RA-29314_48478_CA_IAR_20220518

Initial Abatement Action Report
Edge of Auburn Property Release
7501 Rock Quarry Road
Town of Garner, Wake County, North Carolina 27502
Prepared for:
OCS-HS Lot Option Pool 02 Limited Partnership
Hearthstone Inc
23975 Park Sorrento, Suite 220
Calabasas, CA 91302-4023
Prepared by:
Protocol Sampling Service, Inc.
4114 Laurel Ridge Drive
Raleigh, North Carolina 27612
Protocol Sampling Service, Inc.
“Experts in Environmental Compliance”
Protocol Sampling Service, Inc.
Certification Number: C-569
i
Initial Abatement Action Report
Site Information
1.Site Identification
Date of Report:May 18, 2022 Site Risk: Unknown
Facility I.D.:N/A UST Incident Number (if known): N/A
Site Name: Edge of Auburn Property Release
Street Address:7501 Rock Quarry Road
Town:Garner Zip Code: 27610 County: Wake
Description of Geographical Data Point: Former UST location
Location Method: GPS
Latitude:35.692326° Longitude: -78.526688°
2.Information about Contacts Associated with the Leaking UST System
AST Owner: Unknown Email:
Address:Tel:
AST Operator: Unknown Email:
Address: Tel:
Property Owner:
OCS-HS Lot Option Pool 02
Limited Partnership
Hearthstone Inc
Email:
Address: 23975 Park Sorrento, Suite 220
Calabasas, CA 91302-4023 Tel:
Property Occupant: N/A Email:
Address: Tel:
Consultant: Spangler Environmental, Inc. Email: [e-mail]
Address: 4338 Bland Rd, Raleigh, NC 27609 Tel: [phone]
Consultant: Protocol Sampling Service, Inc. Email: [e-mail]
Address: 4114 Laurel Ridge Dr, Raleigh, NC 27612 Tel: [phone]
Contractor: HERR, Inc. Email: [e-mail]
Address: 303 S Maultsby St, Whiteville, NC 28472 Tel: [phone]
Analytical Lab: Waypoint Analytical, Inc. State Certification No: 402, 37735
Address: 449 Springbrook Rd, Charlotte, NC 28224 Tel: [phone]
Analytical Lab: RED Lab, LLC State Certification No: N/A: UVF
Address: 5598 Marvin K Moss Lane, Suite 2003,
Wilmington NC 28409 Tel: [phone]
3.Information about the Release
Date Discovered:April 7, 2022
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Assumed UST or UST piping
Size and Contents of Tank from
which the Release Occurred: 500 gal, presumed #2 heating oil, kerosene, and/or diesel
ii
4. Certification
I, David E. Meyer, P.G. LSS, a Licensed Geologist for Protocol Sampling Service, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Protocol Sampling Service, Inc. is licensed to practice geology in North Carolina. The certification number of the
company or corporation is: C-569.
iii
Executive Summary
During initial tree clearing operations for residential property development on May 7, 2022, an abandoned
underground storage tank (UST) was discovered at the former home/farmstead site at 7501 Rock Quarry Road in
Garner, NC. The UST appeared to be intact, with the exception of a few punctures in the top of the UST which
appeared to happen during the recent discovery. The UST was nearly full, with a mixture of petroleum product and
assumed rainwater. The initial soil sampling on May 11, 2022 indicated a previous release from the UST system. The
amount of petroleum products released is unknown. Based on laboratory data, the material released appeared to be
diesel fuel.
Initial abatement activities included mobilizing to the site with a photoionization detector (PID) to screen the soils for
total volatile organic compounds (tVOCs), a mobile laboratory (RED Lab, LLC) for initial clearance sample analysis,
and a remediation contractor (HERR, Inc.) to evacuate/remove the UST from the property and excavate/remove the
petroleum impacted soils from the property. The UST was emptied via vacuum-truck and 456 gallons of petroleum
impacted water and residual product were transported under a non-hazardous waste manifest to HERR, LLC in
Thomasville, NC (HERR; EPA ID No NCR000139816). The emptied UST was transported under a non-hazardous
waste manifest for recycling to DH Griffin Wrecking Company in High Point, NC. Excavated soils were loaded
directly onto dump trucks and transported under non-hazardous waste manifests to Triangle Area Earth Corporation
in Zebulon, NC (TAEC; NCDEQ Permit SRU600082).
Eight soil samples were collected for site closure. Six soil samples were collected from approximately four to eight
feet below ground surface (BGS) from the sidewalls of the excavation. Two soil samples were collected from
approximately eight to fifteen feet at the bottom of the excavation. The soil samples were analyzed on-site by PID
screening and Ultraviolet Fluorescence (UVF), then shipped to Waypoint Analytical in Charlotte, NC (Waypoint; NC
Lab ID 402 and 37735) for final closure analysis.
Closure samples collected from the sidewalls and floor of the excavation were initially analyzed on-site by RED Lab
via UVF for Benzene, Toluene, Ethylbenzene, and Xylene (as total BTEX), Total Petroleum Hydrocarbons – Gasoline
Range Organics (TPH-GRO), TPH – Diesel Range Organics (DRO), Total Aromatics, Polycyclic Aromatic
Hydrocarbons, (PAHs), and Benzo(a)pyrene (BaP). The on-site UVF results did not identify petroleum constituents
at concentrations in excess of the NCDEQ Residential Maximum Soil Contaminant Concentrations (MSCCs) or
Action Limits in the samples submitted for site closure.
In accordance with NCDEQ UST closure guidelines, the closure samples were submitted to Waypoint Analytical in
Charlotte, NC for analysis of volatile organic compounds (VOCs) by EPA method 8260, semi-volatile organic
compounds (SVOCs) by EPA method 8270, and volatile petroleum hydrocarbons (VPHs) and extractable petroleum
hydrocarbons (EPHs) by the Massachusetts Department of Environmental Protection (MADEP) method. The
analytical laboratory results from the soil excavation closure samples did not identify petroleum constituents at
concentrations in excess of the Residential MSCCs.
Groundwater, bedrock, or non-aqueous phase liquids (NAPL, also known as ‘free product’) were not encountered
during the excavation activities and the nearest potential surface water receptor is located greater than 400 feet from
the impacted soils exaction. As such, groundwater and surface water characterization was not completed as a part of
this assessment.
Based on the findings during the Initial Abatement Actions and the level of remediation achieved in the soils at the property,
Spangler Environmental, Inc. and Protocol Sampling Service, Inc. request that the incident be granted unrestricted
regulatory closure.
v
Table of Contents
Site Information ............................................................................................................................................................ i
Executive Summary ................................................................................................................................................... iii
Table of Contents ......................................................................................................................................................... v
Site History and Characterization .............................................................................................................................. 1
Initial Response and Abatement Action ...................................................................................................................... 1
Excavation of Contaminated Soil ................................................................................................................................ 2
Conclusions ................................................................................................................................................................... 3
List of Figures, Tables, Appendices ........................................................................................................................... 3
Figures
Tables
Appendix A
Appendix B
Appendix C
Appendix D
1

Site History and Characterization

Historically the site was utilized as a home/farmstead. Numerous residential/agricultural structures were identified at
the property; however, there are no longer any historic structures present. The property is currently undergoing initial
residential development. The area where the release occurred was the presumed former location of a residential
structure. The site is currently owned by OCS-HS Lot Option Pool 02 Limited Partnership Hearthstone Inc of 23975
Park Sorrento, Suite 220, Calabasas, CA 91302-4023, who have assumed responsibility for the release.

During initial tree-clearing activities, the top of a UST was uncovered at approximately two feet BGS. This UST is
located near the presumed foundation of a former residential structure, with the remnants of a CMU septic tank
approximately twenty feet to the south; however, no associated piping, fill ports, dispensers, or any other ancillary
UST equipment has been identified in this area. Based on field screening activities and laboratory analysis, the
petroleum products encountered appear to be constituents of off-road diesel fuel. Based on the location of the UST
and the completed closure sampling, it is believed that the release solely occurred at this location. The dates of
operation of the UST, the date(s) of release, and the quantity of petroleum product released are all unknown.

The release was discovered on April 11, 2022, during initial soil screening and sampling activities. The release was
discovered near the presumed northeast-corner foundation of the former residential structure, along the east side and
at the north and south ends of the UST. There are no other documented releases in the vicinity of this release that
could have comingled. Initial delineation activities included soil collection via hand auger borings on April 11, 2022,
and additional soil sample collection via hollow stem auger on April 15, 2022. The initial delineation identified soil
contamination at depths of up to fourteen feet BGS in an area no larger than approximately forty feet by forty feet.

Several utility easements are present along the western adjoining roadway (Rock Quarry Road) approximately 100
feet west of the UST. The closest surface water to the release is an on-site stream that is located approximately 500
feet away, to the east from the leading edge of the excavation. The majority of the area near the source of the release
has been recently cleared of trees and is undergoing initial site grading activities for residential development. There
are several rural residential properties located greater than 500 feet south of the Excavation area. However, neither
groundwater, bedrock, nor NAPL were encountered in the excavation, and therefore, groundwater and surface water
characterization was not completed as a part of this assessment.

Initial abatement actions to date include excavating and properly disposing of 189.13 tons of petroleum impacted soils
to TAEC. Soils collected from the resultant sidewalls and floor of the excavation were PID screened for and analyzed
on-site by RED Lab via UVF analysis. Upon identifying clean (tVOC < 10 parts per million [ppm] and no UVF
detections above Residential MSCCs) sidewall and floor screening locations at the perimeter of the excavation, an
approximately 3-foot safety berm was constructed around the excavation and the excavation was left open in
anticipation of separate site contractors to backfill and compact. Given ongoing grading operations at the property,
topsoil, seed, and straw were not applied to the excavation area. Based upon the lack of groundwater encountered in
the excavation, no monitoring wells were installed at the property, and groundwater characterization was not
completed.
Initial Response and Abatement Action

Initial Response and Abatement Action included mobilizing to the site with a PID, RED Lab LLC’s mobile UVF lab,
and HERR to evacuate/remove the UST and excavate/remove all petroleum impacted soils that were encountered in
the release area. The release was expected to have occurred solely from the one previously identified UST. There are
no water supply wells in the immediately surrounding area (500 feet) that are at risk from this release.

Based on the location of the identified UST in relation to the former residential structure at the property, this UST
(and/or any former system components) is presumed to be the sole source of petroleum contamination in this area.
This was confirmed during excavation activities when no evidence additional USTs was observed, by the extents of
the excavation area, and the location of clean soils encountered around the perimeter of the excavation. Non-aqueous
Phase Liquid (NAPL) was not encountered during the excavation activities. Petroleum impacted soils were loaded
directly onto dump trucks to prevent any possible spreading of impacted soils on the site.

2
Excavation of Contaminated Soil
The source of the release is presumed to be solely the one 500-gallon diesel UST identified at the property. During
the course of the remediation, 189.13 tons of petroleum impacted soils were excavated and loaded directly into dump
trucks for disposal at TAEC in Zebulon, NC.
The excavation was a rectangle shape when completed. The horizontal extents of the excavation were approximately
18 feet (north to south) by 12 feet (east to west). The total depth of the south end of the excavation was approximately
eight feet BGS, and the total depth of the north end of the excavation was approximately fifteen feet BGS. The
calculated volume of petroleum impacted soils that were removed from the site was approximately 92 cubic yards.
As petroleum impacted soils were excavated, periodic samples were collected for on-site PID screening and UVF
analysis. As the excavation reached clean soils (tVOCs <10 ppm and no UVF detections in excess of Residential
MSCCs) around the sidewalls, the excavation was not extended further in that direction and closure samples were
collected and stored on ice prior to delivery to Waypoint. A Hyundai HX220L excavator was used for excavating the
soils at the site. The soils were then loaded directly into dump trucks for transport to TAEC under non-hazardous
waste manifests. Soils encountered on the site were observed to be tan-orange sandy clays. Neither groundwater nor
bedrock were encountered in the excavation area.
In order to ensure that clean soils had been encountered in the perimeter of the excavation, soil samples were collected
from the final resultant sidewalls at depths of approximately four feet BGS on the south end of the excavation and
approximately eight feet BGS on the north end of the excavation. Similarly, soil samples were collected from the final
resultant floor at depths of approximately eight feet BGS on the south end of the excavation and approximately fifteen
feet BGS on the north end of the excavation.
Soil samples were collected from the sidewalls by using the excavator bucket. A mass of soil was pulled off of the
sidewall and Spangler Environmental, Inc. and Protocol Sampling Service, Inc. utilized new nitrile gloves to extract
soils from this mass in areas that had not encountered the excavator bucket. The soils were transferred to new, unused
Ziplock® bags and screened with a PID and analyzed on-site via UVF. After PID screening and UVF analysis was
completed, select sidewall and floor samples were then transferred into laboratory supplied glassware, properly
labeled, and stored on ice. These soil samples were shipped under proper chain-of-custody protocol to Waypoint for
analysis of VOC, SVOC, VPH, and EPH.
The sample locations can be seen in the attached maps (Figure 2 and Figure 3). A total of six sidewall samples and
two floor samples were collected for analysis. Petroleum constituents were identified in the closure samples submitted,
but each of the detected concentrations were below their respective Residential MSCC. A summary of the full
laboratory data as well as a summary of detections are included in the tables and appendices of this report.
Excavated, petroleum impacted soils were loaded directly onto dump trucks at the site. The soils were then transported
by R&M Trucking (subcontractors of HERR) to TAEC. Certified scales determined that a total of 189.13 tons were
disposed of at TAEC. This amounted to approximately 85 cubic yards of petroleum impacted soil removed from the
property. Following soil removal, an approximately 3-foot safety berm was constructed around the excavation and the
excavation was left open in anticipation of separate site contractors to backfill and compact. Given ongoing grading
operations at the property, topsoil, seed, and straw were not applied to the excavation area.
3
Conclusions
Spangler Environmental, Inc. and Protocol Sampling Service, Inc. directed the excavation of all petroleum impacted soils
encountered from the release at this site. The excavation was extended vertically and horizontally in all directions until
clean soils were encountered in the floor and sidewalls surrounding the perimeter of the excavation. The floor and sidewalls
were determined to be clean by screening the soils with a PID and on-site UVF analysis until locations exhibiting less than
ten ppm tVOCs and no petroleum constituents above Residential MSCCs were identified. Furthermore, laboratory analysis
did not identify any VOC, SVOC, EPH, or VPH concentrations above Residential MSCCs in the floor or sidewall closure
samples. Based on laboratory data obtained, discussions with NCDEQ and Waypoint, no petroleum constituents remain
at the site above regulatory limits in the soils. There were no floor or sidewall samples with detections above Residential
MSCCs.
Groundwater was not encountered during soil excavation activities, and as such, no groundwater characterization was
completed during remediation activities.
Based on the findings during the Initial Abatement Actions and the level of remediation achieved in the soils at the property,
Spangler Environmental and Protocol Sampling Service request that the incident be granted unrestricted regulatory closure.
Figures
Figure 1: Topographic map with 1500-foot radius of the source of the release
Figure 2: Site Map with Area of Excavation
Figure 3: Site Map with Area of Excavation and Soil Analytical Results
Tables
Site History
Summary of Soil Sampling Results
Appendices
Appendix A Soil Disposal Manifests
Liquid Disposal Manifest
Tank Disposal Manifest
Appendix B Copy of all Laboratory Analytical Results and Chain of Custody Records
IAAR:Edge of AuburnProperty Release
7501 Rock Quarry Rd, Garner, NCMay 2022 Project # 20220415
Figure 1:Topo Mapw/ 1500-ft radius
Map Source:USGS
^
Copyright:© 2013 National Geographic Society, i-cubed
Legend
^Site
1,500-foot Radius
³
4338 Bland RoadRaleigh, North CarolinaSpanglerEnvironmental.com(919) 875-4288
0 375 750 1,125 1,500
Feet
IAAR:Edge of AuburnProperty Release
7501 Rock Quarry Rd, Garner, NCMay 2022 Project # 20220415
Figure 2:Site Map withArea of Excavation
Map Source:NC OneMap Aerial ImageryROCKQUARRYROADApproximate locationof CMU septic vault
Legend
Excavation Area
³
4338 Bland RoadRaleigh, North CarolinaSpanglerEnvironmental.com(919) 875-4288
0 10 20 30 40
Feet
IAAR:Edge of AuburnProperty Release
7501 Rock Quarry Rd, Garner, NCMay 2022 Project # 20220415
Figure 3:Site Map withArea of Excavationand Closure Results
!A
!A
!A !A
!A !A!A
!A
!A
SB-4-6.5 6.5ft_BGSDRO 89,800GRO 23,000
W2@8 4ft_BGSAcetone 0.018Jn-Butylbenzene 0.0008Jn-Hexane 0.003JMEK 0.004JMethylene_Chloride 0.056
N4@10 8ft_BGSAcetone 0.014Jn-Hexane 0.002JMEK 0.002JMethylene_Chloride 0.057Naphthalene 0.001J
NE6@8 8ft_BGSAcetone 0.013Jn-Hexane 0.003JMEK 0.001JMethylene_Chloride 0.054Naphthalene 0.001J
E6@8 4ft_BGSAcetone 0.026MEK 0.002J
S4@6 4ft_BGSAcetone 0.017Jn-Hexane 0.001JMEK 0.002J
NW6@8 8ft_BGSAcetone 0.041Chloromethane 0.001Jn-Hexane 0.003JMEK 0.004JMethylene_Chloride 0.076Naphthalene 0.002J
CF@8 8ft_BGSAcetone 0.017Jn-Butylbenzene 0.001Jsec-Butylbenzene 0.001Jn-Hexane 0.003JIsopropylbenzene 0.0006JMEK 0.003JMethylene_Chloride 0.077Naphthalene 0.024n-Propylbenzene 0.0008J1,3,5-Trimethylbenzene 0.002Jo-Xylene 0.001JXylene(total) 0.001JFluorene 0.208J1-Methylnaphthalene 0.550J2-Methylnaphthalene 0.769JPhenanthrene 0.563JPyrene 0.177JAliphatic_C9-C12 8.57JAliphatic_C9-C18 58.6JAliphatic_C19-C36 30.7JAromatic_C11-C22 33.0J
N0@15 15ft_BGSAcetone 0.022Jn-Hexane 0.001JMEK 0.002JMethylene_Chloride 0.041
The northern portion of the excavationwas completed to approximately 15 ft BGS
The southern portion of the excavationwas completed to approximately 8 ft BGS
Legend
Former UST Footprint
Excavation Area
!A Initial Soil Sample
!A Clearance Soil Sample
³
4338 Bland RoadRaleigh, North CarolinaSpanglerEnvironmental.com(919) 875-4288
0 2.5 5 7.5 10
Feet
All results presented in milligrams per kilogram (mg/kg)
Site History – UST System and Other Release Information Revision Date: May 18, 2022 Incident Number and Name: Edge of Auburn Property Release UST ID Number Current / Most-Recent Contents* Previous Contents* Capacity (in gallons) Construction Details** Tank Dimensions Description of Piping and Pumps Date Tank Installed Status of UST*** Release associated with this UST System? 1 Diesel Unknown 500 Single-wall Steel 4x8 Unknown Unknown Removed April 21, 2022 Yes Incident Number Material Released Date of Release Description of Release Unknown Diesel Discovered on April 11, 2022 A previously unidentified UST was discovered during site development activities on April 7, 2022, and a release was identified during initial soil sampling activities on May 11, 2022 *Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non-halogenated or halogenated solvents, etc.** Fiberglass (single- or double-walled), steel (single- or double-walled), steel with FRP (single- or double-walled), steel with liner, other, unknown.*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specifydate)

Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Revision Date: May 18, 2022 Incident Number and Name: Edge of Auburn Property Release

UST ID
Number 1 Facility ID
Number Unknown
Owner Name
(and Contact)
Dates of Operation
(mm/dd/yy to mm/dd/yy)
OCS-HS Lot Option Pool 02
Limited Partnership
Hearthstone Inc
Unknown
Street Address
23975 Park Sorrento, Suite 220
City State Zip Telephone Number
Calabasas CA 91302
-4023 Unknown
Operator Name (and Contact) Dates of Operation
(mm/dd/yy to mm/dd/yy)
Unknown Unknown
Street Address
Unknown
City State Zip Telephone Number
Unknown
Other Incidents Onsite or Commingled/In Close Proximity
Incident
Number N/A Date Incident
Occurred N/A
Name of Responsible Party
for Other Incident
Date Incident
Reported N/A
N/A Date Incident
Closed (i/a) N/A
Street Address
N/A
City State Zip Telephone Number
N/A N/A N/A N/A

Table B-3: Summary of Soil Sampling Results Revision Date: May 18, 2022 Incident Number and Name: Edge of Auburn Property Release Facility ID#: N/A Analytical Method (e.g., VOC by EPA 8260)  TPH (8015) VOC (8260) Contaminant of Concern  DRO GRO Acetone n-Butylbenzenesec-Butylbenzene Chloromethane n-HexaneIsopropylbenzene MEK Methylene Chloride Naphthalene Sample ID Date Collected Source Area Sample Depth Incident Phase SB-4-6.5 04/11/22 UST N End 6.5 LSA 89,800 23,000 --- --- --- --- --- --- --- --- ---W2@8 04/21/22 SW West 4 IAA --- --- 0.018 J 0.0008 J <0.0007 <0.0008 0.003 J <0.0006 0.004 J 0.056 <0.001 CF@8 04/21/22 Floor South 8 IAA --- --- 0.017 J 0.001 J 0.002 J <0.0008 0.003 J 0.0006 J 0.003 J 0.077 0.024 N4@10 04/21/22 SW North 8 IAA --- --- 0.014 J <0.0006 <0.0007 <0.0008 0.002 J <0.0006 0.002 J 0.057 0.001 J N0@15 04/21/22 Floor North 15 IAA --- --- 0.022 J <0.0006 <0.0007 <0.0008 0.001 J <0.0006 0.002 J 0.041 <0.001 NE6@8 04/21/22 SW NE 8 IAA --- --- 0.013 J <0.0006 <0.0007 <0.0008 0.003 J <0.0006 0.001 J 0.054 0.001 J NW6@8 04/21/22 SW NW 8 IAA --- --- 0.041 <0.0007 <0.0008 0.001 J 0.003 J <0.0007 0.004 J 0.076 0.002 J E6@8 04/21/22 SW East 4 IAA --- --- 0.026 <0.0006 <0.0007 <0.0008 <0.0008 <0.0006 0.002 J <0.001 <0.001 S4@6 04/21/22 SW South 4 IAA --- --- 0.017 J <0.0006 <0.0007 <0.0008 0.001 J <0.0006 0.002 J <0.001 <0.001 Minimum Reporting Limit (mg/kg) 2,820 279 0.002 - 0.003 0.006 - 0.007 0.007 - 0.008 0.0008 - 0.0009 0.0008 - 0.0010 0.0006 - 0.0007 0.0008 - 0.0010 0.001-0.002 0.001 Soil to Groundwater MSCC (mg/kg) N/A N/A 24 2.4 2.2 0.014 N/A 1.3 16 0.023 0.2 Residential MSCC (mg/kg) N/A N/A 14,000 782 1,560 51 N/A 1,560 9,380 93.8 5.5 Industrial/Commercial MSCC (mg/kg) N/A N/A 210,000 11,600 23,300 251 N/A 23,300 140,000 1,400 27 MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface All results reported in milligrams per kilogram (mg/kg)
Table B-3: Summary of Soil Sampling Results (continued) Revision Date: May 18, 2022 Incident Number and Name: Edge of Auburn Property Release Facility ID#: N/A Analytical Method (e.g., VOC by EPA 8260)  VOC (8260) SVOC (8270) Contaminant of Concern  n-Propylbenzene 1,3,5-Trimethylbenzene o-Xylene Xylene (total) All other VOCs Fluorene 1-Methylnaphthalene 2-Methylnaphthalene Phenanthrene Pyrene All other SVOCs Sample ID Date Collected Source Area Sample Depth Incident Phase W2@8 04/21/22 SW West 4 IAA <0.0007 <0.0007 <0.0006 <0.0006 --- <0.157 <0.130 <0.122 <0.255 <0.164 --- CF@8 04/21/22 Floor South 8 IAA 0.0008 J 0.002 J 0.001 J 0.001 J --- 0.208 J 0.550 J 0.769 J 0.563 J 0.177 J --- N4@10 04/21/22 SW North 8 IAA <0.0007 <0.0007 <0.0007 <0.0007 --- <0.167 <0.138 <0.130 <0.272 <0.175 --- N0@15 04/21/22 Floor North 15 IAA <0.0007 <0.0007 <0.0006 <0.0006 --- <0.154 <0.128 <0.120 <0.251 <0.162 --- NE6@8 04/21/22 SW NE 8 IAA <0.0007 <0.0007 <0.0006 <0.0006 --- <0.155 <0.128 <0.121 <0.252 <0.162 --- NW6@8 04/21/22 SW NW 8 IAA <0.0008 <0.0008 <0.0007 <0.0007 --- <0.187 <0.155 <0.146 <0.304 <0.196 --- E6@8 04/21/22 SW East 4 IAA <0.0007 <0.0007 <0.0006 <0.0006 --- <0.159 <0.132 <0.124 <0.259 <0.167 --- S4@6 04/21/22 SW South 4 IAA <0.0007 <0.0007 <0.0006 <0.0006 --- <0.156 <0.129 <0.121 <0.253 <0.163 --- Minimum Reporting Limit (mg/kg) 0.0007 - 0.0008 0.0007 - 0.0008 0.0006 - 0.0007 0.0006 - 0.0007 var 0.154 -0.187 0.128 -0.155 0.120 -0.146 0.251 -0.304 0.162 -0.196 var Soil to Groundwater MSCC (mg/kg) 1.4 6.6 6 6 var 55 0.054 1.5 64 210 var Residential MSCC (mg/kg) 1,560 156 3,120 3,120 var 625 22.8 62.5 469 469 var Industrial/Commercial MSCC (mg/kg) 23300 2,330 46,700 46,700 var 9,340 112 934 7,000 7,000 var MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface All results reported in milligrams per kilogram (mg/kg)
Table B-3: Summary of Soil Sampling Results (continued) Revision Date: May 18, 2022 Incident Number and Name: Edge of Auburn Property Release Facility ID#: N/A Analytical Method (e.g., VOC by EPA 8260)  VPH MADEP EPH MADEP Contaminant of Concern  Aliphatic C5-C8 Aliphatic C9-C12 Aromatic C9-C10 Aliphatic C9-C18 Aliphatic C19-C36 Aromatic C11-C22 Sample ID Date Collected Source Area Sample Depth Incident Phase W2@8 04/21/22 SW West 4 IAA <3.37 <12.7 <1.72 <11.4 <15.0 <17.6 CF@8 04/21/22 Floor South 8 IAA <1.70 8.57 J <0.875 58.6 J 30.7 J 33.0 J N4@10 04/21/22 SW North 8 IAA <1.60 <6.01 <0.821 <12.1 <16.0 <18.6 N0@15 04/21/22 Floor North 15 IAA <1.48 <5.51 <0.754 <11.1 <14.8 <17.2 NE6@8 04/21/22 SW NE 8 IAA <3.30 <12.4 <1.70 <11.2 <14.8 <17.3 NW6@8 04/21/22 SW NW 8 IAA <1.79 <6.68 <0.913 <13.4 <17.9 <20.6 E6@8 04/21/22 SW East 4 IAA <1.52 <5.69 <0.778 <11.4 <15.1 <17.6 S4@6 04/21/22 SW South 4 IAA <1.49 <5.56 <0.760 <11.2 <14.9 <17.2 Minimum Reporting Limit (mg/kg) 1.48 -3.37 5.51-12.7 0.754 - 1.7211.1 -13.4 14.7 -17.9 17.1 -20.6 Soil to Groundwater MSCC (mg/kg) N/A N/A N/A N/A N/A N/A Residential MSCC (mg/kg) N/A N/A N/A N/A N/A N/A Industrial/Commercial MSCC (mg/kg) N/A N/A N/A N/A N/A N/A MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface All results reported in milligrams per kilogram (mg/kg)

