RA-29352_48506_CA_LSA_20230322_Phase I LSA

2725 E. Millbrook Road, Suite 121
Raleigh, North Carolina 27604
Telephone [phone]
Fax [phone]
www.oneatlas.com

March 22, 2023

Mr. John Maloy
North Carolina Department of Environmental Quality
Raleigh Regional Office
Division of Waste Management - UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Re: Phase I Limited Site Assessment
Former Circle K Store #2720104
4835 Hope Valley Road
Durham, Durham County, North Carolina
NCDEQ Incident No. 48506

Dear Mr. Maloy:

ATC Associates of North Carolina, LLC (ATC), on behalf of Circle K, Inc., is submitting this Phase I
Limited Site Assessment Report for the referenced facility.

If you have any questions or require additional information, please contact our office at [phone].

Sincerely,
ATC Associates of North Carolina, LLC

Maureen Jackson, P.G.
Senior Project Manager

cc: Mr. Alan Cubberley, Circle K Stores, Inc.

PHASE I LIMITED SITE ASSESSMENT REPORT

For

FORMER CIRCLE K STORE #2720104

4835 HOPE VALLEY ROAD

DURHAM, NORTH CAROLINA 27707

Prepared By:

ATC ASSOCIATES OF NORTH CAROLINA, LLC

2725 EAST MILLBROOK ROAD, SUITE 121

RALEIGH, NORTH CAROLINA 27604

TELEPHONE [phone]

Prepared For:

CIRCLE K STORES, INC.

1100 SITUS COURT, SUITE 100

RALEIGH, NORTH CAROLINA 27606
Site Name:
Site Address:
Facility I.D.:
Latitude:
PHASE I LIMITED SITE ASSESSMENT REPORT
March 22,2023
Former Circle K Store #2720104
4835 Hope Valley Road
Durham, Durham County, North Carolina
0-0000015130 UST Incident Number (if known): 4g506
35.919270" North Longitude: 78.960382" west source: GIS Mapping
UST Owner: Circle K Stores,Inc.Address: I 100 Situs Court, Suite 100
Raleigh, North Carolina 27606
elephone (919) 77 4-67 00
Property
Owner: Domar Corporation, Inc.Address: 1919 Wilshire Drive
Durham, North Carolina 27707
Telephone Unknown
UST Operator: Circle K Stores, Inc.
Address: I100 Situs Court, Suite 100' Raleigh, North Carolina 27606
Telephone (9 I 9) 77 4-67 00
Property
Occupant: Former Circle K Store #2720104Address: 4835 Hope Valley Road
Durham, North Carolina 27707
Telephone [phone]
Consultant: ATC Associates of North Carolina,LLCAddress: 2725E,. Millbrook Road, Suite 121 Raleigh, North Carolina 27604
Telephone (91 9) 87 t-0999
.Analtyical
Laboratory: waypoint Analytical state Certification No. 402Address: 449 Springbrook Road charlotte, North carolina 29217
Telephone [phone]
Release Information
Date Discovered: May I1,2022
Estimated Quantity
Of Release: Unknown
Cause of Release: UST System Operations
UST Information: Two 10,000-gallon gasoline, one 8,000-gallon gasoline, and one 8,000-gallon diesel
information
gis]for ATC Associates of North Carolina, LLC, do certiff that the
accurate to the best of my knowledge.
t..qf$,ee
$3Hlh
number of the company is C-1598.
to practice engineering in North Carolina. The certificationATC Associates
TABLE OF CONTENTS

Section Page
1.0 SITE HISTORY AND CHARACTERIZATION 1
1.1 UST OWNER AND OPERATOR INFORMATION 1
1.2 UST INFORMATION 1
1.3 AST INFORMATION 1
1.4 SITE CHARACTERISTICS 2
1.5 RELEASE INFORMATION 2

2.0 LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE 2

3.0 RECEPTOR PATHWAY INFORMATION 6
3.1 WATER SUPPLY WELLS 6
3.2 PUBLIC WATER SUPPLIES 6
3.3 SURFACE WATER BODIES 6
3.4 WELLHEAD PROTECTION AREAS 6
3.5 REGIONAL GEOLOGY AND HYDROGEOLOGY 6
3.6 SUBSURFACE STRUCTURES 7
3.7 LAND USE 7

4.0 LIMITED SITE ASSESSMENT ACTIVITIES 7
4.1 MONITORING WELL INSTALLATION 7
4.2 SOIL SAMPLING 8
4.3 GROUNDWATER SAMPLING 8

5.0 SITE GEOLOGY AND HYDROGEOLOGY 8
5.1 DESCRIPTION OF SHALLOW SUBSURFACE GEOLOGY 8
5.2 GROUNDWATER OCCURRENCE 9
5.3 GROUNDWATER FLOW DIRECTION 9

6.0 ANALYTICAL RESULTS 9
6.1 SOIL ANALYTICAL RESULTS 9
6.2 GROUNDWATER ANALYTICAL RESULTS 9

7.0 CONCLUSIONS AND RECOMMENDATIONS 10
7.1 CONCLUSIONS 10
7.2 RECOMMENDATIONS 10

8.0 LIMITATIONS 10

TABLES
Table 1 Monitoring Well Construction Details
Table 2 Soil Analytical Results
Table 3 Groundwater Analytical Results

FIGURES
Figure 1 Topographic Map
Figure 2 Site Map
Figure 3 Petroleum-Related Impacts to Soil Map
Figure 4 Dissolved Contaminants of Concern Map

APPENDICES
Appendix A Boring Log and Well Construction Record
Appendix B Soil and Groundwater Laboratory Report and Chain-of-Custody Documents

PHASE I LIMITED SITE ASSESSMENT REPORT
FOR
FORMER CIRCLE K STORE #2720104
4835 HOPE VALLEY ROAD
DURHAM, NORTH CAROLINA

ATC Associates of North Carolina, LLC (ATC) has prepared the following report for Circle K Stores, Inc. on limited site
assessment (LSA) activities performed at the Former Circle K Store #2720104 in Durham, North Carolina. This report
has been prepared pursuant to applicable sections of Title 15A of the North Carolina Administrative Code (NCAC),
Chapter 2, Subchapter 2L and in accordance with the State of North Carolina Department of Environmental Quality
(NCDEQ), Division of Waste Management (DWM), Underground Storage Tank (UST) Section Assessment Guidelines,
January 19, 2021 Version.

1.0 SITE HISTORY AND CHARACTERIZATION
1.1 UST OWNER AND OPERATOR INFORMATION
Two 10,000-gallon gasoline, one 8,000-gallon gasoline, and one 8,000-gallon diesel USTs and their appurtenances were
removed from the referenced facility between May 9 and May 12, 2022. The USTs and their appurtenances were owned
by Circle K Stores, Inc. of Raleigh, North Carolina. Information regarding each of the tanks is provided below.

1.2 UST INFORMATION
UST
ID PRODUCT CAPACITY
(gals.) MATERIALS INSTALLATION
DATE
UST
STATUS
RELEASE
ASSOCIATED
(Yes/No)

1 Gasoline 12,000
UST: Steel w/Internal
lining
Piping: SW Fiberglass
1/1/1982 Removed Yes
2 Gasoline 12,000
UST: Steel w/Internal
lining
Piping: SW Fiberglass
1/1/1982 Removed Yes
3 Gasoline 8,000
UST: Steel w/Internal
lining
Piping: SW Fiberglass
1/1/1982 Removed Yes
4 Diesel 8,000
UST: Steel w/Internal
lining
Piping: SW Fiberglass
1/1/19182 Removed Yes

Figure 1 is a topographical map of the site and surrounding area. Figure 2 is a site map which depicts the site and
pertinent structures, including the location of the USTs and appurtenances.

1.3 AST INFORMATION
No ASTs were observed on the site.

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1.4 SITE CHARACTERISTICS
Presently, the site is an inactive convenience store and retail fuel outlet. Surface cover at the site consists of asphalt and
concrete. The property will be redeveloped in the near future.

1.5 RELEASE INFORMATION
During closure activities, petroleum-impacted soil (odor and visual staining) was identified in the UST basin. A 24-Hour
Release and UST Leak Reporting Form was submitted to the NCDEQ on May 11, 2022. It should be noted
approximately 96.96 tons of petroleum-impacted soil were removed from the UST basin area for off-site disposal during
UST closure activities.

A 20-Day Report was submitted to the NCDEQ Raleigh Regional Office on June 6, 2022. An Initial Abatement Action
Report was submitted to the NCDEQ on August 11, 2022.

On November 2, 2022, DEQ issued a Notice of Regulatory Requirements (NORR) requesting the performance of a Phase
I Limited Site Assessment (LSA) for the referenced facility.

It should be noted two previous releases have been noted for the property (assigned UST incident #24490 and #39800).
The release associated with incident #24490 was discovered in May 1996 during a property transaction. The incident was
ranked as intermediate risk with a land use of residential. This release was issued a Notice of No Further Action (NFA),
following the recordation of a Notice of Residual Petroleum (NORP), on September 12, 2007. The release associated
with incident #39800 was caused when a customer pulled the hose off dispenser ½ causing the premium gasoline meter
seal to rupture. This release was issued a NFA on June 17, 2016. Reports regarding these two incident numbers are on
file at the NCDEQ Raleigh Regional Office.

2.0 LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE
In order to evaluate the following, a review of available site-specific, local and regional data was performed to include:
• A well survey within a 1,500-feet radius of the subject facility, including a record inquiry.
• Identification of wellhead protection areas.
• Researching geology and hydrogeology of the region, including topography, soil types, and surface water
drainage patterns.
• Identification of surface waters within a 1,500-feet radius of the subject facility.
• Land use observations (site reconnaissance) and zoning classifications.
• A visual survey for subsurface structures and potential impacts from the source area.
• Gathering information on adjacent property owners and occupants.
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Part I – Groundwater/Surface Water/Vapor Impacts
High Risk:
1. Has the discharge or release contaminated any water supply well including any used for non-drinking purposes?
NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the discharge or
release? NO
According to the Durham County Department of Public Utilities, public water is supplied to the site and
adjacent properties.

3. Is a water supply well used for any purpose (e.g. irrigation, washing cars, industrial cooling water, filling
swimming pools) located within 250 feet of the source area of the release or discharge? NO

4. Does groundwater within 500 feet of the source area of the discharge or release have the potential for future use
in that there is no other source of water supply other than the groundwater? NO

5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety, or the environment? NO

6. Are there any other factors that would cause the discharge or release to pose an imminent danger to public
health, public safety, or the environment? NO
At the time of this report, factors have not been identified that would appear to pose an imminent danger to public
health, public safety, or the environment.

Intermediate Risk:
7. Is a surface water body located within 500 feet of the source area of the discharge or release? NO
The nearest surface water body, Third Fork Creek, is located approximately 1,500 feet east of the source area.

If yes, does the maximum groundwater contaminant concentration exceed the surface water quality standards and
criteria found in 15A NCAC 2B .0200 by a factor of 10?

8. Is the source area of the discharge or release located within a designated wellhead protection area as defined in
42 USC 300h-7(e)? NO
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9. Is the discharge or release located in the Coastal Plain Physiographic Region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

If yes, is the source area of the discharge or release located in an area in which there is recharge to an
unconfirmed or semi-confined aquifer that is being used or may be used as a source of drinking water? NO

10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (GCLs)
established by the Department? NO

Part II – Land Use
Property Containing Source Area of Discharge or Release:
The questions below pertain to the property containing the source area of the release.

1. Does the property contain one or more primary or secondary (permanent or temporary) residences? NO

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing
home, or other place of public assembly? NO
The property is an inactive convenience store and retail fuel outlet. The property will be redeveloped in the near
future.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g.,
manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise,
and inactive commercial or industrial enterprise, or is the land undeveloped? YES
The property is an inactive convenience store and retail fuel outlet. The property will be redeveloped in the near
future.

4. Do children visit the property? NO
It is assumed children do not visit the property at this time; however, that could change in the future when the
property is redeveloped.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)?
NO
The site is not restricted.

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6. Do pavement, building, or other structures cap the contaminated soil? YES
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain
capped in the foreseeable future?
The property is most likely being redeveloped in the near future.

7. What is the zoning status of the property?
The site is zoned for commercial use (CN – Commercial Neighborhood).

8. Is the use of the property likely to change in the next 20 years? YES
The current property owners are expected to redevelop the property in the near future.

Property Surrounding Source Area of Discharge or Release:
The questions below pertain to the area within 1,500 feet of the source area of the discharge or release (excludes property
containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)?
The nearest residence was identified approximately 400 feet southwest of the source area.

10. What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home, or other place of public assembly?
The Hope Valley Church is located approximately 200 feet northwest of the source area.

11. What is the zoning status of properties in the surrounding area?
Properties surrounding the subject facility are zoned either CN (Commercial Neighborhood), CG (Commercial
General), O&I (office and industrial), and R-10 or R-20 (residential areas). The zoning status of the subject
facility is CN. Commercial businesses and residential areas characterize the surrounding area.

12. Briefly characterize the use and activities of the land in the surrounding area.
The site and adjacent areas are mainly commercial (restaurants, banks, gas stations, offices, shops) with some
residential houses. Properties beyond the site are mainly commercial (restaurants, banks, offices) intermixed with
residential areas (single-family homes and apartment complexes).

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3.0 RECEPTOR PATHWAY INFORMATION
As defined by NCDENR, a receptor is “any human, plant, or animal that is or has the potential to be adversely affected by
the release or migration of contaminants”. With respect to the subject facility, the following sections present information
regarding potential receptor pathways for the migration of contaminants and pathway relationships to the facility.

In an effort to efficiently gather complete and accurate data, ATC personnel performed a receptor survey of the area.
Activities included a visual reconnaissance survey within 1,500 feet radial distance of the site, obtaining utility
information from the Durham County Department of Public Utilities, obtaining property use information from the
Durham County Tax Department. The results of the survey, regarding the potential identification of water wells located
within 1,500 feet of the site, are summarized below.

3.1 WATER SUPPLY WELLS
Water supply wells were not identified within 1,500 feet of the property. It should be noted a previously identified water
supply well (an irrigation well) could not be located as the property has been redeveloped.

3.2 PUBLIC WATER SUPLIES
Public water supplies in the area are provided by the Durham County Department of Public Utilities.

3.3 SURFACE WATER BODIES
As shown on Figure 1, the closest surface water body is Third Fork Creek, located approximately 1,500 feet to the east of
the site.

3.4 WELLHEAD PROTECTION AREAS
At the time of this investigation, the source area is not located within an approved wellhead protection area as defined in
42 USC 300h-7(e).

3.5 REGIONAL GEOLOGY AND HYDROGEOLOGY
The site is located within the Chatham Group of the Triassic Basins. According to the Geologic Map of North Carolina
(Brown, et al., 1985), the site lies in an area which is characterized by tan, medium to very coarse-grained micaceous
arkosic sandstone.

Aquifers of the Piedmont and Mountains are localized, complex fractured metamorphic, igneous, and sedimentary
(Triassic Basin) rocks. The rocks are covered almost everywhere by regolith, which includes soil, saprolite, alluvium, and
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colluvium. Most of the groundwater is stored in the shallow, porous regolith. While the crystalline bedrock has extremely
low porosity, secondary fractures contain groundwater recharged by the overlying regolith.

Groundwater generally occurs everywhere in the Piedmont and Blue Ridge provinces. Groundwater occurs both in the
porous, shallow regolith (below the water table) in large diameter bored wells, and in fractures in the deeper crystalline
bedrock in drilled wells (6-10 inches in diameter). Some types of rock may have lower comparable yields than other rock
types, and finding enough groundwater to sustain supply needs may be difficult. Dry boreholes are possible in rocks that
have few fractures.

3.6 SUBSURFACE STRUCTURES
Subsurface structured identified at the property include water and sewer lines and electrical lines. Other subsurface
utilities may be present.

3.7 LAND USE
The site and adjacent areas are mainly commercial (restaurants, banks, gas stations, offices, shops) with some residential
houses. Properties beyond the site are mainly commercial (restaurants, banks, offices) intermixed with residential areas
(single-family homes and apartment complexes).

4.0 LIMITED SITE ASSESSMENT ACTIVITIES
The limited site assessment activities performed to collect data for this report included researching site-specific, local and
regional data, performing soil and groundwater sampling, and submitting soil and groundwater samples for analytical
testing. Information was also obtained from prior reports, prepared by ATC. The following sections discuss specific
methodologies used in conducting these limited site assessment activities.

4.1 MONITORING WELL INSTALLATION
Monitoring well MW-1 was installed by personnel with Carolina Soil Investigations (CSA) on July 14, 2022, during
initial abatement action activities. The monitoring well was installed in the former UST basin as groundwater was noted
to be int eh UST basin at an approximate depth of 11 feet bgs. The location of the monitoring well is depicted on Figure
2.

Monitoring well MW-1 was installed to a depth of approximately 20 feet bgs. The well was installed using solid stem
augers and was constructed of two-inch diameter well casing made of flush-joint, threaded schedule-40 poly vinyl
chloride (PVC) pipe. The PVC well screen is 0.010-inch slot with a screened interval of 15 feet. A coarse sand pack
(filter pack) was used to backfill the well annulus to a depth of approximately one foot above the well screen. A one-foot-
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thick bentonite seal was placed above the filter pack, and neat cement was used to fill the remainder of the well annulus to
ground surface. Well construction details are provided on Table 1.

The well was installed as flush-mounted and was provided with a sealing and locking cap. A protective, steel,
traffic-bearing cover was placed over the well upon completion. The boring log and well construction record are
presented in Appendix A.

4.2 SOIL SAMPLING
As monitoring well MW-1 was installed in the UST basin and the area consisted of backfilled material, a soil sample was
not collected from the monitoring well borehole.

Twenty-eight (28) soil samples were collected form the UST basin sidewall, from under each dispenser, and along the
product lines during UST closure activities. Additional details regarding these samples were provided in the Initial
Abatement Action Report, dated August 11, 2022, on file at the NCDEQ.

4.3 GROUNDWATER SAMPLING
On July 14, 2022, ATC personnel collected a groundwater sample from monitoring well MW-1. The depth to water
measured in monitoring well MW-1 on this date was 5.25 feet below ground surface (bgs). The monitoring well was
purged prior to sampling by removing a minimum of three well volumes of water from each well. After allowing
sufficient time for recharge, a representative groundwater sample was collected using a new, disposable Teflon bailer.
Upon collection, the groundwater sample was placed into laboratory-approved containers, packed in ice, and delivered
under chain-of-custody to Waypoint Analytical in Charlotte, North Carolina for analyses. Additional details regarding the
sample were provided in the Initial Abatement Action Report, dated August 11, 2022, on file at the NCDEQ.

5.0 SITE GEOLOGY AND HYDROGEOLOGY
5.1 DESCRIPTION OF SHALLOW SUBSURFACE GEOLOGY
According to the Soil Survey of Durham County, North Carolina, as published in the United States Department of
Agriculture Soil Conversation Service (now Natural Resources Conservation Services) in 1977, the predominant site soil
is White Store sandy loam (WsB).

Typically, this soil is composed of sandy loam to six inches below grade. From approximately six to 35 inches below
grade, this soil is typically clay. From 35 to 53 inches below grade, this soil is typically clay loam. From 53 to 80 inches
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below grade, the soil is typically weathered bedrock. Permeability of the subsoil is moderate. Available water capacity is
moderate, and the seasonal high-water table is at 12 to 18 inches.

Soil encountered during the installation of monitoring well MW-1 generally consisted of silty sand to 10 feet bgs. A
brown silty clay was encountered from 10 to 12 feet bgs. From 12 to 20 feet a brown sand with some pea gravel was
encountered. The boring log for MW-10 is provided in Appendix A.

5.2 GROUNDWATER OCCURRENCE
During the groundwater sampling event on July 14, 2022, ATC personnel obtained a groundwater measurement and
groundwater sample from monitoring well MW-1. At the time of sample collection, the depth-to-groundwater
measurement was 5.25 feet below the well top of casing. Table 1 provides a summary of well construction and
depth-to-groundwater measurement.

5.3 GROUNDWATER FLOW DIRECTION
Based on information obtained from the topographic map of the area, it appears groundwater flow would be toward the
southeast.

6.0 ANALYTICAL RESULTS
6.1 SOIL ANALYTICAL RESULTS
Laboratory analytical results of soil samples collected from the UST basin (soil samples W-1, W-7, W-11, W-12, and W-
14), along the product lines (soil samples L-6 and L-7), and under a dispenser (soil sample D-2) detected Total Petroleum
Hydrocarbon (TPH) – Gasoline Range Organics (GRO) and/or TPH – Diesel Range Organics (DRO) and/or
Environmental Protection Agency (EPA) Method 8260 concentrations above the established State Action Level and/or
Soil-to-Groundwater (STGW) Maximum Soil Contaminant Concentrations (MSCCs).

Table 2 provides a summary of the soil sample analytical results and petroleum-related impacts to soil are depicted on
Figure 3. The laboratory report and chain-of-custody document is provided in Appendix B.

6.2 GROUNDWATER ANALYTICAL RESULTS
Laboratory analytical results of the groundwater sample collected from monitoring well MW-1 detected several dissolved
target compound concentrations above North Carolina Groundwater Quality Standards (2L Standards). A summary of the
groundwater analytical data is provided on Table 3. Dissolved contaminants of concern are depicted on Figure 4. The
laboratory report and chain-of-custody document is provided in Appendix B.

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7.0 CONCLUSIONS AND RECOMMENDATIONS
7.1 CONCLUSIONS
Based on the information obtained during this LSA, it appears the site has been impacted from a petroleum release.
• The subject facility and surrounding area obtain drinking water from the City of Durham.
• Water supply wells were not identified within 1,500 feet of the source area.
• The subject facility is not located within an approved Wellhead Protection Area.
• Surface water bodies were not identified within 500 feet of the source area.
• Approximately 96.96 tons of petroleum-impacted soil were removed from the UST basin area during
UST closure activities.
• Laboratory analytical results of soil samples obtained during UST closure activities indicated the presence
of petroleum-related impacts to soil above the State Action Levels and/or established STGW-MSCCs.
• Monitoring well MW-1 was installed in the former UST basin during initial abatement action activities.
• Laboratory analytical results of the groundwater sample collected from monitoring well MW-1 detected
several dissolved target compound concentrations above established 2L Standards.

7.2 RECOMMENDATIONS
The results of the LSA activities indicate that the subject facility meets the criteria for Low-Risk classification with a land
use of residential. A NORP has already been recorded for the property as part of closure activities for another UST
incident at the site.

8.0 LIMITATIONS
This report has been prepared for the exclusive use of Circle K Stores, Inc. The opinions included herein are based on
information obtained during the study, on our experience in accordance with currently accepted hydrogeologic and
engineering practices, and relevant regulatory guidelines at this time and location. Other than this, no warranty is implied
or intended.

