RA-27837_47145_CA_RPTS_20200625_PH2ESA

DUNCKLEE
& DUNHAM

MAILING ADDRESS – POST OFFICE BOX 639 – CARY, NORTH CAROLINA 27512
NORTH CAROLINA BOARD OF EXAMINERS FOR ENGINEERS AND SURVEYORS LICENSE C-3559
NORTH CAROLINA BOARD FOR LICENSING OF GEOLOGISTS LICENSE C-261
NC DEQ REGISTERED ENVIRONMENTAL CONSULTANT NUMBER 00061
DD ENVIRONMENTAL GEOLOGISTS & ENGINEERS
511 KEISLER DRIVE – SUITE 102
CARY, NORTH CAROLINA 27518
OFFICE: (919) 858–9898
WWW.DUNCKLEEDUNHAM.COM

June 25, 2020

Mr. Mark Powers
Division of Waste Management, UST Section
North Carolina Department of Environmental Quality
Raleigh Regional Office
3800 Barrett Drive
Raleigh, North Carolina 27609

Subject: Transmittal Letter
Letter Report of Environmental Services
Davis-McCoy Parcel
Wilson, Wilson County, North Carolina

Dear Mr. Powers:

Attached please find the Letter Report of Environmental Services for the referenced site. We conducted our
assessment for the City of Wilson, which subsequently acquired the parcel for future redevelopment.

Please call me if you have any questions. Thank you for your attention.

Sincerely,

Duncklee & Dunham, P.C.

Richard A. Kolb, L.G.
Senior Geologist

Attachment: Letter Report of Environmental Services

eC: Michelle Brown, City of Wilson (transmittal letter only)

P:\Wilson, City of\Davis-McCoy Parcel-2018280\Report\Transmittal letter -20458.doc

MAILING ADDRESS – POST OFFICE BOX 639 – CARY, NORTH CAROLINA 27512
NORTH CAROLINA BOARD OF EXAMINERS FOR ENGINEERS AND SURVEYORS LICENSE C-3559
NORTH CAROLINA BOARD FOR LICENSING OF GEOLOGISTS LICENSE C-261
NC DEQ REGISTERED ENVIRONMENTAL CONSULTANT NUMBER 00061
ENVIRONMENTAL GEOLOGISTS & ENGINEERS
511 KEISLER DRIVE – SUITE 102
CARY, NORTH CAROLINA 27518
OFFICE: (919) 858–9898
WWW.DUNCKLEEDUNHAM.COM
VIA EMAIL TO: [e-mail]
April 25, 2019 Ms. Michelle Brown, Planner Planning & Development Services
City of Wilson Post Office Box 10 Wilson, North Carolina 27894-0010 Reference: Letter Report of Environmental Services Davis-McCoy Parcel Wilson, North Carolina Dear Ms. Brown:
As authorized by your acceptance of our proposal dated February 22, 2019, Duncklee & Dunham, P.C. (Duncklee & Dunham) is pleased to submit this Letter Report of Environmental Services for the above-referenced site. The objective of our services was to test for the presence of compounds of concern in soil and groundwater.
Background Information The Davis-McCoy parcel is at 526 Stemmery Street South in Wilson, North Carolina (Figure 1). The subject site comprises 5.85 acres and is mostly grass-covered land developed with four vacant buildings and the slab for a razed building. The City of Wilson may acquire the site. Duncklee & Dunham conducted a Phase I Environmental Site Assessment of the site on behalf of the City of Wilson and prepared a report dated December 11, 2018. We cited the following recognized environmental conditions in our report:
• the historical mixing and storage of fertilizer at the subject site,
• an underground storage tank (UST) that had been used to store gasoline from 1983 to 1987,
• the historical storage and use of coal as an energy source for the facilities on the subject site, and
• the groundwater contamination from historical mixing and storage of fertilizers at the adjoining Former Kaiser Agricultural Chemicals site. Duncklee & Dunham could not determine the location of the gasoline UST. The owner of the site when the UST was in place is deceased.
Letter Report of Environmental Services Davis-McCoy Parcel Wilson, North Carolina April 25, 2019 Page 2 of 4
DUNCKLEE & DUNHAM, P.C.
Field Activities Duncklee & Dunham notified North Carolina One Call to locate utilities on the site. We contracted with
Troxler Geologic Services, Inc. (Troxler) to locate underground utilities and construct temporary monitoring wells on the subject site.
Duncklee & Dunham and Troxler mobilized to the site on March 14, 2019. Troxler used a Geoprobe® to advance a soil boring using direct-push technology along the northwestern side of the small building near the center of the site to a depth of 16 feet bls (below land surface) (Figure 2). Duncklee & Dunham collected a representative sample of native material at selected intervals in the soil boring and stored the samples in duplicate Ziploc® bags. After allowing the bags to sit untouched for approximately 15 minutes, we used a photoionization detector (PID) to screen the headspace in one of the duplicate bags from each interval for volatile organic compounds (VOCs). The PID readings ranged from 0.5 to 1.1 parts per million. Because the soil samples did not evoke an anomalous response on the PID, we did not collect a sample from the soil boring. We observed clayey silt and clayey, sandy silt from 0.5 to 2 feet bls; silty clay and sandy, silty clay from 2 to 14 feet bls; and clayey sand from 14 to 16 feet bls. Duncklee & Dunham measured the water table at a depth of 6.81 feet bls in the soil boring. Troxler constructed
TMW-1 in the soil boring using a Geoprobe® with groundwater sampling rods. Troxler constructed TMW-2 through -5 using groundwater sampling rods. We did not observe evidence
of contamination in the soil from the borings for these wells and did not screen the samples with the PID. Troxler constructed TMW-2, -3, and -5 each to a depth of 16 feet bls in the locations shown in Figure 2. Troxler constructed TMW-2 in the former location of aboveground storage tanks (ASTs) shown on
Sanborn maps. These tanks had been used to store “chemicals” near the center of the site. Troxler constructed TMW-3 near the former location of a building that Sanborn maps show was used to store and mix fertilizers on the southern portion of the site, and TMW-5 in the western corner of the site near the location of a building that Sanborn maps show was formerly used to store bulk acid and mix fertilizers. Troxler attempted to construct TMW-4 in the proposed location adjoining another Former Kaiser
Agricultural Chemicals site across Stemmery Street South. However, this boring did not encounter the water table at a depth of approximately 32 feet bls, so Troxler constructed TMW-4 in the northern corner of the site to a depth of 28 feet bls. Temporary monitoring wells TMW-1, -2, -3, and -5 were screened from 12 to 16 feet bls and TMW-4
was screened from 24 to 28 feet bls. Duncklee & Dunham purged groundwater from each well using a peristaltic pump until the purge water appeared clear. Troxler containerized the purge water from each of the five wells in a 55-gallon drum and staged the drum near the concrete pad in the center of the site.
Duncklee & Dunham contacted Eastern Environmental Management, LLC to dispose of the contents of the drum.
Duncklee & Dunham sampled each well with a peristaltic pump using a new length of low-density polyethylene tubing and silicon tubing for the pump head. We placed the groundwater samples in laboratory-supplied containers, placed the containers in a cooler with ice, and brought the cooler back to our office under chain of custody. The courier for ENCO Laboratories (ENCO) delivered the cooler to their laboratory, which tested the groundwater samples for VOCs according to EPA Method 8260D, semivolatile organic compounds (SVOCs) and organophosphate pesticides according to EPA Method 8270E, organochlorine pesticides according to EPA Method 8081B, chlorinated herbicides according to
Letter Report of Environmental Services Davis-McCoy Parcel Wilson, North Carolina April 25, 2019 Page 3 of 4
DUNCKLEE & DUNHAM, P.C.
EPA method 8151A, nitrate according to EPA Method 353.2, phosphorus according to EPA Method 365.4, and sulfate according to EPA Method 300.0.
Troxler abandoned the temporary wells after we collected the groundwater samples and used soil cuttings to backfill the boreholes. A Well Abandonment Record for these wells is attached. Troxler sent a copy of this record to NCDEQ.
Laboratory Results The groundwater test results are summarized on Table 1 and Figure 3; the laboratory report is attached. The laboratory detected 1,2-dichloropropane in TMW-4 at a concentration that exceeded the North Carolina groundwater quality standards promulgated in Title 15A, Subchapter 2L, Section .0202 of the North Carolina Administrative Code (15A NCAC 2L .0202; the “2L standards”). The laboratory also detected nitrate and sulfate in TMW-1 and -5 at concentrations that that exceeded the 2L Standards.
Discussion The highest concentrations of nitrate and sulfate were detected in TMW-1. Coal storage bins and ASTs
used to store “chemicals” were formerly present near this well, and the analytes detected by the laboratory in TMW-1 may have originated from the liquids stored in these ASTs. Fertilizers are commonly comprised of nitrate, phosphorus, and sulfate, which may have been the “chemicals” stored in these
ASTs. The analytes detected in TMW-5 may have originated from these ASTs or from the storage of bulk acid and mixing of fertilizer formerly conducted in the building in the western corner of the site. In the past, 1,2-dichloropropane was used in agricultural practices as a fumigant. It may have been stored on the site. The analytes detected in TMW-4 may have originated from the Kaiser Agricultural Chemicals site formerly across Stemmery Street South from the subject site. Based on topographic observations, we expect groundwater beneath the site flows to the southwest, towards Hominy Swamp. Findings
The laboratory detected 1,2-dichloropropane in TMW-4 and nitrate and sulfate in TMW-1 and -5 at concentrations that exceeded the 2L Standards. Nitrate and sulfate are common agricultural chemicals
and were likely stored on the site in the past. A second possible/additional source of the compounds found in the sample from TMW-4 is the former Kaiser Agricultural Chemicals site across Stemmery Street South.

Letter Report of Environmental Services Davis-McCoy Parcel Wilson, North Carolina April 25, 2019 Page 4 of 4
DUNCKLEE & DUNHAM, P.C.
We appreciate the opportunity to provide our services to the City of Wilson. Please contact us if you have any questions.
Sincerely, Duncklee & Dunham, P.C.

Alec N. Dziwanowski, G.I.T. Staff Geologist

Richard A. Kolb, L.G. Senior Geologist Senior Peer Review
Thomas S. Dunham, P.G. Senior Geologist
Attachments: Figures 1-3 Table 1
Laboratory Test Report Well Abandonment Record

P:\Wilson, City of\2018280 - Davis-McCoy Parcel\Phase II\Report\Environmental Services Letter Report - 19211.doc
Attachments
SITE
0 2000'4000'
1" = 2000'
April 20192018280
Davis-McCoy ParcelWilson, North Carolina
Site Topographic Map
pjs
P:\Wilson, City of\2018280 - Davis-McCoy Parcel\CAD\Site Map.dwg
1
Figure
USGS TopoView: Wilson - 1998
0,18.5" x 11"
511 Keisler Drive Suite 102 [phone]
DUNCKLEE & DUNHAM
ENVIRONMENTAL GEOLOGISTS & ENGINEERSD
Cary, North Carolina 27518 www.dunckleedunham.com
NC Eng. License No. C-3559 NC Geo. License No. C-261
Contour Interval = 10ft
N
Drawn By:Checked By:Project Number:Date:
Scale:Size:Layers:Filename:
References:
Wooded
Pallet
Debris
Ste
m
m
e
r
y

S
t
r
e
e
t

S
o
u
t
h
Maury Street SouthGay Street SouthGrace Street SouthMoore Street South (Unpaved Right-of-way)526
Evening Light Holiness Church
208 Pender Street South
500 Barnes Street South
Undeveloped
(Former Kaiser Agricultural
Chemicals Site)
301 Railroad Street South
Undeveloped
404Pender Street Park403/405408401805 817
530
305309Bar
n
e
s

S
t
r
e
e
t

S
o
u
t
h
Ramp
Truck Scale
Wilson
Metal
Recycling
SFR
Undeveloped
Undeveloped
Grass Field319
T
T
T
T
T
TMW-4
TMW-5 TMW-1
TMW-3
TMW-2
0 120'240'
1" = 120'
April 2019
Davis-McCoy ParcelWilson, North Carolina
Sample Locations
pjs
P:\Wilson, City of\2018280 - Davis-McCoy Parcel\CAD\Site Map.dwg
2
Figure
NC OneMap - Wilson County
8.5" x 11"
DUNCKLEE & DUNHAM
ENVIRONMENTAL GEOLOGISTS & ENGINEERSD
Cary, North Carolina 27518 www.dunckleedunham.com
NC Eng. License No. C-3559 NC Geo. License No. C-261
0-5,7-10
511 Keisler Drive Suite 102 [phone] Drawn By:Checked By:Project Number:Date:
Scale:Size:Layers:Filename:
References:
Legend
526
Boundary of Subject Site
Boundary of Tax Parcel
Right-of-way of Road
Building Footprint
Street Address
Bay Door
Pole-mounted Transformer
Railroad Tracks
SFR Single-family Residence
N
Concrete Slab
2018280
Pole-mounted Transformer
Temporary Monitoring Well
Temporary Monitoring Well
and Soil Boring
T
T
TMW-2
TMW-1
Wooded
Pallet
Debris
Ste
m
m
e
r
y

S
t
r
e
e
t

S
o
u
t
h
Maury Street SouthGay Street SouthGrace Street SouthMoore Street South (Unpaved Right-of-way)526
Evening Light Holiness Church
208 Pender Street South
500 Barnes Street South
Undeveloped
(Former Kaiser Agricultural
Chemicals Site)
301 Railroad Street South
Undeveloped
404Pender Street Park403/405408401805 817
530
305309Bar
n
e
s

S
t
r
e
e
t

S
o
u
t
h
Ramp
Truck Scale
Wilson
Metal
Recycling
SFR
Undeveloped
Undeveloped
Grass Field319
T
T
T
T
T
TMW-4
TMW-5 TMW-1
TMW-3
TMW-2
0 120'240'
1" = 120'
April 2019
Davis-McCoy ParcelWilson, North Carolina
Site Map of Sample Results
pjs
P:\Wilson, City of\2018280 - Davis-McCoy Parcel\CAD\Site Map.dwg
3
Figure
NC OneMap - Wilson County
8.5" x 11"
DUNCKLEE & DUNHAM
ENVIRONMENTAL GEOLOGISTS & ENGINEERSD
Cary, North Carolina 27518 www.dunckleedunham.com
NC Eng. License No. C-3559 NC Geo. License No. C-261
0-5,7,8,10,11
511 Keisler Drive Suite 102 [phone] Drawn By:Checked By:Project Number:Date:
Scale:Size:Layers:Filename:
References:
Legend
526
Boundary of Subject Site
Boundary of Tax Parcel
Right-of-way of Road
Building Footprint
Street Address
Bay Door
Pole-mounted Transformer
Railroad Tracks
SFR Single-family Residence
N
Concrete Slab
2018280
T
T
Pole-mounted Transformer
Temporary Monitoring Well
Temporary Monitoring Well
and Soil Boring
TMW-5
Phosphorus
Sulfate
57 J
35
Nitrite
TMW-4
1,2-Dichloropropane
Nitrate
Phosphorus
Sulfate
460 J D
200
4,100
94,000 D
Nitrite
TMW-1
Methyl-tert-Butyl Ether
Naphthalene
2,4-D
3.8
1.2
1.2
Nitrate
Phosphorus
Sulfate
130,000 D
350
920
380,000 D
Nitrite
TMW-2
Phosphorus
Sulfate
260
660
180,000 D
Nitrite
TMW-3
Nitrate
Phosphorus
Sulfate
6,400 D
540
480
81,000
Nitrite
Note: Groundwater results are in µg/L.
Result in bold exceeds the method reporting limit.
Result in bold with shaded cell exceeds the
respective 2L Standard.
J - Estimated concentration above the method
detection limit and below the method reporting limit.
D - The sample was analyzed at dilution.
33,000 D
360,000 D
7.8
TMW-2
TMW-1
Nitrate