Table B-6: Contiguous Property Owners/ Occupants
Revision Date: May 18, 2022
Incident Number and Name: Edge of Auburn Property Release
Facility ID#: N/A

Tax Parcel
Number/
Map ID
Owner/ Occupant Name
(Last, First MI)
Address
Physical Mailing
1740165280 Bailey, Deborah R &
Roberts, Patrick G 7633 Rock Quarry Road 7620 Rock Quarry Road
Raleigh, NC 27610-9632
1740068636 Mitchiner, Christopher R 7605 Rock Quarry Road 7605 Rock Quarry Road
Raleigh, NC 27610-9632
1740072319 Deacon Holdings LLC
Carlino, Peter N 0 Rock Quarry Road 2505 Haymow Ct
Charlotte, NC 28270-0749
1740287482 OCS-HS Lot Option Pool 01 LP
Hearthstone Inc 7401 Rock Quarry Road 23975 Park Sorrento Ste 220
Calabasas CA 91302-4023

TRIANGLE AREA EARTH
CORPORATION
Certificate of Disposal
NCDEQ Permit SRU600082
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
Triangle Area Earth Corporation, operating under Permit SRU600082, hereby
acknowledges the receipt of 188.91 tons of soil contaminated with petroleum
hydrocarbons and will properly execute the disposal of this soil in the prescribed manner
set forth by the North Carolina Department of Environmental Quality, Division of Waste
Management in accordance with the requirements of SRU600082.
CLIENT
GENERATOR
TRANSPORTER
DATE(S) ACCEPTED
CERTIFICATION BY
TRIANGLE AREA
EARTH CORPORATION
Herr, Inc.
P.O. Box 2345
Whiteville, NC 28472
Hearthstone, Inc.
23975 Park Sorento Ste. 220
Calabasas, CA 91302-4023
Site: Edge of Auburn Project
17512 Old Baucom Road
Garner, NC 27529
Herr, Inc.
P.O. Box 2345
Whiteville, NC 28472
April 21, 2022
H. Ruffin Denton 4/27/2022
Printed Name Date
TRIANGLE AREA EARTH
CORPORATION
(91 9) 980-6200
336 Denton Ln, Zebulon, NC 27597
Manifest [e-mail]
NCDEQ Permit SRU600082
MA$1FEST
WASTE DESCRIPTION Petroleum-Contaminated Soil MANIFEST NUMBER
EPA WASTE CLASS/FICA TION Non-Hazardous DA TE
DOT HAZARD CLASS Non-Regulated GROSS {LCS)
CONTAMINANT(S)
-fr 1.. f...,.... I t>J/
~ ho!ea ""-Co""~s. 1; ~ rARE(LesJ
TRUCK 12 ('A. L/ <{ NET {LBS)
TONS
GENERATOR TRANSPORTER
NAME /d£A(t:["J.(,, 1ft> ,-JC: / r-l C.. NAME
ADDRESS J 3. f7') ?A12.. k ~t2c,,,vJ1)/~'}<. 2:z.r1110DRESS
U[g Wdf e.A 113vz~ V,n.3
SITE CONSULT ANT
OI
1/,/2 I /2.0-z-c.-
b-3,3&)
c2qlt2.0
J.3 1'2bO
l G,. %3~
==============
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
f 2~ 0 c A.1b,, CA-(11r.-e.c-t"
I 257 z.. 0/V [34 Ji v ....,..._/4L
{; Al, N U,. c1 L-~
.5 6 5 5 /l1 A II 1-f 1 f>J J"("
tJh d~ v d ,!.-£-) '--:l rtf11.
k? lit>YfD tfo~01
INSPECTED AND ACCEPTED BY Triangle Area
Earth
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
MA~IFEST
WASTE DESCRIPTION Petroleum-Contaminated Soil
EPA WASTE CLASS/FICA TION Non-Hazardous
DOT HAZARD CLASS Non-Regulated
-# "L ,C..,...I o : I
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST NUMBER
DATE lf lzr I pYZ,1-,
GROSS(LCS)
~ Lo ,;/ I CONTAMINANT(S) #fu tc,.:_ A.-\-A µ..../\.4i TARE(LBS)
~~o
Jg,~00
,.j '-l ,3 (/) TRUCK KM 3J
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME
ADDRESS
PHONE
:J3f75" f'lttL k ,J.,r,,,.,& £; l<-2
CAt«baso..J Ca 'I/Jtn._.c..(.,-z.5
£ ~r.&-(7 r-A,, Iv r c-t1,p)-ed-
l 70 1... 6 /T) OA,A .. gv.... B ~
teMCl'2. tJ <-
NAME
ADDRESS
NAME
ADDRESS
NET(LBS)
TONS 17 , l8
f PA :11J µf l~/) V ,,,.,.,, ,v ....,.....,...,\o,. I )('°~cit._..... ll..t ... , LLC)
'f/4.A.,j ~ "Jc..r
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
lf/;2.J 12.2. D tE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
MA~IFEST
WASTE DESCRIPTION Petroleum-Contaminated Soil
EPA WASTE CLASS/FICA TION Non-Hazardous
DOT HAZARD CLASS Non-Regulated
ps ,z_ f"__.. I o; I
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST NUMBER D3
DATE
GROSS{LI:S)
CONTAMINANT(S) ~l,oh,.o_____ bzsm """wl 1i A TARE{LBS}
S~3CO
~)-lq~C)
TRUCK NET(LBS} 3 \.3&?
TONS \ 5, bg
GENERATOR TRANSPORTER
NAME 1-/l.>.-IZ-{k, 51e1_.e_. I AJ <-NAME
ADDRESS ;23 f~ fe,,tk ~ .S:c~.,J., Ct._1_5.1* 'l'ZY ADDRESS
&kkc5A) (,4( fl3~L-'{i>z_'}
J
SITE CONSULTANT
NAME (JI,(__ e ➔ A.,t,v,._ pk>'-(.£ • .+ fl J
ADDRESS /71;7. o Id &vco,....,, ((2
&/nLNj.;(-N'-
NAME _5fe..v;0 If,. J , Ao> l'A-L,Jc._ I
ADDRESS ~J§lWQ:'"•Av c.,.,1 .. u <Le)
CLIENT CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
[phone]
336 Denton ln, Zebulon, NC 27597
[e-mail]
MANIFEST
WASTE DESCRIPTION Petroleum-Contaminat~d Soil MANIFEST N UMBER e>t..f
EPA WASTE CLASS/FICA TION Non-Hazardous DATE v/2r~
DOT HAZARD CLASS Non-Regulated GROSS(LCS) 4>CJ,D8t> tJ t. ~, 0 :1
CONTAMINANT(S) ~ ~ k ..,.,._ ~-i;;;;: AiJJ. fart TARE(LBS) PB,0®
TRUCK i<M z_ L
GENERATOR
NAME (-k112 ft.-TL £bu fe) L
ADDRESS )Jf'/( f'¥k 't<,c;,l-/4.,/)-c_,, Z/..:>
Cc 111,,u,s t,q-r 13.., 1. -C/pi3 I
SITE
NAME { ~ t>; &ku0r <?.v)""~-+
ADDRESS IW z D /I) &✓ ... t>...,_ fl..!.
CLIENT
NAME
ADDRESS
PHONE
C~v t(fo-/V l
'Jo 1 5 tkd_, f-lsb.-, £'I
/JI,;'}. vf/k cJ' 2R<f 72.
{qVDJ totfb~tfl
NET(LBS)
TRANSPORTER
NAME
ADDRESS
CONSULTANT
NAME
ADDRESS
CERTIFICATION
TONS
.3 q ,tleD
Jq . ~Q
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
~
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MAti,IFEST
WASTE DESCRIPTION Petroleum-Contaminat~d Soil MANIFEST NUMBER
EPA WASTE CLASS/FICA T!ON Non-Hazardous DATE
DOT HAZARD CLASS Non-Regulated GROSS(LCS)
Ji -zFw.J-.,J o;J
CONTAMINANT(S) ?cie ,e...>-cl\~~ 'i5 .·,-TARE(LBS)
6i280
d1,12l)
3q.5w TRUCK
GENERATOR
SITE
CLIENT
NAME
ADDRESS
PHONE
$1 5 fVIAtl½ky 5+-
l,J/,~4 u~lk.-tJC-Ji<(P
810] CPLJ-0:24,/J
NET(LBS)
I
TONS rq,1?5
TRANSPORTER
CONSULTANT
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
Earth C
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST
WASTE DESCRIPTION Petroleum-Contaminat~d Soil MANIFEST NUMBER
EPA WASTE CLASSIFICATION Non-Hazardous DATE
DOT HAZARD CLASS Non-Regulated GROSS(U:S}
CONTAMINANT(S) TARE(LBS)
TRUCK NET(LBS)
TONS
GENERATOR TRANSPORTER
NAME H,~,,..u.. * ,J.(. I,., c... NAME
ADDRESS ;2 3,f7S'° e~I(" ~<.M7 I ,S.,a ~ 1:2,,c> ADDRESS
CA. \,,.\,2 %; ) c er 1 '1130-z. -'-/i> '23
SITE CONSULTANT
NAME (~)',-~ l'L~-.>f .I' en,j._d°
ADDRESS /?{11.. <>/J di,v,~ ~
U,M,,1/_,4-ff I.-
CLIENT CERTIFICATION
64,340
~1,~D
.3(o~o
I i.2..\
INSPECTED AND ACCEPTED BY Triangle Area
NAME
ADDRESS
PHONE
E
3°3 5 tt1AAbb1 K
Wh',\c.."~ \\<.. ,.,"' ;.rf 1'2-
ltj; l)) ta4t, --:J&c 1
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
MAl';JIFEST
WASTE DESCRIPTION Petroleum-Contaminat~d Soil
EPA WASTE CLASS/FICA TION Non-Hazardous
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST NUMBER 07
DATE
DOT HAZARD CLASS Non-Regulated GROSS (LCS) ~~,DJD
~J,(b) CONTAMINANT(S)
JI 2. ~J oi I
Mro\<:.n,,... Cox.\c""' t ~ 7rl TARE (LBSJ
TRUCK fJ£ 4 5 NET (LBS)
GENERATOR TRANSPORTER
NAME &dl 5/b,.s~ /f.J <.. NAME
ADDRESS llf?r fMJ< ~ I $l:.)c.. 'iV> ADDRESS
Cala.h~l"-~ c~J (/13()ZA'i>Z-.:3
SITE
NAME £""4= o-i A..>Lu.... l1'>)<,k+-
ADDR£ss / Zfl 2 ~Jc! &vu-,-.., ~
{,,,w_,v,£L.. #L
CLIENT
CONSULTANT
CERTIFICATION
TONS
3:811$
J 9, ~5
NAME
ADDRESS
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
PHONE
'"p) J /"'t,1..1l-h', Jr
µJ; '4-v,11-< tf' ,2W7Z
010) tL,4oau(7 ~~q~l
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST
WASTE DESCRIPTION Petroleum-Contaminatfd Soil MANIFEST NUMBER
EPA WASTE CLASS/FICA TION Non-Hazardous DATE Wz!/z.vz2-
DOT HAZARD CLASS Non-Regulated
#: z.. F._./L-1 ",: '
CONTAMINANT(S) Pt kt>~ b,.,c \o::;,.:.c,"",dct S-i'
GROSS (LCS) ~g, 0'30
TARE(LBS) a8 ,s{;o
TRUCK RM 3,
GENERATOR
SITE
NAME iJy-er AvlJ✓-a,+c+-+-
ADDREss J_7 J7 2.. ~IJ 4& '-q~ /).tt..
t,-o,~,vl
CLIENT
NAME
ADDRESS
PHONE
NET {LBS} 'i(>~J 0
TONS o/0, l l
TRANSPORTER
NAME
ADDRESS
CONSULTANT
NAME ~W £'Av1~e-f
ADDRESS (fl,~ t!...-oJ.;._, LLtj)
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
WASTE DESCRIPTION
EPA WASTE
CLASS/FICA TION
DOT HAZARD CLASS
CONTAMINANT(S)
TRUCK
GENERATOR
NAME
ADDRESS
SITE
NAME
ADDRESS
CLIENT
NAME HERR, Inc.
MANIFEST
Petroleum-Contaminated Soil
Non-Hazardous
Non-Regulated
-1P2 [l}f.\ o; l
~M44 .
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST NUMBER c,q
DATE Ll/2-1,/22
GROSS(LBS) ~3,0t;O
TARE(LBS) dBt,rt"JO
NET(LBS) 43;;340
TONS Jl~ b=l
TRANSPORTER
CONSULTANT
CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
Earth Corporation:
ADDRESS P.O. Box 2345
Whiteville, NC 28472 ~~ \l.~,uffi,o.~ok SL\.2.L 2.2 ...
PRINTED AME DA TE
TRIANGLE AREA EARTH
CORPORATION
Manifest
NCDEQ Permit SRU600082
MA~IFEST
WASTE DESCRIPTION Petroleum-Contaminat~d Soil
EPA WASTE CLASS/FICA TION Non-Hazardous
DOT HAZARD CLASS Non-Regulated
CONTAMINANT(S) # 2,.. 6.eJ <;;>: /
GENERATOR
[phone]
336 Denton Ln, Zebulon, NC 27597
[e-mail]
MANIFEST NUMBER JD
DA TE '-I /z, /Zdz.:L..
GROSS (LCS) 10, DbD
TARE(LBS) c2'i, b8D
NET(LBS} 'ti ,380
TONS do. to q
TRANSPORTER
NAME /le.edL.. J.Jaw<.. Iv'-NAME
ADDRESS 2.Jf 7 L ,~µc;. 'bf'~ J j,,,7' 2'Z-P ADDRESS
l:A/c.hc:.$4., C.A: f, Jo 2-l/.;,-z.3
SITE CONSULTANT
CLIENT CERTIFICATION
INSPECTED AND ACCEPTED BY Triangle Area
PHONE
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck ~ 44 EW
Customer ----1,,..~~er~c _____ _
.Transporter !(~fvj ti'l9ch ~B
Job ~ J ilh~Lr'.\
NORTH CAROLIN.A
PUBLIC WElGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SlGNED
NOF<TH CAROLINA
STER
E 30, 2022
\\IQ~,. Rll.\JmfHl5-ON "*
NCDEQ Permit SRU600082
[phone]
. 434 Denton Ln, Zebulon, NC 27597
\
63380 lb !3R
,)4/211t'22 11 ! 08.an"t
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
RiB EW
J/-e(C
~
.Transporter ~ t-\ 1£l2~ ~
Job ~e ~ 01uro
NORTH CAROLIN.A
PUBLIC WEIGHMASlER
LICENSE EXPIRES JUNE 30, 2022
LAURABUCHANAN 31739
INVALID UNLESS SIGNED
NOftTH CAROLINA ,ueuc W!tGHMASTER
NE 30, 2022
bllu~U!ROH 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
6.3220 lb GR
04/21/22 i 1: 1 i.,.jm
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 44267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
l{&:45 EW
,:te,<'f
.Transporter Ale bcew
Job ~e., ~ ili)ou Ci\
NORTH CAROLIN.A
PUBLIC WEIGHMASlER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
INVALID UNLESS SIGNED
NOf<TH CAROLINA
T!R
30,2022
llt'IMD-1111:.~1 ON 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
s·noo lt; GR
1}4/21/22 11: 19a!i1
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
{sM2,2, EW
,-krs:
"-..
.Transporter @4-M \t12d:1~
J0b c%e ,p /.L~ucfl
NORTH CAROLIN.A
PUBLIC WEIGHMA8TER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
NOFtTH CAROLINA
.-.. -TER
0,2022
IM-.OI~~ 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
b8i)80 1 t, GR
04/2i/22 11:29am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNEO
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck RM 4 Y EW
Customer _ ..... \-\...J.l,,.,e .. S\~-----
.Transporter Ri M TI:ud: I ni3 d&-di Oon~,n Job
NOf.tTH CAROLINA NORTH CAROUI-I.A
PUBLIC WEIGHMASTER
LICENSE EXP1RES JUNE 30. 2022
LAURA BUCHANAN 31739
..----,j■aa TER
iNvAiJDUNLESSSlGNED
0,2022
4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
69280 lb SR
04/21/22 i2: 24Pli1
5
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'4267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
. Transporter ----1.N~e.:L.l,b..,L.c~w:1..1..:2..;;:.._ __ _ •
Job ~ cl Au-Ovrn
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30. 2022
LAURA BUCHANAN 31739
INVALID UNLESSSlGNED
MOFtTH CAROLINA •ueuc W!IGHMAST!R
NE 30, 2022
TOH4'2"
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
64340 lb GR
04/21/22 12~37Pm
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4"267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET Ntl{S
Truck
Customer ----1\jt...J.J,,,.e.C.( ____ _
.Transporter ~ehren2-
Job z-g, <if -4hmf\
NORTH CAR.OUN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SlGNED
NOl'<TH CAROLINA
!R
0,2022
!IP\~IQ.ll!mullTJn ·11...-n-.Aa..1 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
66020 lb SF.
04/21/22 Ol:51Pm
1
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNEO
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
Job
Rfv133 EW
1+err
NORTH CAROUf-J.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURABUCHANAN 31739
INVALID UNLESS SIGNED
NOF<TH CAROLINA
!R
0,2022
,u.,t,,l~l"il..l 4'266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
t,9080 lb GR
04/21/22 02: 03Pm
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 44267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck RMyy EW
Customer rdex C
.Transporter Rf tYJ Trve-\;:;,\@§
Job Ed&' a£ ~£ l\l'i
NORTH CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
NOFtTH CAROt.tNA
INAIJD UNLESS SlGNED
ER
0,2022 :,~EID~"*
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
73060 lb GR
04/21/22 02: 14F-m
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 44267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck RM2.2. EW
Customer --..k.t1-1.C:..1.C,..l,.C ____ _
.Transporter R? M Tro c.k 1@3
Job E<l:Je eR. {)_t.d:lJ.1rn
NORTH CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURA BUCHANAN 31739
INVALID UNLESS SIGNED
MOf<TH CAROLINA ...----....... STER
E 30, 2022
~~ON 4"266
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
IO
700W lb t3R
04/21/22 02:31Pfit
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
RMYL\@
l~eK
.Transporter g~ M. I NK:k.ii:g
Job ~ J Avbucn
NORTH ~OUN.A
PUBUCWEIGHMA81'ER
LICENSE EXPIRES JUNE 30. 2022
LAURABUCHANAN 31739
1NVALD UNLESS SIGNED
NOrtTH CAROt..tNA
STER
E 30, 2022
1n1.1>1cnTON 4'2"
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
29720 1 t, t3F'.
04/21/22 11; l6.:3m
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
.Transporter ~ettef\:Z.
Job £~e o9 Aoh0\f\
NORTH CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
IAURABUCHANAN 31739
iNVALib UNLESSSlGNED
NOf<TH CAROLINA
tGHNAST!R
E 30, 2022
'"lff-l~III ON 4'2t&
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
27920 lb 13R
04/21,22 11.34am
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Tri.Jck RMJ3 @
Customer _H~er;),,,Jc ______ _
Transporter R~ M JJ:vc\::u'.l~
Job Jcee J l11~0:~
NORTH CAROLIN.A
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
,msuc~739
~UNLESS SIGNED
NOrtTH CAROLINA •ueuc W!tGHMASTER
titlN8! IXP,~ES JUNE 30, 2022
KOWARD RUFFIN DENTON 4'2"
INVALID UMU:SS SIGN!D
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
28860 lb GR
04/2il22 :i..2~ 48Pfil
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL 4'267
INVALID UNLESS SIGNED
TRIANGLE AREA EARTH
CORPORATION
WEIGHT TICKET
Truck
Customer
~c}I\/\ T~~'y . Transporter _.1..r::::: __ ,_ y \.-:...~....;;;;;~ ....... :=.....'-
Job Ei;e , d~ 4u6ufl\
NORTii CAROLIN.A
PUBUCWEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
LAURABUCHANAN 31739
iNvAiJD UNLESSSlGNED
NOF<TH CAROLINA
-•u•Lte W!IGHMASTER es UNE 30, 2022 ,,~~)N "*
NCDEQ Permit SRU600082
[phone]
434 Denton Ln, Zebulon, NC 27597
28680 lb GR
04/21/22 01:QQpm
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
PHILLIP MARSHALL ~267
INVALID UNLESS SIGNED

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/15/2022
Spangler Environmental Cal Rieder
4338 Bland Road Raleigh, NC, 27609
Ref: Analytical Testing
Lab Report Number: 22-103-0004 Client Project Description: Edge of Auburn
Dear Cal Rieder:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/13/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 12
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-103-0004
Page 2 of 12
Report Number:
Sample Summary Table
Client Project Description:
22-103-0004
Edge of Auburn
Lab No Client Sample ID Matrix Date Collected Date Received
04/11/2022 16:30Solids 98426 SB-4-6.5 04/13/2022 10:43
Page 3 of 12
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-103-0004
Report Limit
Project:Edge of Auburn
V 98426SB-4-6.5
89800 04/14/2022 15:118015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 2820
23000 04/14/2022 06:388015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 279
17.3 04/14/2022 17:15SW-DRYWT Moisture %
Page 4 of 12

Client: Spangler Environmental CASE NARRATIVE
Project: Edge of Auburn Lab Report Number: 22-103-0004
Date: 4/15/2022
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 98426 (SB-4-6.5) Analyte: o-Terphenyl
QC Batch No: V17489/V17453 Surrogate(s) was flagged for recovery outside QC limits in this project sample. This sample was diluted 100x due
to high amounts of target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO Sample 98426 (SB-4-6.5) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V17431/V17430 Surrogate(s) was flagged for recovery outside QC limits in this project sample. This sample was re-analyzed for
verification, and/or dilution of target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.

Page 5 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-103-0004
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/13/2022
Edge of Auburn
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:SB-4-6.5
98426 Matrix:
4/11/2022 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.3 %Moisture 1 04/14/22 17:15 SW-DRYWTZSV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 6 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-103-0004
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/13/2022
Edge of Auburn
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:SB-4-6.5
98426 Matrix:
4/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V17453 04/14/22 08:27
89800 mg/Kg - dry 2820 6050Diesel Range Organics (C10-C28)100 04/14/22 15:11 V17489JLK
8015C DROSurrogate: OTP Surrogate 0 *Limits: 31-123%04/14/22 15:11100 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V17430 04/13/22 08:00
23000 mg/Kg - dry 279 676Gasoline Range Organics (C6-C10)5000 04/14/22 06:38 V17431TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 173 *Limits: 50-137%04/14/22 06:385000 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 7 of 12
Quality Control Data
22-103-0004Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V17489QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V17453
Associated Lab Samples: 98426
LRB-V17453 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/14/22 14:0710.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
04/14/22 14:07OTP Surrogate (S)62.1 31-123
LCS-V17453 LCSD-V17453Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
60.3 90.493.562.466.7mg/KgDiesel Range Organics (C10-C28)46-126 3.4 20
61.666.9OTP Surrogate (S)31-123
Page 1 of 3Date:04/15/2022 11:50 AM
Page 8 of 12
Quality Control Data
22-103-0004Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V17431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V17430
Associated Lab Samples: 98426
LRB-V17430 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/13/22 12:175.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
04/13/22 12:17a,a,a-Trifluorotoluene (S)123 50-137
LCS-V17430Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10451.950.0mg/KgGasoline Range Organics (C6-C10)41-138
122a,a,a-Trifluorotoluene (S)50-137
V 98302-MS-V17430 V 98302-MSD-V17430Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
43.4 86.840.850.050.0<2.07mg/KgGasoline Range Organics (C6-C10)81.6 41-138 6.1 34
108a,a,a-Trifluorotoluene (S)106 50-137
Page 2 of 3Date:04/15/2022 11:50 AM
Page 9 of 12
Quality Control Data
22-103-0004Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
Dry Weight Determination
SW-DRYWT
V17490QC Analytical Batch:
Analysis Method:
Analysis Description:
V 97952-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/14/22 17:151.117.818.0%Moisture
V 98426-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/14/22 17:152.217.717.3%Moisture
Page 3 of 3Date:04/15/2022 11:50 AM
Page 10 of 12
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-103-0004
Spangler Environmental
01191
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.9 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:04/13/2022 11:54:37
Special precautions or instructions included?
Comments:
Page 11 of 12
Page 12 of 12

