WA-1016_12613_CA_RPTS_20230130_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

January 30, 2023

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
January 2023
Phelps Amoco
US Highway 64 West
Creswell, Washington County
North Carolina
Facility ID Number: 0-00-0000006306
Incident Number: 12613
GRI Project Number: 2720

Dear Mr. Edwards,

Please find enclosed the referenced report, for the abovementioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: North East Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Ground Water Monitoring Report
January 2023
Phelps Amoco
US Highway 64 West
Creswell, Washington County
North Carolina
Facility ID Number: 0-00-0000006306
Incident Number: 12613
GRI Project Number: 2720

Prepared for:

North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910

January 30, 2023

Colton Coolbaugh
Staff Scientist
William Regenthal, P. G.
Report Editor

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
i
SITE INFORMATION
1. Site Identification
 Phelps Amoco (Facility ID 0-00-0000006306)
 Incident Number 12613 – Intermediate Risk (I140D)
 Location of Source Area: US Highway 64 West
Creswell, NC 27962
Washington County
35.8868333°N, 76.4249722°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, NC 27910
[e-mail]
252-862-0236

UST Operator
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, NC 27910
[e-mail]
252-862-0236

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110

[e-mail]
704-845-4010

Property Owner
NC DOT
1501 Mail Service Center
Raleigh, NC 27699

Email Unknown
919-715-7000

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 402
704-529-6364

Property Occupant
US Highway 64

3. Information about Release
 Release was discovered in May 1994
 An unknown amount of product was released from the leaking UST System
 One 1,000-gallon diesel and three 4,000-gallon gasoline USTs and associated pumps and product
piping were removed in May 1994; one 6,000-gallon gasoline, two 4,000-gallon gasoline, one
1,000-gallon diesel and one 1,000-gallon kerosene USTs were removed from the site in March
2002.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
ii
EXECUTIVE SUMMARY
The former Phelps Amoco site is located along US Highway 64 West, west of the town of Creswell,
Washington County, North Carolina. One 1,000-gallon diesel and three 4,000-gallon gasoline USTs and
associated pumps and product piping were removed in May 1994; one 6,000-gallon gasoline, two 4,000-
gallon gasoline, one 1,000-gallon diesel and one 1,000-gallon kerosene USTs were removed from the site
in March 2002. The adjoining properties are agricultural and residential. The risk classification is currently
ranked as intermediate due to the historical presence of free product and ground water contamination
exceeding the GCL for benzene. Municipal water is available to the surrounding area.

On January 10, 2019, A Plume Stability Analysis using the GSI Mann-Kendall Toolkit was completed. The
results of the Plume Stability Analysis indicate that benzene concentrations are decreasing in MW-14,
while no trend is observed for MW-21.

On January 10, 2023, six monitoring wells were gauged, purged and sampled. Concentrations of individual
BTEX constituents, naphthalene, MTBE, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene
and/or 1,3,5-trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) as
specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-14, MW-
21 and MW-22. A concentration of benzene that exceeded the GCL was reported in the ground water
sample collected from MW-21.

Contaminant mass at the site has decreased by 34.4% since the June 2012 baseline assessment.

Based on this information, GRI recommends that soil and ground water sampling in the vicinity of MW-21
should be conducted in order to define a potential soil excavation area. Soil excavation appears to be the
most feasible contaminant reduction option due to logistical and safety concerns. The soil and ground
water sampling activities should be conducted in the second quarter of 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720

TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 FREE PRODUCT REMOVAL ........................................................................................................2
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 PROPOSED REMEDIAL ACTION .................................................................................................4
6.0 CONCLUSIONS .........................................................................................................................5
7.0 LIMITATIONS ...........................................................................................................................5
8.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Free Product Recovery Results
Table 5: Free Product Recovery Event Information
Table 6: Free Product Recovery Cost Summary
Table 7: Well Construction and Gauging Information
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples
Appendix C: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the January 2023 ground water sampling event at the Phelps Amoco site. The
site is located along US Highway 64 West in Creswell, Washington County, North Carolina (Figure 1). These
activities were conducted in accordance with GRI Proposal No. 22-850, which was submitted to the North
Carolina Department of Environmental Quality (NCDEQ) on November 28, 2022, and was approved as
Task Authorization No. 12613-032 on December 1, 2022. State correspondence has been included as
Appendix A.

The site is currently owned by North Carolina Department of Transportation and formerly operated as a
petroleum retail facility. The property is currently part of US Highway 64. One 1,000-gallon diesel and
three 4,000-gallon gasoline USTs and associated pumps and product piping were removed in May 1994;
one 6,000-gallon gasoline, two 4,000-gallon gasoline, one 1,000-gallon diesel and one 1,000-gallon
kerosene USTs were removed from the site in March 2002. A release was confirmed at the site in May
1994. UST owner/operator information and UST system information are included as Tables 1 and 2,
respectively. The Registered Tank Report is shown below:

The surrounding area is a mixture of agricultural and residential properties. The site is primarily capped
with grass and asphalt. The overall topography at the site is embanked due to the highway. Eleven Type
II monitoring wells (MW-1 through MW-3 and MW-5 through MW-8 and MW-10 through MW-13) and
two Type III monitoring wells (MWD-4 and MWD-9) were installed at the site during previous ground
water assessment activities. Prior to excavation activities, CES abandoned MW-1 through MW-5, MW-7,

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
2
MW-8, MW-9, MW-12 and water supply well DW-1. Monitoring wells MW-10 and MW-11 and water
supply wells DW-2 and DW-3 were reportedly destroyed by the NCDOT and therefore were not properly
abandoned. Nine additional Type II monitoring wells (MW-14 through MW-22) were installed by GRI to
replace monitoring wells abandoned and/or destroyed during CAP implementation activities and NCDOT
construction in 2002.

In July 2008, GRI personnel conducted an updated receptor survey at the site. One water supply well
(WSW-1) was observed during July 2008 updated receptor survey activities, but has since been confirmed
as abandoned and/or destroyed during a site visit and meeting with the property owner in June 2009.
Municipal water is available to the surrounding properties. No surface water bodies were identified within
a 500-foot radius of the site. The site does not lie within a designated wellhead protection area. Adjacent
property owner information is presented in Table 3. A Site Map showing the locations of the monitoring
wells on-site has been included as Figure 2. A Site Vicinity Map showing the locations of property
boundaries is included as Figure 3.

A CAP for the site developed by TRC Triangle (TRC) proposed remediation using soil excavation followed
by natural attenuation and water supply well abandonment. The proposed remediation method was
designed to accommodate the North Carolina Department of Transportation (NCDOT) plans to raze the
facility and construct a new US Highway 64 over the site. As part of the CAP, the UST system installed in
July 1994, associated pumps and product piping, as well as 3,909.89 tons of contaminated soil were
removed from the site in March and April 2002 by Coastal Environmental Services, Inc. (CES).
2.0 FREE PRODUCT REMOVAL
Free product has historically been present in MW-14 and MW-21. Two AFVR events were conducted at
the site between April 2013 and June 2014. A total of 4,175 gallons of fluids, including 2.45 gallons of
liquid and vapor phase free product have been recovered during past AFVR events. Free product was not
observed during the January 2023 ground water sampling activities. Summaries of the historical AFVR
events conducted by GRI are shown in Tables 4 and 5. A cost summary of the events is shown in Table 6.
Free product was last observed at the site in May 2013.
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On January 10, 2023, six Type II monitoring wells (MW-14, MW-15, MW-17, MW-20, MW-21 and MW-22)
were gauged, purged and sampled. No free product was observed during the January 2022 ground water
sampling activities. Depths to ground water in the Type II monitoring wells ranged from 1.23 feet to 9.43
feet below the tops of well casings. Ground water elevations ranged from 96.76 to 97.79 feet. Ground
water flow direction was convergent toward MW-20 and MW-21 during the January 2023 ground water
sampling event. The average horizontal hydraulic gradient was less than 0.01 feet per foot. Well
construction and gauging information is presented in Table 7. A Water Table Surface Map for the January
2023 ground water sampling event is included as Figure 4. A summary of the ground water gauging data
is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
3
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-14 2 – 12 12 99.66 2.84 --- 96.82
MW-15 2 – 12 12 100.00 2.96 --- 97.04
MW-17 10 – 20 20 106.27 9.43 --- 96.84
MW-20 10 – 20 20 105.71 8.95 --- 96.76
MW-21 3 – 12 12 99.19 2.43 --- 96.76
MW-22 2 -- 11 11 99.02 1.23 --- 97.79

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of individual BTEX constituents, naphthalene, MTBE,
isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-14, MW-21 and MW-
22. A Concentration of benzene that exceeded the GCL was reported in the ground water sample
collected from MW-21. A summary of the analytical results for ground water samples collected on January
10, 2023, is presented in Table 8. A Ground Water Quality Map based on the January 2023 data is included
as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the
monitoring wells during the January 2023 sampling event has been included as Appendix B. A summary
of the current ground water analytical data is shown below:

Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-14 583 29.9 105 86.2 <1.40 28.3
MW-15 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-17 0.250 J 0.949 <0.170 0.823 J <0.140 <0.470
MW-20 0.435 J 1.42 0.221 J 1.19 J <0.140 <0.470
MW-21 21,000 32,000 1,930 11,300 50.4 718
MW-22 2.00 8.76 1.72 9.87 <0.140 1.44

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the June 2012 ground water sampling event, as well as the maximum
historical water column height observed in the area. The contaminant plume consists of one area (Area
1) based on the benzene concentrations that exceeded the GCL in June 2012 (MW-14 and MW-21). The
contaminant mass has been reduced by 34.4% since the baseline assessment. Contaminant mass
calculations have been included as Appendix C. A map of the contaminant mass area has been included
as Figure 6. A chart depicting the overall trend for contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
4

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 0.75 to 8 feet BGS.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Free product has historically been observed at the site. Please refer to the project file for additional free
product recovery information. Free product has not been observed at the site since 2013.