Divider
Page
Analyte 2L Standard Value Q Value Q Value Q Value Q Value Q1,2-Dichloropropane 0.6 <0.10 <0.10 <0.107.8<0.10Methyl-tert-Butyl Ether 203.8<0.16 <0.16 <0.16 <0.16Naphthalene 61.2<0.11 <0.11 <0.11 <0.112,4-D 701.2<0.27 <0.27 <0.27 <0.27Nitrate 10,000130,000D <2006,400D 460 J D33,000DNitrite 1,000350 260 540 20057 JPhosphorus NE920 660 480 4,100 35Sulfate 250,000380,000D180,000D81,000 94,000D360,000DNotes:Units are µg/LSamples were collected on March 14, 20192L Standard - North Carolina Groundwater Quality Standard (15A NCAC 2L .0202)Result in bold exceeds the method reporting limitResult in bold with shaded cell exceeds the respective 2L Standard< - Analyte not detected at a concentration that exceeds the method reporting limit shownNE - Not EstablishedQ - QualifierD - The sample was analyzed at dilutionJ - Estimated concentration above the method detection limit and below the method reporting limitChlorinated Herbicides by EPA Method 8151A Chemistry Parameters by EPA Methods 353.2, 365.4, and 300.0Volatile Organic Compounds by EPA Method 8260DWilson, North CarolinaDavis-McCoy ParcelSummary of Laboratory Test Results, Groundwater SamplesTable 1TMW-5TMW-4TMW-3TMW-2TMW-1Sample IdentificationP:\Wilson, City of\2018280 - Davis-McCoy Parcel\Phase II\Tables\Table 1 - GW Results