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/17/2022
Spangler Environmental Cal Rieder
4338 Bland Road Raleigh, NC, 27609
Ref: Analytical Testing
Lab Report Number: 22-115-0003 Client Project Description: Edge of Auburn
Dear Cal Rieder:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/22/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 116
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-115-0003
Page 2 of 116
Report Number:
Sample Summary Table
Client Project Description:
22-115-0003
Edge of Auburn
Lab No Client Sample ID Matrix Date Collected Date Received
04/21/2022 16:00Solids 99475 W2@8 04/22/2022 16:50
04/21/2022 16:05Solids 99476 CF@8 04/22/2022 16:50
04/21/2022 16:10Solids 99477 N4@10 04/22/2022 16:50
04/21/2022 16:15Solids 99478 NO@15 04/22/2022 16:50
04/21/2022 16:20Solids 99479 NE6@8 04/22/2022 16:50
04/21/2022 16:25Solids 99480 NW6@8 04/22/2022 16:50
04/21/2022 16:30Solids 99481 E6@8 04/22/2022 16:50
04/21/2022 16:35Solids 99482 S4@6 04/22/2022 16:50
Page 3 of 116
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-115-0003
Report Limit
Project:Edge of Auburn
V 99475W2@8
J0.018 04/26/2022 18:248260DAcetonemg/Kg - dry 0.002
J0.0008 04/26/2022 18:248260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.003 04/26/2022 18:248260Dn-Hexane mg/Kg - dry 0.0008
J0.004 04/26/2022 18:248260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.056 04/26/2022 18:248260DMethylene Chloride mg/Kg - dry 0.001
18.6 04/29/2022 11:32SW-DRYWT Moisture %
V 99476CF@8
J0.017 04/26/2022 18:528260DAcetonemg/Kg - dry 0.002
J0.001 04/26/2022 18:528260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.002 04/26/2022 18:528260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.003 04/26/2022 18:528260Dn-Hexane mg/Kg - dry 0.0008
J0.0006 04/26/2022 18:528260DIsopropylbenzenemg/Kg - dry 0.0006
J0.003 04/26/2022 18:528260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.077 04/26/2022 18:528260DMethylene Chloride mg/Kg - dry 0.001
0.024 04/26/2022 18:528260DNaphthalenemg/Kg - dry 0.001
J0.0008 04/26/2022 18:528260Dn-Propylbenzene mg/Kg - dry 0.0007
J0.002 04/26/2022 18:528260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 04/26/2022 18:528260Do-Xylene mg/Kg - dry 0.0006
J0.001 04/26/2022 18:528260DXylene (Total)mg/Kg - dry 0.0006
J0.208 04/29/2022 17:298270EFluorenemg/Kg - dry 0.155
J0.550 04/29/2022 17:298270E1-Methylnaphthalene mg/Kg - dry 0.128
J0.769 04/29/2022 17:298270E2-Methylnaphthalene mg/Kg - dry 0.121
J0.563 04/29/2022 17:298270EPhenanthrenemg/Kg - dry 0.252
J0.177 04/29/2022 17:298270EPyrenemg/Kg - dry 0.162
J58.6 05/03/2022 22:49MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 11.1
J30.7 05/03/2022 22:49MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 14.7
J33.0 05/03/2022 22:49MADEP-EPH Aromatic C11-C22 mg/Kg - dry 17.1
J8.57 04/26/2022 17:45MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 6.40
17.6 04/29/2022 11:32SW-DRYWT Moisture %
V 99477N4@10
J0.014 04/26/2022 19:208260DAcetonemg/Kg - dry 0.003
J0.002 04/26/2022 19:208260Dn-Hexane mg/Kg - dry 0.0009
J0.002 04/26/2022 19:208260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
0.057 04/26/2022 19:208260DMethylene Chloride mg/Kg - dry 0.001
J0.001 04/26/2022 19:208260DNaphthalenemg/Kg - dry 0.001
Page 4 of 116
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-115-0003
Report Limit
Project:Edge of Auburn
V 99477N4@10
23.6 04/29/2022 11:32SW-DRYWT Moisture %
V 99478NO@15
J0.022 04/26/2022 19:478260DAcetonemg/Kg - dry 0.002
J0.001 04/26/2022 19:478260Dn-Hexane mg/Kg - dry 0.0008
J0.002 04/26/2022 19:478260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.041 04/26/2022 19:478260DMethylene Chloride mg/Kg - dry 0.001
17.3 04/29/2022 11:32SW-DRYWT Moisture %
V 99479NE6@8
J0.013 04/26/2022 20:158260DAcetonemg/Kg - dry 0.002
J0.003 04/26/2022 20:158260Dn-Hexane mg/Kg - dry 0.0008
J0.001 04/26/2022 20:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.054 04/26/2022 20:158260DMethylene Chloride mg/Kg - dry 0.001
J0.001 04/26/2022 20:158260DNaphthalenemg/Kg - dry 0.001
17.5 04/29/2022 11:32SW-DRYWT Moisture %
V 99480NW6@8
0.041 04/26/2022 20:438260DAcetonemg/Kg - dry 0.003
J0.001 04/26/2022 20:438260DChloromethanemg/Kg - dry 0.0009
J0.003 04/26/2022 20:438260Dn-Hexane mg/Kg - dry 0.001
J0.004 04/26/2022 20:438260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.001
0.076 04/26/2022 20:438260DMethylene Chloride mg/Kg - dry 0.002
J0.002 04/26/2022 20:438260DNaphthalenemg/Kg - dry 0.001
31.7 04/29/2022 11:32SW-DRYWT Moisture %
V 99481E6@8
0.026 04/27/2022 13:138260DAcetonemg/Kg - dry 0.002
J0.002 04/27/2022 13:138260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
19.8 04/29/2022 11:32SW-DRYWT Moisture %
V 99482S4@6
J0.017 04/27/2022 13:418260DAcetonemg/Kg - dry 0.002
J0.001 04/27/2022 13:418260Dn-Hexane mg/Kg - dry 0.0008
J0.002 04/27/2022 13:418260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
18.0 04/29/2022 11:32SW-DRYWT Moisture %
Page 5 of 116

Client: Spangler Environmental CASE NARRATIVE
Project: Edge of Auburn Lab Report Number: 22-115-0003
Date: 5/17/2022
Massachusetts EPH Method MADEP-EPH Analyte: Aliphatic C9-C18 QC Batch No: V18269/V18369
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 40300ug/kg which calculates to a recovery of 67.2% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V18269/V18369 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
37600 ug/kg which calculates to a recovery of 62.7% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18 QC Batch No: V18371/V18369
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 41500ug/Kg which calculates to a recovery of 69.2% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V18371/V18369 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was
39600ug/Kg which calculates to a recovery of 66.1% which is within the acceptable recovery range. Analyte: Aliphatic C9-C18 QC Batch No: V18459/V18369
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 40300ug/Kg which calculates to a recovery of 67.1% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V18459/V18369 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 35800ug/Kg which calculates to a recovery of 59.7% which is within the acceptable recovery range.
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 99590
Analyte: 2,4-Dinitrophenol QC Batch No: V18184/V18088 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 99590 Analyte: 3,3`-Dichlorobenzidine
QC Batch No: V18184/V18088 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 29.6 ug/kg which calculates to a recovery of 1.7% which is below the acceptable recovery range. Sample 99590 Analyte: 3,3`-Dichlorobenzidine
Page 6 of 116