TABLES
TABLE 1
MONITORING WELL CONSTRUCTION DETAILS
FORMER CIRCLE K STORE #2720104
4835 HOPE VALLEY ROAD
DURHAM, DURHAM COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 48506
Depth of
Water (feet)
Depth to
LNAPL (feet)
Groundwater
Elevation (feet)
MW-1 7/14/2022 2 5-20 20.0 100.00 5.25 --94.75
Notes:
1. Elevation is referenced to an arbitrary on-site benchmark of 100.00 feet.
2. Total well depth measured from top of casing.
3. LNAPL denotes light non-aqueous phase liquid.
Date Measured: 7/14/2022
Monitoring
Well ID
Date
Installed
Well
Casing
Diameter
(Inches)
Screened
Interval
(feet)
Depth of Well
(feet)
Top of Casing
(feet)
TABLE 2
SOIL ANALYTICAL RESULTS - UST CLOSURE
FORMER CIRCLE K STORE #27201044835 HOPE VALLEY ROAD
DURHAM, DURHAM COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 48506
MADEP
Method for
VPH
Sample ID
Date
Sampled
Sample
Location
Sample
Depth
(feet)
PID
Reading
(ppm)TPH-GROTPH-DROAcetoneBenzenen-Butylbenzenesec-ButylbenzeneCarbon DisulfideChloroformEthylbenzenen-HexaneIPEIsopropylbenzenep-IsopropyltolueneMethyl Ethyl KetoneMethylene ChlorideMTBENaphthalenen-PropylbenzeneTetrachloroetheneTolueneTrichloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesC5-C8 AliphaticsW-1 5/11/2022 UST Basin 5 82.3 2.63J 109 0.023 0.002J <0.0006 <0.0007 0.026 <0.001 <0.0007 0.002J <0.0005 <0.0005 <0.001 0.006J <0.001 <0.0007 <0.001 <0.0006 <0.001 0.001J <0.001 0.0008J <0.0006 0.0009J --
W-2 5/11/2022 UST Basin 5 5.8 2.46J 32.7 ----------------------------------------------
W-3 5/11/2022 UST Basin 5 0.6 <2.36 <5.30 0.011J <0.0007 <0.0006 <0.0006 <0.0007 <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.001J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0008 <0.001 <0.0006 <0.0006 <0.0006 --
W-4 5/11/2022 UST Basin 5 0.0 3.84J <5.55 0.016J <0.0007 <0.0006 <0.0007 <0.0008 <0.001 <0.0007 <0.0008 <0.0009 <0.0005 <0.001 0.002J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0008 <0.001 <0.0006 <0.0006 <0.0006 --
W-5 5/11/2022 UST Basin 5 12.1 <2.64 13.0 0.017J 0.003J 0.0007J <0.0007 0.008 <0.001 0.001J 0.011J <0.0009 <0.0006 <0.001 0.006J <0.001 <0.0008 <0.001 <0.0007 <0.001 0.012 <0.001 0.009 0.005J 0.026 --
W-6 5/11/2022 UST Basin 5 136.8 10.3 9.06J ----------------------------------------------
W-7 5/11/2022 UST Basin 5 43.2 13.9 23.2 0.035 0.003J <0.0006 <0.0007 0.004J 6.36 <0.0008 <0.0009 <0.0010 <0.0006 <0.001 <0.0009 0.023 <0.0008 <0.001 <0.0007 0.002J 0.001J 0.006J <0.0006 <0.0007 0.0009J --
W-8 5/11/2022 UST Basin 5 1.3 2.64J <5.23 0.044 0.002J <0.0006 <0.0006 <0.0007 <0.001 <0.0007 0.002J 0.0008J <0.005 <0.001 <0.0007 <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0006 <0.0005 <0.0006 --
W-9 5/11/2022 UST Basin 5 37.8 4.68J 15.9 ----------------------------------------------
W-10 5/11/2022 UST Basin 5 27.0 33.6 <6.09 0.017J <0.0008 <0.0006 <0.0007 <0.0008 <0.001 <0.0008 <0.0009 <0.0010 <0.0006 <0.001 <0.0009 <0.001 <0.0008 <0.001 <0.0007 <0.001 <0.0009 <0.001 <0.0006 <0.0007 <0.0007 --
W-11 5/11/2022 UST Basin 5 2,608 63.5 37.4 ----------------------------------------------
W-12 5/11/2022 UST Basin 5 1,907 75.7 53.2 <0.074 0.304 0.491 0.163 <0.019 <0.032 3.30 3.05 <0.022 0.339 0.067J <0.020 <0.045 <0.019 1.13 1.37 <0.028 2.56 <0.028 7.11 1.95 14.5 --
W-13 5/11/2022 UST Basin 5 5.5 7.63 5.87J 0.022J <0.0007 <0.0005 <0.0006 <0.0007 <0.001 <0.0007 <0.0007 <0.0008 <0.0005 <0.001 0.005J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0005 <0.0006 <0.0006 --
W-14 5/11/2022 UST Basin 5 49.9 5.10J 115 0.008J <0.0006 <0.0006 <0.0006 <0.0007 <0.001 <0.0006 <0.0007 <0.0008 <0.0005 <0.001 0.001J <0.001 <0.0007 <0.001 <0.0006 <0.0010 <0.0007 <0.001 <0.0005 <0.0006 <0.0005 --
D-1 5/11/2022 Gasoline
Dispenser 3 5.4 39.1 --0.049 0.002J <0.0006 <0.0007 0.003J <0.001 <0.0007 0.001J <0.0009 <0.0006 <0.001 0.006J <0.001 <0.0008 0.002J <0.0007 <0.001 0.001J <0.001 0.002J 0.0008J 0.003J --
D-2 5/11/2022 Gasoline
Dispenser 3 14.5 3.64J --0.006J 0.015 <0.0006 <0.0007 <0.0008 <0.001 0.005J <0.0009 0.016 0.003J <0.001 <0.0009 <0.001 0.170 0.004J 0.002J <0.001 0.012 <0.001 0.003J 0.001J 0.006J --
D-3 5/11/2022 Gasoline
Dispenser 3 37.0 2.68J --0.013J 0.001J <0.0006 <0.0006 0.002J <0.001 0.0009J 0.004J <0.0008 <0.0005 <0.001 <0.0007 <0.001 <0.0007 0.001J 0.0007J <0.0010 0.003J <0.001 0.003J 0.002J 0.010J --
D-4 5/12/2022 Gasoline
Dispenser 3 2.8 2.99J --0.017J 0.002J <0.0007 <0.0008 <0.0009 <0.001 0.001J <0.0009 <0.0010 0.001J <0.001 <0.0009 <0.001 0.012 <0.001 0.001J <0.001 <0.0009 <0.001 0.008 0.001J 0.015J --
D-5 5/12/2022 Gasoline
Dispenser 3 235 2.75J --0.158 0.002J <0.0005 <0.0006 <0.0007 <0.001 <0.0006 0.005J 0.0009J <0.0005 <0.001 0.049 <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0005 0.0007J 0.006J --
D-6 5/12/2022 Gasoline/Diesel
Dispenser 3 5.7 5.64 77.2 ----------------------------------------------
L-1 5/12/2022 Product Line 3 0.0 2.51J --0.037 <0.0007 <0.0006 <0.0006 0.002J <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.007J <0.001 <0.0007 <0.001 <0.0006 <0.001 0.001J <0.001 <0.0006 <0.0006 <0.0006 --
L-2 5/12/2022 Product Line 3 6.0 <2.67 --0.019J <0.0007 <0.0006 <0.0007 <0.0008 <0.001 <0.0007 <0.0009 <0.0009 <0.0006 <0.001 0.005J <0.001 0.002J <0.001 <0.0007 <0.001 <0.0009 <0.001 <0.0006 <0.0007 <0.0006 --
L-3 5/12/2022 Product Line 3 44.0 25.9 --0.025 0.001J <0.0006 <0.0006 <0.0007 <0.001 0.001J 0.004J <0.0008 <0.0005 <0.001 <0.0007 <0.001 0.004J <0.001 0.0006J <0.001 0.006 <0.001 0.002J 0.001J 0.007J --
L-4 5/12/2022 Product Line 3 22.5 2.78J --0.012J 0.003J <0.0007 <0.0008 <0.0009 <0.001 <0.0008 <0.0009 0.003J <0.0006 <0.001 0.001J <0.001 0.023 <0.001 <0.0007 <0.001 0.001J <0.001 0.001J <0.0007 0.001J --
L-5 5/12/2022 Product Line 3 4.0 <2.59 --0.005J 0.002J <0.0006 <0.0007 <0.0008 <0.001 0.0009J 0.002J 0.001J <0.0006 <0.001 <0.0008 <0.001 0.034 <0.001 <0.0007 <0.001 0.008 <0.001 0.0010J <0.0007 0.004J --
L-6 5/12/2022 Product Line 3 9.0 <2.74 --0.030 0.021 <0.0006 <0.0007 <0.0008 0.001J <0.0008 0.002J <0.0010 <0.0006 <0.001 <0.0009 <0.001 <0.0008 <0.001 <0.0007 <0.001 0.010 <0.001 0.0008J 0.0009J 0.004J --
L-7 5/12/2022 Gasoline Product
Line 3 300 <2.49 --0.047 0.084 0.0007J <0.0007 <0.0008 <0.001 0.003J 0.004J <0.0009 <0.0006 <0.001 0.010J <0.001 <0.0007 0.002J <0.0006 <0.001 0.117 <0.001 0.002J 0.0007J 0.031 1.59J
L-8 5/12/2022 Gasoline Product
Line 3 18.6 <2.38 --0.016J <0.0007 <0.0006 <0.0006 0.002J <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.003J <0.001 <0.0007 0.001J <0.0006 <0.001 0.001J <0.001 0.001J <0.0006 0.002J --
Stockpile 1 5/10/2022 ---->15,000 4,770 759 ----------------------------------------------
Stock 2 5/10/2022 ---->15,000 525 100 ----------------------------------------------
Stock 3 5/10/2022 ---->15,000 2,080 445 ----------------------------------------------
Stock 4 5/10/2022 ----125.4 1,610 153 ----------------------------------------------
50 100 ----------------------------------------------
----24 0.0072 2.4 2.2 3.7 0.34 8 NE 0.32 1.3 0.12 16 0.023 0.085 0.2 1.4 0.005 5.4 0.017 6.6 6.6 6 68
----14,000 12 782 1,560 1,560 21 60.3 NE 156 1,560 1,560 9,380 93.8 156 5.5 1,560 93.8 1,250 7.82 156 156 3,120 939
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. "<" = not detected at or above the laboratory reporting limit.
3. Bold type denotes concentration is equal to or exceeds state action level or Soil-to-Groundwater MSCC.
4. MSCC denotes maximum soil contaminant concentration.
5. J denotes concentration estimated by project laboratory.
6. NE denotes not established.
ANALTYICAL METHOD
State Action Level (mg/kg)
EPA Method 8260
Soil-to-Groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
EPA Method 8015
TABLE 3
GROUNDWATER ANALYTICAL RESULTS - INITIAL ABATEMENT
FORMER CIRCLE K STORE #2720104
4835 HOPE VALLEY ROAD
DURHAM, DURHAM COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 48506
EPA
Method
6020
Sample ID
Date
Sampled Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzeneNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbeznene1,3,5-TrimethylbenzeneTotal Xylenes1-Methylnaphthalene2-MethylnaphthaleneNaphthaleneTICsLeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMW-1 7/14/2022 589 36.6J 23.1J 3,110 265 842 585 8,990 4,740 1,230 16,200 215 431 776 13,920 10.6 17,100 55,690 <124 16,520
1 70 70 600 70 6 70 600 400 400 500 1 30 6 NE 15 400 700 10,000 200
5,000 5,900 8,800 80,000 30,500 6,000 26,100 260,000 28,500 24,100 50,000 1,000 12,000 6,000 NE 15,000 NE NE NE NE
Notes:
1. "<" or ND denotes not detected above method detection limit.
2. NC 2L GW Standard denotes Title 15A NCAC 2L .0202 Groundwater Standard
3. GCL denotes Gross Contaminant Level established by NCDEQ.
4. NE denotes not established.
5. All concentrations in micrograms per liter (ug/L).
6. J value denotes concentration estimated by the laboratory.
7. Bold type indicates concentration above established 2L Standard.
8. TICs denotes tentatively identified compounds via EPA Method 625.
ANALTYICAL
METHOD EPA Method 6200B MADEP Methods for VPH and
EPH
2L GW Standard
GCL
EPA Method 625
FIGURES
HOPE VALLEY ROADWEST STATE HIGHWAY
54FORMERCIRCLE KSTORE #2720104
HOPE VALLEY ROADWEST STATE HIGHWAY
54FORMERCIRCLE KSTORE #2720104
HOPE VALLEY ROADWEST STATE HIGHWAY
54FORMERCIRCLE KSTORE #2720104
APPENDIX A

BORING LOG AND WELL CONSTRUCTION RECORD
WELL CONSTRUCTION RECORD (GW-1)

4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient)
N W
6.Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wellsdrilled:
9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.) If water level is above casing, use “+”
11. Borehole diameter: (in.)
12.Well construction method: (i.e. auger, rotary, cable, direct push, etc.)
22.Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Site diagram or additional well details: You may use the back of this page to provide additional well site details or wellconstruction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well construction to the following:
Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following:
Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed.
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018
Print Form
For Internal Use Only:
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
NC Well Contractor Certification Number
Carolina Soil Investigations, LLC
Company Name
2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
Water Supply Well:
Municipal/Public
Residential Water Supply (single)
Residential Water Supply (shared)
Wells > 100,000 GPD
Agricultural
Geothermal (Heating/Cooling Supply)
Industrial/Commercial Irrigation
17. SCREENFROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUTFROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
Non-Water Supply Well:
Monitoring Recovery
ft. ft.
ft. ft.
Injection Well: Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
ft. ft.
19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS
1.Well Contractor Information:
___________________________________________________________
Well Contractor Name
07-14-2022 S:\Enviro\Pantry\2720366 - Sanford\Boring Log\MW-1.borBoring terminated 20 feet below ground surface (bgs).
No soil or groundwater samples collected.
Hand cleared with hand auger to 5 ft. bgs.
MONITORING WELL: MW-1
(Page 1 of 1)Depth In Feet (BGS)0
2
4
6
8
10
12
14
16
18
20 USCSGRAPHICDESCRIPTION
Client: Circle K Stores, Inc.
ATC Project No. CIRK104CL
Durham, Durham County, NC
4835 Hope Valley Rd
Circle K #2720104 Date(s) Drilled : 7/14/22
Drilling Contractor : CSI
Drilling Method : Solid Stem Augers
Boring Diameter : 6 inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Well: MW-1
Grout
Bentonite
Sand Pack
Cover
Casing
Screen
AR
SM
SM
CL
SW
Concrete
Grayish brown, silty SAND, with small gravel, fine grained, dry
Grayish brown, silty SAND, with small gravel, fine grained, moist
Brown silty CLAY with some small gravel, low plasticity, moist
Brown SAND, with some peagravel, fine grained, saturated, large amount
of water, sheen, strong petroelum odor
End of Boring
APPENDIX B

SOIL AND GROUNDWATER LABORATORY REPORT
AND CHAIN-OF-CUSTODY DOCUMENTS

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/2/2022
ATC Group Services, LLC - Raleigh, NC Maureen Jackson
609A Piner Road Suite 115 Wilminton, NC, 28409
Ref: Analytical Testing
Lab Report Number: 22-196-0032 Client Project Description: CK 2720104
Dear Maureen Jackson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/15/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 34
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-196-0032
Page 2 of 34
Report Number:
Sample Summary Table
Client Project Description:
22-196-0032
CK 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
07/14/2022 13:45Aqueous 94407 MW-1 07/15/2022 14:00
Page 3 of 34
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-196-0032
Report Limit
Project:CK 2720104
V 94407MW-1
0.0106 07/18/2022 19:176020BLeadmg/L 0.0005
589 07/20/2022 23:216200BBenzeneµg/L 18.0
J36.6 07/20/2022 23:216200Bn-Butylbenzene µg/L 18.0
J23.1 07/20/2022 23:216200Bsec-Butyl benzene µg/L 20.0
3110 07/20/2022 23:216200BEthylbenzeneµg/L 17.0
265 07/20/2022 23:216200BIsopropylbenzeneµg/L 18.0
842 07/20/2022 23:216200BNaphthaleneµg/L 47.0
585 07/20/2022 23:216200Bn-Propylbenzene µg/L 19.0
8990 07/20/2022 23:216200BTolueneµg/L 22.0
4740 07/20/2022 23:216200B1,2,4-Trimethylbenzene µg/L 19.0
1230 07/20/2022 23:216200B1,3,5-Trimethylbenzene µg/L 18.0
5320 07/20/2022 23:216200Bo-Xylene µg/L 21.0
10900 07/20/2022 23:216200Bm,p-Xylene µg/L 42.0
16200 07/20/2022 23:216200BXylene (Total)µg/L 21.0
215 07/22/2022 05:01625.1 1-Methylnaphthalene µg/L 5.53
431 07/22/2022 05:01625.1 2-Methylnaphthalene µg/L 34.8
776 07/22/2022 05:01625.1 Naphthalene µg/L 39.6
1890 07/25/2022 19:19MADEP-EPH Aliphatic C9-C18 µg/L 28.2
2520 07/25/2022 19:19MADEP-EPH Aromatic C11-C22 µg/L 61.2
17100 07/18/2022 14:25MADEP-VPH Aliphatic C5-C8 µg/L 1150
53800 07/18/2022 14:25MADEP-VPH Aliphatic C9-C12 µg/L 2580
14000 07/18/2022 14:25MADEP-VPH Aromatic C9-C10 µg/L 402
Page 4 of 34

Client: ATC Group Services, LLC - Raleigh, NC CASE NARRATIVE
Project: CK 2720104 Lab Report Number: 22-196-0032
Date: 8/2/2022
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 94407 (MW-1) QC Batch No: V21824/V21605
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V21824/V21605
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. This target analyte was flagged for recoveries outside QC limits in the associated LCSD. Data for this analyte is
flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: 2-Chloronaphthalene
QC Batch No: V21824/V21605 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
This target analyte was flagged for recoveries outside QC limits in the associated LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Benzidine QC Batch No: V21824/V21605
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid QC Batch No: V21824/V21605 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was XXJ which calculates to a recovery of XX% which is within the acceptable recovery range.
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 8.49 ug/L which calculates to a recovery of 17.9% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V21824/V21605 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was XXJ which calculates to a recovery of XX% which is within the acceptable recovery range. Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
11.37 ug/L which calculates to a recovery of 22.7% which is within the acceptable recovery range. Analyte: Phenol QC Batch No: V21824/V21605 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 5 of 34