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Page
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:
ENCO Workorder(s): CC03837
Cary, NC 27518
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Davis - McCoy Parcel
Attn: Rick Kolb
Duncklee & Dunham, PC (DU009)
511 Keisler Drive, Suite 102
Chuck Smith
Project Manager
Friday, March 29, 2019
RE: Laboratory Results for
Dear Rick Kolb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, March 15, 2019.
Enclosure(s)
Page 1 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
TMW-1 CC03837-01 Sampled:03/14/19 11:10 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 353.2 03/16/19 11:10 03/15/19 12:16 03/15/19 12:16NO PREP
EPA 353.2 03/16/19 11:10 03/28/19 14:02 03/28/19 17:37[CALC]
EPA 365.4 04/11/19 03/25/19 09:16 03/27/19 15:07Same
EPA 8081B 03/21/19 03/18/19 13:38 03/21/19 17:5004/27/19EPA 3510C
EPA 8151A 03/21/19 03/21/19 11:50 03/25/19 13:2504/30/19EPA 3510C
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 01:25EPA 5030B_MS
EPA 8270E 03/21/19 03/18/19 09:14 03/19/19 17:3304/27/19EPA 3510C_MS
EPA 8270E 03/21/19 03/21/19 06:48 03/22/19 15:1304/30/19EPA 3510C_MS
TMW-1 CC03837-01RE1 Sampled:03/14/19 11:10 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 300.0 04/11/19 03/26/19 10:55 03/26/19 10:55NO PREP
TMW-1 CC03837-01RE2 Sampled:03/14/19 11:10 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 353.2 04/11/19 03/28/19 14:02 03/28/19 17:37NO PREP
TMW-2 CC03837-02 Sampled:03/14/19 11:50 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 353.2 03/16/19 11:50 03/15/19 12:17 03/15/19 12:17NO PREP
EPA 353.2 03/16/19 11:50 03/25/19 19:04 03/25/19 19:04[CALC]
EPA 353.2 04/11/19 03/25/19 19:04 03/25/19 19:04NO PREP
EPA 365.4 04/11/19 03/25/19 09:16 03/27/19 15:08Same
EPA 8081B 03/21/19 03/18/19 13:38 03/21/19 18:0704/27/19EPA 3510C
EPA 8151A 03/21/19 03/21/19 11:50 03/25/19 13:5004/30/19EPA 3510C
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 01:56EPA 5030B_MS
EPA 8270E 03/21/19 03/21/19 06:48 03/22/19 15:4704/30/19EPA 3510C_MS
TMW-2 CC03837-02RE1 Sampled:03/14/19 11:50 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 300.0 04/11/19 03/26/19 11:09 03/26/19 11:09NO PREP
EPA 8270E 03/21/19 03/18/19 09:14 03/22/19 22:3104/27/19EPA 3510C_MS
TMW-3 CC03837-03 Sampled:03/14/19 12:50 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 300.0 04/11/19 03/25/19 22:10 03/25/19 22:10NO PREP
EPA 353.2 03/16/19 12:50 03/15/19 12:18 03/15/19 12:18NO PREP
EPA 353.2 03/16/19 12:50 03/25/19 19:06 03/25/19 19:06[CALC]
EPA 353.2 04/11/19 03/25/19 19:06 03/25/19 19:06NO PREP
EPA 365.4 04/11/19 03/25/19 09:16 03/27/19 15:09Same
EPA 8081B 03/21/19 03/18/19 13:38 03/21/19 18:2304/27/19EPA 3510C
EPA 8151A 03/21/19 03/21/19 11:50 03/25/19 14:1504/30/19EPA 3510C
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 02:28EPA 5030B_MS
EPA 8270E 03/21/19 03/18/19 09:14 03/19/19 18:3204/27/19EPA 3510C_MS
EPA 8270E 03/21/19 03/21/19 06:48 03/22/19 16:2004/30/19EPA 3510C_MS
Page 2 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
TMW-4 CC03837-04 Sampled:03/14/19 15:25 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 353.2 03/16/19 15:25 03/15/19 12:19 03/15/19 12:19NO PREP
EPA 353.2 03/16/19 15:25 03/25/19 19:07 03/25/19 19:07[CALC]
EPA 353.2 04/11/19 03/25/19 19:07 03/25/19 19:07NO PREP
EPA 365.4 04/11/19 03/25/19 09:16 03/27/19 15:10Same
EPA 8081B 03/21/19 03/18/19 13:38 03/21/19 18:4004/27/19EPA 3510C
EPA 8151A 03/21/19 03/21/19 11:50 03/25/19 14:4104/30/19EPA 3510C
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 02:59EPA 5030B_MS
EPA 8270E 03/21/19 03/18/19 09:14 03/19/19 19:0204/27/19EPA 3510C_MS
EPA 8270E 03/21/19 03/21/19 06:48 03/22/19 16:5304/30/19EPA 3510C_MS
TMW-4 CC03837-04RE1 Sampled:03/14/19 15:25 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 300.0 04/11/19 03/26/19 11:24 03/26/19 11:24NO PREP
TMW-5 CC03837-05 Sampled:03/14/19 16:15 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 353.2 03/16/19 16:15 03/15/19 12:20 03/15/19 12:20NO PREP
EPA 353.2 03/16/19 16:15 03/28/19 14:02 03/28/19 17:39[CALC]
EPA 365.4 04/11/19 03/25/19 09:16 03/27/19 15:11Same
EPA 8081B 03/21/19 03/18/19 13:38 03/21/19 18:5704/27/19EPA 3510C
EPA 8151A 03/21/19 03/21/19 11:50 03/25/19 15:0604/30/19EPA 3510C
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 03:31EPA 5030B_MS
EPA 8270E 03/21/19 03/18/19 09:14 03/19/19 19:3204/27/19EPA 3510C_MS
EPA 8270E 03/21/19 03/21/19 06:48 03/22/19 17:2604/30/19EPA 3510C_MS
TMW-5 CC03837-05RE1 Sampled:03/14/19 16:15 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 300.0 04/11/19 03/26/19 11:53 03/26/19 11:53NO PREP
EPA 353.2 04/11/19 03/28/19 14:02 03/28/19 17:39NO PREP
Trip Blank CC03837-06 Sampled:03/14/19 11:10 Received:03/15/19 09:32Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8260D 03/28/19 03/15/19 15:00 03/16/19 04:02EPA 5030B_MS
Page 3 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
SAMPLE DETECTION SUMMARY
Lab ID:Client ID:TMW-1 CC03837-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.2 0.50 ug/L EPA 8151A 2,4-D 0.27
3.8 1.0 ug/L EPA 8260D Methyl-tert-Butyl Ether 0.16
1.2 1.0 ug/L EPA 8260D Naphthalene 0.11
130 12 mg/L EPA 353.2D Nitrate as N 4.9
0.35 0.10 mg/L EPA 353.2 Nitrite as N 0.017
0.92 0.030 mg/L EPA 365.4 Phosphorus 0.020
Lab ID:Client ID:TMW-1 CC03837-01RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
380 50 mg/L EPA 300.0D Sulfate as SO4 29
Lab ID:Client ID:TMW-1 CC03837-01RE2
Analyte MethodUnitsPQLResultsFlag NotesMDL
130 12 mg/L EPA 353.2D Nitrate/Nitrite as N 4.9
Lab ID:Client ID:TMW-2 CC03837-02
Analyte MethodUnitsPQLResultsFlag NotesMDL
0.33 0.50 mg/L EPA 353.2JD Nitrate/Nitrite as N 0.20
0.26 0.10 mg/L EPA 353.2 Nitrite as N 0.017
0.66 0.030 mg/L EPA 365.4 Phosphorus 0.020
Lab ID:Client ID:TMW-2 CC03837-02RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
180 10 mg/L EPA 300.0D Sulfate as SO4 5.8
Lab ID:Client ID:TMW-3 CC03837-03
Analyte MethodUnitsPQLResultsFlag NotesMDL
6.4 0.50 mg/L EPA 353.2D Nitrate as N 0.20
6.9 0.50 mg/L EPA 353.2D Nitrate/Nitrite as N 0.20
0.54 0.10 mg/L EPA 353.2 Nitrite as N 0.017
0.48 0.030 mg/L EPA 365.4 Phosphorus 0.020
81 5.0 mg/L EPA 300.0 Sulfate as SO4 2.9
Lab ID:Client ID:TMW-4 CC03837-04
Analyte MethodUnitsPQLResultsFlag NotesMDL
7.8 1.0 ug/L EPA 8260D 1,2-Dichloropropane 0.10
0.46 0.50 mg/L EPA 353.2JD Nitrate as N 0.20
0.66 0.50 mg/L EPA 353.2D Nitrate/Nitrite as N 0.20
0.20 0.10 mg/L EPA 353.2 Nitrite as N 0.017
4.1 0.030 mg/L EPA 365.4 Phosphorus 0.020
Lab ID:Client ID:TMW-4 CC03837-04RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
94 10 mg/L EPA 300.0D Sulfate as SO4 5.8
Lab ID:Client ID:TMW-5 CC03837-05
Analyte MethodUnitsPQLResultsFlag NotesMDL
33 2.0 mg/L EPA 353.2D Nitrate as N 0.82
0.057 0.10 mg/L EPA 353.2J Nitrite as N 0.017
0.035 0.030 mg/L EPA 365.4 Phosphorus 0.020
Lab ID:Client ID:TMW-5 CC03837-05RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
33 2.0 mg/L EPA 353.2D Nitrate/Nitrite as N 0.82
360 25 mg/L EPA 300.0D Sulfate as SO4 14
Lab ID:Client ID:Trip Blank CC03837-06
Analyte MethodUnitsPQLResultsFlag NotesMDL
11 20 ug/L EPA 8260DJB O-01Acetone10
Page 4 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 01:251,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:251,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 01:251,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 01:251,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:251,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 01:251,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:251,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:251,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 01:251,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:251,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:251,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:251,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 01:251,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 01:251,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 01:251,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:251,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:251,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 01:251,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:251,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 01:251,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 01:252,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 01:252-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 01:252-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 01:252-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 01:252-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 01:254-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 01:254-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 01:254-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 01:25Acetone [67-64-1]^10 MRK9C150222010U O-011
ug/L EPA 8260D 03/16/19 01:25Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:25Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 01:25Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 01:25Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 01:25Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:25Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 01:25Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:25Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 01:25Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 01:25cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:25cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 01:25Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 01:25Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 01:25Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 5 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 01:25Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 01:25Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:25m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:25Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.03.8 1
ug/L EPA 8260D 03/16/19 01:25Naphthalene [91-20-3]^0.11 MRK9C150221.01.2 1
ug/L EPA 8260D 03/16/19 01:25n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 01:25n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 01:25o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 01:25sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:25Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 01:25tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:25Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:25trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:25trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:25Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:25Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 01:25Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 01:25Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136103 %MRKEPA 8260D 03/16/19 01:259C150225250.0 1
Dibromofluoromethane 67-12999 %MRKEPA 8260D 03/16/19 01:259C150225050.0 1
Toluene-d8 59-134102 %MRKEPA 8260D 03/16/19 01:259C150225150.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 17:331,2,4-Trichlorobenzene [120-82-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:331,2-Dichlorobenzene [95-50-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:331,3-Dichlorobenzene [541-73-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:331,4-Dichlorobenzene [106-46-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:331-Methylnaphthalene [90-12-0]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 17:332,4,5-Trichlorophenol [95-95-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:332,4,6-Trichlorophenol [88-06-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:332,4-Dichlorophenol [120-83-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:332,4-Dimethylphenol [105-67-9]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 17:332,4-Dinitrophenol [51-28-5]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:332,4-Dinitrotoluene [121-14-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:332,6-Dinitrotoluene [606-20-2]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:332-Chloronaphthalene [91-58-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:332-Chlorophenol [95-57-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 17:332-Methyl-4,6-dinitrophenol [534-52-1]^3.3 DFM9C18010103.3 U 1
ug/L EPA 8270E 03/19/19 17:332-Methylnaphthalene [91-57-6]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:332-Methylphenol [95-48-7]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 17:332-Nitroaniline [88-74-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:332-Nitrophenol [88-75-5]^1.1 DFM9C18010101.1 U 1
Page 6 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 17:333 & 4-Methylphenol [108-39-4/106-44-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 17:333,3’-Dichlorobenzidine [91-94-1]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 17:333-Nitroaniline [99-09-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:334-Bromophenyl-phenylether [101-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:334-Chloro-3-methylphenol [59-50-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:334-Chloroaniline [106-47-8]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 17:334-Chlorophenyl-phenylether [7005-72-3]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:334-Nitroaniline [100-01-6]^3.2 DFM9C18010103.2 U 1
ug/L EPA 8270E 03/19/19 17:334-Nitrophenol [100-02-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:33Acenaphthene [83-32-9]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 17:33Acenaphthylene [208-96-8]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:33Anthracene [120-12-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Benzidine [92-87-5]^1.6 DFM9C18010101.6 U QV-011
ug/L EPA 8270E 03/19/19 17:33Benzo(a)anthracene [56-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Benzo(a)pyrene [50-32-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 17:33Benzo(b)fluoranthene [205-99-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:33Benzo(g,h,i)perylene [191-24-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Benzo(k)fluoranthene [207-08-9]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Benzoic acid [65-85-0]^1.0 DFM9C18010501.0 U QV-021
ug/L EPA 8270E 03/19/19 17:33Benzyl alcohol [100-51-6]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Bis(2-chloroethoxy)methane [111-91-1]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Bis(2-chloroethyl)ether [111-44-4]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:33Bis(2-chloroisopropyl)ether [108-60-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33Bis(2-ethylhexyl)phthalate [117-81-7]^1.9 DFM9C180105.01.9 U 1
ug/L EPA 8270E 03/19/19 17:33Butylbenzylphthalate [85-68-7]^3.8 DFM9C18010103.8 U 1
ug/L EPA 8270E 03/19/19 17:33Chrysene [218-01-9]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 17:33Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 17:33Dibenzofuran [132-64-9]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:33Diethylphthalate [84-66-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 17:33Dimethylphthalate [131-11-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33Di-n-butylphthalate [84-74-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:33Di-n-octylphthalate [117-84-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 17:33Fluoranthene [206-44-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 17:33Fluorene [86-73-7]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33Hexachlorobenzene [118-74-1]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 17:33Hexachlorobutadiene [87-68-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:33Hexachlorocyclopentadiene [77-47-4]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 17:33Hexachloroethane [67-72-1]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 17:33Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 17:33Isophorone [78-59-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33Naphthalene [91-20-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 17:33Nitrobenzene [98-95-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33N-Nitrosodimethylamine [62-75-9]^1.9 DFM9C18010101.9 U 1
ug/L EPA 8270E 03/19/19 17:33N-Nitroso-di-n-propylamine [621-64-7]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 17:33N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4]^
2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 17:33Pentachlorophenol [87-86-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 17:33Phenanthrene [85-01-8]^2.6 DFM9C18010102.6 U 1
Page 7 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 17:33Phenol [108-95-2]^1.7 DFM9C18010101.7 U 1
ug/L EPA 8270E 03/19/19 17:33Pyrene [129-00-0]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 17:33Pyridine [110-86-1]^2.2 DFM9C18010102.2 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17985 %DFMEPA 8270E 03/19/19 17:339C1801085100 1
2-Fluorobiphenyl 10-14972 %DFMEPA 8270E 03/19/19 17:339C180103650.0 1
2-Fluorophenol 10-11050 %DFMEPA 8270E 03/19/19 17:339C1801050100 1
Nitrobenzene-d5 10-14963 %DFMEPA 8270E 03/19/19 17:339C180103250.0 1
Phenol-d5 10-8851 %DFMEPA 8270E 03/19/19 17:339C1801051100 1
Terphenyl-d14 10-18863 %DFMEPA 8270E 03/19/19 17:339C180103150.0 1
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8081B 03/21/19 17:504,4’-DDD [72-54-8]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 17:504,4’-DDE [72-55-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 17:504,4’-DDT [50-29-3]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 17:50Aldrin [309-00-2]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 17:50alpha-BHC [319-84-6]^0.036 LSK9C180350.0500.036 U 1
ug/L EPA 8081B 03/21/19 17:50beta-BHC [319-85-7]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 17:50Chlordane (tech) [12789-03-6]^0.37 LSK9C180350.500.37 U 1
ug/L EPA 8081B 03/21/19 17:50Chlordane-alpha [5103-71-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 17:50Chlordane-gamma [5103-74-2]^0.042 LSK9C180350.0500.042 U 1
ug/L EPA 8081B 03/21/19 17:50delta-BHC [319-86-8]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 17:50Dieldrin [60-57-1]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 17:50Endosulfan I [959-98-8]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 17:50Endosulfan II [33213-65-9]^0.038 LSK9C180350.0500.038 U 1
ug/L EPA 8081B 03/21/19 17:50Endosulfan sulfate [1031-07-8]^0.032 LSK9C180350.0500.032 U 1
ug/L EPA 8081B 03/21/19 17:50Endrin [72-20-8]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 17:50Endrin aldehyde [7421-93-4]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 17:50Endrin ketone [53494-70-5]^0.039 LSK9C180350.0500.039 U 1
ug/L EPA 8081B 03/21/19 17:50gamma-BHC [58-89-9]^0.034 LSK9C180350.0500.034 U 1
ug/L EPA 8081B 03/21/19 17:50Heptachlor [76-44-8]^0.047 LSK9C180350.0500.047 U 1
ug/L EPA 8081B 03/21/19 17:50Heptachlor epoxide [1024-57-3]^0.037 LSK9C180350.0500.037 U 1
ug/L EPA 8081B 03/21/19 17:50Isodrin [465-73-6]^0.031 LSK9C180350.0500.031 U 1
ug/L EPA 8081B 03/21/19 17:50Methoxychlor [72-43-5]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 17:50Mirex [2385-85-5]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 17:50Toxaphene [8001-35-2]^0.28 LSK9C180351.00.28 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,5,6-TCMX 10-139102 %LSKEPA 8081B 03/21/19 17:509C180351.0 1.00 1
Decachlorobiphenyl 10-122110 %LSKEPA 8081B 03/21/19 17:509C180351.1 1.00 1
Page 8 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 353.2 03/28/19 17:37Nitrate as N [14797-55-8]4.9 MKS[CALC]12130D 120
mg/L EPA 353.2 03/28/19 17:37Nitrate/Nitrite as N^4.9 MKS9C2802612130D 120
mg/L EPA 353.2 03/15/19 12:16Nitrite as N [14797-65-0]^0.017 MKS9C150070.100.35 1
mg/L EPA 300.0 03/26/19 10:55Sulfate as SO4 [14808-79-8]^29 MKS9C2503150380D 10
Semivolatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 15:13Azinphos-methyl [86-50-0]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:13Bolstar [35400-43-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:13Chlorpyrifos [2921-88-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:13Coumaphos [56-72-4]0.29 jfi9C210010.500.29 U 1
ug/L EPA 8270E 03/22/19 15:13Demeton [8065-48-3]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:13Diazinon [333-41-5]0.23 jfi9C210010.500.23 U 1
ug/L EPA 8270E 03/22/19 15:13Dichlorofenthion [97-17-6]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:13Dichlorvos [62-73-7]0.35 jfi9C210010.500.35 U 1
ug/L EPA 8270E 03/22/19 15:13Dimethoate [60-51-5]0.27 jfi9C210010.500.27 U 1
ug/L EPA 8270E 03/22/19 15:13Disulfoton [298-04-4]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:13EPN [2104-64-5]0.45 jfi9C210010.500.45 U 1
ug/L EPA 8270E 03/22/19 15:13Ethion [563-12-2]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:13Ethoprop [13194-48-4]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:13Ethyl Parathion [56-38-2]0.31 jfi9C210010.500.31 U 1
ug/L EPA 8270E 03/22/19 15:13Fensulfothion [115-90-2]0.32 jfi9C210010.500.32 U 1
ug/L EPA 8270E 03/22/19 15:13Fenthion [55-38-9]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:13Malathion [121-75-5]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:13Merphos [150-50-5]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:13Methyl parathion [298-00-0]0.33 jfi9C210010.500.33 U 1
ug/L EPA 8270E 03/22/19 15:13Mevinphos [7786-34-7]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:13Monocrotophos [6923-22-4]0.054 jfi9C210010.500.054 U 1
ug/L EPA 8270E 03/22/19 15:13Naled [300-76-5]0.15 jfi9C210011.00.15 U 1
ug/L EPA 8270E 03/22/19 15:13Phorate [298-02-2]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:13Ronnel [299-84-3]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:13Stirophos (Tetrachlorvinphos) [22248-79-9]0.38 jfi9C210010.500.38 U 1
ug/L EPA 8270E 03/22/19 15:13Sulfotep [3689-24-5]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:13TEPP [107-49-3]0.20 jfi9C210011.00.20 U 1
ug/L EPA 8270E 03/22/19 15:13Tokuthion (Prothiofos) [34643-46-4]0.24 jfi9C210010.500.24 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Tributyl Phosphate 50-150112 %jfiEPA 8270E 03/22/19 15:139C210014.5 4.02 1
Triphenyl phosphate 50-15097 %jfiEPA 8270E 03/22/19 15:139C210013.9 4.02 1
Page 9 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-1Description:Lab Sample ID:CC03837-01 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8151A 03/25/19 13:252,4,5-T [93-76-5]^0.28 RGG9C210260.500.28 U 1
ug/L EPA 8151A 03/25/19 13:252,4,5-TP (Silvex) [93-72-1]^0.44 RGG9C210260.500.44 U 1
ug/L EPA 8151A 03/25/19 13:252,4-D [94-75-7]^0.27 RGG9C210260.501.2 1
ug/L EPA 8151A 03/25/19 13:252,4-DB [94-82-6]^0.35 RGG9C210260.500.35 U 1
ug/L EPA 8151A 03/25/19 13:253,5-DCBA [51-365-5]^0.36 RGG9C210260.500.36 U 1
ug/L EPA 8151A 03/25/19 13:254-Nitrophenol [100-02-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 13:25Acifluorfen [50594-66-6]^0.45 RGG9C210260.500.45 U 1
ug/L EPA 8151A 03/25/19 13:25Bentazon [25057-89-0]^0.22 RGG9C210260.500.22 U 1
ug/L EPA 8151A 03/25/19 13:25Chloramben [133-90-4]^0.43 RGG9C210260.500.43 U 1
ug/L EPA 8151A 03/25/19 13:25Dacthal [1861-32-1]^0.23 RGG9C210260.500.23 U 1
ug/L EPA 8151A 03/25/19 13:25Dalapon [75-99-0]^0.49 RGG9C210260.500.49 U 1
ug/L EPA 8151A 03/25/19 13:25Dicamba [1918-00-9]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 13:25Dichlorprop [120-36-5]^0.31 RGG9C210260.500.31 U 1
ug/L EPA 8151A 03/25/19 13:25Dinoseb [88-85-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 13:25MCPA [94-74-6]^34 RGG9C210265034U QV-011