QC Batch No: V18184/V18088
Analyte did not recover during prep.
Sample 99590 Analyte: 3-Nitroaniline
QC Batch No: V18184/V18088 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 99590
Analyte: 4-Nitroaniline QC Batch No: V18184/V18088
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 28.9 ug/kg which calculates to a recovery of 1.7% which is below the acceptable recovery range.
Sample 99481 (E6@8)
Analyte: Benzoic Acid QC Batch No: V18743/V18145
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 99481 (E6@8)
Analyte: Pyridine QC Batch No: V18743/V18145 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 99481 (E6@8) Analyte: Pyridine
QC Batch No: V18743/V18145 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 7 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.6 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.018 J mg/Kg - dry 0.002 0.024Acetone 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/26/22 18:24 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/26/22 18:24 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/22 18:24 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/26/22 18:24 V18030TBL
0.0008 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/26/22 18:24 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/22 18:24 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/26/22 18:24 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/22 18:24 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/22 18:24 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/22 18:24 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/26/22 18:24 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/22 18:24 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/22 18:24 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/22 18:24 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 18:24 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/26/22 18:24 V18030TBL
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 04/26/22 18:24 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/22 18:24 V18030TBL
0.004 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/26/22 18:24 V18030TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/26/22 18:24 V18030TBL
0.056 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/22 18:24 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/26/22 18:24 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/22 18:24 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/26/22 18:24 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/22 18:24 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/22 18:24 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/26/22 18:24 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/26/22 18:24 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/26/22 18:24 V18030
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/26/22 18:241 TBL V18030
Surrogate: Dibromofluoromethane 102 Limits: 84-123%04/26/22 18:241 TBL V18030
Surrogate: Toluene-d8 96.0 Limits: 76-129%04/26/22 18:241 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.142 mg/Kg - dry 0.142 0.810Acenaphthene 1 04/29/22 19:19 V18184JMV
<0.128 mg/Kg - dry 0.128 0.810Acenaphthylene 1 04/29/22 19:19 V18184JMV
<0.186 mg/Kg - dry 0.186 0.810Aniline 1 04/29/22 19:19 V18184JMV
<0.175 mg/Kg - dry 0.175 0.810Anthracene 1 04/29/22 19:19 V18184JMV
<0.170 mg/Kg - dry 0.170 0.810Benzo(a)anthracene 1 04/29/22 19:19 V18184JMV
<0.180 mg/Kg - dry 0.180 0.810Benzo(a)pyrene 1 04/29/22 19:19 V18184JMV
<0.179 mg/Kg - dry 0.179 0.810
Benzo(b)fluoranthene 1 04/29/22 19:19 V18184JMV
<0.167 mg/Kg - dry 0.167 0.810Benzo(g,h,i)perylene 1 04/29/22 19:19 V18184JMV
<0.168 mg/Kg - dry 0.168 0.810Benzo(k)fluoranthene 1 04/29/22 19:19 V18184JMV
<0.712 mg/Kg - dry 0.712 2.46Benzoic Acid 1 04/29/22 19:19 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.128 mg/Kg - dry 0.128 0.810Benzyl alcohol 1 04/29/22 19:19 V18184JMV
<0.144 mg/Kg - dry 0.144 0.810Bis(2-Chloroethoxy)methane 1 04/29/22 19:19 V18184JMV
<0.131 mg/Kg - dry 0.131 0.810Bis(2-Chloroethyl)ether 1 04/29/22 19:19 V18184JMV
<0.167 mg/Kg - dry 0.167 0.405Bis(2-Chloroisopropyl)ether 1 04/29/22 19:19 V18184JMV
<0.147 mg/Kg - dry 0.147 0.810Bis(2-ethylhexyl)phthalate 1 04/29/22 19:19 V18184JMV
<0.133 mg/Kg - dry 0.133 0.8104-Bromophenyl phenyl ether 1 04/29/22 19:19 V18184JMV
<0.138 mg/Kg - dry 0.138 0.405Butyl benzyl phthalate 1 04/29/22 19:19 V18184JMV
<0.113 mg/Kg - dry 0.113 0.8104-Chloro-3-methylphenol 1 04/29/22 19:19 V18184JMV
<0.137 mg/Kg - dry 0.137 0.405
4-Chloroaniline 1 04/29/22 19:19 V18184JMV
<0.142 mg/Kg - dry 0.142 0.8102-Chloronaphthalene 1 04/29/22 19:19 V18184JMV
<0.120 mg/Kg - dry 0.120 0.8102-Chlorophenol 1 04/29/22 19:19 V18184JMV
<0.154 mg/Kg - dry 0.154 1.234-Chlorophenyl phenyl ether 1 04/29/22 19:19 V18184JMV
<0.174 mg/Kg - dry 0.174 0.810Chrysene 1 04/29/22 19:19 V18184JMV
<0.282 mg/Kg - dry 0.282 0.810Dibenz(a,h)anthracene 1 04/29/22 19:19 V18184JMV
<0.146 mg/Kg - dry 0.146 0.810Dibenzofuran 1 04/29/22 19:19 V18184JMV
<0.115 mg/Kg - dry 0.115 0.810
1,2-Dichlorobenzene 1 04/29/22 19:19 V18184JMV
<0.119 mg/Kg - dry 0.119 0.8101,3-Dichlorobenzene 1 04/29/22 19:19 V18184JMV
<0.119 mg/Kg - dry 0.119 0.4051,4-Dichlorobenzene 1 04/29/22 19:19 V18184JMV
<0.180 mg/Kg - dry 0.180 0.8103,3'-Dichlorobenzidine 1 04/29/22 19:19 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8102,4-Dichlorophenol 1 04/29/22 19:19 V18184JMV
<0.221 mg/Kg - dry 0.221 0.810Diethyl phthalate 1 04/29/22 19:19 V18184JMV
<0.213 mg/Kg - dry 0.213 0.810Dimethyl phthalate 1 04/29/22 19:19 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.132 mg/Kg - dry 0.132 0.4052,4-Dimethylphenol 1 04/29/22 19:19 V18184JMV
<0.131 mg/Kg - dry 0.131 0.810Di-n-butyl phthalate 1 04/29/22 19:19 V18184JMV
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 04/29/22 19:19 V18184JMV
<0.638 mg/Kg - dry 0.638 1.842,4-Dinitrophenol 1 04/29/22 19:19 V18184JMV
<0.118 mg/Kg - dry 0.118 0.8102,4-Dinitrotoluene 1 04/29/22 19:19 V18184JMV
<0.132 mg/Kg - dry 0.132 0.8102,6-Dinitrotoluene 1 04/29/22 19:19 V18184JMV
<0.175 mg/Kg - dry 0.175 0.405Di-n-Octyl Phthalate 1 04/29/22 19:19 V18184JMV
<0.151 mg/Kg - dry 0.151 0.810Fluoranthene 1 04/29/22 19:19 V18184JMV
<0.157 mg/Kg - dry 0.157 0.810
Fluorene 1 04/29/22 19:19 V18184JMV
<0.130 mg/Kg - dry 0.130 0.810Hexachlorobenzene 1 04/29/22 19:19 V18184JMV
<0.119 mg/Kg - dry 0.119 0.810Hexachlorobutadiene 1 04/29/22 19:19 V18184JMV
<0.192 mg/Kg - dry 0.192 0.810Hexachlorocyclopentadiene 1 04/29/22 19:19 V18184JMV
<0.097 mg/Kg - dry 0.097 0.810Hexachloroethane 1 04/29/22 19:19 V18184JMV
<0.219 mg/Kg - dry 0.219 0.810Indeno(1,2,3-cd)pyrene 1 04/29/22 19:19 V18184JMV
<0.234 mg/Kg - dry 0.234 0.810Isophorone 1 04/29/22 19:19 V18184JMV
<0.130 mg/Kg - dry 0.130 0.810
1-Methylnaphthalene 1 04/29/22 19:19 V18184JMV
<0.122 mg/Kg - dry 0.122 0.8102-Methylnaphthalene 1 04/29/22 19:19 V18184JMV
<0.119 mg/Kg - dry 0.119 0.8102-Methylphenol 1 04/29/22 19:19 V18184JMV
<0.104 mg/Kg - dry 0.104 0.8103&4 Methylphenol 1 04/29/22 19:19 V18184JMV
<0.176 mg/Kg - dry 0.176 0.810Naphthalene 1 04/29/22 19:19 V18184JMV
<0.118 mg/Kg - dry 0.118 0.8102-Nitroaniline 1 04/29/22 19:19 V18184JMV
<0.147 mg/Kg - dry 0.147 0.8103-Nitroaniline 1 04/29/22 19:19 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.114 mg/Kg - dry 0.114 0.4054-Nitroaniline 1 04/29/22 19:19 V18184JMV
<0.142 mg/Kg - dry 0.142 0.405Nitrobenzene 1 04/29/22 19:19 V18184JMV
<0.109 mg/Kg - dry 0.109 0.8102-Nitrophenol 1 04/29/22 19:19 V18184JMV
<0.143 mg/Kg - dry 0.143 0.8104-Nitrophenol 1 04/29/22 19:19 V18184JMV
<0.323 mg/Kg - dry 0.323 0.810N-Nitrosodimethylamine 1 04/29/22 19:19 V18184JMV
<0.222 mg/Kg - dry 0.222 0.810N-Nitrosodiphenylamine 1 04/29/22 19:19 V18184JMV
<0.144 mg/Kg - dry 0.144 0.810N-Nitroso-di-n-propylamine 1 04/29/22 19:19 V18184JMV
<0.426 mg/Kg - dry 0.426 1.23Pentachlorophenol 1 04/29/22 19:19 V18184JMV
<0.255 mg/Kg - dry 0.255 0.810
Phenanthrene 1 04/29/22 19:19 V18184JMV
<0.137 mg/Kg - dry 0.137 0.810Phenol 1 04/29/22 19:19 V18184JMV
<0.164 mg/Kg - dry 0.164 0.810Pyrene 1 04/29/22 19:19 V18184JMV
<0.097 mg/Kg - dry 0.097 0.405Pyridine 1 04/29/22 19:19 V18184JMV
<0.131 mg/Kg - dry 0.131 0.8101,2,4-Trichlorobenzene 1 04/29/22 19:19 V18184JMV
<0.118 mg/Kg - dry 0.118 0.8102,4,5-Trichlorophenol 1 04/29/22 19:19 V18184JMV
<0.118 mg/Kg - dry 0.118 0.8102,4,6-Trichlorophenol 1 04/29/22 19:19 V18184JMV
8270ESurrogate: Phenol-d5 83.2 Limits: 34-121%04/29/22 19:191 JMV
Surrogate: 2-Fluorobiphenyl 93.4 Limits: 44-115%04/29/22 19:191 JMV V18184
Surrogate: 2-Fluorophenol 97.0 Limits: 35-115%04/29/22 19:191 JMV V18184
Surrogate: Nitrobenzene-d5 80.7 Limits: 37-122%04/29/22 19:191 JMV V18184
Surrogate: 4-Terphenyl-d14 111 Limits: 54-127%04/29/22 19:191 JMV V18184
Surrogate: 2,4,6-Tribromophenol 91.3 Limits: 39-132%04/29/22 19:191 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:W2@8
99475 Matrix:
4/21/2022 16:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18369 05/05/22 10:54
<11.4 mg/Kg - dry 11.4 61.7Aliphatic C9-C18 1 05/06/22 17:55 V18459JLK
<15.0 mg/Kg - dry 15.0 61.7Aliphatic C19-C36 1 05/06/22 17:55 V18459JLK
<17.6 mg/Kg - dry 17.6 61.7Aromatic C11-C22 1 05/06/22 17:55 V18459JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 63.1 Limits: 40-140%05/06/22 17:551 JLK
MADEP-EPHSurrogate: Chlorooctadecane 55.7 Limits: 40-140%05/06/22 17:551 JLK
MADEP-EPHSurrogate: OTP Surrogate 49.8 Limits: 40-140%05/06/22 17:551 JLK
Surrogate: 2-Fluorobiphenyl 67.1 Limits: 40-140%05/06/22 17:551 JLK V18459
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<3.37 mg/Kg - dry 3.37 22.1
Aliphatic C5-C8 100 04/26/22 17:21 V18008TBL
<12.7 mg/Kg - dry 12.7 22.1Aliphatic C9-C12 100 04/26/22 17:21 V18008TBL
<1.72 mg/Kg - dry 1.72 22.1Aromatic C9-C10 100 04/26/22 17:21 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)107 Limits: 70-130%04/26/22 17:21100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)121 Limits: 70-130%04/26/22 17:21100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.6 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.017 J mg/Kg - dry 0.002 0.024Acetone 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/26/22 18:52 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/26/22 18:52 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/26/22 18:52 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/22 18:52 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/26/22 18:52 V18030TBL
0.001 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/22 18:52 V18030TBL
0.002 J mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/22 18:52 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/26/22 18:52 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/26/22 18:52 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/22 18:52 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/26/22 18:52 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/22 18:52 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/22 18:52 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/26/22 18:52 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/22 18:52 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/26/22 18:52 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/22 18:52 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/22 18:52 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/22 18:52 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 18:52 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/26/22 18:52 V18030TBL
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 04/26/22 18:52 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/26/22 18:52 V18030TBL
0.0006 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/22 18:52 V18030TBL
0.003 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/26/22 18:52 V18030TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/26/22 18:52 V18030TBL
0.077 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/26/22 18:52 V18030TBL
0.024 mg/Kg - dry 0.001 0.012Naphthalene 1 04/26/22 18:52 V18030TBL
0.0008 J
mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/22 18:52 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/26/22 18:52 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/26/22 18:52 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/22 18:52 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/22 18:52 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/26/22 18:52 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/22 18:52 V18030TBL
0.002 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/22 18:52 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/26/22 18:52 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/26/22 18:52 V18030TBL
0.001 J mg/Kg - dry 0.0006 0.006o-Xylene 1 04/26/22 18:52 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/26/22 18:52 V18030TBL
0.001 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/26/22 18:52 V18030
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/26/22 18:521 TBL V18030
Surrogate: Dibromofluoromethane 104 Limits: 84-123%04/26/22 18:521 TBL V18030
Surrogate: Toluene-d8 95.0 Limits: 76-129%04/26/22 18:521 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.140 mg/Kg - dry 0.140 0.802Acenaphthene 1 04/29/22 17:29 V18184JMV
<0.127 mg/Kg - dry 0.127 0.802Acenaphthylene 1 04/29/22 17:29 V18184JMV
<0.184 mg/Kg - dry 0.184 0.802Aniline 1 04/29/22 17:29 V18184JMV
<0.173 mg/Kg - dry 0.173 0.802Anthracene 1 04/29/22 17:29 V18184JMV
<0.168 mg/Kg - dry 0.168 0.802Benzo(a)anthracene 1 04/29/22 17:29 V18184JMV
<0.178 mg/Kg - dry 0.178 0.802Benzo(a)pyrene 1 04/29/22 17:29 V18184JMV
<0.177 mg/Kg - dry 0.177 0.802
Benzo(b)fluoranthene 1 04/29/22 17:29 V18184JMV
<0.165 mg/Kg - dry 0.165 0.802Benzo(g,h,i)perylene 1 04/29/22 17:29 V18184JMV
<0.166 mg/Kg - dry 0.166 0.802Benzo(k)fluoranthene 1 04/29/22 17:29 V18184JMV
<0.703 mg/Kg - dry 0.703 2.43Benzoic Acid 1 04/29/22 17:29 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.127 mg/Kg - dry 0.127 0.802Benzyl alcohol 1 04/29/22 17:29 V18184JMV
<0.143 mg/Kg - dry 0.143 0.802Bis(2-Chloroethoxy)methane 1 04/29/22 17:29 V18184JMV
<0.129 mg/Kg - dry 0.129 0.802Bis(2-Chloroethyl)ether 1 04/29/22 17:29 V18184JMV
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 04/29/22 17:29 V18184JMV
<0.145 mg/Kg - dry 0.145 0.802Bis(2-ethylhexyl)phthalate 1 04/29/22 17:29 V18184JMV
<0.132 mg/Kg - dry 0.132 0.8024-Bromophenyl phenyl ether 1 04/29/22 17:29 V18184JMV
<0.137 mg/Kg - dry 0.137 0.401Butyl benzyl phthalate 1 04/29/22 17:29 V18184JMV
<0.112 mg/Kg - dry 0.112 0.8024-Chloro-3-methylphenol 1 04/29/22 17:29 V18184JMV
<0.135 mg/Kg - dry 0.135 0.401
4-Chloroaniline 1 04/29/22 17:29 V18184JMV
<0.140 mg/Kg - dry 0.140 0.8022-Chloronaphthalene 1 04/29/22 17:29 V18184JMV
<0.119 mg/Kg - dry 0.119 0.8022-Chlorophenol 1 04/29/22 17:29 V18184JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 04/29/22 17:29 V18184JMV
<0.172 mg/Kg - dry 0.172 0.802Chrysene 1 04/29/22 17:29 V18184JMV
<0.279 mg/Kg - dry 0.279 0.802Dibenz(a,h)anthracene 1 04/29/22 17:29 V18184JMV
<0.144 mg/Kg - dry 0.144 0.802Dibenzofuran 1 04/29/22 17:29 V18184JMV
<0.114 mg/Kg - dry 0.114 0.802
1,2-Dichlorobenzene 1 04/29/22 17:29 V18184JMV
<0.118 mg/Kg - dry 0.118 0.8021,3-Dichlorobenzene 1 04/29/22 17:29 V18184JMV
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 04/29/22 17:29 V18184JMV
<0.178 mg/Kg - dry 0.178 0.8023,3'-Dichlorobenzidine 1 04/29/22 17:29 V18184JMV
<0.116 mg/Kg - dry 0.116 0.8022,4-Dichlorophenol 1 04/29/22 17:29 V18184JMV
<0.218 mg/Kg - dry 0.218 0.802Diethyl phthalate 1 04/29/22 17:29 V18184JMV
<0.211 mg/Kg - dry 0.211 0.802Dimethyl phthalate 1 04/29/22 17:29 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 04/29/22 17:29 V18184JMV
<0.129 mg/Kg - dry 0.129 0.802Di-n-butyl phthalate 1 04/29/22 17:29 V18184JMV
<0.291 mg/Kg - dry 0.291 1.824,6-Dinitro-2-methylphenol 1 04/29/22 17:29 V18184JMV
<0.631 mg/Kg - dry 0.631 1.822,4-Dinitrophenol 1 04/29/22 17:29 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8022,4-Dinitrotoluene 1 04/29/22 17:29 V18184JMV
<0.131 mg/Kg - dry 0.131 0.8022,6-Dinitrotoluene 1 04/29/22 17:29 V18184JMV
<0.173 mg/Kg - dry 0.173 0.401Di-n-Octyl Phthalate 1 04/29/22 17:29 V18184JMV
<0.149 mg/Kg - dry 0.149 0.802Fluoranthene 1 04/29/22 17:29 V18184JMV
0.208 J
mg/Kg - dry 0.155 0.802
Fluorene 1 04/29/22 17:29 V18184JMV
<0.128 mg/Kg - dry 0.128 0.802Hexachlorobenzene 1 04/29/22 17:29 V18184JMV
<0.118 mg/Kg - dry 0.118 0.802Hexachlorobutadiene 1 04/29/22 17:29 V18184JMV
<0.190 mg/Kg - dry 0.190 0.802Hexachlorocyclopentadiene 1 04/29/22 17:29 V18184JMV
<0.096 mg/Kg - dry 0.096 0.802Hexachloroethane 1 04/29/22 17:29 V18184JMV
<0.217 mg/Kg - dry 0.217 0.802Indeno(1,2,3-cd)pyrene 1 04/29/22 17:29 V18184JMV
<0.231 mg/Kg - dry 0.231 0.802Isophorone 1 04/29/22 17:29 V18184JMV
0.550 J
mg/Kg - dry 0.128 0.802
1-Methylnaphthalene 1 04/29/22 17:29 V18184JMV
0.769 J mg/Kg - dry 0.121 0.8022-Methylnaphthalene 1 04/29/22 17:29 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8022-Methylphenol 1 04/29/22 17:29 V18184JMV
<0.103 mg/Kg - dry 0.103 0.8023&4 Methylphenol 1 04/29/22 17:29 V18184JMV
<0.174 mg/Kg - dry 0.174 0.802Naphthalene 1 04/29/22 17:29 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8022-Nitroaniline 1 04/29/22 17:29 V18184JMV
<0.145 mg/Kg - dry 0.145 0.8023-Nitroaniline 1 04/29/22 17:29 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 04/29/22 17:29 V18184JMV
<0.140 mg/Kg - dry 0.140 0.401Nitrobenzene 1 04/29/22 17:29 V18184JMV
<0.107 mg/Kg - dry 0.107 0.8022-Nitrophenol 1 04/29/22 17:29 V18184JMV
<0.141 mg/Kg - dry 0.141 0.8024-Nitrophenol 1 04/29/22 17:29 V18184JMV
<0.319 mg/Kg - dry 0.319 0.802N-Nitrosodimethylamine 1 04/29/22 17:29 V18184JMV
<0.219 mg/Kg - dry 0.219 0.802N-Nitrosodiphenylamine 1 04/29/22 17:29 V18184JMV
<0.143 mg/Kg - dry 0.143 0.802N-Nitroso-di-n-propylamine 1 04/29/22 17:29 V18184JMV
<0.421 mg/Kg - dry 0.421 1.21Pentachlorophenol 1 04/29/22 17:29 V18184JMV
0.563 J
mg/Kg - dry 0.252 0.802
Phenanthrene 1 04/29/22 17:29 V18184JMV
<0.135 mg/Kg - dry 0.135 0.802Phenol 1 04/29/22 17:29 V18184JMV
0.177 J mg/Kg - dry 0.162 0.802Pyrene 1 04/29/22 17:29 V18184JMV
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 04/29/22 17:29 V18184JMV
<0.129 mg/Kg - dry 0.129 0.8021,2,4-Trichlorobenzene 1 04/29/22 17:29 V18184JMV
<0.116 mg/Kg - dry 0.116 0.8022,4,5-Trichlorophenol 1 04/29/22 17:29 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8022,4,6-Trichlorophenol 1 04/29/22 17:29 V18184JMV
8270ESurrogate: Phenol-d5 83.2 Limits: 34-121%04/29/22 17:291 JMV
Surrogate: 2-Fluorobiphenyl 89.8 Limits: 44-115%04/29/22 17:291 JMV V18184
Surrogate: 2-Fluorophenol 97.3 Limits: 35-115%04/29/22 17:291 JMV V18184
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%04/29/22 17:291 JMV V18184
Surrogate: 4-Terphenyl-d14 112 Limits: 54-127%04/29/22 17:291 JMV V18184
Surrogate: 2,4,6-Tribromophenol 91.0 Limits: 39-132%04/29/22 17:291 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:CF@8
99476 Matrix:
4/21/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18051 04/27/22 09:10
58.6 J mg/Kg - dry 11.1 60.3Aliphatic C9-C18 1 05/03/22 22:49 V18269JC1
30.7 J mg/Kg - dry 14.7 60.3Aliphatic C19-C36 1 05/03/22 22:49 V18269JC1
33.0 J mg/Kg - dry 17.1 60.3Aromatic C11-C22 1 05/03/22 22:49 V18269JC1
MADEP-EPHSurrogate: 2-Bromonaphthalene 71.9 Limits: 40-140%05/03/22 22:491 JC1
MADEP-EPHSurrogate: Chlorooctadecane 55.3 Limits: 40-140%05/03/22 22:491 JC1
MADEP-EPHSurrogate: OTP Surrogate 56.3 Limits: 40-140%05/03/22 22:491 JC1
Surrogate: 2-Fluorobiphenyl 57.3 Limits: 40-140%05/03/22 22:491 JC1 V18269
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.70 mg/Kg - dry 1.70 11.2
Aliphatic C5-C8 100 04/26/22 17:45 V18008TBL
8.57 J mg/Kg - dry 6.40 11.2Aliphatic C9-C12 100 04/26/22 17:45 V18008TBL
<0.875 mg/Kg - dry 0.875 11.2Aromatic C9-C10 100 04/26/22 17:45 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.5 Limits: 70-130%04/26/22 17:45100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)103 Limits: 70-130%04/26/22 17:45100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.6 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.014 J mg/Kg - dry 0.003 0.026Acetone 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 04/26/22 19:20 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/22 19:20 V18030TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 04/26/22 19:20 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/22 19:20 V18030TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 04/26/22 19:20 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 04/26/22 19:20 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/22 19:20 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/26/22 19:20 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/22 19:20 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/22 19:20 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/22 19:20 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/22 19:20 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/22 19:20 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/26/22 19:20 V18030TBL
0.002 J mg/Kg - dry 0.0009 0.013n-Hexane 1 04/26/22 19:20 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 04/26/22 19:20 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/22 19:20 V18030TBL
0.002 J mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/26/22 19:20 V18030TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 04/26/22 19:20 V18030TBL
0.057 mg/Kg - dry 0.001 0.013Methylene Chloride 1 04/26/22 19:20 V18030TBL
0.001 J mg/Kg - dry 0.001 0.013Naphthalene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/22 19:20 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/22 19:20 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 04/26/22 19:20 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.013
1,2,4-Trichlorobenzene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/22 19:20 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/22 19:20 V18030TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 04/26/22 19:20 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/22 19:20 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 04/26/22 19:20 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 04/26/22 19:20 V18030TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/26/22 19:20 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/26/22 19:20 V18030
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/26/22 19:201 TBL V18030
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/26/22 19:201 TBL V18030
Surrogate: Toluene-d8 94.4 Limits: 76-129%04/26/22 19:201 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.151 mg/Kg - dry 0.151 0.863Acenaphthene 1 04/29/22 17:51 V18184JMV
<0.137 mg/Kg - dry 0.137 0.863Acenaphthylene 1 04/29/22 17:51 V18184JMV
<0.198 mg/Kg - dry 0.198 0.863Aniline 1 04/29/22 17:51 V18184JMV
<0.187 mg/Kg - dry 0.187 0.863Anthracene 1 04/29/22 17:51 V18184JMV
<0.181 mg/Kg - dry 0.181 0.863Benzo(a)anthracene 1 04/29/22 17:51 V18184JMV
<0.192 mg/Kg - dry 0.192 0.863Benzo(a)pyrene 1 04/29/22 17:51 V18184JMV
<0.191 mg/Kg - dry 0.191 0.863
Benzo(b)fluoranthene 1 04/29/22 17:51 V18184JMV
<0.178 mg/Kg - dry 0.178 0.863Benzo(g,h,i)perylene 1 04/29/22 17:51 V18184JMV
<0.179 mg/Kg - dry 0.179 0.863Benzo(k)fluoranthene 1 04/29/22 17:51 V18184JMV
<0.759 mg/Kg - dry 0.759 2.62Benzoic Acid 1 04/29/22 17:51 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.137 mg/Kg - dry 0.137 0.863Benzyl alcohol 1 04/29/22 17:51 V18184JMV
<0.154 mg/Kg - dry 0.154 0.863Bis(2-Chloroethoxy)methane 1 04/29/22 17:51 V18184JMV
<0.140 mg/Kg - dry 0.140 0.863Bis(2-Chloroethyl)ether 1 04/29/22 17:51 V18184JMV
<0.178 mg/Kg - dry 0.178 0.431Bis(2-Chloroisopropyl)ether 1 04/29/22 17:51 V18184JMV
<0.157 mg/Kg - dry 0.157 0.863Bis(2-ethylhexyl)phthalate 1 04/29/22 17:51 V18184JMV
<0.142 mg/Kg - dry 0.142 0.8634-Bromophenyl phenyl ether 1 04/29/22 17:51 V18184JMV
<0.147 mg/Kg - dry 0.147 0.431Butyl benzyl phthalate 1 04/29/22 17:51 V18184JMV
<0.120 mg/Kg - dry 0.120 0.8634-Chloro-3-methylphenol 1 04/29/22 17:51 V18184JMV
<0.146 mg/Kg - dry 0.146 0.431
4-Chloroaniline 1 04/29/22 17:51 V18184JMV
<0.151 mg/Kg - dry 0.151 0.8632-Chloronaphthalene 1 04/29/22 17:51 V18184JMV
<0.128 mg/Kg - dry 0.128 0.8632-Chlorophenol 1 04/29/22 17:51 V18184JMV
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 04/29/22 17:51 V18184JMV
<0.185 mg/Kg - dry 0.185 0.863Chrysene 1 04/29/22 17:51 V18184JMV
<0.301 mg/Kg - dry 0.301 0.863Dibenz(a,h)anthracene 1 04/29/22 17:51 V18184JMV
<0.155 mg/Kg - dry 0.155 0.863Dibenzofuran 1 04/29/22 17:51 V18184JMV
<0.123 mg/Kg - dry 0.123 0.863
1,2-Dichlorobenzene 1 04/29/22 17:51 V18184JMV
<0.127 mg/Kg - dry 0.127 0.8631,3-Dichlorobenzene 1 04/29/22 17:51 V18184JMV
<0.127 mg/Kg - dry 0.127 0.4311,4-Dichlorobenzene 1 04/29/22 17:51 V18184JMV
<0.192 mg/Kg - dry 0.192 0.8633,3'-Dichlorobenzidine 1 04/29/22 17:51 V18184JMV
<0.125 mg/Kg - dry 0.125 0.8632,4-Dichlorophenol 1 04/29/22 17:51 V18184JMV
<0.235 mg/Kg - dry 0.235 0.863Diethyl phthalate 1 04/29/22 17:51 V18184JMV
<0.227 mg/Kg - dry 0.227 0.863Dimethyl phthalate 1 04/29/22 17:51 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.141 mg/Kg - dry 0.141 0.4312,4-Dimethylphenol 1 04/29/22 17:51 V18184JMV
<0.140 mg/Kg - dry 0.140 0.863Di-n-butyl phthalate 1 04/29/22 17:51 V18184JMV
<0.314 mg/Kg - dry 0.314 1.964,6-Dinitro-2-methylphenol 1 04/29/22 17:51 V18184JMV
<0.680 mg/Kg - dry 0.680 1.962,4-Dinitrophenol 1 04/29/22 17:51 V18184JMV
<0.126 mg/Kg - dry 0.126 0.8632,4-Dinitrotoluene 1 04/29/22 17:51 V18184JMV
<0.141 mg/Kg - dry 0.141 0.8632,6-Dinitrotoluene 1 04/29/22 17:51 V18184JMV
<0.187 mg/Kg - dry 0.187 0.431Di-n-Octyl Phthalate 1 04/29/22 17:51 V18184JMV
<0.160 mg/Kg - dry 0.160 0.863Fluoranthene 1 04/29/22 17:51 V18184JMV
<0.167 mg/Kg - dry 0.167 0.863
Fluorene 1 04/29/22 17:51 V18184JMV