Massachusetts EPH Method MADEP-EPH
QC Batch No: V21899 LCS and LCSD exhibited aromatic breakthrough on the aliphatic portion of the sample. The batch was refracked
and still showed breakhrough in the LCS/lCSD. The initial data is reported.
Revised Report: Revision 1 1-methylnaphthalene and 2-methylnaphthalene have been added to report by Method 625.
Page 6 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 07/20/22 23:21 6200BJLB
0.0106 mg/L 0.0005 0.0010Lead 1 07/18/22 19:17 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21615 07/20/22 09:00
<180 µg/L 180 1000Acetone 100 07/20/22 23:21 V21617JLB
589 µg/L 18.0 50.0Benzene 100 07/20/22 23:21 V21617JLB
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/20/22 23:21 V21617JLB
<42.0 µg/L 42.0 100Bromochloromethane 100 07/20/22 23:21 V21617JLB
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/20/22 23:21 V21617JLB
<150 µg/L 150 500Bromoform 100 07/20/22 23:21 V21617JLB
<28.0 µg/L 28.0 100Bromomethane 100 07/20/22 23:21 V21617JLB
36.6 J µg/L 18.0 50.0n-Butylbenzene 100 07/20/22 23:21 V21617JLB
23.1 J
µg/L 20.0 50.0
sec-Butyl benzene 100 07/20/22 23:21 V21617JLB
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/20/22 23:21 V21617JLB
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/20/22 23:21 V21617JLB
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/20/22 23:21 V21617JLB
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/20/22 23:21 V21617JLB
<43.0 µg/L 43.0 100Chloroethane 100 07/20/22 23:21 V21617JLB
<22.0 µg/L 22.0 50.0Chloroform 100 07/20/22 23:21 V21617JLB
<22.0 µg/L 22.0 50.0
Chloromethane 100 07/20/22 23:21 V21617JLB
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/20/22 23:21 V21617JLB
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/20/22 23:21 V21617JLB
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/20/22 23:21 V21617JLB
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/20/22 23:21 V21617JLB
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/20/22 23:21 V21617JLB
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/20/22 23:21 V21617JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21615 07/20/22 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/20/22 23:21 V21617JLB
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/20/22 23:21 V21617JLB
<120 µg/L 120 500Dichlorodifluoromethane 100 07/20/22 23:21 V21617JLB
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/20/22 23:21 V21617JLB
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/20/22 23:21 V21617JLB
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/20/22 23:21 V21617JLB
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/20/22 23:21 V21617JLB
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/20/22 23:21 V21617JLB
<19.0 µg/L 19.0 50.0
1,2-Dichloropropane 100 07/20/22 23:21 V21617JLB
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/20/22 23:21 V21617JLB
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/20/22 23:21 V21617JLB
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/20/22 23:21 V21617JLB
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/20/22 23:21 V21617JLB
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/20/22 23:21 V21617JLB
<4200 µg/L 4200 20000Ethanol 100 07/20/22 23:21 V21617JLB
3110 µg/L 17.0 50.0
Ethylbenzene 100 07/20/22 23:21 V21617JLB
<5.90 µg/L 5.90 1000Ethyl Tertiary Butyl Ether (ETBE)100 07/20/22 23:21 V21617JLB
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/20/22 23:21 V21617JLB
<38.0 µg/L 38.0 1002-Hexanone 100 07/20/22 23:21 V21617JLB
265 µg/L 18.0 50.0Isopropylbenzene 100 07/20/22 23:21 V21617JLB
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/20/22 23:21 V21617JLB
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/20/22 23:21 V21617JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21615 07/20/22 09:00
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/20/22 23:21 V21617JLB
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/20/22 23:21 V21617JLB
<33.0 µg/L 33.0 200Methylene Chloride 100 07/20/22 23:21 V21617JLB
842 µg/L 47.0 100Naphthalene 100 07/20/22 23:21 V21617JLB
585 µg/L 19.0 50.0n-Propylbenzene 100 07/20/22 23:21 V21617JLB
<22.0 µg/L 22.0 50.0Styrene 100 07/20/22 23:21 V21617JLB
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/20/22 23:21 V21617JLB
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 07/20/22 23:21 V21617JLB
<190 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 07/20/22 23:21 V21617JLB
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 07/20/22 23:21 V21617JLB
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/20/22 23:21 V21617JLB
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/20/22 23:21 V21617JLB
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/20/22 23:21 V21617JLB
8990 µg/L 22.0 50.0Toluene 100 07/20/22 23:21 V21617JLB
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/20/22 23:21 V21617JLB
<31.0 µg/L 31.0 50.0
1,2,4-Trichlorobenzene 100 07/20/22 23:21 V21617JLB
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/20/22 23:21 V21617JLB
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/20/22 23:21 V21617JLB
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/20/22 23:21 V21617JLB
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/20/22 23:21 V21617JLB
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/20/22 23:21 V21617JLB
4740 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/20/22 23:21 V21617JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21615 07/20/22 09:00
1230 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/20/22 23:21 V21617JLB
<100 µg/L 100 500Vinyl Acetate 100 07/20/22 23:21 V21617JLB
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/20/22 23:21 V21617JLB
5320 µg/L 21.0 50.0o-Xylene 100 07/20/22 23:21 V21617JLB
10900 µg/L 42.0 100m,p-Xylene 100 07/20/22 23:21 V21617JLB
16200 µg/L 21.0 50.0Xylene (Total)100 07/20/22 23:21 V21617
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%07/20/22 23:21100 JLB V21617
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%07/20/22 23:21100 JLB V21617
Surrogate: 1,2-Dichloroethane - d4 86.6 Limits: 70-130%07/20/22 23:21100 JLB V21617
Surrogate: Toluene-d8 80.6 Limits: 70-130%07/20/22 23:21100 JLB V21617
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V21605 07/21/22 08:56
<35.8 µg/L 35.8 50.3Acenaphthene 5 07/22/22 05:01 V21824JMV
<35.0 µg/L 35.0 101Acenaphthylene 5 07/22/22 05:01 V21824JMV
<33.0 µg/L 33.0 50.3Anthracene 5 07/22/22 05:01 V21824JMV
<25.6 µg/L 25.6 50.3Benzidine 5 07/22/22 05:01 V21824JMV
<33.4 µg/L 33.4 50.3Benzo(a)anthracene 5 07/22/22 05:01 V21824JMV
<23.5 µg/L 23.5 50.3Benzo(a)pyrene 5 07/22/22 05:01 V21824JMV
<22.7 µg/L 22.7 50.3
Benzo(b)fluoranthene 5 07/22/22 05:01 V21824JMV
<21.3 µg/L 21.3 50.3Benzo(g,h,i)perylene 5 07/22/22 05:01 V21824JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V21605 07/21/22 08:56
<24.4 µg/L 24.4 50.3Benzo(k)fluoranthene 5 07/22/22 05:01 V21824JMV
<57.7 µg/L 57.7 251Benzoic Acid 5 07/22/22 05:01 V21824JMV
<43.3 µg/L 43.3 50.3Benzyl alcohol 5 07/22/22 05:01 V21824JMV
<28.5 µg/L 28.5 50.3Bis(2-Chloroethoxy)methane 5 07/22/22 05:01 V21824JMV
<36.7 µg/L 36.7 50.3Bis(2-Chloroethyl)ether 5 07/22/22 05:01 V21824JMV
<33.1 µg/L 33.1 50.3Bis(2-Chloroisopropyl)ether 5 07/22/22 05:01 V21824JMV
<44.3 µg/L 44.3 50.3Bis(2-ethylhexyl)phthalate 5 07/22/22 05:01 V21824JMV
<31.6 µg/L 31.6 1014-Bromophenyl phenyl ether 5 07/22/22 05:01 V21824JMV
<22.8 µg/L 22.8 50.3
Butyl benzyl phthalate 5 07/22/22 05:01 V21824JMV
<26.3 µg/L 26.3 50.34-Chloro-3-methylphenol 5 07/22/22 05:01 V21824JMV
<37.3 µg/L 37.3 1012-Chloronaphthalene 5 07/22/22 05:01 V21824JMV
<33.1 µg/L 33.1 50.32-Chlorophenol 5 07/22/22 05:01 V21824JMV
<35.3 µg/L 35.3 1014-Chlorophenyl phenyl ether 5 07/22/22 05:01 V21824JMV
<27.1 µg/L 27.1 50.3Chrysene 5 07/22/22 05:01 V21824JMV
<30.4 µg/L 30.4 101Dibenz(a,h)anthracene 5 07/22/22 05:01 V21824JMV
<25.7 µg/L 25.7 101
Dibenzofuran 5 07/22/22 05:01 V21824JMV
<29.7 µg/L 29.7 50.31,2-Dichlorobenzene 5 07/22/22 05:01 V21824JMV
<29.3 µg/L 29.3 50.31,3-Dichlorobenzene 5 07/22/22 05:01 V21824JMV
<29.7 µg/L 29.7 50.31,4-Dichlorobenzene 5 07/22/22 05:01 V21824JMV
<33.2 µg/L 33.2 50.33,3'-Dichlorobenzidine 5 07/22/22 05:01 V21824JMV
<27.9 µg/L 27.9 50.32,4-Dichlorophenol 5 07/22/22 05:01 V21824JMV
<47.2 µg/L 47.2 101Diethyl phthalate 5 07/22/22 05:01 V21824JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V21605 07/21/22 08:56
<39.3 µg/L 39.3 50.3Dimethyl phthalate 5 07/22/22 05:01 V21824JMV
<55.2 µg/L 55.2 1012,4-Dimethylphenol 5 07/22/22 05:01 V21824JMV
<37.0 µg/L 37.0 50.3Di-n-butyl phthalate 5 07/22/22 05:01 V21824JMV
<49.9 µg/L 49.9 1514,6-Dinitro-2-methylphenol 5 07/22/22 05:01 V21824JMV
<53.6 µg/L 53.6 1512,4-Dinitrophenol 5 07/22/22 05:01 V21824JMV
<26.2 µg/L 26.2 50.32,4-Dinitrotoluene 5 07/22/22 05:01 V21824JMV
<29.8 µg/L 29.8 1012,6-Dinitrotoluene 5 07/22/22 05:01 V21824JMV
<25.2 µg/L 25.2 50.3Di-n-Octyl Phthalate 5 07/22/22 05:01 V21824JMV
<30.3 µg/L 30.3 50.3
Fluoranthene 5 07/22/22 05:01 V21824JMV
<36.6 µg/L 36.6 50.3Fluorene 5 07/22/22 05:01 V21824JMV
<29.0 µg/L 29.0 101Hexachlorobenzene 5 07/22/22 05:01 V21824JMV
<29.7 µg/L 29.7 101Hexachlorobutadiene 5 07/22/22 05:01 V21824JMV
<29.8 µg/L 29.8 101Hexachlorocyclopentadiene 5 07/22/22 05:01 V21824JMV
<26.3 µg/L 26.3 50.3Hexachloroethane 5 07/22/22 05:01 V21824JMV
<31.2 µg/L 31.2 50.3Indeno(1,2,3-cd)pyrene 5 07/22/22 05:01 V21824JMV
<33.8 µg/L 33.8 50.3
Isophorone 5 07/22/22 05:01 V21824JMV
215 µg/L 5.53 50.31-Methylnaphthalene 5 07/22/22 05:01 V21824JMV
431 µg/L 34.8 50.32-Methylnaphthalene 5 07/22/22 05:01 V21824JMV
776 µg/L 39.6 50.3Naphthalene 5 07/22/22 05:01 V21824JMV
<39.6 µg/L 39.6 50.3Nitrobenzene 5 07/22/22 05:01 V21824JMV
<27.6 µg/L 27.6 50.32-Nitrophenol 5 07/22/22 05:01 V21824JMV
<14.1 µg/L 14.1 50.34-Nitrophenol 5 07/22/22 05:01 V21824JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V21605 07/21/22 08:56
<55.2 µg/L 55.2 101N-Nitrosodiphenylamine 5 07/22/22 05:01 V21824JMV
<40.9 µg/L 40.9 101N-Nitroso-di-n-propylamine 5 07/22/22 05:01 V21824JMV
<48.8 µg/L 48.8 251Pentachlorophenol 5 07/22/22 05:01 V21824JMV
<31.9 µg/L 31.9 50.3Phenanthrene 5 07/22/22 05:01 V21824JMV
<14.4 µg/L 14.4 50.3Phenol 5 07/22/22 05:01 V21824JMV
<27.3 µg/L 27.3 50.3Pyrene 5 07/22/22 05:01 V21824JMV
<31.4 µg/L 31.4 50.31,2,4-Trichlorobenzene 5 07/22/22 05:01 V21824JMV
<31.8 µg/L 31.8 1012,4,6-Trichlorophenol 5 07/22/22 05:01 V21824JMV
625.1Surrogate: Phenol-d5 25.7 Limits: 10-63%07/22/22 05:015 JMV
Surrogate: 2-Fluorobiphenyl 67.2 Limits: 49-118%07/22/22 05:015 JMV V21824
Surrogate: 2-Fluorophenol 41.7 Limits: 22-84%07/22/22 05:015 JMV V21824
Surrogate: Nitrobenzene-d5 63.4 Limits: 43-123%07/22/22 05:015 JMV V21824
Surrogate: 4-Terphenyl-d14 76.3 Limits: 49-151%07/22/22 05:015 JMV V21824
Surrogate: 2,4,6-Tribromophenol 76.2 Limits: 31-144%07/22/22 05:015 JMV V21824
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V21593 07/20/22 16:30
<0.00340 µg/L 0.00340 0.02061,2-Dibromoethane 1 07/21/22 01:14 V21719JC1
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 34
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-196-0032
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 07/15/2022
CK 2720104
Report Date : 08/02/2022
Sample ID :
Lab No :
Sampled:MW-1
94407 Matrix:
7/14/2022 13:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V21488 07/19/22 09:12
1890 µg/L 28.2 350Aliphatic C9-C18 1 07/25/22 19:19 V21899JLK
<124 µg/L 124 500Aliphatic C19-C36 1 07/25/22 19:19 V21899JLK
2520 µg/L 61.2 250Aromatic C11-C22 1 07/25/22 19:19 V21899JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 104 Limits: 40-140%07/25/22 19:191 JLK
MADEP-EPHSurrogate: Chlorooctadecane 48.5 Limits: 40-140%07/25/22 19:191 JLK
MADEP-EPHSurrogate: OTP Surrogate 51.0 Limits: 40-140%07/25/22 19:191 JLK
Surrogate: 2-Fluorobiphenyl 88.3 Limits: 40-140%07/25/22 19:191 JLK V21899
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V21452 07/18/22 08:00
17100 µg/L 1150 5000
Aliphatic C5-C8 100 07/18/22 14:25 V21453TBL
53800 µg/L 2580 5000Aliphatic C9-C12 100 07/18/22 14:25 V21453TBL
14000 µg/L 402 5000Aromatic C9-C10 100 07/18/22 14:25 V21453TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)103 Limits: 70-130%07/18/22 14:25100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)115 Limits: 70-130%07/18/22 14:25100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 34
Sample ID Report Lab No
LRB 22-196-0032 LRB-V21605
Paramater Result Units
Dilution
Factor Method Analysis Date/Time Analyst Batch ID
NO TICS REPORTED 0 ug/L 1 625.1 7/21/2022 19:44 JMV V21824
Sample ID Report Lab No
MW-1 22-195-018 V 94288
Paramater Result Units
Dilution
Factor Method Analysis Date/Time Analyst Batch ID
Toluene 1290 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Dimethyl Benzene 1985 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Propyl Benzene 540 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Methyl Ethyl Benzene 2955 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Trimethyl Benzene 3570 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Indane 580 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Methyl Propyl Benzene 495 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Dimethyl Ethyl Benzene 1055 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Tetramethyl Benzene 515 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Dimethyl Ethenyl Benzene 935 ug/L 5 625.1 7/22/2022 5:01 JMV V21824
Page 16 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Metals Analyses
6020B
V21476QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V21377
Associated Lab Samples: 94407
LRB-V21377 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/18/22 17:070.00100.0005<0.0005mg/LLead
LCS-V21377Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1000.09990.100mg/LLead 80-120
V 94190-MS-V21377 V 94190-MSD-V21377Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.102 1020.1010.1000.100<0.0005mg/LLead 101 75-125 0.9 20
V 94190-PDS-V21377Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/18/22 17:391090.0546mg/LLead
Page 1 of 16Date:08/02/2022 02:18 PM
Page 17 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
Associated Lab Samples: 94407
LRB-V21615 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/20/22 13:4610.01.80<1.80µg/LAcetone
07/20/22 13:460.5000.180<0.180µg/LBenzene
07/20/22 13:460.5000.210<0.210µg/LBromobenzene
07/20/22 13:461.000.420<0.420µg/LBromochloromethane
07/20/22 13:460.5000.160<0.160µg/LBromodichloromethane
07/20/22 13:465.001.50<1.50µg/LBromoform
07/20/22 13:461.000.280<0.280µg/LBromomethane
07/20/22 13:460.5000.180<0.180µg/Ln-Butylbenzene
07/20/22 13:460.5000.200<0.200µg/Lsec-Butyl benzene
07/20/22 13:462.000.920<0.920µg/Ltert-Butyl benzene
07/20/22 13:460.5000.180<0.180µg/LCarbon Tetrachloride
07/20/22 13:460.5000.190<0.190µg/LChlorobenzene
07/20/22 13:460.5000.190<0.190µg/LChlorodibromomethane
07/20/22 13:461.000.430<0.430µg/LChloroethane
07/20/22 13:460.5000.220<0.220µg/LChloroform
07/20/22 13:460.5000.220<0.220µg/LChloromethane
07/20/22 13:460.5000.200<0.200µg/L2-Chlorotoluene
07/20/22 13:460.5000.200<0.200µg/L4-Chlorotoluene
07/20/22 13:460.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/20/22 13:462.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/20/22 13:460.5000.230<0.230µg/LDibromomethane
07/20/22 13:460.5000.220<0.220µg/L1,2-Dichlorobenzene
07/20/22 13:460.5000.190<0.190µg/L1,3-Dichlorobenzene
07/20/22 13:460.5000.210<0.210µg/L1,4-Dichlorobenzene
07/20/22 13:465.001.20<1.20µg/LDichlorodifluoromethane
07/20/22 13:460.5000.240<0.240µg/L1,1-Dichloroethane
07/20/22 13:460.5000.150<0.150µg/L1,2-Dichloroethane
Page 2 of 16Date:08/02/2022 02:18 PM
Page 18 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
Associated Lab Samples: 94407
LRB-V21615 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/20/22 13:460.5000.150<0.150µg/L1,1-Dichloroethene
07/20/22 13:460.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/20/22 13:460.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/20/22 13:460.5000.190<0.190µg/L1,2-Dichloropropane
07/20/22 13:460.5000.130<0.130µg/L1,3-Dichloropropane
07/20/22 13:462.000.210<0.210µg/L2,2-Dichloropropane
07/20/22 13:460.5000.200<0.200µg/L1,1-Dichloropropene
07/20/22 13:460.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/20/22 13:460.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/20/22 13:4620042.0<42.0µg/LEthanol
07/20/22 13:460.5000.170<0.170µg/LEthylbenzene
07/20/22 13:4610.00.059<0.059µg/LEthyl Tertiary Butyl Ether (ETBE)
07/20/22 13:463.000.350<0.350µg/LHexachlorobutadiene
07/20/22 13:461.000.380<0.380µg/L2-Hexanone
07/20/22 13:460.5000.180<0.180µg/LIsopropylbenzene
07/20/22 13:460.5000.089<0.089µg/L4-Isopropyl toluene
07/20/22 13:465.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/20/22 13:461.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/20/22 13:461.000.078<0.078µg/L4-Methyl-2-Pentanone
07/20/22 13:462.000.330<0.330µg/LMethylene Chloride
07/20/22 13:461.000.470<0.470µg/LNaphthalene
07/20/22 13:460.5000.190<0.190µg/Ln-Propylbenzene
07/20/22 13:460.5000.220<0.220µg/LStyrene
07/20/22 13:4610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/20/22 13:4610.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/20/22 13:4610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/20/22 13:4610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 3 of 16Date:08/02/2022 02:18 PM
Page 19 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
Associated Lab Samples: 94407
LRB-V21615 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/20/22 13:460.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/20/22 13:460.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/20/22 13:460.5000.220<0.220µg/LTetrachloroethene
07/20/22 13:460.5000.220<0.220µg/LToluene
07/20/22 13:460.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/20/22 13:460.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/20/22 13:460.5000.160<0.160µg/L1,1,1-Trichloroethane
07/20/22 13:460.5000.096<0.096µg/L1,1,2-Trichloroethane
07/20/22 13:460.5000.180<0.180µg/LTrichloroethene
07/20/22 13:460.5000.180<0.180µg/LTrichlorofluoromethane
07/20/22 13:460.5000.270<0.270µg/L1,2,3-Trichloropropane
07/20/22 13:460.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/20/22 13:460.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/20/22 13:465.001.00<1.00µg/LVinyl Acetate
07/20/22 13:460.5000.170<0.170µg/LVinyl Chloride
07/20/22 13:460.5000.210<0.210µg/Lo-Xylene
07/20/22 13:461.000.420<0.420µg/Lm,p-Xylene
07/20/22 13:4610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/20/22 13:464-Bromofluorobenzene (S)98.4 70-130
07/20/22 13:46Dibromofluoromethane (S)103 70-130
07/20/22 13:461,2-Dichloroethane - d4 (S)93.4 70-130
07/20/22 13:46Toluene-d8 (S)82.0 70-130
Page 4 of 16Date:08/02/2022 02:18 PM
Page 20 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
LCS-V21615 LCSD-V21615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
45.1 11311545.940.0µg/LAcetone 40-160 1.7 20.0
25.7 12912825.620.0µg/LBenzene 70-130 0.3 20.0
17.7 88.590.018.020.0µg/LBromobenzene 70-130 1.6 20.0
24.4 12212925.720.0µg/LBromochloromethane 70-130 5.1 20.0
23.6 11812825.620.0µg/LBromodichloromethane 70-130 8.1 20.0
18.4 92.095.019.020.0µg/LBromoform 70-130 3.2 20.0
25.7 12912925.720.0µg/LBromomethane 60-140 0.0 20.0
17.8 89.090.518.120.0µg/Ln-Butylbenzene 70-130 1.6 20.0
18.2 91.092.518.520.0µg/Lsec-Butyl benzene 70-130 1.6 20.0
17.8 89.090.518.120.0µg/Ltert-Butyl benzene 70-130 1.6 20.0
22.8 11412324.520.0µg/LCarbon Tetrachloride 70-130 7.1 20.0
19.4 97.010120.220.0µg/LChlorobenzene 70-130 4.0 20.0
20.9 10510621.220.0µg/LChlorodibromomethane 70-130 1.4 20.0
25.0 12512925.820.0µg/LChloroethane 60-140 3.1 20.0
23.8 11913025.920.0µg/LChloroform 70-130 8.4 20.0
24.7 12412324.520.0µg/LChloromethane 60-140 0.8 20.0
18.1 90.591.518.320.0µg/L2-Chlorotoluene 70-130 1.0 20.0
17.6 88.090.518.120.0µg/L4-Chlorotoluene 70-130 2.8 20.0
23.8 11912525.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.9 20.0
18.3 91.510220.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 10.3 20.0
24.4 12212525.020.0µg/LDibromomethane 70-130 2.4 20.0
17.8 89.090.018.020.0µg/L1,2-Dichlorobenzene 70-130 1.1 20.0
17.8 89.091.518.320.0µg/L1,3-Dichlorobenzene 70-130 2.7 20.0
18.0 90.091.018.220.0µg/L1,4-Dichlorobenzene 70-130 1.1 20.0
23.9 12012725.420.0µg/LDichlorodifluoromethane 60-140 6.0 20.0
24.1 12112925.720.0µg/L1,1-Dichloroethane 70-130 6.4 20.0
Page 5 of 16Date:08/02/2022 02:18 PM
Page 21 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
LCS-V21615 LCSD-V21615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.4 11712424.820.0µg/L1,2-Dichloroethane 70-130 5.8 20.0
23.4 11712725.320.0µg/L1,1-Dichloroethene 70-130 7.8 20.0
23.2 11612625.220.0µg/Lcis-1,2-Dichloroethene 70-130 8.2 20.0
23.9 12012625.120.0µg/Ltrans-1,2-Dichloroethene 70-130 4.8 20.0
24.5 12312925.820.0µg/L1,2-Dichloropropane 70-130 5.1 20.0
19.5 97.510220.320.0µg/L1,3-Dichloropropane 70-130 4.0 20.0
23.7 11913025.920.0µg/L2,2-Dichloropropane 70-130 8.8 20.0
23.5 11812224.420.0µg/L1,1-Dichloropropene 70-130 3.7 20.0
25.7 12913025.920.0µg/Lcis-1,3-Dichloropropene 70-130 0.7 20.0
25.7 12913026.020.0µg/Ltrans-1,3-Dichloropropene 70-130 1.1 20.0
586 117120602500µg/LEthanol 60-140 2.6 20.0
18.7 93.598.019.620.0µg/LEthylbenzene 70-130 4.6 20.0
51.1 12813051.840.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.3 20.0
17.1 85.588.017.620.0µg/LHexachlorobutadiene 70-130 2.8 20.0
18.7 93.598.019.620.0µg/L2-Hexanone 60-140 4.6 20.0
18.2 91.092.018.420.0µg/LIsopropylbenzene 70-130 1.0 20.0
17.7 88.590.018.020.0µg/L4-Isopropyl toluene 70-130 1.6 20.0
21.8 10913025.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 17.1 20.0
25.2 12613025.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.7 20.0
23.5 11812625.120.0µg/L4-Methyl-2-Pentanone 60-140 6.5 20.0
22.7 11412424.820.0µg/LMethylene Chloride 70-130 8.8 20.0
17.6 88.087.517.520.0µg/LNaphthalene 70-130 0.5 20.0
18.0 90.092.018.420.0µg/Ln-Propylbenzene 70-130 2.1 20.0
18.9 94.510220.320.0µg/LStyrene 70-130 7.1 20.0
48.0 12010341.040.0µg/Ltert-Butyl Alcohol (TBA)40-140 15.7 20.0
44.7 11213051.840.0µg/Ltert-Butyl formate (TBF)40-140 14.7 20.0
Page 6 of 16Date:08/02/2022 02:18 PM
Page 22 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21617QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21615
LCS-V21615 LCSD-V21615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.6 10811222.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 3.1 20.0
51.7 12913051.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.3 20.0
18.0 90.095.519.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.9 20.0
18.7 93.588.517.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.4 20.0
18.7 93.597.019.420.0µg/LTetrachloroethene 70-130 3.6 20.0
24.8 12413025.920.0µg/LToluene 70-130 4.3 20.0
18.6 93.098.019.620.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0
18.2 91.089.517.920.0µg/L1,2,4-Trichlorobenzene 70-130 1.6 20.0
23.0 11512525.020.0µg/L1,1,1-Trichloroethane 70-130 8.3 20.0
23.7 11913025.920.0µg/L1,1,2-Trichloroethane 70-130 8.8 20.0
23.9 12013026.020.0µg/LTrichloroethene 70-130 8.4 20.0
22.8 11412224.420.0µg/LTrichlorofluoromethane 60-140 6.7 20.0
15.8 79.081.016.220.0µg/L1,2,3-Trichloropropane 70-130 2.5 20.0
18.0 90.091.518.320.0µg/L1,2,4-Trimethylbenzene 70-130 1.6 20.0
17.9 89.590.018.020.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
18.5 92.510521.020.0µg/LVinyl Acetate 60-140 12.6 20.0
24.0 12012725.420.0µg/LVinyl Chloride 60-140 5.6 20.0
19.5 97.510120.220.0µg/Lo-Xylene 70-130 3.5 20.0
40.4 10110541.940.0µg/Lm,p-Xylene 70-130 3.6 20.0
20.8 10410520.920.0µg/L3,3-Dimethyl-1-butanol 70-130 0.4 20.0
10097.84-Bromofluorobenzene (S)70-130
98.0102Dibromofluoromethane (S)70-130
86.298.01,2-Dichloroethane - d4 (S)70-130
84.085.2Toluene-d8 (S)70-130
Page 7 of 16Date:08/02/2022 02:18 PM
Page 23 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
Associated Lab Samples: 94407
LRB-V21605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/22 19:4410.07.12<7.12µg/LAcenaphthene
07/21/22 19:4420.06.94<6.94µg/LAcenaphthylene
07/21/22 19:4410.06.57<6.57µg/LAnthracene
07/21/22 19:4410.05.08<5.08µg/LBenzidine
07/21/22 19:4410.06.65<6.65µg/LBenzo(a)anthracene
07/21/22 19:4410.04.67<4.67µg/LBenzo(a)pyrene
07/21/22 19:4410.04.52<4.52µg/LBenzo(b)fluoranthene
07/21/22 19:4410.04.24<4.24µg/LBenzo(g,h,i)perylene
07/21/22 19:4410.04.86<4.86µg/LBenzo(k)fluoranthene
07/21/22 19:4450.011.5<11.5µg/LBenzoic Acid
07/21/22 19:4410.08.60<8.60µg/LBenzyl alcohol
07/21/22 19:4410.05.67<5.67µg/LBis(2-Chloroethoxy)methane
07/21/22 19:4410.07.30<7.30µg/LBis(2-Chloroethyl)ether
07/21/22 19:4410.06.59<6.59µg/LBis(2-Chloroisopropyl)ether
07/21/22 19:4410.08.80<8.80µg/LBis(2-ethylhexyl)phthalate
07/21/22 19:4420.06.26<6.26µg/L4-Bromophenyl phenyl ether
07/21/22 19:4410.04.53<4.53µg/LButyl benzyl phthalate
07/21/22 19:4410.05.23<5.23µg/L4-Chloro-3-methylphenol
07/21/22 19:4420.07.38<7.38µg/L2-Chloronaphthalene
07/21/22 19:4410.06.58<6.58µg/L2-Chlorophenol
07/21/22 19:4420.06.99<6.99µg/L4-Chlorophenyl phenyl ether
07/21/22 19:4410.05.38<5.38µg/LChrysene
07/21/22 19:4420.06.01<6.01µg/LDibenz(a,h)anthracene
07/21/22 19:4420.05.08<5.08µg/LDibenzofuran
07/21/22 19:4410.05.91<5.91µg/L1,2-Dichlorobenzene
07/21/22 19:4410.05.83<5.83µg/L1,3-Dichlorobenzene
07/21/22 19:4410.05.91<5.91µg/L1,4-Dichlorobenzene
Page 8 of 16Date:08/02/2022 02:18 PM
Page 24 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
Associated Lab Samples: 94407
LRB-V21605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/22 19:4410.06.60<6.60µg/L3,3'-Dichlorobenzidine
07/21/22 19:4410.05.54<5.54µg/L2,4-Dichlorophenol
07/21/22 19:4420.09.35<9.35µg/LDiethyl phthalate
07/21/22 19:4410.07.82<7.82µg/LDimethyl phthalate
07/21/22 19:4420.010.9<10.9µg/L2,4-Dimethylphenol
07/21/22 19:4410.07.35<7.35µg/LDi-n-butyl phthalate
07/21/22 19:4430.09.92<9.92µg/L4,6-Dinitro-2-methylphenol
07/21/22 19:4430.010.6<10.6µg/L2,4-Dinitrophenol
07/21/22 19:4410.05.20<5.20µg/L2,4-Dinitrotoluene
07/21/22 19:4420.05.90<5.90µg/L2,6-Dinitrotoluene
07/21/22 19:4410.05.01<5.01µg/LDi-n-Octyl Phthalate
07/21/22 19:4410.06.03<6.03µg/LFluoranthene
07/21/22 19:4410.07.27<7.27µg/LFluorene
07/21/22 19:4420.05.75<5.75µg/LHexachlorobenzene
07/21/22 19:4420.05.88<5.88µg/LHexachlorobutadiene
07/21/22 19:4420.05.90<5.90µg/LHexachlorocyclopentadiene
07/21/22 19:4410.05.22<5.22µg/LHexachloroethane
07/21/22 19:4410.06.20<6.20µg/LIndeno(1,2,3-cd)pyrene
07/21/22 19:4410.06.71<6.71µg/LIsophorone
07/21/22 19:4410.01.10<1.10µg/L1-Methylnaphthalene
07/21/22 19:4410.06.92<6.92µg/L2-Methylnaphthalene
07/21/22 19:4410.07.88<7.88µg/LNaphthalene
07/21/22 19:4410.07.88<7.88µg/LNitrobenzene
07/21/22 19:4410.05.49<5.49µg/L2-Nitrophenol
07/21/22 19:4410.02.81<2.81µg/L4-Nitrophenol
07/21/22 19:4420.010.9<10.9µg/LN-Nitrosodiphenylamine
07/21/22 19:4420.08.10<8.10µg/LN-Nitroso-di-n-propylamine
Page 9 of 16Date:08/02/2022 02:18 PM
Page 25 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
Associated Lab Samples: 94407
LRB-V21605 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/21/22 19:4450.09.73<9.73µg/LPentachlorophenol
07/21/22 19:4410.06.34<6.34µg/LPhenanthrene
07/21/22 19:4410.02.86<2.86µg/LPhenol
07/21/22 19:4410.05.42<5.42µg/LPyrene
07/21/22 19:4410.06.25<6.25µg/L1,2,4-Trichlorobenzene
07/21/22 19:4420.06.29<6.29µg/L2,4,6-Trichlorophenol
07/21/22 19:442-Fluorobiphenyl (S)53.8 49-118
07/21/22 19:442-Fluorophenol (S)32.5 22-84
07/21/22 19:44Nitrobenzene-d5 (S)49.0 43-123
07/21/22 19:444-Terphenyl-d14 (S)66.4 49-151
07/21/22 19:442,4,6-Tribromophenol (S)55.9 31-144
07/21/22 19:44Phenol-d5 (S)21.1 10-63
LCS-V21605 LCSD-V21605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.2 58.463.831.950.0µg/LAcenaphthene 47-145 8.8 20.0
29.8 59.666.233.150.0µg/LAcenaphthylene 33-145 10.4 20.0
32.0 64.070.635.350.0µg/LAnthracene 27-133 9.8 20.0
21.5 43.055.427.750.0µg/LBenzidine 15-150 25.2*20.0
31.7 63.467.833.950.0µg/LBenzo(a)anthracene 33-143 6.7 20.0
39.2 78.485.242.650.0µg/LBenzo(a)pyrene 17-163 8.3 20.0
35.5 71.075.637.850.0µg/LBenzo(b)fluoranthene 24-159 6.2 20.0
32.0 64.070.435.250.0µg/LBenzo(g,h,i)perylene 10-219 9.5 20.0
33.5 67.073.036.550.0µg/LBenzo(k)fluoranthene 11-162 8.5 20.0
<11.5 0.0*0.0*<11.550.0µg/LBenzoic Acid 10-125 0.0 20.0
Page 10 of 16* QC Fail Date:08/02/2022 02:18 PM
Page 26 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
LCS-V21605 LCSD-V21605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
27.6 55.262.231.150.0µg/LBenzyl alcohol 16-107 11.9 20.0
26.5 53.058.629.350.0µg/LBis(2-Chloroethoxy)methane 33-184 10.0 20.0
24.7 49.456.228.150.0µg/LBis(2-Chloroethyl)ether 12-158 12.8 20.0
27.4 54.859.029.550.0µg/LBis(2-Chloroisopropyl)ether 36-166 7.3 20.0
37.7 75.481.440.750.0µg/LBis(2-ethylhexyl)phthalate 10-158 7.6 20.0
30.0 60.066.433.250.0µg/L4-Bromophenyl phenyl ether 53-127 10.1 20.0
36.3 72.678.239.150.0µg/LButyl benzyl phthalate 10-152 7.4 20.0
26.8 53.658.629.350.0µg/L4-Chloro-3-methylphenol 22-147 8.9 20.0
28.5 57.0*64.832.450.0µg/L2-Chloronaphthalene 60-118 12.8 20.0
24.8 49.653.826.950.0µg/L2-Chlorophenol 23-134 8.1 20.0
29.2 58.463.831.950.0µg/L4-Chlorophenyl phenyl ether 25-158 8.8 20.0
32.2 64.468.634.350.0µg/LChrysene 17-168 6.3 20.0
31.0 62.069.034.550.0µg/LDibenz(a,h)anthracene 10-227 10.6 20.0
29.2 58.463.831.950.0µg/LDibenzofuran 39-114 8.8 20.0
23.4 46.849.624.850.0µg/L1,2-Dichlorobenzene 32-129 5.8 20.0
22.5 45.048.224.150.0µg/L1,3-Dichlorobenzene 20-124 6.8 20.0
22.5 45.048.024.050.0µg/L1,4-Dichlorobenzene 20-124 6.4 20.0
27.6 55.257.628.850.0µg/L3,3'-Dichlorobenzidine 10-262 4.2 20.0
25.8 51.655.627.850.0µg/L2,4-Dichlorophenol 39-135 7.4 20.0
32.4 64.869.234.650.0µg/LDiethyl phthalate 10-114 6.5 20.0
31.1 62.268.434.250.0µg/LDimethyl phthalate 10-112 9.4 20.0
30.1 60.267.433.750.0µg/L2,4-Dimethylphenol 32-119 11.2 20.0
37.7 75.481.240.650.0µg/LDi-n-butyl phthalate 10-118 7.4 20.0
28.9 57.863.031.550.0µg/L4,6-Dinitro-2-methylphenol 10-181 8.6 20.0
21.9 43.849.624.850.0µg/L2,4-Dinitrophenol 10-191 12.4 20.0
32.3 64.670.235.150.0µg/L2,4-Dinitrotoluene 39-139 8.3 20.0
Page 11 of 16* QC Fail Date:08/02/2022 02:18 PM
Page 27 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
LCS-V21605 LCSD-V21605Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.9 65.870.835.450.0µg/L2,6-Dinitrotoluene 50-158 7.3 20.0
33.8 67.672.436.250.0µg/LDi-n-Octyl Phthalate 10-146 6.8 20.0
32.7 65.470.035.050.0µg/LFluoranthene 26-137 6.7 20.0
29.8 59.665.432.750.0µg/LFluorene 59-121 9.2 20.0
29.7 59.465.032.550.0µg/LHexachlorobenzene 10-152 9.0 20.0
20.9 41.847.223.650.0µg/LHexachlorobutadiene 24-116 12.1 20.0
20.7 41.448.824.450.0µg/LHexachlorocyclopentadiene 32-117 16.4 20.0
21.8 43.646.223.150.0µg/LHexachloroethane 40-113 5.7 20.0
31.2 62.469.634.850.0µg/LIndeno(1,2,3-cd)pyrene 10-171 10.9 20.0
24.4 48.853.026.550.0µg/LIsophorone 21-196 8.2 20.0
24.5 49.054.427.250.0µg/L1-Methylnaphthalene 40-135 10.4 20.0
23.8 47.652.026.050.0µg/L2-Methylnaphthalene 18-121 8.8 20.0
23.8 47.652.226.150.0µg/LNaphthalene 21-133 9.2 20.0
25.9 51.855.827.950.0µg/LNitrobenzene 35-180 7.4 20.0
24.7 49.453.626.850.0µg/L2-Nitrophenol 29-182 8.1 20.0
17.2 34.437.818.950.0µg/L4-Nitrophenol 10-132 9.4 20.0
38.0 76.084.042.050.0µg/LN-Nitrosodiphenylamine 69-152 10.0 20.0
27.1 54.259.029.550.0µg/LN-Nitroso-di-n-propylamine 10-230 8.4 20.0
36.2 72.476.238.150.0µg/LPentachlorophenol 14-176 5.1 20.0
31.8 63.668.834.450.0µg/LPhenanthrene 54-120 7.8 20.0
11.3 22.631.415.750.0µg/LPhenol 10-112 32.5*20.0
32.7 65.470.835.450.0µg/LPyrene 52-115 7.9 20.0
21.8 43.6*48.024.050.0µg/L1,2,4-Trichlorobenzene 44-142 9.6 20.0
28.2 56.464.432.250.0µg/L2,4,6-Trichlorophenol 37-144 13.2 20.0
54.863.82-Fluorobiphenyl (S)49-118
32.635.32-Fluorophenol (S)22-84
Page 12 of 16* QC Fail Date:08/02/2022 02:18 PM
Page 28 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V21824QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V21605
LCS-V21605 LCSD-V21605Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
48.853.4Nitrobenzene-d5 (S)43-123
64.269.64-Terphenyl-d14 (S)49-151
62.166.02,4,6-Tribromophenol (S)31-144
20.723.0Phenol-d5 (S)10-63
Page 13 of 16Date:08/02/2022 02:18 PM
Page 29 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V21719QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V21593
Associated Lab Samples: 94407
LRB-V21593 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/20/22 19:480.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V21593 LCSD-V21593Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.235 94.01000.2500.250µg/L1,2-Dibromoethane 70-130 6.1 20.0
V 93936-DUP-V21593Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/20/22 22:470.0<0.0207< 0.0207µg/L1,2-Dibromoethane
V 93935-MS-V21593Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.230 89.80.256< 0.00338µg/L1,2-Dibromoethane 70-130
Page 14 of 16Date:08/02/2022 02:18 PM
Page 30 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V21899QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V21488
Associated Lab Samples: 94407
LRB-V21488 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/25/22 15:0535028.247.7µg/LAliphatic C9-C18
07/25/22 15:05500124<124µg/LAliphatic C19-C36
07/25/22 15:0525061.2<61.2µg/LAromatic C11-C22
07/25/22 15:052-Fluorobiphenyl (S)88.5 40-140
07/25/22 15:052-Bromonaphthalene (S)87.5 40-140
07/25/22 15:05Chlorooctadecane (S)53.0 40-140
07/25/22 15:05OTP Surrogate (S)56.0 40-140
LCS-V21488 LCSD-V21488Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
402 67.064.6388600µg/LAliphatic C9-C18 40-140 3.5 50.0
562 70.265.8527800µg/LAliphatic C19-C36 40-140 6.4 50.0
1360 80.087.014801700µg/LAromatic C11-C22 40-140 8.4 50.0
85.789.02-Fluorobiphenyl (S)40-140
58.768.52-Bromonaphthalene (S)40-140
58.557.0Chlorooctadecane (S)40-140
56.561.5OTP Surrogate (S)40-140
Page 15 of 16Date:08/02/2022 02:18 PM
Page 31 of 34
Quality Control Data
22-196-0032Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
CK 2720104
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V21453QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V21452
Associated Lab Samples: 94407
LRB-V21452 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/18/22 11:3950.011.5<11.5µg/LAliphatic C5-C8
07/18/22 11:3950.025.8<25.8µg/LAliphatic C9-C12
07/18/22 11:3950.04.02<4.02µg/LAromatic C9-C10
07/18/22 11:392,5-Dibromotoluene (FID) (S)115 70-130
07/18/22 11:392,5-Dibromotoluene (PID) (S)124 70-130
LCS-V21452 LCSD-V21452Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
241 80.379.6239300µg/LAliphatic C5-C8 70-130 0.8 50.0
357 119119357300µg/LAliphatic C9-C12 70-130 0.0 50.0
118 118121121100µg/LAromatic C9-C10 70-130 2.5 50.0
10595.42,5-Dibromotoluene (FID) (S)70-130
1081012,5-Dibromotoluene (PID) (S)70-130
Page 16 of 16Date:08/02/2022 02:18 PM
Page 32 of 34
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-196-0032
ATC Group Services, LLC - Raleigh, NC
01024
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.4 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Paula Blakeborough Date & Time:07/15/2022 15:03:11
Special precautions or instructions included?
Comments:
Page 33 of 34
Page 34 of 34

