RA-8268_46344_CA_RPTS_20200908_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

September 8, 2020

Mr. Sean Patrick
NCDEQ-UST Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628

Re: Ground Water Monitoring Report
August 2020
New Dixie Mart #226
4917 Raleigh Road Parkway West
Wilson, Wilson County,
North Carolina
Facility ID No.: 0-00-0000034646
Incident Number: 46344
GRI Project No: 4841

Dear Mr. Patrick,

Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. John Elam; New Dixie Oil Corporation, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
August 2020
New Dixie Mart #226
4917 Raleigh Road Parkway West
Wilson, Wilson County
North Carolina
Facility ID Number: 0-00-0000034646
Incident Number: 46344
GRI Project Number: 4841

Prepared for:

New Dixie Oil Corporation
1501 Marshall Street
Roanoke Rapids, NC 27870

September 8, 2020

William Regenthal, PG
Project Manager
Ethan Rogerson, GIT
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
i

SITE INFORMATION
1. Site Identification
 New Dixie Mart #226 (Facility ID 0-00-0000034646)
 Incident Number 46344 – High Risk (H130D)
 Location of Source Area: 4917 Raleigh Road Parkway West
Wilson, NC 28677
Wilson County
35.761996°N, 77.998559°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
New Dixie Oil Corporation
1501 Marshall Street
Roanoke Rapids, NC 27870
[e-mail]
252-537-4118

UST Operator
New Dixie Oil Corporation
1501 Marshall Street
Roanoke Rapids, NC 27870
[e-mail]
252-537-4118

Property Owner
New Dixie Oil Corporation
Post Office Box 779
Roanoke Rapids, NC 27870
Email Unknown
252-537-4118

Property Occupant
Down East Auto
4917 Raleigh Road Parkway W.
Wilson, NC 27896
[e-mail]
252-903-1001

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-698-1253

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered on June 26, 2018.
 An unknown amount of product was released from the leaking UST System.
 Two 12,000-gallon gasoline USTs, associated dispensers and product piping were removed from
the site on June 26, 2018.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
ii

EXECUTIVE SUMMARY
New Dixie Mart #226 is located at 4917 Raleigh Road Parkway West in Wilson, Wilson County, North
Carolina. The site is currently owned by New Dixie Oil Corporation and is currently occupied by a used car
dealership. The adjoining properties are commercial. Two 12,000-gallon gasoline underground storage
tanks (USTs), associated dispensers and product piping were removed from the site on June 26, 2018. The
removed USTs were located in one basin in the rear of the former store. A release was confirmed upon
on-site screening of soil removed during the UST closure activities. The site risk classification is currently
ranked as high risk due to two potable water supply wells being located within 1,000-foot radius of the
site.

On August 13, 2020, eight monitoring wells and two telescoping wells were gauged, purged and/or
sampled per NCDEQ guidelines. Free product was observed in monitoring wells MW-4 and MW-8.
Concentrations of individual BTEX constituents, MTBE, naphthalene, n-propylbenzene, 1,2,4-
trimethylbenzene, 1,3,5-trimethylbenzene, TAA, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-C10
aromatics that exceeded the Maximum Allowable Concentrations (MACs) as specified in T15A NCAC
2L.0202 were reported in the ground water samples collected from MW-1, MW-3, MW-6, and TW-1.
Concentrations of benzene that exceeded the Gross Contamination Level (GCL) were reported in the
ground water samples collected from MW-3 and TW-1.

Based on this information, the risk classification for the site should remain high risk. It is recommended
that a free product evaluation should be conducted at the site. Semi-annual ground water monitoring
should be continued. The next sampling event is tentatively scheduled for February 2021.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................3
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................3
5.0 CONCLUSIONS .........................................................................................................................3
6.0 LIMITATIONS ...........................................................................................................................4
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: Toluene Isoconcentration Map
Figure 8: Ethylbenzene Isoconcentration Map
Figure 9: Xylenes Isoconcentration Map
Figure 10: MTBE Isoconcentration Map
Figure 11: Naphthalene Isoconcentration Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
1
1.0 SITE HISTORY AND CHARACTERIZATION
Geological Resources, Inc. (GRI) presents the results of the August 2020 ground water sampling event at
the New Dixie Mart #226 site; located at 4917 Raleigh Road Parkway West in Wilson, Wilson County, North
Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 20-377, which
was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on August 3, 2020,
and was approved as Task Authorization No. 46344-03 on August 4, 2020. State correspondence has been
included as Appendix A.

The site is currently owned by New Dixie Oil Corporation and is currently operated as a used car
dealership. Two 12,000-gallon gasoline underground storage tanks (USTs), associated dispensers and
product piping were removed from the site on June 26, 2018. A release was discovered during the June
2018 UST closure activities. UST owner/operator information and UST system information are included
as Tables 1 and 2, respectively. The Registered Tank Report is shown below:

The site and adjoining properties are commercial. The site contains one building and is primarily capped
with concrete and asphalt. The overall topography at the site is relatively flat. No surface water bodies
were identified within a 500-foot radius of the site. Thirteen Type II monitoring wells (MW-1 through
MW-13) and two Type III monitoring well (TW-1 and TW-2) were installed at the site during Limited Site
Assessment (LSA) and Comprehensive Site Assessment (CSA) activities. A Site Map showing the locations
of the monitoring wells and the structures on-site has been included as Figure 2.

On July 26, 2020, GRI personnel conducted a receptor survey at the site. Three water supply wells were
identified within a 1,500-foot radius of the site. Two potable wells (WSW-1 and WSW-3) were identified
within 1,000 feet of the site. No water supply wells were identified within a 250-foot radius of the source
area. No surface water bodies were identified within 500 feet of the source area. Municipal water is
available to the site and the surrounding properties. Water supply well information is presented in Table
3. Adjacent property owner information is presented in Table 4. A Site Vicinity Map showing the locations
of water supply wells and adjacent properties has been included as Figure 3.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
2
A Corrective Action Plan (CAP) has not been developed for this site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On August 13, 2020, eight Type II monitoring wells (MW-1, MW-3, MW-4, MW-6, MW-8 through MW-11)
and two telescoping well (TW-1 and TW-2) were gauged, purged and/or sampled per NCDEQ guidelines.
Free product was observed in MW-4 and MW-8. Depths to ground water in the Type II monitoring wells
ranged from 4.98 to 11.02 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells ranged from 88.58 feet to 94.74 feet. Ground water flow was generally to the northwest
with a horizontal gradient of approximately 0.04 feet per foot. The average vertical gradient between
paired wells MW-1/TW-1 and MW-1/TW-2 was approximately 0.02 feet per foot in the downward
direction. Well construction and gauging information is presented in Table 5. A Water Table Surface Map
based on the Type II monitoring wells is included as Figure 4. A summary of the current ground water
gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 10 - 20 20 100.00 5.28 --- 94.72
MW-3 3 - 18 18 99.73 6.33 --- 93.40
MW-4 3 - 18 18 100.73 7.29 1.51 94.74
MW-6 3 - 18 18 100.98 8.55 --- 92.43
MW-8 3 - 18 18 99.43 4.98 0.31 94.72
MW-9 3 - 18 18 99.44 5.87 --- 93.57
MW-10 3 - 18 18 99.43 10.02 --- 89.41
MW-11 3 - 18 18 99.60 11.02 --- 88.58
TW-1 45 - 50 50 100.11 5.95 --- 94.16
TW-2 70 - 75 75 99.89 5.87 --- 94.02

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of individual BTEX constituents, MTBE, naphthalene, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, TAA, C5-C8 aliphatics, C9-C12 aliphatics
and/or C9-C10 aromatics that exceeded the Maximum Allowable Concentrations (MACs) as specified in
T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1, MW-3, MW-6 and
TW-1. Concentrations of benzene that exceeded the Gross Contamination Level (GCL) were reported in
the ground water samples collected from MW-3 and TW-1. A summary of the analytical results for ground
water samples collected on August 13, 2020 is presented in Table 6. A Ground Water Quality Map based
on the August 2020 data is included as Figure 5. A complete report of laboratory analyses of the ground
water samples collected from the monitoring wells during the August 2020 sampling event has been
included as Appendix C. A summary of the current ground water analytical data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
3
Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 1,350 4,350 1,050 7,160 <13 210
MW-3 10,200 37,500 2,790 13,400 <310 <310
MW-4 FP FP FP FP FP FP
MW-6 43.5 2.4 0.33 J 43.2 42.9 0.34 J
MW-8 FP FP FP FP FP FP
MW-9 <0.13 0.14 J <0.13 <0.25 0.81 <0.13
MW-10 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-11 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
TW-1 9,480 14,500 830 3,820 508 <63
TW-2 <0.13 <0.13 <0.13 <0.25 3.2 <0.13

A baseline contaminant mass has yet been determined for the site because free product is present.
Therefore, the contaminant mass was not calculated.

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately two to eight feet below ground surface (bgs).
3.0 FREE PRODUCT REMOVAL
No free product has been removed as a part of ground water remediation. Free product thicknesses of
1.51 and 0.31 feet were measured in MW-4 and MW-8, respectively.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is in place at this time.
5.0 CONCLUSIONS
 On August 13, 2020, eight monitoring wells and two telescoping wells were gauged, purged
and/or sampled per NCDEQ guidelines. Ground water flow was generally to the northwest with
a horizontal gradient of approximately 0.04 feet per foot. The average vertical gradient between
paired wells MW-1/TW-1 and MW-1/TW-2 was approximately 0.02 feet per foot in the downward
direction.
 Free product thicknesses of 1.51 and 0.31 feet were measured in MW-4 and MW-8, respectively.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, n-propylbenzene, 1,2,4-
trimethylbenzene, 1,3,5-trimethylbenzene, TAA, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-
C10 aromatics that exceeded the MACs were reported in the ground water samples collected
from MW-1, MW-3, MW-6 and TW-1. Concentrations of benzene that exceeded the GCL were
reported in the ground water samples collected from MW-3 and TW-1.
 Based on this information, the risk classification for the site should remain high risk. It is
recommended that a free product evaluation should be conducted at the site. Semi-annual

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 8, 2020 New Dixie Mart #226
Project Manager: William Regenthal, PG GRI Project No. 4841
4
ground water monitoring should be continued. The next sampling event is tentatively scheduled
for February 2021.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of New Dixie Oil Corporation for specific application
to the referenced site in Wilson County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

FIGURES
Copyright (C) 2009 MyTopo, 2006-2018 TomTom
SCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 9.58° W
MN
Location: 035.7619960° N 077.9985590° WDate: 07/14/18
Scale: 1 inch = 2,000 ft.
Copyright (C) 2009 MyTopo
Figure 1
Site Location Map
New Dixie Mart #226
4917 Highway 264 West, Wilson, Wilson County, NC
Incident No. N/a
GRI Project No. 4841

SITE
2793-41-5379.000
2793-73-2477.000
2793-74-2138.000
2793-63-9773.0002793-73-2703.0002793-73-8175.000
27 93 -84 -3 11 9.0 00
2793-74-0138.0002793-73-2772.000WSW-3
WSW-2
WSW-1
I 95 RAMP RALEIGH ROAD PKWY
MERCK RDBLOOMERY RDCASWELL PLOLD MERCK RDEXPRESSWAY DR
RAMP I 95 BLOO
MERY S
WAMP

FIGURE 3:SITE VICINITY MAPNEWDIXIEMART#2264917RALEIGHROADPARKWAY WEST
WILSON, WILSON COUNTYNORTH CAROLINAINCIDENT NO. 46344
GRI NO. 4841
PREPARED BY:GEOLOGICAL RESOURCES, INC.JULY 19, 20181,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
500-FOOT RADIUS

0 300150
Feet
1 inch = 300 feet
LEGEND
Creek
Water Supply Well
Adjacent Properties and Well Owners
ncrivers
centerlines
nc_wilson_parcels_poly_2018_03_26
D
DDDD
D
DDDD
D
DDDD
D
DDDD
D
DDDD
D
DDDD
D
DDDD
D
DDDD

TABLES
UST ID Number 1-2 Facility ID Number
Owner or Operator?
Owner and Operator09/18/1995 - 06/26/2018
Address Telephone Number
1501 Marshall Street, Roanoke Rapids, NC 27870 252-537-4118
New Dixie Oil Corporation
TABLE 1
UST OWNER/OPERATOR INFORMATION
NEW DIXIE MART #226 (INCIDENT NO. 46344)
00-0-0000034646
Dates of Ownership / OperationName of Owner or Operator
Page 1 of 1
Date: 03/27/20 Facility ID #: 00-0-0000034646
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 12,000 09/18/95 Steel/Clad 8' x 31' 11"Flex Removed
(06/26/18)Yes
2 Gasoline Gasoline 12,000 09/18/95 Steel/Clad 8' x 31' 11"Flex Removed
(06/26/18)Yes
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
NEW DIXIE MART #226 (INCIDENT NO. 46344)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Facility ID #: 00-0-0000034646
Well ID.Parcel ID No.Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Connected to
Municipal Water
Yes/No
Distance from
source area of
release
(ft.)
WSW-1 2793-41-5379 Virginia Lamm Hayes 4957 Raleigh Road Parkway West
Wilson, North Carolina 27896
5105 Raleigh Road Parkway West
Wilson, North Carolina 27896
Potable
Active No ~960' W
WSW-2 2793-84-3119 Helen Daughtry Finch 4828 Raleigh Road Parkway West
Wilson, North Carolina 27896
4828 Raleigh Road Parkway West
Wilson, North Carolina 27896
Potable
Active No ~1,460' NE
WSW-3 2793-73-8175 Ralph R. and
Margie B. Bowen
4737 Old Merck Road
Wilson, NC 27893-9681
4737 Old Merck Road
Wilson, NC 27893-9681
Potable
Active No ~880' SE
Note:
• Water supply wells are keyed to Figure 3.
TABLE 3
WATER SUPPLY WELL INFORMATION
NEW DIXIE MART #226 (INCIDENT NO. 46344)
Date: 03/27/20
Page 1 of 1
Date: 3/27/20 Facility ID #: 00-0-0000034646
PIN Number Property Owner Name Mailing Address
2793-73-2703 (site)New Dixie Oil Corporation P.O. Box 779, Roanoke Rapids, NC
27870
2793-73-2772 Mike and Cynthia H.Glover 2740 W Hornes Church Road, Bailey,
NC 27807
2793-73-2477 Telam Partnership 624 Winter Breeze Court, Raleigh,
NC 27607
2793-63-9773 Plains Coastal, Properties LLC 3204 Bismarck Street, Greenville, NC
27834
2793-74-2138 Wilson County ABC Board P.O. Box 7290, Wilson, NC 27895
2793-74-0138 The Wilson Area Young Men's
Christian Association
3436 C Airport Boulevard, Wilson,
NC 27896
Note:
• Properties are keyed to Figure 3.
NEW DIXIE MART #226 (INCIDENT NO. 46344)
ADJACENT PROPERTY OWNER INFORMATION
TABLE 4
Page 1 of 1
Date: 08/19/20 Facility ID #: 00-0-0000034646
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation (ft.)Comments
07/26/18 8.74 ---91.26
03/07/19 2.72 ---97.28
06/19/19 5.82 ---94.18
08/13/20 5.28 ---94.72
03/07/19 6.48 ---93.38
06/19/19 9.02 ---90.84
03/07/19 3.97 ---95.76
06/19/19 6.65 ---93.08
08/13/20 6.33 ---93.40
03/07/19 3.98 ---96.75
06/19/19 6.73 ---94.00
08/13/20 7.29 1.51 94.74
MW-5 06/12/19 06/19/19 3 3-18 18 99.87 5.32 ---94.55
06/19/19 9.16 ---91.82
08/13/20 8.55 ---92.43
MW-7 06/12/19 06/19/19 3 3-18 18 99.41 10.03 ---89.38
06/19/19 5.22 ---94.21
08/13/20 4.98 0.31 94.72
06/19/19 6.22 ---93.22
08/13/20 5.87 ---93.57
06/19/19 10.65 ---88.78
08/13/20 10.02 ---89.41
06/19/19 11.71 ---87.89
08/13/20 11.02 ---88.58
MW-12 06/12/19 06/19/19 3 3-18 18 105.17 11.01 ---94.16
MW-13 02/05/20 02/14/20 5 5-20 20 102.25 6.50 ---95.75
06/19/19 6.78 ---93.33
08/13/20 5.95 ---94.16
02/14/20 5.64 ---94.25
08/13/20 5.87 ---94.02
Notes:
• ft BGS : feet below ground surface.
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
NEW DIXIE MART #226 (INCIDENT NO. 46344)
1007/26/18MW-1
99.86183-18303/06/19MW-2
100.002010-20
303/06/19MW-3
100.73183-18303/06/19MW-4
99.73183-18
MW-6
99.43183-183MW-8 06/12/19
100.98183-18306/12/19
MW-9
99.43183-18306/12/19MW-10
99.44183-18306/12/19
06/18/19TW-1
99.897570-757002/14/20TW-2
100.115045-5045
MW-11 99.60183-18306/12/19
Page 1 of 1
Date: 09/04/2020 Facility ID #: 00-0-0000034646
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 70 70 400 400 40 128 10 40 47 0.02 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 30,000 28,500 25,000 40,000 12,800 10,000 40,000 47,000 50 15,000 NE NE NE
07/26/18 13,300 23,900 2,200 11,300 326 329 70.5 J 221 J 1,580 418 NR NR NR NR NR <0.0094 34.6 14,100 <3,500 5,650 J
06/19/19 748 5,190 2,190 11,000 <13 533 134 450 3,380 867 NR NR NR NR NR NR NR NR NR NR
08/13/20 1,350 4,350 1,050 7,160 <13 210 41.7 J 180 1,970 546 1,040 <20 <200 <200 <13 NR NR 7,840 4,010 2,540
03/07/19 2,100 536 240 1,660 14.1 J 65.9 11.5 J 26.7 114 46.1 4,040 <10 <100 <100 <6.3 <0.0095 22.8 1,740 217 J 692
06/19/19 1,970 378 206 1,020 11.1 J 58.0 11.9 J 27.1 16.6 J 25.4 NR NR NR NR NR NR NR NR NR NR
03/07/19 11,400 28,000 2,820 14,500 <130 470 J <130 287 J 2,040 571 18,900 <200 <2,000 <2,000 <130 <0.0094 26.3 18,800 1,500 J 7,270
06/19/19 12,100 29,500 2,560 13,300 <130 372 J <130 236 J 1,780 500 NR NR NR NR NR NR NR NR NR NR
08/13/20 10,200 37,500 2,790 13,400 <310 <310 <310 <310 1,580 595 J 27,000 <500 <5,000 <5,000 <310 NR NR 184,000 317,000 132,000
03/07/19 23,300 47,400 3,270 16,500 <130 425 J <130 251 J 1,820 516 4,500 J <200 <2,000 <2,000 <130 <0.0094 128 33,800 <3,500 7,260
06/19/19 20,100 35,200 2,640 13,500 <130 325 J <130 198 J 1,550 427 J NR NR NR NR NR NR NR NR NR NR
08/13/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
MW-5 06/19/19 8.6 <0.13 <0.13 0.93 J <0.13 <0.13 <0.13 <0.13 0.43 J 0.58 NR NR NR NR NR NR NR NR NR NR
06/19/19 448 6.3 1.6 J 128 63.3 7.6 2.5 J <1.3 4.9 J 3.9 J NR NR NR NR NR NR NR NR NR NR
08/13/20 43.5 2.4 0.33 J 43.2 42.9 0.34 J 0.18 J <0.13 2.0 1.7 498 <0.20 <2.0 <2.0 <0.13 NR NR 120 <35 <35
MW-7 06/19/19 5.3 <0.13 <0.13 1.9 1.8 <0.13 <0.13 <0.13 0.17 J <0.13 NR NR NR NR NR NR NR NR NR NR
06/19/19 10,600 23,600 3,010 15,300 <63 470 116 J 319 2,480 650 NR NR NR NR NR NR NR NR NR NR
08/13/20 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/19/19 <0.13 0.32 J 0.18 J 0.84 J <0.13 <0.13 <0.13 <0.13 0.46 J 0.14 J NR NR NR NR NR NR NR NR NR NR
08/13/20 <0.13 0.14 J <0.13 <0.25 0.81 <0.13 <0.13 <0.13 <0.13 <0.13 in <0.20 <2.0 <2.0 <0.13 NR NR <35 <35 <35
06/19/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
08/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <0.20 <2.0 <2.0 <0.13 NR NR <35 <35 <35
06/19/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
08/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <0.20 <2.0 <2.0 <0.13 NR NR <35 <35 <35
MW-12 06/19/19 <0.13 0.17 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
MW-13 02/14/20 <0.13 0.40 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
06/19/19 1,870 66.3 13.6 J 82.1 307 28.5 6.3 J <6.3 9.8 J <6.3 NR NR NR NR NR NR NR NR NR NR
08/13/20 9,480 14,500 830 3,820 508 <63 <63 <63 296 106 J 3,260 J <100 <1,000 <1,000 <63 NR NR 8,240 735 E 1,320 tert-Amyl methyl ether (TAME)Contaminant of Concern

MW-2
GCL (μg/l)MTBENaphthaleneIsopropylbenzeneBenzeneTolueneEthylbenzeneXylenesMAC (μg/l)
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NEW DIXIE MART #226 (INCIDENT NO. 46344)
EPA Method 6200B MADEP Method VPH
1,2-Dibromoethane(EDB)LeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,3,5-Trimethylbenzenetert-Butyl formate(TBF)Ethyl tert-butyl ether (ETBE)tert-Amyl alcohol(TAA)1,2,4-TrimethylbenzeneAnalytical Method
tert-Butyl alcohol(TBA)TW-1
MW-11
MW-10
MW-9
MW-8
MW-6
MW-4
MW-3
MW-1
Page 1 of 2
Date: 09/04/2020 Facility ID #: 00-0-0000034646
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 70 70 400 400 40 128 10 40 47 0.02 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 30,000 28,500 25,000 40,000 12,800 10,000 40,000 47,000 50 15,000 NE NE NEtert-Amyl methyl ether (TAME)Contaminant of Concern

GCL (μg/l)MTBENaphthaleneIsopropylbenzeneBenzeneTolueneEthylbenzeneXylenesMAC (μg/l)
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NEW DIXIE MART #226 (INCIDENT NO. 46344)
EPA Method 6200B MADEP Method VPH
1,2-Dibromoethane(EDB)LeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,3,5-Trimethylbenzenetert-Butyl formate(TBF)Ethyl tert-butyl ether (ETBE)tert-Amyl alcohol(TAA)1,2,4-TrimethylbenzeneAnalytical Method
tert-Butyl alcohol(TBA)02/14/20 979 41.1 8.3 J 28.9 J 179 10.3 J 3.5 J <3.1 <3.1 <3.1 NR NR NR NR NR NR NR NR NR NR
08/13/20 <0.13 <0.13 <0.13 <0.25 3.2 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <0.20 <2.0 <2.0 <0.13 NR NR <35 <35 <35
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum Allowable Concentrations as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established.
• NR: Not Requested.
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• Concentrations in italics indicate the GCLs were below the report concentrations.
• Refer to laboratory report for additional detected constituents.
TW-2
Page 2 of 2

APPENDICES

APPENDIX A
State Correspondence

APPENDIX B
Laboratory Report – Ground Water Samples
08/24/20
Technical Report for
GRI (Geological Resources Inc.)
New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
4841
SGS Job Number: FA77821
Sampling Date: 08/13/20
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 08/24/20
e-Hardcopy 2.0
Automated Report
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SGS is the sole authority for authorizing edits or modifications to this document.
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FA77821
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA77821-1: MW-3 ........................................................................................................8
3.2: FA77821-2: MW-9 ........................................................................................................12
3.3: FA77821-3: MW-10 ......................................................................................................16
3.4: FA77821-4: MW-11 ......................................................................................................20
3.5: FA77821-5: MW-6 ........................................................................................................24
3.6: FA77821-6: TW-2 .........................................................................................................28
3.7: FA77821-7: TW-1 .........................................................................................................32
3.8: FA77821-8: MW-1 ........................................................................................................36
Section 4: Misc. Forms ............................................................................................................40
4.1: Chain of Custody ...........................................................................................................41
Section 5: MS Volatiles - QC Data Summaries .....................................................................43
5.1: Method Blank Summary ................................................................................................44
5.2: Blank Spike Summary ...................................................................................................53
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................62
Section 6: GC Volatiles - QC Data Summaries .....................................................................71
6.1: Method Blank Summary ................................................................................................72
6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................76
6.3: Matrix Spike Summary ..................................................................................................80
6.4: Duplicate Summary .......................................................................................................83 1234562 of 85
FA77821
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA77821
New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Project No: 4841
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA77821-1 08/13/20 10:32 ME 08/14/20 AQ Ground Water MW-3
FA77821-2 08/13/20 10:44 ME 08/14/20 AQ Ground Water MW-9
FA77821-3 08/13/20 10:55 ME 08/14/20 AQ Ground Water MW-10
FA77821-4 08/13/20 11:08 ME 08/14/20 AQ Ground Water MW-11
FA77821-5 08/13/20 11:23 ME 08/14/20 AQ Ground Water MW-6
FA77821-6 08/13/20 12:20 ME 08/14/20 AQ Ground Water TW-2
FA77821-7 08/13/20 12:36 ME 08/14/20 AQ Ground Water TW-1
FA77821-8 08/13/20 12:49 ME 08/14/20 AQ Ground Water MW-1
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Summary of Hits Page 1 of 3
Job Number:FA77821
Account:GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Collected:08/13/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA77821-1 MW-3
Benzene a 10200 1300 310 ug/l SM 6200B
Ethylbenzene a 2790 1300 310 ug/l SM 6200B
Tert-Amyl Alcohol a 27000 25000 5000 ug/l SM 6200B
Toluene a 37500 1300 310 ug/l SM 6200B
1,2,4-Trimethylbenzene a 1580 1300 310 ug/l SM 6200B
1,3,5-Trimethylbenzene a 595 J 1300 310 ug/l SM 6200B
m,p-Xylene a 9460 2500 310 ug/l SM 6200B
o-Xylene a 3950 1300 310 ug/l SM 6200B
Xylene (total) a 13400 3800 630 ug/l SM 6200B
Benzene 11600 500 500 ug/l MADEP VPH REV 2.1
Ethylbenzene 11500 1000 500 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether 2630 1000 500 ug/l MADEP VPH REV 2.1
Naphthalene 28600 2500 1500 ug/l MADEP VPH REV 2.1
Toluene 38000 1000 500 ug/l MADEP VPH REV 2.1
m,p-Xylene 39100 2000 1000 ug/l MADEP VPH REV 2.1
o-Xylene 23700 1000 500 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)236000 50000 18000 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.)399000 100000 35000 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)132000 50000 18000 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics 184000 50000 18000 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics 317000 100000 35000 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics 132000 50000 18000 ug/l MADEP VPH REV 2.1
FA77821-2 MW-9
Methyl Tert Butyl Ether 0.81 0.50 0.13 ug/l SM 6200B
Toluene 0.14 J 0.50 0.13 ug/l SM 6200B
FA77821-3 MW-10
No hits reported in this sample.
FA77821-4 MW-11
Chloroform b 0.19 J 0.50 0.13 ug/l SM 6200B
FA77821-5 MW-6
Benzene 43.5 1.0 0.25 ug/l SM 6200B
Di-Isopropyl Ether 1.2 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.33 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.18 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 42.9 1.0 0.25 ug/l SM 6200B
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Summary of Hits Page 2 of 3
Job Number:FA77821
Account:GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Collected:08/13/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 0.34 J 0.50 0.13 ug/l SM 6200B
Tert-Amyl Alcohol 498 20 4.0 ug/l SM 6200B
Toluene 2.4 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2.0 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.7 0.50 0.13 ug/l SM 6200B
m,p-Xylene 7.1 1.0 0.13 ug/l SM 6200B
o-Xylene 39.0 1.0 0.25 ug/l SM 6200B
Xylene (total)43.2 3.0 0.50 ug/l SM 6200B
Benzene 38.7 1.0 1.0 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether 40.6 2.0 1.0 ug/l MADEP VPH REV 2.1
Toluene 1.5 J 2.0 1.0 ug/l MADEP VPH REV 2.1
m,p-Xylene 6.2 4.0 2.0 ug/l MADEP VPH REV 2.1
o-Xylene 34.8 2.0 1.0 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)201 100 35 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.)49.0 J 100 35 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics 120 100 35 ug/l MADEP VPH REV 2.1
FA77821-6 TW-2
Di-Isopropyl Ether b 0.16 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether b 3.2 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 3.0 2.0 1.0 ug/l MADEP VPH REV 2.1
FA77821-7 TW-1
Benzene 9480 250 63 ug/l SM 6200B
Ethylbenzene 830 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether 508 250 63 ug/l SM 6200B
Tert-Amyl Alcohol 3260 J 5000 1000 ug/l SM 6200B
Toluene 14500 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 296 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 106 J 250 63 ug/l SM 6200B
m,p-Xylene 2600 500 63 ug/l SM 6200B
o-Xylene 1210 250 63 ug/l SM 6200B
Xylene (total)3820 750 130 ug/l SM 6200B
Benzene 7060 50 50 ug/l MADEP VPH REV 2.1
Ethylbenzene 743 10 5.0 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether 543 10 5.0 ug/l MADEP VPH REV 2.1
Naphthalene 57.9 25 15 ug/l MADEP VPH REV 2.1
Toluene 9080 100 50 ug/l MADEP VPH REV 2.1
m,p-Xylene 2250 20 10 ug/l MADEP VPH REV 2.1
o-Xylene 1260 10 5.0 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)24900 5000 1800 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.)3630 1000 350 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)1320 500 180 ug/l MADEP VPH REV 2.1
5 of 85
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Summary of Hits Page 3 of 3
Job Number:FA77821
Account:GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Collected:08/13/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
C5- C8 Aliphatics 8240 5000 1800 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics 735 E 500 180 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics 1320 500 180 ug/l MADEP VPH REV 2.1
FA77821-8 MW-1
Benzene 1350 50 13 ug/l SM 6200B
n-Butylbenzene 18.0 J 50 13 ug/l SM 6200B
Ethylbenzene 1050 50 13 ug/l SM 6200B
Isopropylbenzene 41.7 J 50 13 ug/l SM 6200B
Naphthalene 210 50 13 ug/l SM 6200B
n-Propylbenzene 180 50 13 ug/l SM 6200B
Tert-Amyl Alcohol 1040 1000 200 ug/l SM 6200B
Toluene 4350 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1970 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 546 50 13 ug/l SM 6200B
m,p-Xylene 4670 100 13 ug/l SM 6200B
o-Xylene 2490 50 13 ug/l SM 6200B
Xylene (total)7160 150 25 ug/l SM 6200B
Benzene c 1100 10 10 ug/l MADEP VPH REV 2.1
Ethylbenzene c 838 20 10 ug/l MADEP VPH REV 2.1
Methyl Tert Butyl Ether c 290 2.0 1.0 ug/l MADEP VPH REV 2.1
Naphthalene c 245 5.0 3.0 ug/l MADEP VPH REV 2.1
Toluene c 2910 20 10 ug/l MADEP VPH REV 2.1
m,p-Xylene c 3150 40 20 ug/l MADEP VPH REV 2.1
o-Xylene c 1770 20 10 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.) c 12100 2000 700 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.) c 9840 2000 700 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.) c 2540 1000 350 ug/l MADEP VPH REV 2.1
C5- C8 Aliphatics c 7840 2000 700 ug/l MADEP VPH REV 2.1
C9- C12 Aliphatics c 4010 2000 700 ug/l MADEP VPH REV 2.1
C9- C10 Aromatics c 2540 1000 350 ug/l MADEP VPH REV 2.1
(a) Sample vial(s) contained bubbles greater than 6mm; reported results are considered minimum values.
(b) Associated internal standard response outside control limits. Confirmed by reanalysis.
(c) Sample vial(s) contained significant headspace; reported results are considered minimum values.
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Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 85
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SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA77821-1 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0223119.D 2500 08/19/20 10:50 AB n/a n/a VA2768
Run #2 b A0223092.D 10000 08/18/20 13:36 AB n/a n/a VA2767
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 10200 1300 310 ug/l
108-86-1 Bromobenzene ND 1300 310 ug/l
74-97-5 Bromochloromethane ND 1300 310 ug/l
75-27-4 Bromodichloromethane ND 1300 310 ug/l
75-25-2 Bromoform ND 1300 310 ug/l
104-51-8 n-Butylbenzene ND 1300 310 ug/l
135-98-8 sec-Butylbenzene ND 1300 310 ug/l
98-06-6 tert-Butylbenzene ND 1300 310 ug/l
56-23-5 Carbon Tetrachloride ND 1300 310 ug/l
108-90-7 Chlorobenzene ND 1300 310 ug/l
75-00-3 Chloroethane ND 1300 500 ug/l
67-66-3 Chloroform ND 1300 310 ug/l
95-49-8 o-Chlorotoluene ND 1300 310 ug/l
106-43-4 p-Chlorotoluene ND 1300 310 ug/l
124-48-1 Dibromochloromethane ND 1300 310 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1300 620 ug/l
106-93-4 1,2-Dibromoethane ND 1300 310 ug/l
75-71-8 Dichlorodifluoromethane ND 1300 500 ug/l
95-50-1 1,2-Dichlorobenzene ND 1300 310 ug/l
541-73-1 1,3-Dichlorobenzene ND 1300 310 ug/l
106-46-7 1,4-Dichlorobenzene ND 1300 310 ug/l
75-34-3 1,1-Dichloroethane ND 1300 310 ug/l
107-06-2 1,2-Dichloroethane ND 1300 310 ug/l
75-35-4 1,1-Dichloroethylene ND 1300 310 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1300 310 ug/l
156-60-5 trans-1,2-Dichloroethylene c ND 1300 310 ug/l
78-87-5 1,2-Dichloropropane ND 1300 310 ug/l
142-28-9 1,3-Dichloropropane ND 1300 310 ug/l
594-20-7 2,2-Dichloropropane c ND 1300 310 ug/l
563-58-6 1,1-Dichloropropene ND 1300 310 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1300 310 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1300 310 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA7782133.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA77821-1 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 1300 310 ug/l
100-41-4 Ethylbenzene 2790 1300 310 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 1300 310 ug/l
87-68-3 Hexachlorobutadiene ND 1300 310 ug/l
98-82-8 Isopropylbenzene ND 1300 310 ug/l
99-87-6 p-Isopropyltoluene ND 1300 310 ug/l
74-83-9 Methyl Bromide ND 1300 500 ug/l
74-87-3 Methyl Chloride ND 1300 500 ug/l
74-95-3 Methylene Bromide ND 1300 310 ug/l
75-09-2 Methylene Chloride ND 5000 2500 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1300 310 ug/l
91-20-3 Naphthalene ND 1300 310 ug/l
103-65-1 n-Propylbenzene ND 1300 310 ug/l
100-42-5 Styrene ND 1300 310 ug/l
75-85-4 Tert-Amyl Alcohol 27000 25000 5000 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 2500 500 ug/l
75-65-0 Tert-Butyl Alcohol d ND 25000 5000 ug/l
762-75-4 Tert-Butyl Formate e ND 25000 5000 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1300 310 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1300 310 ug/l
127-18-4 Tetrachloroethylene ND 1300 310 ug/l
108-88-3 Toluene 37500 1300 310 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1300 310 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1300 310 ug/l
71-55-6 1,1,1-Trichloroethane ND 1300 310 ug/l
79-00-5 1,1,2-Trichloroethane ND 1300 310 ug/l
79-01-6 Trichloroethylene ND 1300 310 ug/l
75-69-4 Trichlorofluoromethane ND 1300 500 ug/l
96-18-4 1,2,3-Trichloropropane ND 1300 310 ug/l
95-63-6 1,2,4-Trimethylbenzene 1580 1300 310 ug/l
108-67-8 1,3,5-Trimethylbenzene 595 1300 310 ug/l J
75-01-4 Vinyl Chloride ND 1300 310 ug/l
m,p-Xylene 9460 2500 310 ug/l
95-47-6 o-Xylene 3950 1300 310 ug/l
1330-20-7 Xylene (total)13400 3800 630 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%110%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%116%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA77821-1 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 105%103%70-130%
460-00-4 4-Bromofluorobenzene 109%107%70-130%
(a) Sample vial(s) contained bubbles greater than 6mm; reported results are considered minimum values.
(b) Confirmation run.
(c) Associated CCV outside of control limits high, sample was ND.
(d) Associated CCV and BS outside control limits high.
(e) Associated BS recovery outside control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 85
FA7782133.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA77821-1 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3439.D 500 08/20/20 06:01 EG n/a n/a G1S71
Run #2 1S3419.D 1000 08/19/20 20:41 EG n/a n/a G1S71
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 11600 500 500 ug/l
100-41-4 Ethylbenzene 11500 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether 2630 1000 500 ug/l
91-20-3 Naphthalene 28600 2500 1500 ug/l
108-88-3 Toluene 38000 1000 500 ug/l
m,p-Xylene 39100 2000 1000 ug/l
95-47-6 o-Xylene 23700 1000 500 ug/l
C5- C8 Aliphatics (Unadj.)236000 50000 18000 ug/l
C9- C12 Aliphatics (Unadj.)399000 a 100000 35000 ug/l
C9- C10 Aromatics (Unadj.)132000 50000 18000 ug/l
C5- C8 Aliphatics 184000 50000 18000 ug/l
C9- C12 Aliphatics 317000 a 100000 35000 ug/l
C9- C10 Aromatics 132000 50000 18000 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 142% b 113%70-130%
460-00-4 BFB 104%99%70-130%
(a) Result is from Run# 2
(b) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 85
FA7782133.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-9
Lab Sample ID:FA77821-2 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0223083.D 1 08/18/20 10:12 AB n/a n/a VA2767
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 85
FA7782133.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-9
Lab Sample ID:FA77821-2 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.81 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.14 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 85
FA7782133.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-9
Lab Sample ID:FA77821-2 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 110%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 85
FA7782133.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-9
Lab Sample ID:FA77821-2 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3420.D 1 08/19/20 21:09 EG n/a n/a G1S71
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 101%70-130%
460-00-4 BFB 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 85
FA7782133.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-10
Lab Sample ID:FA77821-3 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0223085.D 1 08/18/20 10:58 AB n/a n/a VA2767
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 85
FA7782133.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-10
Lab Sample ID:FA77821-3 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 85
FA7782133.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-10
Lab Sample ID:FA77821-3 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 109%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 85
FA7782133.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-10
Lab Sample ID:FA77821-3 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3421.D 1 08/19/20 21:37 EG n/a n/a G1S71
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 102%70-130%
460-00-4 BFB 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 85
FA7782133.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-11
Lab Sample ID:FA77821-4 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0223057.D 1 08/17/20 11:53 AB n/a n/a VA2766
Run #2 b A0223086.D 1 08/18/20 11:20 AB n/a n/a VA2767
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane c ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.19 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 85
FA7782133.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-11
Lab Sample ID:FA77821-4 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol d ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%112%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 85
FA7782133.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-11
Lab Sample ID:FA77821-4 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 94%94%70-130%
460-00-4 4-Bromofluorobenzene 106%107%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Confirmation run for internal standard areas.
(c) Associated ECC outside control limits high.
(d) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 85
FA7782133.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-11
Lab Sample ID:FA77821-4 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3422.D 1 08/19/20 22:05 EG n/a n/a G1S71
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 97%70-130%
460-00-4 BFB 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 85
FA7782133.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-6
Lab Sample ID:FA77821-5 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0223058.D 1 08/17/20 12:15 AB n/a n/a VA2766
Run #2 A0223098.D 2 08/18/20 15:51 AB n/a n/a VA2767
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 43.5 a 1.0 0.25 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane b ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 85
FA7782133.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-6
Lab Sample ID:FA77821-5 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.2 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.33 0.50 0.13 ug/l J
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.18 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 42.9 a 1.0 0.25 ug/l
91-20-3 Naphthalene 0.34 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol 498 a 20 4.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol c ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 2.4 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2.0 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.7 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 7.1 1.0 0.13 ug/l
95-47-6 o-Xylene 39.0 a 1.0 0.25 ug/l
1330-20-7 Xylene (total)43.2 a 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 85
FA7782133.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-6
Lab Sample ID:FA77821-5 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 112%110%70-130%
460-00-4 4-Bromofluorobenzene 105%111%70-130%
(a) Result is from Run# 2
(b) Associated ECC outside control limits high.
(c) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 85
FA7782133.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-6
Lab Sample ID:FA77821-5 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3427.D 1 08/20/20 00:26 EG n/a n/a G1S71
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 38.7 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 40.6 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene 1.5 2.0 1.0 ug/l J
m,p-Xylene 6.2 4.0 2.0 ug/l
95-47-6 o-Xylene 34.8 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)201 100 35 ug/l
C9- C12 Aliphatics (Unadj.)49.0 100 35 ug/l J
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics 120 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 99%70-130%
460-00-4 BFB 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 85
FA7782133.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:TW-2
Lab Sample ID:FA77821-6 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0223087.D 1 08/18/20 11:43 AB n/a n/a VA2767
Run #2 b A0223059.D 1 08/17/20 12:38 AB n/a n/a VA2766
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 85
FA7782133.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:TW-2
Lab Sample ID:FA77821-6 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.16 0.50 0.13 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.2 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol c ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%107%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%110%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 85
FA7782133.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:TW-2
Lab Sample ID:FA77821-6 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 104%104%70-130%
460-00-4 4-Bromofluorobenzene 110%109%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
(b) Confirmation run for internal standard areas.
(c) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 85
FA7782133.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TW-2
Lab Sample ID:FA77821-6 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3428.D 1 08/20/20 00:54 EG n/a n/a G1S71
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.0 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 96%70-130%
460-00-4 BFB 94%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 85
FA7782133.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:TW-1
Lab Sample ID:FA77821-7 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0223070.D 500 08/17/20 16:48 AB n/a n/a VA2766
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 9480 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane a ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane ND 250 63 ug/l
75-71-8 Dichlorodifluoromethane ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane ND 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:TW-1
Lab Sample ID:FA77821-7 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
100-41-4 Ethylbenzene 830 250 63 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene ND 250 63 ug/l
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether 508 250 63 ug/l
91-20-3 Naphthalene ND 250 63 ug/l
103-65-1 n-Propylbenzene ND 250 63 ug/l
100-42-5 Styrene ND 250 63 ug/l
75-85-4 Tert-Amyl Alcohol 3260 5000 1000 ug/l J
994-05-8 Tert-Amyl Methyl Ether ND 500 100 ug/l
75-65-0 Tert-Butyl Alcohol b ND 5000 1000 ug/l
762-75-4 Tert-Butyl Formate ND 5000 1000 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 14500 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 296 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 106 250 63 ug/l J
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 2600 500 63 ug/l
95-47-6 o-Xylene 1210 250 63 ug/l
1330-20-7 Xylene (total)3820 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:TW-1
Lab Sample ID:FA77821-7 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 111%70-130%
(a) Associated ECC outside control limits high.
(b) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:TW-1
Lab Sample ID:FA77821-7 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S3490.D 5 08/22/20 20:38 EG n/a n/a G1S74
Run #2 1S3469.D 10 08/21/20 19:15 EG n/a n/a G1S73
Run #3 1S3466.D 50 08/21/20 17:50 EG n/a n/a G1S73
Run #4 a 1S3492.D 2 08/22/20 21:34 EG n/a n/a G1S74
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
Run #3 5.0 ml
Run #4 5.0 ml
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 7060 b 50 50 ug/l
100-41-4 Ethylbenzene 743 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 543 10 5.0 ug/l
91-20-3 Naphthalene 57.9 25 15 ug/l
108-88-3 Toluene 9080 b 100 50 ug/l
m,p-Xylene 2250 20 10 ug/l
95-47-6 o-Xylene 1260 10 5.0 ug/l
C5- C8 Aliphatics (Unadj.)24900 b 5000 1800 ug/l
C9- C12 Aliphatics (Unadj.)3630 c 1000 350 ug/l
C9- C10 Aromatics (Unadj.)1320 500 180 ug/l
C5- C8 Aliphatics 8240 b 5000 1800 ug/l
C9- C12 Aliphatics 735 500 180 ug/l E
C9- C10 Aromatics 1320 500 180 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
460-00-4 BFB 89%95%97%70-130%
460-00-4 BFB 88%94%95%70-130%
(a) Confirmation run.
(b) Result is from Run# 3
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA77821-8 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0223099.D 100 08/18/20 16:15 AB n/a n/a VA2767
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1350 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene 18.0 50 13 ug/l J
135-98-8 sec-Butylbenzene ND 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene ND 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 25 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA77821-8 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 1050 50 13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 41.7 50 13 ug/l J
99-87-6 p-Isopropyltoluene ND 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 50 13 ug/l
91-20-3 Naphthalene 210 50 13 ug/l
103-65-1 n-Propylbenzene 180 50 13 ug/l
100-42-5 Styrene ND 50 13 ug/l
75-85-4 Tert-Amyl Alcohol 1040 1000 200 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 100 20 ug/l
75-65-0 Tert-Butyl Alcohol a ND 1000 200 ug/l
762-75-4 Tert-Butyl Formate ND 1000 200 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 4350 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1970 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 546 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 4670 100 13 ug/l
95-47-6 o-Xylene 2490 50 13 ug/l
1330-20-7 Xylene (total)7160 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA77821-8 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:SM 6200B Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA77821-8 Date Sampled:08/13/20
Matrix:AQ - Ground Water Date Received:08/14/20
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 1S3450.D 1 08/20/20 23:43 EG n/a n/a G1S72
Run #2 a 1S3471.D 10 08/21/20 20:11 EG n/a n/a G1S73
Run #3 a 1S3467.D 20 08/21/20 18:18 EG n/a n/a G1S73
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
Run #3 5.0 ml
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1100 b 10 10 ug/l
100-41-4 Ethylbenzene 838 b 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 290 2.0 1.0 ug/l
91-20-3 Naphthalene 245 5.0 3.0 ug/l
108-88-3 Toluene 2910 b 20 10 ug/l
m,p-Xylene 3150 b 40 20 ug/l
95-47-6 o-Xylene 1770 b 20 10 ug/l
C5- C8 Aliphatics (Unadj.)12100 c 2000 700 ug/l
C9- C12 Aliphatics (Unadj.)9840 c 2000 700 ug/l
C9- C10 Aromatics (Unadj.)2540 b 1000 350 ug/l
C5- C8 Aliphatics 7840 c 2000 700 ug/l
C9- C12 Aliphatics 4010 c 2000 700 ug/l
C9- C10 Aromatics 2540 b 1000 350 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
460-00-4 BFB 176% d 81%78%70-130%
460-00-4 BFB 117%79%76%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Result is from Run# 2
(c) Result is from Run# 3
(d) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
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FA778214
FA77821: Chain of Custody
Page 1 of 2
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FA7782144.1
Job Number:FA77821 Client:GEOLOGICAL RESOURCES, INC.
Date / Time Received:8/14/2020 10:00:00 AM Delivery Method:FEDEX
Project:NEW DIXIE MART #226
Airbill #'s:100963778373
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (0.4);
Cooler 1: (0.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:BRYANG Date:Date:8/14/2020 10:00:00 A
FA77821: Chain of Custody
Page 2 of 2
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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FA778215
Method Blank Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-MB A0223051.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
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FA7782155.1.1
Method Blank Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-MB A0223051.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
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FA7782155.1.1
Method Blank Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-MB A0223051.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 109%70-130%
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FA7782155.1.1
Method Blank Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-MB A0223082.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
47 of 85
FA7782155.1.2
Method Blank Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-MB A0223082.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
48 of 85
FA7782155.1.2
Method Blank Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-MB A0223082.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 112%70-130%
49 of 85
FA7782155.1.2
Method Blank Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-MB A0223116.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
50 of 85
FA7782155.1.3
Method Blank Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-MB A0223116.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l
994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l
75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l
762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%70-130%
51 of 85
FA7782155.1.3
Method Blank Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-MB A0223116.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 109%70-130%
52 of 85
FA7782155.1.3
Blank Spike Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-BS A0223049.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.4 94 70-130
108-86-1 Bromobenzene 10 9.6 96 70-130
74-97-5 Bromochloromethane 10 9.4 94 70-130
75-27-4 Bromodichloromethane 10 9.5 95 70-130
75-25-2 Bromoform 10 8.8 88 70-130
104-51-8 n-Butylbenzene 10 9.1 91 70-130
135-98-8 sec-Butylbenzene 10 9.6 96 70-130
98-06-6 tert-Butylbenzene 10 9.2 92 70-130
56-23-5 Carbon Tetrachloride 10 10.2 102 70-130
108-90-7 Chlorobenzene 10 9.4 94 70-130
75-00-3 Chloroethane 10 9.3 93 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 9.2 92 70-130
124-48-1 Dibromochloromethane 10 9.1 91 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 9.6 96 70-130
75-71-8 Dichlorodifluoromethane 10 9.1 91 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130
75-34-3 1,1-Dichloroethane 10 9.7 97 70-130
107-06-2 1,2-Dichloroethane 10 9.5 95 70-130
75-35-4 1,1-Dichloroethylene 10 10.1 101 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.0 90 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.2 102 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 9.4 94 70-130
594-20-7 2,2-Dichloropropane 10 10.9 109 70-130
563-58-6 1,1-Dichloropropene 10 9.8 98 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130
100-41-4 Ethylbenzene 10 9.4 94 70-130
637-92-3 Ethyl Tert Butyl Ether 10 8.4 84 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
* = Outside of Control Limits.
53 of 85
FA7782155.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-BS A0223049.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 9.2 92 70-130
99-87-6 p-Isopropyltoluene 10 9.3 93 70-130
74-83-9 Methyl Bromide 10 9.3 93 60-140
74-87-3 Methyl Chloride 10 10.2 102 60-140
74-95-3 Methylene Bromide 10 9.1 91 70-130
75-09-2 Methylene Chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.2 102 70-130
91-20-3 Naphthalene 10 8.0 80 70-130
103-65-1 n-Propylbenzene 10 9.4 94 70-130
100-42-5 Styrene 10 8.5 85 70-130
75-85-4 Tert-Amyl Alcohol 100 104 104 70-130
994-05-8 Tert-Amyl Methyl Ether 10 8.9 89 70-130
75-65-0 Tert-Butyl Alcohol 100 138 138*70-130
762-75-4 Tert-Butyl Formate 100 71.0 71 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.3 93 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.2 92 70-130
127-18-4 Tetrachloroethylene 10 9.9 99 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.8 88 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.5 85 70-130
71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130
79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130
79-01-6 Trichloroethylene 10 9.8 98 70-130
75-69-4 Trichlorofluoromethane 10 10.6 106 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.9 89 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.1 91 70-130
75-01-4 Vinyl Chloride 10 10.1 101 60-140
m,p-Xylene 20 18.3 92 70-130
95-47-6 o-Xylene 10 8.8 88 70-130
1330-20-7 Xylene (total)30 27.2 91 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
* = Outside of Control Limits.
54 of 85
FA7782155.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2766-BS A0223049.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
* = Outside of Control Limits.
55 of 85
FA7782155.2.1
Blank Spike Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-BS A0223080.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 10 100 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 9.8 98 70-130
135-98-8 sec-Butylbenzene 10 10.3 103 70-130
98-06-6 tert-Butylbenzene 10 9.9 99 70-130
56-23-5 Carbon Tetrachloride 10 11.0 110 70-130
108-90-7 Chlorobenzene 10 9.9 99 70-130
75-00-3 Chloroethane 10 9.9 99 60-140
67-66-3 Chloroform 10 10.1 101 70-130
95-49-8 o-Chlorotoluene 10 9.8 98 70-130
106-43-4 p-Chlorotoluene 10 9.8 98 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10 100 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 9.3 93 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.5 105 70-130
106-46-7 1,4-Dichlorobenzene 10 9.7 97 70-130
75-34-3 1,1-Dichloroethane 10 10.4 104 70-130
107-06-2 1,2-Dichloroethane 10 10.2 102 70-130
75-35-4 1,1-Dichloroethylene 10 10.8 108 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.0 110 70-130
78-87-5 1,2-Dichloropropane 10 9.9 99 70-130
142-28-9 1,3-Dichloropropane 10 10.0 100 70-130
594-20-7 2,2-Dichloropropane 10 11.9 119 70-130
563-58-6 1,1-Dichloropropene 10 10.6 106 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.6 96 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
637-92-3 Ethyl Tert Butyl Ether 10 9.0 90 70-130
87-68-3 Hexachlorobutadiene 10 11.0 110 70-130
* = Outside of Control Limits.
56 of 85
FA7782155.2.2
Blank Spike Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-BS A0223080.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 9.8 98 70-130
99-87-6 p-Isopropyltoluene 10 9.9 99 70-130
74-83-9 Methyl Bromide 10 9.9 99 60-140
74-87-3 Methyl Chloride 10 11.4 114 60-140
74-95-3 Methylene Bromide 10 9.7 97 70-130
75-09-2 Methylene Chloride 10 9.5 95 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 8.7 87 70-130
103-65-1 n-Propylbenzene 10 10.0 100 70-130
100-42-5 Styrene 10 9.2 92 70-130
75-85-4 Tert-Amyl Alcohol 100 113 113 70-130
994-05-8 Tert-Amyl Methyl Ether 10 9.6 96 70-130
75-65-0 Tert-Butyl Alcohol 100 151 151*70-130
762-75-4 Tert-Butyl Formate 100 70.8 71 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130
127-18-4 Tetrachloroethylene 10 10.5 105 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.0 90 70-130
71-55-6 1,1,1-Trichloroethane 10 10.8 108 70-130
79-00-5 1,1,2-Trichloroethane 10 10.0 100 70-130
79-01-6 Trichloroethylene 10 10.5 105 70-130
75-69-4 Trichlorofluoromethane 10 11.0 110 60-140
96-18-4 1,2,3-Trichloropropane 10 9.6 96 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.4 94 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.8 98 70-130
75-01-4 Vinyl Chloride 10 10.5 105 60-140
m,p-Xylene 20 19.5 98 70-130
95-47-6 o-Xylene 10 9.6 96 70-130
1330-20-7 Xylene (total)30 29.0 97 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
* = Outside of Control Limits.
57 of 85
FA7782155.2.2
Blank Spike Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2767-BS A0223080.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
* = Outside of Control Limits.
58 of 85
FA7782155.2.2
Blank Spike Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-BS A0223114.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 10.0 100 70-130
74-97-5 Bromochloromethane 10 10.1 101 70-130
75-27-4 Bromodichloromethane 10 10.3 103 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 9.7 97 70-130
135-98-8 sec-Butylbenzene 10 10.1 101 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
56-23-5 Carbon Tetrachloride 10 11.1 111 70-130
108-90-7 Chlorobenzene 10 10 100 70-130
75-00-3 Chloroethane 10 9.9 99 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.7 97 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 9.4 94 60-140
95-50-1 1,2-Dichlorobenzene 10 10 100 70-130
541-73-1 1,3-Dichlorobenzene 10 10.5 105 70-130
106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130
75-34-3 1,1-Dichloroethane 10 10.8 108 70-130
107-06-2 1,2-Dichloroethane 10 10.5 105 70-130
75-35-4 1,1-Dichloroethylene 10 11.3 113 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.2 112 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 10.1 101 70-130
594-20-7 2,2-Dichloropropane 10 11.8 118 70-130
563-58-6 1,1-Dichloropropene 10 10.6 106 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.6 96 70-130
108-20-3 Di-Isopropyl Ether 10 10.3 103 70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
637-92-3 Ethyl Tert Butyl Ether 10 8.6 86 70-130
87-68-3 Hexachlorobutadiene 10 11.0 110 70-130
* = Outside of Control Limits.
59 of 85
FA7782155.2.3
Blank Spike Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-BS A0223114.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 9.6 96 70-130
99-87-6 p-Isopropyltoluene 10 9.6 96 70-130
74-83-9 Methyl Bromide 10 9.7 97 60-140
74-87-3 Methyl Chloride 10 11.3 113 60-140
74-95-3 Methylene Bromide 10 10.0 100 70-130
75-09-2 Methylene Chloride 10 10.2 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.8 108 70-130
91-20-3 Naphthalene 10 8.5 85 70-130
103-65-1 n-Propylbenzene 10 9.8 98 70-130
100-42-5 Styrene 10 9.0 90 70-130
75-85-4 Tert-Amyl Alcohol 100 111 111 70-130
994-05-8 Tert-Amyl Methyl Ether 10 9.1 91 70-130
75-65-0 Tert-Butyl Alcohol 100 153 153*70-130
762-75-4 Tert-Butyl Formate 100 65.3 65* a 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.9 89 70-130
71-55-6 1,1,1-Trichloroethane 10 11.0 110 70-130
79-00-5 1,1,2-Trichloroethane 10 10.3 103 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 11.2 112 60-140
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.3 93 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130
75-01-4 Vinyl Chloride 10 10.3 103 60-140
m,p-Xylene 20 19.2 96 70-130
95-47-6 o-Xylene 10 9.2 92 70-130
1330-20-7 Xylene (total)30 28.4 95 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
* = Outside of Control Limits.
60 of 85
FA7782155.2.3
Blank Spike Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2768-BS A0223114.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Sporadic marginal failure.
* = Outside of Control Limits.
61 of 85
FA7782155.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77822-1MS A0223062.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1MSD A0223063.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1 a A0223056.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
FA77822-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 51.7 103 50 54.7 109 6 70-130/20
108-86-1 Bromobenzene ND 50 51.8 104 50 54.6 109 5 70-130/20
74-97-5 Bromochloromethane ND 50 50.8 102 50 54.5 109 7 70-130/20
75-27-4 Bromodichloromethane ND 50 52.4 105 50 55.5 111 6 70-130/20
75-25-2 Bromoform ND 50 43.4 87 50 46.6 93 7 70-130/20
104-51-8 n-Butylbenzene ND 50 45.6 91 50 50.5 101 10 70-130/20
135-98-8 sec-Butylbenzene ND 50 49.0 98 50 52.8 106 7 70-130/20
98-06-6 tert-Butylbenzene ND 50 46.4 93 50 51.0 102 9 70-130/20
56-23-5 Carbon Tetrachloride ND 50 55.8 112 50 58.7 117 5 70-130/20
108-90-7 Chlorobenzene ND 50 50.0 100 50 53.2 106 6 70-130/20
75-00-3 Chloroethane ND 50 50.6 101 50 57.9 116 13 60-140/20
67-66-3 Chloroform ND 50 52.5 105 50 55.6 111 6 70-130/20
95-49-8 o-Chlorotoluene ND 50 48.7 97 50 51.9 104 6 70-130/20
106-43-4 p-Chlorotoluene ND 50 46.4 93 50 50.5 101 8 70-130/20
124-48-1 Dibromochloromethane ND 50 45.9 92 50 49.3 99 7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 46.4 93 50 51.8 104 11 70-130/20
106-93-4 1,2-Dibromoethane ND 50 48.0 96 50 51.7 103 7 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 47.0 94 50 56.7 113 19 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 49.5 99 50 53.1 106 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 52.2 104 50 55.9 112 7 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 49.8 100 50 52.8 106 6 70-130/20
75-34-3 1,1-Dichloroethane ND 50 53.3 107 50 57.0 114 7 70-130/20
107-06-2 1,2-Dichloroethane ND 50 52.7 105 50 55.5 111 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 55.7 111 50 58.3 117 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene 0.13 J 50 46.0 92 50 50.0 100 8 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 53.3 107 50 58.5 117 9 70-130/20
78-87-5 1,2-Dichloropropane ND 50 49.5 99 50 52.8 106 6 70-130/20
142-28-9 1,3-Dichloropropane ND 50 47.3 95 50 50.9 102 7 70-130/20
594-20-7 2,2-Dichloropropane ND 50 52.8 106 50 58.1 116 10 70-130/20
563-58-6 1,1-Dichloropropene ND 50 50.8 102 50 55.3 111 8 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 41.0 82 50 44.4 89 8 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 44.6 89 50 48.1 96 8 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 46.0 92 50 52.2 104 13 70-130/20
100-41-4 Ethylbenzene ND 50 48.1 96 50 51.7 103 7 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 50 39.8 80 50 45.0 90 12 70-130/20
87-68-3 Hexachlorobutadiene ND 50 51.1 102 50 56.6 113 10 70-130/20
* = Outside of Control Limits.
62 of 85
FA7782155.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77822-1MS A0223062.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1MSD A0223063.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1 a A0223056.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
FA77822-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 50 43.4 87 50 48.2 96 10 70-130/20
99-87-6 p-Isopropyltoluene ND 50 45.9 92 50 50.3 101 9 70-130/20
74-83-9 Methyl Bromide ND 50 50.5 101 50 58.0 116 14 60-140/20
74-87-3 Methyl Chloride ND 50 54.6 109 50 62.9 126 14 60-140/20
74-95-3 Methylene Bromide ND 50 51.4 103 50 53.1 106 3 70-130/20
75-09-2 Methylene Chloride ND 50 50.7 101 50 54.0 108 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 50.0 100 50 55.4 111 10 70-130/20
91-20-3 Naphthalene ND 50 35.2 70 50 40.9 82 15 70-130/20
103-65-1 n-Propylbenzene ND 50 48.0 96 50 52.1 104 8 70-130/20
100-42-5 Styrene ND 50 41.9 84 50 46.7 93 11 70-130/20
75-85-4 Tert-Amyl Alcohol ND 500 480 96 500 536 107 11 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 50 41.1 82 50 46.9 94 13 70-130/20
75-65-0 Tert-Butyl Alcohol ND 500 653 131*500 747 149*13 70-130/20
762-75-4 Tert-Butyl Formate ND 500 266 53*500 317 63*17 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 50.2 100 50 53.4 107 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 51.4 103 50 53.9 108 5 70-130/20
127-18-4 Tetrachloroethylene ND 50 52.8 106 50 56.5 113 7 70-130/20
108-88-3 Toluene ND 50 48.7 97 50 52.9 106 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 43.3 87 50 48.4 97 11 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 40.2 80 50 45.6 91 13 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 54.3 109 50 57.9 116 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 49.7 99 50 52.7 105 6 70-130/20
79-01-6 Trichloroethylene ND 50 54.5 109 50 57.0 114 4 70-130/20
75-69-4 Trichlorofluoromethane ND 50 58.7 117 50 68.2 136 15 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 47.9 96 50 50.1 100 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 45.3 91 50 49.1 98 8 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 46.8 94 50 50.3 101 7 70-130/20
75-01-4 Vinyl Chloride ND 50 48.7 97 50 58.2 116 18 60-140/20
m,p-Xylene ND 100 92.3 92 100 99.9 100 8 70-130/20
95-47-6 o-Xylene ND 50 40.4 81 50 45.4 91 12 70-130/20
1330-20-7 Xylene (total)ND 150 133 89 150 145 97 9 70-130/20
CAS No.Surrogate Recoveries MS MSD FA77822-1 Limits
1868-53-7 Dibromofluoromethane 102%101%106%70-130%
* = Outside of Control Limits.
63 of 85
FA7782155.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77822-1MS A0223062.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1MSD A0223063.D 5 08/17/20 AB n/a n/a VA2766
FA77822-1 a A0223056.D 1 08/17/20 AB n/a n/a VA2766
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-4, FA77821-5, FA77821-7
CAS No.Surrogate Recoveries MS MSD FA77822-1 Limits
17060-07-0 1,2-Dichloroethane-D4 105%102%111%70-130%
2037-26-5 Toluene-D8 93%95%102%70-130%
460-00-4 4-Bromofluorobenzene 97%99%106%70-130%
(a) Associated internal standard response outside control limits. Confirmed by reanalysis.
* = Outside of Control Limits.
64 of 85
FA7782155.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-2MS A0223093.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2MSD A0223094.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2 A0223083.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
FA77821-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 51.9 104 50 53.0 106 2 70-130/20
108-86-1 Bromobenzene ND 50 50.7 101 50 52.7 105 4 70-130/20
74-97-5 Bromochloromethane ND 50 51.7 103 50 52.2 104 1 70-130/20
75-27-4 Bromodichloromethane ND 50 53.7 107 50 53.7 107 0 70-130/20
75-25-2 Bromoform ND 50 44.8 90 50 45.9 92 2 70-130/20
104-51-8 n-Butylbenzene ND 50 44.8 90 50 47.7 95 6 70-130/20
135-98-8 sec-Butylbenzene ND 50 48.3 97 50 50.8 102 5 70-130/20
98-06-6 tert-Butylbenzene ND 50 45.9 92 50 48.9 98 6 70-130/20
56-23-5 Carbon Tetrachloride ND 50 56.3 113 50 57.6 115 2 70-130/20
108-90-7 Chlorobenzene ND 50 50.2 100 50 51.5 103 3 70-130/20
75-00-3 Chloroethane ND 50 56.9 114 50 59.5 119 4 60-140/20
67-66-3 Chloroform ND 50 53.7 107 50 54.3 109 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 48.1 96 50 50.3 101 4 70-130/20
106-43-4 p-Chlorotoluene ND 50 45.7 91 50 48.5 97 6 70-130/20
124-48-1 Dibromochloromethane ND 50 46.4 93 50 48.0 96 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 46.7 93 50 49.6 99 6 70-130/20
106-93-4 1,2-Dibromoethane ND 50 47.2 94 50 50.2 100 6 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 51.5 103 50 56.5 113 9 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 48.9 98 50 51.1 102 4 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 51.7 103 50 53.7 107 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 49.7 99 50 50.7 101 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 53.8 108 50 55.8 112 4 70-130/20
107-06-2 1,2-Dichloroethane ND 50 54.2 108 50 54.6 109 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 56.7 113 50 58.0 116 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 46.3 93 50 48.8 98 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 54.0 108 50 56.0 112 4 70-130/20
78-87-5 1,2-Dichloropropane ND 50 50.3 101 50 50.9 102 1 70-130/20
142-28-9 1,3-Dichloropropane ND 50 46.9 94 50 49.5 99 5 70-130/20
594-20-7 2,2-Dichloropropane ND 50 52.4 105 50 56.1 112 7 70-130/20
563-58-6 1,1-Dichloropropene ND 50 50.5 101 50 53.7 107 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 38.2 76 50 40.8 82 7 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 44.1 88 50 46.9 94 6 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 47.0 94 50 50.1 100 6 70-130/20
100-41-4 Ethylbenzene ND 50 48.4 97 50 49.9 100 3 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 50 39.3 79 50 44.3 89 12 70-130/20
87-68-3 Hexachlorobutadiene ND 50 50.1 100 50 53.2 106 6 70-130/20
* = Outside of Control Limits.
65 of 85
FA7782155.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-2MS A0223093.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2MSD A0223094.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2 A0223083.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
FA77821-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 50 42.7 85 50 46.0 92 7 70-130/20
99-87-6 p-Isopropyltoluene ND 50 45.3 91 50 47.8 96 5 70-130/20
74-83-9 Methyl Bromide ND 50 57.5 115 50 60.1 120 4 60-140/20
74-87-3 Methyl Chloride ND 50 58.8 118 50 61.1 122 4 60-140/20
74-95-3 Methylene Bromide ND 50 51.6 103 50 52.4 105 2 70-130/20
75-09-2 Methylene Chloride ND 50 51.4 103 50 52.6 105 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.81 50 51.4 101 50 54.5 107 6 70-130/20
91-20-3 Naphthalene ND 50 34.5 69*50 38.8 78 12 70-130/20
103-65-1 n-Propylbenzene ND 50 47.0 94 50 49.9 100 6 70-130/20
100-42-5 Styrene ND 50 42.0 84 50 44.2 88 5 70-130/20
75-85-4 Tert-Amyl Alcohol ND 500 465 93 500 518 104 11 70-130/20
994-05-8 Tert-Amyl Methyl Ether ND 50 40.4 81 50 45.6 91 12 70-130/20
75-65-0 Tert-Butyl Alcohol ND 500 661 132*500 720 144*9 70-130/20
762-75-4 Tert-Butyl Formate ND 500 242 48*500 301 60*22*70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 50.6 101 50 51.6 103 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 51.9 104 50 53.3 107 3 70-130/20
127-18-4 Tetrachloroethylene ND 50 51.8 104 50 53.3 107 3 70-130/20
108-88-3 Toluene 0.14 J 50 48.7 97 50 51.0 102 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 42.9 86 50 46.2 92 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 39.8 80 50 43.1 86 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 54.7 109 50 56.1 112 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 50.9 102 50 51.9 104 2 70-130/20
79-01-6 Trichloroethylene ND 50 54.4 109 50 55.5 111 2 70-130/20
75-69-4 Trichlorofluoromethane ND 50 64.3 129 50 68.3 137 6 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 49.1 98 50 49.1 98 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 44.6 89 50 46.9 94 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 46.0 92 50 48.4 97 5 70-130/20
75-01-4 Vinyl Chloride ND 50 53.8 108 50 59.2 118 10 60-140/20
m,p-Xylene ND 100 92.2 92 100 96.1 96 4 70-130/20
95-47-6 o-Xylene ND 50 40.7 81 50 43.6 87 7 70-130/20
1330-20-7 Xylene (total)ND 150 133 89 150 140 93 5 70-130/20
CAS No.Surrogate Recoveries MS MSD FA77821-2 Limits
1868-53-7 Dibromofluoromethane 104%101%103%70-130%
* = Outside of Control Limits.
66 of 85
FA7782155.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-2MS A0223093.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2MSD A0223094.D 5 08/18/20 AB n/a n/a VA2767
FA77821-2 A0223083.D 1 08/18/20 AB n/a n/a VA2767
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-2, FA77821-3, FA77821-5, FA77821-6, FA77821-8
CAS No.Surrogate Recoveries MS MSD FA77821-2 Limits
17060-07-0 1,2-Dichloroethane-D4 106%104%108%70-130%
2037-26-5 Toluene-D8 93%95%103%70-130%
460-00-4 4-Bromofluorobenzene 97%100%110%70-130%
* = Outside of Control Limits.
67 of 85
FA7782155.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77823-8MS A0223122.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8MSD A0223123.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8 A0223118.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
FA77823-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 52.6 105 50 54.6 109 4 70-130/20
108-86-1 Bromobenzene ND 50 51.1 102 50 53.2 106 4 70-130/20
74-97-5 Bromochloromethane ND 50 51.9 104 50 54.5 109 5 70-130/20
75-27-4 Bromodichloromethane ND 50 52.5 105 50 53.5 107 2 70-130/20
75-25-2 Bromoform ND 50 39.8 80 50 42.2 84 6 70-130/20
104-51-8 n-Butylbenzene ND 50 46.8 94 50 49.6 99 6 70-130/20
135-98-8 sec-Butylbenzene ND 50 49.8 100 50 52.7 105 6 70-130/20
98-06-6 tert-Butylbenzene ND 50 47.4 95 50 50.1 100 6 70-130/20
56-23-5 Carbon Tetrachloride ND 50 55.8 112 50 58.2 116 4 70-130/20
108-90-7 Chlorobenzene ND 50 50.3 101 50 52.6 105 4 70-130/20
75-00-3 Chloroethane ND 50 54.9 110 50 59.3 119 8 60-140/20
67-66-3 Chloroform ND 50 54.2 108 50 55.6 111 3 70-130/20
95-49-8 o-Chlorotoluene ND 50 49.2 98 50 51.7 103 5 70-130/20
106-43-4 p-Chlorotoluene ND 50 46.6 93 50 49.8 100 7 70-130/20
124-48-1 Dibromochloromethane ND 50 43.4 87 50 46.1 92 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 49.0 98 50 48.4 97 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 48.2 96 50 51.7 103 7 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 48.8 98 50 54.9 110 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 49.8 100 50 52.0 104 4 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 52.1 104 50 54.4 109 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 49.4 99 50 50.6 101 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 55.5 111 50 57.3 115 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 54.6 109 50 55.7 111 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 56.6 113 50 59.8 120 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 46.9 94 50 50.7 101 8 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 55.8 112 50 58.9 118 5 70-130/20
78-87-5 1,2-Dichloropropane ND 50 52.1 104 50 54.2 108 4 70-130/20
142-28-9 1,3-Dichloropropane ND 50 48.0 96 50 51.2 102 6 70-130/20
594-20-7 2,2-Dichloropropane ND 50 58.5 117 50 61.3 123 5 70-130/20
563-58-6 1,1-Dichloropropene ND 50 52.5 105 50 55.2 110 5 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 39.4 79 50 42.7 85 8 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 44.1 88 50 47.9 96 8 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 48.4 97 50 52.8 106 9 70-130/20
100-41-4 Ethylbenzene ND 50 49.5 99 50 51.8 104 5 70-130/20
637-92-3 Ethyl Tert Butyl Ether ND 50 42.7 85 50 45.7 91 7 70-130/20
87-68-3 Hexachlorobutadiene ND 50 52.0 104 50 54.1 108 4 70-130/20
* = Outside of Control Limits.
68 of 85
FA7782155.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77823-8MS A0223122.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8MSD A0223123.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8 A0223118.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
FA77823-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 50 44.7 89 50 48.3 97 8 70-130/20
99-87-6 p-Isopropyltoluene ND 50 46.6 93 50 49.5 99 6 70-130/20
74-83-9 Methyl Bromide ND 50 55.5 111 50 59.1 118 6 60-140/20
74-87-3 Methyl Chloride ND 50 56.1 112 50 62.3 125 10 60-140/20
74-95-3 Methylene Bromide ND 50 51.7 103 50 53.2 106 3 70-130/20
75-09-2 Methylene Chloride ND 50 54.0 108 50 56.2 112 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether 1.6 50 54.8 106 50 57.7 112 5 70-130/20
91-20-3 Naphthalene ND 50 35.9 72 50 40.0 80 11 70-130/20
103-65-1 n-Propylbenzene ND 50 48.6 97 50 51.4 103 6 70-130/20
100-42-5 Styrene ND 50 42.6 85 50 46.0 92 8 70-130/20
75-85-4 Tert-Amyl Alcohol ND 500 504 101 500 543 109 7 70-130/20
994-05-8 Tert-Amyl Methyl Ether 0.44 J 50 45.2 90 50 48.5 96 7 70-130/20
75-65-0 Tert-Butyl Alcohol ND 500 675 135*500 741 148*9 70-130/20
762-75-4 Tert-Butyl Formate ND 500 314 63*500 331 66*5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 50.6 101 50 53.3 107 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 52.0 104 50 53.5 107 3 70-130/20
