofluorobenzene 94.4 2/14/17 2:2970-130
Page 21 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-04
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/8/2017 12:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 2/15/17 3:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
480 100 2/15/17 3:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
160 100 2/15/17 3:52 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
160 100 2/15/17 3:52 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)72.3 2/15/17 3:5240-140
o-Terphenyl (OTP)78.9 2/15/17 3:5240-140
2-Bromonaphthalene 76.5 2/15/17 3:5240-140
2-Fluorobiphenyl 94.4 2/15/17 3:5240-140
Page 22 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-04
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/8/2017 12:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/13/17 19:27 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 2/13/17 19:27 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 100 2/13/17 19:27 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 100 2/13/17 19:27 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 100 2/13/17 19:27 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)109 2/13/17 19:2770-130
2,5-Dibromotoluene (PID)109 2/13/17 19:2770-130
Page 23 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-05
Field Sample #: MW-7A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:55
[TOC_2]17B0473-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/14/17 2:56 EEHg/L4.9 2/13/17SM21-22 6200B1Acetone
1.5 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B1Benzene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1Bromobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.22 2/13/17SM21-22 6200B1Bromochloromethane
ND 0.50 2/14/17 2:56 EEHg/L0.30 2/13/17SM21-22 6200B1Bromodichloromethane
ND 2.0 2/14/17 2:56 EEHg/L0.21 2/13/17SM21-22 6200B1Bromoform
ND 2.0 2/14/17 2:56 EEHg/L0.94 2/13/17SM21-22 6200B1Bromomethane
ND 5.0 2/14/17 2:56 EEHg/L2.4 2/13/17SM21-22 6200B12-Butanone (MEK)
5.4 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1n-Butylbenzene
3.5 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B1sec-Butylbenzene
0.51 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B1tert-Butylbenzene
ND 1.0 2/14/17 2:56 EEHg/L0.25 2/13/17SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/14/17 2:56 EEHg/L0.16 2/13/17SM21-22 6200B1Chlorobenzene
ND 50 2/14/17 2:56 EEHg/L45 2/13/17SM21-22 6200B1Ethanol
ND 0.50 2/14/17 2:56 EEHg/L0.10 2/13/17SM21-22 6200B1Chlorodibromomethane
ND 1.0 2/14/17 2:56 EEHg/L0.28 2/13/17SM21-22 6200B1Chloroethane
ND 0.50 2/14/17 2:56 EEHg/L0.22 2/13/17SM21-22 6200B1Chloroform
ND 2.0 2/14/17 2:56 EEHg/L0.55 2/13/17SM21-22 6200B1L-04Chloromethane
ND 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B12-Chlorotoluene
ND 0.50 2/14/17 2:56 EEHg/L0.14 2/13/17SM21-22 6200B14-Chlorotoluene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/14/17 2:56 EEHg/L0.17 2/13/17SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.17 2/13/17SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.28 2/13/17SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/14/17 2:56 EEHg/L0.16 2/13/17SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/14/17 2:56 EEHg/L0.19 2/13/17SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/14/17 2:56 EEHg/L0.21 2/13/17SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/14/17 2:56 EEHg/L0.21 2/13/17SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/14/17 2:56 EEHg/L0.11 2/13/17SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/14/17 2:56 EEHg/L0.18 2/13/17SM21-22 6200B1Diisopropyl Ether (DIPE)
170 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B1Ethylbenzene
ND 5.0 2/14/17 2:56 EEHg/L1.5 2/13/17SM21-22 6200B12-Hexanone (MBK)
15 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/14/17 2:56 EEHg/L0.090 2/13/17SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/14/17 2:56 EEHg/L3.2 2/13/17SM21-22 6200B1Methylene Chloride
ND 5.0 2/14/17 2:56 EEHg/L1.5 2/13/17SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-05
Field Sample #: MW-7A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
110 0.50 2/14/17 2:56 EEHg/L0.12 2/13/17SM21-22 6200B1Naphthalene
37 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B1n-Propylbenzene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1Styrene
ND 0.50 2/14/17 2:56 EEHg/L0.16 2/13/17SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/14/17 2:56 EEHg/L0.27 2/13/17SM21-22 6200B1Tetrachloroethylene
0.35 0.50 2/14/17 2:56 EEHg/L0.17 2/13/17SM21-22 6200B1JToluene