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/25/2022
ATC Group Services, LLC - Raleigh, NC Maureen Jackson
609A Piner Road Suite 115 Wilminton, NC, 28409
Ref: Analytical Testing
Lab Report Number: 22-137-0007 Client Project Description: Circle K 2720104
Dear Maureen Jackson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/17/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 36
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-137-0007
Page 2 of 36
Report Number:
Sample Summary Table
Client Project Description:
22-137-0007
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/12/2022 13:40Solids 89999 L-7 05/17/2022 14:19
05/12/2022 13:50Solids 90000 L-8 05/17/2022 14:19
05/12/2022 13:35Solids 90001 D-5 05/17/2022 14:19
05/12/2022 13:45Solids 90002 D-6 05/17/2022 14:19
Page 3 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-137-0007
Report Limit
Project:Circle K 2720104
V 89999L-7
0.047 05/21/2022 09:418260DAcetonemg/Kg - dry 0.002
0.084 05/21/2022 09:418260DBenzenemg/Kg - dry 0.0007
J0.0007 05/21/2022 09:418260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.003 05/21/2022 09:418260DEthylbenzenemg/Kg - dry 0.0007
J0.004 05/21/2022 09:418260Dn-Hexane mg/Kg - dry 0.0008
J0.010 05/21/2022 09:418260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/21/2022 09:418260DNaphthalenemg/Kg - dry 0.001
0.117 05/21/2022 09:418260DToluenemg/Kg - dry 0.0008
J0.002 05/21/2022 09:418260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0007 05/21/2022 09:418260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
0.009 05/21/2022 09:418260Do-Xylene mg/Kg - dry 0.0006
0.022 05/21/2022 09:418260Dm,p-Xylene mg/Kg - dry 0.001
0.031 05/21/2022 09:418260DXylene (Total)mg/Kg - dry 0.0006
J1.59 05/18/2022 19:16MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.47
16.9 05/23/2022 13:13SW-DRYWT Moisture %
V 90000L-8
J0.016 05/21/2022 10:088260DAcetonemg/Kg - dry 0.002
J0.002 05/21/2022 10:088260DCarbon Disulfide mg/Kg - dry 0.0007
J0.003 05/21/2022 10:088260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.001 05/21/2022 10:088260DNaphthalenemg/Kg - dry 0.001
J0.001 05/21/2022 10:088260DToluenemg/Kg - dry 0.0008
J0.001 05/21/2022 10:088260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0010 05/21/2022 10:088260Do-Xylene mg/Kg - dry 0.0006
J0.001 05/21/2022 10:088260Dm,p-Xylene mg/Kg - dry 0.001
J0.002 05/21/2022 10:088260DXylene (Total)mg/Kg - dry 0.0006
13.1 05/23/2022 13:13SW-DRYWT Moisture %
V 90001D-5
J2.75 05/18/2022 14:098015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.31
0.158 05/21/2022 10:368260DAcetonemg/Kg - dry 0.002
J0.002 05/21/2022 10:368260DBenzenemg/Kg - dry 0.0006
J0.0009 05/21/2022 10:368260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0008
J0.005 05/21/2022 10:368260Dn-Hexane mg/Kg - dry 0.0007
0.049 05/21/2022 10:368260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.0007 05/21/2022 10:368260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.003 05/21/2022 10:368260Do-Xylene mg/Kg - dry 0.0006
J0.003 05/21/2022 10:368260Dm,p-Xylene mg/Kg - dry 0.001
Page 4 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-137-0007
Report Limit
Project:Circle K 2720104
V 90001D-5
J0.006 05/21/2022 10:368260DXylene (Total)mg/Kg - dry 0.0006
10.2 05/23/2022 13:13SW-DRYWT Moisture %
V 90002D-6
77.2 05/20/2022 06:578015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.08
5.64 05/18/2022 14:378015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.26
8.39 05/23/2022 13:13SW-DRYWT Moisture %
Page 5 of 36

Client: ATC Group Services, LLC - Raleigh, NC CASE NARRATIVE
Project: Circle K 2720104 Lab Report Number: 22-137-0007
Date: 5/24/2022
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 89767 (Stock 3) QC Batch No: V18982/V18830
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO
Sample 89999 (L-7) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18834/V18833 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acetone QC Batch No: V18991/V18990
CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. No further action taken.