127-18-4 Tetrachloroethylene ND 50 52.8 106 50 54.9 110 4 70-130/20
108-88-3 Toluene ND 50 49.9 100 50 52.8 106 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 44.1 88 50 46.4 93 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 40.6 81 50 44.6 89 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 55.8 112 50 57.7 115 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 50.9 102 50 53.2 106 4 70-130/20
79-01-6 Trichloroethylene ND 50 55.2 110 50 57.5 115 4 70-130/20
75-69-4 Trichlorofluoromethane ND 50 60.6 121 50 66.7 133 10 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 49.4 99 50 50.3 101 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 45.9 92 50 48.8 98 6 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 47.0 94 50 49.9 100 6 70-130/20
75-01-4 Vinyl Chloride ND 50 51.9 104 50 58.7 117 12 60-140/20
m,p-Xylene ND 100 94.5 95 100 100 100 6 70-130/20
95-47-6 o-Xylene ND 50 42.1 84 50 46.3 93 10 70-130/20
1330-20-7 Xylene (total)ND 150 137 91 150 147 98 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA77823-8 Limits
1868-53-7 Dibromofluoromethane 102%101%104%70-130%
* = Outside of Control Limits.
69 of 85
FA7782155.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77823-8MS A0223122.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8MSD A0223123.D 5 08/19/20 AB n/a n/a VA2768
FA77823-8 A0223118.D 1 08/19/20 AB n/a n/a VA2768
The QC reported here applies to the following samples:Method: SM 6200B
FA77821-1
CAS No.Surrogate Recoveries MS MSD FA77823-8 Limits
17060-07-0 1,2-Dichloroethane-D4 106%104%112%70-130%
2037-26-5 Toluene-D8 94%96%101%70-130%
460-00-4 4-Bromofluorobenzene 98%101%107%70-130%
* = Outside of Control Limits.
70 of 85
FA7782155.3.3
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
71 of 85
FA778216
Method Blank Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S71-MB 1S3416.D 1 08/19/20 EG n/a n/a G1S71
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-1, FA77821-2, FA77821-3, FA77821-4, FA77821-5, FA77821-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 97%70-130%
460-00-4 BFB 94%70-130%
72 of 85
FA7782166.1.1
Method Blank Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S72-MB 1S3447.D 1 08/20/20 EG n/a n/a G1S72
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-8
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 99%70-130%
460-00-4 BFB 95%70-130%
73 of 85
FA7782166.1.2
Method Blank Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S73-MB 1S3465.D 1 08/21/20 EG n/a n/a G1S73
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7, FA77821-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 95%70-130%
460-00-4 BFB 93%70-130%
74 of 85
FA7782166.1.3
Method Blank Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S74-MB 1S3489.D 1 08/22/20 EG n/a n/a G1S74
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7
CAS No.Compound Result RL MDL Units Q
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 98%70-130%
460-00-4 BFB 95%70-130%
75 of 85
FA7782166.1.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S71-BS 1S3414.D 1 08/19/20 EG n/a n/a G1S71
G1S71-BSD 1S3415.D 1 08/19/20 EG n/a n/a G1S71
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-1, FA77821-2, FA77821-3, FA77821-4, FA77821-5, FA77821-6
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 80 78.0 98 76.1 95 2 70-130/25
100-41-4 Ethylbenzene 80 77.6 97 75.7 95 2 70-130/25
1634-04-4 Methyl Tert Butyl Ether 80 80.0 100 76.3 95 5 70-130/25
91-20-3 Naphthalene 80 77.5 97 76.0 95 2 70-130/25
108-88-3 Toluene 80 77.9 97 76.1 95 2 70-130/25
m,p-Xylene 160 154 96 150 94 3 70-130/25
95-47-6 o-Xylene 80 77.7 97 75.3 94 3 70-130/25
C5- C8 Aliphatics (Unadj.)240 234 98 223 93 5 70-130/25
C9- C12 Aliphatics (Unadj.)160 155 97 151 94 3 70-130/25
C9- C10 Aromatics (Unadj.)80 78.2 98 76.2 95 3 70-130/25
C9- C10 Aromatics 80 78.2 98 76.2 95 3 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 99%90%70-130%
460-00-4 BFB 95%88%70-130%
* = Outside of Control Limits.
76 of 85
FA7782166.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S72-BS a 1S3445.D 1 08/20/20 EG n/a n/a G1S72
G1S72-BSD 1S3446.D 1 08/20/20 EG n/a n/a G1S72
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-8
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 80 75.5 94 74.9 94 1 70-130/25
91-20-3 Naphthalene 80 74.4 93 74.8 94 1 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 100%99%70-130%
460-00-4 BFB 96%96%70-130%
(a) No sample DUP/MS available for this run.
* = Outside of Control Limits.
77 of 85
FA7782166.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S73-BS 1S3463.D 1 08/21/20 EG n/a n/a G1S73
G1S73-BSD 1S3464.D 1 08/21/20 EG n/a n/a G1S73
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7, FA77821-8
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 80 78.3 98 78.7 98 1 70-130/25
100-41-4 Ethylbenzene 80 77.9 97 77.8 97 0 70-130/25
108-88-3 Toluene 80 78.4 98 78.3 98 0 70-130/25
m,p-Xylene 160 154 96 154 96 0 70-130/25
95-47-6 o-Xylene 80 78.4 98 78.0 98 1 70-130/25
C5- C8 Aliphatics (Unadj.)240 237 99 241 100 2 70-130/25
C9- C12 Aliphatics (Unadj.)160 151 94 150 94 1 70-130/25
C9- C10 Aromatics (Unadj.)80 78.3 98 78.1 98 0 70-130/25
C9- C10 Aromatics 80 78.3 98 78.1 98 0 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 93%94%70-130%
460-00-4 BFB 91%92%70-130%
* = Outside of Control Limits.
78 of 85
FA7782166.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S74-BS 1S3487.D 1 08/22/20 EG n/a n/a G1S74
G1S74-BSD 1S3488.D 1 08/22/20 EG n/a n/a G1S74
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
100-41-4 Ethylbenzene 80 79.7 100 81.1 101 2 70-130/25
1634-04-4 Methyl Tert Butyl Ether 80 76.2 95 77.6 97 2 70-130/25
91-20-3 Naphthalene 80 74.6 93 70.3 88 6 70-130/25
m,p-Xylene 160 158 99 160 100 1 70-130/25
95-47-6 o-Xylene 80 79.3 99 80.4 101 1 70-130/25
C9- C10 Aromatics (Unadj.)80 80.1 100 81.3 102 1 70-130/25
C9- C10 Aromatics 80 80.1 100 81.3 102 1 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 96%91%70-130%
460-00-4 BFB 94%89%70-130%
* = Outside of Control Limits.
79 of 85
FA7782166.2.4
Matrix Spike Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-2MS 1S3423.D 1 08/19/20 EG n/a n/a G1S71
FA77821-2 1S3420.D 1 08/19/20 EG n/a n/a G1S71
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-1, FA77821-2, FA77821-3, FA77821-4, FA77821-5, FA77821-6
FA77821-2 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene ND 80 78.7 98 70-130
100-41-4 Ethylbenzene ND 80 78.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether ND 80 77.3 97 70-130
91-20-3 Naphthalene ND 80 74.9 94 70-130
108-88-3 Toluene ND 80 78.5 98 70-130
m,p-Xylene ND 160 154 96 70-130
95-47-6 o-Xylene ND 80 78.6 98 70-130
C5- C8 Aliphatics (Unadj.)ND 480 508 106 70-130
C9- C12 Aliphatics (Unadj.)ND 400 552 138*70-130
C9- C10 Aromatics (Unadj.)ND 240 97.8 41*70-130
C9- C10 Aromatics ND 240 97.8 41*70-130
CAS No.Surrogate Recoveries MS FA77821-2 Limits
460-00-4 BFB 98%101%70-130%
460-00-4 BFB 96%98%70-130%
* = Outside of Control Limits.
80 of 85
FA7782166.3.1
Matrix Spike Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-8MS 1S3472.D 20 08/21/20 EG n/a n/a G1S73
FA77821-8 a 1S3471.D 10 08/21/20 EG n/a n/a G1S73
FA77821-8 a 1S3467.D 20 08/21/20 EG n/a n/a G1S73
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7, FA77821-8
FA77821-8 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 1100 1600 2740 103 70-130
100-41-4 Ethylbenzene 838 1600 2440 100 70-130
108-88-3 Toluene 2910 1600 4540 102 70-130
m,p-Xylene 3150 3200 6270 98 70-130
95-47-6 o-Xylene 1770 1600 3350 99 70-130
C5- C8 Aliphatics (Unadj.)12100 b 9600 23000 114 70-130
C9- C12 Aliphatics (Unadj.)9840 b 8000 20900 138*70-130
C9- C10 Aromatics (Unadj.)2540 4800 4540 42*70-130
C9- C10 Aromatics 2540 4800 4540 42*70-130
CAS No.Surrogate Recoveries MS FA77821-8 FA77821-8 Limits
460-00-4 BFB 76%81%78%70-130%
460-00-4 BFB 73%79%76%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Result is from Run #2.
* = Outside of Control Limits.
81 of 85
FA7782166.3.2
Matrix Spike Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-7MS 1S3494.D 5 08/22/20 EG n/a n/a G1S74
FA77821-7 a 1S3492.D 2 08/22/20 EG n/a n/a G1S74
FA77821-7 1S3490.D 5 08/22/20 EG n/a n/a G1S74
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7
FA77821-7 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
100-41-4 Ethylbenzene 743 b 400 1140 119 70-130
1634-04-4 Methyl Tert Butyl Ether 543 b 400 1120 151*70-130
91-20-3 Naphthalene 57.9 b 400 424 92 70-130
m,p-Xylene 2250 b 800 3000 94 70-130
95-47-6 o-Xylene 1260 b 400 1660 100 70-130
C9- C10 Aromatics (Unadj.)1320 b 1200 1820 42*70-130
C9- C10 Aromatics 1320 b 1200 1820 42*70-130
CAS No.Surrogate Recoveries MS FA77821-7 FA77821-7 Limits
460-00-4 BFB 87%88%89%70-130%
460-00-4 BFB 88%88%88%70-130%
(a) Confirmation run.
(b) Result is from Run #2.
* = Outside of Control Limits.
82 of 85
FA7782166.3.3
Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-2DUP 1S3426.D 1 08/19/20 EG n/a n/a G1S71
FA77821-2 1S3420.D 1 08/19/20 EG n/a n/a G1S71
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-1, FA77821-2, FA77821-3, FA77821-4, FA77821-5, FA77821-6
FA77821-2 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FA77821-2 Limits
460-00-4 BFB 93%101%70-130%
460-00-4 BFB 91%98%70-130%
* = Outside of Control Limits.
83 of 85
FA7782166.4.1
Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-8DUP 1S3468.D 20 08/21/20 EG n/a n/a G1S73
FA77821-8 a 1S3471.D 10 08/21/20 EG n/a n/a G1S73
FA77821-8 a 1S3467.D 20 08/21/20 EG n/a n/a G1S73
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7, FA77821-8
FA77821-8 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 1100 1100 0 50
100-41-4 Ethylbenzene 838 834 0 50
108-88-3 Toluene 2910 2920 0 50
m,p-Xylene 3150 3190 1 50
95-47-6 o-Xylene 1770 1780 1 50
C5- C8 Aliphatics (Unadj.)12100 b 12000 1 50
C9- C12 Aliphatics (Unadj.)9840 b 9710 1 50
C9- C10 Aromatics (Unadj.)2540 2530 0 50
C5- C8 Aliphatics 7840 b 7710 2 50
C9- C12 Aliphatics 4010 b 3910 3 50
C9- C10 Aromatics 2540 2530 0 50
CAS No.Surrogate Recoveries DUP FA77821-8 FA77821-8 Limits
460-00-4 BFB 80%81%78%70-130%
460-00-4 BFB 78%79%76%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Result is from Run #2.
* = Outside of Control Limits.
84 of 85
FA7782166.4.2
Duplicate Summary Page 1 of 1
Job Number:FA77821
Account:GRINCC GRI (Geological Resources Inc.)
Project:New Dixie 226; 4917 Raleigh Rd & Parkway W, Wilson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA77821-7DUP 1S3491.D 5 08/22/20 EG n/a n/a G1S74
FA77821-7 a 1S3492.D 2 08/22/20 EG n/a n/a G1S74
FA77821-7 1S3490.D 5 08/22/20 EG n/a n/a G1S74
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA77821-7
FA77821-7 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
100-41-4 Ethylbenzene 743 b 747 11 50
1634-04-4 Methyl Tert Butyl Ether 543 b 550 6 50
91-20-3 Naphthalene 57.9 b 56.7 2 50
m,p-Xylene 2250 b 2250 0 50
95-47-6 o-Xylene 1260 b 1270 1 50
C9- C10 Aromatics (Unadj.)1320 b 1320 0 50
C9- C12 Aliphatics 735 b E 690 E 13 50
C9- C10 Aromatics 1320 b 1320 0 50
CAS No.Surrogate Recoveries DUP FA77821-7 FA77821-7 Limits
460-00-4 BFB 85%88%89%70-130%
460-00-4 BFB 84%88%88%70-130%
(a) Confirmation run.
(b) Result is from Run #2.
* = Outside of Control Limits.
85 of 85
FA7782166.4.3