5.0 PROPOSED REMEDIAL ACTION
The former site has been razed and replaced with a major highway. The site risk classification is ranked
as intermediate based on the past presence of free product and contaminant concentrations exceeding
the GCL for benzene. Free product has not been observed at the site since 2013. Contaminant
concentrations remain greater than the GCL for benzene in MW-21. The Mann-Kendall Toolkit for Plume
Stability indicated in 2019 that contaminant concentrations in MW-21 were exhibiting no discernable
trend. Two AFVR events have been conducted during past site activities, with limited results. More
aggressive means of contaminant reduction activities via ground water extraction are limited due to
logistical and safety concerns.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: January 30, 2023 Phelps Amoco
Project Manager: Colton Coolbaugh GRI Project No. 2720
5
Due to MW-21 being the only monitoring well with contaminant concentrations that exceed the GCLs and
the shallow depth to ground water at the site, a soil excavation in the immediate vicinity of MW-21 may
be feasible.

In order to define a potential area of soil excavation, multiple temporary monitoring wells should be
installed in the vicinity of MW-21. Ground water samples should be collected from the temporary wells
in order to define the benzene GCL plume. Soil samples could be collected during the temporary
monitoring well installation activities to define the vertical extent of the proposed soil excavation.
6.0 CONCLUSIONS
 On January 10, 2023, six Type II monitoring wells were gauged, purged and sampled. Ground
water flow was convergent toward MW-20 and MW-21 with a horizontal gradient of less than
0.01 feet per foot.
 Concentrations of individual BTEX constituents, naphthalene, MTBE, isopropylbenzene, n-
propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-14, MW-21 and MW-22. A
concentration of benzene that exceeded the GCL was reported in the ground water sample
collected from MW-21.
 Contaminant mass at the site was reduced by 34.4% since the June 2012 baseline assessment.
 Based on this information, GRI recommends that soil and ground water sampling in the vicinity of
MW-21 should be conducted in order to define a potential soil excavation area. Soil excavation
appears to be the most feasible contaminant reduction option due to logistical and safety
concerns. The soil and ground water sampling activities should be conducted in the second
quarter of 2023.
7.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application
to the referenced site in Washington County, North Carolina. The activities were conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

8.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO

FIGURES
(Destroyed/Abandoned)