Page 6 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.9 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
<2.49 mg/Kg - dry 2.49 6.02Gasoline Range Organics (C6-C10)50 05/18/22 13:13 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 142 *Limits: 50-137%05/18/22 13:1350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.047 mg/Kg - dry 0.002 0.024Acetone 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/21/22 09:41 V18991TBL
0.084 mg/Kg - dry 0.0007 0.006Benzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/21/22 09:41 V18991TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/21/22 09:41 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/21/22 09:41 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/21/22 09:41 V18991TBL
0.003 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/21/22 09:41 V18991TBL
0.004 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/21/22 09:41 V18991TBL
0.010 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 05/21/22 09:41 V18991TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/21/22 09:41 V18991TBL
0.002 J mg/Kg - dry 0.001 0.012Naphthalene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/21/22 09:41 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/21/22 09:41 V18991TBL
0.117 mg/Kg - dry 0.0008 0.006Toluene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/21/22 09:41 V18991TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/21/22 09:41 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/21/22 09:41 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/21/22 09:41 V18991TBL
0.009 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/21/22 09:41 V18991TBL
0.022 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/21/22 09:41 V18991TBL
0.031 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/21/22 09:41 V18991
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/21/22 09:411 TBL V18991
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/21/22 09:411 TBL V18991
Surrogate: Toluene-d8 84.3 Limits: 76-129%05/21/22 09:411 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18846 05/18/22 08:00
1.59 J mg/Kg - dry 1.47 9.63Aliphatic C5-C8 100 05/18/22 19:16 V18847TBL
<5.49 mg/Kg - dry 5.49 9.63Aliphatic C9-C12 100 05/18/22 19:16 V18847TBL
<0.750 mg/Kg - dry 0.750 9.63Aromatic C9-C10 100 05/18/22 19:16 V18847TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)101 Limits: 70-130%05/18/22 19:16100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)102 Limits: 70-130%05/18/22 19:16100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
<2.38 mg/Kg - dry 2.38 5.75Gasoline Range Organics (C6-C10)50 05/18/22 13:42 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 128 Limits: 50-137%05/18/22 13:4250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.016 J mg/Kg - dry 0.002 0.023Acetone 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/21/22 10:08 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/21/22 10:08 V18991TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/21/22 10:08 V18991TBL
0.003 J mg/Kg - dry 0.0007 0.023Methyl Ethyl Ketone (MEK)1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/21/22 10:08 V18991TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.001 0.011Naphthalene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/21/22 10:08 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/21/22 10:08 V18991TBL
0.0010 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/21/22 10:08 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/21/22 10:08 V18991
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/21/22 10:081 TBL V18991
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/21/22 10:081 TBL V18991
Surrogate: Toluene-d8 85.8 Limits: 76-129%05/21/22 10:081 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.2 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
2.75 J mg/Kg - dry 2.31 5.57Gasoline Range Organics (C6-C10)50 05/18/22 14:09 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 136 Limits: 50-137%05/18/22 14:0950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.158 mg/Kg - dry 0.002 0.022Acetone 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/21/22 10:36 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.005Benzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/21/22 10:36 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/21/22 10:36 V18991TBL
0.0009 J mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/21/22 10:36 V18991TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/21/22 10:36 V18991TBL
0.005 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/21/22 10:36 V18991TBL
0.049 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/21/22 10:36 V18991TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/21/22 10:36 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/21/22 10:36 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/21/22 10:36 V18991TBL
0.003 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/21/22 10:36 V18991TBL
0.003 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/21/22 10:36 V18991TBL
0.006 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/21/22 10:36 V18991
Surrogate: 4-Bromofluorobenzene 99.5 Limits: 70-130%05/21/22 10:361 TBL V18991
Surrogate: Dibromofluoromethane 99.5 Limits: 84-123%05/21/22 10:361 TBL V18991
Surrogate: Toluene-d8 86.0 Limits: 76-129%05/21/22 10:361 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-6
90002 Matrix:
5/12/2022 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.39 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-6
90002 Matrix:
5/12/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
77.2 mg/Kg - dry 5.08 10.9Diesel Range Organics (C10-C28)1 05/20/22 06:57 V18982JLK
8015C DROSurrogate: OTP Surrogate 97.7 Limits: 31-123%05/20/22 06:571 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
5.64 mg/Kg - dry 2.26 5.46Gasoline Range Organics (C6-C10)50 05/18/22 14:37 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 130 Limits: 50-137%05/18/22 14:3750 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V18982QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18830
Associated Lab Samples: 90002
LRB-V18830 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/19/22 21:2410.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
05/19/22 21:24OTP Surrogate (S)96.2 31-123
LCS-V18830Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10469.566.7mg/KgDiesel Range Organics (C10-C28)46-126
84.9OTP Surrogate (S)31-123
V 89767-MS-V18830 V 89767-MSD-V18830Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
291 -140*28266.666.6386mg/KgDiesel Range Organics (C10-C28)-140*50-117 3.1 24
70.9OTP Surrogate (S)67.3 31-123
Page 1 of 10* QC Fail Date:05/25/2022 02:51 PM
Page 25 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18834QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18833
Associated Lab Samples: 89999, 90000, 90001, 90002
LRB-V18833 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/18/22 12:455.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/18/22 12:45a,a,a-Trifluorotoluene (S)129 50-137
LCS-V18833Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10452.050.0mg/KgGasoline Range Organics (C6-C10)41-138
128a,a,a-Trifluorotoluene (S)50-137
V 89999-MS-V18833 V 89999-MSD-V18833Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
59.4 11958.350.050.0<2.07mg/KgGasoline Range Organics (C6-C10)117 41-138 1.8 34
137a,a,a-Trifluorotoluene (S)135 50-137
Page 2 of 10Date:05/25/2022 02:51 PM
Page 26 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0200.002<0.002mg/KgAcetone
05/21/22 02:170.0200.001<0.001mg/KgAcrolein
05/21/22 02:170.0200.0008<0.0008mg/KgAcrylonitrile
05/21/22 02:170.0050.0006<0.0006mg/KgBenzene
05/21/22 02:170.0050.0005<0.0005mg/KgBromobenzene
05/21/22 02:170.0050.0008<0.0008mg/KgBromochloromethane
05/21/22 02:170.0050.001<0.001mg/KgBromodichloromethane
05/21/22 02:170.0050.001<0.001mg/KgBromoform
05/21/22 02:170.0100.001<0.001mg/KgBromomethane
05/21/22 02:170.0050.0005<0.0005mg/Kgn-Butylbenzene
05/21/22 02:170.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/21/22 02:170.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/21/22 02:170.0050.0006<0.0006mg/KgCarbon Disulfide
05/21/22 02:170.0050.001<0.001mg/KgCarbon Tetrachloride
05/21/22 02:170.0050.0007<0.0007mg/KgChlorobenzene
05/21/22 02:170.0050.0009<0.0009mg/KgChlorodibromomethane
05/21/22 02:170.0100.0009<0.0009mg/KgChloroethane
05/21/22 02:170.0050.001<0.001mg/KgChloroform
05/21/22 02:170.0100.0006<0.0006mg/KgChloromethane
05/21/22 02:170.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/21/22 02:170.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/21/22 02:170.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/21/22 02:170.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/21/22 02:170.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/21/22 02:170.0050.0006<0.0006mg/KgDibromomethane
05/21/22 02:170.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/21/22 02:170.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 3 of 10Date:05/25/2022 02:51 PM
Page 27 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/21/22 02:170.0100.001<0.001mg/KgDichlorodifluoromethane
05/21/22 02:170.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/21/22 02:170.0050.001<0.001mg/Kg1,2-Dichloroethane
05/21/22 02:170.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/21/22 02:170.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/21/22 02:170.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/21/22 02:170.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/21/22 02:170.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/21/22 02:170.0050.001<0.001mg/Kg2,2-Dichloropropane
05/21/22 02:170.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/21/22 02:170.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/21/22 02:170.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/21/22 02:170.0050.0006<0.0006mg/KgEthylbenzene
05/21/22 02:170.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/21/22 02:170.0100.0008<0.0008mg/KgHexachlorobutadiene
05/21/22 02:170.0100.0007<0.0007mg/Kgn-Hexane
05/21/22 02:170.0200.0006<0.0006mg/Kg2-Hexanone
05/21/22 02:170.0050.0005<0.0005mg/KgIsopropylbenzene
05/21/22 02:170.0050.001<0.001mg/Kg4-Isopropyl toluene
05/21/22 02:170.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/21/22 02:170.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/21/22 02:170.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/21/22 02:170.0100.001<0.001mg/KgMethylene Chloride
05/21/22 02:170.0100.0010<0.0010mg/KgNaphthalene
05/21/22 02:170.0050.0005<0.0005mg/Kgn-Propylbenzene
05/21/22 02:170.0050.001<0.001mg/KgStyrene
Page 4 of 10Date:05/25/2022 02:51 PM
Page 28 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/21/22 02:170.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/21/22 02:170.0050.0009<0.0009mg/KgTetrachloroethene
05/21/22 02:170.0050.0007<0.0007mg/KgToluene
05/21/22 02:170.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/21/22 02:170.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/21/22 02:170.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/21/22 02:170.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/21/22 02:170.0050.0009<0.0009mg/KgTrichloroethene
05/21/22 02:170.0100.002<0.002mg/KgTrichlorofluoromethane
05/21/22 02:170.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/21/22 02:170.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/21/22 02:170.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/21/22 02:170.0100.0005<0.0005mg/KgVinyl Acetate
05/21/22 02:170.0100.0005<0.0005mg/KgVinyl Chloride
05/21/22 02:170.0050.0005<0.0005mg/Kgo-Xylene
05/21/22 02:170.0100.001<0.001mg/Kgm,p-Xylene
05/21/22 02:174-Bromofluorobenzene (S)104 70-130
05/21/22 02:17Dibromofluoromethane (S)105 84-123
05/21/22 02:17Toluene-d8 (S)86.8 76-129
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.090 90.181.00.0810.100mg/KgAcetone 29-198 10.6 20
0.078 78.393.80.0930.100mg/KgAcrolein 70-130 18.0 20
Page 5 of 10Date:05/25/2022 02:51 PM
Page 29 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.085 85.080.80.0800.100mg/KgAcrylonitrile 65-134 5.0 20
0.057 1151120.0550.050mg/KgBenzene 74-127 2.8 20
0.044 88.889.20.0440.050mg/KgBromobenzene 73-125 0.4 20
0.056 1131130.0560.050mg/KgBromochloromethane 72-134 0.5 20
0.060 1211150.0570.050mg/KgBromodichloromethane 75-122 4.7 20
0.047 94.091.80.0450.050mg/KgBromoform 66-135 2.3 20
0.054 1091050.0520.050mg/KgBromomethane 20-180 3.3 20
0.046 92.094.40.0470.050mg/Kgn-Butylbenzene 65-135 2.5 20
0.044 89.290.60.0450.050mg/Kgsec-Butyl benzene 66-131 1.5 20
0.043 87.288.60.0440.050mg/Kgtert-Butyl benzene 67-132 1.5 20
0.055 1121080.0540.050mg/KgCarbon Disulfide 61-129 3.2 20
0.054 1081070.0530.050mg/KgCarbon Tetrachloride 64-143 1.6 20
0.047 95.093.20.0460.050mg/KgChlorobenzene 74-118 1.9 20
0.047 94.293.00.0460.050mg/KgChlorodibromomethane 73-122 1.2 20
0.060 1201180.0590.050mg/KgChloroethane 33-149 1.8 20
0.057 1161120.0550.050mg/KgChloroform 73-127 3.5 20
0.042 84.087.80.0430.050mg/KgChloromethane 45-143 4.4 20
0.044 88.288.60.0440.050mg/Kg2-Chlorotoluene 67-124 0.4 20
0.045 90.291.60.0450.050mg/Kg4-Chlorotoluene 71-126 1.5 20
0.045 90.487.40.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.3 20
0.040 81.481.60.0400.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.2 20
0.047 95.094.20.0470.050mg/Kg1,2-Dibromoethane 70-132 0.8 20
0.058 1171150.0570.050mg/KgDibromomethane 74-133 1.9 20
0.043 86.686.80.0430.050mg/Kg1,2-Dichlorobenzene 72-123 0.2 20
0.043 87.887.20.0430.050mg/Kg1,3-Dichlorobenzene 71-120 0.6 20
0.043 86.486.40.0430.050mg/Kg1,4-Dichlorobenzene 71-123 0.0 20
Page 6 of 10Date:05/25/2022 02:51 PM
Page 30 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.057 1151120.0560.050mg/KgDichlorodifluoromethane 26-146 1.9 20
0.052 1041020.0510.050mg/Kg1,1-Dichloroethane 74-127 1.5 20
0.053 1071040.0510.050mg/Kg1,2-Dichloroethane 68-128 2.8 20
0.047 95.894.20.0470.050mg/Kg1,1-Dichloroethene 67-149 1.6 20
0.049 99.696.00.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 3.6 20
0.048 97.693.80.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.9 20
0.052 1051010.0500.050mg/Kg1,2-Dichloropropane 73-130 4.6 20
0.046 93.692.00.0460.050mg/Kg1,3-Dichloropropane 75-124 1.7 20
0.057 1141120.0550.050mg/Kg2,2-Dichloropropane 50-142 2.1 20
0.055 1101080.0540.050mg/Kg1,1-Dichloropropene 71-130 1.8 20
0.057 1151110.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 2.8 20
0.056 1131100.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.5 20
0.047 95.094.60.0470.050mg/KgEthylbenzene 74-128 0.4 20
0.097 97.092.60.0920.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.6 20
0.041 83.687.20.0430.050mg/KgHexachlorobutadiene 64-125 4.2 20
0.057 1151100.0540.050mg/Kgn-Hexane 70-130 4.6 20
0.031 62.862.80.0310.050mg/Kg2-Hexanone 61-157 0.0 20
0.044 89.890.40.0450.050mg/KgIsopropylbenzene 68-126 0.6 20
0.044 88.089.60.0440.050mg/Kg4-Isopropyl toluene 68-129 1.8 20
0.049 99.493.40.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 6.2 20
0.052 10498.80.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.1 20
0.042 84.079.80.0390.050mg/Kg4-Methyl-2-Pentanone 57-162 5.1 20
0.045 90.290.80.0450.050mg/KgMethylene Chloride 74-129 0.6 20
0.043 87.687.20.0430.050mg/KgNaphthalene 57-157 0.4 20
0.046 93.694.20.0470.050mg/Kgn-Propylbenzene 67-130 0.6 20
0.048 96.896.60.0480.050mg/KgStyrene 77-121 0.2 20
Page 7 of 10Date:05/25/2022 02:51 PM
Page 31 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 96.495.40.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.043 86.685.00.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.8 20
0.054 1101080.0540.050mg/KgTetrachloroethene 68-130 1.4 20
0.056 1131110.0550.050mg/KgToluene 71-129 2.5 20
0.042 84.685.00.0420.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.4 20
0.042 85.085.80.0420.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.9 20
0.058 1161110.0550.050mg/Kg1,1,1-Trichloroethane 67-131 4.9 20
0.047 95.294.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.2 20
0.056 1131110.0550.050mg/KgTrichloroethene 75-133 1.7 20
0.051 1041050.0520.050mg/KgTrichlorofluoromethane 44-146 0.9 20
0.042 85.084.40.0420.050mg/Kg1,2,3-Trichloropropane 60-137 0.7 20
0.043 87.288.80.0440.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.8 20
0.044 89.290.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.5 20
0.048 97.893.80.0460.050mg/KgVinyl Acetate 60-140 4.1 20
0.047 95.295.00.0470.050mg/KgVinyl Chloride 48-147 0.2 20
0.047 95.695.20.0470.050mg/Kgo-Xylene 74-126 0.4 20
0.096 96.296.60.0960.100mg/Kgm,p-Xylene 75-124 0.4 20
1001014-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
87.286.2Toluene-d8 (S)76-129
Page 8 of 10Date:05/25/2022 02:51 PM
Page 32 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V18847QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V18846
Associated Lab Samples: 89999
LRB-V18846 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/18/22 17:418.001.22<1.22mg/KgAliphatic C5-C8
05/18/22 17:418.004.56<4.56mg/KgAliphatic C9-C12
05/18/22 17:418.000.624<0.624mg/KgAromatic C9-C10
05/18/22 17:412,5-Dibromotoluene (FID) (S)84.0 70-130
05/18/22 17:412,5-Dibromotoluene (PID) (S)96.2 70-130
LCS-V18846 LCSD-V18846Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.7 10510333.032.0mg/KgAliphatic C5-C8 70-130 2.0 50
34.9 10911336.132.0mg/KgAliphatic C9-C12 70-130 3.3 50
12.6 11811912.710.7mg/KgAromatic C9-C10 70-130 0.7 50
85.886.92,5-Dibromotoluene (FID) (S)70-130
86.594.32,5-Dibromotoluene (PID) (S)70-130
Page 9 of 10Date:05/25/2022 02:51 PM
Page 33 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V19044QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89998-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/23/22 13:130.89.839.75%Moisture
V 90064-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/23/22 13:130.517.917.8%Moisture
Page 10 of 10Date:05/25/2022 02:51 PM
Page 34 of 36
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-137-0007
ATC Group Services, LLC - Raleigh, NC
01024
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:05/17/2022 14:59:08
Special precautions or instructions included?
Comments:
Page 35 of 36
Page 36 of 36

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/23/2022
ATC Group Services, LLC - Raleigh, NC Maureen Jackson
609A Piner Road Suite 115 Wilminton, NC, 28409
Ref: Analytical Testing
Lab Report Number: 22-133-0023 Client Project Description: Circle K 2720104
Dear Maureen Jackson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/13/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 166
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-133-0023
Page 2 of 166
Report Number:
Sample Summary Table
Client Project Description:
22-133-0023
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/10/2022 13:10Solids 89765 Stockpile 1 05/13/2022 11:00
05/10/2022 10:10Solids 89766 Stock 2 05/13/2022 11:00
05/10/2022 10:15Solids 89767 Stock 3 05/13/2022 11:00
05/10/2022 10:20Solids 89768 Stock 4 05/13/2022 11:00
05/11/2022 09:10Solids 89769 D-1 05/13/2022 11:00
05/11/2022 09:15Solids 89770 D-2 05/13/2022 11:00
05/11/2022 15:40Solids 89771 D-3 05/13/2022 11:00
05/11/2022 10:30Solids 89772 W-1 05/13/2022 11:00
05/11/2022 10:35Solids 89773 W-2 05/13/2022 11:00
05/11/2022 10:40Solids 89774 W-3 05/13/2022 11:00
05/11/2022 10:45Solids 89775 W-4 05/13/2022 11:00
05/11/2022 10:50Solids 89776 W-5 05/13/2022 11:00
05/11/2022 13:00Solids 89777 W-6 05/13/2022 11:00
05/11/2022 13:05Solids 89778 W-7 05/13/2022 11:00
05/11/2022 14:30Solids 89779 W-8 05/13/2022 11:00
05/11/2022 14:35Solids 89780 W-9 05/13/2022 11:00
05/11/2022 14:40Solids 89781 W-10 05/13/2022 11:00
05/11/2022 16:15Solids 89782 W-11 05/13/2022 11:00
05/11/2022 16:20Solids 89783 W-12 05/13/2022 11:00
05/11/2022 16:25Solids 89784 W-13 05/13/2022 11:00
05/11/2022 16:30Solids 89785 W-14 05/13/2022 11:00
05/12/2022 08:10Solids 89786 D-4 05/13/2022 11:00
05/12/2022 08:00Solids 89787 L-1 05/13/2022 11:00
05/12/2022 08:05Solids 89788 L-2 05/13/2022 11:00
05/12/2022 11:00Solids 89789 L-3 05/13/2022 11:00
05/12/2022 11:05Solids 89790 L-4 05/13/2022 11:00
05/12/2022 11:10Solids 89791 L-5 05/13/2022 11:00
Page 3 of 166
Report Number:
Sample Summary Table
Client Project Description:
22-133-0023
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/12/2022 13:30Solids 89792 L-6 05/13/2022 11:00
Page 4 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89765Stockpile 1
759 05/19/2022 22:498015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 106
4770 05/16/2022 18:258015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 23.6
12.2 05/20/2022 12:52SW-DRYWT Moisture %
V 89766Stock 2
100 05/19/2022 23:108015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.61
525 05/16/2022 17:578015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.50
17.1 05/19/2022 10:40SW-DRYWT Moisture %
V 89767Stock 3
445 05/20/2022 13:308015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 26.9
2080 05/16/2022 18:538015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 23.9
13.3 05/19/2022 10:40SW-DRYWT Moisture %
V 89768Stock 4
153 05/19/2022 23:538015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.80
1610 05/16/2022 19:218015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 25.8
19.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89769D-1
39.1 05/16/2022 11:538015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.55
0.049 05/16/2022 17:428260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 17:428260DBenzenemg/Kg - dry 0.0007
J0.003 05/16/2022 17:428260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 05/16/2022 17:428260Dn-Hexane mg/Kg - dry 0.0008
J0.006 05/16/2022 17:428260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/16/2022 17:428260DNaphthalenemg/Kg - dry 0.001
J0.001 05/16/2022 17:428260DToluenemg/Kg - dry 0.0008
J0.002 05/16/2022 17:428260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0008 05/16/2022 17:428260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 17:428260Do-Xylene mg/Kg - dry 0.0006
J0.001 05/16/2022 17:428260Dm,p-Xylene mg/Kg - dry 0.001
J0.003 05/16/2022 17:428260DXylene (Total)mg/Kg - dry 0.0006
18.7 05/18/2022 11:01SW-DRYWT Moisture %
V 89770D-2
J3.64 05/16/2022 12:218015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.72
J0.006 05/16/2022 18:108260DAcetonemg/Kg - dry 0.003
0.015 05/16/2022 18:108260DBenzenemg/Kg - dry 0.0008
Page 5 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89770D-2
0.016 05/16/2022 18:108260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.001
J0.005 05/16/2022 18:108260DEthylbenzenemg/Kg - dry 0.0008
J0.003 05/16/2022 18:108260DIsopropylbenzenemg/Kg - dry 0.0006
0.170 05/16/2022 18:108260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.004 05/16/2022 18:108260DNaphthalenemg/Kg - dry 0.001
J0.002 05/16/2022 18:108260Dn-Propylbenzene mg/Kg - dry 0.0007
0.012 05/16/2022 18:108260DToluenemg/Kg - dry 0.0009
J0.003 05/16/2022 18:108260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/16/2022 18:108260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 18:108260Do-Xylene mg/Kg - dry 0.0007
J0.005 05/16/2022 18:108260Dm,p-Xylene mg/Kg - dry 0.001
J0.006 05/16/2022 18:108260DXylene (Total)mg/Kg - dry 0.0007
23.8 05/18/2022 11:01SW-DRYWT Moisture %
V 89771D-3
J2.68 05/16/2022 12:498015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.28
J0.013 05/16/2022 18:388260DAcetonemg/Kg - dry 0.002
J0.001 05/16/2022 18:388260DBenzenemg/Kg - dry 0.0006
J0.002 05/16/2022 18:388260DCarbon Disulfide mg/Kg - dry 0.0007
J0.0009 05/16/2022 18:388260DEthylbenzenemg/Kg - dry 0.0006
J0.004 05/16/2022 18:388260Dn-Hexane mg/Kg - dry 0.0007
J0.001 05/16/2022 18:388260DNaphthalenemg/Kg - dry 0.001
J0.0007 05/16/2022 18:388260Dn-Propylbenzene mg/Kg - dry 0.0006
J0.003 05/16/2022 18:388260DToluenemg/Kg - dry 0.0007
J0.003 05/16/2022 18:388260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.002 05/16/2022 18:388260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
0.006 05/16/2022 18:388260Do-Xylene mg/Kg - dry 0.0006
J0.004 05/16/2022 18:388260Dm,p-Xylene mg/Kg - dry 0.001
J0.010 05/16/2022 18:388260DXylene (Total)mg/Kg - dry 0.0006
9.36 05/18/2022 11:01SW-DRYWT Moisture %
V 89772W-1
109 05/20/2022 00:148015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.46
J2.63 05/16/2022 13:178015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.43
0.023 05/16/2022 19:068260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 19:068260DBenzenemg/Kg - dry 0.0007
0.026 05/16/2022 19:068260DCarbon Disulfide mg/Kg - dry 0.0008
J0.002 05/16/2022 19:068260Dn-Hexane mg/Kg - dry 0.0008
Page 6 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89772W-1
J0.006 05/16/2022 19:068260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.001 05/16/2022 19:068260DToluenemg/Kg - dry 0.0008
J0.0008 05/16/2022 19:068260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0009 05/16/2022 19:068260Do-Xylene mg/Kg - dry 0.0006
J0.0009 05/16/2022 19:068260DXylene (Total)mg/Kg - dry 0.0006
14.8 05/18/2022 11:01SW-DRYWT Moisture %
V 89773W-2
32.7 05/20/2022 00:358015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.22
J2.46 05/16/2022 13:458015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.33
11.0 05/18/2022 11:01SW-DRYWT Moisture %
V 89774W-3
J0.011 05/16/2022 20:018260DAcetonemg/Kg - dry 0.002
J0.001 05/16/2022 20:018260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
12.3 05/18/2022 11:01SW-DRYWT Moisture %
V 89775W-4
J3.84 05/16/2022 14:418015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.47
J0.016 05/16/2022 20:288260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 20:288260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
16.2 05/18/2022 11:01SW-DRYWT Moisture %
V 89776W-5
13.0 05/20/2022 02:218015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.92
J0.017 05/16/2022 20:568260DAcetonemg/Kg - dry 0.003
J0.003 05/16/2022 20:568260DBenzenemg/Kg - dry 0.0007
J0.0007 05/16/2022 20:568260Dn-Butylbenzene mg/Kg - dry 0.0006
0.008 05/16/2022 20:568260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 05/16/2022 20:568260DEthylbenzenemg/Kg - dry 0.0007
J0.011 05/16/2022 20:568260Dn-Hexane mg/Kg - dry 0.0008
J0.006 05/16/2022 20:568260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.012 05/16/2022 20:568260DToluenemg/Kg - dry 0.0008
0.009 05/16/2022 20:568260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.005 05/16/2022 20:568260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.008 05/16/2022 20:568260Do-Xylene mg/Kg - dry 0.0006
0.018 05/16/2022 20:568260Dm,p-Xylene mg/Kg - dry 0.001
0.026 05/16/2022 20:568260DXylene (Total)mg/Kg - dry 0.0006
Page 7 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89776W-5
21.5 05/18/2022 11:01SW-DRYWT Moisture %
V 89777W-6
J9.06 05/20/2022 02:428015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.73
10.3 05/16/2022 16:058015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.55
18.9 05/18/2022 11:01SW-DRYWT Moisture %
V 89778W-7
23.2 05/20/2022 03:048015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.09
13.9 05/16/2022 16:338015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.71
0.035 05/16/2022 21:248260DAcetonemg/Kg - dry 0.003
J0.003 05/16/2022 21:248260DBenzenemg/Kg - dry 0.0008
J0.004 05/16/2022 21:248260DCarbon Disulfide mg/Kg - dry 0.0008
6.36 05/17/2022 23:578260DChloroformmg/Kg - dry 0.344
0.023 05/16/2022 21:248260DMethylene Chloride mg/Kg - dry 0.001
J0.002 05/16/2022 21:248260DTetrachloroethenemg/Kg - dry 0.001
J0.001 05/16/2022 21:248260DToluenemg/Kg - dry 0.0009
J0.006 05/16/2022 21:248260DTrichloroethenemg/Kg - dry 0.001
J0.0009 05/16/2022 21:248260Do-Xylene mg/Kg - dry 0.0007
J0.0009 05/16/2022 21:248260DXylene (Total)mg/Kg - dry 0.0007
23.6 05/19/2022 10:40SW-DRYWT Moisture %
V 89779W-8
J2.64 05/16/2022 17:008015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.33
0.044 05/17/2022 23:298260DAcetonemg/Kg - dry 0.002
J0.002 05/17/2022 23:298260DBenzenemg/Kg - dry 0.0007
J0.0008 05/17/2022 23:298260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0008
J0.002 05/17/2022 23:298260Dn-Hexane mg/Kg - dry 0.0007
11.1 05/19/2022 10:40SW-DRYWT Moisture %
V 89780W-9
15.9 05/20/2022 03:468015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.74
J4.68 05/16/2022 17:298015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.56
19.0 05/19/2022 10:40SW-DRYWT Moisture %
V 89781W-10
33.6 05/17/2022 15:248015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.71
J0.017 05/16/2022 22:198260DAcetonemg/Kg - dry 0.003
Page 8 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89781W-10
23.7 05/19/2022 10:40SW-DRYWT Moisture %
V 89782W-11
37.4 05/20/2022 04:298015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.88
63.5 05/17/2022 20:318015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.62
20.9 05/19/2022 10:40SW-DRYWT Moisture %
V 89783W-12
53.2 05/20/2022 04:508015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.80
75.7 05/17/2022 20:598015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.58
0.304 05/20/2022 13:218260DBenzenemg/Kg - dry 0.018
0.491 05/20/2022 13:218260Dn-Butylbenzene mg/Kg - dry 0.015
0.163 05/20/2022 13:218260Dsec-Butyl benzene mg/Kg - dry 0.017
3.30 05/20/2022 13:218260DEthylbenzenemg/Kg - dry 0.018
3.05 05/20/2022 13:218260Dn-Hexane mg/Kg - dry 0.020
0.339 05/20/2022 13:218260DIsopropylbenzenemg/Kg - dry 0.014
J0.067 05/20/2022 13:218260D4-Isopropyl toluene mg/Kg - dry 0.040
1.13 05/20/2022 13:218260DNaphthalenemg/Kg - dry 0.030
1.37 05/20/2022 13:218260Dn-Propylbenzene mg/Kg - dry 0.016
2.56 05/20/2022 13:218260DToluenemg/Kg - dry 0.020
7.11 05/20/2022 13:218260D1,2,4-Trimethylbenzene mg/Kg - dry 0.015
1.95 05/20/2022 13:218260D1,3,5-Trimethylbenzene mg/Kg - dry 0.016
3.39 05/20/2022 13:218260Do-Xylene mg/Kg - dry 0.015
11.1 05/20/2022 13:218260Dm,p-Xylene mg/Kg - dry 0.039
14.5 05/20/2022 13:218260DXylene (Total)mg/Kg - dry 0.015
19.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89784W-13
J5.87 05/20/2022 05:548015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.21
7.63 05/17/2022 15:528015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.41
J0.022 05/17/2022 21:388260DAcetonemg/Kg - dry 0.002
J0.005 05/17/2022 21:388260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
10.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89785W-14
115 05/20/2022 06:158015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.10
J5.10 05/17/2022 16:208015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.27
J0.008 05/20/2022 12:268260DAcetonemg/Kg - dry 0.002
Page 9 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89785W-14
J0.001 05/20/2022 12:268260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
8.78 05/19/2022 10:40SW-DRYWT Moisture %
V 89786D-4
J2.99 05/17/2022 16:488015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.81
J0.017 05/16/2022 22:478260DAcetonemg/Kg - dry 0.003
J0.002 05/16/2022 22:478260DBenzenemg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260DEthylbenzenemg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260DIsopropylbenzenemg/Kg - dry 0.0006
0.012 05/16/2022 22:478260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260Dn-Propylbenzene mg/Kg - dry 0.0007
0.008 05/16/2022 22:478260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 22:478260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 22:478260Do-Xylene mg/Kg - dry 0.0007
0.013 05/16/2022 22:478260Dm,p-Xylene mg/Kg - dry 0.001
J0.015 05/16/2022 22:478260DXylene (Total)mg/Kg - dry 0.0007
26.3 05/19/2022 10:40SW-DRYWT Moisture %
V 89787L-1
J2.51 05/17/2022 17:168015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.40
0.037 05/16/2022 23:158260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 23:158260DCarbon Disulfide mg/Kg - dry 0.0007
J0.007 05/16/2022 23:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.001 05/16/2022 23:158260DToluenemg/Kg - dry 0.0008
13.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89788L-2
J0.019 05/16/2022 23:428260DAcetonemg/Kg - dry 0.003
J0.005 05/16/2022 23:428260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/16/2022 23:428260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
22.4 05/19/2022 10:40SW-DRYWT Moisture %
V 89789L-3
25.9 05/17/2022 18:128015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.34
0.025 05/17/2022 13:478260DAcetonemg/Kg - dry 0.002
J0.001 05/17/2022 13:478260DBenzenemg/Kg - dry 0.0007
J0.001 05/17/2022 13:478260DEthylbenzenemg/Kg - dry 0.0007
J0.004 05/17/2022 13:478260Dn-Hexane mg/Kg - dry 0.0007
Page 10 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89789L-3
J0.004 05/17/2022 13:478260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.0006 05/17/2022 13:478260Dn-Propylbenzene mg/Kg - dry 0.0006
0.006 05/17/2022 13:478260DToluenemg/Kg - dry 0.0007
J0.002 05/17/2022 13:478260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/17/2022 13:478260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.002 05/17/2022 13:478260Do-Xylene mg/Kg - dry 0.0006
J0.005 05/17/2022 13:478260Dm,p-Xylene mg/Kg - dry 0.001
J0.007 05/17/2022 13:478260DXylene (Total)mg/Kg - dry 0.0006
11.7 05/19/2022 10:40SW-DRYWT Moisture %
V 89790L-4
J2.78 05/17/2022 18:408015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.78
J0.012 05/17/2022 14:158260DAcetonemg/Kg - dry 0.003
J0.003 05/17/2022 14:158260DBenzenemg/Kg - dry 0.0008
J0.003 05/17/2022 14:158260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.001
J0.001 05/17/2022 14:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
0.023 05/17/2022 14:158260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 05/17/2022 14:158260DToluenemg/Kg - dry 0.0009
J0.001 05/17/2022 14:158260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/17/2022 14:158260Do-Xylene mg/Kg - dry 0.0007
J0.001 05/17/2022 14:158260DXylene (Total)mg/Kg - dry 0.0007
25.6 05/19/2022 10:40SW-DRYWT Moisture %
V 89791L-5
J0.005 05/17/2022 14:438260DAcetonemg/Kg - dry 0.003
J0.002 05/17/2022 14:438260DBenzenemg/Kg - dry 0.0007
J0.001 05/17/2022 14:438260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0009
J0.0009 05/17/2022 14:438260DEthylbenzenemg/Kg - dry 0.0007
J0.002 05/17/2022 14:438260Dn-Hexane mg/Kg - dry 0.0008
0.034 05/17/2022 14:438260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
0.008 05/17/2022 14:438260DToluenemg/Kg - dry 0.0008
J0.0010 05/17/2022 14:438260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/17/2022 14:438260Do-Xylene mg/Kg - dry 0.0006
J0.002 05/17/2022 14:438260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 05/17/2022 14:438260DXylene (Total)mg/Kg - dry 0.0006
20.0 05/19/2022 10:40SW-DRYWT Moisture %
Page 11 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89792L-6
0.030 05/17/2022 15:108260DAcetonemg/Kg - dry 0.003
0.021 05/17/2022 15:108260DBenzenemg/Kg - dry 0.0008
J0.001 05/17/2022 15:108260DChloroformmg/Kg - dry 0.001
J0.002 05/17/2022 15:108260Dn-Hexane mg/Kg - dry 0.0009
0.010 05/17/2022 15:108260DToluenemg/Kg - dry 0.0009
J0.0008 05/17/2022 15:108260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0009 05/17/2022 15:108260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/17/2022 15:108260Do-Xylene mg/Kg - dry 0.0007
J0.003 05/17/2022 15:108260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 05/17/2022 15:108260DXylene (Total)mg/Kg - dry 0.0007
24.4 05/19/2022 10:40SW-DRYWT Moisture %
Page 12 of 166

