RA-7785_39880_CA_RPTS_20151222

EXECUTIVE SUMMARY

Red Apple Market #5 is a former petroleum retail facility and convenience store located at 101 East
Jefferson Street, in Jackson, Northampton County, North Carolina. The adjoining properties are
commercial and municipal. Municipal water is available to the site and surrounding properties.

In September 1992, a release was discovered underground storage tank (UST) removal activities
conducted at the site. The release was assigned UST Incident Number 9329. On January 11, 2007, a
Notice of Residual Petroleum (NRP) was filed on the deed of the subject property; and, on February 22,
2013, a Notice of No Further Action was issued.

On November 24, 2015, one 4,000-gallon kerosene UST, one 6,000-gallon gasoline UST, one 10,000-
gallon gasoline UST, associated dispensers, and product piping were removed from the site. Based on
field observations, no over-excavation activities were conducted in the UST basin, dispensers, or product
piping areas. Upon completion of UST extraction activities, confirmation soil samples were collected
from the sidewalls of the excavation. No concentrations of requested method constituents that exceeded
the soil-to-water Maximum Contaminant Concentrations were reported in the soil samples collected
during the UST closure activities.

Although ground water was encountered during UST removal, no ground water assessment was
conducted because an NRP had been filed on the subject property deed in 2007.

Based on these results, a release has not occurred from the UST system that was removed in November
2015. No further assessment is warranted for this site.

TABLE OF CONTENTS

A. SITE INFORMATION ............................................................................................................. 1

B. SITE HISTORY AND CHARACTERIZATION .................................................................... 2

C. SITE CHECK ........................................................................................................................... 3

D. UST CLOSURE ........................................................................................................................ 3

E. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT .................................... 4

F. GROUND WATER INVESTIGATION................................................................................... 4

G. INITIAL RESPONSE AND ABATEMENT ACTION ............................................................ 4

H. EXCAVATION OF CONTAMINATED SOIL ....................................................................... 5

I. SOIL AND GROUND WATER SAMPLE RESULTS ............................................................ 5

J. SUMMARY AND CONCLUSIONS ........................................................................................ 6

K. LIMITATIONS ......................................................................................................................... 6

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Soil Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results

APPENDICES
Appendix A: UST-3 Form
Appendix B: UST-2 Form
Appendix C: Site Specific Heath and Safety Plan
Appendix D: UST Disposal Manifest
Appendix E: Laboratory Report – Soil Samples

1

A. SITE INFORMATION
1. Site Identification:
Date of Report: December 22, 2015
Facility ID Number: 0-026626 Incident Number: 9329
Site Name: Red Apple Market #5
Site Address: 101 East Jefferson Street
City: Jackson State: NC Zip Code: 27845 County: Northampton
Description of Geographical Data Point: Calculated from topographic map.
Latitude: 36.389504° N Longitude: 77.419269° W
2. Contacts Associated with Leaking UST System:
UST Owner: North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910
[phone]
UST Operator: Northeast Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910
[phone]
Property Owner: Eastern Fuels, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910
Closure Contractor: Greenwood Applied Services, LLC (GAS)
133 River Street
Colerain, North Carolina 27924
[phone]
Primary Consultant: Geological Resources, Inc. (GRI)
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
Laboratory: Accutest Laboratories - Southeast
4405 Vineland Road, Suite C-15
Orlando, Florida 32811
[phone]
North Carolina Certification No. 573
3. Release Information
Date Discovered: In September 1992, a release was discovered at the site during the
removal of three (3) 4,000-gallon gasoline USTs and one (1) 1,000-
gallon gasoline UST.
Estimated Quantity of Release: Unknown
Cause of Release: Leaking UST systems
Source of Release: Leaking UST systems
UST Size/Contents: On November 24, 2015, one 4,000-gallon kerosene UST, one 6,000-
gallon gasoline UST, one 10,000-gallon gasoline UST, associated
dispensers, and product piping were removed from the site.

3

C. SITE CHECK
A site check was not part of the initial abatement activities.
D. UST CLOSURE
1. Preparation for Closure:
In October 2015, North East Oil Company, Inc. contracted GRI to coordinate and supervise the UST
removal activities. GAS was responsible for the removal and proper disposal of the UST system. Prior to
closure activities, GRI personnel notified the Northampton County building inspector, however, no permit
was required prior to UST removal. A Notice of Intent: UST Permanent Closure or Change-in-Service
(UST-3 Form) Form was submitted to the North Carolina Department of Environmental Quality
(NCDEQ) Raleigh Regional office on October 12, 2015 and is included as Appendix A. A copy of the
Site Investigation Report for Permanent Closure or Change-in-Service of UST Form (UST-2 Form) is
included as Appendix B. A copy of the site specific health and safety plan is included as Appendix C.
2. Closure Procedure:
On November 24, 2015, one 4,000-gallon kerosene, one 6,000-gallon gasoline and one 10,000-gallon
gasoline USTs were uncovered using a track mounted excavator. The USTs were covered with
approximately 3 foot of concrete and soil. Upon completion of properly purging the USTs of explosive
vapors, the USTs were removed. The USTs were in good condition with no visible pitting or corrosion.
The 10,000-gallon UST was approximately 8 feet in diameter by 26 feet 7 inches in length; the 6,000-
gallon UST was approximately 8 feet in diameter by 16 feet in length. The 4,000-gallon UST was
approximately 64 inches in diameter by 24 feet in length. Subsequent to removal, the USTs were
transported off-site. A disposal manifest for the USTs is included in Appendix D.
3. Residual Material:
No residual product or water was present in the USTs prior to closure.
4. Release Information:
In September 1992, during UST closure, a release was discovered. The release was assigned Incident
Number 9329 by NCDENR. On January 11, 2007, an NRP for ground water was filed on the deed of the
subject property. On February 22, 2013, the NCDENR issued A Notice of No Further Action for the
incident.
5. Soil Excavation Activities:
Based on the observations and direction of GRI staff, no contaminated soil was removed from the site
during the November 24, 2015 UST closure activities. The excavation boundaries are shown on Figure
2.

4

6. Site Investigation:
Since ground water was encountered in the gasoline UST basin, soil samples CS-1 (7’) through CS-4 (7’)
were collected along the sidewalls of the UST excavation at depths of approximately seven feet below
ground surface. Soil samples CS-1 (7’), CS-3 (7’) and CS-4 (7’) were submitted for laboratory analyses
of volatile organic compounds using EPA Method 8260B, semi-volatile organic compounds using EPA
Method 8270 as well as VPH and EPH using the MADEP Methods. Soil sample CS-2 (7’) was submitted
for analyses of EPA Method 8260 and MADEP Method VPH only.

Soil sample SP-1 was collected from the soil stockpile and was submitted for analyses of TPH-GRO and
TPH-DRO.

All soil samples were collected using either a hand auger or directly from the bucket of the excavator.
Soil sample locations have been included on Figure 3.

E. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT
Free product was not encountered during the November 2015 UST closure activities.

F. GROUND WATER INVESTIGATION
Although ground water was encountered in the former UST basin, no ground water assessment was
warranted because an NRP for ground water was recorded on the deed of the subject property in 2007.

G. INITIAL RESPONSE AND ABATEMENT ACTION
Initial Response Actions:
On November 24, 2015, one 4,000-gallon kerosene UST, one 6,000-gallon gasoline UST, one 10,000-
gallon gasoline UST, associated dispensers, and product piping were removed from the site. No residual
product or water was present in the USTs prior to closure activities. Petroleum odor was not encountered
in the excavation during UST closure activities. The excavation basin was backfilled to grade with clean
fill material.
 Source Control Actions: One 4,000-gallon kerosene UST, one 6,000-gallon gasoline UST, one
10,000-gallon gasoline UST, associated dispensers, and product piping were removed from the site on
November 24, 2015.
 Contaminant Migration Control Measures: The release was to the sub-surface; therefore no

5

contaminant migration control measures were necessary.
 Measures Taken to Mitigate Fire/Safety Hazards: Prior to closure, the appropriate officials were
notified (i.e. Fire Marshal). Free product was not encountered during closure activities. There do not
appear to be any immediate fire or safety hazards present as a result of a release.
 Measures Taken to Identify and Mitigate Pollution Hazards: The release was to the sub-surface;
therefore, no migration control measures were necessary.
2. Initial Abatement Actions:
 Contaminated Soil Storage/Treatment and/or Disposal: On November 24, 2015, GRI directed the
soil excavation activities. Soil was excavated, loaded and transported to a permitted facility for
disposal.

H. EXCAVATION OF CONTAMINATED SOIL
1. Extent of Soil Contamination:
Petroleum odor was not encountered in the UST basin during closure activities, therefore, excavation
activities were limited to removal of the UST system.
2. Excavation Process:
The excavation activities were conducted using a track-mounted excavator. GRI directed the
equipment operators as to what excavate.
3. Sampling Description:
All soil samples were collected directly from the bucket of the excavator by GRI personnel. Samples
were collected with clean, disposable latex gloves, immediately placed in laboratory-supplied
glassware and placed on ice.

I. SOIL AND GROUND WATER SAMPLE RESULTS
 Soil:
Concentrations of TPH-GRO and TPH-DRO that exceeded the Regulatory Allowable Limits (RALs)
were reported in the soil sample collected from stockpile sample SP-1. No concentrations of
requested method constituents that exceeded the soil-to-water Maximum Soil Contaminant
Concentrations (MCCs) were reported in CS-1 (7’) through CS-4 (7’). A summary of soil sample
analytical results is presented as Table 3. A Soil Quality Map has been included as Figure 3. A
copy of the laboratory report is included as Appendix E.
 Ground Water:
Ground water samples were not collected during the November 2015 UST closure activities.