ug/L EPA 8151A 03/25/19 13:25MCPP [7085-19-0]^46 RGG9C210265046U 1
ug/L EPA 8151A 03/25/19 13:25Pentachlorophenol [87-86-5]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 13:25Picloram [1918-02-1]^0.23 RGG9C210260.500.23 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4-DCAA 37-134125 %RGGEPA 8151A 03/25/19 13:259C210262.6 2.04 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 365.4 03/27/19 15:07Phosphorus [7723-14-0]^0.020 kgonz9C250150.0300.92 1
Page 10 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 01:561,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:561,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 01:561,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 01:561,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:561,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 01:561,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:561,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:561,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 01:561,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:561,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:561,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:561,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 01:561,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 01:561,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 01:561,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:561,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:561,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 01:561,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:561,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 01:561,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 01:562,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 01:562-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 01:562-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 01:562-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 01:562-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 01:564-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 01:564-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 01:564-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 01:56Acetone [67-64-1]^10 MRK9C150222010U O-011
ug/L EPA 8260D 03/16/19 01:56Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:56Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 01:56Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 01:56Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 01:56Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:56Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 01:56Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:56Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 01:56Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 01:56cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:56cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 01:56Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 01:56Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 01:56Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 11 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 01:56Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 01:56Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:56m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 01:56Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 01:56Naphthalene [91-20-3]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 01:56n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 01:56n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 01:56o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 01:56sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 01:56Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 01:56tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 01:56Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 01:56trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 01:56trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:56Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 01:56Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 01:56Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 01:56Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136104 %MRKEPA 8260D 03/16/19 01:569C150225250.0 1
Dibromofluoromethane 67-129101 %MRKEPA 8260D 03/16/19 01:569C150225050.0 1
Toluene-d8 59-134103 %MRKEPA 8260D 03/16/19 01:569C150225150.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 22:311,2,4-Trichlorobenzene [120-82-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:311,2-Dichlorobenzene [95-50-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:311,3-Dichlorobenzene [541-73-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:311,4-Dichlorobenzene [106-46-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:311-Methylnaphthalene [90-12-0]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/22/19 22:312,4,5-Trichlorophenol [95-95-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:312,4,6-Trichlorophenol [88-06-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:312,4-Dichlorophenol [120-83-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:312,4-Dimethylphenol [105-67-9]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/22/19 22:312,4-Dinitrophenol [51-28-5]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:312,4-Dinitrotoluene [121-14-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:312,6-Dinitrotoluene [606-20-2]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:312-Chloronaphthalene [91-58-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:312-Chlorophenol [95-57-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/22/19 22:312-Methyl-4,6-dinitrophenol [534-52-1]^3.3 DFM9C18010103.3 U 1
ug/L EPA 8270E 03/22/19 22:312-Methylnaphthalene [91-57-6]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:312-Methylphenol [95-48-7]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/22/19 22:312-Nitroaniline [88-74-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:312-Nitrophenol [88-75-5]^1.1 DFM9C18010101.1 U 1
Page 12 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 22:313 & 4-Methylphenol [108-39-4/106-44-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/22/19 22:313,3’-Dichlorobenzidine [91-94-1]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/22/19 22:313-Nitroaniline [99-09-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:314-Bromophenyl-phenylether [101-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:314-Chloro-3-methylphenol [59-50-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:314-Chloroaniline [106-47-8]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/22/19 22:314-Chlorophenyl-phenylether [7005-72-3]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:314-Nitroaniline [100-01-6]^3.2 DFM9C18010103.2 U 1
ug/L EPA 8270E 03/22/19 22:314-Nitrophenol [100-02-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:31Acenaphthene [83-32-9]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/22/19 22:31Acenaphthylene [208-96-8]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:31Anthracene [120-12-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Benzidine [92-87-5]^1.6 DFM9C18010101.6 U 1
ug/L EPA 8270E 03/22/19 22:31Benzo(a)anthracene [56-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Benzo(a)pyrene [50-32-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/22/19 22:31Benzo(b)fluoranthene [205-99-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:31Benzo(g,h,i)perylene [191-24-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Benzo(k)fluoranthene [207-08-9]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Benzoic acid [65-85-0]^1.0 DFM9C18010501.0 U 1
ug/L EPA 8270E 03/22/19 22:31Benzyl alcohol [100-51-6]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Bis(2-chloroethoxy)methane [111-91-1]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Bis(2-chloroethyl)ether [111-44-4]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:31Bis(2-chloroisopropyl)ether [108-60-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31Bis(2-ethylhexyl)phthalate [117-81-7]^1.9 DFM9C180105.01.9 U 1
ug/L EPA 8270E 03/22/19 22:31Butylbenzylphthalate [85-68-7]^3.8 DFM9C18010103.8 U 1
ug/L EPA 8270E 03/22/19 22:31Chrysene [218-01-9]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/22/19 22:31Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/22/19 22:31Dibenzofuran [132-64-9]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:31Diethylphthalate [84-66-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/22/19 22:31Dimethylphthalate [131-11-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31Di-n-butylphthalate [84-74-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:31Di-n-octylphthalate [117-84-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/22/19 22:31Fluoranthene [206-44-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/22/19 22:31Fluorene [86-73-7]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31Hexachlorobenzene [118-74-1]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/22/19 22:31Hexachlorobutadiene [87-68-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:31Hexachlorocyclopentadiene [77-47-4]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/22/19 22:31Hexachloroethane [67-72-1]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/22/19 22:31Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/22/19 22:31Isophorone [78-59-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31Naphthalene [91-20-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/22/19 22:31Nitrobenzene [98-95-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31N-Nitrosodimethylamine [62-75-9]^1.9 DFM9C18010101.9 U 1
ug/L EPA 8270E 03/22/19 22:31N-Nitroso-di-n-propylamine [621-64-7]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/22/19 22:31N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4]^
2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/22/19 22:31Pentachlorophenol [87-86-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/22/19 22:31Phenanthrene [85-01-8]^2.6 DFM9C18010102.6 U 1
Page 13 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 22:31Phenol [108-95-2]^1.7 DFM9C18010101.7 U 1
ug/L EPA 8270E 03/22/19 22:31Pyrene [129-00-0]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/22/19 22:31Pyridine [110-86-1]^2.2 DFM9C18010102.2 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17990 %DFMEPA 8270E 03/22/19 22:319C1801090100 1
2-Fluorobiphenyl 10-14986 %DFMEPA 8270E 03/22/19 22:319C180104350.0 1
2-Fluorophenol 10-11065 %DFMEPA 8270E 03/22/19 22:319C1801065100 1
Nitrobenzene-d5 10-14977 %DFMEPA 8270E 03/22/19 22:319C180103950.0 1
Phenol-d5 10-8864 %DFMEPA 8270E 03/22/19 22:319C1801064100 1
Terphenyl-d14 10-18879 %DFMEPA 8270E 03/22/19 22:319C180103950.0 1
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8081B 03/21/19 18:074,4’-DDD [72-54-8]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:074,4’-DDE [72-55-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:074,4’-DDT [50-29-3]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:07Aldrin [309-00-2]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:07alpha-BHC [319-84-6]^0.036 LSK9C180350.0500.036 U 1
ug/L EPA 8081B 03/21/19 18:07beta-BHC [319-85-7]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:07Chlordane (tech) [12789-03-6]^0.37 LSK9C180350.500.37 U 1
ug/L EPA 8081B 03/21/19 18:07Chlordane-alpha [5103-71-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:07Chlordane-gamma [5103-74-2]^0.042 LSK9C180350.0500.042 U 1
ug/L EPA 8081B 03/21/19 18:07delta-BHC [319-86-8]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:07Dieldrin [60-57-1]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:07Endosulfan I [959-98-8]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:07Endosulfan II [33213-65-9]^0.038 LSK9C180350.0500.038 U 1
ug/L EPA 8081B 03/21/19 18:07Endosulfan sulfate [1031-07-8]^0.032 LSK9C180350.0500.032 U 1
ug/L EPA 8081B 03/21/19 18:07Endrin [72-20-8]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:07Endrin aldehyde [7421-93-4]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:07Endrin ketone [53494-70-5]^0.039 LSK9C180350.0500.039 U 1
ug/L EPA 8081B 03/21/19 18:07gamma-BHC [58-89-9]^0.034 LSK9C180350.0500.034 U 1
ug/L EPA 8081B 03/21/19 18:07Heptachlor [76-44-8]^0.047 LSK9C180350.0500.047 U 1
ug/L EPA 8081B 03/21/19 18:07Heptachlor epoxide [1024-57-3]^0.037 LSK9C180350.0500.037 U 1
ug/L EPA 8081B 03/21/19 18:07Isodrin [465-73-6]^0.031 LSK9C180350.0500.031 U 1
ug/L EPA 8081B 03/21/19 18:07Methoxychlor [72-43-5]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:07Mirex [2385-85-5]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:07Toxaphene [8001-35-2]^0.28 LSK9C180351.00.28 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,5,6-TCMX 10-13972 %LSKEPA 8081B 03/21/19 18:079C180350.72 1.00 1
Decachlorobiphenyl 10-12284 %LSKEPA 8081B 03/21/19 18:079C180350.84 1.00 1
Page 14 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 353.2 03/25/19 19:04Nitrate as N [14797-55-8]0.20 MKS[CALC]0.500.20 UD 5
mg/L EPA 353.2 03/25/19 19:04Nitrate/Nitrite as N^0.20 MKS9C250370.500.33 JD 5
mg/L EPA 353.2 03/15/19 12:17Nitrite as N [14797-65-0]^0.017 MKS9C150070.100.26 1
mg/L EPA 300.0 03/26/19 11:09Sulfate as SO4 [14808-79-8]^5.8 MKS9C2503110180D 2
Semivolatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 15:47Azinphos-methyl [86-50-0]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:47Bolstar [35400-43-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:47Chlorpyrifos [2921-88-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:47Coumaphos [56-72-4]0.29 jfi9C210010.500.29 U 1
ug/L EPA 8270E 03/22/19 15:47Demeton [8065-48-3]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:47Diazinon [333-41-5]0.23 jfi9C210010.500.23 U 1
ug/L EPA 8270E 03/22/19 15:47Dichlorofenthion [97-17-6]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 15:47Dichlorvos [62-73-7]0.35 jfi9C210010.500.35 U 1
ug/L EPA 8270E 03/22/19 15:47Dimethoate [60-51-5]0.27 jfi9C210010.500.27 U 1
ug/L EPA 8270E 03/22/19 15:47Disulfoton [298-04-4]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:47EPN [2104-64-5]0.45 jfi9C210010.500.45 U 1
ug/L EPA 8270E 03/22/19 15:47Ethion [563-12-2]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:47Ethoprop [13194-48-4]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:47Ethyl Parathion [56-38-2]0.31 jfi9C210010.500.31 U 1
ug/L EPA 8270E 03/22/19 15:47Fensulfothion [115-90-2]0.32 jfi9C210010.500.32 U 1
ug/L EPA 8270E 03/22/19 15:47Fenthion [55-38-9]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:47Malathion [121-75-5]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:47Merphos [150-50-5]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 15:47Methyl parathion [298-00-0]0.33 jfi9C210010.500.33 U 1
ug/L EPA 8270E 03/22/19 15:47Mevinphos [7786-34-7]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 15:47Monocrotophos [6923-22-4]0.054 jfi9C210010.500.054 U 1
ug/L EPA 8270E 03/22/19 15:47Naled [300-76-5]0.15 jfi9C210011.00.15 U 1
ug/L EPA 8270E 03/22/19 15:47Phorate [298-02-2]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:47Ronnel [299-84-3]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:47Stirophos (Tetrachlorvinphos) [22248-79-9]0.38 jfi9C210010.500.38 U 1
ug/L EPA 8270E 03/22/19 15:47Sulfotep [3689-24-5]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 15:47TEPP [107-49-3]0.20 jfi9C210011.00.20 U 1
ug/L EPA 8270E 03/22/19 15:47Tokuthion (Prothiofos) [34643-46-4]0.24 jfi9C210010.500.24 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Tributyl Phosphate 50-150104 %jfiEPA 8270E 03/22/19 15:479C210014.2 4.02 1
Triphenyl phosphate 50-15088 %jfiEPA 8270E 03/22/19 15:479C210013.6 4.02 1
Page 15 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-2Description:Lab Sample ID:CC03837-02 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8151A 03/25/19 13:502,4,5-T [93-76-5]^0.28 RGG9C210260.500.28 U 1
ug/L EPA 8151A 03/25/19 13:502,4,5-TP (Silvex) [93-72-1]^0.44 RGG9C210260.500.44 U 1
ug/L EPA 8151A 03/25/19 13:502,4-D [94-75-7]^0.27 RGG9C210260.500.27 U 1
ug/L EPA 8151A 03/25/19 13:502,4-DB [94-82-6]^0.35 RGG9C210260.500.35 U 1
ug/L EPA 8151A 03/25/19 13:503,5-DCBA [51-365-5]^0.36 RGG9C210260.500.36 U 1
ug/L EPA 8151A 03/25/19 13:504-Nitrophenol [100-02-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 13:50Acifluorfen [50594-66-6]^0.45 RGG9C210260.500.45 U 1
ug/L EPA 8151A 03/25/19 13:50Bentazon [25057-89-0]^0.22 RGG9C210260.500.22 U 1
ug/L EPA 8151A 03/25/19 13:50Chloramben [133-90-4]^0.43 RGG9C210260.500.43 U 1
ug/L EPA 8151A 03/25/19 13:50Dacthal [1861-32-1]^0.23 RGG9C210260.500.23 U 1
ug/L EPA 8151A 03/25/19 13:50Dalapon [75-99-0]^0.49 RGG9C210260.500.49 U 1
ug/L EPA 8151A 03/25/19 13:50Dicamba [1918-00-9]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 13:50Dichlorprop [120-36-5]^0.31 RGG9C210260.500.31 U 1
ug/L EPA 8151A 03/25/19 13:50Dinoseb [88-85-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 13:50MCPA [94-74-6]^34 RGG9C210265034U QV-011
ug/L EPA 8151A 03/25/19 13:50MCPP [7085-19-0]^46 RGG9C210265046U 1
ug/L EPA 8151A 03/25/19 13:50Pentachlorophenol [87-86-5]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 13:50Picloram [1918-02-1]^0.23 RGG9C210260.500.23 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4-DCAA 37-134107 %RGGEPA 8151A 03/25/19 13:509C210262.1 2.00 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 365.4 03/27/19 15:08Phosphorus [7723-14-0]^0.020 kgonz9C250150.0300.66 1
Page 16 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 02:281,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:281,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 02:281,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 02:281,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:281,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 02:281,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:281,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:281,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 02:281,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:281,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:281,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 02:281,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 02:281,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 02:281,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 02:281,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:281,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 02:281,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 02:281,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:281,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:281,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 02:282,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 02:282-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 02:282-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 02:282-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 02:282-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 02:284-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 02:284-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 02:284-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 02:28Acetone [67-64-1]^10 MRK9C150222010U O-011
ug/L EPA 8260D 03/16/19 02:28Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:28Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:28Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 02:28Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 02:28Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:28Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 02:28Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:28Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 02:28Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 02:28cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:28cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 02:28Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 02:28Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 02:28Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 17 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 02:28Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 02:28Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:28m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:28Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:28Naphthalene [91-20-3]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 02:28n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 02:28n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 02:28o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 02:28sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 02:28Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 02:28tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:28Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:28trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:28trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:28Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:28Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 02:28Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 02:28Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260D 03/16/19 02:289C150225150.0 1
Dibromofluoromethane 67-129101 %MRKEPA 8260D 03/16/19 02:289C150225150.0 1
Toluene-d8 59-134104 %MRKEPA 8260D 03/16/19 02:289C150225250.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 18:321,2,4-Trichlorobenzene [120-82-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:321,2-Dichlorobenzene [95-50-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:321,3-Dichlorobenzene [541-73-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:321,4-Dichlorobenzene [106-46-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:321-Methylnaphthalene [90-12-0]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 18:322,4,5-Trichlorophenol [95-95-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:322,4,6-Trichlorophenol [88-06-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:322,4-Dichlorophenol [120-83-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:322,4-Dimethylphenol [105-67-9]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 18:322,4-Dinitrophenol [51-28-5]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:322,4-Dinitrotoluene [121-14-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:322,6-Dinitrotoluene [606-20-2]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:322-Chloronaphthalene [91-58-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:322-Chlorophenol [95-57-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 18:322-Methyl-4,6-dinitrophenol [534-52-1]^3.3 DFM9C18010103.3 U 1
ug/L EPA 8270E 03/19/19 18:322-Methylnaphthalene [91-57-6]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:322-Methylphenol [95-48-7]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 18:322-Nitroaniline [88-74-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:322-Nitrophenol [88-75-5]^1.1 DFM9C18010101.1 U 1
Page 18 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 18:323 & 4-Methylphenol [108-39-4/106-44-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 18:323,3’-Dichlorobenzidine [91-94-1]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 18:323-Nitroaniline [99-09-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:324-Bromophenyl-phenylether [101-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:324-Chloro-3-methylphenol [59-50-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:324-Chloroaniline [106-47-8]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 18:324-Chlorophenyl-phenylether [7005-72-3]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:324-Nitroaniline [100-01-6]^3.2 DFM9C18010103.2 U 1