ND 0.50 2/14/17 2:56 EEHg/L0.14 2/13/17SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.19 2/13/17SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/14/17 2:56 EEHg/L0.24 2/13/17SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/14/17 2:56 EEHg/L0.20 2/13/17SM21-22 6200B1Trichloroethylene
ND 0.50 2/14/17 2:56 EEHg/L0.15 2/13/17SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/14/17 2:56 EEHg/L0.22 2/13/17SM21-22 6200B11,2,3-Trichloropropane
0.23 0.50 2/14/17 2:56 EEHg/L0.18 2/13/17SM21-22 6200B1J1,2,4-Trimethylbenzene
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 2/14/17 2:56 EEHg/L1.4 2/13/17SM21-22 6200B1Vinyl Acetate
ND 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B1Vinyl Chloride
0.58 1.0 2/14/17 2:56 EEHg/L0.26 2/13/17SM21-22 6200B1Jm+p Xylene
0.93 0.50 2/14/17 2:56 EEHg/L0.13 2/13/17SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 2/14/17 2:5670-130
Toluene-d8 99.6 2/14/17 2:5670-130
4-Bromofluorobenzene 99.0 2/14/17 2:5670-130
Page 25 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-05
Field Sample #: MW-7A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
130 100 2/15/17 4:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 100 2/15/17 4:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
390 100 2/15/17 4:12 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
340 100 2/15/17 4:12 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)70.1 2/15/17 4:1240-140
o-Terphenyl (OTP)77.5 2/15/17 4:1240-140
2-Bromonaphthalene 79.2 2/15/17 4:1240-140
2-Fluorobiphenyl 98.2 2/15/17 4:1240-140
Page 26 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-05
Field Sample #: MW-7A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/13/17 19:56 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 2/13/17 19:56 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
750 100 2/13/17 19:56 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
140 100 2/13/17 19:56 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
460 100 2/13/17 19:56 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)115 2/13/17 19:5670-130
2,5-Dibromotoluene (PID)119 2/13/17 19:5670-130
Page 27 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-06
Field Sample #: T-1A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:00
[TOC_2]17B0473-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/14/17 19:31 MFFg/L4.9 2/14/17SM21-22 6200B1Acetone
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B1Benzene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1Bromobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.22 2/14/17SM21-22 6200B1Bromochloromethane
ND 0.50 2/14/17 19:31 MFFg/L0.30 2/14/17SM21-22 6200B1Bromodichloromethane
ND 2.0 2/14/17 19:31 MFFg/L0.21 2/14/17SM21-22 6200B1Bromoform
ND 2.0 2/14/17 19:31 MFFg/L0.94 2/14/17SM21-22 6200B1Bromomethane
ND 5.0 2/14/17 19:31 MFFg/L2.4 2/14/17SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1n-Butylbenzene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B1tert-Butylbenzene
ND 1.0 2/14/17 19:31 MFFg/L0.25 2/14/17SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/14/17 19:31 MFFg/L0.16 2/14/17SM21-22 6200B1Chlorobenzene
ND 50 2/14/17 19:31 MFFg/L45 2/14/17SM21-22 6200B1Ethanol
ND 0.50 2/14/17 19:31 MFFg/L0.10 2/14/17SM21-22 6200B1Chlorodibromomethane
ND 1.0 2/14/17 19:31 MFFg/L0.28 2/14/17SM21-22 6200B1Chloroethane
ND 0.50 2/14/17 19:31 MFFg/L0.22 2/14/17SM21-22 6200B1Chloroform
ND 2.0 2/14/17 19:31 MFFg/L0.55 2/14/17SM21-22 6200B1Chloromethane
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B12-Chlorotoluene
ND 0.50 2/14/17 19:31 MFFg/L0.14 2/14/17SM21-22 6200B14-Chlorotoluene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/14/17 19:31 MFFg/L0.17 2/14/17SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.17 2/14/17SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.28 2/14/17SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/14/17 19:31 MFFg/L0.16 2/14/17SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/14/17 19:31 MFFg/L0.19 2/14/17SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/14/17 19:31 MFFg/L0.21 2/14/17SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/14/17 19:31 MFFg/L0.21 2/14/17SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/14/17 19:31 MFFg/L0.11 2/14/17SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/14/17 19:31 MFFg/L0.18 2/14/17SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B1Ethylbenzene
ND 5.0 2/14/17 19:31 MFFg/L1.5 2/14/17SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/14/17 19:31 MFFg/L0.090 2/14/17SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/14/17 19:31 MFFg/L3.2 2/14/17SM21-22 6200B1Methylene Chloride
ND 5.0 2/14/17 19:31 MFFg/L1.5 2/14/17SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-06