TABLES
UST ID Number A1 - A5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-2 Facility ID Number
Owner or Operator?
Owner/Operator
Post Office Box 1386, Ahoskie, North Carolina 27910 Unknown
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
North East Oil Company, Inc.3/9/1961 - 5/31/1994
Post Office Box 1386, Ahoskie, North Carolina 27910 Unknown
00-0-0000006306
Name of Owner or Operator Dates of Ownership / Operation
North East Oil Company, Inc.3/4/1982 - 5/31/1994
Address Telephone Number
Address Telephone Number
Post Office Box 1386, Ahoskie, North Carolina 27910 Unknown
00-0-0000006306
00-0-0000006306
Name of Owner or Operator Dates of Ownership / Operation
North East Oil Company, Inc.3/8/1966 - 5/31/1994
Post Office Box 1386, Ahoskie, North Carolina 27910 Unknown
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
00-0-0000006306
Name of Owner or Operator Dates of Ownership / Operation
North East Oil Company, Inc.7/13/1994 - 3/29/2002
Address
Page 1 of 1
Date: 03/17/2021
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 4,000 3/9/1961 Single Wall Steel Unknown Single Wall Steel Removed No
2 Gasoline 4,000 3/9/1961 Single Wall Steel Unknown Single Wall Steel Removed No
3 Gasoline 4,000 3/4/1982 Single Wall Steel Unknown Single Wall Steel Removed No
4 Diesel 1,000 3/8/1966 Single Wall Steel Unknown Single Wall Steel Removed No
A1 Diesel 1,000 7/13/1994 Single Wall Steel Unknown Other Removed Yes
A2 Kerosene 1,000 7/13/1994 Single Wall Steel Unknown Other Removed Yes
A3 Gasoline 4,000 7/13/1994 Single Wall Steel Unknown Other Removed Yes
A4 Gasoline 6,000 7/13/1994 Single Wall Steel Unknown Other Removed Yes
A5 Gasoline 4,000 7/13/1994 Single Wall Steel Unknown Other Removed Yes
Notes:
• FRP: Fiberglass reinforced plastic.
TABLE 2
UST SYSTEM INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Facility ID # : 00-0-0000006306
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Date: 12/07/11 Facility ID # : 00-0-0000006306
Parcel Number Owner Name Address
0417-71-3109 (Site)NC DEPT. OF TRANSPORTATION NEW US HWY 64
CRESWELL, NC 27928
0417-71-6242 TRUSTEES ST. JOHN MISSIONARY
BAPTIST c/o ELWOOD PHELPS
22649 US HWY 64 EAST
CRESWELL, NC 27928
0417-71-8250 SANTIAGO, ARMANI C.22451 US HIGHWAY 64 EAST
CRESWELL, NORTH CAROLINA 27928
0417-70-7669 SWETT, MARVELL & EFFIE 25025 US HWY 64 EAST
CRESWELL, NC 27928
0417-70-3851 SWETT, MARVELL, JR. & LYNN R.1091 TOM PEPPER RD
CRESWELL, NC 27928
0417-70-2627 MRS. SAM S. WOODLEY, ESTATE
C/O SAMUEL S. WOOD, JR.
POST OFFICE BOX 7100
ROCKY MOUNT, NORTH CAROLINA 27804
0417-71-1123 PHELPS, ELWOOD AND KATIE S.10866 NC HIGHWAY 94
NORTH CRESWELL, NC 27928
Note:
• Properties are keyed to Figure 3.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Page 1 of 1
Date: 08/01/14 Facility ID#: 0-006306
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
Before Recovery
(feet)
Product Thickness
After Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-14 0.00 0.00
MW-21 0.00 0.00
MW-14 0.00 0.00
MW-21 0.00 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and Field Notes).
• NM: Not measured.
1.61
TABLE 4
FREE PRODUCT RECOVERY RESULTS
FORMER PHELPS AMOCO (INCIDENT NO. 12163)
Interface probe at top-of-casing
Gasoline 04/03/13 AFVR 2 2,260 0.84
Gasoline 07/23/14 AFVR 2 1,915
Date: 08/01/14 Facility ID #: 0-006306
MW-14
MW-21
MW-14
MW-21
2.45 4,175 0.00 2.45
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
21.2
TABLE 5
FREE PRODUCT RECOVERY EVENT INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12163)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
0.84 2,260 0.00 0.84
07/23/14 AFVR 4,024 238.3 33.7 1.61 1,915 0.00 1.61
04/03/13 AFVR 3,032 174.9
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Amount of Product Removed (in gallons)
Current Event 1,916.61 1.61
Total To Date 4,177.45 2.45
Date: 08/01/14 Facility ID #: 0-006306
Wells Included
in Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product
Recovered
(gallons)
Total Fluids
Recovered
(gallons)
Cost of Free
Product
Recovery Event
Cost Per Gallon
Free Product
Cost Per Gallon
Total Fluids
MW-14
MW-21
MW-14
MW-21
2.45 4,175.06 $7,845.96 $3,202.43 $1.88
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TABLE 6
FREE PRODUCT RECOVERY COST SUMMARY
FORMER PHELPS AMOCO (INCIDENT NO. 12163)
Comments
AFVR 04/03/13 0.84 2,260.02 $3,957.35 $4,711.13
TOTAL (to date)
$1.75
Cost per gallon for the event is based
on a total volume of 2,260.02 gallons
of contaminated water and vaporized
product.
AFVR 07/23/14 1.61 1,915.04 $3,888.61 $2,415.29 $2.03
Cost per gallon for the event is based
on a total volume of 1,915.04 gallons
of contaminated water and vaporized
product.
Date: 01/10/2023
EPA
504.1
EPA
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 3,000 28,500 24,100 50 15,000 NE NE NE NE
11/11/08 <0.11 <0.10 <0.13 <0.22 <0.10 <0.10 <0.10 <0.15 <0.20 <0.11 <0.13 <0.10 <0.13 <0.02017 3.4 170 <211 <111 <211
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 5 <100 <100 NR <100
06/08/11 <0.13 0.37 J <0.15 0.81 J <0.13 0.54 <0.16 <0.10 <0.11 <0.11 <0.18 0.72 J 0.21 J NR 6.3 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/08 5,400 940 550 1,700 <10 49 JB <10 30 J <20 52 J 23 J 170 78 J <0.02059 5.5 2,500 1,100 <105 1,100 E
06/02/09 14,300 15,600 1,350 7,080 <16.5 459 51.1 60 J <83.5 110 <16.5 1,210 358 NR 9.03 12,500 3,600 NR 3,820
06/08/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
11/17/11 8,970 7,770 1,050 6,020 <33 261 <41 46.4 J <27 109 J <45 1,200 416 NR NR NR NR NR NR
06/12/12 14,600 17,700 1,540 8,630 <33 343 <41 54.7 J <27 131 <45 1,410 438 NR NR NR NR NR NR
05/07/13 12,500 15,800 1,760 10,600 <10 483 32.9 J 92.0 <10 266 <10 2,380 699 NR NR NR NR NR NR
10/03/13 13,500 17,600 1,420 7,970 <50 275 <50 <50 <50 114 J <50 1,040 304 NR NR NR NR NR NR
09/11/14 7,030 8,080 1,150 6,750 <20 289 <20 56.2 J <20 151 <20 1,390 412 NR NR NR NR NR NR
04/01/15 8,340 9,980 1,030 6,350 <8.2 315 26.4 50.0 <8.0 124 <7.3 1,230 390 NR NR NR NR NR NR
11/11/15 1,750 1,310 337 1,580 <8.2 115 <8.2 17.3 J <8.0 49.3 <7.3 445 146 NR NR NR NR NR NR
07/18/16 2,920 3,960 1,250 5,350 <3.1 568 15.3 140 <3.1 442 <3.1 1,960 1,160 NR NR NR NR NR NR
02/07/17 1,370 1,370 130 716 <6.3 28.2 <6.3 <6.3 <6.3 <6.3 <6.3 91.9 29.3 NR NR NR NR NR NR
05/02/17 225 466 88.1 602 <1.3 36.8 <1.3 9.8 <1.3 18.7 <1.3 230 78.0 NR NR NR NR NR NR
10/31/17 1,310 1,970 255 1,790 <6.3 142 <6.3 23.1 J <6.3 57.1 <6.3 785 276 NR NR NR NR NR NR
12/27/18 194 76.9 27.7 102 <0.63 6.4 <0.63 1.6 J <0.63 3.5 <0.63 26.9 8.8 NR NR NR NR NR NR
02/23/21 870 121 193 465 <3.1 56.3 <3.1 8.1 J <3.1 18.5 <3.1 113 35.6 NR NR NR NR NR NR
01/10/23 583 29.9 105 86.2 <1.40 28.3 <1.50 7.78 <5.00 18.2 <1.80 46.8 4.62 J NR NR NR NR NR NR
11/11/08 2.6 4.0 0.87 J 4.6 <0.10 <0.10 <0.10 <0.15 <0.20 0.25 J <0.13 1.1 0.42 J <0.02077 19.2 <100 <211 <111 <211
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 30.2 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 48.4 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/13/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/10/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.180 <0.190 <0.180 NR NR NR NR NR NR
Analytical Method EPA Method 6200B/ EPA Method 610 MADEP VPH and/or EPH
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Facility ID # : 00-0-0000006306 TrichloroetheneContaminant of Concern BenzeneTolueneEthylbenzeneXylenesMTBEC19-C36 AliphaticsC9-C22 AromaticsMACs (μg/l)
GCL (μg/l)
MW-6 1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneEDBLeadC5-C8 AliphaticsC9-C18 AliphaticsNaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-PropylbenzeneMW-14
MW-15
Page 1 of 3
Date: 01/10/2023
EPA
504.1
EPA
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 3,000 28,500 24,100 50 15,000 NE NE NE NE
Analytical Method EPA Method 6200B/ EPA Method 610 MADEP VPH and/or EPH
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Facility ID # : 00-0-0000006306 TrichloroetheneContaminant of Concern BenzeneTolueneEthylbenzeneXylenesMTBEC19-C36 AliphaticsC9-C22 AromaticsMACs (μg/l)
GCL (μg/l)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneEDBLeadC5-C8 AliphaticsC9-C18 AliphaticsNaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-Propylbenzene11/11/08 <0.11 <0.10 <0.13 <0.22 <0.10 <0.10 <0.10 <0.15 <0.20 <0.11 <0.13 <0.10 <0.13 <0.02244 1.6 J <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 2.01 J <100 <100 NR <100
06/08/11 <0.13 0.37 J <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 7.9 <35 <145 <110 <145
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/11/08 9.2 100 73 610 <0.50 23 B <0.50 18 <1.0 24 <0.65 100 53 <0.02047 <1.5 1,200 470 182 420 E
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 5.06 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 23.0 <35 <535 <500 <535
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
02/23/21 <0.13 0.27 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/10/23 0.250 J 0.949 <0.170 0.823 J <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.180 0.295 J <0.180 NR NR NR NR NR NR
11/10/08 <0.14 0.75 J <0.15 <0.12 <0.25 <0.070 <0.11 <0.12 <0.20 <0.22 <0.15 <0.14 <0.13 <0.02000 26.6 <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 7.57 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 17.6 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/10/08 800 26 190 170 <0.25 65 0.47 J 13 2.3 J 21 <0.15 3.0 1.9 <0.02000 6.7 2,500 300 <105 210
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 12.5 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 59.4 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/10/08 0.28 J <0.19 0.18 J <0.12 3.1 0.40 J <0.11 <0.12 <0.20 <0.22 <0.15 <0.14 <0.13 <0.02000 10.0 <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 10.7 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR <5.0 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
02/23/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/10/23 0.435 J 1.42 0.221 J 1.19 J <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.180 0.455 J <0.180 NR NR NR NR NR NR
MW-16
MW-18
MW-19
MW-20
MW-17
Page 2 of 3
Date: 01/10/2023
EPA
504.1
EPA
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 3,000 28,500 24,100 50 15,000 NE NE NE NE
Analytical Method EPA Method 6200B/ EPA Method 610 MADEP VPH and/or EPH
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Facility ID # : 00-0-0000006306 TrichloroetheneContaminant of Concern BenzeneTolueneEthylbenzeneXylenesMTBEC19-C36 AliphaticsC9-C22 AromaticsMACs (μg/l)
GCL (μg/l)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneEDBLeadC5-C8 AliphaticsC9-C18 AliphaticsNaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-Propylbenzene06/08/11 19,400 20,900 1,300 7,400 <65 565 806 72.4 J <54 215 J <90 2,260 632 NR 98.4 78,300 84,300 1,000 33,400
06/12/12 26,000 32,000 1,780 11,800 <65 564 1,020 78.4 J <54 273 <90 3,410 1,110 NR NR NR NR NR NR
05/07/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/03/13 26,500 40,900 1,930 10,500 <100 380 J 855 <100 <100 172 J <100 1,350 386 J NR NR NR NR NR NR
09/11/14 22,800 22,800 1,880 11,500 85.1 J 622 <50 67.1 J <50 236 J <50 2,270 645 NR NR NR NR NR NR
04/01/15 26,900 36,700 1,670 11,200 191 J 1,630 1,230 <120 <160 177 J <150 2,280 601 NR NR NR NR NR NR
11/11/15 24,800 18,300 1,760 9,420 84.8 686 212 57.8 32.4 J 197 <15 2,100 557 NR NR NR NR NR NR
07/18/16 30,800 47,100 2,970 15,300 159 1,380 1,410 144 50.1 562 <13 3,800 1,470 NR NR NR NR NR NR
02/07/17 32,700 49,200 1,920 10,200 <130 541 1,190 <130 <130 <130 <130 1,190 335 J NR NR NR NR NR NR
05/02/17 30,400 42,400 1,890 11,100 124 669 1,090 45.9 J 46.0 J 170 <13 1,740 445 NR NR NR NR NR NR
10/31/17 9,680 30,700 2,060 12,700 <63 851 172 J <63 <63 176 J <63 2,010 568 NR NR NR NR NR NR
12/27/18 28,200 31,600 1,520 9,020 <130 362 J 157 J <130 <130 <130 <130 1,180 351 J NR NR NR NR NR NR
02/23/21 25,300 13,300 1,600 6,170 <130 373 J <130 <130 <130 <130 <130 948 322 J NR NR NR NR NR NR
01/10/23 21,000 32,000 1,930 11,300 50.4 718 <1.50 82.3 26.6 276 <1.80 2,090 765 NR NR NR NR NR NR
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 874 <35 <535 <500 <535
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
01/10/23 2.00 8.76 1.72 9.87 <0.140 1.44 <0.150 <0.180 <0.500 0.705 <0.180 5.43 1.67 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
07/18/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
02/07/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/31/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.44 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
Trip Blank 01/10/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.150 <0.180 <0.500 <0.190 <0.180 <0.190 <0.180 NR NR NR NR NR NR
Notes:
• GCL: Gross contamination level.
• NE: Standard not established.
• NS: Not sampled
• Concentrations in bold face type exceeded the 2L standard; concentrations in italics exceeded the GCLs.
• J: The compound is present, but the calculated result is less than the EQL.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• Results reported in µg/l (micrograms per liter).
• 2L Standard: as specified in T15A NCAC 2L.0202.
MW-21
• < : Less than the method detection limit specified in the analytical report.
• B: Compound was also detected in the method blank.
MW-22
MW-23
MW-24
Page 3 of 3