Client: ATC Group Services, LLC - Raleigh, NC CASE NARRATIVE
Project: Circle K 2720104 Lab Report Number: 22-133-0023
Date: 5/23/2022
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 89767 (Stock 3) QC Batch No: V18982/V18830
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO
Sample 89772 (W-1) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18714/V18713 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 89773 (W-2)
Analyte: a,a,a-Trifluorotoluene QC Batch No: V18714/V18713
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits. Sample 89774 (W-3) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18714/V18713 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Chloroethane QC Batch No: V18810/V18747
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Chloroethane QC Batch No: V18871/V18747 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 13 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stockpile 1
89765 Matrix:
5/10/2022 13:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.2 %Moisture 1 05/20/22 12:52 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stockpile 1
89765 Matrix:
5/10/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
759 mg/Kg - dry 106 228Diesel Range Organics (C10-C28)20 05/19/22 22:49 V18982JLK
8015C DROSurrogate: OTP Surrogate 82.0 Limits: 31-123%05/19/22 22:4920 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
4770 mg/Kg - dry 23.6 56.9Gasoline Range Organics (C6-C10)500 05/16/22 18:25 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 124 Limits: 50-137%05/16/22 18:25500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 2
89766 Matrix:
5/10/2022 10:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.1 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 2
89766 Matrix:
5/10/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
100 mg/Kg - dry 5.61 12.1Diesel Range Organics (C10-C28)1 05/19/22 23:10 V18982JLK
8015C DROSurrogate: OTP Surrogate 83.5 Limits: 31-123%05/19/22 23:101 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
525 mg/Kg - dry 2.50 6.03Gasoline Range Organics (C6-C10)50 05/16/22 17:57 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 77.0 Limits: 50-137%05/16/22 17:5750 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 3
89767 Matrix:
5/10/2022 10:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.3 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 3
89767 Matrix:
5/10/2022 10:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
445 mg/Kg - dry 26.9 57.7Diesel Range Organics (C10-C28)5 05/20/22 13:30 V18982JLK
8015C DROSurrogate: OTP Surrogate 75.9 Limits: 31-123%05/20/22 13:305 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2080 mg/Kg - dry 23.9 57.7Gasoline Range Organics (C6-C10)500 05/16/22 18:53 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 125 Limits: 50-137%05/16/22 18:53500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 4
89768 Matrix:
5/10/2022 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 4
89768 Matrix:
5/10/2022 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
153 mg/Kg - dry 5.80 12.5Diesel Range Organics (C10-C28)1 05/19/22 23:53 V18982JLK
8015C DROSurrogate: OTP Surrogate 92.5 Limits: 31-123%05/19/22 23:531 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
1610 mg/Kg - dry 25.8 62.3Gasoline Range Organics (C6-C10)500 05/16/22 19:21 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 85.4 Limits: 50-137%05/16/22 19:21500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.7 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
39.1 mg/Kg - dry 2.55 6.15Gasoline Range Organics (C6-C10)50 05/16/22 11:53 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 134 Limits: 50-137%05/16/22 11:5350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.049 mg/Kg - dry 0.002 0.024Acetone 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 17:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/16/22 17:42 V18748TBL
0.003 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 17:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 17:42 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 17:42 V18748TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 17:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.006Toluene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 17:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 17:42 V18748TBL
0.0008 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 17:42 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 17:42 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 17:421 TBL V18748
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/16/22 17:421 TBL V18748
Surrogate: Toluene-d8 86.1 Limits: 76-129%05/16/22 17:421 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.8 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
3.64 J mg/Kg - dry 2.72 6.56Gasoline Range Organics (C6-C10)50 05/16/22 12:21 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/16/22 12:2150 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.006 J mg/Kg - dry 0.003 0.026Acetone 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 18:10 V18748TBL
0.015 mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 18:10 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 18:10 V18748TBL
0.016 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 18:10 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 18:10 V18748TBL
0.005 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 18:10 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 18:10 V18748TBL
0.170 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 18:10 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 18:10 V18748TBL
0.004 J mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 18:10 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 18:10 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 18:10 V18748TBL
0.012 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 18:10 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 18:10 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 18:10 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 18:10 V18748TBL
0.005 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 18:10 V18748TBL
0.006 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 18:10 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 18:101 TBL V18748
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/16/22 18:101 TBL V18748
Surrogate: Toluene-d8 88.7 Limits: 76-129%05/16/22 18:101 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.36 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.68 J mg/Kg - dry 2.28 5.52Gasoline Range Organics (C6-C10)50 05/16/22 12:49 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 134 Limits: 50-137%05/16/22 12:4950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.013 J mg/Kg - dry 0.002 0.022Acetone 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/16/22 18:38 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.005Benzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/16/22 18:38 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/16/22 18:38 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 18:38 V18748TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/16/22 18:38 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 18:38 V18748TBL
0.004 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 18:38 V18748TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 18:38 V18748TBL
0.001 J mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 18:38 V18748TBL
0.0007 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 18:38 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 05/16/22 18:38 V18748TBL
0.003 J mg/Kg - dry 0.0007 0.005Toluene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 18:38 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 18:38 V18748TBL
0.003 J mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/16/22 18:38 V18748TBL
0.002 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/16/22 18:38 V18748TBL
0.006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 18:38 V18748TBL
0.004 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 18:38 V18748TBL
0.010 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 18:38 V18748
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/16/22 18:381 TBL V18748
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/16/22 18:381 TBL V18748
Surrogate: Toluene-d8 88.2 Limits: 76-129%05/16/22 18:381 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.8 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
109 mg/Kg - dry 5.46 11.7Diesel Range Organics (C10-C28)1 05/20/22 00:14 V18982JLK
8015C DROSurrogate: OTP Surrogate 96.2 Limits: 31-123%05/20/22 00:141 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.63 J mg/Kg - dry 2.43 5.87Gasoline Range Organics (C6-C10)50 05/16/22 13:17 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 155 *Limits: 50-137%05/16/22 13:1750 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.023 mg/Kg - dry 0.002 0.023
Acetone 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 19:06 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 19:06 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 19:06 V18748TBL
0.026 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005
Dibromomethane 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 19:06 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 19:06 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 19:06 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 19:06 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 19:06 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,1,2-Trichloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 19:06 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 19:06 V18748TBL
0.0008 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 19:06 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 19:06 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 19:06 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 19:061 TBL V18748
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/16/22 19:061 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 19:061 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-2
89773 Matrix:
5/11/2022 10:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.0 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-2
89773 Matrix:
5/11/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
32.7 mg/Kg - dry 5.22 11.2Diesel Range Organics (C10-C28)1 05/20/22 00:35 V18982JLK
8015C DROSurrogate: OTP Surrogate 87.2 Limits: 31-123%05/20/22 00:351 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.46 J mg/Kg - dry 2.33 5.62Gasoline Range Organics (C6-C10)50 05/16/22 13:45 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 157 *Limits: 50-137%05/16/22 13:4550 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.3 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.30 mg/Kg - dry 5.30 11.4Diesel Range Organics (C10-C28)1 05/20/22 01:39 V18982JLK
8015C DROSurrogate: OTP Surrogate 87.3 Limits: 31-123%05/20/22 01:391 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
<2.36 mg/Kg - dry 2.36 5.70Gasoline Range Organics (C6-C10)50 05/16/22 14:13 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 153 *Limits: 50-137%05/16/22 14:1350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.011 J
mg/Kg - dry 0.002 0.022
Acetone 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 20:01 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 20:01 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 20:01 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 20:01 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 20:01 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 20:011 TBL V18748
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/16/22 20:011 TBL V18748
Surrogate: Toluene-d8 87.7 Limits: 76-129%05/16/22 20:011 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.2 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.55 mg/Kg - dry 5.55 11.9Diesel Range Organics (C10-C28)1 05/20/22 02:00 V18982JLK
8015C DROSurrogate: OTP Surrogate 91.8 Limits: 31-123%05/20/22 02:001 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
3.84 J mg/Kg - dry 2.47 5.97Gasoline Range Organics (C6-C10)50 05/16/22 14:41 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 120 Limits: 50-137%05/16/22 14:4150 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.016 J
mg/Kg - dry 0.002 0.023
Acetone 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 20:28 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005
Dibromomethane 1 05/16/22 20:28 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005
trans-1,3-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 20:28 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 20:28 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 20:28 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,1,2-Trichloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 20:28 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 20:28 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 20:281 TBL V18748
Surrogate: Dibromofluoromethane 108 Limits: 84-123%05/16/22 20:281 TBL V18748
Surrogate: Toluene-d8 88.1 Limits: 76-129%05/16/22 20:281 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.5 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
13.0 mg/Kg - dry 5.92 12.7Diesel Range Organics (C10-C28)1 05/20/22 02:21 V18982JLK
8015C DROSurrogate: OTP Surrogate 98.5 Limits: 31-123%05/20/22 02:211 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
<2.64 mg/Kg - dry 2.64 6.37Gasoline Range Organics (C6-C10)50 05/16/22 15:09 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 122 Limits: 50-137%05/16/22 15:0950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J
mg/Kg - dry 0.003 0.025
Acetone 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/16/22 20:56 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/16/22 20:56 V18748TBL
0.003 J mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.0007 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/16/22 20:56 V18748TBL
0.008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/16/22 20:56 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 20:56 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 20:56 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/16/22 20:56 V18748TBL
0.011 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 20:56 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 20:56 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 20:56 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 20:56 V18748TBL
0.012 mg/Kg - dry 0.0008 0.006Toluene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 20:56 V18748TBL
0.009 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 20:56 V18748TBL
0.005 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 20:56 V18748TBL
0.008 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 20:56 V18748TBL
0.018 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 20:56 V18748TBL
0.026 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 20:56 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 20:561 TBL V18748
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/16/22 20:561 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 20:561 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 58 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-6
89777 Matrix:
5/11/2022 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.9 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 59 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-6
89777 Matrix:
5/11/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
9.06 J mg/Kg - dry 5.73 12.3Diesel Range Organics (C10-C28)1 05/20/22 02:42 V18982JLK
8015C DROSurrogate: OTP Surrogate 88.0 Limits: 31-123%05/20/22 02:421 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
10.3 mg/Kg - dry 2.55 6.17Gasoline Range Organics (C6-C10)50 05/16/22 16:05 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 136 Limits: 50-137%05/16/22 16:0550 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 60 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.6 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 61 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
23.2 mg/Kg - dry 6.09 13.1Diesel Range Organics (C10-C28)1 05/20/22 03:04 V18982JLK
8015C DROSurrogate: OTP Surrogate 91.0 Limits: 31-123%05/20/22 03:041 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
13.9 mg/Kg - dry 2.71 6.54Gasoline Range Organics (C6-C10)50 05/16/22 16:33 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 127 Limits: 50-137%05/16/22 16:3350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
0.035 mg/Kg - dry 0.003 0.026
Acetone 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 21:24 V18748TBL
0.003 J mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 62 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/16/22 21:24 V18748TBL
0.004 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 21:24 V18748TBL
6.36 mg/Kg - dry 0.344 1.64
Chloroform 500 05/17/22 23:57 V18871TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 21:24 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 21:24 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 63 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 21:24 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 21:24 V18748TBL
0.023 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 64 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 21:24 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 21:24 V18748TBL
0.002 J mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 21:24 V18748TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 21:24 V18748TBL
0.006 J mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 21:24 V18748TBL
0.0009 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 65 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
0.0009 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 21:24 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 21:241 TBL V18748
Surrogate: Dibromofluoromethane 112 Limits: 84-123%05/16/22 21:241 TBL V18748
Surrogate: Toluene-d8 87.1 Limits: 76-129%05/16/22 21:241 TBL V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 23:57500 TBL V18871
Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/17/22 23:57500 TBL V18871
Surrogate: Toluene-d8 88.9 Limits: 76-129%05/17/22 23:57500 TBL V18871
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 66 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.1 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 67 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.23 mg/Kg - dry 5.23 11.2Diesel Range Organics (C10-C28)1 05/20/22 03:25 V18982JLK
8015C DROSurrogate: OTP Surrogate 95.5 Limits: 31-123%05/20/22 03:251 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.64 J mg/Kg - dry 2.33 5.62Gasoline Range Organics (C6-C10)50 05/16/22 17:00 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 126 Limits: 50-137%05/16/22 17:0050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.044 mg/Kg - dry 0.002 0.022
Acetone 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 23:29 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/17/22 23:29 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 68 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 23:29 V18810TBL
0.0008 J mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 23:29 V18810TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 69 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 23:29 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 23:29 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 70 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 23:29 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 23:29 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 23:291 TBL V18810
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/17/22 23:291 TBL V18810
Surrogate: Toluene-d8 87.2 Limits: 76-129%05/17/22 23:291 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 71 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-9
89780 Matrix:
5/11/2022 14:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.0 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 72 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-9
89780 Matrix:
5/11/2022 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
15.9 mg/Kg - dry 5.74 12.3Diesel Range Organics (C10-C28)1 05/20/22 03:46 V18982JLK
8015C DROSurrogate: OTP Surrogate 84.2 Limits: 31-123%05/20/22 03:461 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
4.68 J mg/Kg - dry 2.56 6.17Gasoline Range Organics (C6-C10)50 05/16/22 17:29 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 122 Limits: 50-137%05/16/22 17:2950 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 73 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.7 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 74 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<6.09 mg/Kg - dry 6.09 13.1Diesel Range Organics (C10-C28)1 05/20/22 04:07 V18982JLK
8015C DROSurrogate: OTP Surrogate 89.5 Limits: 31-123%05/20/22 04:071 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
33.6 mg/Kg - dry 2.71 6.55Gasoline Range Organics (C6-C10)50 05/17/22 15:24 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 114 Limits: 50-137%05/17/22 15:2450 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J
mg/Kg - dry 0.003 0.026
Acetone 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 75 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 22:19 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 22:19 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 76 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 22:19 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 77 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 22:19 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 22:19 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 22:191 TBL V18748
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/16/22 22:191 TBL V18748
Surrogate: Toluene-d8 85.3 Limits: 76-129%05/16/22 22:191 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 78 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-11
89782 Matrix:
5/11/2022 16:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.9 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 79 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-11
89782 Matrix:
5/11/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
37.4 mg/Kg - dry 5.88 12.6Diesel Range Organics (C10-C28)1 05/20/22 04:29 V18982JLK
8015C DROSurrogate: OTP Surrogate 84.3 Limits: 31-123%05/20/22 04:291 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
63.5 mg/Kg - dry 2.62 6.32Gasoline Range Organics (C6-C10)50 05/17/22 20:31 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 110 Limits: 50-137%05/17/22 20:3150 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 80 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 81 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
53.2 mg/Kg - dry 5.80 12.5Diesel Range Organics (C10-C28)1 05/20/22 04:50 V18982JLK
8015C DROSurrogate: OTP Surrogate 94.0 Limits: 31-123%05/20/22 04:501 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
75.7 mg/Kg - dry 2.58 6.23Gasoline Range Organics (C6-C10)50 05/17/22 20:59 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 112 Limits: 50-137%05/17/22 20:5950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.074 mg/Kg - dry 0.074 0.623
Acetone 50 05/20/22 13:21 V18989TBL
<0.037 mg/Kg - dry 0.037 0.623Acrolein 50 05/20/22 13:21 V18989TBL
<0.023 mg/Kg - dry 0.023 0.623Acrylonitrile 50 05/20/22 13:21 V18989TBL
0.304 mg/Kg - dry 0.018 0.155Benzene 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.155Bromobenzene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155Bromochloromethane 50 05/20/22 13:21 V18989TBL
<0.037 mg/Kg - dry 0.037 0.155Bromodichloromethane 50 05/20/22 13:21 V18989TBL
<0.031 mg/Kg - dry 0.031 0.155
Bromoform 50 05/20/22 13:21 V18989TBL
<0.056 mg/Kg - dry 0.056 0.311Bromomethane 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 82 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
0.491 mg/Kg - dry 0.015 0.155n-Butylbenzene 50 05/20/22 13:21 V18989TBL
0.163 mg/Kg - dry 0.017 0.155sec-Butyl benzene 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.155tert-Butyl benzene 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.155Carbon Disulfide 50 05/20/22 13:21 V18989TBL
<0.049 mg/Kg - dry 0.049 0.155Carbon Tetrachloride 50 05/20/22 13:21 V18989TBL
<0.020 mg/Kg - dry 0.020 0.155Chlorobenzene 50 05/20/22 13:21 V18989TBL
<0.027 mg/Kg - dry 0.027 0.155Chlorodibromomethane 50 05/20/22 13:21 V18989TBL
<0.027 mg/Kg - dry 0.027 0.311Chloroethane 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.155
Chloroform 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.311Chloromethane 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.1552-Chlorotoluene 50 05/20/22 13:21 V18989TBL
<0.012 mg/Kg - dry 0.012 0.1554-Chlorotoluene 50 05/20/22 13:21 V18989TBL
<0.022 mg/Kg - dry 0.022 0.155Di-Isopropyl Ether (DIPE)50 05/20/22 13:21 V18989TBL
<0.013 mg/Kg - dry 0.013 0.3111,2-Dibromo-3-Chloropropane 50 05/20/22 13:21 V18989TBL
<0.018 mg/Kg - dry 0.018 0.1551,2-Dibromoethane 50 05/20/22 13:21 V18989TBL
<0.030 mg/Kg - dry 0.030 0.155
Dibromomethane 50 05/20/22 13:21 V18989TBL
<0.009 mg/Kg - dry 0.009 0.1551,2-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.011 mg/Kg - dry 0.011 0.1551,3-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.018 mg/Kg - dry 0.018 0.1551,4-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.041 mg/Kg - dry 0.041 0.311Dichlorodifluoromethane 50 05/20/22 13:21 V18989TBL
<0.025 mg/Kg - dry 0.025 0.1551,1-Dichloroethane 50 05/20/22 13:21 V18989TBL
<0.043 mg/Kg - dry 0.043 0.1551,2-Dichloroethane 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 83 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.022 mg/Kg - dry 0.022 0.1551,1-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155cis-1,2-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.155trans-1,2-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.013 mg/Kg - dry 0.013 0.1551,2-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.017 mg/Kg - dry 0.017 0.1551,3-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.039 mg/Kg - dry 0.039 0.1552,2-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.023 mg/Kg - dry 0.023 0.1551,1-Dichloropropene 50 05/20/22 13:21 V18989TBL
<0.016 mg/Kg - dry 0.016 0.155cis-1,3-Dichloropropene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155
trans-1,3-Dichloropropene 50 05/20/22 13:21 V18989TBL
3.30 mg/Kg - dry 0.018 0.155Ethylbenzene 50 05/20/22 13:21 V18989TBL
<0.025 mg/Kg - dry 0.025 3.12Ethyl Tertiary Butyl Ether (ETBE)50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.311Hexachlorobutadiene 50 05/20/22 13:21 V18989TBL
3.05 mg/Kg - dry 0.020 0.311n-Hexane 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.6232-Hexanone 50 05/20/22 13:21 V18989TBL
0.339 mg/Kg - dry 0.014 0.155Isopropylbenzene 50 05/20/22 13:21 V18989TBL
0.067 J
mg/Kg - dry 0.040 0.155
4-Isopropyl toluene 50 05/20/22 13:21 V18989TBL
<0.020 mg/Kg - dry 0.020 0.623Methyl Ethyl Ketone (MEK)50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.155Methyl tert-butyl ether (MTBE)50 05/20/22 13:21 V18989TBL
<0.467 mg/Kg - dry 0.467 0.6234-Methyl-2-Pentanone 50 05/20/22 13:21 V18989TBL
<0.045 mg/Kg - dry 0.045 0.155Methylene Chloride 50 05/20/22 13:21 V18989TBL
1.13 mg/Kg - dry 0.030 0.311Naphthalene 50 05/20/22 13:21 V18989TBL
1.37 mg/Kg - dry 0.016 0.155n-Propylbenzene 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 84 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.044 mg/Kg - dry 0.044 0.155Styrene 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.1551,1,1,2-Tetrachloroethane 50 05/20/22 13:21 V18989TBL
<0.009 mg/Kg - dry 0.009 0.1551,1,2,2-Tetrachloroethane 50 05/20/22 13:21 V18989TBL