6

J. SUMMARY AND CONCLUSIONS
 One 4,000-gallon kerosene UST, one 6,000-gallon gasoline UST, one 10,000-gallon gasoline UST,
associated dispensers, and product piping were removed from the site on November 24, 2015.
 The site is located in a commercial and municipal area in the Town of Jackson, Northampton County.
Municipal water is available to the site and surrounding properties.
 Petroleum odor was not present in the UST basin; therefore, over excavation was not conducted.
 Concentrations of TPH-GRO and TPH-DRO that exceeded the RALs were reported in the stockpile
sample SP-1.
 No concentrations of requested method constituents that exceeded the soil-to-water MCCs were
reported in CS-1 (7’) through CS-4 (7’).
 Although ground water was encountered in the former UST basin, no ground water assessment was
warranted because an NRP for ground water was recorded on the deed of the subject property in
2007.
 Based on these results, a release has not occurred from the UST system that was removed in
November 2015. No further assessment is warranted for this site.

K. LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Bertie County, North Carolina. The assessment was conducted based
on the scope of work and level of effort specified by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1SITE LOCATION MAPRAM #5101 EAST JEFFERSON STREETJACKSON, NORTHAMPTON COUNTY,NORTH CAROLINAINCIDENT NO. 9329
PREPARED BY:GEOLOGICAL RESOURCES, INC.DECEMBER 8, 201502,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 36.389504° NLONGITUDE: 77.419269° W
`
SITE LOCATION
³

TABLES
UST ID Number 1 - 4 Facility ID Number
Owner or Operator?
Owner and Operator
UST ID Number 5 - 7 Facility ID Number
Owner or Operator?
Owner and Operator
Post Office Box 1386, Ahoskie, North Carolina 27910 252-862-0236
Address Telephone Number
Red Apple Markets, Inc.06/09/75 - 09/09/92
Address Telephone Number
Post Office Box 1386, Ahoskie, North Carolina 27910 252-862-0236
0-026626
Name of Owner or Operator Dates of Ownership / Operation
Red Apple Markets, Inc.10/09/92 - 11/24/15
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
RED APPLE MARKET #5 (INCIDENT NO. 9329)
0-026626
Page 1 of 1
Date: 12/16/15
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 4,000 06/09/75 Steel 64" x 24'Unknown Removed
(09/09/92)Yes
2 Gasoline Gasoline 4,000 06/09/75 Steel 64" x 24'Unknown Removed
(09/09/92)Yes
3 Gasoline Gasoline 4,000 06/09/75 Steel 64" x 24'Unknown Removed
(09/09/92)Yes
4 Gasoline Gasoline 1,000 06/09/75 Steel 64" x 72"Unknown Removed
(09/09/92)Yes
5 Kerosene Kerosene 4,000 10/09/92 ACT-100 64" x 24'Flex and
Fiberglass
Removed
(11/24/15)No
6 Gasoline Gasoline 6,000 10/09/92 ACT-100 8' x 16'Flex and
Fiberglass
Removed
(11/24/15)No
7 Gasoline Gasoline 10,000 10/09/92 ACT-100 8' x 26' 7"Flex and
Fiberglass
Removed
(11/24/15)No
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
RED APPLE MARKET #5 (INCIDENT NO. 9329)
Facility ID #: 0-026626
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 12/16/15
→5030/
8015B
3550/
8015B
10 10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA 0.0056 4.3 4.9 4.6 0.091 0.16 1.7 1.7 8.3 8.5 68 540 540 NE 31 31
NA NA 18 1,200 1,560 3,129 350 313 1,564 626 782 782 939 1,500 1,500 31,000 469 469
SP-1 11/24/15 Stockpile ---231 97.2 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
CS-1 (7')11/24/15 7 NR NR 0.0020 J 0.0081 <0.0011 0.0035 J <0.0013 <0.0022 <0.0011 <0.0011 <0.0011 <0.0011 <2.4 <2.4 <5.9 <5.9 <2.4 <8.9
CS-2 (7')11/24/15 7 NR NR 0.0013 J 0.0040 J <0.0011 <0.0022 <0.0013 <0.0021 <0.0011 <0.0011 <0.0011 <0.0011 <2.4 <2.4 NR NR <2.4 NR
CS-3 (7')11/24/15 7 NR NR <0.001 <0.001 <0.001 <0.0021 <0.0012 <0.002 <0.001 <0.001 <0.001 <0.001 <2.0 <2.0 <6.0 <6.0 <2.0 <9.0
CS-4 (7')11/24/15 7 NR NR <0.001 <0.001 <0.001 <0.0021 <0.0012 <0.002 <0.001 <0.001 <0.001 <0.001 <2.1 <2.1 <5.8 <5.8 <2.1 <8.8
Notes:
• Results reported in milligrams per kilogram (mg/kg).
• < : Less than the method detection limit specified in the laboratory report.
• RAL: Regulatory Action Level.
• MCC: Maximum Contaminant Concentration.
• NA: Not Applicable.
• NE: Not Established.
• NR: Analyses Not Requested.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
MADEP Methods VPH and EPH
Isopropylbenzenen-Propylbenzene1,3,5-Trimethylbenzene1,2,4-TrimethylbenzeneC11-C22 AromaticsC9-C18 AliphaticsC19-C36 AliphaticsTABLE 3
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #5 (INCIDENT NO. 9329)
Facility ID #: 0-026626
C9-C10 AromaticsC5-C8 AliphaticsResidential Soil Cleanup Level
UST Basin
Sidewalls
Soil-to-Water MCC MTBEXylenesNaphthaleneC9-C12 Aliphatics Analytical Method EPA Methods 8260B and 8270
Sample IDDate Collected (mm/dd/yy)RAL Sample LocationSample Depth (ft-BGS)Gasoline-Range TPHDiesel-Range TPHBenzeneTolueneEthylbenzenePage 1 of 1

APPENDICES

APPENDIX A
UST-3 Form

APPENDIX B
UST-2 Form

APPENDIX C
Site Specific Health and Safety Plan

APPENDIX D
UST Disposal Manifest

APPENDIX E
Laboratory Report – Soil Samples
12/08/15
Technical Report for
GRI (Geological Resources Inc.)
Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
9329
Accutest Job Number: FA29570
Sampling Date: 11/24/15
Report to:
GRI
[e-mail]
[e-mail]; [e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
12/08/15
Reissue #1
e-Hardcopy 2.0
Automated Report
62
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 62
FA29570
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]  htpp://www.accutest.com www.accutest.com

December 8, 2015

Mr. William Regenthal
Geological Resources Inc
3502 Hayes Rd
Monroe, NC 28110

RE: Accutest job FA29570 Reissue

Dear Mr. Regenthal,

The final report for job number FA29570 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The reporting units have been revised.

Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.

Sincerely,

Accutest Laboratories, SE

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FA29570
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................6
3.1: FA29570-1: CS-1 7' ......................................................................................................7
3.2: FA29570-2: CS-2 7' ......................................................................................................13
3.3: FA29570-3: CS-3 7' ......................................................................................................16
3.4: FA29570-4: SP-1 ..........................................................................................................22
3.5: FA29570-5: CS-4 7' ......................................................................................................24
Section 4: Misc. Forms ............................................................................................................30
4.1: Chain of Custody ...........................................................................................................31
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................34
5.1: Method Blank Summary ................................................................................................35
5.2: Blank Spike Summary ...................................................................................................37
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................39
Section 6: GC/MS Semi-volatiles - QC Data Summaries .....................................................41
6.1: Method Blank Summary ................................................................................................42
6.2: Blank Spike Summary ...................................................................................................45
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................47
Section 7: GC Volatiles - QC Data Summaries .....................................................................49
7.1: Method Blank Summary ................................................................................................50
7.2: Blank Spike Summary ...................................................................................................52
7.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................53
7.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................54
7.5: Duplicate Summary .......................................................................................................55
Section 8: GC Semi-volatiles - QC Data Summaries ............................................................56
8.1: Method Blank Summary ................................................................................................57
8.2: Blank Spike Summary ...................................................................................................59
8.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................60
8.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................61
8.5: Duplicate Summary .......................................................................................................62 123456783 of 62
FA29570
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA29570
Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Project No: 9329
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA29570-1 11/24/15 10:56 WR 11/25/15 SO Soil CS-1 7'
FA29570-2 11/24/15 11:00 WR 11/25/15 SO Soil CS-2 7'
FA29570-3 11/24/15 11:17 WR 11/25/15 SO Soil CS-3 7'
FA29570-4 11/24/15 12:13 WR 11/25/15 SO Soil SP-1
FA29570-5 11/24/15 00:00 WR 11/25/15 SO Soil CS-4 7'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 62
FA29570 1
Summary of Hits Page 1 of 1
Job Number:FA29570
Account:GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Collected:11/24/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA29570-1 CS-1 7'
Acetone 0.0429 J 0.055 0.017 mg/kg SW846 8260B
Benzene 0.0020 J 0.0055 0.0011 mg/kg SW846 8260B
Toluene 0.0081 0.0055 0.0011 mg/kg SW846 8260B
Xylene (total)0.0035 J 0.017 0.0023 mg/kg SW846 8260B
Di-n-butyl Phthalate 0.235 J 0.40 0.040 mg/kg SW846 8270D
FA29570-2 CS-2 7'
Acetone 0.0623 0.053 0.016 mg/kg SW846 8260B
Benzene 0.0013 J 0.0053 0.0011 mg/kg SW846 8260B
2-Butanone (MEK)0.0090 J 0.027 0.0090 mg/kg SW846 8260B
Toluene 0.0040 J 0.0053 0.0011 mg/kg SW846 8260B
FA29570-3 CS-3 7'
Acetone 0.0370 J 0.050 0.015 mg/kg SW846 8260B
Di-n-butyl Phthalate 0.224 J 0.39 0.039 mg/kg SW846 8270D
FA29570-4 SP-1
TPH-GRO (C6-C10)231 55 27 mg/kg SW846 8015C
TPH (C10-C28) a 97.2 7.0 4.2 mg/kg SW846 8015C
FA29570-5 CS-4 7'
Acetone 0.0417 J 0.051 0.015 mg/kg SW846 8260B
Di-n-butyl Phthalate 0.142 J 0.39 0.039 mg/kg SW846 8270D
(a) Petroleum hydrocarbon pattern begins before C10.
5 of 62
FA29570 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
6 of 62
FA29570 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y24433.D 1 11/30/15 AD n/a n/a VY1030
Run #2
Initial Weight Final Volume
Run #1 5.55 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0429 0.055 0.017 mg/kg J
71-43-2 Benzene 0.0020 0.0055 0.0011 mg/kg J
75-27-4 Bromodichloromethane ND 0.0055 0.0011 mg/kg
75-25-2 Bromoform ND 0.0055 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.028 0.0094 mg/kg
104-51-8 n-Butylbenzene ND 0.0055 0.0011 mg/kg
75-15-0 Carbon Disulfide ND 0.0055 0.0016 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0055 0.0011 mg/kg
108-90-7 Chlorobenzene ND 0.0055 0.0011 mg/kg
75-00-3 Chloroethane ND 0.0055 0.0022 mg/kg
67-66-3 Chloroform ND 0.0055 0.0011 mg/kg
110-82-7 Cyclohexane ND 0.0055 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0055 0.0011 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0055 0.0015 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0055 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0055 0.0015 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0055 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0055 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0055 0.0011 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0055 0.0011 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0055 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0055 0.0015 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0055 0.0011 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0055 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0055 0.0011 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg
100-41-4 Ethylbenzene ND 0.0055 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.028 0.0090 mg/kg
98-82-8 Isopropylbenzene ND 0.0055 0.0011 mg/kg
79-20-9 Methyl Acetate ND 0.028 0.011 mg/kg
74-83-9 Methyl Bromide ND 0.0055 0.0024 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0055 0.0022 mg/kg
108-87-2 Methylcyclohexane ND 0.0055 0.0012 mg/kg
75-09-2 Methylene Chloride ND 0.011 0.0044 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.028 0.0059 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0055 0.0013 mg/kg
91-20-3 Naphthalene ND 0.0055 0.0022 mg/kg
103-65-1 n-Propylbenzene ND 0.0055 0.0011 mg/kg
100-42-5 Styrene ND 0.0055 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0055 0.0012 mg/kg
127-18-4 Tetrachloroethylene ND 0.0055 0.0018 mg/kg
108-88-3 Toluene 0.0081 0.0055 0.0011 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0055 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0055 0.0014 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0055 0.0014 mg/kg
79-01-6 Trichloroethylene ND 0.0055 0.0011 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0055 0.0019 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0055 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0055 0.0011 mg/kg
75-01-4 Vinyl Chloride ND 0.0055 0.0018 mg/kg
1330-20-7 Xylene (total)0.0035 0.017 0.0023 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 111%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 117%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684836.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.0 0.20 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.20 0.020 mg/kg
95-57-8 2-Chlorophenol ND 0.20 0.020 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.20 0.020 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.20 0.020 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.0 0.20 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.40 0.081 mg/kg
95-48-7 2-Methylphenol ND 0.20 0.020 mg/kg
3&4-Methylphenol ND 0.20 0.040 mg/kg
88-75-5 2-Nitrophenol ND 0.20 0.020 mg/kg
100-02-7 4-Nitrophenol ND 1.0 0.16 mg/kg
87-86-5 Pentachlorophenol ND 1.0 0.16 mg/kg
108-95-2 Phenol ND 0.20 0.020 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.20 0.020 mg/kg
83-32-9 Acenaphthene ND 0.20 0.020 mg/kg
208-96-8 Acenaphthylene ND 0.20 0.020 mg/kg
120-12-7 Anthracene ND 0.20 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.20 0.020 mg/kg
50-32-8 Benzo(a)pyrene ND 0.20 0.020 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.20 0.020 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.20 0.020 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.20 0.020 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.20 0.020 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.20 0.040 mg/kg
106-47-8 4-Chloroaniline ND 0.20 0.020 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.20 0.020 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.20 0.020 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.20 0.020 mg/kg
91-58-7 2-Chloronaphthalene ND 0.20 0.024 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.20 0.020 mg/kg
218-01-9 Chrysene ND 0.20 0.020 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.20 0.020 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.20 0.020 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.20 0.020 mg/kg
84-66-2 Diethyl Phthalate ND 0.40 0.040 mg/kg
131-11-3 Dimethyl Phthalate ND 0.20 0.040 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.20 0.040 mg/kg
84-74-2 Di-n-butyl Phthalate 0.235 0.40 0.040 mg/kg J
121-14-2 2,4-Dinitrotoluene ND 0.20 0.020 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.20 0.020 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.40 0.040 mg/kg
206-44-0 Fluoranthene ND 0.20 0.020 mg/kg
86-73-7 Fluorene ND 0.20 0.020 mg/kg
118-74-1 Hexachlorobenzene ND 0.20 0.020 mg/kg
87-68-3 Hexachlorobutadiene ND 0.20 0.020 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.20 0.040 mg/kg
67-72-1 Hexachloroethane ND 0.20 0.020 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 0.020 mg/kg
78-59-1 Isophorone ND 0.20 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.20 0.020 mg/kg
91-57-6 2-Methylnaphthalene ND 0.20 0.020 mg/kg
91-20-3 Naphthalene ND 0.20 0.020 mg/kg
98-95-3 Nitrobenzene ND 0.20 0.020 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.20 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.20 0.020 mg/kg
85-01-8 Phenanthrene ND 0.20 0.020 mg/kg
129-00-0 Pyrene ND 0.20 0.020 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 70%40-102%
4165-62-2 Phenol-d5 77%41-100%
118-79-6 2,4,6-Tribromophenol 85%42-108%
4165-60-0 Nitrobenzene-d5 71%40-105%
321-60-8 2-Fluorobiphenyl 75%43-107%
1718-51-0 Terphenyl-d14 89%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP VPH REV 1.1 Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV072642.D 1 11/30/15 AH n/a n/a GUV3870
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.56 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.067 0.067 mg/kg
100-41-4 Ethylbenzene ND 0.13 0.067 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.13 0.067 mg/kg
91-20-3 Naphthalene ND 0.34 0.20 mg/kg
108-88-3 Toluene ND 0.13 0.067 mg/kg
m,p-Xylene ND 0.27 0.13 mg/kg
95-47-6 o-Xylene ND 0.13 0.067 mg/kg
C5- C8 Aliphatics (Unadj.)ND 6.7 2.4 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.7 2.4 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.7 2.4 mg/kg
C5- C8 Aliphatics ND 6.7 2.4 mg/kg
C9- C12 Aliphatics ND 6.7 2.4 mg/kg
C9- C10 Aromatics ND 6.7 2.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 118%70-130%
460-00-4 BFB 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-1 7'
Lab Sample ID:FA29570-1 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:81.6
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN014378.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
Run #2
Initial Weight Final Volume
Run #1 20.7 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.24 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.24 0.12 mg/kg
120-12-7 Anthracene ND 0.24 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.24 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.24 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.24 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.24 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.24 0.12 mg/kg
218-01-9 Chrysene ND 0.24 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.24 0.12 mg/kg
206-44-0 Fluoranthene ND 0.24 0.12 mg/kg
86-73-7 Fluorene ND 0.24 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.24 0.12 mg/kg
91-57-6 2-Methylnaphthalene ND 0.24 0.12 mg/kg
91-20-3 Naphthalene ND 0.24 0.12 mg/kg
85-01-8 Phenanthrene ND 0.24 0.12 mg/kg
129-00-0 Pyrene ND 0.24 0.12 mg/kg
C11-C22 Aromatics (Unadj.)ND 12 8.9 mg/kg
C11-C22 Aromatics ND 12 8.9 mg/kg
C9-C18 Aliphatics ND 12 5.9 mg/kg
C19-C36 Aliphatics ND 12 5.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 64%40-140%
580-13-2 2-Bromonaphthalene 72%40-140%
84-15-1 o-Terphenyl 52%40-140%
321-60-8 2-Fluorobiphenyl 71%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 62
FA29570 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-2 7'
Lab Sample ID:FA29570-2 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:79.7
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y24434.D 1 11/30/15 AD n/a n/a VY1030
Run #2
Initial Weight Final Volume
Run #1 5.91 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0623 0.053 0.016 mg/kg
71-43-2 Benzene 0.0013 0.0053 0.0011 mg/kg J
75-27-4 Bromodichloromethane ND 0.0053 0.0011 mg/kg
75-25-2 Bromoform ND 0.0053 0.0011 mg/kg
78-93-3 2-Butanone (MEK)0.0090 0.027 0.0090 mg/kg J
104-51-8 n-Butylbenzene ND 0.0053 0.0011 mg/kg
75-15-0 Carbon Disulfide ND 0.0053 0.0016 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0053 0.0011 mg/kg
108-90-7 Chlorobenzene ND 0.0053 0.0011 mg/kg
75-00-3 Chloroethane ND 0.0053 0.0021 mg/kg
67-66-3 Chloroform ND 0.0053 0.0011 mg/kg
110-82-7 Cyclohexane ND 0.0053 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0053 0.0011 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0053 0.0015 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0053 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0053 0.0015 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0053 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0053 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0053 0.0011 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0053 0.0011 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0053 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0053 0.0014 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0053 0.0011 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0053 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0053 0.0011 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
100-41-4 Ethylbenzene ND 0.0053 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.027 0.0087 mg/kg
98-82-8 Isopropylbenzene ND 0.0053 0.0011 mg/kg
79-20-9 Methyl Acetate ND 0.027 0.010 mg/kg
74-83-9 Methyl Bromide ND 0.0053 0.0023 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 62
FA29570 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-2 7'
Lab Sample ID:FA29570-2 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:79.7
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0053 0.0021 mg/kg
108-87-2 Methylcyclohexane ND 0.0053 0.0012 mg/kg
75-09-2 Methylene Chloride ND 0.011 0.0042 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.027 0.0057 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0053 0.0013 mg/kg
91-20-3 Naphthalene ND 0.0053 0.0021 mg/kg
103-65-1 n-Propylbenzene ND 0.0053 0.0011 mg/kg
100-42-5 Styrene ND 0.0053 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0053 0.0012 mg/kg
127-18-4 Tetrachloroethylene ND 0.0053 0.0017 mg/kg
108-88-3 Toluene 0.0040 0.0053 0.0011 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.0053 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0053 0.0014 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0053 0.0013 mg/kg
79-01-6 Trichloroethylene ND 0.0053 0.0011 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0053 0.0019 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0053 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0053 0.0011 mg/kg
75-01-4 Vinyl Chloride ND 0.0053 0.0017 mg/kg
1330-20-7 Xylene (total)ND 0.016 0.0022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 110%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 62
FA29570 33.2
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-2 7'
Lab Sample ID:FA29570-2 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP VPH REV 1.1 Percent Solids:79.7
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV072644.D 1 11/30/15 AH n/a n/a GUV3870
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.71 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.069 0.069 mg/kg
100-41-4 Ethylbenzene ND 0.14 0.069 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.14 0.069 mg/kg
91-20-3 Naphthalene ND 0.34 0.21 mg/kg
108-88-3 Toluene ND 0.14 0.069 mg/kg
m,p-Xylene ND 0.28 0.14 mg/kg
95-47-6 o-Xylene ND 0.14 0.069 mg/kg
C5- C8 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.9 2.4 mg/kg
C5- C8 Aliphatics ND 6.9 2.4 mg/kg
C9- C12 Aliphatics ND 6.9 2.4 mg/kg
C9- C10 Aromatics ND 6.9 2.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 123%70-130%
460-00-4 BFB 114%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 62
FA29570 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y24437.D 1 11/30/15 AD n/a n/a VY1030
Run #2
Initial Weight Final Volume
Run #1 5.92 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0370 0.050 0.015 mg/kg J
71-43-2 Benzene ND 0.0050 0.0010 mg/kg
75-27-4 Bromodichloromethane ND 0.0050 0.0010 mg/kg
75-25-2 Bromoform ND 0.0050 0.0010 mg/kg
78-93-3 2-Butanone (MEK)ND 0.025 0.0085 mg/kg
104-51-8 n-Butylbenzene ND 0.0050 0.0010 mg/kg
75-15-0 Carbon Disulfide ND 0.0050 0.0015 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0050 0.0010 mg/kg
108-90-7 Chlorobenzene ND 0.0050 0.0010 mg/kg
75-00-3 Chloroethane ND 0.0050 0.0020 mg/kg
67-66-3 Chloroform ND 0.0050 0.0010 mg/kg
110-82-7 Cyclohexane ND 0.0050 0.0010 mg/kg
124-48-1 Dibromochloromethane ND 0.0050 0.0010 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0050 0.0014 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0050 0.0010 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0050 0.0014 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0050 0.0010 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0050 0.0010 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0050 0.0010 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0050 0.0010 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0050 0.0010 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0050 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0050 0.0010 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0050 0.0010 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0050 0.0010 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0050 0.0010 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0050 0.0010 mg/kg
100-41-4 Ethylbenzene ND 0.0050 0.0010 mg/kg
591-78-6 2-Hexanone ND 0.025 0.0082 mg/kg
98-82-8 Isopropylbenzene ND 0.0050 0.0010 mg/kg
79-20-9 Methyl Acetate ND 0.025 0.0098 mg/kg
74-83-9 Methyl Bromide ND 0.0050 0.0022 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0050 0.0020 mg/kg
108-87-2 Methylcyclohexane ND 0.0050 0.0011 mg/kg
75-09-2 Methylene Chloride ND 0.010 0.0040 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.025 0.0054 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0050 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0050 0.0020 mg/kg
103-65-1 n-Propylbenzene ND 0.0050 0.0010 mg/kg
100-42-5 Styrene ND 0.0050 0.0010 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0050 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0050 0.0016 mg/kg
108-88-3 Toluene ND 0.0050 0.0010 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0050 0.0010 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0050 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0050 0.0013 mg/kg
79-01-6 Trichloroethylene ND 0.0050 0.0010 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0050 0.0018 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0050 0.0010 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0050 0.0010 mg/kg
75-01-4 Vinyl Chloride ND 0.0050 0.0016 mg/kg
1330-20-7 Xylene (total)ND 0.015 0.0021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 120%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 112%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684839.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.98 0.20 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.20 0.020 mg/kg
95-57-8 2-Chlorophenol ND 0.20 0.020 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.20 0.020 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.20 0.020 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.98 0.20 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.39 0.079 mg/kg
95-48-7 2-Methylphenol ND 0.20 0.020 mg/kg
3&4-Methylphenol ND 0.20 0.039 mg/kg
88-75-5 2-Nitrophenol ND 0.20 0.020 mg/kg
100-02-7 4-Nitrophenol ND 0.98 0.16 mg/kg
87-86-5 Pentachlorophenol ND 0.98 0.16 mg/kg
108-95-2 Phenol ND 0.20 0.020 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.20 0.020 mg/kg
83-32-9 Acenaphthene ND 0.20 0.020 mg/kg
208-96-8 Acenaphthylene ND 0.20 0.020 mg/kg
120-12-7 Anthracene ND 0.20 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.20 0.020 mg/kg
50-32-8 Benzo(a)pyrene ND 0.20 0.020 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.20 0.020 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.20 0.020 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.20 0.020 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.20 0.020 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.20 0.039 mg/kg
106-47-8 4-Chloroaniline ND 0.20 0.020 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.20 0.020 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.20 0.020 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.20 0.020 mg/kg
91-58-7 2-Chloronaphthalene ND 0.20 0.023 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.20 0.020 mg/kg
218-01-9 Chrysene ND 0.20 0.020 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.20 0.020 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.20 0.020 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.20 0.020 mg/kg
84-66-2 Diethyl Phthalate ND 0.39 0.039 mg/kg
131-11-3 Dimethyl Phthalate ND 0.20 0.039 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.20 0.039 mg/kg
84-74-2 Di-n-butyl Phthalate 0.224 0.39 0.039 mg/kg J
121-14-2 2,4-Dinitrotoluene ND 0.20 0.020 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.20 0.020 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.39 0.039 mg/kg
206-44-0 Fluoranthene ND 0.20 0.020 mg/kg
86-73-7 Fluorene ND 0.20 0.020 mg/kg
118-74-1 Hexachlorobenzene ND 0.20 0.020 mg/kg
87-68-3 Hexachlorobutadiene ND 0.20 0.020 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.20 0.039 mg/kg
67-72-1 Hexachloroethane ND 0.20 0.020 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 0.020 mg/kg
78-59-1 Isophorone ND 0.20 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.20 0.020 mg/kg
91-57-6 2-Methylnaphthalene ND 0.20 0.020 mg/kg
91-20-3 Naphthalene ND 0.20 0.020 mg/kg
98-95-3 Nitrobenzene ND 0.20 0.020 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.20 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.20 0.020 mg/kg
85-01-8 Phenanthrene ND 0.20 0.020 mg/kg
129-00-0 Pyrene ND 0.20 0.020 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 75%40-102%
4165-62-2 Phenol-d5 81%41-100%
118-79-6 2,4,6-Tribromophenol 92%42-108%
4165-60-0 Nitrobenzene-d5 78%40-105%
321-60-8 2-Fluorobiphenyl 82%43-107%
1718-51-0 Terphenyl-d14 91%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP VPH REV 1.1 Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV072645.D 1 11/30/15 AH n/a n/a GUV3870
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.35 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.057 0.057 mg/kg
100-41-4 Ethylbenzene ND 0.11 0.057 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.11 0.057 mg/kg
91-20-3 Naphthalene ND 0.28 0.17 mg/kg
108-88-3 Toluene ND 0.11 0.057 mg/kg
m,p-Xylene ND 0.23 0.11 mg/kg
95-47-6 o-Xylene ND 0.11 0.057 mg/kg
C5- C8 Aliphatics (Unadj.)ND 5.7 2.0 mg/kg
C9- C12 Aliphatics (Unadj.)ND 5.7 2.0 mg/kg
C9- C10 Aromatics (Unadj.)ND 5.7 2.0 mg/kg
C5- C8 Aliphatics ND 5.7 2.0 mg/kg
C9- C12 Aliphatics ND 5.7 2.0 mg/kg
C9- C10 Aromatics ND 5.7 2.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 116%70-130%
460-00-4 BFB 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-3 7'
Lab Sample ID:FA29570-3 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:84.3
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN014380.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
Run #2
Initial Weight Final Volume
Run #1 19.8 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.24 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.24 0.12 mg/kg
120-12-7 Anthracene ND 0.24 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.24 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.24 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.24 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.24 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.24 0.12 mg/kg
218-01-9 Chrysene ND 0.24 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.24 0.12 mg/kg
206-44-0 Fluoranthene ND 0.24 0.12 mg/kg
86-73-7 Fluorene ND 0.24 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.24 0.12 mg/kg
91-57-6 2-Methylnaphthalene ND 0.24 0.12 mg/kg
91-20-3 Naphthalene ND 0.24 0.12 mg/kg
85-01-8 Phenanthrene ND 0.24 0.12 mg/kg
129-00-0 Pyrene ND 0.24 0.12 mg/kg
C11-C22 Aromatics (Unadj.)ND 12 9.0 mg/kg
C11-C22 Aromatics ND 12 9.0 mg/kg
C9-C18 Aliphatics ND 12 6.0 mg/kg
C19-C36 Aliphatics ND 12 6.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 55%40-140%
580-13-2 2-Bromonaphthalene 79%40-140%
84-15-1 o-Terphenyl 57%40-140%
321-60-8 2-Fluorobiphenyl 77%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 62
FA29570 33.3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:SP-1
Lab Sample ID:FA29570-4 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8015C Percent Solids:86.7
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV072698.D 1 12/02/15 AH n/a n/a GUV3873
Run #2 a UV072655.D 1 11/30/15 AH n/a n/a GUV3871
Initial Weight Final Volume Methanol Aliquot
Run #1 6.11 g 5.0 ml 10.0 ul
Run #2 6.11 g 5.0 ml 100 ul
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)231 55 27 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 105%107%56-149%
98-08-8 aaa-Trifluorotoluene 100%100%66-132%
(a) Confirmation run.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 62
FA29570 33.4
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:SP-1
Lab Sample ID:FA29570-4 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8015C SW846 3546 Percent Solids:86.7
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ010380.D 1 12/01/15 SJL 11/30/15 OP58521 GJJ460
Run #2
Initial Weight Final Volume
Run #1 20.5 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28) a 97.2 7.0 4.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 102% b 56-122%
(a) Petroleum hydrocarbon pattern begins before C10.
(b) Calculated from actual spike mix concentration.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 62
FA29570 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y24438.D 1 11/30/15 AD n/a n/a VY1030
Run #2
Initial Weight Final Volume
Run #1 5.75 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0417 0.051 0.015 mg/kg J
71-43-2 Benzene ND 0.0051 0.0010 mg/kg
75-27-4 Bromodichloromethane ND 0.0051 0.0010 mg/kg
75-25-2 Bromoform ND 0.0051 0.0010 mg/kg
78-93-3 2-Butanone (MEK)ND 0.026 0.0087 mg/kg
104-51-8 n-Butylbenzene ND 0.0051 0.0010 mg/kg
75-15-0 Carbon Disulfide ND 0.0051 0.0015 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0051 0.0010 mg/kg
108-90-7 Chlorobenzene ND 0.0051 0.0010 mg/kg
75-00-3 Chloroethane ND 0.0051 0.0020 mg/kg
67-66-3 Chloroform ND 0.0051 0.0010 mg/kg
110-82-7 Cyclohexane ND 0.0051 0.0010 mg/kg
124-48-1 Dibromochloromethane ND 0.0051 0.0010 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0051 0.0014 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0051 0.0010 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0051 0.0014 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0051 0.0010 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0051 0.0010 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0051 0.0010 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0051 0.0010 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0051 0.0010 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0051 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0051 0.0010 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0051 0.0010 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0051 0.0010 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg
100-41-4 Ethylbenzene ND 0.0051 0.0010 mg/kg
591-78-6 2-Hexanone ND 0.026 0.0083 mg/kg
98-82-8 Isopropylbenzene ND 0.0051 0.0010 mg/kg
79-20-9 Methyl Acetate ND 0.026 0.010 mg/kg
74-83-9 Methyl Bromide ND 0.0051 0.0022 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 62
FA29570 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8260B Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0051 0.0020 mg/kg
108-87-2 Methylcyclohexane ND 0.0051 0.0011 mg/kg
75-09-2 Methylene Chloride ND 0.010 0.0041 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.026 0.0055 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0051 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0051 0.0020 mg/kg
103-65-1 n-Propylbenzene ND 0.0051 0.0010 mg/kg
100-42-5 Styrene ND 0.0051 0.0010 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0051 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0051 0.0017 mg/kg
108-88-3 Toluene ND 0.0051 0.0010 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0051 0.0010 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0051 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0051 0.0013 mg/kg
79-01-6 Trichloroethylene ND 0.0051 0.0010 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0051 0.0018 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0051 0.0010 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0051 0.0010 mg/kg
75-01-4 Vinyl Chloride ND 0.0051 0.0016 mg/kg
1330-20-7 Xylene (total)ND 0.015 0.0021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 101%75-126%
460-00-4 4-Bromofluorobenzene 111%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 62
FA29570 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684840.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.97 0.19 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.19 0.019 mg/kg
95-57-8 2-Chlorophenol ND 0.19 0.019 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.19 0.019 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.19 0.019 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.97 0.19 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.39 0.077 mg/kg
95-48-7 2-Methylphenol ND 0.19 0.019 mg/kg
3&4-Methylphenol ND 0.19 0.039 mg/kg
88-75-5 2-Nitrophenol ND 0.19 0.019 mg/kg
100-02-7 4-Nitrophenol ND 0.97 0.15 mg/kg
87-86-5 Pentachlorophenol ND 0.97 0.15 mg/kg
108-95-2 Phenol ND 0.19 0.019 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.19 0.020 mg/kg
83-32-9 Acenaphthene ND 0.19 0.019 mg/kg
208-96-8 Acenaphthylene ND 0.19 0.019 mg/kg
120-12-7 Anthracene ND 0.19 0.019 mg/kg
56-55-3 Benzo(a)anthracene ND 0.19 0.019 mg/kg
50-32-8 Benzo(a)pyrene ND 0.19 0.019 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.19 0.019 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.19 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.19 0.019 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.19 0.019 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.19 0.039 mg/kg
106-47-8 4-Chloroaniline ND 0.19 0.019 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.19 0.019 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.19 0.019 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.19 0.019 mg/kg
91-58-7 2-Chloronaphthalene ND 0.19 0.023 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.19 0.019 mg/kg
218-01-9 Chrysene ND 0.19 0.019 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.19 0.019 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 62
FA29570 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:SW846 8270D SW846 3550C Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.19 0.019 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.19 0.019 mg/kg
84-66-2 Diethyl Phthalate ND 0.39 0.039 mg/kg
131-11-3 Dimethyl Phthalate ND 0.19 0.039 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.19 0.039 mg/kg
84-74-2 Di-n-butyl Phthalate 0.142 0.39 0.039 mg/kg J
121-14-2 2,4-Dinitrotoluene ND 0.19 0.019 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.19 0.019 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.39 0.039 mg/kg
206-44-0 Fluoranthene ND 0.19 0.019 mg/kg
86-73-7 Fluorene ND 0.19 0.019 mg/kg
118-74-1 Hexachlorobenzene ND 0.19 0.019 mg/kg
87-68-3 Hexachlorobutadiene ND 0.19 0.019 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.19 0.039 mg/kg
67-72-1 Hexachloroethane ND 0.19 0.019 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.19 0.019 mg/kg
78-59-1 Isophorone ND 0.19 0.019 mg/kg
90-12-0 1-Methylnaphthalene ND 0.19 0.019 mg/kg
91-57-6 2-Methylnaphthalene ND 0.19 0.019 mg/kg
91-20-3 Naphthalene ND 0.19 0.019 mg/kg
98-95-3 Nitrobenzene ND 0.19 0.019 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.19 0.019 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.19 0.019 mg/kg
85-01-8 Phenanthrene ND 0.19 0.019 mg/kg
129-00-0 Pyrene ND 0.19 0.019 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 79%40-102%
4165-62-2 Phenol-d5 82%41-100%
118-79-6 2,4,6-Tribromophenol 92%42-108%
4165-60-0 Nitrobenzene-d5 78%40-105%
321-60-8 2-Fluorobiphenyl 84%43-107%
1718-51-0 Terphenyl-d14 94%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 62
FA29570 33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP VPH REV 1.1 Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV072647.D 1 11/30/15 AH n/a n/a GUV3870
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.84 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.060 0.060 mg/kg
100-41-4 Ethylbenzene ND 0.12 0.060 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.12 0.060 mg/kg
91-20-3 Naphthalene ND 0.30 0.18 mg/kg
108-88-3 Toluene ND 0.12 0.060 mg/kg
m,p-Xylene ND 0.24 0.12 mg/kg
95-47-6 o-Xylene ND 0.12 0.060 mg/kg
C5- C8 Aliphatics (Unadj.)ND 6.0 2.1 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.0 2.1 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.0 2.1 mg/kg
C5- C8 Aliphatics ND 6.0 2.1 mg/kg
C9- C12 Aliphatics ND 6.0 2.1 mg/kg
C9- C10 Aromatics ND 6.0 2.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 115%70-130%
460-00-4 BFB 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 62
FA29570 33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:CS-4 7'
Lab Sample ID:FA29570-5 Date Sampled:11/24/15
Matrix:SO - Soil Date Received:11/25/15
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:85.1
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN014381.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
Run #2
Initial Weight Final Volume
Run #1 20.1 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.23 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.23 0.12 mg/kg
120-12-7 Anthracene ND 0.23 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.23 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.23 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.23 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.23 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.23 0.12 mg/kg
218-01-9 Chrysene ND 0.23 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.23 0.12 mg/kg
206-44-0 Fluoranthene ND 0.23 0.12 mg/kg
86-73-7 Fluorene ND 0.23 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.23 0.12 mg/kg
91-57-6 2-Methylnaphthalene ND 0.23 0.12 mg/kg
91-20-3 Naphthalene ND 0.23 0.12 mg/kg
85-01-8 Phenanthrene ND 0.23 0.12 mg/kg
129-00-0 Pyrene ND 0.23 0.12 mg/kg
C11-C22 Aromatics (Unadj.)ND 12 8.8 mg/kg
C11-C22 Aromatics ND 12 8.8 mg/kg
C9-C18 Aliphatics ND 12 5.8 mg/kg
C19-C36 Aliphatics ND 12 5.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 62%40-140%
580-13-2 2-Bromonaphthalene 83%40-140%
84-15-1 o-Terphenyl 63%40-140%
321-60-8 2-Fluorobiphenyl 79%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 62
FA29570 33.5
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
30 of 62
FA29570 4
FA29570: Chain of Custody
Page 1 of 3
31 of 62
FA29570 44.1
FA29570: Chain of Custody
Page 2 of 3
32 of 62
FA29570 44.1
FA29570: Chain of Custody
Page 3 of 3
33 of 62
FA29570 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
34 of 62
FA29570 5
Method Blank Summary Page 1 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1030-MB Y24427.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 15 ug/kg
71-43-2 Benzene ND 5.0 1.0 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 8.5 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.5 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.0 ug/kg
110-82-7 Cyclohexane ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.4 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 1.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 8.2 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
79-20-9 Methyl Acetate ND 25 9.8 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.2 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.1 ug/kg
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 5.4 ug/kg
35 of 62
FA29570 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1030-MB Y24427.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.2 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.6 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.8 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.6 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%75-124%
17060-07-0 1,2-Dichloroethane-D4 102%72-135%
2037-26-5 Toluene-D8 107%75-126%
460-00-4 4-Bromofluorobenzene 121%71-133%
36 of 62
FA29570 55.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1030-BS Y24426.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 229 92 61-152
71-43-2 Benzene 50 56.5 113 76-126
75-27-4 Bromodichloromethane 50 57.9 116 74-130
75-25-2 Bromoform 50 56.4 113 76-127
78-93-3 2-Butanone (MEK)250 242 97 75-137
104-51-8 n-Butylbenzene 50 55.8 112 71-128
75-15-0 Carbon Disulfide 50 48.8 98 72-122
56-23-5 Carbon Tetrachloride 50 59.3 119 78-133
108-90-7 Chlorobenzene 50 54.7 109 81-129
75-00-3 Chloroethane 50 49.3 99 68-133
67-66-3 Chloroform 50 55.6 111 72-123
110-82-7 Cyclohexane 50 53.6 107 73-126
124-48-1 Dibromochloromethane 50 56.3 113 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 54.1 108 70-137
106-93-4 1,2-Dibromoethane 50 51.7 103 77-126
75-71-8 Dichlorodifluoromethane 50 48.6 97 68-168
95-50-1 1,2-Dichlorobenzene 50 56.8 114 80-129
541-73-1 1,3-Dichlorobenzene 50 57.9 116 81-129
106-46-7 1,4-Dichlorobenzene 50 57.6 115 76-130
75-34-3 1,1-Dichloroethane 50 57.4 115 73-125
107-06-2 1,2-Dichloroethane 50 55.2 110 74-128
75-35-4 1,1-Dichloroethylene 50 54.6 109 81-136
156-59-2 cis-1,2-Dichloroethylene 50 52.9 106 74-126
156-60-5 trans-1,2-Dichloroethylene 50 59.6 119 70-127
78-87-5 1,2-Dichloropropane 50 55.0 110 74-125
10061-01-5 cis-1,3-Dichloropropene 50 59.9 120 80-123
10061-02-6 trans-1,3-Dichloropropene 50 60.5 121 75-131
100-41-4 Ethylbenzene 50 56.4 113 77-123
591-78-6 2-Hexanone 250 234 94 72-133
98-82-8 Isopropylbenzene 50 51.5 103 80-136
79-20-9 Methyl Acetate 250 262 105 67-137
74-83-9 Methyl Bromide 50 52.5 105 65-139
74-87-3 Methyl Chloride 50 53.7 107 71-144
108-87-2 Methylcyclohexane 50 55.2 110 75-128
75-09-2 Methylene Chloride 50 40.6 81 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 234 94 76-132
* = Outside of Control Limits.
37 of 62
FA29570 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1030-BS Y24426.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 55.9 112 77-120
91-20-3 Naphthalene 50 57.5 115 79-129
103-65-1 n-Propylbenzene 50 58.1 116 80-135
100-42-5 Styrene 50 53.3 107 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 52.7 105 71-126
127-18-4 Tetrachloroethylene 50 50.0 100 79-130
108-88-3 Toluene 50 53.4 107 76-124
120-82-1 1,2,4-Trichlorobenzene 50 60.0 120 78-130
71-55-6 1,1,1-Trichloroethane 50 54.7 109 70-129
79-00-5 1,1,2-Trichloroethane 50 51.5 103 74-124
79-01-6 Trichloroethylene 50 55.4 111 75-128
75-69-4 Trichlorofluoromethane 50 51.3 103 73-145
95-63-6 1,2,4-Trimethylbenzene 50 56.9 114 74-123
108-67-8 1,3,5-Trimethylbenzene 50 60.9 122 73-122
75-01-4 Vinyl Chloride 50 52.7 105 76-141
1330-20-7 Xylene (total)150 157 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 99%72-135%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 103%71-133%
* = Outside of Control Limits.
38 of 62
FA29570 55.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA29570-2MS Y24435.D 1 11/30/15 AD n/a n/a VY1030
FA29570-2MSD Y24436.D 1 11/30/15 AD n/a n/a VY1030
FA29570-2 Y24434.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
FA29570-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 62.3 392 330 68 391 317 65 4 61-152/27
71-43-2 Benzene 1.3 J 78.4 75.1 94 78.2 76.2 96 1 76-126/26
75-27-4 Bromodichloromethane ND 78.4 78.6 100 78.2 79.2 101 1 74-130/25
75-25-2 Bromoform ND 78.4 74.8 95 78.2 73.9 94 1 76-127/26
78-93-3 2-Butanone (MEK)9.0 J 392 344 85 391 351 87 2 75-137/25
104-51-8 n-Butylbenzene ND 78.4 71.0 91 78.2 78.7 101 10 71-128/35
75-15-0 Carbon Disulfide ND 78.4 43.4 55*78.2 69.7 89 47*72-122/29
56-23-5 Carbon Tetrachloride ND 78.4 68.4 87 78.2 71.5 91 4 78-133/29
108-90-7 Chlorobenzene ND 78.4 73.5 94 78.2 74.9 96 2 81-129/29
75-00-3 Chloroethane ND 78.4 58.0 74 78.2 60.4 77 4 68-133/29
67-66-3 Chloroform ND 78.4 74.1 94 78.2 75.6 97 2 72-123/26
110-82-7 Cyclohexane ND 78.4 57.0 73 78.2 59.6 76 4 73-126/32
124-48-1 Dibromochloromethane ND 78.4 74.0 94 78.2 76.5 98 3 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 78.4 69.0 88 78.2 78.5 100 13 70-137/29
106-93-4 1,2-Dibromoethane ND 78.4 69.8 89 78.2 71.5 91 2 77-126/26
75-71-8 Dichlorodifluoromethane ND 78.4 48.5 62*78.2 50.0 64*3 68-168/29
95-50-1 1,2-Dichlorobenzene ND 78.4 77.3 99 78.2 80.2 103 4 80-129/32
541-73-1 1,3-Dichlorobenzene ND 78.4 78.3 100 78.2 81.3 104 4 81-129/33
106-46-7 1,4-Dichlorobenzene ND 78.4 80.2 102 78.2 82.0 105 2 76-130/32
75-34-3 1,1-Dichloroethane ND 78.4 71.3 91 78.2 73.4 94 3 73-125/27
107-06-2 1,2-Dichloroethane ND 78.4 77.6 99 78.2 77.4 99 0 74-128/23
75-35-4 1,1-Dichloroethylene ND 78.4 48.6 62*78.2 69.2 88 35*81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 78.4 71.8 92 78.2 72.3 92 1 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 78.4 73.6 94 78.2 75.4 96 2 70-127/27
78-87-5 1,2-Dichloropropane ND 78.4 77.7 99 78.2 78.6 100 1 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND 78.4 78.6 100 78.2 80.2 103 2 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 78.4 76.6 98 78.2 80.6 103 5 75-131/28
100-41-4 Ethylbenzene ND 78.4 75.9 97 78.2 77.7 99 2 77-123/31
591-78-6 2-Hexanone ND 392 349 89 391 369 94 6 72-133/26
98-82-8 Isopropylbenzene ND 78.4 64.2 82 78.2 68.0 87 6 80-136/32
79-20-9 Methyl Acetate ND 392 473 121 391 458 117 3 67-137/30
74-83-9 Methyl Bromide ND 78.4 69.1 88 78.2 68.3 87 1 65-139/31