<0.138 mg/Kg - dry 0.138 0.863Hexachlorobenzene 1 04/29/22 17:51 V18184JMV
<0.127 mg/Kg - dry 0.127 0.863Hexachlorobutadiene 1 04/29/22 17:51 V18184JMV
<0.205 mg/Kg - dry 0.205 0.863Hexachlorocyclopentadiene 1 04/29/22 17:51 V18184JMV
<0.103 mg/Kg - dry 0.103 0.863Hexachloroethane 1 04/29/22 17:51 V18184JMV
<0.234 mg/Kg - dry 0.234 0.863Indeno(1,2,3-cd)pyrene 1 04/29/22 17:51 V18184JMV
<0.250 mg/Kg - dry 0.250 0.863Isophorone 1 04/29/22 17:51 V18184JMV
<0.138 mg/Kg - dry 0.138 0.863
1-Methylnaphthalene 1 04/29/22 17:51 V18184JMV
<0.130 mg/Kg - dry 0.130 0.8632-Methylnaphthalene 1 04/29/22 17:51 V18184JMV
<0.126 mg/Kg - dry 0.126 0.8632-Methylphenol 1 04/29/22 17:51 V18184JMV
<0.111 mg/Kg - dry 0.111 0.8633&4 Methylphenol 1 04/29/22 17:51 V18184JMV
<0.188 mg/Kg - dry 0.188 0.863Naphthalene 1 04/29/22 17:51 V18184JMV
<0.126 mg/Kg - dry 0.126 0.8632-Nitroaniline 1 04/29/22 17:51 V18184JMV
<0.157 mg/Kg - dry 0.157 0.8633-Nitroaniline 1 04/29/22 17:51 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.122 mg/Kg - dry 0.122 0.4314-Nitroaniline 1 04/29/22 17:51 V18184JMV
<0.151 mg/Kg - dry 0.151 0.431Nitrobenzene 1 04/29/22 17:51 V18184JMV
<0.116 mg/Kg - dry 0.116 0.8632-Nitrophenol 1 04/29/22 17:51 V18184JMV
<0.153 mg/Kg - dry 0.153 0.8634-Nitrophenol 1 04/29/22 17:51 V18184JMV
<0.344 mg/Kg - dry 0.344 0.863N-Nitrosodimethylamine 1 04/29/22 17:51 V18184JMV
<0.236 mg/Kg - dry 0.236 0.863N-Nitrosodiphenylamine 1 04/29/22 17:51 V18184JMV
<0.154 mg/Kg - dry 0.154 0.863N-Nitroso-di-n-propylamine 1 04/29/22 17:51 V18184JMV
<0.454 mg/Kg - dry 0.454 1.31Pentachlorophenol 1 04/29/22 17:51 V18184JMV
<0.272 mg/Kg - dry 0.272 0.863
Phenanthrene 1 04/29/22 17:51 V18184JMV
<0.146 mg/Kg - dry 0.146 0.863Phenol 1 04/29/22 17:51 V18184JMV
<0.175 mg/Kg - dry 0.175 0.863Pyrene 1 04/29/22 17:51 V18184JMV
<0.103 mg/Kg - dry 0.103 0.431Pyridine 1 04/29/22 17:51 V18184JMV
<0.140 mg/Kg - dry 0.140 0.8631,2,4-Trichlorobenzene 1 04/29/22 17:51 V18184JMV
<0.125 mg/Kg - dry 0.125 0.8632,4,5-Trichlorophenol 1 04/29/22 17:51 V18184JMV
<0.126 mg/Kg - dry 0.126 0.8632,4,6-Trichlorophenol 1 04/29/22 17:51 V18184JMV
8270ESurrogate: Phenol-d5 79.6 Limits: 34-121%04/29/22 17:511 JMV
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%04/29/22 17:511 JMV V18184
Surrogate: 2-Fluorophenol 93.1 Limits: 35-115%04/29/22 17:511 JMV V18184
Surrogate: Nitrobenzene-d5 75.9 Limits: 37-122%04/29/22 17:511 JMV V18184
Surrogate: 4-Terphenyl-d14 108 Limits: 54-127%04/29/22 17:511 JMV V18184
Surrogate: 2,4,6-Tribromophenol 88.0 Limits: 39-132%04/29/22 17:511 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:N4@10
99477 Matrix:
4/21/2022 16:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18051 04/27/22 09:10
<12.1 mg/Kg - dry 12.1 65.6Aliphatic C9-C18 1 05/03/22 23:25 V18269JC1
<16.0 mg/Kg - dry 16.0 65.6Aliphatic C19-C36 1 05/03/22 23:25 V18269JC1
<18.6 mg/Kg - dry 18.6 65.6Aromatic C11-C22 1 05/03/22 23:25 V18269JC1
MADEP-EPHSurrogate: 2-Bromonaphthalene 70.1 Limits: 40-140%05/03/22 23:251 JC1
MADEP-EPHSurrogate: Chlorooctadecane 56.0 Limits: 40-140%05/03/22 23:251 JC1
MADEP-EPHSurrogate: OTP Surrogate 59.5 Limits: 40-140%05/03/22 23:251 JC1
Surrogate: 2-Fluorobiphenyl 62.1 Limits: 40-140%05/03/22 23:251 JC1 V18269
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.60 mg/Kg - dry 1.60 10.5
Aliphatic C5-C8 100 04/26/22 18:09 V18008TBL
<6.01 mg/Kg - dry 6.01 10.5Aliphatic C9-C12 100 04/26/22 18:09 V18008TBL
<0.821 mg/Kg - dry 0.821 10.5Aromatic C9-C10 100 04/26/22 18:09 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.8 Limits: 70-130%04/26/22 18:09100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)101 Limits: 70-130%04/26/22 18:09100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.3 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.022 J mg/Kg - dry 0.002 0.024Acetone 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/26/22 19:47 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/26/22 19:47 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/22 19:47 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/26/22 19:47 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/26/22 19:47 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/22 19:47 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/26/22 19:47 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/22 19:47 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/26/22 19:47 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/22 19:47 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/22 19:47 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/26/22 19:47 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/22 19:47 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/26/22 19:47 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/22 19:47 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/22 19:47 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/22 19:47 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 19:47 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/26/22 19:47 V18030TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 04/26/22 19:47 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/22 19:47 V18030TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 04/26/22 19:47 V18030TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/26/22 19:47 V18030TBL
0.041 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/22 19:47 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/22 19:47 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/26/22 19:47 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/22 19:47 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/26/22 19:47 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/22 19:47 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/22 19:47 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/26/22 19:47 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/26/22 19:47 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/26/22 19:47 V18030
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%04/26/22 19:471 TBL V18030
Surrogate: Dibromofluoromethane 104 Limits: 84-123%04/26/22 19:471 TBL V18030
Surrogate: Toluene-d8 94.2 Limits: 76-129%04/26/22 19:471 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.140 mg/Kg - dry 0.140 0.799Acenaphthene 1 04/29/22 18:35 V18184JMV
<0.126 mg/Kg - dry 0.126 0.799Acenaphthylene 1 04/29/22 18:35 V18184JMV
<0.183 mg/Kg - dry 0.183 0.799Aniline 1 04/29/22 18:35 V18184JMV
<0.172 mg/Kg - dry 0.172 0.799Anthracene 1 04/29/22 18:35 V18184JMV
<0.168 mg/Kg - dry 0.168 0.799Benzo(a)anthracene 1 04/29/22 18:35 V18184JMV
<0.177 mg/Kg - dry 0.177 0.799Benzo(a)pyrene 1 04/29/22 18:35 V18184JMV
<0.176 mg/Kg - dry 0.176 0.799
Benzo(b)fluoranthene 1 04/29/22 18:35 V18184JMV
<0.164 mg/Kg - dry 0.164 0.799Benzo(g,h,i)perylene 1 04/29/22 18:35 V18184JMV
<0.165 mg/Kg - dry 0.165 0.799Benzo(k)fluoranthene 1 04/29/22 18:35 V18184JMV
<0.701 mg/Kg - dry 0.701 2.42Benzoic Acid 1 04/29/22 18:35 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.126 mg/Kg - dry 0.126 0.799Benzyl alcohol 1 04/29/22 18:35 V18184JMV
<0.142 mg/Kg - dry 0.142 0.799Bis(2-Chloroethoxy)methane 1 04/29/22 18:35 V18184JMV
<0.129 mg/Kg - dry 0.129 0.799Bis(2-Chloroethyl)ether 1 04/29/22 18:35 V18184JMV
<0.164 mg/Kg - dry 0.164 0.400Bis(2-Chloroisopropyl)ether 1 04/29/22 18:35 V18184JMV
<0.145 mg/Kg - dry 0.145 0.799Bis(2-ethylhexyl)phthalate 1 04/29/22 18:35 V18184JMV
<0.131 mg/Kg - dry 0.131 0.7994-Bromophenyl phenyl ether 1 04/29/22 18:35 V18184JMV
<0.136 mg/Kg - dry 0.136 0.400Butyl benzyl phthalate 1 04/29/22 18:35 V18184JMV
<0.111 mg/Kg - dry 0.111 0.7994-Chloro-3-methylphenol 1 04/29/22 18:35 V18184JMV
<0.135 mg/Kg - dry 0.135 0.400
4-Chloroaniline 1 04/29/22 18:35 V18184JMV
<0.140 mg/Kg - dry 0.140 0.7992-Chloronaphthalene 1 04/29/22 18:35 V18184JMV
<0.118 mg/Kg - dry 0.118 0.7992-Chlorophenol 1 04/29/22 18:35 V18184JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 04/29/22 18:35 V18184JMV
<0.171 mg/Kg - dry 0.171 0.799Chrysene 1 04/29/22 18:35 V18184JMV
<0.278 mg/Kg - dry 0.278 0.799Dibenz(a,h)anthracene 1 04/29/22 18:35 V18184JMV
<0.143 mg/Kg - dry 0.143 0.799Dibenzofuran 1 04/29/22 18:35 V18184JMV
<0.114 mg/Kg - dry 0.114 0.799
1,2-Dichlorobenzene 1 04/29/22 18:35 V18184JMV
<0.117 mg/Kg - dry 0.117 0.7991,3-Dichlorobenzene 1 04/29/22 18:35 V18184JMV
<0.118 mg/Kg - dry 0.118 0.4001,4-Dichlorobenzene 1 04/29/22 18:35 V18184JMV
<0.177 mg/Kg - dry 0.177 0.7993,3'-Dichlorobenzidine 1 04/29/22 18:35 V18184JMV
<0.115 mg/Kg - dry 0.115 0.7992,4-Dichlorophenol 1 04/29/22 18:35 V18184JMV
<0.217 mg/Kg - dry 0.217 0.799Diethyl phthalate 1 04/29/22 18:35 V18184JMV
<0.210 mg/Kg - dry 0.210 0.799Dimethyl phthalate 1 04/29/22 18:35 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.130 mg/Kg - dry 0.130 0.4002,4-Dimethylphenol 1 04/29/22 18:35 V18184JMV
<0.129 mg/Kg - dry 0.129 0.799Di-n-butyl phthalate 1 04/29/22 18:35 V18184JMV
<0.290 mg/Kg - dry 0.290 1.814,6-Dinitro-2-methylphenol 1 04/29/22 18:35 V18184JMV
<0.628 mg/Kg - dry 0.628 1.812,4-Dinitrophenol 1 04/29/22 18:35 V18184JMV
<0.116 mg/Kg - dry 0.116 0.7992,4-Dinitrotoluene 1 04/29/22 18:35 V18184JMV
<0.130 mg/Kg - dry 0.130 0.7992,6-Dinitrotoluene 1 04/29/22 18:35 V18184JMV
<0.172 mg/Kg - dry 0.172 0.400Di-n-Octyl Phthalate 1 04/29/22 18:35 V18184JMV
<0.148 mg/Kg - dry 0.148 0.799Fluoranthene 1 04/29/22 18:35 V18184JMV
<0.154 mg/Kg - dry 0.154 0.799
Fluorene 1 04/29/22 18:35 V18184JMV
<0.128 mg/Kg - dry 0.128 0.799Hexachlorobenzene 1 04/29/22 18:35 V18184JMV
<0.118 mg/Kg - dry 0.118 0.799Hexachlorobutadiene 1 04/29/22 18:35 V18184JMV
<0.189 mg/Kg - dry 0.189 0.799Hexachlorocyclopentadiene 1 04/29/22 18:35 V18184JMV
<0.095 mg/Kg - dry 0.095 0.799Hexachloroethane 1 04/29/22 18:35 V18184JMV
<0.216 mg/Kg - dry 0.216 0.799Indeno(1,2,3-cd)pyrene 1 04/29/22 18:35 V18184JMV
<0.230 mg/Kg - dry 0.230 0.799Isophorone 1 04/29/22 18:35 V18184JMV
<0.128 mg/Kg - dry 0.128 0.799
1-Methylnaphthalene 1 04/29/22 18:35 V18184JMV
<0.120 mg/Kg - dry 0.120 0.7992-Methylnaphthalene 1 04/29/22 18:35 V18184JMV
<0.117 mg/Kg - dry 0.117 0.7992-Methylphenol 1 04/29/22 18:35 V18184JMV
<0.102 mg/Kg - dry 0.102 0.7993&4 Methylphenol 1 04/29/22 18:35 V18184JMV
<0.174 mg/Kg - dry 0.174 0.799Naphthalene 1 04/29/22 18:35 V18184JMV
<0.117 mg/Kg - dry 0.117 0.7992-Nitroaniline 1 04/29/22 18:35 V18184JMV
<0.145 mg/Kg - dry 0.145 0.7993-Nitroaniline 1 04/29/22 18:35 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.113 mg/Kg - dry 0.113 0.4004-Nitroaniline 1 04/29/22 18:35 V18184JMV
<0.140 mg/Kg - dry 0.140 0.400Nitrobenzene 1 04/29/22 18:35 V18184JMV
<0.107 mg/Kg - dry 0.107 0.7992-Nitrophenol 1 04/29/22 18:35 V18184JMV
<0.141 mg/Kg - dry 0.141 0.7994-Nitrophenol 1 04/29/22 18:35 V18184JMV
<0.318 mg/Kg - dry 0.318 0.799N-Nitrosodimethylamine 1 04/29/22 18:35 V18184JMV
<0.218 mg/Kg - dry 0.218 0.799N-Nitrosodiphenylamine 1 04/29/22 18:35 V18184JMV
<0.142 mg/Kg - dry 0.142 0.799N-Nitroso-di-n-propylamine 1 04/29/22 18:35 V18184JMV
<0.419 mg/Kg - dry 0.419 1.21Pentachlorophenol 1 04/29/22 18:35 V18184JMV
<0.251 mg/Kg - dry 0.251 0.799
Phenanthrene 1 04/29/22 18:35 V18184JMV
<0.135 mg/Kg - dry 0.135 0.799Phenol 1 04/29/22 18:35 V18184JMV
<0.162 mg/Kg - dry 0.162 0.799Pyrene 1 04/29/22 18:35 V18184JMV
<0.096 mg/Kg - dry 0.096 0.400Pyridine 1 04/29/22 18:35 V18184JMV
<0.129 mg/Kg - dry 0.129 0.7991,2,4-Trichlorobenzene 1 04/29/22 18:35 V18184JMV
<0.116 mg/Kg - dry 0.116 0.7992,4,5-Trichlorophenol 1 04/29/22 18:35 V18184JMV
<0.116 mg/Kg - dry 0.116 0.7992,4,6-Trichlorophenol 1 04/29/22 18:35 V18184JMV
8270ESurrogate: Phenol-d5 81.4 Limits: 34-121%04/29/22 18:351 JMV
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%04/29/22 18:351 JMV V18184
Surrogate: 2-Fluorophenol 95.8 Limits: 35-115%04/29/22 18:351 JMV V18184
Surrogate: Nitrobenzene-d5 76.6 Limits: 37-122%04/29/22 18:351 JMV V18184
Surrogate: 4-Terphenyl-d14 107 Limits: 54-127%04/29/22 18:351 JMV V18184
Surrogate: 2,4,6-Tribromophenol 89.5 Limits: 39-132%04/29/22 18:351 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NO@15
99478 Matrix:
4/21/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18051 04/27/22 09:10
<11.1 mg/Kg - dry 11.1 60.6Aliphatic C9-C18 1 05/04/22 00:01 V18269JC1
<14.8 mg/Kg - dry 14.8 60.6Aliphatic C19-C36 1 05/04/22 00:01 V18269JC1
<17.2 mg/Kg - dry 17.2 60.6Aromatic C11-C22 1 05/04/22 00:01 V18269JC1
MADEP-EPHSurrogate: 2-Bromonaphthalene 66.8 Limits: 40-140%05/04/22 00:011 JC1
MADEP-EPHSurrogate: Chlorooctadecane 54.0 Limits: 40-140%05/04/22 00:011 JC1
MADEP-EPHSurrogate: OTP Surrogate 50.5 Limits: 40-140%05/04/22 00:011 JC1
Surrogate: 2-Fluorobiphenyl 62.1 Limits: 40-140%05/04/22 00:011 JC1 V18269
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.48 mg/Kg - dry 1.48 9.67
Aliphatic C5-C8 100 04/26/22 18:33 V18008TBL
<5.51 mg/Kg - dry 5.51 9.67Aliphatic C9-C12 100 04/26/22 18:33 V18008TBL
<0.754 mg/Kg - dry 0.754 9.67Aromatic C9-C10 100 04/26/22 18:33 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)85.9 Limits: 70-130%04/26/22 18:33100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)83.7 Limits: 70-130%04/26/22 18:33100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.5 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.013 J mg/Kg - dry 0.002 0.024Acetone 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/26/22 20:15 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/26/22 20:15 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/22 20:15 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/26/22 20:15 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/22 20:15 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/26/22 20:15 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/22 20:15 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/22 20:15 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/26/22 20:15 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/22 20:15 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/26/22 20:15 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/22 20:15 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/22 20:15 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/22 20:15 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 20:15 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/26/22 20:15 V18030TBL
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 04/26/22 20:15 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/22 20:15 V18030TBL
0.001 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/26/22 20:15 V18030TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/26/22 20:15 V18030TBL
0.054 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/26/22 20:15 V18030TBL
0.001 J mg/Kg - dry 0.001 0.012Naphthalene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/22 20:15 V18030TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/26/22 20:15 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/22 20:15 V18030TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/26/22 20:15 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/22 20:15 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/22 20:15 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/26/22 20:15 V18030TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/26/22 20:15 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/26/22 20:15 V18030
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/26/22 20:151 TBL V18030
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/26/22 20:151 TBL V18030
Surrogate: Toluene-d8 94.0 Limits: 76-129%04/26/22 20:151 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.140 mg/Kg - dry 0.140 0.800Acenaphthene 1 04/29/22 18:13 V18184JMV
<0.127 mg/Kg - dry 0.127 0.800Acenaphthylene 1 04/29/22 18:13 V18184JMV
<0.184 mg/Kg - dry 0.184 0.800Aniline 1 04/29/22 18:13 V18184JMV
<0.173 mg/Kg - dry 0.173 0.800Anthracene 1 04/29/22 18:13 V18184JMV
<0.168 mg/Kg - dry 0.168 0.800Benzo(a)anthracene 1 04/29/22 18:13 V18184JMV
<0.178 mg/Kg - dry 0.178 0.800Benzo(a)pyrene 1 04/29/22 18:13 V18184JMV
<0.176 mg/Kg - dry 0.176 0.800
Benzo(b)fluoranthene 1 04/29/22 18:13 V18184JMV
<0.164 mg/Kg - dry 0.164 0.800Benzo(g,h,i)perylene 1 04/29/22 18:13 V18184JMV
<0.166 mg/Kg - dry 0.166 0.800Benzo(k)fluoranthene 1 04/29/22 18:13 V18184JMV
<0.703 mg/Kg - dry 0.703 2.42Benzoic Acid 1 04/29/22 18:13 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.127 mg/Kg - dry 0.127 0.800Benzyl alcohol 1 04/29/22 18:13 V18184JMV
<0.143 mg/Kg - dry 0.143 0.800Bis(2-Chloroethoxy)methane 1 04/29/22 18:13 V18184JMV
<0.129 mg/Kg - dry 0.129 0.800Bis(2-Chloroethyl)ether 1 04/29/22 18:13 V18184JMV
<0.164 mg/Kg - dry 0.164 0.400Bis(2-Chloroisopropyl)ether 1 04/29/22 18:13 V18184JMV
<0.145 mg/Kg - dry 0.145 0.800Bis(2-ethylhexyl)phthalate 1 04/29/22 18:13 V18184JMV
<0.132 mg/Kg - dry 0.132 0.8004-Bromophenyl phenyl ether 1 04/29/22 18:13 V18184JMV
<0.136 mg/Kg - dry 0.136 0.400Butyl benzyl phthalate 1 04/29/22 18:13 V18184JMV
<0.112 mg/Kg - dry 0.112 0.8004-Chloro-3-methylphenol 1 04/29/22 18:13 V18184JMV
<0.135 mg/Kg - dry 0.135 0.400
4-Chloroaniline 1 04/29/22 18:13 V18184JMV
<0.140 mg/Kg - dry 0.140 0.8002-Chloronaphthalene 1 04/29/22 18:13 V18184JMV
<0.119 mg/Kg - dry 0.119 0.8002-Chlorophenol 1 04/29/22 18:13 V18184JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 04/29/22 18:13 V18184JMV
<0.172 mg/Kg - dry 0.172 0.800Chrysene 1 04/29/22 18:13 V18184JMV
<0.278 mg/Kg - dry 0.278 0.800Dibenz(a,h)anthracene 1 04/29/22 18:13 V18184JMV
<0.144 mg/Kg - dry 0.144 0.800Dibenzofuran 1 04/29/22 18:13 V18184JMV
<0.114 mg/Kg - dry 0.114 0.800
1,2-Dichlorobenzene 1 04/29/22 18:13 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8001,3-Dichlorobenzene 1 04/29/22 18:13 V18184JMV
<0.118 mg/Kg - dry 0.118 0.4001,4-Dichlorobenzene 1 04/29/22 18:13 V18184JMV
<0.178 mg/Kg - dry 0.178 0.8003,3'-Dichlorobenzidine 1 04/29/22 18:13 V18184JMV
<0.116 mg/Kg - dry 0.116 0.8002,4-Dichlorophenol 1 04/29/22 18:13 V18184JMV
<0.218 mg/Kg - dry 0.218 0.800Diethyl phthalate 1 04/29/22 18:13 V18184JMV
<0.210 mg/Kg - dry 0.210 0.800Dimethyl phthalate 1 04/29/22 18:13 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.130 mg/Kg - dry 0.130 0.4002,4-Dimethylphenol 1 04/29/22 18:13 V18184JMV
<0.129 mg/Kg - dry 0.129 0.800Di-n-butyl phthalate 1 04/29/22 18:13 V18184JMV
<0.290 mg/Kg - dry 0.290 1.824,6-Dinitro-2-methylphenol 1 04/29/22 18:13 V18184JMV
<0.630 mg/Kg - dry 0.630 1.822,4-Dinitrophenol 1 04/29/22 18:13 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8002,4-Dinitrotoluene 1 04/29/22 18:13 V18184JMV
<0.130 mg/Kg - dry 0.130 0.8002,6-Dinitrotoluene 1 04/29/22 18:13 V18184JMV
<0.173 mg/Kg - dry 0.173 0.400Di-n-Octyl Phthalate 1 04/29/22 18:13 V18184JMV
<0.149 mg/Kg - dry 0.149 0.800Fluoranthene 1 04/29/22 18:13 V18184JMV
<0.155 mg/Kg - dry 0.155 0.800
Fluorene 1 04/29/22 18:13 V18184JMV
<0.128 mg/Kg - dry 0.128 0.800Hexachlorobenzene 1 04/29/22 18:13 V18184JMV
<0.118 mg/Kg - dry 0.118 0.800Hexachlorobutadiene 1 04/29/22 18:13 V18184JMV
<0.190 mg/Kg - dry 0.190 0.800Hexachlorocyclopentadiene 1 04/29/22 18:13 V18184JMV
<0.096 mg/Kg - dry 0.096 0.800Hexachloroethane 1 04/29/22 18:13 V18184JMV
<0.216 mg/Kg - dry 0.216 0.800Indeno(1,2,3-cd)pyrene 1 04/29/22 18:13 V18184JMV
<0.231 mg/Kg - dry 0.231 0.800Isophorone 1 04/29/22 18:13 V18184JMV
<0.128 mg/Kg - dry 0.128 0.800
1-Methylnaphthalene 1 04/29/22 18:13 V18184JMV
<0.121 mg/Kg - dry 0.121 0.8002-Methylnaphthalene 1 04/29/22 18:13 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8002-Methylphenol 1 04/29/22 18:13 V18184JMV
<0.102 mg/Kg - dry 0.102 0.8003&4 Methylphenol 1 04/29/22 18:13 V18184JMV
<0.174 mg/Kg - dry 0.174 0.800Naphthalene 1 04/29/22 18:13 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8002-Nitroaniline 1 04/29/22 18:13 V18184JMV
<0.145 mg/Kg - dry 0.145 0.8003-Nitroaniline 1 04/29/22 18:13 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.113 mg/Kg - dry 0.113 0.4004-Nitroaniline 1 04/29/22 18:13 V18184JMV
<0.140 mg/Kg - dry 0.140 0.400Nitrobenzene 1 04/29/22 18:13 V18184JMV
<0.107 mg/Kg - dry 0.107 0.8002-Nitrophenol 1 04/29/22 18:13 V18184JMV
<0.141 mg/Kg - dry 0.141 0.8004-Nitrophenol 1 04/29/22 18:13 V18184JMV
<0.318 mg/Kg - dry 0.318 0.800N-Nitrosodimethylamine 1 04/29/22 18:13 V18184JMV
<0.219 mg/Kg - dry 0.219 0.800N-Nitrosodiphenylamine 1 04/29/22 18:13 V18184JMV
<0.143 mg/Kg - dry 0.143 0.800N-Nitroso-di-n-propylamine 1 04/29/22 18:13 V18184JMV
<0.420 mg/Kg - dry 0.420 1.21Pentachlorophenol 1 04/29/22 18:13 V18184JMV
<0.252 mg/Kg - dry 0.252 0.800
Phenanthrene 1 04/29/22 18:13 V18184JMV
<0.135 mg/Kg - dry 0.135 0.800Phenol 1 04/29/22 18:13 V18184JMV
<0.162 mg/Kg - dry 0.162 0.800Pyrene 1 04/29/22 18:13 V18184JMV
<0.096 mg/Kg - dry 0.096 0.400Pyridine 1 04/29/22 18:13 V18184JMV
<0.129 mg/Kg - dry 0.129 0.8001,2,4-Trichlorobenzene 1 04/29/22 18:13 V18184JMV
<0.116 mg/Kg - dry 0.116 0.8002,4,5-Trichlorophenol 1 04/29/22 18:13 V18184JMV
<0.117 mg/Kg - dry 0.117 0.8002,4,6-Trichlorophenol 1 04/29/22 18:13 V18184JMV
8270ESurrogate: Phenol-d5 82.3 Limits: 34-121%04/29/22 18:131 JMV
Surrogate: 2-Fluorobiphenyl 90.4 Limits: 44-115%04/29/22 18:131 JMV V18184
Surrogate: 2-Fluorophenol 95.5 Limits: 35-115%04/29/22 18:131 JMV V18184
Surrogate: Nitrobenzene-d5 77.2 Limits: 37-122%04/29/22 18:131 JMV V18184
Surrogate: 4-Terphenyl-d14 111 Limits: 54-127%04/29/22 18:131 JMV V18184
Surrogate: 2,4,6-Tribromophenol 90.7 Limits: 39-132%04/29/22 18:131 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NE6@8
99479 Matrix:
4/21/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18051 04/27/22 09:10
<11.2 mg/Kg - dry 11.2 60.8Aliphatic C9-C18 1 05/04/22 00:37 V18269JC1
<14.8 mg/Kg - dry 14.8 60.8Aliphatic C19-C36 1 05/04/22 00:37 V18269JC1
<17.3 mg/Kg - dry 17.3 60.8Aromatic C11-C22 1 05/04/22 00:37 V18269JC1
MADEP-EPHSurrogate: 2-Bromonaphthalene 65.7 Limits: 40-140%05/04/22 00:371 JC1
MADEP-EPHSurrogate: Chlorooctadecane 56.2 Limits: 40-140%05/04/22 00:371 JC1
MADEP-EPHSurrogate: OTP Surrogate 49.4 Limits: 40-140%05/04/22 00:371 JC1
Surrogate: 2-Fluorobiphenyl 57.5 Limits: 40-140%05/04/22 00:371 JC1 V18269
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<3.30 mg/Kg - dry 3.30 21.7
Aliphatic C5-C8 100 04/26/22 18:56 V18008TBL
<12.4 mg/Kg - dry 12.4 21.7Aliphatic C9-C12 100 04/26/22 18:56 V18008TBL
<1.70 mg/Kg - dry 1.70 21.7Aromatic C9-C10 100 04/26/22 18:56 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)122 Limits: 70-130%04/26/22 18:56100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)109 Limits: 70-130%04/26/22 18:56100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
31.7 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
0.041 mg/Kg - dry 0.003 0.029Acetone 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.029Acrolein 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 04/26/22 20:43 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 04/26/22 20:43 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 04/26/22 20:43 V18030TBL
0.001 J mg/Kg - dry 0.0009 0.014Chloromethane 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 04/26/22 20:43 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 04/26/22 20:43 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 04/26/22 20:43 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 04/26/22 20:43 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 04/26/22 20:43 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 04/26/22 20:43 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 04/26/22 20:43 V18030TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.073Ethyl Tertiary Butyl Ether (ETBE)1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 04/26/22 20:43 V18030TBL
0.003 J mg/Kg - dry 0.0010 0.014n-Hexane 1 04/26/22 20:43 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0292-Hexanone 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 04/26/22 20:43 V18030TBL
0.004 J mg/Kg - dry 0.0010 0.029Methyl Ethyl Ketone (MEK)1 04/26/22 20:43 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 04/26/22 20:43 V18030TBL
<0.021 mg/Kg - dry 0.021 0.0294-Methyl-2-Pentanone 1 04/26/22 20:43 V18030TBL
0.076 mg/Kg - dry 0.002 0.014Methylene Chloride 1 04/26/22 20:43 V18030TBL
0.002 J mg/Kg - dry 0.001 0.014Naphthalene 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.007
n-Propylbenzene 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 04/26/22 20:43 V18030TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 04/26/22 20:43 V18030TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 04/26/22 20:43 V18030TBL
<0.0009 mg/Kg - dry 0.0009 0.014
1,2,4-Trichlorobenzene 1 04/26/22 20:43 V18030TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 04/26/22 20:43 V18030TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 04/26/22 20:43 V18030TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 04/26/22 20:43 V18030TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18029 04/26/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 04/26/22 20:43 V18030TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 04/26/22 20:43 V18030TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 04/26/22 20:43 V18030
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/26/22 20:431 TBL V18030
Surrogate: Dibromofluoromethane 105 Limits: 84-123%04/26/22 20:431 TBL V18030
Surrogate: Toluene-d8 94.4 Limits: 76-129%04/26/22 20:431 TBL V18030
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.169 mg/Kg - dry 0.169 0.966Acenaphthene 1 04/29/22 18:57 V18184JMV
<0.153 mg/Kg - dry 0.153 0.966Acenaphthylene 1 04/29/22 18:57 V18184JMV
<0.222 mg/Kg - dry 0.222 0.966Aniline 1 04/29/22 18:57 V18184JMV
<0.209 mg/Kg - dry 0.209 0.966Anthracene 1 04/29/22 18:57 V18184JMV
<0.203 mg/Kg - dry 0.203 0.966Benzo(a)anthracene 1 04/29/22 18:57 V18184JMV
<0.215 mg/Kg - dry 0.215 0.966Benzo(a)pyrene 1 04/29/22 18:57 V18184JMV
<0.213 mg/Kg - dry 0.213 0.966
Benzo(b)fluoranthene 1 04/29/22 18:57 V18184JMV