<0.028 mg/Kg - dry 0.028 0.155Tetrachloroethene 50 05/20/22 13:21 V18989TBL
2.56 mg/Kg - dry 0.020 0.155Toluene 50 05/20/22 13:21 V18989TBL
<0.016 mg/Kg - dry 0.016 0.3111,2,3-Trichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.3111,2,4-Trichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.044 mg/Kg - dry 0.044 0.1551,1,1-Trichloroethane 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.155
1,1,2-Trichloroethane 50 05/20/22 13:21 V18989TBL
<0.028 mg/Kg - dry 0.028 0.155Trichloroethene 50 05/20/22 13:21 V18989TBL
<0.065 mg/Kg - dry 0.065 0.311Trichlorofluoromethane 50 05/20/22 13:21 V18989TBL
<0.022 mg/Kg - dry 0.022 0.1551,2,3-Trichloropropane 50 05/20/22 13:21 V18989TBL
7.11 mg/Kg - dry 0.015 0.1551,2,4-Trimethylbenzene 50 05/20/22 13:21 V18989TBL
1.95 mg/Kg - dry 0.016 0.1551,3,5-Trimethylbenzene 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.311Vinyl Acetate 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.311
Vinyl Chloride 50 05/20/22 13:21 V18989TBL
3.39 mg/Kg - dry 0.015 0.155o-Xylene 50 05/20/22 13:21 V18989TBL
11.1 mg/Kg - dry 0.039 0.311m,p-Xylene 50 05/20/22 13:21 V18989TBL
14.5 mg/Kg - dry 0.015 0.155Xylene (Total)50 05/20/22 13:21 V18989
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%05/20/22 13:2150 TBL V18989
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%05/20/22 13:2150 TBL V18989
Surrogate: Toluene-d8 86.6 Limits: 76-129%05/20/22 13:2150 TBL V18989
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 85 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 86 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
5.87 J mg/Kg - dry 5.21 11.2Diesel Range Organics (C10-C28)1 05/20/22 05:54 V18982JLK
8015C DROSurrogate: OTP Surrogate 102 Limits: 31-123%05/20/22 05:541 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
7.63 mg/Kg - dry 2.41 5.83Gasoline Range Organics (C6-C10)50 05/17/22 15:52 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/17/22 15:5250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.022 J
mg/Kg - dry 0.002 0.022
Acetone 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/17/22 21:38 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 87 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/17/22 21:38 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 21:38 V18810TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 88 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 21:38 V18810TBL
0.005 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 21:38 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 89 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 21:38 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 21:38 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 21:381 TBL V18810
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/17/22 21:381 TBL V18810
Surrogate: Toluene-d8 86.7 Limits: 76-129%05/17/22 21:381 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 90 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.78 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 91 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
115 mg/Kg - dry 5.10 11.0Diesel Range Organics (C10-C28)1 05/20/22 06:15 V18982JLK
8015C DROSurrogate: OTP Surrogate 106 Limits: 31-123%05/20/22 06:151 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
5.10 J mg/Kg - dry 2.27 5.48Gasoline Range Organics (C6-C10)50 05/17/22 16:20 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/17/22 16:2050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
0.008 J
mg/Kg - dry 0.002 0.021
Acetone 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 92 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/20/22 12:26 V18987TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 93 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/20/22 12:26 V18987TBL
0.001 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/20/22 12:26 V18987TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 94 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/20/22 12:26 V18987TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.010
Vinyl Chloride 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 05/20/22 12:26 V18987
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%05/20/22 12:261 TBL V18987
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/20/22 12:261 TBL V18987
Surrogate: Toluene-d8 85.0 Limits: 76-129%05/20/22 12:261 TBL V18987
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 95 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.3 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 96 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.99 J mg/Kg - dry 2.81 6.78Gasoline Range Organics (C6-C10)50 05/17/22 16:48 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 116 Limits: 50-137%05/17/22 16:4850 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J mg/Kg - dry 0.003 0.027Acetone 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 05/16/22 22:47 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 97 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 22:47 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 05/16/22 22:47 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 98 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 05/16/22 22:47 V18748TBL
0.012 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 22:47 V18748TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 22:47 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 99 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/16/22 22:47 V18748TBL
0.008 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.013
Vinyl Chloride 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 22:47 V18748TBL
0.013 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 22:47 V18748TBL
0.015 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 22:47 V18748
Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%05/16/22 22:471 TBL V18748
Surrogate: Dibromofluoromethane 105 Limits: 84-123%05/16/22 22:471 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 22:471 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 100 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 101 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.51 J mg/Kg - dry 2.40 5.80Gasoline Range Organics (C6-C10)50 05/17/22 17:16 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 128 Limits: 50-137%05/17/22 17:1650 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.037 mg/Kg - dry 0.002 0.023Acetone 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/16/22 23:15 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/16/22 23:15 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 102 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 23:15 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 103 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 23:15 V18748TBL
0.007 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 23:15 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 23:15 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 104 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 23:15 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 23:15 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 23:151 TBL V18748
Surrogate: Dibromofluoromethane 99.8 Limits: 84-123%05/16/22 23:151 TBL V18748
Surrogate: Toluene-d8 85.9 Limits: 76-129%05/16/22 23:151 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 105 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.4 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 106 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.67 mg/Kg - dry 2.67 6.44Gasoline Range Organics (C6-C10)50 05/17/22 17:44 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 115 Limits: 50-137%05/17/22 17:4450 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.019 J mg/Kg - dry 0.003 0.025Acetone 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/16/22 23:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 107 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 23:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 23:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 108 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 23:42 V18748TBL
0.005 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/16/22 23:42 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 23:42 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 23:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 109 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 23:42 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 23:421 TBL V18748
Surrogate: Dibromofluoromethane 100 Limits: 84-123%05/16/22 23:421 TBL V18748
Surrogate: Toluene-d8 91.1 Limits: 76-129%05/16/22 23:421 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 110 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.7 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 111 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
25.9 mg/Kg - dry 2.34 5.66Gasoline Range Organics (C6-C10)50 05/17/22 18:12 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 133 Limits: 50-137%05/17/22 18:1250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.025 mg/Kg - dry 0.002 0.022Acetone 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/17/22 13:47 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 112 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 113 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 13:47 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 13:47 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 13:47 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 13:47 V18810TBL
0.0006 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 13:47 V18810TBL
0.006 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 114 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 13:47 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 13:47 V18810TBL
0.002 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 13:47 V18810TBL
0.002 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 13:47 V18810TBL
0.005 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 13:47 V18810TBL
0.007 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 13:47 V18810
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/17/22 13:471 TBL V18810
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/17/22 13:471 TBL V18810
Surrogate: Toluene-d8 89.0 Limits: 76-129%05/17/22 13:471 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 115 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.6 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 116 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.78 J mg/Kg - dry 2.78 6.72Gasoline Range Organics (C6-C10)50 05/17/22 18:40 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%05/17/22 18:4050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.012 J mg/Kg - dry 0.003 0.026Acetone 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 05/17/22 14:15 V18810TBL
0.003 J mg/Kg - dry 0.0008 0.006Benzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 117 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/17/22 14:15 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 14:15 V18810TBL
0.003 J mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 05/17/22 14:15 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 14:15 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 118 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/17/22 14:15 V18810TBL
0.023 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 14:15 V18810TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 14:15 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 119 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/17/22 14:15 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/17/22 14:15 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 14:151 TBL V18810
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/17/22 14:151 TBL V18810
Surrogate: Toluene-d8 87.8 Limits: 76-129%05/17/22 14:151 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 120 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 121 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.59 mg/Kg - dry 2.59 6.25Gasoline Range Organics (C6-C10)50 05/17/22 19:08 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%05/17/22 19:0850 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.005 J mg/Kg - dry 0.003 0.025Acetone 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.006Benzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 14:43 V18810TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 122 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/17/22 14:43 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 14:43 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/17/22 14:43 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 123 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 14:43 V18810TBL
0.0009 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/17/22 14:43 V18810TBL
0.034 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 14:43 V18810TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 14:43 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 14:43 V18810TBL
0.008 mg/Kg - dry 0.0008 0.006Toluene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 124 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 14:43 V18810TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/17/22 14:43 V18810TBL
0.0010 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/17/22 14:43 V18810TBL
0.001 J mg/Kg - dry 0.0006 0.006o-Xylene 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/17/22 14:43 V18810TBL
0.004 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/17/22 14:43 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 14:431 TBL V18810
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/17/22 14:431 TBL V18810
Surrogate: Toluene-d8 87.9 Limits: 76-129%05/17/22 14:431 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 125 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.4 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 126 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.74 mg/Kg - dry 2.74 6.61Gasoline Range Organics (C6-C10)50 05/17/22 19:36 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 104 Limits: 50-137%05/17/22 19:3650 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.030 mg/Kg - dry 0.003 0.026Acetone 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/17/22 15:10 V18810TBL
0.021 mg/Kg - dry 0.0008 0.006Benzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/17/22 15:10 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 127 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/17/22 15:10 V18810TBL
0.001 J mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/17/22 15:10 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/17/22 15:10 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 128 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/17/22 15:10 V18810TBL
0.002 J mg/Kg - dry 0.0009 0.013n-Hexane 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 15:10 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 15:10 V18810TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 15:10 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 15:10 V18810TBL
0.010 mg/Kg - dry 0.0009 0.006Toluene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 129 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/17/22 15:10 V18810TBL
0.0008 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/17/22 15:10 V18810TBL
0.0009 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/17/22 15:10 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/17/22 15:10 V18810TBL
0.003 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/17/22 15:10 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/17/22 15:10 V18810
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%05/17/22 15:101 TBL V18810
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/17/22 15:101 TBL V18810
Surrogate: Toluene-d8 89.7 Limits: 76-129%05/17/22 15:101 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 130 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V18982QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18830
Associated Lab Samples: 89765, 89766, 89767, 89768, 89772, 89773, 89774, 89775, 89776, 89777, 89778, 89779, 89780, 89781, 89782,
89783, 89784, 89785
LRB-V18830 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/19/22 21:2410.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
05/19/22 21:24OTP Surrogate (S)96.2 31-123
LCS-V18830Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10469.566.7mg/KgDiesel Range Organics (C10-C28)46-126
84.9OTP Surrogate (S)31-123
V 89767-MS-V18830 V 89767-MSD-V18830Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
291 -140*28266.666.6386mg/KgDiesel Range Organics (C10-C28)-140*50-117 3.1 24
70.9OTP Surrogate (S)67.3 31-123
Page 1 of 31* QC Fail Date:05/23/2022 04:56 PM
Page 131 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18714QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18713
Associated Lab Samples: 89765, 89766, 89767, 89768, 89769, 89770, 89771, 89772, 89773, 89774, 89775, 89776, 89777, 89778, 89779,
89780
LRB-V18713 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 10:305.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/16/22 10:30a,a,a-Trifluorotoluene (S)105 50-137
LCS-V18713Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.249.150.0mg/KgGasoline Range Organics (C6-C10)41-138
119a,a,a-Trifluorotoluene (S)50-137
V 89612-MS-V18713 V 89612-MSD-V18713Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
59.2 11855.550.050.02.60mg/KgGasoline Range Organics (C6-C10)111 41-138 6.4 34
126a,a,a-Trifluorotoluene (S)121 50-137
Page 2 of 31Date:05/23/2022 04:56 PM
Page 132 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18785QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18784
Associated Lab Samples: 89781, 89782, 89783, 89784, 89785, 89786, 89787, 89788, 89789, 89790, 89791, 89792
LRB-V18784 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 14:565.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/17/22 14:56a,a,a-Trifluorotoluene (S)126 50-137
LCS-V18784Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10853.950.0mg/KgGasoline Range Organics (C6-C10)41-138
121a,a,a-Trifluorotoluene (S)50-137
V 89781-MS-V18784 V 89781-MSD-V18784Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
55.2 59.254.950.050.025.6mg/KgGasoline Range Organics (C6-C10)58.6 41-138 0.5 34
135a,a,a-Trifluorotoluene (S)135 50-137
Page 3 of 31Date:05/23/2022 04:56 PM
Page 133 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0200.002<0.002mg/KgAcetone
05/16/22 12:100.0200.001<0.001mg/KgAcrolein
05/16/22 12:100.0200.0008<0.0008mg/KgAcrylonitrile
05/16/22 12:100.0050.0006<0.0006mg/KgBenzene
05/16/22 12:100.0050.0005<0.0005mg/KgBromobenzene
05/16/22 12:100.0050.0008<0.0008mg/KgBromochloromethane
05/16/22 12:100.0050.001<0.001mg/KgBromodichloromethane
05/16/22 12:100.0050.001<0.001mg/KgBromoform
05/16/22 12:100.0100.001<0.001mg/KgBromomethane
05/16/22 12:100.0050.0005<0.0005mg/Kgn-Butylbenzene
05/16/22 12:100.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/16/22 12:100.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/16/22 12:100.0050.0006<0.0006mg/KgCarbon Disulfide
05/16/22 12:100.0050.001<0.001mg/KgCarbon Tetrachloride
05/16/22 12:100.0050.0007<0.0007mg/KgChlorobenzene
05/16/22 12:100.0050.0009<0.0009mg/KgChlorodibromomethane
05/16/22 12:100.0100.0009<0.0009mg/KgChloroethane
05/16/22 12:100.0050.001<0.001mg/KgChloroform
05/16/22 12:100.0100.0006<0.0006mg/KgChloromethane
05/16/22 12:100.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/16/22 12:100.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/16/22 12:100.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/16/22 12:100.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/16/22 12:100.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/16/22 12:100.0050.0006<0.0006mg/KgDibromomethane
05/16/22 12:100.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/16/22 12:100.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 31Date:05/23/2022 04:56 PM
Page 134 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/16/22 12:100.0100.001<0.001mg/KgDichlorodifluoromethane
05/16/22 12:100.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/16/22 12:100.0050.001<0.001mg/Kg1,2-Dichloroethane
05/16/22 12:100.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/16/22 12:100.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/16/22 12:100.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/16/22 12:100.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/16/22 12:100.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/16/22 12:100.0050.001<0.001mg/Kg2,2-Dichloropropane
05/16/22 12:100.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/16/22 12:100.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/16/22 12:100.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/16/22 12:100.0050.0006<0.0006mg/KgEthylbenzene
05/16/22 12:100.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/16/22 12:100.0100.0008<0.0008mg/KgHexachlorobutadiene
05/16/22 12:100.0100.0007<0.0007mg/Kgn-Hexane
05/16/22 12:100.0200.0006<0.0006mg/Kg2-Hexanone
05/16/22 12:100.0050.0005<0.0005mg/KgIsopropylbenzene
05/16/22 12:100.0050.001<0.001mg/Kg4-Isopropyl toluene
05/16/22 12:100.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/16/22 12:100.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/16/22 12:100.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/16/22 12:100.0100.001<0.001mg/KgMethylene Chloride
05/16/22 12:100.0100.0010<0.0010mg/KgNaphthalene
05/16/22 12:100.0050.0005<0.0005mg/Kgn-Propylbenzene
05/16/22 12:100.0050.001<0.001mg/KgStyrene
Page 5 of 31Date:05/23/2022 04:56 PM
Page 135 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/16/22 12:100.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/16/22 12:100.0050.0009<0.0009mg/KgTetrachloroethene
05/16/22 12:100.0050.0007<0.0007mg/KgToluene
05/16/22 12:100.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/16/22 12:100.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/16/22 12:100.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/16/22 12:100.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/16/22 12:100.0050.0009<0.0009mg/KgTrichloroethene
05/16/22 12:100.0100.002<0.002mg/KgTrichlorofluoromethane
05/16/22 12:100.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/16/22 12:100.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/16/22 12:100.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/16/22 12:100.0100.0005<0.0005mg/KgVinyl Acetate
05/16/22 12:100.0100.0005<0.0005mg/KgVinyl Chloride
05/16/22 12:100.0050.0005<0.0005mg/Kgo-Xylene
05/16/22 12:100.0100.001<0.001mg/Kgm,p-Xylene
05/16/22 12:104-Bromofluorobenzene (S)101 70-130
05/16/22 12:10Dibromofluoromethane (S)101 84-123
05/16/22 12:10Toluene-d8 (S)89.0 76-129
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.112 1121080.1080.100mg/KgAcetone 29-198 3.6 20
0.093 93.592.30.0920.100mg/KgAcrolein 70-130 1.2 20
Page 6 of 31Date:05/23/2022 04:56 PM
Page 136 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101090.1090.100mg/KgAcrylonitrile 65-134 0.9 20
0.051 1041060.0530.050mg/KgBenzene 74-127 2.2 20
0.043 86.285.80.0420.050mg/KgBromobenzene 73-125 0.4 20
0.057 1151160.0570.050mg/KgBromochloromethane 72-134 0.5 20
0.055 1111100.0550.050mg/KgBromodichloromethane 75-122 0.7 20
0.048 97.897.80.0480.050mg/KgBromoform 66-135 0.0 20
0.042 85.286.80.0430.050mg/KgBromomethane 20-180 1.8 20
0.043 86.490.40.0450.050mg/Kgn-Butylbenzene 65-135 4.5 20
0.041 82.686.00.0430.050mg/Kgsec-Butyl benzene 66-131 4.0 20
0.041 83.086.20.0430.050mg/Kgtert-Butyl benzene 67-132 3.7 20
0.048 97.21050.0520.050mg/KgCarbon Disulfide 61-129 7.5 20
0.048 96.61020.0510.050mg/KgCarbon Tetrachloride 64-143 5.4 20
0.046 93.495.60.0470.050mg/KgChlorobenzene 74-118 2.3 20
0.048 96.696.20.0480.050mg/KgChlorodibromomethane 73-122 0.4 20
0.056 1141080.0530.050mg/KgChloroethane 33-149 5.2 20
0.052 1051080.0540.050mg/KgChloroform 73-127 3.0 20
0.043 86.285.20.0420.050mg/KgChloromethane 45-143 1.1 20
0.042 85.686.00.0430.050mg/Kg2-Chlorotoluene 67-124 0.4 20
0.042 85.086.20.0430.050mg/Kg4-Chlorotoluene 71-126 1.4 20
0.052 1061070.0530.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.3 20
0.049 98.492.80.0460.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.8 20
0.048 96.898.20.0490.050mg/Kg1,2-Dibromoethane 70-132 1.4 20
0.056 1121110.0550.050mg/KgDibromomethane 74-133 1.4 20
0.044 89.087.20.0430.050mg/Kg1,2-Dichlorobenzene 72-123 2.0 20
0.044 88.288.20.0440.050mg/Kg1,3-Dichlorobenzene 71-120 0.0 20
0.044 88.487.60.0430.050mg/Kg1,4-Dichlorobenzene 71-123 0.9 20
Page 7 of 31Date:05/23/2022 04:56 PM
Page 137 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 76.685.00.0420.050mg/KgDichlorodifluoromethane 26-146 10.3 20
0.051 1021050.0520.050mg/Kg1,1-Dichloroethane 74-127 3.0 20
0.053 1081070.0530.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.81010.0500.050mg/Kg1,1-Dichloroethene 67-149 8.6 20
0.051 1031030.0510.050mg/Kgcis-1,2-Dichloroethene 76-134 0.7 20
0.049 98.81040.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.3 20
0.053 1071060.0530.050mg/Kg1,2-Dichloropropane 73-130 0.5 20
0.048 96.095.20.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.050 1021090.0540.050mg/Kg2,2-Dichloropropane 50-142 6.4 20
0.048 96.41040.0510.050mg/Kg1,1-Dichloropropene 71-130 7.3 20
0.055 1111100.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 0.5 20
0.056 1121120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.044 88.694.00.0470.050mg/KgEthylbenzene 74-128 5.9 20
0.117 1171160.1160.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.8 20
0.043 86.689.40.0440.050mg/KgHexachlorobutadiene 64-125 3.1 20
0.048 97.01070.0530.050mg/Kgn-Hexane 70-130 9.8 20
0.044 88.290.60.0450.050mg/Kg2-Hexanone 61-157 2.6 20
0.041 83.486.60.0430.050mg/KgIsopropylbenzene 68-126 3.7 20
0.042 84.887.00.0430.050mg/Kg4-Isopropyl toluene 68-129 2.5 20
0.044 88.289.00.0440.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.9 20
0.054 1091090.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.0 20
0.054 1081080.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 0.1 20
0.049 99.61010.0500.050mg/KgMethylene Chloride 74-129 1.7 20
0.053 1071070.0530.050mg/KgNaphthalene 57-157 0.3 20
0.042 84.687.60.0430.050mg/Kgn-Propylbenzene 67-130 3.4 20
0.048 96.098.20.0490.050mg/KgStyrene 77-121 2.2 20
Page 8 of 31Date:05/23/2022 04:56 PM
Page 138 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.297.60.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.5 20
0.044 89.487.60.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.0 20
0.050 1011070.0530.050mg/KgTetrachloroethene 68-130 6.3 20
0.051 1031060.0530.050mg/KgToluene 71-129 3.4 20
0.048 96.094.60.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.4 20
0.047 95.093.80.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.049 99.61060.0520.050mg/Kg1,1,1-Trichloroethane 67-131 6.0 20
0.048 96.497.80.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.4 20
0.051 1031070.0530.050mg/KgTrichloroethene 75-133 3.6 20
0.045 90.298.00.0490.050mg/KgTrichlorofluoromethane 44-146 8.2 20
0.043 87.889.80.0440.050mg/Kg1,2,3-Trichloropropane 60-137 2.2 20
0.043 86.286.60.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 0.4 20
0.042 85.287.80.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.0 20
0.051 1031020.0500.050mg/KgVinyl Acetate 60-140 1.5 20
0.042 84.684.80.0420.050mg/KgVinyl Chloride 48-147 0.2 20
0.045 91.894.60.0470.050mg/Kgo-Xylene 74-126 3.0 20
0.092 92.395.60.0950.100mg/Kgm,p-Xylene 75-124 3.5 20
97.695.44-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
88.490.8Toluene-d8 (S)76-129
Page 9 of 31Date:05/23/2022 04:56 PM
Page 139 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0200.002<0.002mg/KgAcetone
05/17/22 12:520.0200.001<0.001mg/KgAcrolein
05/17/22 12:520.0200.0008<0.0008mg/KgAcrylonitrile
05/17/22 12:520.0050.0006<0.0006mg/KgBenzene