APPENDICES

APPENDIX A
State Correspondence
2720 Received DEC 02 2022

APPENDIX B
Laboratory Report – Ground Water Samples

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/18/2023
Geological Resources, Inc. Ethan Rogerson
113 W. Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-011-0002 Client Project Description: Former Phelps Amoco
GRI #2720
Dear Ethan Rogerson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 43
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-011-0002
Page 2 of 43
Report Number:
Sample Summary Table
Client Project Description:
23-011-0002
Former Phelps Amoco
GRI #2720
Lab No Client Sample ID Matrix Date Collected Date Received
01/10/2023 08:31Aqueous 97215 Trip Blank 01/11/2023 09:50
01/10/2023 09:57Aqueous 97216 MW-14 01/11/2023 09:50
01/10/2023 10:12Aqueous 97217 MW-15 01/11/2023 09:50
01/10/2023 10:26Aqueous 97218 MW-17 01/11/2023 09:50
01/10/2023 10:41Aqueous 97219 MW-22 01/11/2023 09:50
01/10/2023 10:58Aqueous 97220 MW-21 01/11/2023 09:50
01/10/2023 11:14Aqueous 97221 MW-20 01/11/2023 09:50
Page 3 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0002
Report Limit
Project:Former Phelps Amoco
V 97216MW-14
583 01/17/2023 08:576200BBenzeneµg/L 1.80
J3.26 01/17/2023 08:576200Bn-Butylbenzene µg/L 1.80
105 01/17/2023 08:576200BEthylbenzeneµg/L 1.70
7.78 01/17/2023 08:576200BIsopropylbenzeneµg/L 1.80
28.3 01/17/2023 08:576200BNaphthaleneµg/L 4.70
18.2 01/17/2023 08:576200Bn-Propylbenzene µg/L 1.90
29.9 01/17/2023 08:576200BTolueneµg/L 2.20
46.8 01/17/2023 08:576200B1,2,4-Trimethylbenzene µg/L 1.90
J4.62 01/17/2023 08:576200B1,3,5-Trimethylbenzene µg/L 1.80
12.3 01/17/2023 08:576200Bo-Xylene µg/L 2.10
73.9 01/17/2023 08:576200Bm,p-Xylene µg/L 4.20
86.2 01/17/2023 08:576200BXylene (Total)µg/L 2.10
V 97217MW-15
J2.77 01/17/2023 06:516200BAcetoneµg/L 1.80
V 97218MW-17
J0.250 01/17/2023 07:166200BBenzeneµg/L 0.180
0.949 01/17/2023 07:166200BTolueneµg/L 0.220
J0.295 01/17/2023 07:166200B1,2,4-Trimethylbenzene µg/L 0.190
J0.275 01/17/2023 07:166200Bo-Xylene µg/L 0.210
J0.548 01/17/2023 07:166200Bm,p-Xylene µg/L 0.420
J0.823 01/17/2023 07:166200BXylene (Total)µg/L 0.210
V 97219MW-22
J1.96 01/17/2023 07:426200BAcetoneµg/L 1.80
2.00 01/17/2023 07:426200BBenzeneµg/L 0.180
0.644 01/17/2023 07:426200Bn-Butylbenzene µg/L 0.180
1.72 01/17/2023 07:426200BEthylbenzeneµg/L 0.170
1.44 01/17/2023 07:426200BNaphthaleneµg/L 0.470
0.705 01/17/2023 07:426200Bn-Propylbenzene µg/L 0.190
8.76 01/17/2023 07:426200BTolueneµg/L 0.220
5.43 01/17/2023 07:426200B1,2,4-Trimethylbenzene µg/L 0.190
1.67 01/17/2023 07:426200B1,3,5-Trimethylbenzene µg/L 0.180
2.87 01/17/2023 07:426200Bo-Xylene µg/L 0.210
7.00 01/17/2023 07:426200Bm,p-Xylene µg/L 0.420
9.87 01/17/2023 07:426200BXylene (Total)µg/L 0.210
Page 4 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0002
Report Limit
Project:Former Phelps Amoco
V 97220MW-21
21000 01/18/2023 11:216200BBenzeneµg/L 180
75.1 01/17/2023 09:226200Bn-Butylbenzene µg/L 1.80
18.1 01/17/2023 09:226200Bsec-Butyl benzene µg/L 2.00
26.6 01/17/2023 09:226200BDi-Isopropyl Ether (DIPE)µg/L 5.00
1930 01/18/2023 11:216200BEthylbenzeneµg/L 170
82.3 01/17/2023 09:226200BIsopropylbenzeneµg/L 1.80
10.8 01/17/2023 09:226200B4-Isopropyl toluene µg/L 0.890
227 01/17/2023 09:226200BMethyl Ethyl Ketone (MEK)µg/L 7.10
50.4 01/17/2023 09:226200BMethyl tert-butyl ether (MTBE)µg/L 1.40
718 01/17/2023 09:226200BNaphthaleneµg/L 4.70
276 01/17/2023 09:226200Bn-Propylbenzene µg/L 1.90
17.2 01/17/2023 09:226200BStyreneµg/L 2.20
32000 01/18/2023 11:216200BTolueneµg/L 220
2090 01/18/2023 11:216200B1,2,4-Trimethylbenzene µg/L 190
765 01/17/2023 09:226200B1,3,5-Trimethylbenzene µg/L 1.80
3340 01/18/2023 11:216200Bo-Xylene µg/L 210
8000 01/18/2023 11:216200Bm,p-Xylene µg/L 420
11300 01/18/2023 11:216200BXylene (Total)µg/L 210
V 97221MW-20
J0.435 01/17/2023 08:076200BBenzeneµg/L 0.180
J0.221 01/17/2023 08:076200BEthylbenzeneµg/L 0.170
1.42 01/17/2023 08:076200BTolueneµg/L 0.220
J0.445 01/17/2023 08:076200B1,2,4-Trimethylbenzene µg/L 0.190
J0.373 01/17/2023 08:076200Bo-Xylene µg/L 0.210
J0.821 01/17/2023 08:076200Bm,p-Xylene µg/L 0.420
J1.19 01/17/2023 08:076200BXylene (Total)µg/L 0.210
Page 5 of 43