<0.199 mg/Kg - dry 0.199 0.966Benzo(g,h,i)perylene 1 04/29/22 18:57 V18184JMV
<0.200 mg/Kg - dry 0.200 0.966Benzo(k)fluoranthene 1 04/29/22 18:57 V18184JMV
<0.849 mg/Kg - dry 0.849 2.93Benzoic Acid 1 04/29/22 18:57 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.153 mg/Kg - dry 0.153 0.966Benzyl alcohol 1 04/29/22 18:57 V18184JMV
<0.172 mg/Kg - dry 0.172 0.966Bis(2-Chloroethoxy)methane 1 04/29/22 18:57 V18184JMV
<0.156 mg/Kg - dry 0.156 0.966Bis(2-Chloroethyl)ether 1 04/29/22 18:57 V18184JMV
<0.199 mg/Kg - dry 0.199 0.483Bis(2-Chloroisopropyl)ether 1 04/29/22 18:57 V18184JMV
<0.175 mg/Kg - dry 0.175 0.966Bis(2-ethylhexyl)phthalate 1 04/29/22 18:57 V18184JMV
<0.159 mg/Kg - dry 0.159 0.9664-Bromophenyl phenyl ether 1 04/29/22 18:57 V18184JMV
<0.165 mg/Kg - dry 0.165 0.483Butyl benzyl phthalate 1 04/29/22 18:57 V18184JMV
<0.135 mg/Kg - dry 0.135 0.9664-Chloro-3-methylphenol 1 04/29/22 18:57 V18184JMV
<0.163 mg/Kg - dry 0.163 0.483
4-Chloroaniline 1 04/29/22 18:57 V18184JMV
<0.169 mg/Kg - dry 0.169 0.9662-Chloronaphthalene 1 04/29/22 18:57 V18184JMV
<0.143 mg/Kg - dry 0.143 0.9662-Chlorophenol 1 04/29/22 18:57 V18184JMV
<0.184 mg/Kg - dry 0.184 1.464-Chlorophenyl phenyl ether 1 04/29/22 18:57 V18184JMV
<0.207 mg/Kg - dry 0.207 0.966Chrysene 1 04/29/22 18:57 V18184JMV
<0.336 mg/Kg - dry 0.336 0.966Dibenz(a,h)anthracene 1 04/29/22 18:57 V18184JMV
<0.174 mg/Kg - dry 0.174 0.966Dibenzofuran 1 04/29/22 18:57 V18184JMV
<0.138 mg/Kg - dry 0.138 0.966
1,2-Dichlorobenzene 1 04/29/22 18:57 V18184JMV
<0.142 mg/Kg - dry 0.142 0.9661,3-Dichlorobenzene 1 04/29/22 18:57 V18184JMV
<0.142 mg/Kg - dry 0.142 0.4831,4-Dichlorobenzene 1 04/29/22 18:57 V18184JMV
<0.215 mg/Kg - dry 0.215 0.9663,3'-Dichlorobenzidine 1 04/29/22 18:57 V18184JMV
<0.140 mg/Kg - dry 0.140 0.9662,4-Dichlorophenol 1 04/29/22 18:57 V18184JMV
<0.263 mg/Kg - dry 0.263 0.966Diethyl phthalate 1 04/29/22 18:57 V18184JMV
<0.254 mg/Kg - dry 0.254 0.966Dimethyl phthalate 1 04/29/22 18:57 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.158 mg/Kg - dry 0.158 0.4832,4-Dimethylphenol 1 04/29/22 18:57 V18184JMV
<0.156 mg/Kg - dry 0.156 0.966Di-n-butyl phthalate 1 04/29/22 18:57 V18184JMV
<0.351 mg/Kg - dry 0.351 2.204,6-Dinitro-2-methylphenol 1 04/29/22 18:57 V18184JMV
<0.761 mg/Kg - dry 0.761 2.202,4-Dinitrophenol 1 04/29/22 18:57 V18184JMV
<0.141 mg/Kg - dry 0.141 0.9662,4-Dinitrotoluene 1 04/29/22 18:57 V18184JMV
<0.158 mg/Kg - dry 0.158 0.9662,6-Dinitrotoluene 1 04/29/22 18:57 V18184JMV
<0.209 mg/Kg - dry 0.209 0.483Di-n-Octyl Phthalate 1 04/29/22 18:57 V18184JMV
<0.180 mg/Kg - dry 0.180 0.966Fluoranthene 1 04/29/22 18:57 V18184JMV
<0.187 mg/Kg - dry 0.187 0.966
Fluorene 1 04/29/22 18:57 V18184JMV
<0.155 mg/Kg - dry 0.155 0.966Hexachlorobenzene 1 04/29/22 18:57 V18184JMV
<0.142 mg/Kg - dry 0.142 0.966Hexachlorobutadiene 1 04/29/22 18:57 V18184JMV
<0.229 mg/Kg - dry 0.229 0.966Hexachlorocyclopentadiene 1 04/29/22 18:57 V18184JMV
<0.115 mg/Kg - dry 0.115 0.966Hexachloroethane 1 04/29/22 18:57 V18184JMV
<0.262 mg/Kg - dry 0.262 0.966Indeno(1,2,3-cd)pyrene 1 04/29/22 18:57 V18184JMV
<0.279 mg/Kg - dry 0.279 0.966Isophorone 1 04/29/22 18:57 V18184JMV
<0.155 mg/Kg - dry 0.155 0.966
1-Methylnaphthalene 1 04/29/22 18:57 V18184JMV
<0.146 mg/Kg - dry 0.146 0.9662-Methylnaphthalene 1 04/29/22 18:57 V18184JMV
<0.142 mg/Kg - dry 0.142 0.9662-Methylphenol 1 04/29/22 18:57 V18184JMV
<0.124 mg/Kg - dry 0.124 0.9663&4 Methylphenol 1 04/29/22 18:57 V18184JMV
<0.210 mg/Kg - dry 0.210 0.966Naphthalene 1 04/29/22 18:57 V18184JMV
<0.141 mg/Kg - dry 0.141 0.9662-Nitroaniline 1 04/29/22 18:57 V18184JMV
<0.175 mg/Kg - dry 0.175 0.9663-Nitroaniline 1 04/29/22 18:57 V18184JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18088 04/28/22 08:48
<0.136 mg/Kg - dry 0.136 0.4834-Nitroaniline 1 04/29/22 18:57 V18184JMV
<0.169 mg/Kg - dry 0.169 0.483Nitrobenzene 1 04/29/22 18:57 V18184JMV
<0.130 mg/Kg - dry 0.130 0.9662-Nitrophenol 1 04/29/22 18:57 V18184JMV
<0.171 mg/Kg - dry 0.171 0.9664-Nitrophenol 1 04/29/22 18:57 V18184JMV
<0.385 mg/Kg - dry 0.385 0.966N-Nitrosodimethylamine 1 04/29/22 18:57 V18184JMV
<0.265 mg/Kg - dry 0.265 0.966N-Nitrosodiphenylamine 1 04/29/22 18:57 V18184JMV
<0.172 mg/Kg - dry 0.172 0.966N-Nitroso-di-n-propylamine 1 04/29/22 18:57 V18184JMV
<0.508 mg/Kg - dry 0.508 1.46Pentachlorophenol 1 04/29/22 18:57 V18184JMV
<0.304 mg/Kg - dry 0.304 0.966
Phenanthrene 1 04/29/22 18:57 V18184JMV
<0.163 mg/Kg - dry 0.163 0.966Phenol 1 04/29/22 18:57 V18184JMV
<0.196 mg/Kg - dry 0.196 0.966Pyrene 1 04/29/22 18:57 V18184JMV
<0.115 mg/Kg - dry 0.115 0.483Pyridine 1 04/29/22 18:57 V18184JMV
<0.156 mg/Kg - dry 0.156 0.9661,2,4-Trichlorobenzene 1 04/29/22 18:57 V18184JMV
<0.140 mg/Kg - dry 0.140 0.9662,4,5-Trichlorophenol 1 04/29/22 18:57 V18184JMV
<0.141 mg/Kg - dry 0.141 0.9662,4,6-Trichlorophenol 1 04/29/22 18:57 V18184JMV
8270ESurrogate: Phenol-d5 81.7 Limits: 34-121%04/29/22 18:571 JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%04/29/22 18:571 JMV V18184
Surrogate: 2-Fluorophenol 95.5 Limits: 35-115%04/29/22 18:571 JMV V18184
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%04/29/22 18:571 JMV V18184
Surrogate: 4-Terphenyl-d14 110 Limits: 54-127%04/29/22 18:571 JMV V18184
Surrogate: 2,4,6-Tribromophenol 93.4 Limits: 39-132%04/29/22 18:571 JMV V18184
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:NW6@8
99480 Matrix:
4/21/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18051 04/27/22 09:10
<13.4 mg/Kg - dry 13.4 72.9Aliphatic C9-C18 1 05/03/22 21:00 V18269JC1
<17.9 mg/Kg - dry 17.9 72.9Aliphatic C19-C36 1 05/03/22 21:00 V18269JC1
<20.6 mg/Kg - dry 20.6 72.9Aromatic C11-C22 1 05/03/22 21:00 V18269JC1
MADEP-EPHSurrogate: 2-Bromonaphthalene 71.4 Limits: 40-140%05/03/22 21:001 JC1
MADEP-EPHSurrogate: Chlorooctadecane 73.4 Limits: 40-140%05/03/22 21:001 JC1
MADEP-EPHSurrogate: OTP Surrogate 62.3 Limits: 40-140%05/03/22 21:001 JC1
Surrogate: 2-Fluorobiphenyl 69.8 Limits: 40-140%05/03/22 21:001 JC1 V18269
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.79 mg/Kg - dry 1.79 11.7
Aliphatic C5-C8 100 04/26/22 19:20 V18008TBL
<6.68 mg/Kg - dry 6.68 11.7Aliphatic C9-C12 100 04/26/22 19:20 V18008TBL
<0.913 mg/Kg - dry 0.913 11.7Aromatic C9-C10 100 04/26/22 19:20 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)85.3 Limits: 70-130%04/26/22 19:20100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)96.7 Limits: 70-130%04/26/22 19:20100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
0.026 mg/Kg - dry 0.002 0.024Acetone 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/27/22 13:13 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/27/22 13:13 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/27/22 13:13 V18106TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/27/22 13:13 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/27/22 13:13 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/27/22 13:13 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/27/22 13:13 V18106TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/27/22 13:13 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/27/22 13:13 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/27/22 13:13 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/27/22 13:13 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/27/22 13:13 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/27/22 13:13 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 04/27/22 13:13 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 04/27/22 13:13 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/27/22 13:13 V18106TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/27/22 13:13 V18106TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/27/22 13:13 V18106TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/27/22 13:13 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/27/22 13:13 V18106TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/27/22 13:13 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/27/22 13:13 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/27/22 13:13 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/27/22 13:13 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/27/22 13:13 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/27/22 13:13 V18106
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/27/22 13:131 TBL V18106
Surrogate: Dibromofluoromethane 104 Limits: 84-123%04/27/22 13:131 TBL V18106
Surrogate: Toluene-d8 94.6 Limits: 76-129%04/27/22 13:131 TBL V18106
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.144 mg/Kg - dry 0.144 0.822Acenaphthene 1 05/13/22 23:24 V18743JMV
<0.130 mg/Kg - dry 0.130 0.822Acenaphthylene 1 05/13/22 23:24 V18743JMV
<0.189 mg/Kg - dry 0.189 0.822Aniline 1 05/13/22 23:24 V18743JMV
<0.178 mg/Kg - dry 0.178 0.822Anthracene 1 05/13/22 23:24 V18743JMV
<0.173 mg/Kg - dry 0.173 0.822Benzo(a)anthracene 1 05/13/22 23:24 V18743JMV
<0.183 mg/Kg - dry 0.183 0.822Benzo(a)pyrene 1 05/13/22 23:24 V18743JMV
<0.182 mg/Kg - dry 0.182 0.822
Benzo(b)fluoranthene 1 05/13/22 23:24 V18743JMV
<0.169 mg/Kg - dry 0.169 0.822Benzo(g,h,i)perylene 1 05/13/22 23:24 V18743JMV
<0.170 mg/Kg - dry 0.170 0.822Benzo(k)fluoranthene 1 05/13/22 23:24 V18743JMV
<0.723 mg/Kg - dry 0.723 2.49Benzoic Acid 1 05/13/22 23:24 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.130 mg/Kg - dry 0.130 0.822Benzyl alcohol 1 05/13/22 23:24 V18743JMV
<0.147 mg/Kg - dry 0.147 0.822Bis(2-Chloroethoxy)methane 1 05/13/22 23:24 V18743JMV
<0.133 mg/Kg - dry 0.133 0.822Bis(2-Chloroethyl)ether 1 05/13/22 23:24 V18743JMV
<0.169 mg/Kg - dry 0.169 0.411Bis(2-Chloroisopropyl)ether 1 05/13/22 23:24 V18743JMV
<0.149 mg/Kg - dry 0.149 0.822Bis(2-ethylhexyl)phthalate 1 05/13/22 23:24 V18743JMV
<0.135 mg/Kg - dry 0.135 0.8224-Bromophenyl phenyl ether 1 05/13/22 23:24 V18743JMV
<0.140 mg/Kg - dry 0.140 0.411Butyl benzyl phthalate 1 05/13/22 23:24 V18743JMV
<0.115 mg/Kg - dry 0.115 0.8224-Chloro-3-methylphenol 1 05/13/22 23:24 V18743JMV
<0.139 mg/Kg - dry 0.139 0.411
4-Chloroaniline 1 05/13/22 23:24 V18743JMV
<0.144 mg/Kg - dry 0.144 0.8222-Chloronaphthalene 1 05/13/22 23:24 V18743JMV
<0.122 mg/Kg - dry 0.122 0.8222-Chlorophenol 1 05/13/22 23:24 V18743JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 05/13/22 23:24 V18743JMV
<0.177 mg/Kg - dry 0.177 0.822Chrysene 1 05/13/22 23:24 V18743JMV
<0.286 mg/Kg - dry 0.286 0.822Dibenz(a,h)anthracene 1 05/13/22 23:24 V18743JMV
<0.148 mg/Kg - dry 0.148 0.822Dibenzofuran 1 05/13/22 23:24 V18743JMV
<0.117 mg/Kg - dry 0.117 0.822
1,2-Dichlorobenzene 1 05/13/22 23:24 V18743JMV
<0.121 mg/Kg - dry 0.121 0.8221,3-Dichlorobenzene 1 05/13/22 23:24 V18743JMV
<0.121 mg/Kg - dry 0.121 0.4111,4-Dichlorobenzene 1 05/13/22 23:24 V18743JMV
<0.183 mg/Kg - dry 0.183 0.8223,3'-Dichlorobenzidine 1 05/13/22 23:24 V18743JMV
<0.119 mg/Kg - dry 0.119 0.8222,4-Dichlorophenol 1 05/13/22 23:24 V18743JMV
<0.224 mg/Kg - dry 0.224 0.822Diethyl phthalate 1 05/13/22 23:24 V18743JMV
<0.216 mg/Kg - dry 0.216 0.822Dimethyl phthalate 1 05/13/22 23:24 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.134 mg/Kg - dry 0.134 0.4112,4-Dimethylphenol 1 05/13/22 23:24 V18743JMV
<0.133 mg/Kg - dry 0.133 0.822Di-n-butyl phthalate 1 05/13/22 23:24 V18743JMV
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 05/13/22 23:24 V18743JMV
<0.648 mg/Kg - dry 0.648 1.872,4-Dinitrophenol 1 05/13/22 23:24 V18743JMV
<0.120 mg/Kg - dry 0.120 0.8222,4-Dinitrotoluene 1 05/13/22 23:24 V18743JMV
<0.134 mg/Kg - dry 0.134 0.8222,6-Dinitrotoluene 1 05/13/22 23:24 V18743JMV
<0.178 mg/Kg - dry 0.178 0.411Di-n-Octyl Phthalate 1 05/13/22 23:24 V18743JMV
<0.153 mg/Kg - dry 0.153 0.822Fluoranthene 1 05/13/22 23:24 V18743JMV
<0.159 mg/Kg - dry 0.159 0.822
Fluorene 1 05/13/22 23:24 V18743JMV
<0.132 mg/Kg - dry 0.132 0.822Hexachlorobenzene 1 05/13/22 23:24 V18743JMV
<0.121 mg/Kg - dry 0.121 0.822Hexachlorobutadiene 1 05/13/22 23:24 V18743JMV
<0.195 mg/Kg - dry 0.195 0.822Hexachlorocyclopentadiene 1 05/13/22 23:24 V18743JMV
<0.098 mg/Kg - dry 0.098 0.822Hexachloroethane 1 05/13/22 23:24 V18743JMV
<0.223 mg/Kg - dry 0.223 0.822Indeno(1,2,3-cd)pyrene 1 05/13/22 23:24 V18743JMV
<0.238 mg/Kg - dry 0.238 0.822Isophorone 1 05/13/22 23:24 V18743JMV
<0.132 mg/Kg - dry 0.132 0.822
1-Methylnaphthalene 1 05/13/22 23:24 V18743JMV
<0.124 mg/Kg - dry 0.124 0.8222-Methylnaphthalene 1 05/13/22 23:24 V18743JMV
<0.120 mg/Kg - dry 0.120 0.8222-Methylphenol 1 05/13/22 23:24 V18743JMV
<0.105 mg/Kg - dry 0.105 0.8223&4 Methylphenol 1 05/13/22 23:24 V18743JMV
<0.179 mg/Kg - dry 0.179 0.822Naphthalene 1 05/13/22 23:24 V18743JMV
<0.120 mg/Kg - dry 0.120 0.8222-Nitroaniline 1 05/13/22 23:24 V18743JMV
<0.149 mg/Kg - dry 0.149 0.8223-Nitroaniline 1 05/13/22 23:24 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.116 mg/Kg - dry 0.116 0.4114-Nitroaniline 1 05/13/22 23:24 V18743JMV
<0.144 mg/Kg - dry 0.144 0.411Nitrobenzene 1 05/13/22 23:24 V18743JMV
<0.110 mg/Kg - dry 0.110 0.8222-Nitrophenol 1 05/13/22 23:24 V18743JMV
<0.145 mg/Kg - dry 0.145 0.8224-Nitrophenol 1 05/13/22 23:24 V18743JMV
<0.327 mg/Kg - dry 0.327 0.822N-Nitrosodimethylamine 1 05/13/22 23:24 V18743JMV
<0.225 mg/Kg - dry 0.225 0.822N-Nitrosodiphenylamine 1 05/13/22 23:24 V18743JMV
<0.147 mg/Kg - dry 0.147 0.822N-Nitroso-di-n-propylamine 1 05/13/22 23:24 V18743JMV
<0.432 mg/Kg - dry 0.432 1.25Pentachlorophenol 1 05/13/22 23:24 V18743JMV
<0.259 mg/Kg - dry 0.259 0.822
Phenanthrene 1 05/13/22 23:24 V18743JMV
<0.139 mg/Kg - dry 0.139 0.822Phenol 1 05/13/22 23:24 V18743JMV
<0.167 mg/Kg - dry 0.167 0.822Pyrene 1 05/13/22 23:24 V18743JMV
<0.098 mg/Kg - dry 0.098 0.411Pyridine 1 05/13/22 23:24 V18743JMV
<0.133 mg/Kg - dry 0.133 0.8221,2,4-Trichlorobenzene 1 05/13/22 23:24 V18743JMV
<0.119 mg/Kg - dry 0.119 0.8222,4,5-Trichlorophenol 1 05/13/22 23:24 V18743JMV
<0.120 mg/Kg - dry 0.120 0.8222,4,6-Trichlorophenol 1 05/13/22 23:24 V18743JMV
8270ESurrogate: Phenol-d5 80.8 Limits: 34-121%05/13/22 23:241 JMV
Surrogate: 2-Fluorobiphenyl 87.4 Limits: 44-115%05/13/22 23:241 JMV V18743
Surrogate: 2-Fluorophenol 87.1 Limits: 35-115%05/13/22 23:241 JMV V18743
Surrogate: Nitrobenzene-d5 86.8 Limits: 37-122%05/13/22 23:241 JMV V18743
Surrogate: 4-Terphenyl-d14 93.4 Limits: 54-127%05/13/22 23:241 JMV V18743
Surrogate: 2,4,6-Tribromophenol 97.9 Limits: 39-132%05/13/22 23:241 JMV V18743
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:E6@8
99481 Matrix:
4/21/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18067 04/27/22 13:50
<11.4 mg/Kg - dry 11.4 62.0Aliphatic C9-C18 1 05/03/22 19:47 V18371JLK
<15.1 mg/Kg - dry 15.1 62.0Aliphatic C19-C36 1 05/03/22 19:47 V18371JLK
<17.6 mg/Kg - dry 17.6 62.0Aromatic C11-C22 1 05/03/22 19:47 V18371JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 73.0 Limits: 40-140%05/03/22 19:471 JLK
MADEP-EPHSurrogate: Chlorooctadecane 72.4 Limits: 40-140%05/03/22 19:471 JLK
MADEP-EPHSurrogate: OTP Surrogate 54.8 Limits: 40-140%05/03/22 19:471 JLK
Surrogate: 2-Fluorobiphenyl 73.0 Limits: 40-140%05/03/22 19:471 JLK V18371
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.52 mg/Kg - dry 1.52 9.98
Aliphatic C5-C8 100 04/26/22 19:44 V18008TBL
<5.69 mg/Kg - dry 5.69 9.98Aliphatic C9-C12 100 04/26/22 19:44 V18008TBL
<0.778 mg/Kg - dry 0.778 9.98Aromatic C9-C10 100 04/26/22 19:44 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)92.5 Limits: 70-130%04/26/22 19:44100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)106 Limits: 70-130%04/26/22 19:44100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.0 %Moisture 1 04/29/22 11:32 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
0.017 J mg/Kg - dry 0.002 0.024Acetone 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/27/22 13:41 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/27/22 13:41 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/27/22 13:41 V18106TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/27/22 13:41 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/27/22 13:41 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/27/22 13:41 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/27/22 13:41 V18106TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/27/22 13:41 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/27/22 13:41 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/27/22 13:41 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/27/22 13:41 V18106TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/27/22 13:41 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/27/22 13:41 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/27/22 13:41 V18106TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/27/22 13:41 V18106TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 04/27/22 13:41 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/27/22 13:41 V18106TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/27/22 13:41 V18106TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/27/22 13:41 V18106TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/27/22 13:41 V18106TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/27/22 13:41 V18106TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/27/22 13:41 V18106TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/27/22 13:41 V18106TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/27/22 13:41 V18106TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18105 04/27/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/27/22 13:41 V18106TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/27/22 13:41 V18106TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/27/22 13:41 V18106
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/27/22 13:411 TBL V18106
Surrogate: Dibromofluoromethane 102 Limits: 84-123%04/27/22 13:411 TBL V18106
Surrogate: Toluene-d8 94.6 Limits: 76-129%04/27/22 13:411 TBL V18106
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.141 mg/Kg - dry 0.141 0.804Acenaphthene 1 05/13/22 23:47 V18743JMV
<0.128 mg/Kg - dry 0.128 0.804Acenaphthylene 1 05/13/22 23:47 V18743JMV
<0.185 mg/Kg - dry 0.185 0.804Aniline 1 05/13/22 23:47 V18743JMV
<0.174 mg/Kg - dry 0.174 0.804Anthracene 1 05/13/22 23:47 V18743JMV
<0.169 mg/Kg - dry 0.169 0.804Benzo(a)anthracene 1 05/13/22 23:47 V18743JMV
<0.179 mg/Kg - dry 0.179 0.804Benzo(a)pyrene 1 05/13/22 23:47 V18743JMV
<0.178 mg/Kg - dry 0.178 0.804
Benzo(b)fluoranthene 1 05/13/22 23:47 V18743JMV
<0.165 mg/Kg - dry 0.165 0.804Benzo(g,h,i)perylene 1 05/13/22 23:47 V18743JMV
<0.167 mg/Kg - dry 0.167 0.804Benzo(k)fluoranthene 1 05/13/22 23:47 V18743JMV
<0.707 mg/Kg - dry 0.707 2.44Benzoic Acid 1 05/13/22 23:47 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.128 mg/Kg - dry 0.128 0.804Benzyl alcohol 1 05/13/22 23:47 V18743JMV
<0.143 mg/Kg - dry 0.143 0.804Bis(2-Chloroethoxy)methane 1 05/13/22 23:47 V18743JMV
<0.130 mg/Kg - dry 0.130 0.804Bis(2-Chloroethyl)ether 1 05/13/22 23:47 V18743JMV
<0.165 mg/Kg - dry 0.165 0.402Bis(2-Chloroisopropyl)ether 1 05/13/22 23:47 V18743JMV
<0.146 mg/Kg - dry 0.146 0.804Bis(2-ethylhexyl)phthalate 1 05/13/22 23:47 V18743JMV
<0.132 mg/Kg - dry 0.132 0.8044-Bromophenyl phenyl ether 1 05/13/22 23:47 V18743JMV
<0.137 mg/Kg - dry 0.137 0.402Butyl benzyl phthalate 1 05/13/22 23:47 V18743JMV
<0.112 mg/Kg - dry 0.112 0.8044-Chloro-3-methylphenol 1 05/13/22 23:47 V18743JMV
<0.136 mg/Kg - dry 0.136 0.402
4-Chloroaniline 1 05/13/22 23:47 V18743JMV
<0.141 mg/Kg - dry 0.141 0.8042-Chloronaphthalene 1 05/13/22 23:47 V18743JMV
<0.119 mg/Kg - dry 0.119 0.8042-Chlorophenol 1 05/13/22 23:47 V18743JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 05/13/22 23:47 V18743JMV
<0.173 mg/Kg - dry 0.173 0.804Chrysene 1 05/13/22 23:47 V18743JMV
<0.280 mg/Kg - dry 0.280 0.804Dibenz(a,h)anthracene 1 05/13/22 23:47 V18743JMV
<0.145 mg/Kg - dry 0.145 0.804Dibenzofuran 1 05/13/22 23:47 V18743JMV
<0.115 mg/Kg - dry 0.115 0.804
1,2-Dichlorobenzene 1 05/13/22 23:47 V18743JMV
<0.118 mg/Kg - dry 0.118 0.8041,3-Dichlorobenzene 1 05/13/22 23:47 V18743JMV
<0.118 mg/Kg - dry 0.118 0.4021,4-Dichlorobenzene 1 05/13/22 23:47 V18743JMV
<0.179 mg/Kg - dry 0.179 0.8043,3'-Dichlorobenzidine 1 05/13/22 23:47 V18743JMV
<0.116 mg/Kg - dry 0.116 0.8042,4-Dichlorophenol 1 05/13/22 23:47 V18743JMV
<0.219 mg/Kg - dry 0.219 0.804Diethyl phthalate 1 05/13/22 23:47 V18743JMV
<0.212 mg/Kg - dry 0.212 0.804Dimethyl phthalate 1 05/13/22 23:47 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.131 mg/Kg - dry 0.131 0.4022,4-Dimethylphenol 1 05/13/22 23:47 V18743JMV
<0.130 mg/Kg - dry 0.130 0.804Di-n-butyl phthalate 1 05/13/22 23:47 V18743JMV
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 05/13/22 23:47 V18743JMV
<0.634 mg/Kg - dry 0.634 1.832,4-Dinitrophenol 1 05/13/22 23:47 V18743JMV
<0.117 mg/Kg - dry 0.117 0.8042,4-Dinitrotoluene 1 05/13/22 23:47 V18743JMV
<0.131 mg/Kg - dry 0.131 0.8042,6-Dinitrotoluene 1 05/13/22 23:47 V18743JMV
<0.174 mg/Kg - dry 0.174 0.402Di-n-Octyl Phthalate 1 05/13/22 23:47 V18743JMV
<0.150 mg/Kg - dry 0.150 0.804Fluoranthene 1 05/13/22 23:47 V18743JMV
<0.156 mg/Kg - dry 0.156 0.804
Fluorene 1 05/13/22 23:47 V18743JMV
<0.129 mg/Kg - dry 0.129 0.804Hexachlorobenzene 1 05/13/22 23:47 V18743JMV
<0.119 mg/Kg - dry 0.119 0.804Hexachlorobutadiene 1 05/13/22 23:47 V18743JMV
<0.191 mg/Kg - dry 0.191 0.804Hexachlorocyclopentadiene 1 05/13/22 23:47 V18743JMV
<0.096 mg/Kg - dry 0.096 0.804Hexachloroethane 1 05/13/22 23:47 V18743JMV
<0.218 mg/Kg - dry 0.218 0.804Indeno(1,2,3-cd)pyrene 1 05/13/22 23:47 V18743JMV
<0.232 mg/Kg - dry 0.232 0.804Isophorone 1 05/13/22 23:47 V18743JMV
<0.129 mg/Kg - dry 0.129 0.804
1-Methylnaphthalene 1 05/13/22 23:47 V18743JMV
<0.121 mg/Kg - dry 0.121 0.8042-Methylnaphthalene 1 05/13/22 23:47 V18743JMV
<0.118 mg/Kg - dry 0.118 0.8042-Methylphenol 1 05/13/22 23:47 V18743JMV
<0.103 mg/Kg - dry 0.103 0.8043&4 Methylphenol 1 05/13/22 23:47 V18743JMV
<0.175 mg/Kg - dry 0.175 0.804Naphthalene 1 05/13/22 23:47 V18743JMV
<0.117 mg/Kg - dry 0.117 0.8042-Nitroaniline 1 05/13/22 23:47 V18743JMV
<0.146 mg/Kg - dry 0.146 0.8043-Nitroaniline 1 05/13/22 23:47 V18743JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V18145 04/29/22 08:51
<0.113 mg/Kg - dry 0.113 0.4024-Nitroaniline 1 05/13/22 23:47 V18743JMV
<0.141 mg/Kg - dry 0.141 0.402Nitrobenzene 1 05/13/22 23:47 V18743JMV
<0.108 mg/Kg - dry 0.108 0.8042-Nitrophenol 1 05/13/22 23:47 V18743JMV
<0.142 mg/Kg - dry 0.142 0.8044-Nitrophenol 1 05/13/22 23:47 V18743JMV
<0.320 mg/Kg - dry 0.320 0.804N-Nitrosodimethylamine 1 05/13/22 23:47 V18743JMV
<0.220 mg/Kg - dry 0.220 0.804N-Nitrosodiphenylamine 1 05/13/22 23:47 V18743JMV
<0.143 mg/Kg - dry 0.143 0.804N-Nitroso-di-n-propylamine 1 05/13/22 23:47 V18743JMV
<0.423 mg/Kg - dry 0.423 1.22Pentachlorophenol 1 05/13/22 23:47 V18743JMV
<0.253 mg/Kg - dry 0.253 0.804
Phenanthrene 1 05/13/22 23:47 V18743JMV
<0.136 mg/Kg - dry 0.136 0.804Phenol 1 05/13/22 23:47 V18743JMV
<0.163 mg/Kg - dry 0.163 0.804Pyrene 1 05/13/22 23:47 V18743JMV
<0.096 mg/Kg - dry 0.096 0.402Pyridine 1 05/13/22 23:47 V18743JMV
<0.130 mg/Kg - dry 0.130 0.8041,2,4-Trichlorobenzene 1 05/13/22 23:47 V18743JMV
<0.117 mg/Kg - dry 0.117 0.8042,4,5-Trichlorophenol 1 05/13/22 23:47 V18743JMV
<0.117 mg/Kg - dry 0.117 0.8042,4,6-Trichlorophenol 1 05/13/22 23:47 V18743JMV
8270ESurrogate: Phenol-d5 86.5 Limits: 34-121%05/13/22 23:471 JMV
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%05/13/22 23:471 JMV V18743
Surrogate: 2-Fluorophenol 91.0 Limits: 35-115%05/13/22 23:471 JMV V18743
Surrogate: Nitrobenzene-d5 90.4 Limits: 37-122%05/13/22 23:471 JMV V18743
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%05/13/22 23:471 JMV V18743
Surrogate: 2,4,6-Tribromophenol 105 Limits: 39-132%05/13/22 23:471 JMV V18743
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 116
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27609
22-115-0003
01191
Spangler Environmental
4338 Bland Road
Cal Rieder
Raleigh
Received : 04/22/2022
Edge of Auburn
Report Date : 05/17/2022
Sample ID :
Lab No :
Sampled:S4@6
99482 Matrix:
4/21/2022 16:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V18067 04/27/22 13:50
<11.2 mg/Kg - dry 11.2 60.7Aliphatic C9-C18 1 05/03/22 20:23 V18371JLK
<14.9 mg/Kg - dry 14.9 60.7Aliphatic C19-C36 1 05/03/22 20:23 V18371JLK
<17.2 mg/Kg - dry 17.2 60.7Aromatic C11-C22 1 05/03/22 20:23 V18371JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 80.4 Limits: 40-140%05/03/22 20:231 JLK
MADEP-EPHSurrogate: Chlorooctadecane 69.8 Limits: 40-140%05/03/22 20:231 JLK
MADEP-EPHSurrogate: OTP Surrogate 55.3 Limits: 40-140%05/03/22 20:231 JLK
Surrogate: 2-Fluorobiphenyl 79.4 Limits: 40-140%05/03/22 20:231 JLK V18371
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18007 04/26/22 08:00
<1.49 mg/Kg - dry 1.49 9.76
Aliphatic C5-C8 100 04/26/22 20:07 V18008TBL
<5.56 mg/Kg - dry 5.56 9.76Aliphatic C9-C12 100 04/26/22 20:07 V18008TBL
<0.760 mg/Kg - dry 0.760 9.76Aromatic C9-C10 100 04/26/22 20:07 V18008TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)79.7 Limits: 70-130%04/26/22 20:07100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.1 Limits: 70-130%04/26/22 20:07100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18029 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/22 14:150.0200.002<0.002mg/KgAcetone
04/26/22 14:150.0200.001<0.001mg/KgAcrolein
04/26/22 14:150.0200.0008<0.0008mg/KgAcrylonitrile
04/26/22 14:150.0050.0006<0.0006mg/KgBenzene
04/26/22 14:150.0050.0005<0.0005mg/KgBromobenzene
04/26/22 14:150.0050.0008<0.0008mg/KgBromochloromethane
04/26/22 14:150.0050.001<0.001mg/KgBromodichloromethane
04/26/22 14:150.0050.001<0.001mg/KgBromoform
04/26/22 14:150.0100.001<0.001mg/KgBromomethane
04/26/22 14:150.0050.0005<0.0005mg/Kgn-Butylbenzene
04/26/22 14:150.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/26/22 14:150.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/26/22 14:150.0050.0006<0.0006mg/KgCarbon Disulfide
04/26/22 14:150.0050.001<0.001mg/KgCarbon Tetrachloride