74-87-3 Methyl Chloride ND 78.4 68.0 87 78.2 69.2 88 2 71-144/27
108-87-2 Methylcyclohexane ND 78.4 54.8 70*78.2 57.6 74*5 75-128/31
75-09-2 Methylene Chloride ND 78.4 94.7 121 78.2 94.0 120 1 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 392 351 90 391 369 94 5 76-132/26
* = Outside of Control Limits.
39 of 62
FA29570 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA29570-2MS Y24435.D 1 11/30/15 AD n/a n/a VY1030
FA29570-2MSD Y24436.D 1 11/30/15 AD n/a n/a VY1030
FA29570-2 Y24434.D 1 11/30/15 AD n/a n/a VY1030
The QC reported here applies to the following samples:Method: SW846 8260B
FA29570-1, FA29570-2, FA29570-3, FA29570-5
FA29570-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND 78.4 77.9 99 78.2 79.9 102 3 77-120/24
91-20-3 Naphthalene ND 78.4 70.6 90 78.2 79.0 101 11 79-129/33
103-65-1 n-Propylbenzene ND 78.4 74.5 95 78.2 80.4 103 8 80-135/33
100-42-5 Styrene ND 78.4 71.4 91 78.2 73.2 94 2 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND 78.4 73.5 94 78.2 78.3 100 6 71-126/30
127-18-4 Tetrachloroethylene ND 78.4 60.1 77*78.2 62.5 80 4 79-130/31
108-88-3 Toluene 4.0 J 78.4 71.8 86 78.2 75.9 92 6 76-124/30
120-82-1 1,2,4-Trichlorobenzene ND 78.4 80.5 103 78.2 90.2 115 11 78-130/34
71-55-6 1,1,1-Trichloroethane ND 78.4 68.7 88 78.2 70.8 91 3 70-129/27
79-00-5 1,1,2-Trichloroethane ND 78.4 72.6 93 78.2 73.7 94 2 74-124/28
79-01-6 Trichloroethylene ND 78.4 69.3 88 78.2 71.9 92 4 75-128/27
75-69-4 Trichlorofluoromethane ND 78.4 56.6 72*78.2 61.3 78 8 73-145/31
95-63-6 1,2,4-Trimethylbenzene ND 78.4 76.0 97 78.2 80.9 103 6 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 78.4 81.5 104 78.2 87.5 112 7 73-122/33
75-01-4 Vinyl Chloride ND 78.4 61.9 79 78.2 65.3 83 5 76-141/27
1330-20-7 Xylene (total)ND 235 209 89 235 222 95 6 80-129/30
CAS No.Surrogate Recoveries MS MSD FA29570-2 Limits
1868-53-7 Dibromofluoromethane 101%100%101%75-124%
17060-07-0 1,2-Dichloroethane-D4 100%98%114%72-135%
2037-26-5 Toluene-D8 95%99%104%75-126%
460-00-4 4-Bromofluorobenzene 102%106%110%71-133%
* = Outside of Control Limits.
40 of 62
FA29570 55.3.1
Accutest Laboratories
GC/MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 6
41 of 62
FA29570 6
Method Blank Summary Page 1 of 3
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-MB L0684827.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 17 ug/kg
95-57-8 2-Chlorophenol ND 170 17 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 17 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 17 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 17 ug/kg
3&4-Methylphenol ND 170 33 ug/kg
88-75-5 2-Nitrophenol ND 170 17 ug/kg
100-02-7 4-Nitrophenol ND 830 130 ug/kg
87-86-5 Pentachlorophenol ND 830 130 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 17 ug/kg
83-32-9 Acenaphthene ND 170 17 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 17 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 17 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 17 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 17 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 17 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 17 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 170 17 ug/kg
91-58-7 2-Chloronaphthalene ND 170 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 17 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 17 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
42 of 62
FA29570 66.1.1
Method Blank Summary Page 2 of 3
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-MB L0684827.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 33 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 17 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 17 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 17 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 17 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 17 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 17 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 77%40-102%
4165-62-2 Phenol-d5 82%41-100%
118-79-6 2,4,6-Tribromophenol 90%42-108%
4165-60-0 Nitrobenzene-d5 78%40-105%
321-60-8 2-Fluorobiphenyl 85%43-107%
1718-51-0 Terphenyl-d14 97%45-119%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
79-00-5 Ethane, 1,1,2-trichloro-3.19 170 ug/kg JN
43 of 62
FA29570 66.1.1
Method Blank Summary Page 3 of 3
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-MB L0684827.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method:
FA29570-1, FA29570-3, FA29570-5
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
79-34-5 Ethane, 1,1,2,2-tetrachloro-4.50 310 ug/kg JN
Total TIC, Semi-Volatile 480 ug/kg J
44 of 62
FA29570 66.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-BS L0684826.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 2770 83 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1400 84 52-108
95-57-8 2-Chlorophenol 1670 1330 80 48-104
120-83-2 2,4-Dichlorophenol 1670 1300 78 51-105
105-67-9 2,4-Dimethylphenol 1670 1210 73 43-96
51-28-5 2,4-Dinitrophenol 3330 2470 74 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3440 103 64-121
95-48-7 2-Methylphenol 1670 1360 82 46-107
3&4-Methylphenol 3330 2660 80 44-111
88-75-5 2-Nitrophenol 1670 1300 78 49-104
100-02-7 4-Nitrophenol 3330 2970 89 56-116
87-86-5 Pentachlorophenol 3330 2850 86 61-114
108-95-2 Phenol 1670 1400 84 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1520 91 56-109
83-32-9 Acenaphthene 1670 1590 95 56-109
208-96-8 Acenaphthylene 1670 1410 85 56-106
120-12-7 Anthracene 1670 1710 103 61-110
56-55-3 Benzo(a)anthracene 1670 1720 103 66-111
50-32-8 Benzo(a)pyrene 1670 1660 100 59-104
205-99-2 Benzo(b)fluoranthene 1670 1710 103 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1620 97 67-113
207-08-9 Benzo(k)fluoranthene 1670 1690 101 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1560 94 62-110
85-68-7 Butyl benzyl phthalate 1670 1580 95 65-113
106-47-8 4-Chloroaniline 1670 1160 70 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1280 77 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1250 75 46-103
108-60-1 bis(2-Chloroisopropyl)ether 1670 1280 77 40-110
91-58-7 2-Chloronaphthalene 1670 1350 81 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1430 86 58-106
218-01-9 Chrysene 1670 1790 107 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1700 102 68-115
132-64-9 Dibenzofuran 1670 1360 82 57-108
91-94-1 3,3'-Dichlorobenzidine 1670 1300 78 36-114
84-66-2 Diethyl Phthalate 1670 1480 89 61-109
131-11-3 Dimethyl Phthalate 1670 1470 88 59-108
* = Outside of Control Limits.
45 of 62
FA29570 66.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-BS L0684826.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1580 95 64-119
84-74-2 Di-n-butyl Phthalate 1670 1550 93 63-108
121-14-2 2,4-Dinitrotoluene 1670 1580 95 59-109
606-20-2 2,6-Dinitrotoluene 1670 1510 91 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1610 97 64-115
206-44-0 Fluoranthene 1670 1490 89 60-108
86-73-7 Fluorene 1670 1570 94 58-109
118-74-1 Hexachlorobenzene 1670 1520 91 59-111
87-68-3 Hexachlorobutadiene 1670 1170 70 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1480 89 49-110
67-72-1 Hexachloroethane 1670 1170 70 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1660 100 66-116
78-59-1 Isophorone 1670 1290 77 42-89
90-12-0 1-Methylnaphthalene 1670 1310 79 49-106
91-57-6 2-Methylnaphthalene 1670 1230 74 47-106
91-20-3 Naphthalene 1670 1190 71 44-104
98-95-3 Nitrobenzene 1670 1190 71 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1380 83 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1510 91 62-110
85-01-8 Phenanthrene 1670 1670 100 63-111
129-00-0 Pyrene 1670 1720 103 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 82%40-102%
4165-62-2 Phenol-d5 83%41-100%
118-79-6 2,4,6-Tribromophenol 94%42-108%
4165-60-0 Nitrobenzene-d5 74%40-105%
321-60-8 2-Fluorobiphenyl 82%43-107%
1718-51-0 Terphenyl-d14 103%45-119%
* = Outside of Control Limits.
46 of 62
FA29570 66.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-MS X043752.D 1 12/01/15 MV 11/30/15 OP58518 SX1970
OP58518-MSD L0684838.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
FA29570-1 L0684836.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
FA29570-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 4080 4060 99 4070 3200 79 24 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 2040 1910 94 2040 1630 80 16 52-108/21
95-57-8 2-Chlorophenol ND 2040 1730 85 2040 1600 79 8 48-104/26
120-83-2 2,4-Dichlorophenol ND 2040 1840 90 2040 1510 74 20 51-105/27
105-67-9 2,4-Dimethylphenol ND 2040 1690 83 2040 1440 71 16 43-96/23
51-28-5 2,4-Dinitrophenol ND 4080 3890 95 4070 2820 69 32 40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 4080 4270 105 4070 3950 97 8 64-121/29
95-48-7 2-Methylphenol ND 2040 1780 87 2040 1620 80 9 46-107/24
3&4-Methylphenol ND 4080 4260 104 4070 3160 78 30*44-111/24
88-75-5 2-Nitrophenol ND 2040 1770 87 2040 1460 72 19 49-104/27
100-02-7 4-Nitrophenol ND 4080 3940 96 4070 3700 91 6 56-116/23
87-86-5 Pentachlorophenol ND 4080 4270 105 4070 3380 83 23 61-114/23
108-95-2 Phenol ND 2040 1940 95 2040 1660 82 16 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 2040 1850 91 2040 1780 87 4 56-109/25
83-32-9 Acenaphthene ND 2040 1960 96 2040 1900 93 3 56-109/23
208-96-8 Acenaphthylene ND 2040 1770 87 2040 1690 83 5 56-106/23
120-12-7 Anthracene ND 2040 2050 100 2040 2010 99 2 61-110/21
56-55-3 Benzo(a)anthracene ND 2040 1990 97 2040 2080 102 4 66-111/23
50-32-8 Benzo(a)pyrene ND 2040 2030 99 2040 2020 99 0 59-104/23
205-99-2 Benzo(b)fluoranthene ND 2040 1980 97 2040 2020 99 2 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 2040 2140 105 2040 1900 93 12 67-113/21
207-08-9 Benzo(k)fluoranthene ND 2040 1960 96 2040 1980 97 1 67-114/22
101-55-3 4-Bromophenyl phenyl ether ND 2040 1860 91 2040 1750 86 6 62-110/21
85-68-7 Butyl benzyl phthalate ND 2040 1710 84 2040 1800 88 5 65-113/20
106-47-8 4-Chloroaniline ND 2040 1650 81 2040 1400 69 16 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 2040 1800 88 2040 1440 71 22 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 2040 1670 82 2040 1460 72 13 46-103/27
108-60-1 bis(2-Chloroisopropyl)ether ND 2040 1790 88 2040 1480 73 19 40-110/25
91-58-7 2-Chloronaphthalene ND 2040 1700 83 2040 1600 79 6 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 2040 1840 90 2040 1690 83 8 58-106/21
218-01-9 Chrysene ND 2040 2140 105 2040 2160 106 1 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 2040 2250 110 2040 1980 97 13 68-115/23
132-64-9 Dibenzofuran ND 2040 1790 88 2040 1650 81 8 57-108/22
91-94-1 3,3'-Dichlorobenzidine ND 2040 1670 82 2040 1460 72 13 36-114/28
84-66-2 Diethyl Phthalate ND 2040 1810 89 2040 1790 88 1 61-109/20
131-11-3 Dimethyl Phthalate ND 2040 1810 89 2040 1790 88 1 59-108/20
* = Outside of Control Limits.
47 of 62
FA29570 66.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58518-MS X043752.D 1 12/01/15 MV 11/30/15 OP58518 SX1970
OP58518-MSD L0684838.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