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Former Phelps Amoco Lab Report Number: 23-011-0002
Date: 1/18/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Carbon Tetrachloride QC Batch No: V28980/V28947
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V28980/V28947
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 6 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97215 Matrix:
1/10/2023 8:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500Benzene 1 01/17/23 03:30 V28948MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/17/23 03:30 V28948MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/17/23 03:30 V28948MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/17/23 03:30 V28948MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/17/23 03:30 V28948MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/17/23 03:30 V28948MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/17/23 03:30 V28948MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/17/23 03:30 V28948MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/17/23 03:30 V28948MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/17/23 03:30 V28948MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/17/23 03:30 V28948MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/17/23 03:30 V28948MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/17/23 03:30 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97215 Matrix:
1/10/2023 8:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/17/23 03:30 V28948MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/17/23 03:30 V28948MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/17/23 03:30 V28948MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/17/23 03:30 V28948MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/17/23 03:30 V28948MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/17/23 03:30 V28948MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/17/23 03:30 V28948MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/17/23 03:30 V28948MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/17/23 03:30 V28948MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/17/23 03:30 V28948MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/17/23 03:30 V28948MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/17/23 03:30 V28948MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/17/23 03:30 V28948MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/17/23 03:30 V28948MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/17/23 03:30 V28948MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/17/23 03:30 V28948MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/17/23 03:30 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97215 Matrix:
1/10/2023 8:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/17/23 03:30 V28948MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/17/23 03:30 V28948MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/17/23 03:30 V28948MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/17/23 03:30 V28948MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/17/23 03:30 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/17/23 03:30 V28948MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/17/23 03:30 V28948MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/17/23 03:30 V28948MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/17/23 03:30 V28948MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/17/23 03:30 V28948MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/17/23 03:30 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/17/23 03:30 V28948MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/17/23 03:30 V28948MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/17/23 03:30 V28948MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/17/23 03:30 V28948MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/17/23 03:30 V28948MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/17/23 03:30 V28948MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/17/23 03:30 V28948MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/17/23 03:30 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97215 Matrix:
1/10/2023 8:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/17/23 03:30 V28948MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 01/17/23 03:30 V28948
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%01/17/23 03:301 MSA V28948
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%01/17/23 03:301 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%01/17/23 03:301 MSA V28948
Surrogate: Toluene-d8 99.6 Limits: 70-130%01/17/23 03:301 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-14
97216 Matrix:
1/10/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<18.0 µg/L 18.0 100Acetone 10 01/17/23 08:57 V28948MSA
583 µg/L 1.80 5.00Benzene 10 01/17/23 08:57 V28948MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 01/17/23 08:57 V28948MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 01/17/23 08:57 V28948MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 01/17/23 08:57 V28948MSA
<15.0 µg/L 15.0 50.0Bromoform 10 01/17/23 08:57 V28948MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 01/17/23 08:57 V28948MSA
3.26 J µg/L 1.80 5.00n-Butylbenzene 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.00
sec-Butyl benzene 10 01/17/23 08:57 V28948MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 01/17/23 08:57 V28948MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 01/17/23 08:57 V28948MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 01/17/23 08:57 V28948MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 01/17/23 08:57 V28948MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 01/17/23 08:57 V28948MSA
<2.20 µg/L 2.20 5.00Chloroform 10 01/17/23 08:57 V28948MSA
<2.20 µg/L 2.20 5.00
Chloromethane 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 01/17/23 08:57 V28948MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 01/17/23 08:57 V28948MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 01/17/23 08:57 V28948MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 01/17/23 08:57 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-14
97216 Matrix:
1/10/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 01/17/23 08:57 V28948MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 01/17/23 08:57 V28948MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 01/17/23 08:57 V28948MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 01/17/23 08:57 V28948MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 01/17/23 08:57 V28948MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 01/17/23 08:57 V28948MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 01/17/23 08:57 V28948MSA
<1.80 µg/L 1.80 5.00
trans-1,2-Dichloroethene 10 01/17/23 08:57 V28948MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 01/17/23 08:57 V28948MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 01/17/23 08:57 V28948MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 01/17/23 08:57 V28948MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 01/17/23 08:57 V28948MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 01/17/23 08:57 V28948MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 01/17/23 08:57 V28948MSA
<420 µg/L 420 2000
Ethanol 10 01/17/23 08:57 V28948MSA
105 µg/L 1.70 5.00Ethylbenzene 10 01/17/23 08:57 V28948MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 01/17/23 08:57 V28948MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 01/17/23 08:57 V28948MSA
7.78 µg/L 1.80 5.00Isopropylbenzene 10 01/17/23 08:57 V28948MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 01/17/23 08:57 V28948MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 01/17/23 08:57 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-14
97216 Matrix:
1/10/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<1.40 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/17/23 08:57 V28948MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 01/17/23 08:57 V28948MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 01/17/23 08:57 V28948MSA
28.3 µg/L 4.70 10.0Naphthalene 10 01/17/23 08:57 V28948MSA
18.2 µg/L 1.90 5.00n-Propylbenzene 10 01/17/23 08:57 V28948MSA
<2.20 µg/L 2.20 5.00Styrene 10 01/17/23 08:57 V28948MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 01/17/23 08:57 V28948MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 01/17/23 08:57 V28948MSA
<2.20 µg/L 2.20 5.00
Tetrachloroethene 10 01/17/23 08:57 V28948MSA
29.9 µg/L 2.20 5.00Toluene 10 01/17/23 08:57 V28948MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 01/17/23 08:57 V28948MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 01/17/23 08:57 V28948MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 01/17/23 08:57 V28948MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 01/17/23 08:57 V28948MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 01/17/23 08:57 V28948MSA
<1.80 µg/L 1.80 5.00
Trichlorofluoromethane 10 01/17/23 08:57 V28948MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 01/17/23 08:57 V28948MSA
46.8 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 01/17/23 08:57 V28948MSA
4.62 J µg/L 1.80 5.001,3,5-Trimethylbenzene 10 01/17/23 08:57 V28948MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 01/17/23 08:57 V28948MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 01/17/23 08:57 V28948MSA
12.3 µg/L 2.10 5.00o-Xylene 10 01/17/23 08:57 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-14
97216 Matrix:
1/10/2023 9:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
73.9 µg/L 4.20 10.0m,p-Xylene 10 01/17/23 08:57 V28948MSA
86.2 µg/L 2.10 5.00Xylene (Total)10 01/17/23 08:57 V28948
Surrogate: 4-Bromofluorobenzene 108 Limits: 70-130%01/17/23 08:5710 MSA V28948
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%01/17/23 08:5710 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%01/17/23 08:5710 MSA V28948
Surrogate: Toluene-d8 101 Limits: 70-130%01/17/23 08:5710 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-15
97217 Matrix:
1/10/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
2.77 J µg/L 1.80 10.0Acetone 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500Benzene 1 01/17/23 06:51 V28948MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/17/23 06:51 V28948MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/17/23 06:51 V28948MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/17/23 06:51 V28948MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/17/23 06:51 V28948MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/17/23 06:51 V28948MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/17/23 06:51 V28948MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/17/23 06:51 V28948MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/17/23 06:51 V28948MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/17/23 06:51 V28948MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/17/23 06:51 V28948MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/17/23 06:51 V28948MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/17/23 06:51 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-15
97217 Matrix:
1/10/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/17/23 06:51 V28948MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/17/23 06:51 V28948MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/17/23 06:51 V28948MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/17/23 06:51 V28948MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/17/23 06:51 V28948MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/17/23 06:51 V28948MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/17/23 06:51 V28948MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/17/23 06:51 V28948MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/17/23 06:51 V28948MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/17/23 06:51 V28948MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/17/23 06:51 V28948MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/17/23 06:51 V28948MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/17/23 06:51 V28948MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/17/23 06:51 V28948MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/17/23 06:51 V28948MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/17/23 06:51 V28948MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/17/23 06:51 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-15
97217 Matrix:
1/10/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/17/23 06:51 V28948MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/17/23 06:51 V28948MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/17/23 06:51 V28948MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/17/23 06:51 V28948MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/17/23 06:51 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/17/23 06:51 V28948MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/17/23 06:51 V28948MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/17/23 06:51 V28948MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/17/23 06:51 V28948MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/17/23 06:51 V28948MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/17/23 06:51 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/17/23 06:51 V28948MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/17/23 06:51 V28948MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/17/23 06:51 V28948MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/17/23 06:51 V28948MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/17/23 06:51 V28948MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/17/23 06:51 V28948MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/17/23 06:51 V28948MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/17/23 06:51 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-15
97217 Matrix:
1/10/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/17/23 06:51 V28948MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 01/17/23 06:51 V28948
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%01/17/23 06:511 MSA V28948
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%01/17/23 06:511 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%01/17/23 06:511 MSA V28948
Surrogate: Toluene-d8 98.8 Limits: 70-130%01/17/23 06:511 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-17
97218 Matrix:
1/10/2023 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 01/17/23 07:16 V28948MSA
0.250 J µg/L 0.180 0.500Benzene 1 01/17/23 07:16 V28948MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/17/23 07:16 V28948MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/17/23 07:16 V28948MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/17/23 07:16 V28948MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/17/23 07:16 V28948MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/17/23 07:16 V28948MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/17/23 07:16 V28948MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/17/23 07:16 V28948MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/17/23 07:16 V28948MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/17/23 07:16 V28948MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/17/23 07:16 V28948MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/17/23 07:16 V28948MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/17/23 07:16 V28948MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/17/23 07:16 V28948MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/17/23 07:16 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-17