04/26/22 14:150.0050.0007<0.0007mg/KgChlorobenzene
04/26/22 14:150.0050.0009<0.0009mg/KgChlorodibromomethane
04/26/22 14:150.0100.0009<0.0009mg/KgChloroethane
04/26/22 14:150.0050.001<0.001mg/KgChloroform
04/26/22 14:150.0100.0006<0.0006mg/KgChloromethane
04/26/22 14:150.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/26/22 14:150.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/26/22 14:150.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/26/22 14:150.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/26/22 14:150.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/26/22 14:150.0050.0006<0.0006mg/KgDibromomethane
04/26/22 14:150.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/26/22 14:150.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 35Date:05/17/2022 11:33 AM
Page 80 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18029 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/22 14:150.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/26/22 14:150.0100.001<0.001mg/KgDichlorodifluoromethane
04/26/22 14:150.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/26/22 14:150.0050.001<0.001mg/Kg1,2-Dichloroethane
04/26/22 14:150.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/26/22 14:150.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/26/22 14:150.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/26/22 14:150.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/26/22 14:150.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/26/22 14:150.0050.001<0.001mg/Kg2,2-Dichloropropane
04/26/22 14:150.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/26/22 14:150.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/26/22 14:150.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/26/22 14:150.0050.0006<0.0006mg/KgEthylbenzene
04/26/22 14:150.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/26/22 14:150.0100.0008<0.0008mg/KgHexachlorobutadiene
04/26/22 14:150.0100.0007<0.0007mg/Kgn-Hexane
04/26/22 14:150.0200.0006<0.0006mg/Kg2-Hexanone
04/26/22 14:150.0050.0005<0.0005mg/KgIsopropylbenzene
04/26/22 14:150.0050.001<0.001mg/Kg4-Isopropyl toluene
04/26/22 14:150.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/26/22 14:150.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/26/22 14:150.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/26/22 14:150.0100.001<0.001mg/KgMethylene Chloride
04/26/22 14:150.0100.0010<0.0010mg/KgNaphthalene
04/26/22 14:150.0050.0005<0.0005mg/Kgn-Propylbenzene
04/26/22 14:150.0050.001<0.001mg/KgStyrene
Page 2 of 35Date:05/17/2022 11:33 AM
Page 81 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18029 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/22 14:150.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/26/22 14:150.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/26/22 14:150.0050.0009<0.0009mg/KgTetrachloroethene
04/26/22 14:150.0050.0007<0.0007mg/KgToluene
04/26/22 14:150.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/26/22 14:150.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/26/22 14:150.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/26/22 14:150.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/26/22 14:150.0050.0009<0.0009mg/KgTrichloroethene
04/26/22 14:150.0100.002<0.002mg/KgTrichlorofluoromethane
04/26/22 14:150.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/26/22 14:150.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/26/22 14:150.0100.0005<0.0005mg/KgVinyl Acetate
04/26/22 14:150.0100.0005<0.0005mg/KgVinyl Chloride
04/26/22 14:150.0050.0005<0.0005mg/Kgo-Xylene
04/26/22 14:150.0100.001<0.001mg/Kgm,p-Xylene
04/26/22 14:154-Bromofluorobenzene (S)101 70-130
04/26/22 14:15Dibromofluoromethane (S)102 84-123
04/26/22 14:15Toluene-d8 (S)95.4 76-129
LCS-V18029 LCSD-V18029Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.078 78.480.80.0800.100mg/KgAcetone 29-198 3.0 20
0.114 1141150.1150.100mg/KgAcrolein 70-130 0.8 20
0.115 1151140.1140.100mg/KgAcrylonitrile 65-134 0.8 20
Page 3 of 35Date:05/17/2022 11:33 AM
Page 82 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
LCS-V18029 LCSD-V18029Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.61010.0500.050mg/KgBenzene 74-127 3.0 20
0.044 89.691.60.0450.050mg/KgBromobenzene 73-125 2.2 20
0.053 1061060.0530.050mg/KgBromochloromethane 72-134 0.3 20
0.050 1011010.0500.050mg/KgBromodichloromethane 75-122 0.5 20
0.051 10399.80.0490.050mg/KgBromoform 66-135 2.7 20
0.045 91.292.20.0460.050mg/KgBromomethane 20-180 1.0 20
0.045 90.893.80.0460.050mg/Kgn-Butylbenzene 65-135 3.2 20
0.044 89.092.20.0460.050mg/Kgsec-Butyl benzene 66-131 3.5 20
0.044 89.292.20.0460.050mg/Kgtert-Butyl benzene 67-132 3.3 20
0.046 92.096.00.0480.050mg/KgCarbon Disulfide 61-129 4.2 20
0.045 91.899.00.0490.050mg/KgCarbon Tetrachloride 64-143 7.5 20
0.047 94.293.40.0460.050mg/KgChlorobenzene 74-118 0.8 20
0.048 97.296.40.0480.050mg/KgChlorodibromomethane 73-122 0.8 20
0.048 97.697.00.0480.050mg/KgChloroethane 33-149 0.6 20
0.048 97.898.20.0490.050mg/KgChloroform 73-127 0.4 20
0.045 91.290.00.0450.050mg/KgChloromethane 45-143 1.3 20
0.044 89.290.40.0450.050mg/Kg2-Chlorotoluene 67-124 1.3 20
0.044 89.891.80.0450.050mg/Kg4-Chlorotoluene 71-126 2.2 20
0.049 99.61010.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.9 20
0.056 1131130.0560.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.1 20
0.049 99.299.00.0490.050mg/Kg1,2-Dibromoethane 70-132 0.2 20
0.051 1031050.0520.050mg/KgDibromomethane 74-133 1.3 20
0.045 91.092.60.0460.050mg/Kg1,2-Dichlorobenzene 72-123 1.7 20
0.045 90.891.20.0450.050mg/Kg1,3-Dichlorobenzene 71-120 0.4 20
0.045 90.491.20.0450.050mg/Kg1,4-Dichlorobenzene 71-123 0.8 20
0.037 75.679.00.0390.050mg/KgDichlorodifluoromethane 26-146 4.3 20
Page 4 of 35Date:05/17/2022 11:33 AM
Page 83 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
LCS-V18029 LCSD-V18029Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.21000.0500.050mg/Kg1,1-Dichloroethane 74-127 1.8 20
0.050 1021010.0500.050mg/Kg1,2-Dichloroethane 68-128 0.9 20
0.046 92.897.60.0480.050mg/Kg1,1-Dichloroethene 67-149 5.0 20
0.048 97.898.40.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 0.6 20
0.047 94.298.20.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.1 20
0.048 97.81000.0500.050mg/Kg1,2-Dichloropropane 73-130 2.2 20
0.049 98.297.20.0480.050mg/Kg1,3-Dichloropropane 75-124 1.0 20
0.049 98.21030.0510.050mg/Kg2,2-Dichloropropane 50-142 4.7 20
0.047 94.81000.0500.050mg/Kg1,1-Dichloropropene 71-130 5.5 20
0.051 1031040.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 0.7 20
0.052 1051050.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.0 20
0.046 92.292.80.0460.050mg/KgEthylbenzene 74-128 0.6 20
0.084 84.984.20.0840.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.8 20
0.044 89.493.60.0460.050mg/KgHexachlorobutadiene 64-125 4.5 20
0.049 98.81050.0520.050mg/Kgn-Hexane 70-130 6.4 20
0.053 1061040.0520.050mg/Kg2-Hexanone 61-157 1.9 20
0.044 89.691.60.0450.050mg/KgIsopropylbenzene 68-126 2.2 20
0.045 91.093.00.0460.050mg/Kg4-Isopropyl toluene 68-129 2.1 20
0.048 96.097.60.0480.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.6 20
0.046 93.493.00.0460.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.4 20
0.058 1161170.0580.050mg/Kg4-Methyl-2-Pentanone 57-162 0.3 20
0.047 95.296.80.0480.050mg/KgMethylene Chloride 74-129 1.6 20
0.058 1171210.0600.050mg/KgNaphthalene 57-157 2.8 20
0.045 91.092.60.0460.050mg/Kgn-Propylbenzene 67-130 1.7 20
0.048 97.097.40.0480.050mg/KgStyrene 77-121 0.4 20
0.047 95.493.40.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.1 20
Page 5 of 35Date:05/17/2022 11:33 AM
Page 84 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18030QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18029
LCS-V18029 LCSD-V18029Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 10099.20.0490.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.8 20
0.048 97.21000.0500.050mg/KgTetrachloroethene 68-130 3.0 20
0.048 96.899.80.0490.050mg/KgToluene 71-129 3.0 20
0.049 98.499.40.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.0 20
0.048 96.497.80.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.4 20
0.048 96.61000.0500.050mg/Kg1,1,1-Trichloroethane 67-131 3.4 20
0.049 98.696.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 2.0 20
0.048 97.698.80.0490.050mg/KgTrichloroethene 75-133 1.2 20
0.044 88.292.80.0460.050mg/KgTrichlorofluoromethane 44-146 5.0 20
0.051 10299.00.0490.050mg/Kg1,2,3-Trichloropropane 60-137 3.1 20
0.045 90.892.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.9 20
0.055 1121080.0530.050mg/KgVinyl Acetate 60-140 3.6 20
0.043 87.490.40.0450.050mg/KgVinyl Chloride 48-147 3.3 20
0.046 92.893.20.0460.050mg/Kgo-Xylene 74-126 0.4 20
0.094 94.494.80.0940.100mg/Kgm,p-Xylene 75-124 0.4 20
99.499.84-Bromofluorobenzene (S)70-130
103103Dibromofluoromethane (S)84-123
95.494.2Toluene-d8 (S)76-129
Page 6 of 35Date:05/17/2022 11:33 AM
Page 85 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
Associated Lab Samples: 99481, 99482
LRB-V18105 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/27/22 11:500.0200.002<0.002mg/KgAcetone
04/27/22 11:500.0200.001<0.001mg/KgAcrolein
04/27/22 11:500.0200.0008<0.0008mg/KgAcrylonitrile
04/27/22 11:500.0050.0006<0.0006mg/KgBenzene
04/27/22 11:500.0050.0005<0.0005mg/KgBromobenzene
04/27/22 11:500.0050.0008<0.0008mg/KgBromochloromethane
04/27/22 11:500.0050.001<0.001mg/KgBromodichloromethane
04/27/22 11:500.0050.001<0.001mg/KgBromoform
04/27/22 11:500.0100.001<0.001mg/KgBromomethane
04/27/22 11:500.0050.0005<0.0005mg/Kgn-Butylbenzene
04/27/22 11:500.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/27/22 11:500.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/27/22 11:500.0050.0006<0.0006mg/KgCarbon Disulfide
04/27/22 11:500.0050.001<0.001mg/KgCarbon Tetrachloride
04/27/22 11:500.0050.0007<0.0007mg/KgChlorobenzene
04/27/22 11:500.0050.0009<0.0009mg/KgChlorodibromomethane
04/27/22 11:500.0100.0009<0.0009mg/KgChloroethane
04/27/22 11:500.0050.001<0.001mg/KgChloroform
04/27/22 11:500.0100.0006<0.0006mg/KgChloromethane
04/27/22 11:500.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/27/22 11:500.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/27/22 11:500.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/27/22 11:500.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/27/22 11:500.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/27/22 11:500.0050.0006<0.0006mg/KgDibromomethane
04/27/22 11:500.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/27/22 11:500.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 7 of 35Date:05/17/2022 11:33 AM
Page 86 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
Associated Lab Samples: 99481, 99482
LRB-V18105 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/27/22 11:500.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/27/22 11:500.0100.001<0.001mg/KgDichlorodifluoromethane
04/27/22 11:500.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/27/22 11:500.0050.001<0.001mg/Kg1,2-Dichloroethane
04/27/22 11:500.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/27/22 11:500.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/27/22 11:500.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/27/22 11:500.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/27/22 11:500.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/27/22 11:500.0050.001<0.001mg/Kg2,2-Dichloropropane
04/27/22 11:500.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/27/22 11:500.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/27/22 11:500.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/27/22 11:500.0050.0006<0.0006mg/KgEthylbenzene
04/27/22 11:500.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/27/22 11:500.0100.0008<0.0008mg/KgHexachlorobutadiene
04/27/22 11:500.0100.0007<0.0007mg/Kgn-Hexane
04/27/22 11:500.0200.0006<0.0006mg/Kg2-Hexanone
04/27/22 11:500.0050.0005<0.0005mg/KgIsopropylbenzene
04/27/22 11:500.0050.001<0.001mg/Kg4-Isopropyl toluene
04/27/22 11:500.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/27/22 11:500.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/27/22 11:500.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/27/22 11:500.0100.001<0.001mg/KgMethylene Chloride
04/27/22 11:500.0100.0010<0.0010mg/KgNaphthalene
04/27/22 11:500.0050.0005<0.0005mg/Kgn-Propylbenzene
04/27/22 11:500.0050.001<0.001mg/KgStyrene
Page 8 of 35Date:05/17/2022 11:33 AM
Page 87 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
Associated Lab Samples: 99481, 99482
LRB-V18105 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/27/22 11:500.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/27/22 11:500.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/27/22 11:500.0050.0009<0.0009mg/KgTetrachloroethene
04/27/22 11:500.0050.0007<0.0007mg/KgToluene
04/27/22 11:500.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/27/22 11:500.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/27/22 11:500.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/27/22 11:500.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/27/22 11:500.0050.0009<0.0009mg/KgTrichloroethene
04/27/22 11:500.0100.002<0.002mg/KgTrichlorofluoromethane
04/27/22 11:500.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/27/22 11:500.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/27/22 11:500.0100.0005<0.0005mg/KgVinyl Acetate
04/27/22 11:500.0100.0005<0.0005mg/KgVinyl Chloride
04/27/22 11:500.0050.0005<0.0005mg/Kgo-Xylene
04/27/22 11:500.0100.001<0.001mg/Kgm,p-Xylene
04/27/22 11:504-Bromofluorobenzene (S)103 70-130
04/27/22 11:50Dibromofluoromethane (S)102 84-123
04/27/22 11:50Toluene-d8 (S)94.4 76-129
LCS-V18105 LCSD-V18105Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.106 10696.30.0960.100mg/KgAcetone 29-198 9.5 20
0.097 97.091.40.0910.100mg/KgAcrolein 70-130 5.9 20
0.107 10798.50.0980.100mg/KgAcrylonitrile 65-134 8.2 20
Page 9 of 35Date:05/17/2022 11:33 AM
Page 88 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
LCS-V18105 LCSD-V18105Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.41000.0500.050mg/KgBenzene 74-127 2.8 20
0.045 90.291.60.0450.050mg/KgBromobenzene 73-125 1.5 20
0.052 1041030.0510.050mg/KgBromochloromethane 72-134 0.5 20
0.050 1011020.0500.050mg/KgBromodichloromethane 75-122 0.3 20
0.050 10095.60.0470.050mg/KgBromoform 66-135 4.8 20
0.046 92.898.60.0490.050mg/KgBromomethane 20-180 6.0 20
0.045 91.496.00.0480.050mg/Kgn-Butylbenzene 65-135 4.9 20
0.045 90.094.00.0470.050mg/Kgsec-Butyl benzene 66-131 4.3 20
0.045 90.293.80.0460.050mg/Kgtert-Butyl benzene 67-132 3.9 20
0.046 92.697.20.0480.050mg/KgCarbon Disulfide 61-129 4.8 20
0.047 94.41000.0500.050mg/KgCarbon Tetrachloride 64-143 6.1 20
0.047 95.896.60.0480.050mg/KgChlorobenzene 74-118 0.8 20
0.048 96.694.40.0470.050mg/KgChlorodibromomethane 73-122 2.3 20
0.047 95.61020.0500.050mg/KgChloroethane 33-149 6.0 20
0.049 98.61010.0500.050mg/KgChloroform 73-127 2.8 20
0.047 94.296.60.0480.050mg/KgChloromethane 45-143 2.5 20
0.045 90.493.00.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.045 90.493.20.0460.050mg/Kg4-Chlorotoluene 71-126 3.0 20
0.049 99.01000.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.0 20
0.051 10393.20.0460.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 9.7 20
0.049 99.096.60.0480.050mg/Kg1,2-Dibromoethane 70-132 2.4 20
0.051 1021010.0500.050mg/KgDibromomethane 74-133 1.5 20
0.045 91.491.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 0.2 20
0.045 91.492.80.0460.050mg/Kg1,3-Dichlorobenzene 71-120 1.5 20
0.045 91.292.00.0460.050mg/Kg1,4-Dichlorobenzene 71-123 0.8 20
0.035 70.475.40.0370.050mg/KgDichlorodifluoromethane 26-146 6.8 20
Page 10 of 35Date:05/17/2022 11:33 AM
Page 89 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
LCS-V18105 LCSD-V18105Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.81010.0500.050mg/Kg1,1-Dichloroethane 74-127 3.2 20
0.050 10099.00.0490.050mg/Kg1,2-Dichloroethane 68-128 1.2 20
0.046 93.499.60.0490.050mg/Kg1,1-Dichloroethene 67-149 6.4 20
0.049 98.299.60.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 1.4 20
0.047 95.499.20.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.9 20
0.049 98.899.40.0490.050mg/Kg1,2-Dichloropropane 73-130 0.6 20
0.048 96.295.80.0470.050mg/Kg1,3-Dichloropropane 75-124 0.4 20
0.050 1001050.0520.050mg/Kg2,2-Dichloropropane 50-142 4.4 20
0.048 96.41010.0500.050mg/Kg1,1-Dichloropropene 71-130 4.6 20
0.051 1021010.0500.050mg/Kgcis-1,3-Dichloropropene 71-125 0.7 20
0.052 1041020.0500.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.5 20
0.046 92.695.80.0470.050mg/KgEthylbenzene 74-128 3.3 20
0.096 96.296.00.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.2 20
0.045 90.294.00.0470.050mg/KgHexachlorobutadiene 64-125 4.1 20
0.050 1021050.0520.050mg/Kgn-Hexane 70-130 3.2 20
0.048 97.689.40.0440.050mg/Kg2-Hexanone 61-157 8.7 20
0.045 90.293.20.0460.050mg/KgIsopropylbenzene 68-126 3.2 20
0.045 91.894.60.0470.050mg/Kg4-Isopropyl toluene 68-129 3.0 20
0.044 88.01060.0530.050mg/KgMethyl Ethyl Ketone (MEK)63-149 18.7 20
0.043 87.084.20.0420.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.2 20
0.053 10698.20.0490.050mg/Kg4-Methyl-2-Pentanone 57-162 7.6 20
0.047 94.895.20.0470.050mg/KgMethylene Chloride 74-129 0.4 20
0.055 1121060.0530.050mg/KgNaphthalene 57-157 4.7 20
0.045 91.494.60.0470.050mg/Kgn-Propylbenzene 67-130 3.4 20
0.049 98.099.80.0490.050mg/KgStyrene 77-121 1.8 20
0.047 95.297.60.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.4 20
Page 11 of 35Date:05/17/2022 11:33 AM
Page 90 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18106QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18105
LCS-V18105 LCSD-V18105Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.091.00.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 6.3 20
0.049 98.41010.0500.050mg/KgTetrachloroethene 68-130 2.6 20
0.048 96.899.80.0490.050mg/KgToluene 71-129 3.0 20
0.048 97.296.00.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.2 20
0.048 96.896.60.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.2 20
0.048 96.61000.0500.050mg/Kg1,1,1-Trichloroethane 67-131 3.8 20
0.048 96.494.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 2.5 20
0.048 96.81010.0500.050mg/KgTrichloroethene 75-133 4.2 20
0.042 84.889.00.0440.050mg/KgTrichlorofluoromethane 44-146 4.8 20
0.048 96.889.20.0440.050mg/Kg1,2,3-Trichloropropane 60-137 8.1 20
0.045 91.493.80.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.5 20
0.045 91.092.60.0460.050mg/KgVinyl Acetate 60-140 1.7 20
0.042 84.489.00.0440.050mg/KgVinyl Chloride 48-147 5.3 20
0.047 94.296.80.0480.050mg/Kgo-Xylene 74-126 2.7 20
0.094 94.899.00.0990.100mg/Kgm,p-Xylene 75-124 4.3 20
99.098.04-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)84-123
95.095.6Toluene-d8 (S)76-129
Page 12 of 35Date:05/17/2022 11:33 AM
Page 91 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18088 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/22 11:380.6600.116<0.116mg/KgAcenaphthene
04/29/22 11:380.6600.105<0.105mg/KgAcenaphthylene
04/29/22 11:380.6600.152<0.152mg/KgAniline
04/29/22 11:380.6600.143<0.143mg/KgAnthracene
04/29/22 11:380.6600.139<0.139mg/KgBenzo(a)anthracene
04/29/22 11:380.6600.147<0.147mg/KgBenzo(a)pyrene
04/29/22 11:380.6600.146<0.146mg/KgBenzo(b)fluoranthene
04/29/22 11:380.6600.136<0.136mg/KgBenzo(g,h,i)perylene
04/29/22 11:380.6600.137<0.137mg/KgBenzo(k)fluoranthene
04/29/22 11:382.000.580<0.580mg/KgBenzoic Acid
04/29/22 11:380.6600.105<0.105mg/KgBenzyl alcohol
04/29/22 11:380.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
04/29/22 11:380.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
04/29/22 11:380.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
04/29/22 11:380.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
04/29/22 11:380.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
04/29/22 11:380.3300.113<0.113mg/KgButyl benzyl phthalate
04/29/22 11:380.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
04/29/22 11:380.3300.112<0.112mg/Kg4-Chloroaniline
04/29/22 11:380.6600.116<0.116mg/Kg2-Chloronaphthalene
04/29/22 11:380.6600.098<0.098mg/Kg2-Chlorophenol
04/29/22 11:381.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
04/29/22 11:380.6600.142<0.142mg/KgChrysene
04/29/22 11:380.6600.230<0.230mg/KgDibenz(a,h)anthracene
04/29/22 11:380.6600.119<0.119mg/KgDibenzofuran
04/29/22 11:380.6600.094<0.094mg/Kg1,2-Dichlorobenzene
04/29/22 11:380.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 13 of 35Date:05/17/2022 11:33 AM
Page 92 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18088 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/22 11:380.3300.097<0.097mg/Kg1,4-Dichlorobenzene
04/29/22 11:380.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
04/29/22 11:380.6600.095<0.095mg/Kg2,4-Dichlorophenol
04/29/22 11:380.6600.180<0.180mg/KgDiethyl phthalate
04/29/22 11:380.6600.174<0.174mg/KgDimethyl phthalate
04/29/22 11:380.3300.108<0.108mg/Kg2,4-Dimethylphenol
04/29/22 11:380.6600.107<0.107mg/KgDi-n-butyl phthalate
04/29/22 11:381.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
04/29/22 11:381.500.520<0.520mg/Kg2,4-Dinitrophenol
04/29/22 11:380.6600.096<0.096mg/Kg2,4-Dinitrotoluene
04/29/22 11:380.6600.108<0.108mg/Kg2,6-Dinitrotoluene
04/29/22 11:380.3300.143<0.143mg/KgDi-n-Octyl Phthalate
04/29/22 11:380.6600.123<0.123mg/KgFluoranthene
04/29/22 11:380.6600.128<0.128mg/KgFluorene
04/29/22 11:380.6600.106<0.106mg/KgHexachlorobenzene
04/29/22 11:380.6600.097<0.097mg/KgHexachlorobutadiene
04/29/22 11:380.6600.157<0.157mg/KgHexachlorocyclopentadiene
04/29/22 11:380.6600.079<0.079mg/KgHexachloroethane
04/29/22 11:380.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
04/29/22 11:380.6600.191<0.191mg/KgIsophorone
04/29/22 11:380.6600.106<0.106mg/Kg1-Methylnaphthalene
04/29/22 11:380.6600.100<0.100mg/Kg2-Methylnaphthalene
04/29/22 11:380.6600.097<0.097mg/Kg2-Methylphenol
04/29/22 11:380.6600.084<0.084mg/Kg3&4 Methylphenol
04/29/22 11:380.6600.144<0.144mg/KgNaphthalene
04/29/22 11:380.6600.096<0.096mg/Kg2-Nitroaniline
04/29/22 11:380.6600.120<0.120mg/Kg3-Nitroaniline
Page 14 of 35Date:05/17/2022 11:33 AM
Page 93 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480
LRB-V18088 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/22 11:380.3300.093<0.093mg/Kg4-Nitroaniline
04/29/22 11:380.3300.116<0.116mg/KgNitrobenzene
04/29/22 11:380.6600.088<0.088mg/Kg2-Nitrophenol
04/29/22 11:380.6600.117<0.117mg/Kg4-Nitrophenol
04/29/22 11:380.6600.263<0.263mg/KgN-Nitrosodimethylamine
04/29/22 11:380.6600.181<0.181mg/KgN-Nitrosodiphenylamine
04/29/22 11:380.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
04/29/22 11:381.000.347<0.347mg/KgPentachlorophenol
04/29/22 11:380.6600.208<0.208mg/KgPhenanthrene
04/29/22 11:380.6600.112<0.112mg/KgPhenol
04/29/22 11:380.6600.134<0.134mg/KgPyrene
04/29/22 11:380.3300.079<0.079mg/KgPyridine
04/29/22 11:380.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
04/29/22 11:380.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
04/29/22 11:380.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
04/29/22 11:382-Fluorobiphenyl (S)92.8 44-115
04/29/22 11:382-Fluorophenol (S)96.6 35-115
04/29/22 11:38Nitrobenzene-d5 (S)82.0 37-122
04/29/22 11:384-Terphenyl-d14 (S)117 54-127
04/29/22 11:382,4,6-Tribromophenol (S)91.2 39-132
04/29/22 11:38Phenol-d5 (S)84.6 34-121
LCS-V18088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/KgAcenaphthene 40-123
92.81.551.67mg/KgAcenaphthylene 32-132
Page 15 of 35Date:05/17/2022 11:33 AM
Page 94 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
LCS-V18088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/KgAniline 12-197
91.01.521.67mg/KgAnthracene 47-123
88.61.481.67mg/KgBenzo(a)anthracene 49-126
1091.821.67mg/KgBenzo(a)pyrene 45-129
92.81.551.67mg/KgBenzo(b)fluoranthene 45-132
93.41.561.67mg/KgBenzo(g,h,i)perylene 43-134
1011.691.67mg/KgBenzo(k)fluoranthene 47-132
53.50.8941.67mg/KgBenzoic Acid 10-83
68.21.141.67mg/KgBenzyl alcohol 29-122
78.41.311.67mg/KgBis(2-Chloroethoxy)methane 36-121
76.01.271.67mg/KgBis(2-Chloroethyl)ether 31-120
79.01.321.67mg/KgBis(2-Chloroisopropyl)ether 33-131
95.81.601.67mg/KgBis(2-ethylhexyl)phthalate 51-133
83.81.401.67mg/Kg4-Bromophenyl phenyl ether 46-124
95.21.591.67mg/KgButyl benzyl phthalate 48-132
74.21.241.67mg/Kg4-Chloro-3-methylphenol 45-122
63.41.061.67mg/Kg4-Chloroaniline 17-106
84.41.411.67mg/Kg2-Chloronaphthalene 41-114
80.81.351.67mg/Kg2-Chlorophenol 34-121
85.61.431.67mg/Kg4-Chlorophenyl phenyl ether 45-121
92.81.551.67mg/KgChrysene 50-124
72.41.211.67mg/KgDibenz(a,h)anthracene 45-134
88.01.471.67mg/KgDibenzofuran 44-120
73.01.221.67mg/Kg1,2-Dichlorobenzene 33-117
70.61.181.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
55.30.9241.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 16 of 35Date:05/17/2022 11:33 AM
Page 95 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
LCS-V18088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
75.41.261.67mg/Kg2,4-Dichlorophenol 40-122
85.01.421.67mg/KgDiethyl phthalate 50-124
83.81.401.67mg/KgDimethyl phthalate 48-124
76.01.271.67mg/Kg2,4-Dimethylphenol 30-127
94.61.581.67mg/KgDi-n-butyl phthalate 51-128
60.41.011.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
45.20.7561.67mg/Kg2,4-Dinitrophenol 27-129
91.01.521.67mg/Kg2,4-Dinitrotoluene 48-126
91.01.521.67mg/Kg2,6-Dinitrotoluene 46-124
99.41.661.67mg/KgDi-n-Octyl Phthalate 45-140
87.41.461.67mg/KgFluoranthene 50-127
89.21.491.67mg/KgFluorene 43-125
87.41.461.67mg/KgHexachlorobenzene 45-122
69.41.161.67mg/KgHexachlorobutadiene 32-123
46.20.7731.67mg/KgHexachlorocyclopentadiene 32-117
70.01.171.67mg/KgHexachloroethane 28-117
1091.821.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
63.41.061.67mg/KgIsophorone 30-122
71.81.201.67mg/Kg1-Methylnaphthalene 40-119
69.41.161.67mg/Kg2-Methylnaphthalene 38-122
87.41.461.67mg/Kg2-Methylphenol 32-122
73.61.231.67mg/Kg3&4 Methylphenol 34-119