FA29570-1 L0684836.D 1 11/30/15 MV 11/30/15 OP58518 SL3754
The QC reported here applies to the following samples:Method: SW846 8270D
FA29570-1, FA29570-3, FA29570-5
FA29570-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
117-84-0 Di-n-octyl Phthalate ND 2040 1570 77 2040 1860 91 17 64-119/21
84-74-2 Di-n-butyl Phthalate 235 J 2040 2110 92 2040 1960 85 7 63-108/19
121-14-2 2,4-Dinitrotoluene ND 2040 1960 96 2040 1860 91 5 59-109/20
606-20-2 2,6-Dinitrotoluene ND 2040 1790 88 2040 1810 89 1 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 2040 1840 90 2040 1960 96 6 64-115/23
206-44-0 Fluoranthene ND 2040 1850 91 2040 1790 88 3 60-108/25
86-73-7 Fluorene ND 2040 1990 97 2040 1890 93 5 58-109/21
118-74-1 Hexachlorobenzene ND 2040 1800 88 2040 1750 86 3 59-111/21
87-68-3 Hexachlorobutadiene ND 2040 1580 77 2040 1250 61 23 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 2040 1680 82 2040 1420 70 17 49-110/31
67-72-1 Hexachloroethane ND 2040 1500 73 2040 1200 59 22 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 2040 2300 113 2040 1990 98 14 66-116/22
78-59-1 Isophorone ND 2040 1750 86 2040 1530 75 13 42-89/22
90-12-0 1-Methylnaphthalene ND 2040 1840 90 2040 1510 74 20 49-106/26
91-57-6 2-Methylnaphthalene ND 2040 1700 83 2040 1400 69 19 47-106/27
91-20-3 Naphthalene ND 2040 1740 85 2040 1340 66 26 44-104/27
98-95-3 Nitrobenzene ND 2040 1710 84 2040 1360 67 23 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 2040 2060 101 2040 1590 78 26 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 2040 1860 91 2040 1740 85 7 62-110/21
85-01-8 Phenanthrene ND 2040 1980 97 2040 1960 96 1 63-111/22
129-00-0 Pyrene ND 2040 1800 88 2040 2030 100 12 65-115/25
CAS No.Surrogate Recoveries MS MSD FA29570-1 Limits
367-12-4 2-Fluorophenol 86%79%70%40-102%
4165-62-2 Phenol-d5 91%80%77%41-100%
118-79-6 2,4,6-Tribromophenol 96%90%85%42-108%
4165-60-0 Nitrobenzene-d5 82%70%71%40-105%
321-60-8 2-Fluorobiphenyl 82%80%75%43-107%
1718-51-0 Terphenyl-d14 91%103%89%45-119%
* = Outside of Control Limits.
48 of 62
FA29570 66.3.1
Accutest Laboratories
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 7
49 of 62
FA29570 7
Method Blank Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3870-MB UV072637.D 1 11/30/15 AH n/a n/a GUV3870
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA29570-1, FA29570-2, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 51 51 ug/kg
100-41-4 Ethylbenzene ND 100 51 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 100 51 ug/kg
91-20-3 Naphthalene ND 260 150 ug/kg
108-88-3 Toluene ND 100 51 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene ND 100 51 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 97%70-130%
460-00-4 BFB 89%70-130%
50 of 62
FA29570 77.1.1
Method Blank Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3873-MB UV072697.D 1 12/02/15 AH n/a n/a GUV3873
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.5 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97%56-149%
98-08-8 aaa-Trifluorotoluene 96%66-132%
51 of 62
FA29570 77.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3873-BS UV072696.D 1 12/02/15 AH n/a n/a GUV3873
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 15.1 76 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 103%56-149%
98-08-8 aaa-Trifluorotoluene 100%66-132%
* = Outside of Control Limits.
52 of 62
FA29570 77.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3870-BS UV072634.D 1 11/30/15 AH n/a n/a GUV3870
GUV3870-BSD UV072635.D 1 11/30/15 AH n/a n/a GUV3870
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA29570-1, FA29570-2, FA29570-3, FA29570-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 4160 3450 83 3720 89 8 70-130/25
100-41-4 Ethylbenzene 4160 3530 85 3800 91 7 70-130/25
1634-04-4 Methyl Tert Butyl Ether 4160 3750 90 4190 101 11 70-130/25
91-20-3 Naphthalene 4160 3530 85 3730 90 6 70-130/25
108-88-3 Toluene 4160 3680 88 3970 95 8 70-130/25
m,p-Xylene 8320 6980 84 7510 90 7 70-130/25
95-47-6 o-Xylene 4160 3720 89 4020 97 8 70-130/25
C5- C8 Aliphatics (Unadj.)12500 14900 119 15500 124 4 70-130/25
C9- C12 Aliphatics (Unadj.)8320 8860 106 9420 113 6 70-130/25
C9- C10 Aromatics (Unadj.)4160 3430 82 3600 87 5 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 99%98%70-130%
460-00-4 BFB 90%89%70-130%
* = Outside of Control Limits.
53 of 62
FA29570 77.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA29549-2MS UV072704.D 1 12/02/15 AH n/a n/a GUV3873
FA29549-2MSD UV072705.D 1 12/02/15 AH n/a n/a GUV3873
FA29549-2 UV072700.D 1 12/02/15 AH n/a n/a GUV3873
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
FA29549-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 28.9 24.0 83 28.9 24.5 85 2 74-128/17
CAS No.Surrogate Recoveries MS MSD FA29549-2 Limits
460-00-4 4-Bromofluorobenzene 102%102%100%56-149%
98-08-8 aaa-Trifluorotoluene 101%102%97%66-132%
* = Outside of Control Limits.
54 of 62
FA29570 77.4.1
Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA29570-1DUP UV072643.D 1 11/30/15 AH n/a n/a GUV3870
FA29570-1 UV072642.D 1 11/30/15 AH n/a n/a GUV3870
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA29570-1, FA29570-2, FA29570-3, FA29570-5
FA29570-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FA29570-1 Limits
460-00-4 BFB 115%118%70-130%
460-00-4 BFB 105%108%70-130%
* = Outside of Control Limits.
55 of 62
FA29570 77.5.1
Accutest Laboratories
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 8
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FA29570 8
Method Blank Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58545-MB NN014375.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA29570-1, FA29570-3, FA29570-5
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 7500 ug/kg
C11-C22 Aromatics ND 10000 7500 ug/kg
C9-C18 Aliphatics ND 10000 5000 ug/kg
C19-C36 Aliphatics ND 10000 5000 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 52%40-140%
580-13-2 2-Bromonaphthalene 81%40-140%
84-15-1 o-Terphenyl 60%40-140%
321-60-8 2-Fluorobiphenyl 79%40-140%
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FA29570 88.1.1
Method Blank Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58521-MB JJ010345.D 1 11/30/15 SJL 11/30/15 OP58521 GJJ459
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 6.3 3.8 mg/kg
CAS No.Surrogate Recoveries Limits
84-15-1 o-Terphenyl 96% a 56-122%
(a) Calculated from actual spike mix concentration.
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FA29570 88.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58521-BS JJ010344.D 1 11/30/15 SJL 11/30/15 OP58521 GJJ459
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH (C10-C28)50 49.6 99 62-116
CAS No.Surrogate Recoveries BSP Limits
84-15-1 o-Terphenyl 112% a 56-122%
(a) Calculated from actual spike mix concentration.
* = Outside of Control Limits.
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FA29570 88.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58545-BS NN014376.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
OP58545-BSD NN014377.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA29570-1, FA29570-3, FA29570-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 3590 72 3200 64 11 40-140/30
208-96-8 Acenaphthylene 5000 3430 69 3090 62 10 40-140/30
120-12-7 Anthracene 5000 3910 78 3490 70 11 40-140/30
56-55-3 Benzo(a)anthracene 5000 4270 85 3800 76 12 40-140/30
50-32-8 Benzo(a)pyrene 5000 4390 88 3890 78 12 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 4550 91 4040 81 12 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 4070 81 3620 72 12 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 4170 83 3710 74 12 40-140/30
218-01-9 Chrysene 5000 4180 84 3730 75 11 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 4000 80 3560 71 12 40-140/30
206-44-0 Fluoranthene 5000 4120 82 3670 73 12 40-140/30
86-73-7 Fluorene 5000 3700 74 3300 66 11 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 3400 68 3020 60 12 40-140/30
91-57-6 2-Methylnaphthalene 5000 3320 66 2970 59 11 40-140/30
91-20-3 Naphthalene 5000 2990 60 2740 55 9 40-140/30
85-01-8 Phenanthrene 5000 4150 83 3690 74 12 40-140/30
129-00-0 Pyrene 5000 4250 85 3790 76 11 40-140/30
C11-C22 Aromatics (Unadj.)85000 63300 74 56600 67 11 40-140/30
C9-C18 Aliphatics 30000 17700 59 17600 59 1 40-140/30
C19-C36 Aliphatics 40000 31000 78 30700 77 1 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 67%66%40-140%
580-13-2 2-Bromonaphthalene 87%76%40-140%
84-15-1 o-Terphenyl 65%57%40-140%
321-60-8 2-Fluorobiphenyl 81%72%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP58545-BS 2-Methylnaphthalene 3320 ND 0.0%5.0
OP58545-BS Naphthalene 2990 ND 0.0%5.0
OP58545-BSD 2-Methylnaphthalene 2970 ND 0.0%5.0
OP58545-BSD Naphthalene 2740 ND 0.0%5.0
* = Outside of Control Limits.
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FA29570 88.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58521-MS JJ010350.D 1 11/30/15 SJL 11/30/15 OP58521 GJJ459
OP58521-MSD JJ010351.D 1 11/30/15 SJL 11/30/15 OP58521 GJJ459
FA29463-1 JJ010346.D 1 11/30/15 SJL 11/30/15 OP58521 GJJ459
The QC reported here applies to the following samples:Method: SW846 8015C
FA29570-4
FA29463-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH (C10-C28)ND 72 62.8 87 72.7 63.3 87 1 62-116/35
CAS No.Surrogate Recoveries MS MSD FA29463-1 Limits
84-15-1 o-Terphenyl 110% a 101% a 96% a 56-122%
(a) Calculated from actual spike mix concentration.
* = Outside of Control Limits.
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FA29570 88.4.1
Duplicate Summary Page 1 of 1
Job Number:FA29570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 5; 101 W Jefferson St (Hwy 158), Jackson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP58545-DUP NN014379.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
FA29570-1 NN014378.D 1 12/02/15 FS 12/01/15 OP58545 GNN675
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA29570-1, FA29570-3, FA29570-5
FA29570-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 a
208-96-8 Acenaphthylene ND ND nc 30 a
120-12-7 Anthracene ND ND nc 30 a
56-55-3 Benzo(a)anthracene ND ND nc 30 a
50-32-8 Benzo(a)pyrene ND ND nc 30 a
205-99-2 Benzo(b)fluoranthene ND ND nc 30 a
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a
207-08-9 Benzo(k)fluoranthene ND ND nc 30 a
218-01-9 Chrysene ND ND nc 30 a
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a
206-44-0 Fluoranthene ND ND nc 30 a
86-73-7 Fluorene ND ND nc 30 a
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a
91-57-6 2-Methylnaphthalene ND ND nc 30 a
91-20-3 Naphthalene ND ND nc 30 a
85-01-8 Phenanthrene ND ND nc 30 a
129-00-0 Pyrene ND ND nc 30 a
C11-C22 Aromatics (Unadj.)ND ND nc 30 a
C11-C22 Aromatics ND ND nc 30 a
C9-C18 Aliphatics ND ND nc 30 a
C19-C36 Aliphatics ND ND nc 30 a
CAS No.Surrogate Recoveries DUP FA29570-1 Limits
3386-33-2 1-Chlorooctadecane 71%64%40-140%
580-13-2 2-Bromonaphthalene 97%72%40-140%
84-15-1 o-Terphenyl 68%52%40-140%
321-60-8 2-Fluorobiphenyl 92%71%40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
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FA29570 88.5.1