ug/L EPA 8270E 03/19/19 18:324-Nitrophenol [100-02-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:32Acenaphthene [83-32-9]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 18:32Acenaphthylene [208-96-8]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:32Anthracene [120-12-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Benzidine [92-87-5]^1.6 DFM9C18010101.6 U QV-011
ug/L EPA 8270E 03/19/19 18:32Benzo(a)anthracene [56-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Benzo(a)pyrene [50-32-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 18:32Benzo(b)fluoranthene [205-99-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:32Benzo(g,h,i)perylene [191-24-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Benzo(k)fluoranthene [207-08-9]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Benzoic acid [65-85-0]^1.0 DFM9C18010501.0 U QV-021
ug/L EPA 8270E 03/19/19 18:32Benzyl alcohol [100-51-6]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Bis(2-chloroethoxy)methane [111-91-1]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Bis(2-chloroethyl)ether [111-44-4]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:32Bis(2-chloroisopropyl)ether [108-60-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32Bis(2-ethylhexyl)phthalate [117-81-7]^1.9 DFM9C180105.01.9 U 1
ug/L EPA 8270E 03/19/19 18:32Butylbenzylphthalate [85-68-7]^3.8 DFM9C18010103.8 U 1
ug/L EPA 8270E 03/19/19 18:32Chrysene [218-01-9]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 18:32Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 18:32Dibenzofuran [132-64-9]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:32Diethylphthalate [84-66-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 18:32Dimethylphthalate [131-11-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32Di-n-butylphthalate [84-74-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:32Di-n-octylphthalate [117-84-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 18:32Fluoranthene [206-44-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 18:32Fluorene [86-73-7]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32Hexachlorobenzene [118-74-1]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 18:32Hexachlorobutadiene [87-68-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:32Hexachlorocyclopentadiene [77-47-4]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 18:32Hexachloroethane [67-72-1]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 18:32Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 18:32Isophorone [78-59-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32Naphthalene [91-20-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 18:32Nitrobenzene [98-95-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32N-Nitrosodimethylamine [62-75-9]^1.9 DFM9C18010101.9 U 1
ug/L EPA 8270E 03/19/19 18:32N-Nitroso-di-n-propylamine [621-64-7]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 18:32N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4]^
2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 18:32Pentachlorophenol [87-86-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 18:32Phenanthrene [85-01-8]^2.6 DFM9C18010102.6 U 1
Page 19 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 18:32Phenol [108-95-2]^1.7 DFM9C18010101.7 U 1
ug/L EPA 8270E 03/19/19 18:32Pyrene [129-00-0]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 18:32Pyridine [110-86-1]^2.2 DFM9C18010102.2 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17972 %DFMEPA 8270E 03/19/19 18:329C1801072100 1
2-Fluorobiphenyl 10-14980 %DFMEPA 8270E 03/19/19 18:329C180104050.0 1
2-Fluorophenol 10-11048 %DFMEPA 8270E 03/19/19 18:329C1801048100 1
Nitrobenzene-d5 10-14975 %DFMEPA 8270E 03/19/19 18:329C180103850.0 1
Phenol-d5 10-8846 %DFMEPA 8270E 03/19/19 18:329C1801046100 1
Terphenyl-d14 10-188100 %DFMEPA 8270E 03/19/19 18:329C180105050.0 1
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8081B 03/21/19 18:234,4’-DDD [72-54-8]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:234,4’-DDE [72-55-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:234,4’-DDT [50-29-3]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:23Aldrin [309-00-2]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:23alpha-BHC [319-84-6]^0.036 LSK9C180350.0500.036 U 1
ug/L EPA 8081B 03/21/19 18:23beta-BHC [319-85-7]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:23Chlordane (tech) [12789-03-6]^0.37 LSK9C180350.500.37 U 1
ug/L EPA 8081B 03/21/19 18:23Chlordane-alpha [5103-71-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:23Chlordane-gamma [5103-74-2]^0.042 LSK9C180350.0500.042 U 1
ug/L EPA 8081B 03/21/19 18:23delta-BHC [319-86-8]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:23Dieldrin [60-57-1]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:23Endosulfan I [959-98-8]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:23Endosulfan II [33213-65-9]^0.038 LSK9C180350.0500.038 U 1
ug/L EPA 8081B 03/21/19 18:23Endosulfan sulfate [1031-07-8]^0.032 LSK9C180350.0500.032 U 1
ug/L EPA 8081B 03/21/19 18:23Endrin [72-20-8]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:23Endrin aldehyde [7421-93-4]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:23Endrin ketone [53494-70-5]^0.039 LSK9C180350.0500.039 U 1
ug/L EPA 8081B 03/21/19 18:23gamma-BHC [58-89-9]^0.034 LSK9C180350.0500.034 U 1
ug/L EPA 8081B 03/21/19 18:23Heptachlor [76-44-8]^0.047 LSK9C180350.0500.047 U 1
ug/L EPA 8081B 03/21/19 18:23Heptachlor epoxide [1024-57-3]^0.037 LSK9C180350.0500.037 U 1
ug/L EPA 8081B 03/21/19 18:23Isodrin [465-73-6]^0.031 LSK9C180350.0500.031 U 1
ug/L EPA 8081B 03/21/19 18:23Methoxychlor [72-43-5]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:23Mirex [2385-85-5]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:23Toxaphene [8001-35-2]^0.28 LSK9C180351.00.28 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,5,6-TCMX 10-13984 %LSKEPA 8081B 03/21/19 18:239C180350.84 1.00 1
Decachlorobiphenyl 10-122111 %LSKEPA 8081B 03/21/19 18:239C180351.1 1.00 1
Page 20 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 353.2 03/25/19 19:06Nitrate as N [14797-55-8]0.20 MKS[CALC]0.506.4 D 5
mg/L EPA 353.2 03/25/19 19:06Nitrate/Nitrite as N^0.20 MKS9C250370.506.9 D 5
mg/L EPA 353.2 03/15/19 12:18Nitrite as N [14797-65-0]^0.017 MKS9C150070.100.54 1
mg/L EPA 300.0 03/25/19 22:10Sulfate as SO4 [14808-79-8]^2.9 MKS9C250315.081 1
Semivolatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 16:20Azinphos-methyl [86-50-0]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:20Bolstar [35400-43-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:20Chlorpyrifos [2921-88-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:20Coumaphos [56-72-4]0.29 jfi9C210010.500.29 U 1
ug/L EPA 8270E 03/22/19 16:20Demeton [8065-48-3]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:20Diazinon [333-41-5]0.23 jfi9C210010.500.23 U 1
ug/L EPA 8270E 03/22/19 16:20Dichlorofenthion [97-17-6]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:20Dichlorvos [62-73-7]0.35 jfi9C210010.500.35 U 1
ug/L EPA 8270E 03/22/19 16:20Dimethoate [60-51-5]0.27 jfi9C210010.500.27 U 1
ug/L EPA 8270E 03/22/19 16:20Disulfoton [298-04-4]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:20EPN [2104-64-5]0.45 jfi9C210010.500.45 U 1
ug/L EPA 8270E 03/22/19 16:20Ethion [563-12-2]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:20Ethoprop [13194-48-4]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:20Ethyl Parathion [56-38-2]0.31 jfi9C210010.500.31 U 1
ug/L EPA 8270E 03/22/19 16:20Fensulfothion [115-90-2]0.32 jfi9C210010.500.32 U 1
ug/L EPA 8270E 03/22/19 16:20Fenthion [55-38-9]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:20Malathion [121-75-5]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:20Merphos [150-50-5]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:20Methyl parathion [298-00-0]0.33 jfi9C210010.500.33 U 1
ug/L EPA 8270E 03/22/19 16:20Mevinphos [7786-34-7]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:20Monocrotophos [6923-22-4]0.054 jfi9C210010.500.054 U 1
ug/L EPA 8270E 03/22/19 16:20Naled [300-76-5]0.15 jfi9C210011.00.15 U 1
ug/L EPA 8270E 03/22/19 16:20Phorate [298-02-2]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:20Ronnel [299-84-3]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:20Stirophos (Tetrachlorvinphos) [22248-79-9]0.38 jfi9C210010.500.38 U 1
ug/L EPA 8270E 03/22/19 16:20Sulfotep [3689-24-5]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:20TEPP [107-49-3]0.20 jfi9C210011.00.20 U 1
ug/L EPA 8270E 03/22/19 16:20Tokuthion (Prothiofos) [34643-46-4]0.24 jfi9C210010.500.24 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Tributyl Phosphate 50-150107 %jfiEPA 8270E 03/22/19 16:209C210014.3 4.02 1
Triphenyl phosphate 50-15093 %jfiEPA 8270E 03/22/19 16:209C210013.8 4.02 1
Page 21 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-3Description:Lab Sample ID:CC03837-03 03/15/19 09:32Received:
CC03837Work Order:03/14/19 12:50Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8151A 03/25/19 14:152,4,5-T [93-76-5]^0.28 RGG9C210260.500.28 U 1
ug/L EPA 8151A 03/25/19 14:152,4,5-TP (Silvex) [93-72-1]^0.44 RGG9C210260.500.44 U 1
ug/L EPA 8151A 03/25/19 14:152,4-D [94-75-7]^0.27 RGG9C210260.500.27 U 1
ug/L EPA 8151A 03/25/19 14:152,4-DB [94-82-6]^0.35 RGG9C210260.500.35 U 1
ug/L EPA 8151A 03/25/19 14:153,5-DCBA [51-365-5]^0.36 RGG9C210260.500.36 U 1
ug/L EPA 8151A 03/25/19 14:154-Nitrophenol [100-02-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 14:15Acifluorfen [50594-66-6]^0.45 RGG9C210260.500.45 U 1
ug/L EPA 8151A 03/25/19 14:15Bentazon [25057-89-0]^0.22 RGG9C210260.500.22 U 1
ug/L EPA 8151A 03/25/19 14:15Chloramben [133-90-4]^0.43 RGG9C210260.500.43 U 1
ug/L EPA 8151A 03/25/19 14:15Dacthal [1861-32-1]^0.23 RGG9C210260.500.23 U 1
ug/L EPA 8151A 03/25/19 14:15Dalapon [75-99-0]^0.49 RGG9C210260.500.49 U 1
ug/L EPA 8151A 03/25/19 14:15Dicamba [1918-00-9]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 14:15Dichlorprop [120-36-5]^0.31 RGG9C210260.500.31 U 1
ug/L EPA 8151A 03/25/19 14:15Dinoseb [88-85-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 14:15MCPA [94-74-6]^34 RGG9C210265034U QV-011
ug/L EPA 8151A 03/25/19 14:15MCPP [7085-19-0]^46 RGG9C210265046U 1
ug/L EPA 8151A 03/25/19 14:15Pentachlorophenol [87-86-5]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 14:15Picloram [1918-02-1]^0.23 RGG9C210260.500.23 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4-DCAA 37-134110 %RGGEPA 8151A 03/25/19 14:159C210262.2 2.00 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 365.4 03/27/19 15:09Phosphorus [7723-14-0]^0.020 kgonz9C250150.0300.48 1
Page 22 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 02:591,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:591,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 02:591,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 02:591,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:591,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 02:591,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:591,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:591,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 02:591,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:591,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:591,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 02:591,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 02:591,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 02:591,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 02:591,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:591,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.07.8 1
ug/L EPA 8260D 03/16/19 02:591,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 02:591,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:591,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:591,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 02:592,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 02:592-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 02:592-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 02:592-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 02:592-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 02:594-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 02:594-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 02:594-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 02:59Acetone [67-64-1]^10 MRK9C150222010U O-011
ug/L EPA 8260D 03/16/19 02:59Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:59Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:59Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 02:59Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 02:59Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:59Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 02:59Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:59Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 02:59Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 02:59cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:59cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 02:59Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 02:59Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 02:59Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 23 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 02:59Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 02:59Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:59m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 02:59Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 02:59Naphthalene [91-20-3]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 02:59n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 02:59n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 02:59o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 02:59sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 02:59Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 02:59tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 02:59Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 02:59trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 02:59trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:59Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 02:59Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 02:59Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 02:59Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136105 %MRKEPA 8260D 03/16/19 02:599C150225350.0 1
Dibromofluoromethane 67-12999 %MRKEPA 8260D 03/16/19 02:599C150224950.0 1
Toluene-d8 59-134103 %MRKEPA 8260D 03/16/19 02:599C150225250.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:021,2,4-Trichlorobenzene [120-82-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:021,2-Dichlorobenzene [95-50-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:021,3-Dichlorobenzene [541-73-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:021,4-Dichlorobenzene [106-46-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:021-Methylnaphthalene [90-12-0]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:022,4,5-Trichlorophenol [95-95-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:022,4,6-Trichlorophenol [88-06-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:022,4-Dichlorophenol [120-83-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:022,4-Dimethylphenol [105-67-9]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:022,4-Dinitrophenol [51-28-5]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:022,4-Dinitrotoluene [121-14-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:022,6-Dinitrotoluene [606-20-2]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:022-Chloronaphthalene [91-58-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:022-Chlorophenol [95-57-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:022-Methyl-4,6-dinitrophenol [534-52-1]^3.3 DFM9C18010103.3 U 1
ug/L EPA 8270E 03/19/19 19:022-Methylnaphthalene [91-57-6]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:022-Methylphenol [95-48-7]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 19:022-Nitroaniline [88-74-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:022-Nitrophenol [88-75-5]^1.1 DFM9C18010101.1 U 1
Page 24 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:023 & 4-Methylphenol [108-39-4/106-44-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 19:023,3’-Dichlorobenzidine [91-94-1]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 19:023-Nitroaniline [99-09-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:024-Bromophenyl-phenylether [101-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:024-Chloro-3-methylphenol [59-50-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:024-Chloroaniline [106-47-8]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 19:024-Chlorophenyl-phenylether [7005-72-3]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:024-Nitroaniline [100-01-6]^3.2 DFM9C18010103.2 U 1
ug/L EPA 8270E 03/19/19 19:024-Nitrophenol [100-02-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:02Acenaphthene [83-32-9]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:02Acenaphthylene [208-96-8]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:02Anthracene [120-12-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Benzidine [92-87-5]^1.6 DFM9C18010101.6 U QV-011
ug/L EPA 8270E 03/19/19 19:02Benzo(a)anthracene [56-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Benzo(a)pyrene [50-32-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:02Benzo(b)fluoranthene [205-99-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:02Benzo(g,h,i)perylene [191-24-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Benzo(k)fluoranthene [207-08-9]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Benzoic acid [65-85-0]^1.0 DFM9C18010501.0 U QV-021
ug/L EPA 8270E 03/19/19 19:02Benzyl alcohol [100-51-6]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Bis(2-chloroethoxy)methane [111-91-1]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Bis(2-chloroethyl)ether [111-44-4]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:02Bis(2-chloroisopropyl)ether [108-60-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02Bis(2-ethylhexyl)phthalate [117-81-7]^1.9 DFM9C180105.01.9 U 1
ug/L EPA 8270E 03/19/19 19:02Butylbenzylphthalate [85-68-7]^3.8 DFM9C18010103.8 U 1
ug/L EPA 8270E 03/19/19 19:02Chrysene [218-01-9]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:02Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:02Dibenzofuran [132-64-9]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:02Diethylphthalate [84-66-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:02Dimethylphthalate [131-11-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02Di-n-butylphthalate [84-74-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:02Di-n-octylphthalate [117-84-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 19:02Fluoranthene [206-44-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 19:02Fluorene [86-73-7]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02Hexachlorobenzene [118-74-1]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:02Hexachlorobutadiene [87-68-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:02Hexachlorocyclopentadiene [77-47-4]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:02Hexachloroethane [67-72-1]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:02Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:02Isophorone [78-59-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02Naphthalene [91-20-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:02Nitrobenzene [98-95-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02N-Nitrosodimethylamine [62-75-9]^1.9 DFM9C18010101.9 U 1
ug/L EPA 8270E 03/19/19 19:02N-Nitroso-di-n-propylamine [621-64-7]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:02N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4]^
2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:02Pentachlorophenol [87-86-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 19:02Phenanthrene [85-01-8]^2.6 DFM9C18010102.6 U 1
Page 25 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:02Phenol [108-95-2]^1.7 DFM9C18010101.7 U 1
ug/L EPA 8270E 03/19/19 19:02Pyrene [129-00-0]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 19:02Pyridine [110-86-1]^2.2 DFM9C18010102.2 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17982 %DFMEPA 8270E 03/19/19 19:029C1801082100 1
2-Fluorobiphenyl 10-14979 %DFMEPA 8270E 03/19/19 19:029C180104050.0 1
2-Fluorophenol 10-11055 %DFMEPA 8270E 03/19/19 19:029C1801055100 1
Nitrobenzene-d5 10-14983 %DFMEPA 8270E 03/19/19 19:029C180104250.0 1
Phenol-d5 10-8841 %DFMEPA 8270E 03/19/19 19:029C1801041100 1
Terphenyl-d14 10-188102 %DFMEPA 8270E 03/19/19 19:029C180105150.0 1
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8081B 03/21/19 18:404,4’-DDD [72-54-8]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:404,4’-DDE [72-55-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:404,4’-DDT [50-29-3]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:40Aldrin [309-00-2]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:40alpha-BHC [319-84-6]^0.036 LSK9C180350.0500.036 U 1
ug/L EPA 8081B 03/21/19 18:40beta-BHC [319-85-7]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:40Chlordane (tech) [12789-03-6]^0.37 LSK9C180350.500.37 U 1
ug/L EPA 8081B 03/21/19 18:40Chlordane-alpha [5103-71-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:40Chlordane-gamma [5103-74-2]^0.042 LSK9C180350.0500.042 U 1
ug/L EPA 8081B 03/21/19 18:40delta-BHC [319-86-8]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:40Dieldrin [60-57-1]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:40Endosulfan I [959-98-8]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:40Endosulfan II [33213-65-9]^0.038 LSK9C180350.0500.038 U 1
ug/L EPA 8081B 03/21/19 18:40Endosulfan sulfate [1031-07-8]^0.032 LSK9C180350.0500.032 U 1
ug/L EPA 8081B 03/21/19 18:40Endrin [72-20-8]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:40Endrin aldehyde [7421-93-4]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:40Endrin ketone [53494-70-5]^0.039 LSK9C180350.0500.039 U 1
ug/L EPA 8081B 03/21/19 18:40gamma-BHC [58-89-9]^0.034 LSK9C180350.0500.034 U 1
ug/L EPA 8081B 03/21/19 18:40Heptachlor [76-44-8]^0.047 LSK9C180350.0500.047 U 1
ug/L EPA 8081B 03/21/19 18:40Heptachlor epoxide [1024-57-3]^0.037 LSK9C180350.0500.037 U 1
ug/L EPA 8081B 03/21/19 18:40Isodrin [465-73-6]^0.031 LSK9C180350.0500.031 U 1
ug/L EPA 8081B 03/21/19 18:40Methoxychlor [72-43-5]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:40Mirex [2385-85-5]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:40Toxaphene [8001-35-2]^0.28 LSK9C180351.00.28 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,5,6-TCMX 10-139106 %LSKEPA 8081B 03/21/19 18:409C180351.1 1.00 1
Decachlorobiphenyl 10-122109 %LSKEPA 8081B 03/21/19 18:409C180351.1 1.00 1
Page 26 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 353.2 03/25/19 19:07Nitrate as N [14797-55-8]0.20 MKS[CALC]0.500.46 JD 5
mg/L EPA 353.2 03/25/19 19:07Nitrate/Nitrite as N^0.20 MKS9C250370.500.66 D 5
mg/L EPA 353.2 03/15/19 12:19Nitrite as N [14797-65-0]^0.017 MKS9C150070.100.20 1
mg/L EPA 300.0 03/26/19 11:24Sulfate as SO4 [14808-79-8]^5.8 MKS9C250311094D 2
Semivolatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 16:53Azinphos-methyl [86-50-0]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:53Bolstar [35400-43-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:53Chlorpyrifos [2921-88-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:53Coumaphos [56-72-4]0.29 jfi9C210010.500.29 U 1
ug/L EPA 8270E 03/22/19 16:53Demeton [8065-48-3]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:53Diazinon [333-41-5]0.23 jfi9C210010.500.23 U 1
ug/L EPA 8270E 03/22/19 16:53Dichlorofenthion [97-17-6]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 16:53Dichlorvos [62-73-7]0.35 jfi9C210010.500.35 U 1
ug/L EPA 8270E 03/22/19 16:53Dimethoate [60-51-5]0.27 jfi9C210010.500.27 U 1
ug/L EPA 8270E 03/22/19 16:53Disulfoton [298-04-4]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:53EPN [2104-64-5]0.45 jfi9C210010.500.45 U 1
ug/L EPA 8270E 03/22/19 16:53Ethion [563-12-2]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:53Ethoprop [13194-48-4]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:53Ethyl Parathion [56-38-2]0.31 jfi9C210010.500.31 U 1
ug/L EPA 8270E 03/22/19 16:53Fensulfothion [115-90-2]0.32 jfi9C210010.500.32 U 1
ug/L EPA 8270E 03/22/19 16:53Fenthion [55-38-9]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:53Malathion [121-75-5]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:53Merphos [150-50-5]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 16:53Methyl parathion [298-00-0]0.33 jfi9C210010.500.33 U 1
ug/L EPA 8270E 03/22/19 16:53Mevinphos [7786-34-7]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 16:53Monocrotophos [6923-22-4]0.054 jfi9C210010.500.054 U 1
ug/L EPA 8270E 03/22/19 16:53Naled [300-76-5]0.15 jfi9C210011.00.15 U 1
ug/L EPA 8270E 03/22/19 16:53Phorate [298-02-2]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:53Ronnel [299-84-3]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:53Stirophos (Tetrachlorvinphos) [22248-79-9]0.38 jfi9C210010.500.38 U 1
ug/L EPA 8270E 03/22/19 16:53Sulfotep [3689-24-5]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 16:53TEPP [107-49-3]0.20 jfi9C210011.00.20 U 1
ug/L EPA 8270E 03/22/19 16:53Tokuthion (Prothiofos) [34643-46-4]0.24 jfi9C210010.500.24 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Tributyl Phosphate 50-150100 %jfiEPA 8270E 03/22/19 16:539C210014.0 4.02 1
Triphenyl phosphate 50-15086 %jfiEPA 8270E 03/22/19 16:539C210013.5 4.02 1
Page 27 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-4Description:Lab Sample ID:CC03837-04 03/15/19 09:32Received:
CC03837Work Order:03/14/19 15:25Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8151A 03/25/19 14:412,4,5-T [93-76-5]^0.28 RGG9C210260.500.28 U 1
ug/L EPA 8151A 03/25/19 14:412,4,5-TP (Silvex) [93-72-1]^0.44 RGG9C210260.500.44 U 1
ug/L EPA 8151A 03/25/19 14:412,4-D [94-75-7]^0.27 RGG9C210260.500.27 U 1
ug/L EPA 8151A 03/25/19 14:412,4-DB [94-82-6]^0.35 RGG9C210260.500.35 U 1
ug/L EPA 8151A 03/25/19 14:413,5-DCBA [51-365-5]^0.36 RGG9C210260.500.36 U 1
ug/L EPA 8151A 03/25/19 14:414-Nitrophenol [100-02-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 14:41Acifluorfen [50594-66-6]^0.45 RGG9C210260.500.45 U 1
ug/L EPA 8151A 03/25/19 14:41Bentazon [25057-89-0]^0.22 RGG9C210260.500.22 U 1
ug/L EPA 8151A 03/25/19 14:41Chloramben [133-90-4]^0.43 RGG9C210260.500.43 U 1
ug/L EPA 8151A 03/25/19 14:41Dacthal [1861-32-1]^0.23 RGG9C210260.500.23 U 1
ug/L EPA 8151A 03/25/19 14:41Dalapon [75-99-0]^0.49 RGG9C210260.500.49 U 1
ug/L EPA 8151A 03/25/19 14:41Dicamba [1918-00-9]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 14:41Dichlorprop [120-36-5]^0.31 RGG9C210260.500.31 U 1
ug/L EPA 8151A 03/25/19 14:41Dinoseb [88-85-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 14:41MCPA [94-74-6]^34 RGG9C210265034U QV-011
ug/L EPA 8151A 03/25/19 14:41MCPP [7085-19-0]^46 RGG9C210265046U 1
ug/L EPA 8151A 03/25/19 14:41Pentachlorophenol [87-86-5]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 14:41Picloram [1918-02-1]^0.23 RGG9C210260.500.23 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4-DCAA 37-134105 %RGGEPA 8151A 03/25/19 14:419C210262.1 2.00 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 365.4 03/27/19 15:10Phosphorus [7723-14-0]^0.020 kgonz9C250150.0304.1 1
Page 28 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 03:311,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:311,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 03:311,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 03:311,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 03:311,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 03:311,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 03:311,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:311,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 03:311,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 03:311,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 03:311,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 03:311,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 03:311,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 03:311,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 03:311,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 03:311,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 03:311,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 03:311,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:311,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 03:311,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 03:312,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 03:312-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 03:312-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 03:312-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 03:312-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 03:314-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 03:314-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 03:314-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 03:31Acetone [67-64-1]^10 MRK9C150222010U O-011
ug/L EPA 8260D 03/16/19 03:31Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:31Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 03:31Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 03:31Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 03:31Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 03:31Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 03:31Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 03:31Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 03:31Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 03:31cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:31cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 03:31Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 03:31Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 03:31Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 29 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 03:31Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 03:31Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 03:31m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 03:31Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 03:31Naphthalene [91-20-3]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 03:31n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 03:31n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 03:31o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 03:31sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 03:31Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 03:31tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 03:31Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 03:31trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 03:31trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:31Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 03:31Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 03:31Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 03:31Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260D 03/16/19 03:319C150225050.0 1
Dibromofluoromethane 67-129102 %MRKEPA 8260D 03/16/19 03:319C150225150.0 1
Toluene-d8 59-134102 %MRKEPA 8260D 03/16/19 03:319C150225150.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:321,2,4-Trichlorobenzene [120-82-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:321,2-Dichlorobenzene [95-50-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:321,3-Dichlorobenzene [541-73-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:321,4-Dichlorobenzene [106-46-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:321-Methylnaphthalene [90-12-0]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:322,4,5-Trichlorophenol [95-95-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:322,4,6-Trichlorophenol [88-06-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:322,4-Dichlorophenol [120-83-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:322,4-Dimethylphenol [105-67-9]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:322,4-Dinitrophenol [51-28-5]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:322,4-Dinitrotoluene [121-14-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:322,6-Dinitrotoluene [606-20-2]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:322-Chloronaphthalene [91-58-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:322-Chlorophenol [95-57-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:322-Methyl-4,6-dinitrophenol [534-52-1]^3.3 DFM9C18010103.3 U 1
ug/L EPA 8270E 03/19/19 19:322-Methylnaphthalene [91-57-6]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:322-Methylphenol [95-48-7]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 19:322-Nitroaniline [88-74-4]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:322-Nitrophenol [88-75-5]^1.1 DFM9C18010101.1 U 1
Page 30 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:323 & 4-Methylphenol [108-39-4/106-44-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 19:323,3’-Dichlorobenzidine [91-94-1]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 19:323-Nitroaniline [99-09-2]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:324-Bromophenyl-phenylether [101-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:324-Chloro-3-methylphenol [59-50-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:324-Chloroaniline [106-47-8]^2.0 DFM9C18010102.0 U 1
ug/L EPA 8270E 03/19/19 19:324-Chlorophenyl-phenylether [7005-72-3]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:324-Nitroaniline [100-01-6]^3.2 DFM9C18010103.2 U 1
ug/L EPA 8270E 03/19/19 19:324-Nitrophenol [100-02-7]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:32Acenaphthene [83-32-9]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:32Acenaphthylene [208-96-8]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:32Anthracene [120-12-7]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Benzidine [92-87-5]^1.6 DFM9C18010101.6 U QV-011
ug/L EPA 8270E 03/19/19 19:32Benzo(a)anthracene [56-55-3]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Benzo(a)pyrene [50-32-8]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:32Benzo(b)fluoranthene [205-99-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:32Benzo(g,h,i)perylene [191-24-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Benzo(k)fluoranthene [207-08-9]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Benzoic acid [65-85-0]^1.0 DFM9C18010501.0 U QV-021
ug/L EPA 8270E 03/19/19 19:32Benzyl alcohol [100-51-6]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Bis(2-chloroethoxy)methane [111-91-1]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Bis(2-chloroethyl)ether [111-44-4]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:32Bis(2-chloroisopropyl)ether [108-60-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32Bis(2-ethylhexyl)phthalate [117-81-7]^1.9 DFM9C180105.01.9 U 1
ug/L EPA 8270E 03/19/19 19:32Butylbenzylphthalate [85-68-7]^3.8 DFM9C18010103.8 U 1
ug/L EPA 8270E 03/19/19 19:32Chrysene [218-01-9]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:32Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:32Dibenzofuran [132-64-9]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:32Diethylphthalate [84-66-2]^2.4 DFM9C18010102.4 U 1
ug/L EPA 8270E 03/19/19 19:32Dimethylphthalate [131-11-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32Di-n-butylphthalate [84-74-2]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:32Di-n-octylphthalate [117-84-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 19:32Fluoranthene [206-44-0]^3.1 DFM9C18010103.1 U 1
ug/L EPA 8270E 03/19/19 19:32Fluorene [86-73-7]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32Hexachlorobenzene [118-74-1]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:32Hexachlorobutadiene [87-68-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:32Hexachlorocyclopentadiene [77-47-4]^2.7 DFM9C18010102.7 U 1
ug/L EPA 8270E 03/19/19 19:32Hexachloroethane [67-72-1]^2.6 DFM9C18010102.6 U 1
ug/L EPA 8270E 03/19/19 19:32Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM9C18010102.2 U 1
ug/L EPA 8270E 03/19/19 19:32Isophorone [78-59-1]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32Naphthalene [91-20-3]^2.8 DFM9C18010102.8 U 1
ug/L EPA 8270E 03/19/19 19:32Nitrobenzene [98-95-3]^2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32N-Nitrosodimethylamine [62-75-9]^1.9 DFM9C18010101.9 U 1
ug/L EPA 8270E 03/19/19 19:32N-Nitroso-di-n-propylamine [621-64-7]^2.3 DFM9C18010102.3 U 1
ug/L EPA 8270E 03/19/19 19:32N-nitrosodiphenylamine/Diphenylamine
[86-30-6/122-39-4]^
2.5 DFM9C18010102.5 U 1
ug/L EPA 8270E 03/19/19 19:32Pentachlorophenol [87-86-5]^2.1 DFM9C18010102.1 U 1
ug/L EPA 8270E 03/19/19 19:32Phenanthrene [85-01-8]^2.6 DFM9C18010102.6 U 1
Page 31 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/19/19 19:32Phenol [108-95-2]^1.7 DFM9C18010101.7 U 1
ug/L EPA 8270E 03/19/19 19:32Pyrene [129-00-0]^3.5 DFM9C18010103.5 U 1
ug/L EPA 8270E 03/19/19 19:32Pyridine [110-86-1]^2.2 DFM9C18010102.2 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,6-Tribromophenol 10-17984 %DFMEPA 8270E 03/19/19 19:329C1801084100 1
2-Fluorobiphenyl 10-14982 %DFMEPA 8270E 03/19/19 19:329C180104150.0 1
2-Fluorophenol 10-11051 %DFMEPA 8270E 03/19/19 19:329C1801051100 1
Nitrobenzene-d5 10-14974 %DFMEPA 8270E 03/19/19 19:329C180103750.0 1
Phenol-d5 10-8843 %DFMEPA 8270E 03/19/19 19:329C1801043100 1
Terphenyl-d14 10-18896 %DFMEPA 8270E 03/19/19 19:329C180104850.0 1
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8081B 03/21/19 18:574,4’-DDD [72-54-8]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:574,4’-DDE [72-55-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:574,4’-DDT [50-29-3]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:57Aldrin [309-00-2]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:57alpha-BHC [319-84-6]^0.036 LSK9C180350.0500.036 U 1
ug/L EPA 8081B 03/21/19 18:57beta-BHC [319-85-7]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:57Chlordane (tech) [12789-03-6]^0.37 LSK9C180350.500.37 U 1
ug/L EPA 8081B 03/21/19 18:57Chlordane-alpha [5103-71-9]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:57Chlordane-gamma [5103-74-2]^0.042 LSK9C180350.0500.042 U 1
ug/L EPA 8081B 03/21/19 18:57delta-BHC [319-86-8]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:57Dieldrin [60-57-1]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:57Endosulfan I [959-98-8]^0.045 LSK9C180350.0500.045 U 1
ug/L EPA 8081B 03/21/19 18:57Endosulfan II [33213-65-9]^0.038 LSK9C180350.0500.038 U 1
ug/L EPA 8081B 03/21/19 18:57Endosulfan sulfate [1031-07-8]^0.032 LSK9C180350.0500.032 U 1
ug/L EPA 8081B 03/21/19 18:57Endrin [72-20-8]^0.041 LSK9C180350.0500.041 U 1
ug/L EPA 8081B 03/21/19 18:57Endrin aldehyde [7421-93-4]^0.049 LSK9C180350.0500.049 U 1
ug/L EPA 8081B 03/21/19 18:57Endrin ketone [53494-70-5]^0.039 LSK9C180350.0500.039 U 1
ug/L EPA 8081B 03/21/19 18:57gamma-BHC [58-89-9]^0.034 LSK9C180350.0500.034 U 1
ug/L EPA 8081B 03/21/19 18:57Heptachlor [76-44-8]^0.047 LSK9C180350.0500.047 U 1
ug/L EPA 8081B 03/21/19 18:57Heptachlor epoxide [1024-57-3]^0.037 LSK9C180350.0500.037 U 1
ug/L EPA 8081B 03/21/19 18:57Isodrin [465-73-6]^0.031 LSK9C180350.0500.031 U 1
ug/L EPA 8081B 03/21/19 18:57Methoxychlor [72-43-5]^0.048 LSK9C180350.0500.048 U 1
ug/L EPA 8081B 03/21/19 18:57Mirex [2385-85-5]^0.044 LSK9C180350.0500.044 U 1
ug/L EPA 8081B 03/21/19 18:57Toxaphene [8001-35-2]^0.28 LSK9C180351.00.28 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4,5,6-TCMX 10-139106 %LSKEPA 8081B 03/21/19 18:579C180351.1 1.00 1
Decachlorobiphenyl 10-122101 %LSKEPA 8081B 03/21/19 18:579C180351.0 1.00 1
Page 32 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 353.2 03/28/19 17:39Nitrate as N [14797-55-8]0.82 MKS[CALC]2.033D 20
mg/L EPA 353.2 03/28/19 17:39Nitrate/Nitrite as N^0.82 MKS9C280262.033D 20
mg/L EPA 353.2 03/15/19 12:20Nitrite as N [14797-65-0]^0.017 MKS9C150070.100.057 J 1
mg/L EPA 300.0 03/26/19 11:53Sulfate as SO4 [14808-79-8]^14 MKS9C2503125360D 5
Semivolatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8270E 03/22/19 17:26Azinphos-methyl [86-50-0]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 17:26Bolstar [35400-43-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 17:26Chlorpyrifos [2921-88-2]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 17:26Coumaphos [56-72-4]0.29 jfi9C210010.500.29 U 1
ug/L EPA 8270E 03/22/19 17:26Demeton [8065-48-3]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 17:26Diazinon [333-41-5]0.23 jfi9C210010.500.23 U 1
ug/L EPA 8270E 03/22/19 17:26Dichlorofenthion [97-17-6]0.25 jfi9C210010.500.25 U 1
ug/L EPA 8270E 03/22/19 17:26Dichlorvos [62-73-7]0.35 jfi9C210010.500.35 U 1
ug/L EPA 8270E 03/22/19 17:26Dimethoate [60-51-5]0.27 jfi9C210010.500.27 U 1
ug/L EPA 8270E 03/22/19 17:26Disulfoton [298-04-4]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 17:26EPN [2104-64-5]0.45 jfi9C210010.500.45 U 1
ug/L EPA 8270E 03/22/19 17:26Ethion [563-12-2]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 17:26Ethoprop [13194-48-4]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 17:26Ethyl Parathion [56-38-2]0.31 jfi9C210010.500.31 U 1
ug/L EPA 8270E 03/22/19 17:26Fensulfothion [115-90-2]0.32 jfi9C210010.500.32 U 1
ug/L EPA 8270E 03/22/19 17:26Fenthion [55-38-9]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 17:26Malathion [121-75-5]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 17:26Merphos [150-50-5]0.24 jfi9C210010.500.24 U 1
ug/L EPA 8270E 03/22/19 17:26Methyl parathion [298-00-0]0.33 jfi9C210010.500.33 U 1
ug/L EPA 8270E 03/22/19 17:26Mevinphos [7786-34-7]0.28 jfi9C210010.500.28 U 1
ug/L EPA 8270E 03/22/19 17:26Monocrotophos [6923-22-4]0.054 jfi9C210010.500.054 U 1
ug/L EPA 8270E 03/22/19 17:26Naled [300-76-5]0.15 jfi9C210011.00.15 U 1
ug/L EPA 8270E 03/22/19 17:26Phorate [298-02-2]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 17:26Ronnel [299-84-3]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 17:26Stirophos (Tetrachlorvinphos) [22248-79-9]0.38 jfi9C210010.500.38 U 1
ug/L EPA 8270E 03/22/19 17:26Sulfotep [3689-24-5]0.26 jfi9C210010.500.26 U 1
ug/L EPA 8270E 03/22/19 17:26TEPP [107-49-3]0.20 jfi9C210011.00.20 U 1
ug/L EPA 8270E 03/22/19 17:26Tokuthion (Prothiofos) [34643-46-4]0.24 jfi9C210010.500.24 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
Tributyl Phosphate 50-15091 %jfiEPA 8270E 03/22/19 17:269C210013.7 4.02 1
Triphenyl phosphate 50-15084 %jfiEPA 8270E 03/22/19 17:269C210013.4 4.02 1
Page 33 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
TMW-5Description:Lab Sample ID:CC03837-05 03/15/19 09:32Received:
CC03837Work Order:03/14/19 16:15Sampled:Ground WaterMatrix:
Kevin KeltSampled By:Project:Davis - McCoy Parcel
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8151A 03/25/19 15:062,4,5-T [93-76-5]^0.28 RGG9C210260.500.28 U 1
ug/L EPA 8151A 03/25/19 15:062,4,5-TP (Silvex) [93-72-1]^0.44 RGG9C210260.500.44 U 1
ug/L EPA 8151A 03/25/19 15:062,4-D [94-75-7]^0.27 RGG9C210260.500.27 U 1
ug/L EPA 8151A 03/25/19 15:062,4-DB [94-82-6]^0.35 RGG9C210260.500.35 U 1
ug/L EPA 8151A 03/25/19 15:063,5-DCBA [51-365-5]^0.36 RGG9C210260.500.36 U 1
ug/L EPA 8151A 03/25/19 15:064-Nitrophenol [100-02-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 15:06Acifluorfen [50594-66-6]^0.45 RGG9C210260.500.45 U 1
ug/L EPA 8151A 03/25/19 15:06Bentazon [25057-89-0]^0.22 RGG9C210260.500.22 U 1
ug/L EPA 8151A 03/25/19 15:06Chloramben [133-90-4]^0.43 RGG9C210260.500.43 U 1
ug/L EPA 8151A 03/25/19 15:06Dacthal [1861-32-1]^0.23 RGG9C210260.500.23 U 1
ug/L EPA 8151A 03/25/19 15:06Dalapon [75-99-0]^0.49 RGG9C210260.500.49 U 1
ug/L EPA 8151A 03/25/19 15:06Dicamba [1918-00-9]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 15:06Dichlorprop [120-36-5]^0.31 RGG9C210260.500.31 U 1
ug/L EPA 8151A 03/25/19 15:06Dinoseb [88-85-7]^0.32 RGG9C210260.500.32 U 1
ug/L EPA 8151A 03/25/19 15:06MCPA [94-74-6]^34 RGG9C210265034U QV-011
ug/L EPA 8151A 03/25/19 15:06MCPP [7085-19-0]^46 RGG9C210265046U 1
ug/L EPA 8151A 03/25/19 15:06Pentachlorophenol [87-86-5]^0.19 RGG9C210260.500.19 U 1
ug/L EPA 8151A 03/25/19 15:06Picloram [1918-02-1]^0.23 RGG9C210260.500.23 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,4-DCAA 37-13499 %RGGEPA 8151A 03/25/19 15:069C210262.0 2.02 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 365.4 03/27/19 15:11Phosphorus [7723-14-0]^0.020 kgonz9C250150.0300.035 1
Page 34 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CC03837-06 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:WaterMatrix:
ENCOSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 04:021,1,1,2-Tetrachloroethane [630-20-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:021,1,1-Trichloroethane [71-55-6]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 04:021,1,2,2-Tetrachloroethane [79-34-5]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 04:021,1,2-Trichloroethane [79-00-5]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 04:021,1-Dichloroethane [75-34-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 04:021,1-Dichloroethene [75-35-4]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 04:021,1-Dichloropropene [563-58-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:021,2,3-Trichlorobenzene [87-61-6]^0.012 MRK9C150221.00.012 U 1
ug/L EPA 8260D 03/16/19 04:021,2,3-Trichloropropane [96-18-4]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 04:021,2,4-Trichlorobenzene [120-82-1]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 04:021,2,4-Trimethylbenzene [95-63-6]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 04:021,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 04:021,2-Dibromoethane [106-93-4]^0.66 MRK9C150221.00.66 U 1
ug/L EPA 8260D 03/16/19 04:021,2-Dichlorobenzene [95-50-1]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 04:021,2-Dichloroethane [107-06-2]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 04:021,2-Dichloropropane [78-87-5]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 04:021,3,5-Trimethylbenzene [108-67-8]^0.30 MRK9C150221.00.30 U 1
ug/L EPA 8260D 03/16/19 04:021,3-Dichlorobenzene [541-73-1]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:021,3-Dichloropropane [142-28-9]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 04:021,4-Dichlorobenzene [106-46-7]^0.19 MRK9C150221.00.19 U 1
ug/L EPA 8260D 03/16/19 04:022,2-Dichloropropane [594-20-7]^0.28 MRK9C150221.00.28 U 1
ug/L EPA 8260D 03/16/19 04:022-Butanone [78-93-3]^1.3 MRK9C150225.01.3 U 1