71.21.191.67mg/KgNaphthalene 35-123
82.01.371.67mg/Kg2-Nitroaniline 44-127
83.81.401.67mg/Kg3-Nitroaniline 33-119
82.01.371.67mg/Kg4-Nitroaniline 63-147
71.21.191.67mg/KgNitrobenzene 34-122
Page 17 of 35Date:05/17/2022 11:33 AM
Page 96 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
LCS-V18088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
73.61.231.67mg/Kg2-Nitrophenol 36-123
93.41.561.67mg/Kg4-Nitrophenol 30-132
65.81.101.67mg/KgN-Nitrosodimethylamine 10-146
1071.791.67mg/KgN-Nitrosodiphenylamine 38-127
76.61.281.67mg/KgN-Nitroso-di-n-propylamine 36-120
88.61.481.67mg/KgPentachlorophenol 25-133
88.61.481.67mg/KgPhenanthrene 50-121
88.01.471.67mg/KgPhenol 34-121
98.81.651.67mg/KgPyrene 47-127
50.50.8441.67mg/KgPyridine 10-80
67.61.131.67mg/Kg1,2,4-Trichlorobenzene 34-118
80.81.351.67mg/Kg2,4,5-Trichlorophenol 41-124
81.41.361.67mg/Kg2,4,6-Trichlorophenol 39-126
88.02-Fluorobiphenyl (S)44-115
92.72-Fluorophenol (S)35-115
70.0Nitrobenzene-d5 (S)37-122
98.84-Terphenyl-d14 (S)54-127
87.32,4,6-Tribromophenol (S)39-132
81.0Phenol-d5 (S)34-121
V 99590-MS-V18088 V 99590-MSD-V18088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.10 65.81.241.671.67<0.116mg/KgAcenaphthene 74.2 40-123 11.9 20
1.20 71.81.331.671.67<0.105mg/KgAcenaphthylene 79.6 32-132 10.2 20
0.527 31.50.5531.671.67<0.152mg/KgAniline 33.1 12-197 4.8 20
Page 18 of 35Date:05/17/2022 11:33 AM
Page 97 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
V 99590-MS-V18088 V 99590-MSD-V18088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.25 74.81.361.671.67<0.143mg/KgAnthracene 81.4 47-123 8.4 20
1.09 65.21.201.671.67<0.139mg/KgBenzo(a)anthracene 71.8 49-126 9.6 20
1.36 81.41.521.671.67<0.147mg/KgBenzo(a)pyrene 91.0 45-129 11.1 20
1.05 62.81.161.671.67<0.146mg/KgBenzo(b)fluoranthene 69.4 45-132 9.9 20
0.981 58.71.091.671.67<0.136mg/KgBenzo(g,h,i)perylene 65.2 43-134 10.5 20
0.977 58.51.081.671.67<0.137mg/KgBenzo(k)fluoranthene 64.6 47-132 10.0 20
1.07 64.01.251.671.67<0.580mg/KgBenzoic Acid 74.8 10-83 15.5 20
0.943 56.41.091.671.67<0.105mg/KgBenzyl alcohol 65.2 29-122 14.4 20
1.03 61.61.151.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 68.8 36-121 11.0 20
1.11 66.41.261.671.67<0.107mg/KgBis(2-Chloroethyl)ether 75.4 31-120 12.6 20
0.948 56.70.9951.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 59.5 33-131 4.8 20
3.47 208*3.431.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 205*51-133 1.1 20
1.13 67.61.461.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 87.4 46-124 25.4*20
1.15 68.81.201.671.67<0.113mg/KgButyl benzyl phthalate 71.8 48-132 4.2 20
0.987 59.11.111.671.67<0.092mg/Kg4-Chloro-3-methylphenol 66.4 45-122 11.7 20
0.704 42.10.6491.671.67<0.112mg/Kg4-Chloroaniline 38.8 17-106 8.1 20
1.07 64.01.251.671.67<0.116mg/Kg2-Chloronaphthalene 74.8 41-114 15.5 20
0.980 58.61.131.671.67<0.098mg/Kg2-Chlorophenol 67.6 34-121 14.2 20
1.14 68.21.261.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 75.4 45-121 10.0 20
1.31 78.41.411.671.67<0.142mg/KgChrysene 84.4 50-124 7.3 20
0.893 53.40.9701.671.67<0.230mg/KgDibenz(a,h)anthracene 58.0 45-134 8.2 20
1.16 69.41.281.671.67<0.119mg/KgDibenzofuran 76.6 44-120 9.8 20
0.863 51.61.021.671.67<0.094mg/Kg1,2-Dichlorobenzene 61.0 33-117 16.6 20
0.814 48.70.9751.671.67<0.097mg/Kg1,3-Dichlorobenzene 58.3 30-115 17.9 20
0.818 48.90.9751.671.67<0.097mg/Kg1,4-Dichlorobenzene 58.3 31-115 17.5 20
<0.147 0.0*<0.1471.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 0.0*22-121 0.0 20
Page 19 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 98 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
V 99590-MS-V18088 V 99590-MSD-V18088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.996 59.61.171.671.67<0.095mg/Kg2,4-Dichlorophenol 70.0 40-122 16.0 20
1.18 70.61.321.671.67<0.180mg/KgDiethyl phthalate 79.0 50-124 11.2 20
1.12 67.01.291.671.67<0.174mg/KgDimethyl phthalate 77.2 48-124 14.1 30
1.05 62.81.181.671.67<0.108mg/Kg2,4-Dimethylphenol 70.6 30-127 11.6 20
1.26 75.41.351.671.67<0.107mg/KgDi-n-butyl phthalate 80.8 51-128 6.8 20
1.14 68.21.541.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 92.2 29-132 29.8*20
1.01 60.41.441.671.67<0.520mg/Kg2,4-Dinitrophenol 86.2 27-129 35.1*20
1.32 79.01.461.671.67<0.096mg/Kg2,4-Dinitrotoluene 87.4 48-126 10.0 20
1.34 80.21.481.671.67<0.108mg/Kg2,6-Dinitrotoluene 88.6 46-124 9.9 20
0.595 35.6*0.7551.671.67<0.143mg/KgDi-n-Octyl Phthalate 45.2 45-140 23.7*20
1.44 86.21.451.671.67<0.123mg/KgFluoranthene 86.8 50-127 0.6 20
1.19 71.21.281.671.67<0.128mg/KgFluorene 76.6 43-125 7.2 20
1.08 64.61.231.671.67<0.106mg/KgHexachlorobenzene 73.6 45-122 12.9 20
0.883 52.81.071.671.67<0.097mg/KgHexachlorobutadiene 64.0 32-123 19.1 20
0.251 15.0*0.2551.671.67<0.157mg/KgHexachlorocyclopentadiene 15.2*32-117 1.5 20
0.828 49.50.9381.671.67<0.079mg/KgHexachloroethane 56.1 28-117 12.4 20
1.17 70.01.331.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 79.6 45-133 12.8 20
0.815 48.80.9161.671.67<0.191mg/KgIsophorone 54.8 30-122 11.6 20
0.932 55.81.041.671.67<0.106mg/Kg1-Methylnaphthalene 62.2 40-119 10.9 20
0.902 54.01.011.671.67<0.100mg/Kg2-Methylnaphthalene 60.4 38-122 11.2 20
1.02 61.01.101.671.67<0.097mg/Kg2-Methylphenol 65.8 32-122 7.5 20
0.887 53.10.9701.671.67<0.085mg/Kg3&4 Methylphenol 58.0 34-119 8.9 20
0.907 54.31.031.671.67<0.144mg/KgNaphthalene 61.6 35-123 12.7 20
1.06 63.41.181.671.67<0.096mg/Kg2-Nitroaniline 70.6 44-127 10.7 20
0.735 44.00.5701.671.67<0.120mg/Kg3-Nitroaniline 34.1 33-119 25.2*20
<0.093 0.0*0.5181.671.67<0.093mg/Kg4-Nitroaniline 31.0*63-147 139*20
Page 20 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 99 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18088
V 99590-MS-V18088 V 99590-MSD-V18088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.907 54.31.021.671.67<0.116mg/KgNitrobenzene 61.0 34-122 11.7 20
0.956 57.21.141.671.67<0.088mg/Kg2-Nitrophenol 68.2 32-123 17.5 20
1.29 77.21.401.671.67<0.117mg/Kg4-Nitrophenol 83.8 30-132 8.1 20
0.808 48.30.9321.671.67<0.263mg/KgN-Nitrosodimethylamine 55.8 10-146 14.2 30
1.57 94.01.801.671.67<0.181mg/KgN-Nitrosodiphenylamine 108 38-127 13.6 20
1.14 68.21.191.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 71.2 36-120 4.2 20
1.60 95.81.841.671.67<0.347mg/KgPentachlorophenol 110 25-133 13.9 20
1.20 71.81.311.671.67<0.208mg/KgPhenanthrene 78.4 50-121 8.7 20
1.05 62.81.141.671.67<0.112mg/KgPhenol 68.2 34-121 8.2 20
2.38 143*2.431.671.67<0.134mg/KgPyrene 146*47-127 2.0 20
0.573 34.30.6941.671.67<0.079mg/KgPyridine 41.5 10-80 19.1 20
0.879 52.61.041.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 62.2 34-118 16.7 20
1.11 66.41.351.671.67<0.096mg/Kg2,4,5-Trichlorophenol 80.8 41-124 19.5 20
1.04 62.21.221.671.67<0.096mg/Kg2,4,6-Trichlorophenol 73.0 39-126 15.9 20
64.02-Fluorobiphenyl (S)75.4 44-115
64.92-Fluorophenol (S)76.5 35-115
51.6Nitrobenzene-d5 (S)57.1 37-122
1254-Terphenyl-d14 (S)132*54-127
70.32,4,6-Tribromophenol (S)76.8 39-132
55.9Phenol-d5 (S)63.3 34-121
Page 21 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 100 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
Associated Lab Samples: 99481, 99482
LRB-V18145 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/13/22 19:340.6600.116<0.116mg/KgAcenaphthene
05/13/22 19:340.6600.105<0.105mg/KgAcenaphthylene
05/13/22 19:340.6600.152<0.152mg/KgAniline
05/13/22 19:340.6600.143<0.143mg/KgAnthracene
05/13/22 19:340.6600.139<0.139mg/KgBenzo(a)anthracene
05/13/22 19:340.6600.147<0.147mg/KgBenzo(a)pyrene
05/13/22 19:340.6600.146<0.146mg/KgBenzo(b)fluoranthene
05/13/22 19:340.6600.136<0.136mg/KgBenzo(g,h,i)perylene
05/13/22 19:340.6600.137<0.137mg/KgBenzo(k)fluoranthene
05/13/22 19:342.000.580<0.580mg/KgBenzoic Acid
05/13/22 19:340.6600.105<0.105mg/KgBenzyl alcohol
05/13/22 19:340.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
05/13/22 19:340.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
05/13/22 19:340.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
05/13/22 19:340.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
05/13/22 19:340.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
05/13/22 19:340.3300.113<0.113mg/KgButyl benzyl phthalate
05/13/22 19:340.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
05/13/22 19:340.3300.112<0.112mg/Kg4-Chloroaniline
05/13/22 19:340.6600.116<0.116mg/Kg2-Chloronaphthalene
05/13/22 19:340.6600.098<0.098mg/Kg2-Chlorophenol
05/13/22 19:341.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
05/13/22 19:340.6600.142<0.142mg/KgChrysene
05/13/22 19:340.6600.230<0.230mg/KgDibenz(a,h)anthracene
05/13/22 19:340.6600.119<0.119mg/KgDibenzofuran
05/13/22 19:340.6600.094<0.094mg/Kg1,2-Dichlorobenzene
05/13/22 19:340.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 22 of 35Date:05/17/2022 11:33 AM
Page 101 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
Associated Lab Samples: 99481, 99482
LRB-V18145 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/13/22 19:340.3300.097<0.097mg/Kg1,4-Dichlorobenzene
05/13/22 19:340.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
05/13/22 19:340.6600.095<0.095mg/Kg2,4-Dichlorophenol
05/13/22 19:340.6600.180<0.180mg/KgDiethyl phthalate
05/13/22 19:340.6600.174<0.174mg/KgDimethyl phthalate
05/13/22 19:340.3300.108<0.108mg/Kg2,4-Dimethylphenol
05/13/22 19:340.6600.107<0.107mg/KgDi-n-butyl phthalate
05/13/22 19:341.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
05/13/22 19:341.500.520<0.520mg/Kg2,4-Dinitrophenol
05/13/22 19:340.6600.096<0.096mg/Kg2,4-Dinitrotoluene
05/13/22 19:340.6600.108<0.108mg/Kg2,6-Dinitrotoluene
05/13/22 19:340.3300.143<0.143mg/KgDi-n-Octyl Phthalate
05/13/22 19:340.6600.123<0.123mg/KgFluoranthene
05/13/22 19:340.6600.128<0.128mg/KgFluorene
05/13/22 19:340.6600.106<0.106mg/KgHexachlorobenzene
05/13/22 19:340.6600.097<0.097mg/KgHexachlorobutadiene
05/13/22 19:340.6600.157<0.157mg/KgHexachlorocyclopentadiene
05/13/22 19:340.6600.079<0.079mg/KgHexachloroethane
05/13/22 19:340.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
05/13/22 19:340.6600.191<0.191mg/KgIsophorone
05/13/22 19:340.6600.106<0.106mg/Kg1-Methylnaphthalene
05/13/22 19:340.6600.100<0.100mg/Kg2-Methylnaphthalene
05/13/22 19:340.6600.097<0.097mg/Kg2-Methylphenol
05/13/22 19:340.6600.084<0.084mg/Kg3&4 Methylphenol
05/13/22 19:340.6600.144<0.144mg/KgNaphthalene
05/13/22 19:340.6600.096<0.096mg/Kg2-Nitroaniline
05/13/22 19:340.6600.120<0.120mg/Kg3-Nitroaniline
Page 23 of 35Date:05/17/2022 11:33 AM
Page 102 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
Associated Lab Samples: 99481, 99482
LRB-V18145 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/13/22 19:340.3300.093<0.093mg/Kg4-Nitroaniline
05/13/22 19:340.3300.116<0.116mg/KgNitrobenzene
05/13/22 19:340.6600.088<0.088mg/Kg2-Nitrophenol
05/13/22 19:340.6600.117<0.117mg/Kg4-Nitrophenol
05/13/22 19:340.6600.263<0.263mg/KgN-Nitrosodimethylamine
05/13/22 19:340.6600.181<0.181mg/KgN-Nitrosodiphenylamine
05/13/22 19:340.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
05/13/22 19:341.000.347<0.347mg/KgPentachlorophenol
05/13/22 19:340.6600.208<0.208mg/KgPhenanthrene
05/13/22 19:340.6600.112<0.112mg/KgPhenol
05/13/22 19:340.6600.134<0.134mg/KgPyrene
05/13/22 19:340.3300.079<0.079mg/KgPyridine
05/13/22 19:340.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
05/13/22 19:340.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
05/13/22 19:340.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
05/13/22 19:342-Fluorobiphenyl (S)95.2 44-115
05/13/22 19:342-Fluorophenol (S)102 35-115
05/13/22 19:34Nitrobenzene-d5 (S)96.4 37-122
05/13/22 19:344-Terphenyl-d14 (S)106 54-127
05/13/22 19:342,4,6-Tribromophenol (S)96.3 39-132
05/13/22 19:34Phenol-d5 (S)95.4 34-121
LCS-V18145Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
73.01.221.67mg/KgAcenaphthene 40-123
76.01.271.67mg/KgAcenaphthylene 32-132
Page 24 of 35Date:05/17/2022 11:33 AM
Page 103 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
LCS-V18145Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/KgAniline 12-197
76.61.281.67mg/KgAnthracene 47-123
73.61.231.67mg/KgBenzo(a)anthracene 49-126
88.01.471.67mg/KgBenzo(a)pyrene 45-129
79.01.321.67mg/KgBenzo(b)fluoranthene 45-132
75.41.261.67mg/KgBenzo(g,h,i)perylene 43-134
78.41.311.67mg/KgBenzo(k)fluoranthene 47-132
58.60.9801.67mg/KgBenzoic Acid 10-83
76.61.281.67mg/KgBenzyl alcohol 29-122
64.61.081.67mg/KgBis(2-Chloroethoxy)methane 36-121
71.21.191.67mg/KgBis(2-Chloroethyl)ether 31-120
79.61.331.67mg/KgBis(2-Chloroisopropyl)ether 33-131
83.81.401.67mg/KgBis(2-ethylhexyl)phthalate 51-133
73.61.231.67mg/Kg4-Bromophenyl phenyl ether 46-124
80.81.351.67mg/KgButyl benzyl phthalate 48-132
69.41.161.67mg/Kg4-Chloro-3-methylphenol 45-122
57.40.9591.67mg/Kg4-Chloroaniline 17-106
72.41.211.67mg/Kg2-Chloronaphthalene 41-114
71.21.191.67mg/Kg2-Chlorophenol 34-121
73.01.221.67mg/Kg4-Chlorophenyl phenyl ether 45-121
77.81.301.67mg/KgChrysene 50-124
55.80.9321.67mg/KgDibenz(a,h)anthracene 45-134
72.41.211.67mg/KgDibenzofuran 44-120
65.21.091.67mg/Kg1,2-Dichlorobenzene 33-117
62.81.051.67mg/Kg1,3-Dichlorobenzene 30-115
60.41.011.67mg/Kg1,4-Dichlorobenzene 31-115
54.10.9041.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 25 of 35Date:05/17/2022 11:33 AM
Page 104 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
LCS-V18145Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
65.21.091.67mg/Kg2,4-Dichlorophenol 40-122
77.81.301.67mg/KgDiethyl phthalate 50-124
74.81.251.67mg/KgDimethyl phthalate 48-124
67.61.131.67mg/Kg2,4-Dimethylphenol 30-127
91.01.521.67mg/KgDi-n-butyl phthalate 51-128
73.01.221.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
82.01.371.67mg/Kg2,4-Dinitrophenol 27-129
89.81.501.67mg/Kg2,4-Dinitrotoluene 48-126
88.01.471.67mg/Kg2,6-Dinitrotoluene 46-124
80.81.351.67mg/KgDi-n-Octyl Phthalate 45-140
75.41.261.67mg/KgFluoranthene 50-127
73.01.221.67mg/KgFluorene 43-125
74.21.241.67mg/KgHexachlorobenzene 45-122
62.81.051.67mg/KgHexachlorobutadiene 32-123
51.90.8681.67mg/KgHexachlorocyclopentadiene 32-117
61.01.021.67mg/KgHexachloroethane 28-117
71.81.201.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
57.40.9601.67mg/KgIsophorone 30-122
63.41.061.67mg/Kg1-Methylnaphthalene 40-119
61.61.031.67mg/Kg2-Methylnaphthalene 38-122
73.01.221.67mg/Kg2-Methylphenol 32-122
67.01.121.67mg/Kg3&4 Methylphenol 34-119
62.21.041.67mg/KgNaphthalene 35-123
69.41.161.67mg/Kg2-Nitroaniline 44-127
73.01.221.67mg/Kg3-Nitroaniline 33-119
74.21.241.67mg/Kg4-Nitroaniline 63-147
64.61.081.67mg/KgNitrobenzene 34-122
Page 26 of 35Date:05/17/2022 11:33 AM
Page 105 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
LCS-V18145Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
64.61.081.67mg/Kg2-Nitrophenol 36-123
74.21.241.67mg/Kg4-Nitrophenol 30-132
55.10.9211.67mg/KgN-Nitrosodimethylamine 10-146
92.81.551.67mg/KgN-Nitrosodiphenylamine 38-127
70.61.181.67mg/KgN-Nitroso-di-n-propylamine 36-120
79.01.321.67mg/KgPentachlorophenol 25-133
76.61.281.67mg/KgPhenanthrene 50-121
74.21.241.67mg/KgPhenol 34-121
77.21.291.67mg/KgPyrene 47-127
40.80.6831.67mg/KgPyridine 10-80
59.81.001.67mg/Kg1,2,4-Trichlorobenzene 34-118
71.81.201.67mg/Kg2,4,5-Trichlorophenol 41-124
70.01.171.67mg/Kg2,4,6-Trichlorophenol 39-126
72.42-Fluorobiphenyl (S)44-115
78.62-Fluorophenol (S)35-115
62.8Nitrobenzene-d5 (S)37-122
77.84-Terphenyl-d14 (S)54-127
78.92,4,6-Tribromophenol (S)39-132
71.7Phenol-d5 (S)34-121
V 99481-MS-V18145 V 99481-MSD-V18145Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.46 87.41.521.671.67<0.116mg/KgAcenaphthene 91.0 40-123 4.0 20
1.52 91.01.561.671.67<0.105mg/KgAcenaphthylene 93.4 32-132 2.5 20
0.891 53.31.001.671.67<0.152mg/KgAniline 59.8 12-197 11.5 20
Page 27 of 35Date:05/17/2022 11:33 AM
Page 106 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
V 99481-MS-V18145 V 99481-MSD-V18145Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.51 90.41.491.671.67<0.143mg/KgAnthracene 89.2 47-123 1.3 20
1.48 88.61.451.671.67<0.139mg/KgBenzo(a)anthracene 86.8 49-126 2.0 20
1.63 97.61.621.671.67<0.147mg/KgBenzo(a)pyrene 97.0 45-129 0.6 20
1.51 90.41.451.671.67<0.146mg/KgBenzo(b)fluoranthene 86.8 45-132 4.0 20
1.46 87.41.431.671.67<0.136mg/KgBenzo(g,h,i)perylene 85.6 43-134 2.0 20
1.46 87.41.421.671.67<0.137mg/KgBenzo(k)fluoranthene 85.0 47-132 2.7 20
1.59 95.2*1.581.671.67<0.580mg/KgBenzoic Acid 94.6*10-83 0.6 20
1.46 87.41.491.671.67<0.105mg/KgBenzyl alcohol 89.2 29-122 2.0 20
1.28 76.61.301.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 77.8 36-121 1.5 20
1.39 83.21.341.671.67<0.107mg/KgBis(2-Chloroethyl)ether 80.2 31-120 3.6 20
1.32 79.01.341.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 80.2 33-131 1.5 20
1.81 1081.781.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 107 51-133 1.6 20
1.55 92.81.541.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 92.2 46-124 0.6 20
1.78 1071.721.671.67<0.113mg/KgButyl benzyl phthalate 103 48-132 3.4 20
1.37 82.01.381.671.67<0.092mg/Kg4-Chloro-3-methylphenol 82.6 45-122 0.7 20
0.995 59.51.021.671.67<0.112mg/Kg4-Chloroaniline 61.0 17-106 2.4 20
1.44 86.21.501.671.67<0.116mg/Kg2-Chloronaphthalene 89.8 41-114 4.0 20
1.36 81.41.401.671.67<0.098mg/Kg2-Chlorophenol 83.8 34-121 2.8 20
1.50 89.81.521.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 91.0 45-121 1.3 20
1.47 88.01.481.671.67<0.142mg/KgChrysene 88.6 50-124 0.6 20
1.18 70.61.121.671.67<0.230mg/KgDibenz(a,h)anthracene 67.0 45-134 5.2 20
1.46 87.41.491.671.67<0.119mg/KgDibenzofuran 89.2 44-120 2.0 20
1.31 78.41.281.671.67<0.094mg/Kg1,2-Dichlorobenzene 76.6 33-117 2.3 20
1.29 77.21.261.671.67<0.097mg/Kg1,3-Dichlorobenzene 75.4 30-115 2.3 20
1.27 76.01.241.671.67<0.097mg/Kg1,4-Dichlorobenzene 74.2 31-115 2.3 20
0.757 45.30.8681.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 51.9 22-121 13.6 20
Page 28 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 107 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
V 99481-MS-V18145 V 99481-MSD-V18145Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.36 81.41.401.671.67<0.095mg/Kg2,4-Dichlorophenol 83.8 40-122 2.8 20
1.52 91.01.521.671.67<0.180mg/KgDiethyl phthalate 91.0 50-124 0.0 20
1.50 89.81.521.671.67<0.174mg/KgDimethyl phthalate 91.0 48-124 1.3 30
1.38 82.61.431.671.67<0.108mg/Kg2,4-Dimethylphenol 85.6 30-127 3.5 20
1.76 1051.721.671.67<0.107mg/KgDi-n-butyl phthalate 103 51-128 2.2 20
1.45 86.81.491.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 89.2 29-132 2.7 20
1.51 90.41.591.671.67<0.520mg/Kg2,4-Dinitrophenol 95.2 27-129 5.1 20
2.01 1202.201.671.67<0.096mg/Kg2,4-Dinitrotoluene 132*48-126 9.0 20
1.86 1112.051.671.67<0.108mg/Kg2,6-Dinitrotoluene 123 46-124 9.7 20
1.76 1051.741.671.67<0.143mg/KgDi-n-Octyl Phthalate 104 45-140 1.1 20
1.53 91.61.511.671.67<0.123mg/KgFluoranthene 90.4 50-127 1.3 20
1.49 89.21.511.671.67<0.128mg/KgFluorene 90.4 43-125 1.3 20
1.57 94.01.551.671.67<0.106mg/KgHexachlorobenzene 92.8 45-122 1.2 20
1.31 78.41.311.671.67<0.097mg/KgHexachlorobutadiene 78.4 32-123 0.0 20
1.16 69.41.231.671.67<0.157mg/KgHexachlorocyclopentadiene 73.6 32-117 5.8 20
1.23 73.61.201.671.67<0.079mg/KgHexachloroethane 71.8 28-117 2.4 20
1.45 86.81.381.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 82.6 45-133 4.9 20
1.13 67.61.131.671.67<0.191mg/KgIsophorone 67.6 30-122 0.0 20
1.26 75.41.291.671.67<0.106mg/Kg1-Methylnaphthalene 77.2 40-119 2.3 20
1.23 73.61.241.671.67<0.100mg/Kg2-Methylnaphthalene 74.2 38-122 0.8 20
1.40 83.81.401.671.67<0.097mg/Kg2-Methylphenol 83.8 32-122 0.0 20
1.27 76.01.271.671.67<0.085mg/Kg3&4 Methylphenol 76.0 34-119 0.0 20
1.23 73.61.251.671.67<0.144mg/KgNaphthalene 74.8 35-123 1.6 20
1.45 86.81.561.671.67<0.096mg/Kg2-Nitroaniline 93.4 44-127 7.3 20
1.39 83.21.481.671.67<0.120mg/Kg3-Nitroaniline 88.6 33-119 6.2 20
1.53 91.61.611.671.67<0.093mg/Kg4-Nitroaniline 96.4 63-147 5.0 20
Page 29 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 108 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V18743QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18145
V 99481-MS-V18145 V 99481-MSD-V18145Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.36 81.41.461.671.67<0.116mg/KgNitrobenzene 87.4 34-122 7.0 20
1.44 86.21.541.671.67<0.088mg/Kg2-Nitrophenol 92.2 32-123 6.7 20
1.59 95.21.641.671.67<0.117mg/Kg4-Nitrophenol 98.2 30-132 3.0 20
1.07 64.00.9971.671.67<0.263mg/KgN-Nitrosodimethylamine 59.7 10-146 7.0 30
1.78 1071.791.671.67<0.181mg/KgN-Nitrosodiphenylamine 107 38-127 0.5 20
1.34 80.21.401.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 83.8 36-120 4.3 20
1.78 1071.841.671.67<0.347mg/KgPentachlorophenol 110 25-133 3.3 20
1.51 90.41.491.671.67<0.208mg/KgPhenanthrene 89.2 50-121 1.3 20
1.39 83.21.431.671.67<0.112mg/KgPhenol 85.6 34-121 2.8 20
1.50 89.81.471.671.67<0.134mg/KgPyrene 88.0 47-127 2.0 20
0.397 23.7<0.0791.671.67<0.079mg/KgPyridine 0.0*10-80 133*20
1.20 71.81.251.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 74.8 34-118 4.0 20
1.54 92.21.591.671.67<0.096mg/Kg2,4,5-Trichlorophenol 95.2 41-124 3.1 20
1.55 92.81.631.671.67<0.096mg/Kg2,4,6-Trichlorophenol 97.6 39-126 5.0 20
86.82-Fluorobiphenyl (S)92.2 44-115
87.12-Fluorophenol (S)88.9 35-115
83.2Nitrobenzene-d5 (S)85.6 37-122
93.44-Terphenyl-d14 (S)94.0 54-127
1072,4,6-Tribromophenol (S)112 39-132
83.2Phenol-d5 (S)85.0 34-121
Page 30 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 109 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V18269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V18051
Associated Lab Samples: 99476, 99477, 99478, 99479, 99480
LRB-V18051 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/22 14:5050.09.20<9.20mg/KgAliphatic C9-C18
04/30/22 14:5050.012.2<12.2mg/KgAliphatic C19-C36
04/30/22 14:5050.014.2<14.2mg/KgAromatic C11-C22
04/30/22 14:502-Fluorobiphenyl (S)73.2 40-140
04/30/22 14:502-Bromonaphthalene (S)101 40-140
04/30/22 14:50Chlorooctadecane (S)83.0 40-140
04/30/22 14:50OTP Surrogate (S)65.0 40-140
LCS-V18051 LCSD-V18051Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.3 0.0*0.0*37.660.0mg/KgAliphatic C9-C18 40-140 0.0 50
73.6 92.087.570.080.0mg/KgAliphatic C19-C36 40-140 5.0 50
178 10588.2150170mg/KgAromatic C11-C22 40-140 17.0 50
99.098.52-Fluorobiphenyl (S)40-140
1191092-Bromonaphthalene (S)40-140
76.576.5Chlorooctadecane (S)40-140
82.074.5OTP Surrogate (S)40-140
Page 31 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 110 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V18371QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V18067
Associated Lab Samples: 99481, 99482
LRB-V18067 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/22 17:5850.09.20<9.20mg/KgAliphatic C9-C18
05/03/22 17:5850.012.2<12.2mg/KgAliphatic C19-C36
05/03/22 17:5850.014.2<14.2mg/KgAromatic C11-C22
05/03/22 17:582-Fluorobiphenyl (S)67.0 40-140
05/03/22 17:582-Bromonaphthalene (S)72.2 40-140
05/03/22 17:58Chlorooctadecane (S)64.5 40-140
05/03/22 17:58OTP Surrogate (S)58.0 40-140
LCS-V18067 LCSD-V18067Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.6 0.0*0.0*41.560.0mg/KgAliphatic C9-C18 40-140 0.0 50
66.4 83.085.168.180.0mg/KgAliphatic C19-C36 40-140 2.5 50
138 81.182.3140170mg/KgAromatic C11-C22 40-140 1.4 50
90.790.72-Fluorobiphenyl (S)40-140
96.094.22-Bromonaphthalene (S)40-140
86.092.0Chlorooctadecane (S)40-140
87.088.5OTP Surrogate (S)40-140
Page 32 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 111 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V18459QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V18369
Associated Lab Samples: 99475
LRB-V18369 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/06/22 16:0650.09.20<9.20mg/KgAliphatic C9-C18
05/06/22 16:0650.012.2<12.2mg/KgAliphatic C19-C36
05/06/22 16:0650.014.2<14.2mg/KgAromatic C11-C22
05/06/22 16:062-Fluorobiphenyl (S)68.5 40-140
05/06/22 16:062-Bromonaphthalene (S)66.2 40-140
05/06/22 16:06Chlorooctadecane (S)52.5 40-140
05/06/22 16:06OTP Surrogate (S)55.0 40-140
LCS-V18369 LCSD-V18369Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.3 0.0*0.0*35.860.0mg/KgAliphatic C9-C18 40-140 0.0 50
70.8 88.577.261.880.0mg/KgAliphatic C19-C36 40-140 13.5 50
132 77.665.8112170mg/KgAromatic C11-C22 40-140 16.3 50
89.273.52-Fluorobiphenyl (S)40-140
94.076.02-Bromonaphthalene (S)40-140
67.061.0Chlorooctadecane (S)40-140
68.556.0OTP Surrogate (S)40-140
Page 33 of 35* QC Fail Date:05/17/2022 11:33 AM
Page 112 of 116
Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V18008QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V18007
Associated Lab Samples: 99475, 99476, 99477, 99478, 99479, 99480, 99481, 99482
LRB-V18007 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/22 16:578.001.22<1.22mg/KgAliphatic C5-C8
04/26/22 16:578.004.56<4.56mg/KgAliphatic C9-C12
04/26/22 16:578.000.624<0.624mg/KgAromatic C9-C10
04/26/22 16:572,5-Dibromotoluene (FID) (S)81.2 70-130
04/26/22 16:572,5-Dibromotoluene (PID) (S)91.5 70-130
LCS-V18007 LCSD-V18007Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.0 96.893.730.032.0mg/KgAliphatic C5-C8 70-130 3.2 50
35.4 11110633.932.0mg/KgAliphatic C9-C12 70-130 4.3 50
11.6 10810711.410.7mg/KgAromatic C9-C10 70-130 1.7 50
76.676.62,5-Dibromotoluene (FID) (S)70-130
87.988.72,5-Dibromotoluene (PID) (S)70-130
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Quality Control Data
22-115-0003Report No:
Project Description:
Client ID:Spangler Environmental
Edge of Auburn
Dry Weight Determination
SW-DRYWT
V18159QC Analytical Batch:
Analysis Method:
Analysis Description:
V 99454-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/29/22 11:320.86.846.90%Moisture
V 99456-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/29/22 11:323.710.910.5%Moisture
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Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-115-0003
Spangler Environmental
01191
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Zoe S. Vigilant Date & Time:04/25/2022 10:19:05
Special precautions or instructions included?
Comments:
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