05/17/22 12:520.0050.0005<0.0005mg/KgBromobenzene
05/17/22 12:520.0050.0008<0.0008mg/KgBromochloromethane
05/17/22 12:520.0050.001<0.001mg/KgBromodichloromethane
05/17/22 12:520.0050.001<0.001mg/KgBromoform
05/17/22 12:520.0100.001<0.001mg/KgBromomethane
05/17/22 12:520.0050.0005<0.0005mg/Kgn-Butylbenzene
05/17/22 12:520.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/17/22 12:520.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/17/22 12:520.0050.0006<0.0006mg/KgCarbon Disulfide
05/17/22 12:520.0050.001<0.001mg/KgCarbon Tetrachloride
05/17/22 12:520.0050.0007<0.0007mg/KgChlorobenzene
05/17/22 12:520.0050.0009<0.0009mg/KgChlorodibromomethane
05/17/22 12:520.0100.0009<0.0009mg/KgChloroethane
05/17/22 12:520.0050.001<0.001mg/KgChloroform
05/17/22 12:520.0100.0006<0.0006mg/KgChloromethane
05/17/22 12:520.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/17/22 12:520.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/17/22 12:520.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/17/22 12:520.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/17/22 12:520.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/17/22 12:520.0050.0006<0.0006mg/KgDibromomethane
05/17/22 12:520.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/17/22 12:520.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 31Date:05/23/2022 04:56 PM
Page 140 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/17/22 12:520.0100.001<0.001mg/KgDichlorodifluoromethane
05/17/22 12:520.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/17/22 12:520.0050.001<0.001mg/Kg1,2-Dichloroethane
05/17/22 12:520.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/17/22 12:520.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/17/22 12:520.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/17/22 12:520.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/17/22 12:520.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/17/22 12:520.0050.001<0.001mg/Kg2,2-Dichloropropane
05/17/22 12:520.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/17/22 12:520.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/17/22 12:520.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/17/22 12:520.0050.0006<0.0006mg/KgEthylbenzene
05/17/22 12:520.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/17/22 12:520.0100.0008<0.0008mg/KgHexachlorobutadiene
05/17/22 12:520.0100.0007<0.0007mg/Kgn-Hexane
05/17/22 12:520.0200.0006<0.0006mg/Kg2-Hexanone
05/17/22 12:520.0050.0005<0.0005mg/KgIsopropylbenzene
05/17/22 12:520.0050.001<0.001mg/Kg4-Isopropyl toluene
05/17/22 12:520.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/17/22 12:520.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/17/22 12:520.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/17/22 12:520.0100.001<0.001mg/KgMethylene Chloride
05/17/22 12:520.0100.0010<0.0010mg/KgNaphthalene
05/17/22 12:520.0050.0005<0.0005mg/Kgn-Propylbenzene
05/17/22 12:520.0050.001<0.001mg/KgStyrene
Page 11 of 31Date:05/23/2022 04:56 PM
Page 141 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/17/22 12:520.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/17/22 12:520.0050.0009<0.0009mg/KgTetrachloroethene
05/17/22 12:520.0050.0007<0.0007mg/KgToluene
05/17/22 12:520.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/17/22 12:520.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/17/22 12:520.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/17/22 12:520.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/17/22 12:520.0050.0009<0.0009mg/KgTrichloroethene
05/17/22 12:520.0100.002<0.002mg/KgTrichlorofluoromethane
05/17/22 12:520.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/17/22 12:520.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/17/22 12:520.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/17/22 12:520.0100.0005<0.0005mg/KgVinyl Acetate
05/17/22 12:520.0100.0005<0.0005mg/KgVinyl Chloride
05/17/22 12:520.0050.0005<0.0005mg/Kgo-Xylene
05/17/22 12:520.0100.001<0.001mg/Kgm,p-Xylene
05/17/22 12:524-Bromofluorobenzene (S)104 70-130
05/17/22 12:52Dibromofluoromethane (S)105 84-123
05/17/22 12:52Toluene-d8 (S)87.8 76-129
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.125 1251140.1140.100mg/KgAcetone 29-198 9.2 20
0.105 1051040.1040.100mg/KgAcrolein 70-130 0.9 20
Page 12 of 31Date:05/23/2022 04:56 PM
Page 142 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101070.1070.100mg/KgAcrylonitrile 65-134 2.7 20
0.054 1091140.0570.050mg/KgBenzene 74-127 4.2 20
0.043 86.890.40.0450.050mg/KgBromobenzene 73-125 4.0 20
0.057 1161180.0590.050mg/KgBromochloromethane 72-134 2.0 20
0.057 1151170.0580.050mg/KgBromodichloromethane 75-122 1.2 20
0.049 99.41000.0500.050mg/KgBromoform 66-135 1.0 20
0.042 84.084.40.0420.050mg/KgBromomethane 20-180 0.4 20
0.045 90.495.60.0470.050mg/Kgn-Butylbenzene 65-135 5.5 20
0.043 87.293.20.0460.050mg/Kgsec-Butyl benzene 66-131 6.6 20
0.043 87.292.20.0460.050mg/Kgtert-Butyl benzene 67-132 5.5 20
0.054 1101170.0580.050mg/KgCarbon Disulfide 61-129 6.7 20
0.054 1091160.0580.050mg/KgCarbon Tetrachloride 64-143 6.2 20
0.048 96.61000.0500.050mg/KgChlorobenzene 74-118 3.4 20
0.049 98.61000.0500.050mg/KgChlorodibromomethane 73-122 1.6 20
0.059 11890.00.0450.050mg/KgChloroethane 33-149 27.0*20
0.055 1111160.0580.050mg/KgChloroform 73-127 4.5 20
0.044 88.487.40.0430.050mg/KgChloromethane 45-143 1.1 20
0.043 87.092.20.0460.050mg/Kg2-Chlorotoluene 67-124 5.8 20
0.044 88.891.80.0450.050mg/Kg4-Chlorotoluene 71-126 3.3 20
0.053 1081100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.8 20
0.045 90.887.60.0430.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.5 20
0.049 99.298.80.0490.050mg/Kg1,2-Dibromoethane 70-132 0.4 20
0.057 1151150.0570.050mg/KgDibromomethane 74-133 0.5 20
0.045 90.292.20.0460.050mg/Kg1,2-Dichlorobenzene 72-123 2.1 20
0.044 89.092.60.0460.050mg/Kg1,3-Dichlorobenzene 71-120 3.9 20
0.044 89.492.40.0460.050mg/Kg1,4-Dichlorobenzene 71-123 3.3 20
Page 13 of 31* QC Fail Date:05/23/2022 04:56 PM
Page 143 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.058 1171060.0530.050mg/KgDichlorodifluoromethane 26-146 9.6 20
0.053 1081120.0550.050mg/Kg1,1-Dichloroethane 74-127 3.6 20
0.055 1121120.0560.050mg/Kg1,2-Dichloroethane 68-128 0.5 20
0.051 1041100.0550.050mg/Kg1,1-Dichloroethene 67-149 6.3 20
0.053 1061100.0550.050mg/Kgcis-1,2-Dichloroethene 76-134 3.3 20
0.052 1051090.0540.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.7 20
0.054 1091090.0540.050mg/Kg1,2-Dichloropropane 73-130 0.3 20
0.048 96.897.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.054 1091170.0580.050mg/Kg2,2-Dichloropropane 50-142 7.6 20
0.053 1071130.0560.050mg/Kg1,1-Dichloropropene 71-130 5.8 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.056 1131160.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.047 94.298.60.0490.050mg/KgEthylbenzene 74-128 4.5 20
0.109 1091100.1100.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.044 88.691.80.0450.050mg/KgHexachlorobutadiene 64-125 3.5 20
0.057 1161220.0600.050mg/Kgn-Hexane 70-130 5.0 20
0.047 95.491.60.0450.050mg/Kg2-Hexanone 61-157 4.0 20
0.043 87.092.20.0460.050mg/KgIsopropylbenzene 68-126 5.8 20
0.044 89.094.20.0470.050mg/Kg4-Isopropyl toluene 68-129 5.6 20
0.056 1131040.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 7.9 20
0.054 1081080.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.054 1081040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 3.3 20
0.054 1081110.0550.050mg/KgMethylene Chloride 74-129 2.0 20
0.047 94.693.60.0460.050mg/KgNaphthalene 57-157 1.0 20
0.044 89.294.40.0470.050mg/Kgn-Propylbenzene 67-130 5.6 20
0.050 1001020.0510.050mg/KgStyrene 77-121 1.9 20
Page 14 of 31Date:05/23/2022 04:56 PM
Page 144 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.61020.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.3 20
0.044 88.490.40.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.053 1081130.0560.050mg/KgTetrachloroethene 68-130 4.8 20
0.054 1081140.0560.050mg/KgToluene 71-129 4.8 20
0.046 92.094.00.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.1 20
0.045 91.294.20.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.2 20
0.054 1091140.0570.050mg/Kg1,1,1-Trichloroethane 67-131 4.8 20
0.048 97.898.40.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.6 20
0.054 1091150.0570.050mg/KgTrichloroethene 75-133 5.3 20
0.056 1131140.0560.050mg/KgTrichlorofluoromethane 44-146 0.3 20
0.045 90.890.00.0450.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.043 87.892.20.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 4.8 20
0.044 89.093.20.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.6 20
0.054 1081170.0580.050mg/KgVinyl Acetate 60-140 7.2 20
0.054 1091140.0570.050mg/KgVinyl Chloride 48-147 5.0 20
0.047 95.298.40.0490.050mg/Kgo-Xylene 74-126 3.3 20
0.096 96.41010.1010.100mg/Kgm,p-Xylene 75-124 4.6 20
98.298.44-Bromofluorobenzene (S)70-130
104102Dibromofluoromethane (S)84-123
89.088.6Toluene-d8 (S)76-129
Page 15 of 31Date:05/23/2022 04:56 PM
Page 145 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18871QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18870
Associated Lab Samples: 89778
LRB-V18870 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.001<0.001mg/KgChloroform
05/17/22 12:524-Bromofluorobenzene (S)104 70-130
05/17/22 12:52Dibromofluoromethane (S)105 70-130
05/17/22 12:52Toluene-d8 (S)87.8 76-129
LCS-V18870 LCSD-V18870Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1111160.0580.050mg/KgChloroform 73-127 4.5 20
98.298.44-Bromofluorobenzene (S)70-130
104102Dibromofluoromethane (S)70-130
89.088.6Toluene-d8 (S)76-129
Page 16 of 31Date:05/23/2022 04:56 PM
Page 146 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0200.002<0.002mg/KgAcetone
05/20/22 11:580.0200.001<0.001mg/KgAcrolein
05/20/22 11:580.0200.0008<0.0008mg/KgAcrylonitrile
05/20/22 11:580.0050.0006<0.0006mg/KgBenzene
05/20/22 11:580.0050.0005<0.0005mg/KgBromobenzene
05/20/22 11:580.0050.0008<0.0008mg/KgBromochloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromodichloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromoform
05/20/22 11:580.0100.001<0.001mg/KgBromomethane
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Butylbenzene
05/20/22 11:580.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/20/22 11:580.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/20/22 11:580.0050.0006<0.0006mg/KgCarbon Disulfide
05/20/22 11:580.0050.001<0.001mg/KgCarbon Tetrachloride
05/20/22 11:580.0050.0007<0.0007mg/KgChlorobenzene
05/20/22 11:580.0050.0009<0.0009mg/KgChlorodibromomethane
05/20/22 11:580.0100.0009<0.0009mg/KgChloroethane
05/20/22 11:580.0050.001<0.001mg/KgChloroform
05/20/22 11:580.0100.0006<0.0006mg/KgChloromethane
05/20/22 11:580.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/20/22 11:580.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/20/22 11:580.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/20/22 11:580.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/20/22 11:580.0050.0006<0.0006mg/KgDibromomethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 17 of 31Date:05/23/2022 04:56 PM
Page 147 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/20/22 11:580.0100.001<0.001mg/KgDichlorodifluoromethane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/20/22 11:580.0050.001<0.001mg/Kg1,2-Dichloroethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/20/22 11:580.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/20/22 11:580.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/20/22 11:580.0050.001<0.001mg/Kg2,2-Dichloropropane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/20/22 11:580.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/20/22 11:580.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/20/22 11:580.0050.0006<0.0006mg/KgEthylbenzene
05/20/22 11:580.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/20/22 11:580.0100.0008<0.0008mg/KgHexachlorobutadiene
05/20/22 11:580.0100.0007<0.0007mg/Kgn-Hexane
05/20/22 11:580.0200.0006<0.0006mg/Kg2-Hexanone
05/20/22 11:580.0050.0005<0.0005mg/KgIsopropylbenzene
05/20/22 11:580.0050.001<0.001mg/Kg4-Isopropyl toluene
05/20/22 11:580.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/20/22 11:580.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/20/22 11:580.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/20/22 11:580.0100.001<0.001mg/KgMethylene Chloride
05/20/22 11:580.0100.0010<0.0010mg/KgNaphthalene
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Propylbenzene
05/20/22 11:580.0050.001<0.001mg/KgStyrene
Page 18 of 31Date:05/23/2022 04:56 PM
Page 148 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTetrachloroethene
05/20/22 11:580.0050.0007<0.0007mg/KgToluene
05/20/22 11:580.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/20/22 11:580.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTrichloroethene
05/20/22 11:580.0100.002<0.002mg/KgTrichlorofluoromethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/20/22 11:580.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Acetate
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Chloride
05/20/22 11:580.0050.0005<0.0005mg/Kgo-Xylene
05/20/22 11:580.0100.001<0.001mg/Kgm,p-Xylene
05/20/22 11:584-Bromofluorobenzene (S)103 70-130
05/20/22 11:58Dibromofluoromethane (S)101 84-123
05/20/22 11:58Toluene-d8 (S)86.6 76-129
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.882.00.0820.100mg/KgAcetone 29-198 13.4 20
0.090 90.488.40.0880.100mg/KgAcrolein 70-130 2.2 20
Page 19 of 31Date:05/23/2022 04:56 PM
Page 149 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.090 90.386.00.0860.100mg/KgAcrylonitrile 65-134 4.8 20
0.055 1101140.0570.050mg/KgBenzene 74-127 3.9 20
0.044 89.691.00.0450.050mg/KgBromobenzene 73-125 1.5 20
0.057 1151170.0580.050mg/KgBromochloromethane 72-134 2.4 20
0.058 1171200.0590.050mg/KgBromodichloromethane 75-122 2.0 20
0.052 1041000.0500.050mg/KgBromoform 66-135 3.7 20
0.047 95.61010.0500.050mg/KgBromomethane 20-180 5.4 20
0.046 92.697.20.0480.050mg/Kgn-Butylbenzene 65-135 4.8 20
0.044 88.693.00.0460.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.043 86.691.60.0450.050mg/Kgtert-Butyl benzene 67-132 5.6 20
0.051 1041110.0550.050mg/KgCarbon Disulfide 61-129 6.5 20
0.054 1101180.0590.050mg/KgCarbon Tetrachloride 64-143 7.5 20
0.049 98.498.20.0490.050mg/KgChlorobenzene 74-118 0.2 20
0.050 10197.20.0480.050mg/KgChlorodibromomethane 73-122 3.4 20
0.062 1241260.0620.050mg/KgChloroethane 33-149 0.9 20
0.056 1131160.0580.050mg/KgChloroform 73-127 2.6 20
0.034 69.674.80.0370.050mg/KgChloromethane 45-143 7.2 20
0.044 89.492.00.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.044 89.893.00.0460.050mg/Kg4-Chlorotoluene 71-126 3.5 20
0.042 85.487.20.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.045 91.489.00.0440.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.6 20
0.050 10097.20.0480.050mg/Kg1,2-Dibromoethane 70-132 3.2 20
0.060 1201190.0590.050mg/KgDibromomethane 74-133 1.5 20
0.044 88.489.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.043 87.890.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.044 88.290.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
Page 20 of 31Date:05/23/2022 04:56 PM
Page 150 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1061130.0560.050mg/KgDichlorodifluoromethane 26-146 6.9 20
0.050 1001040.0510.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
0.053 1071090.0540.050mg/Kg1,2-Dichloroethane 68-128 1.4 20
0.045 91.097.40.0480.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.047 95.898.40.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 2.6 20
0.046 93.096.00.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.1 20
0.051 1021040.0520.050mg/Kg1,2-Dichloropropane 73-130 1.7 20
0.048 96.296.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.056 1131190.0590.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.054 1091130.0560.050mg/Kg1,1-Dichloropropene 71-130 3.4 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.058 1161140.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.049 98.21010.0500.050mg/KgEthylbenzene 74-128 2.4 20
0.094 94.294.80.0940.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.043 87.892.60.0460.050mg/KgHexachlorobutadiene 64-125 5.3 20
0.054 1081120.0560.050mg/Kgn-Hexane 70-130 3.9 20
0.035 70.468.40.0340.050mg/Kg2-Hexanone 61-157 2.8 20
0.044 88.291.80.0450.050mg/KgIsopropylbenzene 68-126 4.0 20
0.044 88.692.20.0460.050mg/Kg4-Isopropyl toluene 68-129 3.9 20
0.045 90.092.80.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.0 20
0.052 1041040.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.043 87.685.40.0420.050mg/Kg4-Methyl-2-Pentanone 57-162 2.5 20
0.041 82.090.20.0450.050mg/KgMethylene Chloride 74-129 9.5 20
0.047 94.488.60.0440.050mg/KgNaphthalene 57-157 6.3 20
0.045 91.295.60.0470.050mg/Kgn-Propylbenzene 67-130 4.7 20
0.049 99.41010.0500.050mg/KgStyrene 77-121 1.3 20
Page 21 of 31Date:05/23/2022 04:56 PM
Page 151 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.01000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.044 88.487.40.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.1 20
0.055 1111160.0580.050mg/KgTetrachloroethene 68-130 4.5 20
0.055 1111150.0570.050mg/KgToluene 71-129 3.5 20
0.045 90.689.40.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.3 20
0.046 92.092.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.057 1161190.0590.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.049 98.299.00.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.055 1111160.0580.050mg/KgTrichloroethene 75-133 4.7 20
0.051 1031110.0550.050mg/KgTrichlorofluoromethane 44-146 7.5 20
0.044 89.085.80.0420.050mg/Kg1,2,3-Trichloropropane 60-137 3.6 20
0.044 88.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.7 20
0.044 88.291.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.059 1181160.0570.050mg/KgVinyl Acetate 60-140 2.2 20
0.044 89.692.60.0460.050mg/KgVinyl Chloride 48-147 3.2 20
0.049 99.099.60.0490.050mg/Kgo-Xylene 74-126 0.6 20
0.099 99.91020.1020.100mg/Kgm,p-Xylene 75-124 2.0 20
1011024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)84-123
87.085.6Toluene-d8 (S)76-129
Page 22 of 31Date:05/23/2022 04:56 PM
Page 152 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0200.002<0.002mg/KgAcetone
05/20/22 11:580.0200.001<0.001mg/KgAcrolein
05/20/22 11:580.0200.0008<0.0008mg/KgAcrylonitrile
05/20/22 11:580.0050.0006<0.0006mg/KgBenzene
05/20/22 11:580.0050.0005<0.0005mg/KgBromobenzene
05/20/22 11:580.0050.0008<0.0008mg/KgBromochloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromodichloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromoform
05/20/22 11:580.0100.001<0.001mg/KgBromomethane
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Butylbenzene
05/20/22 11:580.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/20/22 11:580.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/20/22 11:580.0050.0006<0.0006mg/KgCarbon Disulfide
05/20/22 11:580.0050.001<0.001mg/KgCarbon Tetrachloride
05/20/22 11:580.0050.0007<0.0007mg/KgChlorobenzene
05/20/22 11:580.0050.0009<0.0009mg/KgChlorodibromomethane
05/20/22 11:580.0100.0009<0.0009mg/KgChloroethane
05/20/22 11:580.0050.001<0.001mg/KgChloroform
05/20/22 11:580.0100.0006<0.0006mg/KgChloromethane
05/20/22 11:580.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/20/22 11:580.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/20/22 11:580.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/20/22 11:580.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/20/22 11:580.0050.0010<0.0010mg/KgDibromomethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 23 of 31Date:05/23/2022 04:56 PM
Page 153 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/20/22 11:580.0100.001<0.001mg/KgDichlorodifluoromethane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/20/22 11:580.0050.001<0.001mg/Kg1,2-Dichloroethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/20/22 11:580.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/20/22 11:580.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/20/22 11:580.0050.001<0.001mg/Kg2,2-Dichloropropane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/20/22 11:580.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/20/22 11:580.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/20/22 11:580.0050.0006<0.0006mg/KgEthylbenzene
05/20/22 11:580.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/20/22 11:580.0100.0008<0.0008mg/KgHexachlorobutadiene
05/20/22 11:580.0100.0007<0.0007mg/Kgn-Hexane
05/20/22 11:580.0200.0006<0.0006mg/Kg2-Hexanone
05/20/22 11:580.0050.0005<0.0005mg/KgIsopropylbenzene
05/20/22 11:580.0050.001<0.001mg/Kg4-Isopropyl toluene
05/20/22 11:580.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/20/22 11:580.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/20/22 11:580.0050.001<0.001mg/KgMethylene Chloride
05/20/22 11:580.0100.0010<0.0010mg/KgNaphthalene
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Propylbenzene
05/20/22 11:580.0050.001<0.001mg/KgStyrene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 24 of 31Date:05/23/2022 04:56 PM
Page 154 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTetrachloroethene
05/20/22 11:580.0050.0007<0.0007mg/KgToluene
05/20/22 11:580.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/20/22 11:580.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTrichloroethene
05/20/22 11:580.0100.002<0.002mg/KgTrichlorofluoromethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/20/22 11:580.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Acetate
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Chloride
05/20/22 11:580.0050.0005<0.0005mg/Kgo-Xylene
05/20/22 11:580.0100.001<0.001mg/Kgm,p-Xylene
05/20/22 11:584-Bromofluorobenzene (S)103 70-130
05/20/22 11:58Dibromofluoromethane (S)101 70-130
05/20/22 11:58Toluene-d8 (S)86.6 76-129
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.882.00.0820.100mg/KgAcetone 29-198 13.4 20
0.090 90.488.40.0880.100mg/KgAcrolein 70-130 2.2 20
0.090 90.386.00.0860.100mg/KgAcrylonitrile 65-134 4.8 20
Page 25 of 31Date:05/23/2022 04:56 PM
Page 155 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1101140.0570.050mg/KgBenzene 74-127 3.9 20
0.044 89.691.00.0450.050mg/KgBromobenzene 73-125 1.5 20
0.057 1151170.0580.050mg/KgBromochloromethane 72-134 2.4 20
0.058 1171200.0590.050mg/KgBromodichloromethane 75-122 2.0 20
0.052 1041000.0500.050mg/KgBromoform 66-135 3.7 20
0.047 95.61010.0500.050mg/KgBromomethane 20-180 5.4 20
0.046 92.697.20.0480.050mg/Kgn-Butylbenzene 65-135 4.8 20
0.044 88.693.00.0460.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.043 86.691.60.0450.050mg/Kgtert-Butyl benzene 67-132 5.6 20
0.051 1041110.0550.050mg/KgCarbon Disulfide 61-129 6.5 20
0.054 1101180.0590.050mg/KgCarbon Tetrachloride 64-143 7.5 20
0.049 98.498.20.0490.050mg/KgChlorobenzene 74-118 0.2 20
0.050 10197.20.0480.050mg/KgChlorodibromomethane 73-122 3.4 20
0.062 1241260.0620.050mg/KgChloroethane 33-149 0.9 20
0.056 1131160.0580.050mg/KgChloroform 73-127 2.6 20
0.034 69.674.80.0370.050mg/KgChloromethane 45-143 7.2 20
0.044 89.492.00.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.044 89.893.00.0460.050mg/Kg4-Chlorotoluene 71-126 3.5 20
0.042 85.487.20.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.045 91.489.00.0440.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.6 20
0.050 10097.20.0480.050mg/Kg1,2-Dibromoethane 70-132 3.2 20
0.060 1201190.0590.050mg/KgDibromomethane 74-133 1.5 20
0.044 88.489.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.043 87.890.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.044 88.290.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
0.052 1061130.0560.050mg/KgDichlorodifluoromethane 26-146 6.9 20
Page 26 of 31Date:05/23/2022 04:56 PM
Page 156 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1001040.0510.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
0.053 1071090.0540.050mg/Kg1,2-Dichloroethane 68-128 1.4 20
0.045 91.097.40.0480.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.047 95.898.40.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 2.6 20
0.046 93.096.00.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.1 20
0.051 1021040.0520.050mg/Kg1,2-Dichloropropane 73-130 1.7 20
0.048 96.296.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.056 1131190.0590.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.054 1091130.0560.050mg/Kg1,1-Dichloropropene 71-130 3.4 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.058 1161140.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.049 98.21010.0500.050mg/KgEthylbenzene 74-128 2.4 20
0.094 94.294.80.0940.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.043 87.892.60.0460.050mg/KgHexachlorobutadiene 64-125 5.3 20
0.054 1081120.0560.050mg/Kgn-Hexane 70-130 3.9 20
0.035 70.468.40.0340.050mg/Kg2-Hexanone 61-157 2.8 20
0.044 88.291.80.0450.050mg/KgIsopropylbenzene 68-126 4.0 20
0.044 88.692.20.0460.050mg/Kg4-Isopropyl toluene 68-129 3.9 20
0.045 90.092.80.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.0 20
0.052 1041040.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.041 82.090.20.0450.050mg/KgMethylene Chloride 74-129 9.5 20
0.047 94.488.60.0440.050mg/KgNaphthalene 57-157 6.3 20
0.045 91.295.60.0470.050mg/Kgn-Propylbenzene 67-130 4.7 20
0.049 99.41010.0500.050mg/KgStyrene 77-121 1.3 20
0.049 99.01000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.044 88.487.40.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.1 20
Page 27 of 31Date:05/23/2022 04:56 PM
Page 157 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1111160.0580.050mg/KgTetrachloroethene 68-130 4.5 20
0.055 1111150.0570.050mg/KgToluene 71-129 3.5 20
0.045 90.689.40.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.3 20
0.046 92.092.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.057 1161190.0590.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.049 98.299.00.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.055 1111160.0580.050mg/KgTrichloroethene 75-133 4.7 20
0.051 1031110.0550.050mg/KgTrichlorofluoromethane 44-146 7.5 20
0.044 89.085.80.0420.050mg/Kg1,2,3-Trichloropropane 60-137 3.6 20
0.044 88.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.7 20
0.044 88.291.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.059 1181160.0570.050mg/KgVinyl Acetate 60-140 2.2 20
0.044 89.692.60.0460.050mg/KgVinyl Chloride 48-147 3.2 20
0.049 99.099.60.0490.050mg/Kgo-Xylene 74-126 0.6 20
0.099 99.91020.1020.100mg/Kgm,p-Xylene 75-124 2.0 20
1011024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)70-130
87.085.6Toluene-d8 (S)76-129
Page 28 of 31Date:05/23/2022 04:56 PM
Page 158 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18823QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89427-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/18/22 11:010.013.913.9%Moisture
V 89775-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/18/22 11:011.815.916.2%Moisture
Page 29 of 31Date:05/23/2022 04:56 PM
Page 159 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18876QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89785-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/19/22 10:402.49.008.78%Moisture
V 89793-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/19/22 10:400.824.724.9%Moisture
Page 30 of 31Date:05/23/2022 04:56 PM
Page 160 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18961QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89795-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/20/22 12:520.910.210.1%Moisture
V 90119-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/20/22 12:521.821.922.3%Moisture
Page 31 of 31Date:05/23/2022 04:56 PM
Page 161 of 166
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-133-0023
ATC Group Services, LLC - Raleigh, NC
01024
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 6.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:05/13/2022 15:55:14
Special precautions or instructions included?
Comments:
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