ug/L EPA 8260D 03/16/19 04:022-Chloroethyl Vinyl Ether [110-75-8]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 04:022-Chlorotoluene [95-49-8]^0.081 MRK9C150221.00.081 U 1
ug/L EPA 8260D 03/16/19 04:022-Hexanone [591-78-6]^0.88 MRK9C150225.00.88 U 1
ug/L EPA 8260D 03/16/19 04:024-Chlorotoluene [106-43-4]^0.068 MRK9C150221.00.068 U 1
ug/L EPA 8260D 03/16/19 04:024-Isopropyltoluene [99-87-6]^0.085 MRK9C150221.00.085 U 1
ug/L EPA 8260D 03/16/19 04:024-Methyl-2-pentanone [108-10-1]^1.1 MRK9C150225.01.1 U 1
ug/L EPA 8260D 03/16/19 04:02Acetone [67-64-1]^10 MRK9C150222011JB O-011
ug/L EPA 8260D 03/16/19 04:02Benzene [71-43-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:02Bromobenzene [108-86-1]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 04:02Bromochloromethane [74-97-5]^0.48 MRK9C150221.00.48 U 1
ug/L EPA 8260D 03/16/19 04:02Bromodichloromethane [75-27-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Bromoform [75-25-2]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 04:02Bromomethane [74-83-9]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 04:02Carbon disulfide [75-15-0]^1.5 MRK9C150225.01.5 U 1
ug/L EPA 8260D 03/16/19 04:02Carbon tetrachloride [56-23-5]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Chlorobenzene [108-90-7]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Chloroethane [75-00-3]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 04:02Chloroform [67-66-3]^0.18 MRK9C150221.00.18 U 1
ug/L EPA 8260D 03/16/19 04:02Chloromethane [74-87-3]^0.13 MRK9C150221.00.13 U 1
ug/L EPA 8260D 03/16/19 04:02cis-1,2-Dichloroethene [156-59-2]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:02cis-1,3-Dichloropropene [10061-01-5]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 04:02Dibromochloromethane [124-48-1]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Dibromomethane [74-95-3]^0.27 MRK9C150221.00.27 U 1
ug/L EPA 8260D 03/16/19 04:02Dichlorodifluoromethane [75-71-8]^0.20 MRK9C150221.00.20 U 1
ug/L EPA 8260D 03/16/19 04:02Ethylbenzene [100-41-4]^0.13 MRK9C150221.00.13 U 1
Page 35 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CC03837-06 03/15/19 09:32Received:
CC03837Work Order:03/14/19 11:10Sampled:WaterMatrix:
ENCOSampled By:Project:Davis - McCoy Parcel
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 8260D 03/16/19 04:02Hexachlorobutadiene [87-68-3]^0.22 MRK9C150221.00.22 U 1
ug/L EPA 8260D 03/16/19 04:02Isopropylbenzene [98-82-8]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 04:02m,p-Xylenes [108-38-3/106-42-3]^0.17 MRK9C150222.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Methylene chloride [75-09-2]^0.23 MRK9C150221.00.23 U 1
ug/L EPA 8260D 03/16/19 04:02Methyl-tert-Butyl Ether [1634-04-4]^0.16 MRK9C150221.00.16 U 1
ug/L EPA 8260D 03/16/19 04:02Naphthalene [91-20-3]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 04:02n-Butyl Benzene [104-51-8]^0.058 MRK9C150221.00.058 U 1
ug/L EPA 8260D 03/16/19 04:02n-Propyl Benzene [103-65-1]^0.12 MRK9C150221.00.12 U 1
ug/L EPA 8260D 03/16/19 04:02o-Xylene [95-47-6]^0.065 MRK9C150221.00.065 U 1
ug/L EPA 8260D 03/16/19 04:02sec-Butylbenzene [135-98-8]^0.10 MRK9C150221.00.10 U 1
ug/L EPA 8260D 03/16/19 04:02Styrene [100-42-5]^0.11 MRK9C150221.00.11 U 1
ug/L EPA 8260D 03/16/19 04:02tert-Butylbenzene [98-06-6]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Tetrachloroethene [127-18-4]^0.17 MRK9C150221.00.17 U 1
ug/L EPA 8260D 03/16/19 04:02Toluene [108-88-3]^0.14 MRK9C150221.00.14 U 1
ug/L EPA 8260D 03/16/19 04:02trans-1,2-Dichloroethene [156-60-5]^0.21 MRK9C150221.00.21 U 1
ug/L EPA 8260D 03/16/19 04:02trans-1,3-Dichloropropene [10061-02-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:02Trichloroethene [79-01-6]^0.15 MRK9C150221.00.15 U 1
ug/L EPA 8260D 03/16/19 04:02Trichlorofluoromethane [75-69-4]^0.24 MRK9C150221.00.24 U 1
ug/L EPA 8260D 03/16/19 04:02Vinyl chloride [75-01-4]^0.32 MRK9C150221.00.32 U 1
ug/L EPA 8260D 03/16/19 04:02Xylenes (Total) [1330-20-7]^0.45 MRK9C150223.00.45 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136108 %MRKEPA 8260D 03/16/19 04:029C150225450.0 1
Dibromofluoromethane 67-129102 %MRKEPA 8260D 03/16/19 04:029C150225150.0 1
Toluene-d8 59-134104 %MRKEPA 8260D 03/16/19 04:029C150225250.0 1
Page 36 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9C15022 - EPA 5030B_MS
Prepared: 03/15/2019 15:00 Analyzed: 03/15/2019 19:08Blank (9C15022-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.15 U 1,1-Dichloropropene
ug/L1.00.012 U 1,2,3-Trichlorobenzene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.14 U 1,2,4-Trichlorobenzene
ug/L1.00.10 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.30 U 1,3,5-Trimethylbenzene
ug/L1.00.15 U 1,3-Dichlorobenzene
ug/L1.00.16 U 1,3-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L1.00.28 U 2,2-Dichloropropane
ug/L5.01.3 U 2-Butanone
ug/L5.01.1 U 2-Chloroethyl Vinyl Ether
ug/L1.00.081 U 2-Chlorotoluene
ug/L5.00.88 U 2-Hexanone
ug/L1.00.068 U 4-Chlorotoluene
ug/L1.00.085 U 4-Isopropyltoluene
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2012J O-01Acetone
ug/L1.00.15 U Benzene
ug/L1.00.16 U Bromobenzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.20 U Dichlorodifluoromethane
ug/L1.00.13 U Ethylbenzene
ug/L1.00.22 U Hexachlorobutadiene
ug/L1.00.14 U Isopropylbenzene
Page 37 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9C15022 - EPA 5030B_MS - Continued
Prepared: 03/15/2019 15:00 Analyzed: 03/15/2019 19:08Blank (9C15022-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.16 U Methyl-tert-Butyl Ether
ug/L1.00.11 U Naphthalene
ug/L1.00.058 U n-Butyl Benzene
ug/L1.00.12 U n-Propyl Benzene
ug/L1.00.065 U o-Xylene
ug/L1.00.10 U sec-Butylbenzene
ug/L1.00.11 U Styrene
ug/L1.00.17 U tert-Butylbenzene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
ug/L 50.0 53-1364-Bromofluorobenzene 10151
ug/L 50.0 67-129Dibromofluoromethane10753
ug/L 50.0 59-134Toluene-d8 10050
Prepared: 03/15/2019 15:00 Analyzed: 03/15/2019 17:02LCS (9C15022-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 75-13310621 1,1-Dichloroethene
ug/L1.0 20.0 80-13411222 Benzene
ug/L1.0 20.0 80-12010321 Chlorobenzene
ug/L1.0 20.0 71-12010321 Toluene
ug/L1.0 20.0 74-12010421 Trichloroethene
ug/L 50.0 53-1364-Bromofluorobenzene 10553
ug/L 50.0 67-129Dibromofluoromethane10352
ug/L 50.0 59-134Toluene-d8 10251
Prepared: 03/15/2019 15:00 Analyzed: 03/15/2019 17:34Matrix Spike (9C15022-MS1)
Source: CC04558-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 75-1331000.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 80-1341120.15 U22 Benzene
ug/L1.0 20.0 80-120950.17 U19 Chlorobenzene
ug/L1.0 20.0 71-1201000.14 U20 Toluene
ug/L1.0 20.0 74-120980.15 U20 Trichloroethene
ug/L 50.0 53-1364-Bromofluorobenzene 10553
ug/L 50.0 67-129Dibromofluoromethane9849
ug/L 50.0 59-134Toluene-d8 10251
Page 38 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9C15022 - EPA 5030B_MS - Continued
Prepared: 03/15/2019 15:00 Analyzed: 03/15/2019 18:05Matrix Spike Dup (9C15022-MSD1)
Source: CC04558-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 2075-13397 30.21 U19 1,1-Dichloroethene
ug/L1.0 20.0 1780-134110 20.15 U22 Benzene
ug/L1.0 20.0 1680-12093 20.17 U19 Chlorobenzene
ug/L1.0 20.0 1771-12096 30.14 U19 Toluene
ug/L1.0 20.0 2274-12098 0.050.15 U20 Trichloroethene
ug/L 50.0 53-1364-Bromofluorobenzene 10452
ug/L 50.0 67-129Dibromofluoromethane10050
ug/L 50.0 59-134Toluene-d8 10351
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9C18010 - EPA 3510C_MS
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 13:33Blank (9C18010-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L102.5 U 1,2,4-Trichlorobenzene
ug/L102.5 U 1,2-Dichlorobenzene
ug/L102.5 U 1,3-Dichlorobenzene
ug/L102.4 U 1,4-Dichlorobenzene
ug/L102.7 U 1-Methylnaphthalene
ug/L102.5 U 2,4,5-Trichlorophenol
ug/L102.6 U 2,4,6-Trichlorophenol
ug/L102.6 U 2,4-Dichlorophenol
ug/L102.3 U 2,4-Dimethylphenol
ug/L102.6 U 2,4-Dinitrophenol
ug/L102.6 U 2,4-Dinitrotoluene
ug/L102.5 U 2,6-Dinitrotoluene
ug/L102.8 U 2-Chloronaphthalene
ug/L102.2 U 2-Chlorophenol
ug/L103.3 U 2-Methyl-4,6-dinitrophenol
ug/L102.8 U 2-Methylnaphthalene
ug/L102.0 U 2-Methylphenol
ug/L102.5 U 2-Nitroaniline
ug/L101.1 U 2-Nitrophenol
ug/L102.1 U 3 & 4-Methylphenol
ug/L103.5 U 3,3’-Dichlorobenzidine
ug/L102.6 U 3-Nitroaniline
ug/L102.4 U 4-Bromophenyl-phenylether
ug/L102.4 U 4-Chloro-3-methylphenol
ug/L102.0 U 4-Chloroaniline
ug/L102.6 U 4-Chlorophenyl-phenylether
ug/L103.2 U 4-Nitroaniline
ug/L102.8 U 4-Nitrophenol
ug/L102.7 U Acenaphthene
ug/L102.6 U Acenaphthylene
ug/L102.4 U Anthracene
ug/L101.6 U QV-01Benzidine
ug/L102.4 U Benzo(a)anthracene
Page 39 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9C18010 - EPA 3510C_MS - Continued
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 13:33Blank (9C18010-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L102.2 U Benzo(a)pyrene
ug/L102.8 U Benzo(b)fluoranthene
ug/L102.4 U Benzo(g,h,i)perylene
ug/L102.4 U Benzo(k)fluoranthene
ug/L501.0 U QV-02Benzoic acid
ug/L102.4 U Benzyl alcohol
ug/L102.4 U Bis(2-chloroethoxy)methane
ug/L102.6 U Bis(2-chloroethyl)ether
ug/L102.5 U Bis(2-chloroisopropyl)ether
ug/L5.01.9 U Bis(2-ethylhexyl)phthalate
ug/L103.8 U Butylbenzylphthalate
ug/L102.2 U Chrysene
ug/L102.3 U Dibenzo(a,h)anthracene
ug/L102.6 U Dibenzofuran
ug/L102.4 U Diethylphthalate
ug/L102.5 U Dimethylphthalate
ug/L102.8 U Di-n-butylphthalate
ug/L103.1 U Di-n-octylphthalate
ug/L103.1 U Fluoranthene
ug/L102.5 U Fluorene
ug/L102.3 U Hexachlorobenzene
ug/L102.8 U Hexachlorobutadiene
ug/L102.7 U Hexachlorocyclopentadiene
ug/L102.6 U Hexachloroethane
ug/L102.2 U Indeno(1,2,3-cd)pyrene
ug/L102.5 U Isophorone
ug/L102.8 U Naphthalene
ug/L102.5 U Nitrobenzene
ug/L101.9 U N-Nitrosodimethylamine
ug/L102.3 U N-Nitroso-di-n-propylamine
ug/L102.5 U N-nitrosodiphenylamine/Diphenylamine
ug/L102.1 U Pentachlorophenol
ug/L102.6 U Phenanthrene
ug/L101.7 U Phenol
ug/L103.5 U Pyrene
ug/L102.2 U Pyridine
ug/L 200 10-1792,4,6-Tribromophenol 76150
ug/L 100 10-1492-Fluorobiphenyl 8282
ug/L 200 10-1102-Fluorophenol 4997
ug/L 100 10-149Nitrobenzene-d5 7474
ug/L 200 10-88Phenol-d5 3774
ug/L 100 10-188Terphenyl-d14 6363
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 14:03LCS (9C18010-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 27-906934 1,2,4-Trichlorobenzene
ug/L10 50.0 23-845829 1,4-Dichlorobenzene
ug/L10 50.0 67-1328040 2,4-Dinitrotoluene
Page 40 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9C18010 - EPA 3510C_MS - Continued
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 14:03LCS (9C18010-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 40-1097035 2-Chlorophenol
ug/L10 50.0 58-1217739 4-Chloro-3-methylphenol
ug/L10 50.0 33-1055427 4-Nitrophenol
ug/L10 50.0 39-1257839 Acenaphthene
ug/L10 50.0 48-1267336 N-Nitroso-di-n-propylamine
ug/L10 50.0 51-1356834 Pentachlorophenol
ug/L10 50.0 19-784824 Phenol
ug/L10 50.0 44-1378844 Pyrene
ug/L 100 10-1792,4,6-Tribromophenol 8484
ug/L 50.0 10-1492-Fluorobiphenyl 7437
ug/L 100 10-1102-Fluorophenol 5050
ug/L 50.0 10-149Nitrobenzene-d5 6733
ug/L 100 10-88Phenol-d5 4444
ug/L 50.0 10-188Terphenyl-d14 7638
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 15:03Matrix Spike (9C18010-MS1)
Source: CC04567-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 27-90802.5 U40 1,2,4-Trichlorobenzene
ug/L10 50.0 23-84682.4 U34 1,4-Dichlorobenzene
ug/L10 50.0 67-132932.6 U46 2,4-Dinitrotoluene
ug/L10 50.0 40-109752.2 U37 2-Chlorophenol
ug/L10 50.0 58-121832.4 U42 4-Chloro-3-methylphenol
ug/L10 50.0 33-105632.8 U31 4-Nitrophenol
ug/L10 50.0 39-125882.7 U44 Acenaphthene
ug/L10 50.0 48-126802.3 U40 N-Nitroso-di-n-propylamine
ug/L10 50.0 51-135792.1 U40 Pentachlorophenol
ug/L10 50.0 19-78511.7 U26 Phenol
ug/L10 50.0 44-1371093.5 U54 Pyrene
ug/L 100 10-1792,4,6-Tribromophenol 9797
ug/L 50.0 10-1492-Fluorobiphenyl 8442
ug/L 100 10-1102-Fluorophenol 5656
ug/L 50.0 10-149Nitrobenzene-d5 7638
ug/L 100 10-88Phenol-d5 4747
ug/L 50.0 10-188Terphenyl-d14 9749
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 15:33Matrix Spike Dup (9C18010-MSD1)
Source: CC04567-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 4327-9081 0.72.5 U40 1,2,4-Trichlorobenzene
ug/L10 50.0 3923-8469 12.4 U34 1,4-Dichlorobenzene
ug/L10 50.0 1767-13289 42.6 U45 2,4-Dinitrotoluene
ug/L10 50.0 2240-10974 0.42.2 U37 2-Chlorophenol
ug/L10 50.0 2258-12187 52.4 U44 4-Chloro-3-methylphenol
ug/L10 50.0 2733-10568 72.8 U34 4-Nitrophenol
ug/L10 50.0 2539-12584 52.7 U42 Acenaphthene
ug/L10 50.0 2348-12682 32.3 U41 N-Nitroso-di-n-propylamine
ug/L10 50.0 1151-13582 32.1 U41 Pentachlorophenol
Page 41 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9C18010 - EPA 3510C_MS - Continued
Prepared: 03/18/2019 09:14 Analyzed: 03/19/2019 15:33Matrix Spike Dup (9C18010-MSD1) Continued
Source: CC04567-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 1819-7856 81.7 U28 Phenol
ug/L10 50.0 2444-137101 73.5 U50 Pyrene
ug/L 100 10-1792,4,6-Tribromophenol 6969
ug/L 50.0 10-1492-Fluorobiphenyl 6331
ug/L 100 10-1102-Fluorophenol 3939
ug/L 50.0 10-149Nitrobenzene-d5 5527
ug/L 100 10-88Phenol-d5 3232
ug/L 50.0 10-188Terphenyl-d14 6935
Organochlorine Pesticides by GC - Quality Control
Batch 9C18035 - EPA 3510C
Prepared: 03/18/2019 13:38 Analyzed: 03/21/2019 16:26Blank (9C18035-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.0500.044 U 4,4’-DDD
ug/L0.0500.048 U 4,4’-DDE
ug/L0.0500.049 U 4,4’-DDT
ug/L0.0500.041 U Aldrin
ug/L0.0500.036 U alpha-BHC
ug/L0.0500.041 U beta-BHC
ug/L0.500.37 U Chlordane (tech)
ug/L0.0500.048 U Chlordane-alpha
ug/L0.0500.042 U Chlordane-gamma
ug/L0.0500.048 U delta-BHC
ug/L0.0500.045 U Dieldrin
ug/L0.0500.045 U Endosulfan I
ug/L0.0500.038 U Endosulfan II
ug/L0.0500.032 U Endosulfan sulfate
ug/L0.0500.041 U Endrin
ug/L0.0500.049 U Endrin aldehyde
ug/L0.0500.039 U Endrin ketone
ug/L0.0500.034 U gamma-BHC
ug/L0.0500.047 U Heptachlor
ug/L0.0500.037 U Heptachlor epoxide
ug/L0.0500.031 U Isodrin
ug/L0.0500.048 U Methoxychlor
ug/L0.0500.044 U Mirex
ug/L1.00.28 U Toxaphene
ug/L 1.00 10-1392,4,5,6-TCMX 850.85
ug/L 1.00 10-122Decachlorobiphenyl810.81
Prepared: 03/18/2019 13:38 Analyzed: 03/21/2019 16:43LCS (9C18035-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.050 2.00 37-1391022.0 4,4’-DDT
ug/L0.050 2.00 46-132901.8 Dieldrin
ug/L0.050 2.00 43-133982.0 Endrin
Page 42 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Organochlorine Pesticides by GC - Quality Control
Batch 9C18035 - EPA 3510C - Continued
Prepared: 03/18/2019 13:38 Analyzed: 03/21/2019 16:43LCS (9C18035-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L 1.00 10-1392,4,5,6-TCMX 900.90
ug/L 1.00 10-122Decachlorobiphenyl740.74
Prepared: 03/18/2019 13:38 Analyzed: 03/21/2019 17:00Matrix Spike (9C18035-MS1)
Source: CC04567-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.050 2.00 37-1391020.049 U2.0 4,4’-DDT
ug/L0.050 2.00 46-132740.045 U1.5 Dieldrin
ug/L0.050 2.00 43-133970.041 U1.9 Endrin
ug/L 1.00 10-1392,4,5,6-TCMX 820.82
ug/L 1.00 10-122Decachlorobiphenyl940.94
Prepared: 03/18/2019 13:38 Analyzed: 03/21/2019 17:16Matrix Spike Dup (9C18035-MSD1)
Source: CC04567-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.050 2.00 2637-13998 40.049 U2.0 4,4’-DDT
ug/L0.050 2.00 2746-13270 60.045 U1.4 Dieldrin
ug/L0.050 2.00 2643-13394 30.041 U1.9 Endrin
ug/L 1.00 10-1392,4,5,6-TCMX 920.92
ug/L 1.00 10-122Decachlorobiphenyl970.97
Classical Chemistry Parameters - Quality Control
Batch 9C15007 - NO PREP
Prepared: 03/15/2019 10:00 Analyzed: 03/15/2019 10:00Blank (9C15007-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.100.017 U Nitrite as N
Prepared: 03/15/2019 09:51 Analyzed: 03/15/2019 09:51LCS (9C15007-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.00 90-110990.99 Nitrite as N
Prepared: 03/15/2019 10:03 Analyzed: 03/15/2019 10:03Matrix Spike (9C15007-MS1)
Source: CC02462-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.00 90-110960.017 U0.96 Nitrite as N
Prepared: 03/15/2019 10:04 Analyzed: 03/15/2019 10:04Matrix Spike Dup (9C15007-MSD1)
Source: CC02462-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.00 1090-11097 10.017 U0.97 Nitrite as N
Batch 9C25029 - NO PREP
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9C25029 - NO PREP - Continued
Prepared: 03/25/2019 15:47 Analyzed: 03/25/2019 15:47Blank (9C25029-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.100.041 U Nitrate/Nitrite as N
Prepared: 03/25/2019 15:49 Analyzed: 03/25/2019 15:49LCS (9C25029-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.25 90-1101041.3 Nitrate/Nitrite as N
Prepared: 03/25/2019 15:56 Analyzed: 03/25/2019 15:56Matrix Spike (9C25029-MS1)
Source: CC01618-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L10 50.0 90-1101023485 Nitrate/Nitrite as N
Prepared: 03/25/2019 19:54 Analyzed: 03/25/2019 19:54Matrix Spike (9C25029-MS2)
Source: CC02704-01RE1
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 0.521 90-110920.801.3 Nitrate/Nitrite as N
Prepared: 03/25/2019 15:58 Analyzed: 03/25/2019 15:58Matrix Spike Dup (9C25029-MSD1)
Source: CC01618-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L10 50.0 1090-110108 33488 Nitrate/Nitrite as N
Batch 9C25031 - NO PREP
Prepared & Analyzed: 03/25/2019 15:52Blank (9C25031-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.02.9 U Sulfate as SO4
Prepared & Analyzed: 03/25/2019 16:07LCS (9C25031-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 50.0 90-1109949 Sulfate as SO4
Prepared & Analyzed: 03/25/2019 16:21Matrix Spike (9C25031-MS1)
Source: CC00759-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 20.0 90-1101032.9 U21 Sulfate as SO4
Prepared & Analyzed: 03/25/2019 16:51Matrix Spike (9C25031-MS2)
Source: CC00759-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 20.0 90-1101042.9 U21 Sulfate as SO4
Prepared & Analyzed: 03/25/2019 16:36Matrix Spike Dup (9C25031-MSD1)
Source: CC00759-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9C25031 - NO PREP - Continued
Prepared & Analyzed: 03/25/2019 16:36Matrix Spike Dup (9C25031-MSD1) Continued
Source: CC00759-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 20.0 1090-110105 32.9 U21 Sulfate as SO4
Batch 9C25037 - NO PREP
Prepared: 03/25/2019 18:18 Analyzed: 03/25/2019 18:18Blank (9C25037-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.100.041 U Nitrate/Nitrite as N
Prepared: 03/25/2019 18:20 Analyzed: 03/25/2019 18:20LCS (9C25037-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.25 90-110941.2 Nitrate/Nitrite as N
Prepared: 03/25/2019 18:24 Analyzed: 03/25/2019 18:24Matrix Spike (9C25037-MS1)
Source: CB11379-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.20 1.00 90-110897.58.4 E QM-07Nitrate/Nitrite as N
Prepared: 03/25/2019 18:29 Analyzed: 03/25/2019 18:29Matrix Spike (9C25037-MS2)
Source: CC01511-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L10 50.0 90-1109154100 Nitrate/Nitrite as N
Prepared: 03/25/2019 18:26 Analyzed: 03/25/2019 18:26Matrix Spike Dup (9C25037-MSD1)
Source: CB11379-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.20 1.00 1090-110111 37.58.6 E QM-07Nitrate/Nitrite as N
Batch 9C28026 - NO PREP
Prepared: 03/28/2019 14:02 Analyzed: 03/28/2019 17:05Blank (9C28026-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.100.041 U Nitrate/Nitrite as N
Prepared: 03/28/2019 14:02 Analyzed: 03/28/2019 17:03LCS (9C28026-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.10 1.25 90-1101061.3 Nitrate/Nitrite as N
Prepared: 03/28/2019 14:02 Analyzed: 03/28/2019 17:08Matrix Spike (9C28026-MS1)
Source: CB11379-02RE1
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.50 2.50 90-1101148.011 QM-07Nitrate/Nitrite as N
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9C28026 - NO PREP - Continued
Prepared: 03/28/2019 14:02 Analyzed: 03/29/2019 09:25Matrix Spike (9C28026-MS2)
Source: CC01618-01RE3
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L10 50.0 90-110964188 Nitrate/Nitrite as N
Prepared: 03/28/2019 14:02 Analyzed: 03/28/2019 17:10Matrix Spike Dup (9C28026-MSD1)
Source: CB11379-02RE1
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.50 2.50 1090-11088 68.010 QM-07Nitrate/Nitrite as N
Chlorinated Herbicides by GC - Quality Control
Batch 9C21026 - EPA 3510C
Prepared: 03/21/2019 11:50 Analyzed: 03/25/2019 10:54Blank (9C21026-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.500.28 U 2,4,5-T
ug/L0.500.44 U 2,4,5-TP (Silvex)
ug/L0.500.27 U 2,4-D
ug/L0.500.35 U 2,4-DB
ug/L0.500.36 U 3,5-DCBA
ug/L0.500.32 U 4-Nitrophenol
ug/L0.500.45 U Acifluorfen
ug/L0.500.22 U Bentazon
ug/L0.500.43 U Chloramben
ug/L0.500.23 U Dacthal
ug/L0.500.49 U Dalapon
ug/L0.500.19 U Dicamba
ug/L0.500.31 U Dichlorprop
ug/L0.500.32 U Dinoseb
ug/L5034U MCPA
ug/L5046U MCPP
ug/L0.500.19 U Pentachlorophenol
ug/L0.500.23 U Picloram
ug/L 2.00 37-1342,4-DCAA 1122.2
Prepared: 03/21/2019 11:50 Analyzed: 03/25/2019 11:44LCS (9C21026-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L0.50 2.00 24-1351212.4 2,4,5-TP (Silvex)
ug/L0.50 2.00 20-1341182.4 2,4-D
ug/L0.50 2.00 16-1421362.7 2,4-DB
ug/L0.50 2.00 10-150881.8 Bentazon
ug/L0.50 2.00 10-174721.4 Dalapon
ug/L0.50 2.00 25-1281282.6 Dicamba
ug/L0.50 2.00 18-128941.9 Picloram
ug/L 2.00 37-1342,4-DCAA 1092.2
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QUALITY CONTROL DATA
Chlorinated Herbicides by GC - Quality Control
Batch 9C21026 - EPA 3510C - Continued
Prepared: 03/21/2019 11:50 Analyzed: 03/25/2019 12:09Matrix Spike (9C21026-MS1)
Source: AC01714-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L2.5 10.0 24-1351122.2 U11 2,4,5-TP (Silvex)
ug/L2.5 10.0 20-1341531.4 U15 QM-072,4-D
ug/L2.5 10.0 16-1421011.8 U10 2,4-DB
ug/L2.5 10.0 10-150671.1 U6.7 Bentazon
ug/L2.5 10.0 10-174312.4 U3.1 Dalapon
ug/L2.5 10.0 25-1281160.95 U12 Dicamba
ug/L2.5 10.0 18-128761.2 U7.6 Picloram
ug/L 10.0 37-1342,4-DCAA [2C]757.5
Prepared: 03/21/2019 11:50 Analyzed: 03/25/2019 12:34Matrix Spike Dup (9C21026-MSD1)
Source: AC01714-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L2.5 10.0 1924-135104 72.2 U10 2,4,5-TP (Silvex)
ug/L2.5 10.0 1920-13486 561.4 U8.6 QM-112,4-D
ug/L2.5 10.0 2116-142107 61.8 U11 2,4-DB
ug/L2.5 10.0 2310-15072 81.1 U7.2 Bentazon
ug/L2.5 10.0 2910-17444 342.4 U4.4 QM-11Dalapon
ug/L2.5 10.0 1725-128108 80.95 U11 Dicamba
ug/L2.5 10.0 1818-12872 71.2 U7.2 Picloram
ug/L 10.0 37-1342,4-DCAA [2C]919.1
Classical Chemistry Parameters - Quality Control
Batch 9C25015 - NO PREP
Prepared: 03/25/2019 09:16 Analyzed: 03/27/2019 14:53Blank (9C25015-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.0300.020 U Phosphorus
Prepared: 03/25/2019 09:16 Analyzed: 03/27/2019 14:59LCS (9C25015-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.030 2.50 90-1101032.6 Phosphorus
Prepared: 03/25/2019 09:16 Analyzed: 03/27/2019 15:25Matrix Spike (9C25015-MS2)
Source: AC00561-01RE1
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.060 2.50 90-110944.06.4 D Phosphorus
Prepared: 03/25/2019 09:16 Analyzed: 03/27/2019 15:27Matrix Spike Dup (9C25015-MSD2)
Source: AC00561-01RE1
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.060 2.50 1090-11087 34.06.2 D QM-07Phosphorus
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.PQL
Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.[CALC]
This compound is a common laboratory contaminant.O-01
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-07
Precision between duplicate matrix spikes of the same sample was outside acceptance limits.QM-11
The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
QV-01
The associated continuing calibration verification standard exhibited low bias; the reported result should
be considered to be a minimum estimate.
QV-02
Page 48 of 49This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