97218 Matrix:
1/10/2023 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/17/23 07:16 V28948MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/17/23 07:16 V28948MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/17/23 07:16 V28948MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/17/23 07:16 V28948MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/17/23 07:16 V28948MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/17/23 07:16 V28948MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/17/23 07:16 V28948MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/17/23 07:16 V28948MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/17/23 07:16 V28948MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/17/23 07:16 V28948MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/17/23 07:16 V28948MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/17/23 07:16 V28948MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/17/23 07:16 V28948MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/17/23 07:16 V28948MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/17/23 07:16 V28948MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/17/23 07:16 V28948MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/17/23 07:16 V28948MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/17/23 07:16 V28948MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/17/23 07:16 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-17
97218 Matrix:
1/10/2023 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/17/23 07:16 V28948MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/17/23 07:16 V28948MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/17/23 07:16 V28948MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/17/23 07:16 V28948MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/17/23 07:16 V28948MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/17/23 07:16 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/17/23 07:16 V28948MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/17/23 07:16 V28948MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/17/23 07:16 V28948MSA
0.949 µg/L 0.220 0.500Toluene 1 01/17/23 07:16 V28948MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/17/23 07:16 V28948MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/17/23 07:16 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/17/23 07:16 V28948MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/17/23 07:16 V28948MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/17/23 07:16 V28948MSA
0.295 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/17/23 07:16 V28948MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/17/23 07:16 V28948MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/17/23 07:16 V28948MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/17/23 07:16 V28948MSA
0.275 J µg/L 0.210 0.500o-Xylene 1 01/17/23 07:16 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-17
97218 Matrix:
1/10/2023 10:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
0.548 J µg/L 0.420 1.00m,p-Xylene 1 01/17/23 07:16 V28948MSA
0.823 J µg/L 0.210 0.500Xylene (Total)1 01/17/23 07:16 V28948
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/17/23 07:161 MSA V28948
Surrogate: Dibromofluoromethane 94.6 Limits: 70-130%01/17/23 07:161 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%01/17/23 07:161 MSA V28948
Surrogate: Toluene-d8 103 Limits: 70-130%01/17/23 07:161 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-22
97219 Matrix:
1/10/2023 10:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
1.96 J µg/L 1.80 10.0Acetone 1 01/17/23 07:42 V28948MSA
2.00 µg/L 0.180 0.500Benzene 1 01/17/23 07:42 V28948MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/17/23 07:42 V28948MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/17/23 07:42 V28948MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/17/23 07:42 V28948MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/17/23 07:42 V28948MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/17/23 07:42 V28948MSA
0.644 µg/L 0.180 0.500n-Butylbenzene 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/17/23 07:42 V28948MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/17/23 07:42 V28948MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/17/23 07:42 V28948MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/17/23 07:42 V28948MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/17/23 07:42 V28948MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/17/23 07:42 V28948MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/17/23 07:42 V28948MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/17/23 07:42 V28948MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/17/23 07:42 V28948MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/17/23 07:42 V28948MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/17/23 07:42 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-22
97219 Matrix:
1/10/2023 10:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/17/23 07:42 V28948MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/17/23 07:42 V28948MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/17/23 07:42 V28948MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/17/23 07:42 V28948MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/17/23 07:42 V28948MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/17/23 07:42 V28948MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/17/23 07:42 V28948MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/17/23 07:42 V28948MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/17/23 07:42 V28948MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/17/23 07:42 V28948MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/17/23 07:42 V28948MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/17/23 07:42 V28948MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/17/23 07:42 V28948MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/17/23 07:42 V28948MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/17/23 07:42 V28948MSA
1.72 µg/L 0.170 0.500Ethylbenzene 1 01/17/23 07:42 V28948MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/17/23 07:42 V28948MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/17/23 07:42 V28948MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/17/23 07:42 V28948MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/17/23 07:42 V28948MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/17/23 07:42 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-22
97219 Matrix:
1/10/2023 10:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/17/23 07:42 V28948MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/17/23 07:42 V28948MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/17/23 07:42 V28948MSA
1.44 µg/L 0.470 1.00Naphthalene 1 01/17/23 07:42 V28948MSA
0.705 µg/L 0.190 0.500n-Propylbenzene 1 01/17/23 07:42 V28948MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/17/23 07:42 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/17/23 07:42 V28948MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/17/23 07:42 V28948MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/17/23 07:42 V28948MSA
8.76 µg/L 0.220 0.500Toluene 1 01/17/23 07:42 V28948MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/17/23 07:42 V28948MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/17/23 07:42 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/17/23 07:42 V28948MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/17/23 07:42 V28948MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/17/23 07:42 V28948MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/17/23 07:42 V28948MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/17/23 07:42 V28948MSA
5.43 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/17/23 07:42 V28948MSA
1.67 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/17/23 07:42 V28948MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/17/23 07:42 V28948MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/17/23 07:42 V28948MSA
2.87 µg/L 0.210 0.500o-Xylene 1 01/17/23 07:42 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-22
97219 Matrix:
1/10/2023 10:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
7.00 µg/L 0.420 1.00m,p-Xylene 1 01/17/23 07:42 V28948MSA
9.87 µg/L 0.210 0.500Xylene (Total)1 01/17/23 07:42 V28948
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/17/23 07:421 MSA V28948
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%01/17/23 07:421 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%01/17/23 07:421 MSA V28948
Surrogate: Toluene-d8 98.6 Limits: 70-130%01/17/23 07:421 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-21
97220 Matrix:
1/10/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00 V28979 01/17/23 14:00
<18.0 µg/L 18.0 100Acetone 10 01/17/23 09:22 V28948MSA
21000 µg/L 180 500Benzene 1000 01/18/23 11:21 V28980MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 01/17/23 09:22 V28948MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 01/17/23 09:22 V28948MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 01/17/23 09:22 V28948MSA
<15.0 µg/L 15.0 50.0Bromoform 10 01/17/23 09:22 V28948MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 01/17/23 09:22 V28948MSA
75.1 µg/L 1.80 5.00n-Butylbenzene 10 01/17/23 09:22 V28948MSA
18.1 µg/L 2.00 5.00
sec-Butyl benzene 10 01/17/23 09:22 V28948MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 01/17/23 09:22 V28948MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 01/17/23 09:22 V28948MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 01/17/23 09:22 V28948MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 01/17/23 09:22 V28948MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 01/17/23 09:22 V28948MSA
<2.20 µg/L 2.20 5.00Chloroform 10 01/17/23 09:22 V28948MSA
<2.20 µg/L 2.20 5.00
Chloromethane 10 01/17/23 09:22 V28948MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 01/17/23 09:22 V28948MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 01/17/23 09:22 V28948MSA
26.6 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 01/17/23 09:22 V28948MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 01/17/23 09:22 V28948MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 01/17/23 09:22 V28948MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 01/17/23 09:22 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-21
97220 Matrix:
1/10/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00 V28979 01/17/23 14:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 01/17/23 09:22 V28948MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 01/17/23 09:22 V28948MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 01/17/23 09:22 V28948MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 01/17/23 09:22 V28948MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 01/17/23 09:22 V28948MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 01/17/23 09:22 V28948MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 01/17/23 09:22 V28948MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 01/17/23 09:22 V28948MSA
<1.80 µg/L 1.80 5.00
trans-1,2-Dichloroethene 10 01/17/23 09:22 V28948MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 01/17/23 09:22 V28948MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 01/17/23 09:22 V28948MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 01/17/23 09:22 V28948MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 01/17/23 09:22 V28948MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 01/17/23 09:22 V28948MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 01/17/23 09:22 V28948MSA
<420 µg/L 420 2000
Ethanol 10 01/17/23 09:22 V28948MSA
1930 µg/L 170 500Ethylbenzene 1000 01/18/23 11:21 V28980MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 01/17/23 09:22 V28948MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 01/17/23 09:22 V28948MSA
82.3 µg/L 1.80 5.00Isopropylbenzene 10 01/17/23 09:22 V28948MSA
10.8 µg/L 0.890 5.004-Isopropyl toluene 10 01/17/23 09:22 V28948MSA
227 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 01/17/23 09:22 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-21
97220 Matrix:
1/10/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00 V28979 01/17/23 14:00
50.4 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/17/23 09:22 V28948MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 01/17/23 09:22 V28948MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 01/17/23 09:22 V28948MSA
718 µg/L 4.70 10.0Naphthalene 10 01/17/23 09:22 V28948MSA
276 µg/L 1.90 5.00n-Propylbenzene 10 01/17/23 09:22 V28948MSA
17.2 µg/L 2.20 5.00Styrene 10 01/17/23 09:22 V28948MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 01/17/23 09:22 V28948MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 01/17/23 09:22 V28948MSA
<2.20 µg/L 2.20 5.00
Tetrachloroethene 10 01/17/23 09:22 V28948MSA
32000 µg/L 220 500Toluene 1000 01/18/23 11:21 V28980MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 01/17/23 09:22 V28948MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 01/17/23 09:22 V28948MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 01/17/23 09:22 V28948MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 01/17/23 09:22 V28948MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 01/17/23 09:22 V28948MSA
<1.80 µg/L 1.80 5.00
Trichlorofluoromethane 10 01/17/23 09:22 V28948MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 01/17/23 09:22 V28948MSA
2090 µg/L 190 5001,2,4-Trimethylbenzene 1000 01/18/23 11:21 V28980MSA
765 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 01/17/23 09:22 V28948MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 01/17/23 09:22 V28948MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 01/17/23 09:22 V28948MSA
3340 µg/L 210 500o-Xylene 1000 01/18/23 11:21 V28980MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-21
97220 Matrix:
1/10/2023 10:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00 V28979 01/17/23 14:00
8000 µg/L 420 1000m,p-Xylene 1000 01/18/23 11:21 V28980MSA
11300 µg/L 210 500Xylene (Total)1000 01/18/23 11:21 V28980
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%01/17/23 09:2210 MSA V28948
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%01/17/23 09:2210 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 108 Limits: 70-130%01/17/23 09:2210 MSA V28948
Surrogate: Toluene-d8 97.6 Limits: 70-130%01/17/23 09:2210 MSA V28948
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%01/18/23 11:211000 MSA V28980
Surrogate: Dibromofluoromethane 89.2 Limits: 70-130%01/18/23 11:211000 MSA V28980
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%01/18/23 11:211000 MSA V28980
Surrogate: Toluene-d8 99.4 Limits: 70-130%01/18/23 11:211000 MSA V28980
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-20
97221 Matrix:
1/10/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 01/17/23 08:07 V28948MSA
0.435 J µg/L 0.180 0.500Benzene 1 01/17/23 08:07 V28948MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/17/23 08:07 V28948MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/17/23 08:07 V28948MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/17/23 08:07 V28948MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/17/23 08:07 V28948MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/17/23 08:07 V28948MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/17/23 08:07 V28948MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/17/23 08:07 V28948MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/17/23 08:07 V28948MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/17/23 08:07 V28948MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/17/23 08:07 V28948MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/17/23 08:07 V28948MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/17/23 08:07 V28948MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/17/23 08:07 V28948MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/17/23 08:07 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-20
97221 Matrix:
1/10/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/17/23 08:07 V28948MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/17/23 08:07 V28948MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/17/23 08:07 V28948MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/17/23 08:07 V28948MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/17/23 08:07 V28948MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/17/23 08:07 V28948MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/17/23 08:07 V28948MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/17/23 08:07 V28948MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/17/23 08:07 V28948MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/17/23 08:07 V28948MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/17/23 08:07 V28948MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/17/23 08:07 V28948MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/17/23 08:07 V28948MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/17/23 08:07 V28948MSA
0.221 J µg/L 0.170 0.500Ethylbenzene 1 01/17/23 08:07 V28948MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/17/23 08:07 V28948MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/17/23 08:07 V28948MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/17/23 08:07 V28948MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/17/23 08:07 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-20
97221 Matrix:
1/10/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/17/23 08:07 V28948MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/17/23 08:07 V28948MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/17/23 08:07 V28948MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/17/23 08:07 V28948MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/17/23 08:07 V28948MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/17/23 08:07 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/17/23 08:07 V28948MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/17/23 08:07 V28948MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/17/23 08:07 V28948MSA
1.42 µg/L 0.220 0.500Toluene 1 01/17/23 08:07 V28948MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/17/23 08:07 V28948MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/17/23 08:07 V28948MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/17/23 08:07 V28948MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/17/23 08:07 V28948MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/17/23 08:07 V28948MSA
0.445 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/17/23 08:07 V28948MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/17/23 08:07 V28948MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/17/23 08:07 V28948MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/17/23 08:07 V28948MSA
0.373 J µg/L 0.210 0.500o-Xylene 1 01/17/23 08:07 V28948MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-011-0002
00087
Geological Resources, Inc.
113 W. Firetower Road, Suite G
Ethan Rogerson
Winterville
Danyale Love
Project Manager
GRI #2720 Received : 01/11/2023
Former Phelps Amoco
Report Date : 01/18/2023
Sample ID :
Lab No :
Sampled:MW-20
97221 Matrix:
1/10/2023 11:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28947 01/16/23 14:00
0.821 J µg/L 0.420 1.00m,p-Xylene 1 01/17/23 08:07 V28948MSA
1.19 J µg/L 0.210 0.500Xylene (Total)1 01/17/23 08:07 V28948
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%01/17/23 08:071 MSA V28948
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%01/17/23 08:071 MSA V28948
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%01/17/23 08:071 MSA V28948
Surrogate: Toluene-d8 102 Limits: 70-130%01/17/23 08:071 MSA V28948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
Associated Lab Samples: 97215, 97216, 97217, 97218, 97219, 97220, 97221
LRB-V28947 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/17/23 02:3910.01.80<1.80µg/LAcetone
01/17/23 02:390.5000.180<0.180µg/LBenzene
01/17/23 02:390.5000.210<0.210µg/LBromobenzene
01/17/23 02:391.000.420<0.420µg/LBromochloromethane
01/17/23 02:390.5000.160<0.160µg/LBromodichloromethane
01/17/23 02:395.001.50<1.50µg/LBromoform
01/17/23 02:391.000.280<0.280µg/LBromomethane
01/17/23 02:390.5000.180<0.180µg/Ln-Butylbenzene
01/17/23 02:390.5000.200<0.200µg/Lsec-Butyl benzene
01/17/23 02:392.000.920<0.920µg/Ltert-Butyl benzene
01/17/23 02:390.5000.180<0.180µg/LCarbon Tetrachloride
01/17/23 02:390.5000.190<0.190µg/LChlorobenzene
01/17/23 02:390.5000.190<0.190µg/LChlorodibromomethane
01/17/23 02:391.000.430<0.430µg/LChloroethane
01/17/23 02:390.5000.220<0.220µg/LChloroform
01/17/23 02:390.5000.220<0.220µg/LChloromethane
01/17/23 02:390.5000.200<0.200µg/L2-Chlorotoluene
01/17/23 02:390.5000.200<0.200µg/L4-Chlorotoluene
01/17/23 02:390.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
01/17/23 02:392.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
01/17/23 02:390.5000.200<0.200µg/L1,2-Dibromoethane
01/17/23 02:390.5000.230<0.230µg/LDibromomethane
01/17/23 02:390.5000.220<0.220µg/L1,2-Dichlorobenzene
01/17/23 02:390.5000.190<0.190µg/L1,3-Dichlorobenzene
01/17/23 02:390.5000.210<0.210µg/L1,4-Dichlorobenzene
01/17/23 02:395.001.20<1.20µg/LDichlorodifluoromethane
01/17/23 02:390.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 7Date:01/18/2023 05:31 PM
Page 35 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
Associated Lab Samples: 97215, 97216, 97217, 97218, 97219, 97220, 97221
LRB-V28947 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/17/23 02:390.5000.150<0.150µg/L1,2-Dichloroethane
01/17/23 02:390.5000.150<0.150µg/L1,1-Dichloroethene
01/17/23 02:390.5000.200<0.200µg/Lcis-1,2-Dichloroethene
01/17/23 02:390.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
01/17/23 02:390.5000.190<0.190µg/L1,2-Dichloropropane
01/17/23 02:390.5000.130<0.130µg/L1,3-Dichloropropane
01/17/23 02:392.000.210<0.210µg/L2,2-Dichloropropane
01/17/23 02:390.5000.200<0.200µg/L1,1-Dichloropropene
01/17/23 02:390.5000.210<0.210µg/Lcis-1,3-Dichloropropene
01/17/23 02:390.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
01/17/23 02:3920042.0<42.0µg/LEthanol
01/17/23 02:390.5000.170<0.170µg/LEthylbenzene
01/17/23 02:393.000.350<0.350µg/LHexachlorobutadiene
01/17/23 02:391.000.380<0.380µg/L2-Hexanone
01/17/23 02:390.5000.180<0.180µg/LIsopropylbenzene
01/17/23 02:390.5000.089<0.089µg/L4-Isopropyl toluene
01/17/23 02:395.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
01/17/23 02:391.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/17/23 02:391.000.078<0.078µg/L4-Methyl-2-Pentanone
01/17/23 02:392.000.330<0.330µg/LMethylene Chloride
01/17/23 02:391.000.470<0.470µg/LNaphthalene
01/17/23 02:390.5000.190<0.190µg/Ln-Propylbenzene
01/17/23 02:390.5000.220<0.220µg/LStyrene
01/17/23 02:390.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
01/17/23 02:390.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
01/17/23 02:390.5000.220<0.220µg/LTetrachloroethene
01/17/23 02:390.5000.220<0.220µg/LToluene
Page 2 of 7Date:01/18/2023 05:31 PM
Page 36 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
Associated Lab Samples: 97215, 97216, 97217, 97218, 97219, 97220, 97221
LRB-V28947 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/17/23 02:390.5000.380<0.380µg/L1,2,3-Trichlorobenzene
01/17/23 02:390.5000.310<0.310µg/L1,2,4-Trichlorobenzene
01/17/23 02:390.5000.160<0.160µg/L1,1,1-Trichloroethane
01/17/23 02:390.5000.096<0.096µg/L1,1,2-Trichloroethane
01/17/23 02:390.5000.180<0.180µg/LTrichloroethene
01/17/23 02:390.5000.180<0.180µg/LTrichlorofluoromethane
01/17/23 02:390.5000.270<0.270µg/L1,2,3-Trichloropropane
01/17/23 02:390.5000.190<0.190µg/L1,2,4-Trimethylbenzene
01/17/23 02:390.5000.180<0.180µg/L1,3,5-Trimethylbenzene
01/17/23 02:395.001.00<1.00µg/LVinyl Acetate
01/17/23 02:390.5000.170<0.170µg/LVinyl Chloride
01/17/23 02:390.5000.210<0.210µg/Lo-Xylene
01/17/23 02:391.000.420<0.420µg/Lm,p-Xylene
01/17/23 02:394-Bromofluorobenzene (S)102 70-130
01/17/23 02:39Dibromofluoromethane (S)100 70-130
01/17/23 02:391,2-Dichloroethane - d4 (S)95.8 70-130
01/17/23 02:39Toluene-d8 (S)97.4 70-130
LCS-V28947 LCSD-V28947Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.5 78.776.730.740.0µg/LAcetone 40-160 2.5 20.0
20.7 10410621.220.0µg/LBenzene 70-130 2.3 20.0
20.6 10311222.420.0µg/LBromobenzene 70-130 8.3 20.0
21.5 10810621.220.0µg/LBromochloromethane 70-130 1.4 20.0
21.3 10710921.820.0µg/LBromodichloromethane 70-130 2.3 20.0
Page 3 of 7Date:01/18/2023 05:31 PM
Page 37 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
LCS-V28947 LCSD-V28947Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.8 10911122.220.0µg/LBromoform 70-130 1.8 20.0
22.5 11311222.420.0µg/LBromomethane 60-140 0.4 20.0
20.8 10410320.520.0µg/Ln-Butylbenzene 70-130 1.4 20.0
20.4 10210821.620.0µg/Lsec-Butyl benzene 70-130 5.7 20.0
21.3 10710721.420.0µg/Ltert-Butyl benzene 70-130 0.4 20.0
20.2 10110320.520.0µg/LCarbon Tetrachloride 70-130 1.4 20.0
21.5 10811122.120.0µg/LChlorobenzene 70-130 2.7 20.0
20.6 10310420.820.0µg/LChlorodibromomethane 70-130 0.9 20.0
20.8 10410821.620.0µg/LChloroethane 60-140 3.7 20.0
21.3 10710721.420.0µg/LChloroform 70-130 0.4 20.0
21.3 10711222.420.0µg/LChloromethane 60-140 5.0 20.0
20.4 10210921.820.0µg/L2-Chlorotoluene 70-130 6.6 20.0
20.5 10310821.620.0µg/L4-Chlorotoluene 70-130 5.2 20.0
21.1 10610320.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.8 20.0
22.0 11010220.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 7.5 20.0
22.0 11011022.020.0µg/L1,2-Dibromoethane 70-130 0.0 20.0
21.2 10610721.420.0µg/LDibromomethane 70-130 0.9 20.0
20.9 10510921.720.0µg/L1,2-Dichlorobenzene 70-130 3.7 20.0
21.0 10510921.720.0µg/L1,3-Dichlorobenzene 70-130 3.2 20.0
21.1 10610721.420.0µg/L1,4-Dichlorobenzene 70-130 1.4 20.0
23.2 11611923.820.0µg/LDichlorodifluoromethane 60-140 2.5 20.0
21.7 10910621.120.0µg/L1,1-Dichloroethane 70-130 2.8 20.0
21.1 10611021.920.0µg/L1,2-Dichloroethane 70-130 3.7 20.0
21.1 10610921.720.0µg/L1,1-Dichloroethene 70-130 2.8 20.0
21.2 10611021.920.0µg/Lcis-1,2-Dichloroethene 70-130 3.2 20.0
21.7 10910921.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.0 20.0
Page 4 of 7Date:01/18/2023 05:31 PM
Page 38 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
LCS-V28947 LCSD-V28947Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10911122.120.0µg/L1,2-Dichloropropane 70-130 1.8 20.0
20.8 10411022.020.0µg/L1,3-Dichloropropane 70-130 5.6 20.0
19.7 98.595.019.020.0µg/L2,2-Dichloropropane 70-130 3.6 20.0
21.8 10911322.620.0µg/L1,1-Dichloropropene 70-130 3.6 20.0
21.0 10510621.220.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0
20.9 10510621.220.0µg/Ltrans-1,3-Dichloropropene 70-130 1.4 20.0
433 86.692.8464500µg/LEthanol 60-140 6.9 20.0
21.3 10710921.720.0µg/LEthylbenzene 70-130 1.8 20.0
21.5 10811322.620.0µg/LHexachlorobutadiene 70-130 4.9 20.0
20.8 10410320.520.0µg/L2-Hexanone 60-140 1.4 20.0
20.9 10511322.520.0µg/LIsopropylbenzene 70-130 7.3 20.0
21.2 10611322.520.0µg/L4-Isopropyl toluene 70-130 5.9 20.0
22.3 11296.019.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.9 20.0
21.7 10910220.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.6 20.0
20.4 10210520.920.0µg/L4-Methyl-2-Pentanone 60-140 2.4 20.0
21.0 10510520.920.0µg/LMethylene Chloride 70-130 0.4 20.0
23.8 11911723.420.0µg/LNaphthalene 70-130 1.6 20.0
20.5 10311322.520.0µg/Ln-Propylbenzene 70-130 9.3 20.0
20.7 10411422.720.0µg/LStyrene 70-130 9.2 20.0
21.9 11011122.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.9 20.0
21.1 10611322.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 6.8 20.0
22.2 11110921.820.0µg/LTetrachloroethene 70-130 1.8 20.0
21.2 10610721.320.0µg/LToluene 70-130 0.4 20.0
22.8 11412424.820.0µg/L1,2,3-Trichlorobenzene 70-130 8.4 20.0
23.5 11811522.920.0µg/L1,2,4-Trichlorobenzene 70-130 2.5 20.0
21.0 10510721.320.0µg/L1,1,1-Trichloroethane 70-130 1.4 20.0
Page 5 of 7Date:01/18/2023 05:31 PM
Page 39 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28947
LCS-V28947 LCSD-V28947Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.010621.220.0µg/L1,1,2-Trichloroethane 70-130 6.8 20.0
22.0 11011222.320.0µg/LTrichloroethene 70-130 1.3 20.0
19.9 99.510420.820.0µg/LTrichlorofluoromethane 60-140 4.4 20.0
20.7 10410821.520.0µg/L1,2,3-Trichloropropane 70-130 3.7 20.0
21.4 10711021.920.0µg/L1,2,4-Trimethylbenzene 70-130 2.3 20.0
20.5 10310921.820.0µg/L1,3,5-Trimethylbenzene 70-130 6.1 20.0
18.7 93.595.519.120.0µg/LVinyl Acetate 60-140 2.1 20.0
20.7 10412324.520.0µg/LVinyl Chloride 60-140 16.8 20.0
20.9 10510821.620.0µg/Lo-Xylene 70-130 3.2 20.0
43.8 11011244.740.0µg/Lm,p-Xylene 70-130 2.0 20.0
96.298.84-Bromofluorobenzene (S)70-130
10199.8Dibromofluoromethane (S)70-130
95.81001,2-Dichloroethane - d4 (S)70-130
101103Toluene-d8 (S)70-130
Page 6 of 7Date:01/18/2023 05:31 PM
Page 40 of 43
Quality Control Data
23-011-0002Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former Phelps Amoco
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28980QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28979
Associated Lab Samples: 97220
LRB-V28979 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/18/23 03:480.5000.180<0.180µg/LBenzene
01/18/23 03:480.5000.170<0.170µg/LEthylbenzene
01/18/23 03:480.5000.220<0.220µg/LToluene
01/18/23 03:480.5000.190<0.190µg/L1,2,4-Trimethylbenzene
01/18/23 03:480.5000.210<0.210µg/Lo-Xylene
01/18/23 03:481.000.420<0.420µg/Lm,p-Xylene
01/18/23 03:484-Bromofluorobenzene (S)102 70-130
01/18/23 03:48Dibromofluoromethane (S)94.8 70-130
01/18/23 03:481,2-Dichloroethane - d4 (S)94.0 70-130
01/18/23 03:48Toluene-d8 (S)98.4 70-130
LCS-V28979 LCSD-V28979Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310220.420.0µg/LBenzene 70-130 0.9 20.0
20.2 10110420.820.0µg/LEthylbenzene 70-130 2.9 20.0
19.7 98.510520.920.0µg/LToluene 70-130 5.9 20.0
21.9 11010521.020.0µg/L1,2,4-Trimethylbenzene 70-130 4.1 20.0
21.2 10610721.320.0µg/Lo-Xylene 70-130 0.4 20.0
41.5 10410742.740.0µg/Lm,p-Xylene 70-130 2.8 20.0
10995.44-Bromofluorobenzene (S)70-130
99.6101Dibromofluoromethane (S)70-130
1011001,2-Dichloroethane - d4 (S)70-130
93.896.0Toluene-d8 (S)70-130
Page 7 of 7Date:01/18/2023 05:31 PM
Page 41 of 43
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-011-0002
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:01/11/2023 10:03:28
Special precautions or instructions included?
Comments:
Page 42 of 43
Page 43 of 43

APPENDIX C
Contaminant Mass Calculations
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-14
MW-21
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red.To Date Red.
MW-14 14,600 17,700 1,540 8,630 0 343 42813.00 4.06
MW-21 26,000 32,000 1,780 11,800 0 564 72144.00 3.10
Avg.20,300 24,850 1,660 10,215 0 454 57,479 3.58
MW-14 12,500 15,800 1,760 10,600 0 483 41143.00 3.80
MW-21 26,000 32,000 1,780 11,800 0 564 72144.00 3.58
Avg.19,250 23,900 1,770 11,200 0 524 56,644 3.69
MW-14 13,500 17,600 1,420 7,970 0 275 40765.00 5.21
MW-21 26,500 40,900 1,930 10,500 0 380 80210.00 4.72
Avg.20,000 29,250 1,675 9,235 0 328 60,488 4.97
MW-14 7,030 8,080 1,150 6,750 0 289 23299.00 2.46
MW-21 22,800 22,800 1,880 11,500 85.1 622 59687.10 2.11
Avg.14,915 15,440 1,515 9,125 43 456 41,493 2.29
MW-14 8,340 9,980 1,030 6,350 0 315 26015.00 2.31
MW-21 26,900 36,700 1,670 11,200 191 1,630 78291.00 1.87
Avg.17,620 23,340 1,350 8,775 96 973 52,153 2.09
MW-14 1,750 1,310 337 1,580 0 115 5092.00 1.84
MW-21 24,800 18,300 1,760 9,420 84.8 686 55050.80 1.35
Avg.13,275 9,805 1,049 5,500 42 401 30,071 1.60
MW-14 2,920 3,960 1,250 5,350 0 568 8130.00 3.90
MW-21 30,800 47,100 2,970 15,300 159 1,380 97709.00 3.62
Avg.16,860 25,530 2,110 15,300 80 1,380 52,920 3.76
MW-14 1,370 1,370 130 716 0 28.2 3614.20 2.61
MW-21 32,700 49,200 1,920 10,200 0 541 94561.00 2.56
Avg.17,035 25,285 1,025 5,458 0 285 49,088 2.59
MW-14 225 466 88.1 602 0 36.8 1417.90 2.29
MW-21 30,400 42,400 1,890 11,100 124 669 86583.00 2.64
Avg.15,313 21,433 989 5,851 62 353 44,000 2.47
MW-14 1,310 1,970 255 1,790 0 142 5467.00 5.05
MW-21 9,680 30,700 2,060 12,700 0 851 55991.00 5.18
Avg.5,495 16,335 1,158 7,245 0 497 30,729 5.12
MW-14 194 76.9 27.7 102 0 6.4 407.00 2.68
MW-21 28,200 31,600 1,520 9,020 0 362.00 70702.00 1.77
Avg.14,197 15,838 774 4,561 0 184 35,555 2.23
9.9%-39.4%8,012.328.24
13.3%9.2%7,708.919.54
9.42 8,491.95 -6.0%4.5%
12.1%9.6%7,818.897.04
28.2%-64.3%6,385.979.78
6.89 3,887.48 49.6%56.3%
-6.8%-28.2%9,496.609.91
16.7%5.3%7,406.859.72
2.38123,244.5
2.7%2.7%8,649.018.31
------8,892.688.42
35.3%39.5%5,749.2510.41
176,7630.20883,81331,2129.62
05/07/13
06/12/12
1
Area 1
APPENDIX C
PERCENTAGE REDUCTIONS
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Baseline Event
12/27/18
10/31/17
05/02/17
02/07/17
07/18/16
11/11/15
04/01/15
09/11/14
10/03/13
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-14
MW-21
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red.To Date Red.
2.38123,244.5 176,7630.20883,81331,2129.621
APPENDIX C
PERCENTAGE REDUCTIONS
FORMER PHELPS AMOCO (INCIDENT NO. 12613)
Baseline Event
MW-14 870 121 193 465 0 56.30 1705.30 1.75
MW-21 25300 13300 1600 6170 0 373.00 46743.00 1.20
Avg.13,085 6,711 897 3,318 0 215 24,224 1.48
Date
Average Water
Column Height
(ft.)
06/12/12 8.42
05/07/13 8.31
10/03/13 7.04
09/11/14 9.72
04/01/15 9.91
11/11/15 10.41
07/18/16 8.24
02/07/17 9.42
05/02/17 9.54
10/31/17 6.89
12/27/18 9.78
02/23/21 10.53
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 6
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
Area 1
(Cont.)
3,887 49.6%56%
6,386 -64.3%28%
-6.0%5%
7,709 9.2%13%
10.53 4,684.74 26.6%47.3%
4,685 26.6%47%
7,407 5.3%17%
9,497 -28.2%-7%
5,749 39.5%35%
8,012 -39.4%10%
8,492
8,649 2.7%3%
7,819 9.6%12%
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
8,893 ------
02/23/21