Field Sample #: T-1A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 2/14/17 19:31 MFFg/L0.12 2/14/17SM21-22 6200B1Naphthalene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B1n-Propylbenzene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1Styrene
ND 0.50 2/14/17 19:31 MFFg/L0.16 2/14/17SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/14/17 19:31 MFFg/L0.27 2/14/17SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/14/17 19:31 MFFg/L0.17 2/14/17SM21-22 6200B1Toluene
ND 0.50 2/14/17 19:31 MFFg/L0.14 2/14/17SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.19 2/14/17SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/14/17 19:31 MFFg/L0.24 2/14/17SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/14/17 19:31 MFFg/L0.20 2/14/17SM21-22 6200B1Trichloroethylene
ND 0.50 2/14/17 19:31 MFFg/L0.15 2/14/17SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/14/17 19:31 MFFg/L0.22 2/14/17SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/14/17 19:31 MFFg/L0.18 2/14/17SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B11,3,5-Trimethylbenzene
ND 5.0 2/14/17 19:31 MFFg/L1.4 2/14/17SM21-22 6200B1Vinyl Acetate
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B1Vinyl Chloride
ND 1.0 2/14/17 19:31 MFFg/L0.26 2/14/17SM21-22 6200B1m+p Xylene
ND 0.50 2/14/17 19:31 MFFg/L0.13 2/14/17SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.6 2/14/17 19:3170-130
Toluene-d8 101 2/14/17 19:3170-130
4-Bromofluorobenzene 94.6 2/14/17 19:3170-130
Page 29 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-06
Field Sample #: T-1A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 100 2/15/17 4:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 100 2/15/17 4:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C19-C36 Aliphatics
120 100 2/15/17 4:32 PJGg/L 2/11/17MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
120 100 2/15/17 4:32 PJGg/L 2/11/17MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)67.2 2/15/17 4:3240-140
o-Terphenyl (OTP)76.0 2/15/17 4:3240-140
2-Bromonaphthalene 75.7 2/15/17 4:3240-140
2-Fluorobiphenyl 90.5 2/15/17 4:3240-140
Page 30 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/9/2017
Work Order: 17B0473Sample Description:Project Location: New Bern, NC
Sample ID: 17B0473-06
Field Sample #: T-1A
Sample Matrix: Ground Water
Sampled: 2/8/2017 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 2/13/17 20:26 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 2/13/17 20:26 EEHg/L 2/13/17MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 100 2/13/17 20:26 EEHg/L 2/13/17MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 100 2/13/17 20:26 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 100 2/13/17 20:26 EEHg/L 2/13/17MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 2/13/17 20:2670-130
2,5-Dibromotoluene (PID)101 2/13/17 20:2670-130
Page 31 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3510C-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B170179 02/11/171000 2.0017B0473-01 [MW-1]
B170179 02/11/17880 1.7017B0473-02 [MW-2]
B170179 02/11/171000 2.0017B0473-03 [MW-4A]
B170179 02/11/171000 2.0017B0473-04 [MW-6]
B170179 02/11/171000 2.0017B0473-05 [MW-7A]
B170179 02/11/171000 2.0017B0473-06 [T-1A]
Prep Method: MA VPH-MADEP-VPH-04-1.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B170421 02/13/175 5.0017B0473-01 [MW-1]
B170421 02/13/175 5.0017B0473-02 [MW-2]
B170421 02/13/175 5.0017B0473-03 [MW-4A]
B170421 02/13/175 5.0017B0473-04 [MW-6]
B170421 02/13/175 5.0017B0473-05 [MW-7A]
B170421 02/13/175 5.0017B0473-06 [T-1A]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B170298 02/13/172.5 5.0017B0473-01 [MW-1]
B170298 02/13/175 5.0017B0473-02 [MW-2]
B170298 02/13/175 5.0017B0473-03 [MW-4A]
B170298 02/13/175 5.0017B0473-04 [MW-6]
B170298 02/13/175 5.0017B0473-05 [MW-7A]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B170372 02/14/175 5.0017B0473-06 [T-1A]
[TOC_1]Sample Preparation Information[TOC]
Page 32 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B170298 - SW-846 5030B
[TOC_3]B170298[TOC]
Blank (B170298-BLK1) Prepared: 02/13/17 Analyzed: 02/14/17
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60 L-04ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 33 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170298 - SW-846 5030B
Blank (B170298-BLK1) Prepared: 02/13/17 Analyzed: 02/14/17
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.6
g/L 25.0 70-130Surrogate: Toluene-d8 99.925.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.023.5
LCS (B170298-BS1) Prepared & Analyzed: 02/13/17
Acetone g/L50 100 70-13098.298.2
Benzene g/L0.50 10.0 70-13098.29.82
Bromobenzene g/L0.50 10.0 70-13090.29.02
Bromochloromethane g/L0.50 10.0 70-13098.59.85
Bromodichloromethane g/L0.50 10.0 70-13093.99.39
Bromoform g/L0.50 10.0 70-13086.78.67
Bromomethane g/L1.0 10.0 60-14099.09.90
2-Butanone (MEK)g/L5.0 100 70-13085.385.3
n-Butylbenzene g/L0.50 10.0 70-13010210.2
sec-Butylbenzene g/L0.50 10.0 70-13098.09.80
tert-Butylbenzene g/L0.50 10.0 70-13098.89.88
Carbon Tetrachloride g/L0.50 10.0 70-13096.59.65
Chlorobenzene g/L0.50 10.0 70-13098.59.85
Ethanol g/L50 100 70-13093.093.0
Chlorodibromomethane g/L0.50 10.0 70-13010010.0
Chloroethane g/L0.50 10.0 60-14010210.2
Chloroform g/L0.50 10.0 70-13093.09.30
Chloromethane g/L0.60 10.0 L-0460-14045.4 *4.54
2-Chlorotoluene g/L0.50 10.0 70-13082.68.26
4-Chlorotoluene g/L0.50 10.0 70-13088.88.88
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13093.79.37
1,2-Dichlorobenzene g/L0.50 10.0 70-13010010.0
1,3-Dichlorobenzene g/L0.50 10.0 70-13093.19.31
1,4-Dichlorobenzene g/L0.50 10.0 70-13097.39.73
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010110.1
1,1-Dichloroethane g/L0.50 10.0 70-13096.59.65
1,2-Dichloroethane g/L0.50 10.0 70-13087.38.73
1,1-Dichloroethylene g/L0.50 10.0 70-13010810.8
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13097.99.79
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13094.49.44
1,2-Dichloropropane g/L0.50 10.0 70-13085.68.56
1,3-Dichloropropane g/L0.50 10.0 70-13091.59.15
2,2-Dichloropropane g/L0.50 10.0 70-13075.57.55
1,1-Dichloropropene g/L0.50 10.0 70-13097.69.76
cis-1,3-Dichloropropene g/L0.50 10.0 70-13089.28.92
trans-1,3-Dichloropropene g/L0.50 10.0 70-13095.39.53
Page 34 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170298 - SW-846 5030B
LCS (B170298-BS1) Prepared & Analyzed: 02/13/17
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13085.98.59
Ethylbenzene g/L0.50 10.0 70-13097.59.75
2-Hexanone (MBK)g/L5.0 100 70-13080.980.9
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13094.19.41
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010010.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13092.69.26
Methylene Chloride g/L5.0 10.0 70-13096.49.64
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13083.983.9
Naphthalene g/L0.50 10.0 70-13080.18.01
n-Propylbenzene g/L0.50 10.0 70-13096.19.61
Styrene g/L0.50 10.0 70-13092.79.27
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13094.59.45
Tetrachloroethylene g/L0.50 10.0 70-13093.29.32
Toluene g/L0.50 10.0 70-13095.19.51
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13084.88.48
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13088.48.84
1,1,1-Trichloroethane g/L0.50 10.0 70-13096.29.62
1,1,2-Trichloroethane g/L0.50 10.0 70-13010110.1
Trichloroethylene g/L0.50 10.0 70-13099.59.95
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13010410.4
1,2,3-Trichloropropane g/L0.50 10.0 70-13097.29.72
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13098.09.80
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13093.49.34
Vinyl Acetate g/L5.0 100 70-13076.676.6
Vinyl Chloride g/L0.50 10.0 60-14095.09.50
m+p Xylene g/L1.0 20.0 70-13092.318.5
o-Xylene g/L0.50 10.0 70-13096.39.63
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.5
g/L 25.0 70-130Surrogate: Toluene-d8 99.424.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.524.4
LCS Dup (B170298-BSD1) Prepared & Analyzed: 02/13/17
Acetone g/L50 100 2570-13090.0 8.7090.0
Benzene g/L0.50 10.0 2570-13099.0 0.8119.90
Bromobenzene g/L0.50 10.0 2570-13092.4 2.419.24
Bromochloromethane g/L0.50 10.0 2570-13099.1 0.6079.91
Bromodichloromethane g/L0.50 10.0 2570-13095.2 1.379.52
Bromoform g/L0.50 10.0 2570-13084.9 2.108.49
Bromomethane g/L1.0 10.0 2560-14096.0 3.089.60
2-Butanone (MEK)g/L5.0 100 2570-13081.2 5.0381.2
n-Butylbenzene g/L0.50 10.0 2570-13099.6 1.899.96
sec-Butylbenzene g/L0.50 10.0 2570-13098.8 0.8139.88
tert-Butylbenzene g/L0.50 10.0 2570-13098.9 0.1019.89
Carbon Tetrachloride g/L0.50 10.0 2570-13098.7 2.259.87
Chlorobenzene g/L0.50 10.0 2570-13098.1 0.4079.81
Ethanol g/L50 100 2570-13097.1 4.3297.1
Chlorodibromomethane g/L0.50 10.0 2570-130101 0.89210.1
Chloroethane g/L0.50 10.0 2560-14099.2 2.599.92
Chloroform g/L0.50 10.0 2570-13091.4 1.749.14
Chloromethane g/L0.60 10.0 25 L-0460-14053.0 15.4*5.30
2-Chlorotoluene g/L0.50 10.0 2570-13081.5 1.348.15
4-Chlorotoluene g/L0.50 10.0 2570-13087.7 1.258.77
Page 35 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170298 - SW-846 5030B
LCS Dup (B170298-BSD1) Prepared & Analyzed: 02/13/17
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13098.1 4.599.81
1,2-Dichlorobenzene g/L0.50 10.0 2570-130100 0.49910.0
1,3-Dichlorobenzene g/L0.50 10.0 2570-13094.3 1.289.43
1,4-Dichlorobenzene g/L0.50 10.0 2570-13097.2 0.1039.72
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14099.5 1.799.95
1,1-Dichloroethane g/L0.50 10.0 2570-13095.5 1.049.55
1,2-Dichloroethane g/L0.50 10.0 2570-13087.3 0.008.73
1,1-Dichloroethylene g/L0.50 10.0 2570-130112 3.9911.2
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13098.0 0.1029.80
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13093.9 0.5319.39
1,2-Dichloropropane g/L0.50 10.0 2570-13084.0 1.898.40
1,3-Dichloropropane g/L0.50 10.0 2570-13096.2 5.019.62
2,2-Dichloropropane g/L0.50 10.0 2570-13073.0 3.377.30
1,1-Dichloropropene g/L0.50 10.0 2570-13095.7 1.979.57
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13089.2 0.008.92
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13094.4 0.9499.44
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13086.3 0.4658.63
Ethylbenzene g/L0.50 10.0 2570-13097.1 0.4119.71
2-Hexanone (MBK)g/L5.0 100 2570-13075.3 7.1875.3
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13094.0 0.1069.40
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13098.4 2.019.84
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13093.9 1.399.39
Methylene Chloride g/L5.0 10.0 2570-13092.8 3.819.28
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13078.4 6.8078.4
Naphthalene g/L0.50 10.0 2570-13071.4 11.57.14
n-Propylbenzene g/L0.50 10.0 2570-13094.2 2.009.42
Styrene g/L0.50 10.0 2570-13093.8 1.189.38
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13088.5 6.568.85
Tetrachloroethylene g/L0.50 10.0 2570-13095.5 2.449.55
Toluene g/L0.50 10.0 2570-13093.5 1.709.35
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13075.9 11.17.59
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13084.1 4.998.41
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.8 1.659.78
1,1,2-Trichloroethane g/L0.50 10.0 2570-130103 2.2610.3
Trichloroethylene g/L0.50 10.0 2570-13099.6 0.1009.96
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130104 0.38510.4
1,2,3-Trichloropropane g/L0.50 10.0 2570-13090.0 7.699.00
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13096.9 1.139.69
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13093.0 0.4299.30
Vinyl Acetate g/L5.0 100 2570-13075.0 2.0375.0
Vinyl Chloride g/L0.50 10.0 2560-140108 12.910.8
m+p Xylene g/L1.0 20.0 2570-13091.0 1.4218.2
o-Xylene g/L0.50 10.0 2570-13092.9 3.599.29
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.2
g/L 25.0 70-130Surrogate: Toluene-d8 99.825.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.723.9
Page 36 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170372 - SW-846 5030B
[TOC_3]B170372[TOC]
Blank (B170372-BLK1) Prepared & Analyzed: 02/14/17
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 37 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170372 - SW-846 5030B
Blank (B170372-BLK1) Prepared & Analyzed: 02/14/17
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.2
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 92.523.1
LCS (B170372-BS1) Prepared & Analyzed: 02/14/17
Acetone g/L50 100 70-130109109
Benzene g/L0.50 10.0 70-13011011.0
Bromobenzene g/L0.50 10.0 70-13094.69.46
Bromochloromethane g/L0.50 10.0 70-13097.29.72
Bromodichloromethane g/L0.50 10.0 70-13095.99.59
Bromoform g/L0.50 10.0 70-13092.99.29
Bromomethane g/L1.0 10.0 60-14011611.6
2-Butanone (MEK)g/L5.0 100 70-13089.989.9
n-Butylbenzene g/L0.50 10.0 70-13011311.3
sec-Butylbenzene g/L0.50 10.0 70-13010710.7
tert-Butylbenzene g/L0.50 10.0 70-13010610.6
Carbon Tetrachloride g/L0.50 10.0 70-13010710.7
Chlorobenzene g/L0.50 10.0 70-13010510.5
Ethanol g/L50 100 70-13090.790.7
Chlorodibromomethane g/L0.50 10.0 70-13010310.3
Chloroethane g/L0.50 10.0 60-14010710.7
Chloroform g/L0.50 10.0 70-13095.99.59
Chloromethane g/L0.60 10.0 60-14066.16.61
2-Chlorotoluene g/L0.50 10.0 70-13087.08.70
4-Chlorotoluene g/L0.50 10.0 70-13094.09.40
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13096.99.69
1,2-Dichlorobenzene g/L0.50 10.0 70-13010610.6
1,3-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,4-Dichlorobenzene g/L0.50 10.0 70-13010310.3
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010510.5
1,1-Dichloroethane g/L0.50 10.0 70-13099.09.90
1,2-Dichloroethane g/L0.50 10.0 70-13086.18.61
1,1-Dichloroethylene g/L0.50 10.0 70-13012412.4
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13099.49.94
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13099.79.97
1,2-Dichloropropane g/L0.50 10.0 70-13086.68.66
1,3-Dichloropropane g/L0.50 10.0 70-13098.79.87
2,2-Dichloropropane g/L0.50 10.0 70-13089.18.91
1,1-Dichloropropene g/L0.50 10.0 70-13010410.4
cis-1,3-Dichloropropene g/L0.50 10.0 70-13094.99.49
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010010.0
Page 38 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170372 - SW-846 5030B
LCS (B170372-BS1) Prepared & Analyzed: 02/14/17
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13085.18.51
Ethylbenzene g/L0.50 10.0 70-13010710.7
2-Hexanone (MBK)g/L5.0 100 70-13081.881.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010010.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010810.8
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13095.79.57
Methylene Chloride g/L5.0 10.0 70-13092.49.24
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13083.183.1
Naphthalene g/L0.50 10.0 70-13010510.5
n-Propylbenzene g/L0.50 10.0 70-13010310.3
Styrene g/L0.50 10.0 70-13097.19.71
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13098.99.89
Tetrachloroethylene g/L0.50 10.0 70-13098.29.82
Toluene g/L0.50 10.0 70-13010410.4
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13010510.5
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010510.5
1,1,1-Trichloroethane g/L0.50 10.0 70-13010110.1
1,1,2-Trichloroethane g/L0.50 10.0 70-13010310.3
Trichloroethylene g/L0.50 10.0 70-13010210.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011611.6
1,2,3-Trichloropropane g/L0.50 10.0 70-13097.79.77
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011011.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13098.59.85
Vinyl Acetate g/L5.0 100 70-13084.084.0
Vinyl Chloride g/L0.50 10.0 60-14097.79.77
m+p Xylene g/L1.0 20.0 70-13010420.8
o-Xylene g/L0.50 10.0 70-13010510.5
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.4
g/L 25.0 70-130Surrogate: Toluene-d8 98.824.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.424.1
LCS Dup (B170372-BSD1) Prepared & Analyzed: 02/14/17
Acetone g/L50 100 2570-130103 5.74103
Benzene g/L0.50 10.0 2570-130109 0.45710.9
Bromobenzene g/L0.50 10.0 2570-13093.1 1.609.31
Bromochloromethane g/L0.50 10.0 2570-13095.0 2.299.50
Bromodichloromethane g/L0.50 10.0 2570-13096.3 0.4169.63
Bromoform g/L0.50 10.0 2570-13088.7 4.638.87
Bromomethane g/L1.0 10.0 2560-140120 3.0512.0
2-Butanone (MEK)g/L5.0 100 2570-13087.3 2.9187.3
n-Butylbenzene g/L0.50 10.0 2570-130107 5.0110.7
sec-Butylbenzene g/L0.50 10.0 2570-130103 3.3310.3
tert-Butylbenzene g/L0.50 10.0 2570-13099.3 6.539.93
Carbon Tetrachloride g/L0.50 10.0 2570-130101 5.7610.1
Chlorobenzene g/L0.50 10.0 2570-130100 4.3910.0
Ethanol g/L50 100 2570-13084.2 7.4984.2
Chlorodibromomethane g/L0.50 10.0 2570-130103 0.0010.3
Chloroethane g/L0.50 10.0 2560-140103 3.4210.3
Chloroform g/L0.50 10.0 2570-13092.2 3.939.22
Chloromethane g/L0.60 10.0 2560-14063.6 3.866.36
2-Chlorotoluene g/L0.50 10.0 2570-13084.0 3.518.40
4-Chlorotoluene g/L0.50 10.0 2570-13092.9 1.189.29
Page 39 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B170372 - SW-846 5030B
LCS Dup (B170372-BSD1) Prepared & Analyzed: 02/14/17
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13097.0 0.1039.70
1,2-Dichlorobenzene g/L0.50 10.0 2570-130102 3.6510.2
1,3-Dichlorobenzene g/L0.50 10.0 2570-13098.3 3.309.83
1,4-Dichlorobenzene g/L0.50 10.0 2570-130101 2.0610.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-140101 3.9910.1
1,1-Dichloroethane g/L0.50 10.0 2570-13093.1 6.149.31
1,2-Dichloroethane g/L0.50 10.0 2570-13084.4 1.998.44
1,1-Dichloroethylene g/L0.50 10.0 2570-130120 3.2812.0
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13097.0 2.449.70
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.9 2.859.69
1,2-Dichloropropane g/L0.50 10.0 2570-13084.8 2.108.48
1,3-Dichloropropane g/L0.50 10.0 2570-13092.6 6.389.26
2,2-Dichloropropane g/L0.50 10.0 2570-13087.1 2.278.71
1,1-Dichloropropene g/L0.50 10.0 2570-130102 2.0410.2
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13093.3 1.709.33
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13099.2 0.8039.92
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13082.1 3.598.21
Ethylbenzene g/L0.50 10.0 2570-130105 1.7010.5
2-Hexanone (MBK)g/L5.0 100 2570-13080.5 1.6680.5
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13097.3 3.149.73
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130103 4.2710.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13092.9 2.979.29
Methylene Chloride g/L5.0 10.0 2570-13099.6 7.509.96
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13081.3 2.1981.3
Naphthalene g/L0.50 10.0 2570-13089.5 15.88.95
n-Propylbenzene g/L0.50 10.0 2570-130100 2.5610.0
Styrene g/L0.50 10.0 2570-13095.7 1.459.57
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13095.8 3.189.58
Tetrachloroethylene g/L0.50 10.0 2570-130101 2.7110.1
Toluene g/L0.50 10.0 2570-130102 1.5610.2
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-13093.9 10.99.39
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13097.9 7.009.79
1,1,1-Trichloroethane g/L0.50 10.0 2570-13098.6 2.509.86
1,1,2-Trichloroethane g/L0.50 10.0 2570-130101 2.0610.1
Trichloroethylene g/L0.50 10.0 2570-13099.9 2.379.99
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130110 5.1211.0
1,2,3-Trichloropropane g/L0.50 10.0 2570-13095.6 2.179.56
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130107 2.7610.7
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13096.8 1.749.68
Vinyl Acetate g/L5.0 100 2570-13080.7 3.9680.7
Vinyl Chloride g/L0.50 10.0 2560-14095.1 2.709.51
m+p Xylene g/L1.0 20.0 2570-130102 1.5020.5
o-Xylene g/L0.50 10.0 2570-130104 1.3410.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.724.9
g/L 25.0 70-130Surrogate: Toluene-d8 98.124.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.024.3
Page 40 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B170179 - SW-846 3510C
[TOC_3]B170179[TOC]
Blank (B170179-BLK1) Prepared: 02/11/17 Analyzed: 02/13/17
C9-C18 Aliphatics g/L100ND
C19-C36 Aliphatics g/L100ND
Unadjusted C11-C22 Aromatics g/L100ND
C11-C22 Aromatics g/L100ND
Acenaphthene g/L2.0ND
Acenaphthylene g/L2.0ND
Anthracene g/L2.0ND
Benzo(a)anthracene g/L2.0ND
Benzo(a)pyrene g/L2.0ND
Benzo(b)fluoranthene g/L2.0ND
Benzo(g,h,i)perylene g/L2.0ND
Benzo(k)fluoranthene g/L2.0ND
Chrysene g/L2.0ND
Dibenz(a,h)anthracene g/L2.0ND
Fluoranthene g/L2.0ND
Fluorene g/L2.0ND
Indeno(1,2,3-cd)pyrene g/L2.0ND
2-Methylnaphthalene g/L2.0ND
Naphthalene g/L2.0ND
Phenanthrene g/L2.0ND
Pyrene g/L2.0ND
n-Decane g/L2.0ND
n-Docosane g/L2.0ND
n-Dodecane g/L2.0ND
n-Eicosane g/L2.0ND
n-Hexacosane g/L2.0ND
n-Hexadecane g/L2.0ND
n-Hexatriacontane g/L2.0ND
n-Nonadecane g/L2.0ND
n-Nonane g/L2.0ND
n-Octacosane g/L2.0ND
n-Octadecane g/L2.0ND
n-Tetracosane g/L2.0ND
n-Tetradecane g/L2.0ND
n-Triacontane g/L2.0ND
Naphthalene-aliphatic fraction g/L2.0ND
2-Methylnaphthalene-aliphatic fraction g/L2.0ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)77.977.9
g/L 100 40-140Surrogate: o-Terphenyl (OTP)85.185.1
g/L 100 40-140Surrogate: 2-Bromonaphthalene 80.880.8
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 99.899.8
LCS (B170179-BS1) Prepared: 02/11/17 Analyzed: 02/13/17
Acenaphthene g/L2.0 100 40-14077.677.6
Acenaphthylene g/L2.0 100 40-14074.174.1
Anthracene g/L2.0 100 40-14085.385.3
Benzo(a)anthracene g/L2.0 100 40-14090.290.2
Benzo(a)pyrene g/L2.0 100 40-14089.189.1
Benzo(b)fluoranthene g/L2.0 100 40-14092.392.3
Benzo(g,h,i)perylene g/L2.0 100 40-14092.192.1
Benzo(k)fluoranthene g/L2.0 100 40-14084.884.8
Chrysene g/L2.0 100 40-14085.585.5
Page 41 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B170179 - SW-846 3510C
LCS (B170179-BS1) Prepared: 02/11/17 Analyzed: 02/13/17
Dibenz(a,h)anthracene g/L2.0 100 40-14094.894.8
Fluoranthene g/L2.0 100 40-14088.888.8
Fluorene g/L2.0 100 40-14082.982.9
Indeno(1,2,3-cd)pyrene g/L2.0 100 40-14095.895.8
2-Methylnaphthalene g/L2.0 100 40-14070.770.7
Naphthalene g/L2.0 100 40-14058.358.3
Phenanthrene g/L2.0 100 40-14088.388.3
Pyrene g/L2.0 100 40-14089.989.9
n-Decane g/L2.0 100 40-14044.544.5
n-Docosane g/L2.0 100 40-14083.083.0
n-Dodecane g/L2.0 100 40-14056.756.7
n-Eicosane g/L2.0 100 40-14084.384.3
n-Hexacosane g/L2.0 100 40-14082.882.8
n-Hexadecane g/L2.0 100 40-14079.479.4
n-Hexatriacontane g/L2.0 100 40-14091.091.0
n-Nonadecane g/L2.0 100 40-14083.083.0
n-Nonane g/L2.0 100 30-14034.034.0
n-Octacosane g/L2.0 100 40-14082.182.1
n-Octadecane g/L2.0 100 40-14085.085.0
n-Tetracosane g/L2.0 100 40-14083.783.7
n-Tetradecane g/L2.0 100 40-14070.470.4
n-Triacontane g/L2.0 100 40-14084.384.3
Naphthalene-aliphatic fraction g/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction g/L2.0 100 0-5ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)76.476.4
g/L 100 40-140Surrogate: o-Terphenyl (OTP)87.687.6
g/L 100 40-140Surrogate: 2-Bromonaphthalene 82.282.2
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 100100
LCS Dup (B170179-BSD1) Prepared: 02/11/17 Analyzed: 02/13/17
Acenaphthene g/L2.0 100 2540-14075.8 2.3375.8
Acenaphthylene g/L2.0 100 2540-14072.6 2.0272.6
Anthracene g/L2.0 100 2540-14079.6 7.0379.6
Benzo(a)anthracene g/L2.0 100 2540-14084.2 6.8184.2
Benzo(a)pyrene g/L2.0 100 2540-14083.2 6.7683.2
Benzo(b)fluoranthene g/L2.0 100 2540-14086.6 6.3886.6
Benzo(g,h,i)perylene g/L2.0 100 2540-14087.1 5.6287.1
Benzo(k)fluoranthene g/L2.0 100 2540-14079.6 6.3679.6
Chrysene g/L2.0 100 2540-14079.9 6.7579.9
Dibenz(a,h)anthracene g/L2.0 100 2540-14089.4 5.8689.4
Fluoranthene g/L2.0 100 2540-14082.8 7.0182.8
Fluorene g/L2.0 100 2540-14079.3 4.5279.3
Indeno(1,2,3-cd)pyrene g/L2.0 100 2540-14090.5 5.6290.5
2-Methylnaphthalene g/L2.0 100 2540-14070.3 0.68470.3
Naphthalene g/L2.0 100 2540-14059.2 1.5559.2
Phenanthrene g/L2.0 100 2540-14082.5 6.8282.5
Pyrene g/L2.0 100 2540-14083.7 7.0883.7
n-Decane g/L2.0 100 2540-14045.8 2.8145.8
n-Docosane g/L2.0 100 2540-14078.1 6.0678.1
n-Dodecane g/L2.0 100 2540-14057.4 1.2157.4
n-Eicosane g/L2.0 100 2540-14079.5 5.9079.5
n-Hexacosane g/L2.0 100 2540-14078.1 5.8378.1
Page 42 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B170179 - SW-846 3510C
LCS Dup (B170179-BSD1) Prepared: 02/11/17 Analyzed: 02/13/17
n-Hexadecane g/L2.0 100 2540-14076.4 3.9276.4
n-Hexatriacontane g/L2.0 100 2540-14087.5 3.8887.5
n-Nonadecane g/L2.0 100 2540-14078.3 5.7478.3
n-Nonane g/L2.0 100 2530-14035.5 4.3535.5
n-Octacosane g/L2.0 100 2540-14077.8 5.4677.8
n-Octadecane g/L2.0 100 2540-14080.5 5.4980.5
n-Tetracosane g/L2.0 100 2540-14078.8 6.0778.8
n-Tetradecane g/L2.0 100 2540-14070.1 0.44170.1
n-Triacontane g/L2.0 100 2540-14080.1 5.1180.1
Naphthalene-aliphatic fraction g/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction g/L2.0 100 0-5ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)68.868.8
g/L 100 40-140Surrogate: o-Terphenyl (OTP)81.481.4
g/L 100 40-140Surrogate: 2-Bromonaphthalene 82.282.2
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 92.692.6
Page 43 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B170421 - MA VPH
[TOC_3]B170421[TOC]
Blank (B170421-BLK1) Prepared & Analyzed: 02/13/17
Unadjusted C5-C8 Aliphatics g/L100ND
C5-C8 Aliphatics g/L100ND
Unadjusted C9-C12 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10542.2
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10843.0
LCS (B170421-BS1) Prepared & Analyzed: 02/13/17
Benzene g/L1.0 100 70-13098.198.1
Butylcyclohexane g/L1.0 100 70-13082.382.3
Decane g/L1.0 100 70-13086.086.0
Ethylbenzene g/L1.0 100 70-13096.896.8
Methyl tert-Butyl Ether (MTBE)g/L1.0 100 70-13094.494.4
2-Methylpentane g/L1.0 100 70-13099.499.4
Naphthalene g/L5.0 100 70-130101101
Nonane g/L1.0 100 70-13081.381.3
Pentane g/L1.0 100 70-13096.696.6
Toluene g/L1.0 100 70-13097.697.6
1,2,4-Trimethylbenzene g/L1.0 100 70-13094.394.3
2,2,4-Trimethylpentane g/L1.0 100 70-13086.286.2
m+p Xylene g/L2.0 200 70-13096.3193
o-Xylene g/L1.0 100 70-13097.097.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10843.2
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11144.4
LCS Dup (B170421-BSD1) Prepared & Analyzed: 02/13/17
Benzene g/L1.0 100 2570-13099.3 1.2899.3
Butylcyclohexane g/L1.0 100 2570-13083.2 1.0983.2
Decane g/L1.0 100 2570-13087.8 2.0487.8
Ethylbenzene g/L1.0 100 2570-13097.8 1.1197.8
Methyl tert-Butyl Ether (MTBE)g/L1.0 100 2570-13099.9 5.6999.9
2-Methylpentane g/L1.0 100 2570-13098.9 0.51298.9
Naphthalene g/L5.0 100 2570-13099.1 1.7299.1
Nonane g/L1.0 100 2570-13082.4 1.3882.4
Pentane g/L1.0 100 2570-13096.2 0.41896.2
Toluene g/L1.0 100 2570-13098.8 1.2898.8
1,2,4-Trimethylbenzene g/L1.0 100 2570-13095.6 1.2995.6
Page 44 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B170421 - MA VPH
LCS Dup (B170421-BSD1) Prepared & Analyzed: 02/13/17
2,2,4-Trimethylpentane g/L1.0 100 2570-13085.8 0.53685.8
m+p Xylene g/L2.0 200 2570-13097.5 1.18195
o-Xylene g/L1.0 100 2570-13098.0 1.0698.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11044.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10943.7
Page 45 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
Page 46 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Water
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PNaphthalene
MADEP-VPH-04-1.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
[TOC_1]Certifications[TOC]
Page 47 of 54
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 02/1/2018
M-MA100Massachusetts DEPMA 06/30/2017
PH-0567Connecticut Department of Publilc HealthCT 09/30/2017
10899 NELAPNew York State Department of HealthNY 04/1/2017
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2018
LAO00112Rhode Island Department of HealthRI 12/30/2017
652North Carolina Div. of Water QualityNC 12/31/2017
MA007 NELAPNew Jersey DEPNJ 06/30/2017
E871027 NELAPFlorida Department of HealthFL 06/30/2017
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2017
2011028State of MaineME 06/9/2017
460217Commonwealth of VirginiaVA 12/14/2017
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2017
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Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 8
17B0707-01 8
17B0707-02 12
Sample Preparation Information 16
QC Data 17
Volatile Organic Compounds by GC/MS 17
B170618 17
B170790 21
Petroleum Hydrocarbons Analyses - EPH 25
B170683 25
Petroleum Hydrocarbons Analyses - VPH 28
B170720 28
B170822 29
Flag/Qualifier Summary 31
Certifications 32
Chain of Custody/Sample Receipt 35
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