Divider
Page
WELL ABANDONMENT RECORD
This form can be used for single or multiple wells
Form GW-30 North Carolina Department of Environment and Natural Resources – Division of Water Resources Revised August 2013

1. Well Contractor Information:

Well Contractor Name (or well owner personally abandoning well on his/her property)

NC Well Contractor Certification Number

Company Name

2. Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)

4. Date well(s) abandoned:

5a. Well location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)

5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W

CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply
wells ONLY with the same construction/abandonment, you can submit one form.

6a. Well ID#:

6b. Total well depth: (ft.)

6c. Borehole diameter: (in.)

6d. Water level below ground surface: (ft.)

6e. Outer casing length (if known): (ft.)

6f. Inner casing/tubing length (if known): (ft.)

6g. Screen length (if known): (ft.)

WELL ABANDONMENT DETAILS

7a. Number of wells being abandoned:
For multiple injection or non-water supply wells ONLY with the same
construction/abandonment, you can submit one form.

7b. Approximate volume of water remaining in well(s): (gal.)

FOR WATER SUPPLY WELLS ONLY:

7c. Type of disinfectant used:

7d. Amount of disinfectant used:

7e. Sealing materials used (check all that apply):
□ Neat Cement Grout □ Bentonite Chips or Pellets
□ Sand Cement Grout □ Dry Clay
□ Concrete Grout □ Drill Cuttings
□ Specialty Grout □ Gravel
□ Bentonite Slurry □ Other (explain under 7g)

7f. For each material selected above, provide amount of materials used:

7g. Provide a brief description of the abandonment procedure:

8. Certification:

Signature of Certified Well Contractor or Well Owner Date

By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.

9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:

Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617

10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636

10c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well abandonment to the county health department of the county
where abandoned.
For Internal Use ONLY: