RA-6738_33892_CA_RPTS_20160217_MRP

2512 Independence Blvd., Suite 200-34
Wilmington, North Carolina 28412
Telephone [phone]
Fax [phone]
www.atcgroupservices.com

February 17, 2016

Mr. Sean Patrick
North Carolina Department of Environmental Quality
Raleigh Regional Office
Division of Waste Management - UST Section
1628 Mail Service Center
Raleigh, North Carolina 27699-1628

Re: Initial Pre-CAP Monitoring Report
Pantry #3471
4940 U.S. Highway 264 West
Wilson, Wilson County, North Carolina
NCDEQ Incident No. 33892
NCDEQ Risk Classification: H155A

Dear Mr. Patrick:

ATC Associates of North Carolina, P.C. (ATC), on behalf of Circle K, Inc., is submitting this Initial
Pr-Corrective Action Plan (CAP) Monitoring Report to document the installation of a Type III monitoring
well for vertical delineation and the results of the recent soil and groundwater sampling events.

If you have any questions or require additional information, please contact our office at [phone].

Sincerely,
ATC Associates of North Carolina, P.C.

Maureen Jackson, P.G.
Senior Project Manager

cc: Mr. Brent Puzak, Circle K

Initial Pre-CAP Monitoring Report
Pantry #3471
4940 U.S. Highway 264 West
Wilson, Wilson County, North Carolina
NCDEQ Incident No. 33892
NCDEQ Risk Classification: H155A
February 17, 2016

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892

TABLE OF CONTENTS
1.0 INTRODUCTION..................................................................................................1
2.0 SITE BACKGROUND ..........................................................................................1
3.0 SOIL SAMPLING .................................................................................................3
4.0 MONITORING WELL INSTALLATION .........................................................4
5.0 GROUNDWATER MONITORING ....................................................................4
5.1 Groundwater Elevations .......................................................................................4
5.2 Groundwater Analytical Results ..........................................................................5
5.3 Water Supply Well Sampling ..............................................................................5
6.0 CONCLUSIONS AND RECOMMENDATIONS ...............................................6

TABLES

Table 1 UST System Information
Table 2 Water Supply Well Information
Table 3 Soil Analytical Data
Table 4 Monitoring Well Construction Details
Table 5 Groundwater Elevation Data
Table 6 Historical Groundwater Elevation Data
Table 7 Groundwater Analytical Data
Table 8 Historical Groundwater Analytical Data
Table 9 Water Supply Well Analytical Data

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Site Vicinity Map
Figure 4 Soil Boring Location Map
Figure 5 Geologic Cross-Section Transect Map
Figure 6 Geologic Cross-Section A-A’
Figure 7 Geologic Cross-Section B-B’

APPENDICES

Appendix A Boring Logs and Monitoring Well Construction Records
Appendix B Laboratory Reports and Chain-of-Custody Documents

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 1

1.0 INTRODUCTION
ATC Associates of North Carolina, P.C. (ATC), on behalf of The Pantry, Inc. (Pantry), is submitting this
Initial Pre-Corrective Action Plan (CAP) Monitoring Report for the Pantry #3471 facility located at 4940
U.S. Highway 264 West, Wilson, North Carolina (Incident # 33892). A site topographic map is
presented as Figure 1 and a site map is presented as Figure 2.

The Pantry #3471 (Facility ID No. 0-035356) is currently a single-story convenience store with retail
fuel. Five underground storage tanks (USTs) are currently in operation at the site. The USTs include
one 15,000-gallon gasoline UST, one 12,000-gallon gasoline UST, one 10,000-gallon kerosene UST, and
two 15,000-gallon diesel USTs. The site is located at 4940 U.S. Highway 264 West in Wilson, North
Carolina. The zoning designation for the site is Business. North of the site property is Bloomery
Swamp. East of the site is a Citgo Station/Subway followed by The Waffle House. To the south beyond
Raleigh Road Parkway (US 264 West), is K Mart #2 Shell Station and Aunt Sarah’s Pancake House
followed by Quality Inn Hotel. To the west is a vacant undeveloped parcel. This report documents the
soil sampling event conducted on November 30, 2015, the monitoring well installation event conducted
November 20, 2015, and the groundwater sampling events conducted on November 24, 2015 and January
26, 2016.
2.0 SITE BACKGROUND
The site currently operates as a convenience store and retail fuel sales facility. The USTs were installed in
December 1996. UST system information is summarized in Table 1.

On February 17, 2009, the North Carolina Department of Environmental Quality (NCDEQ) conducted a
compliance inspection at the Pantry #3471. On February 18, 2009, NCDEQ issued a Notice of Violation
(NOV) to the Pantry as the premium gasoline UST was not in compliance with current NC UST
regulations. In the NOV, the following violations were noted: premium UST did not have any spill
protection, failure to report a suspected release, and failure to investigate a suspected release.

In response to the NOV, ATC personnel initiated site check activities. As part of the site check
activities, a soil boring (SB-1) was collected near the premium gasoline UST fill port. The soil analytical
data did not detect total petroleum hydrocarbons (TPH) - gasoline range organics (GRO) above the
established NCDEQ Action Level of 10 micrograms/kilogram (mg/kg). A Site Check Report was
submitted to NCDEQ on July 9, 2009.

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 2

In response to the findings presented in the Site Check Report, NCDEQ issued a Notice of Regulatory
Requirements (NORR) on November 16, 2009 requesting a site check addendum. On January 20, 2010,
ATC supervised the installation of monitoring well MW-1. Subsequently, a groundwater sample was
collected from well MW-1. Groundwater laboratory analytical results of the groundwater sample
collected from monitoring well MW-1 indicated target compound concentrations exceeding the NCDEQ
Groundwater Quality 2L Standards (2L Standards).

Based on the results of the groundwater sample, NDEQ issued a NORR, September 8, 2010, requesting a
limited site check in the area of the diesel and kerosene UST systems. ATC advanced forty-seven soil
borings at various locations around the site. Laboratory analytical results of the soil samples detected
TPH-diesel range organics (DRO) above the established action level in several of the soil samples. A
second monitoring well, MW-2, was installed at the site adjacent to the diesel dispensers. Laboratory
analytical results of the groundwater sample collected from monitoring well MW-2 did not detect target
compound concentrations above established 2L Standards. A receptor survey was completed during this
time and two potable water supply wells (one active and one inactive) were identified within 1,500 feet of
the site. A Site Check and Receptor Survey Report was submitted to NCDEQ on January 3, 2011.

During May 2011, The Pantry installed spill containment sumps at eight of the twelve gasoline dispenser
islands. During these activities, petroleum staining and odor was detected in the soil. Between May and
June 2011, as part of initial abatement activities, approximately 35.89 tons of petroleum-impacted soil
was excavated from the site for off-site disposal. Laboratory analytical results of soil samples detected
TPH-DRO and TPH-GRO above the action level for several of the soil samples.

During February 2013, The Pantry conducted gasoline piping replacement at six of the gasoline
dispensers located on the eastern portion of the property. During these activities, petroleum staining and
odor was detected in the soil. As part of initial abatement activities, approximately 200 tons of
petroleum-impacted soil was excavated from the site for off-site disposal. Laboratory analytical results
of soil samples detected TPH-DRO and TPH-GRO above the action level for several of the soil samples.
Based on the soil analytical results, a Phase I Limited Site Assessment (LSA) was initiated.

As part of LSA activities, three monitoring wells were installed and subsequently sampled. Free product
was measured in monitoring well MW-3 at a thickness of 0.58 feet. Laboratory analytical results of the
groundwater samples collected from the remaining wells detected target compound concentrations in
exceedance of 2L Standards. ATC also conducted a receptor survey which identified one water supply

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 3
well within 1,000 feet of the site. The well, PW-1, is located approximately 550 feet southwest of the site
and is used for drinking purposes. Receptor information is summarized in Table 2 and the location of the
water supply well is noted on Figure 3. Based on a “high risk” classification of the site, ATC
recommended the completion of a Comprehensive Site Assessment (CSA).

CSA activities were conducted at the site in February 2015. During CSA activities, six monitoring wells
were advanced to delineate impacted groundwater at the site, a comprehensive groundwater sampling event
was conducted and slug testing was performed to determine aquifer characteristics. Based on laboratory
analytical results of the groundwater samples, dissolved target compound concentrations exceeding 2L
Standards were observed in several monitoring wells. A CSA Report was submitted to NCDEQ on May 8,
2015.

On August 3, 2015, NCDEQ issued a NORR for deficiencies noted in the CSA Report: soil
contamination was not delineated using risk-based analytical parameters and the vertical delineation of
petroleum-impacted groundwater above 2L Standards was not completed. The preparation and submittal
of an Initial Pre-CAP Monitoring Report was requested prior to the preparation and submittal of a
Corrective Action Plan.

This report documents the performance of risk-based soil sampling at various locations around the site as
well as the installation and subsequent groundwater sampling of a Type III monitoring well, and the
sampling of water supply well, PW-1.

3.0 SOIL SAMPLING
On November 30, 2015, soil sampling was performed by ATC to assist in the vertical and horizontal
delineation of petroleum-impacted soil at the referenced site. The soil samples were collected for
laboratory analyses using direct-push technology. The sample collection depth was approximately five
and one-half feet to seven feet below ground surface (bgs). Soil borings are provided in Appendix A.

Upon collection, the soil samples were placed in laboratory-supplied containers, labeled (SD-10, SD-11,
SD-13, SD-17, SD-19, SD-25, SD-26, SK-25, and SK-30), and placed in ice and delivered under
chain-of-custody to Pace Analytical Services, Inc. (Pace) in Huntersville, North Carolina for analyses.
The soil samples were analyzed for volatile organic compounds (VOCs) via EPA Method 8260 and
semi-volatile organic compounds (SVOCs) via EPA Method 8270. Additionally, the soil samples were
analyzed by Massachusetts Department of Environmental Protection (MADEP) Methods for volatile

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 4
petroleum hydrocarbon fractions (VPH) and extractable petroleum hydrocarbon fractions (EPH). The
soil sample locations are depicted in Figure 4.

The presence of petroleum-related impacts to soil, above Soil-to-Groundwater Maximum Contaminant
Concentrations (STGW-MSCCs), were identified in soil samples SD-10 and SK-30. Soil sample SD-10
was collected near the gasoline dispenser islands and sol sample SK-30 was located near the kerosene
product line. It should be noted petroleum-related impacts to soil were not identified above the
applicable residential MSCCs. Table 3 provides a summary of laboratory results of the soil sample
submitted for analyses. Copies of the laboratory report and chain-of-custody documents are included in
Appendix B.
4.0 MONITORING WELL INSTALLATION
On November 19 and 20, 2015, ATC provided oversight for the installation of Type III monitoring well
DW-2 for vertical delineation purposes. This well was installed by Geologic Exploration, Inc. of
Statesville, North Carolina. The location of the well is provided in Figure 2.

Construction of deep well DW-2 included the installation of a six-inch diameter, schedule-40 PVC outer
casing using the hollow-stem auger drilling method. The casing was set at 40 feet bgs. A two-inch
diameter, schedule-40 PVC inner well casing and 0.010-inch slot PVC well screen were installed using
the mud rotary/rock drilling method. The total well depth for deep well DW-2 is 80 feet bgs with a
five-foot screened interval from 75 to 80 feet bgs.

The filter pack for the deep well was placed in the well annulus to two feet above the well screen. A
four-foot-thick bentonite seal for the well was placed above the filter pack, and neat cement was used to
fill the remaining well annulus to ground surface.

The well was installed as flush-mounted and was provided with a sealing and locking cap. A protective
traffic-bearing cover was placed over the well upon completion. Well construction details are provided
in Table 4. The boring and well construction record are provided in Appendix A.

5.0 GROUNDWATER MONITORING
5.1 Groundwater Elevations
On November 24, 2015, ATC collected a depth to water measurement from well DW-2 (8.46 feet bgs).
During the groundwater resampling event on January 26, 2016, a depth to water measurement was again
collected from well DW-2 (7.22 feet bgs). Based on historical groundwater elevation data, presented in

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 5
previous reports on file at DEQ, groundwater appears to flow north to northeast across the site. Current
groundwater elevation data is provided in Table 5. Historical groundwater elevation data is included in
Table 6.

5.2 Groundwater Analytical Results
On November 24, 2015, ATC personnel collected a groundwater sample from monitoring well DW-2.
The sample was collected into laboratory-approved containers, packed in ice and delivered under
chain-of-custody to Pace in Huntersville, North Carolina. The groundwater sample was analyzed for
VOCs via EPA Method 6200B, SVOCs by EPA Method 625, EPA Method 6010 for lead, and MADEP
Methods for VPH and EPH.

Laboratory analytical results of the groundwater sample collected from well DW-2 detected dissolved
benzene at a concentration exceeding the established 2L Standard. Dissolved MTBE and
Bis(2-ethylhexyl)phthalate concentrations were detected above the laboratory method detection limit
(MDL) but below established 2L Standards. ATC does not believe that the presence of
Bis(2-Ethylhexyl)phthalate is related to the petroleum release as this compound is generally used in the
manufacturing of plastics.

On January 26, 2016, ATC personnel re-sampled monitoring well DW-2 to confirm the presence of
dissolved benzene above 2L Standard. The sample was collected into laboratory-approved containers,
packed in ice and delivered under chain-of-custody to Con-test Analytical Laboratory (Con-test) in east
Longmeadow, Massachusetts. The groundwater sample was analyzed via EPA Method 6200B.

Laboratory analytical results of the groundwater sample collected from well DW-2 during January 2016 did
not detect the presence of dissolved target compound concentrations above established 2L Standards.

A summary of the recent groundwater analytical data is presented in Table 7 and a historical summary of
groundwater analytical data is presented in Table 8. Geologic Cross-Sections are presented as Figures 5
through 7. Isoconcentration contour maps of contaminants of concern are presented in previous reports
on file at DEQ. Copies of the laboratory analytical reports are included as Appendix B.

5.3 Water Supply Well Sampling
On November 24, 2015, ATC personnel sampled the active water supply well (labeled PW-1) located at
4957 Raleigh Road Parkway. The approximate location of the water supply well is provided in Figure 3.
Prior to the collection of the sample, a spigot located at the front of the residence was allowed to run for

Initial Pre-CAP Monitoring Report February 17, 2016
NCDEQ Incident No. 33892
Page 6
approximately 15 minutes. The sample was collected into laboratory-approved containers, packed in ice
and delivered under chain-of-custody to Pace in Huntersville, North Carolina, and submitted for chemical
analysis by EPA Method 6200B. The laboratory analytical results did not detect target compound
concentrations above the laboratory MDLs. Current analytical data for the water supply well is included
in Table 9. The laboratory analytical report is presented in Appendix B.

6.0 CONCLUSIONS AND RECOMMENDATIONS
ATC has performed a soil sampling event, monitoring well installation, and groundwater sampling event
at the Pantry #3471 facility in Wilson, North Carolina. Based on field activities, observations, and soil
and groundwater analytical results, ATC concludes the following:

· Laboratory analytical results of soil samples SD-10 and SK-30 detected target compound
concentrations above established STGW-MSCCs but below Residential MSCCs. Soil sample SD-10
was collected near the gasoline dispensers and soil sample SK-30 was collected near the kerosene
product line;
· The land use classification for this site should be Residential; therefore, it appears soil has been
adequately defined at the site;
· The inferred shallow groundwater flow direction is to the north and northeast across the site;
· It appears water supply well PW-1 is located hydraulically upgradient of the source area;
· A groundwater sample collected from water supply well PW-1 did not detect target compound
concentrations above laboratory MDLs;
· Type III monitoring well DW-2 was installed and subsequently sampled. A groundwater sample
collected from this well during January 2016 did not detect dissolved target compound
concentrations above 2L Standards; therefore, vertical delineation has been completed;
· Based on information submitted in the CSA Report on file at NCDEQ, it appears the dissolved
petroleum plume has been horizontally defined.

ATC recommends the installation of Biosocks in select wells to assist with natural attenuation activities.
ATC recommends semi-annual groundwater sampling and reporting.

TABLES
TABLE 1
UST SYSTEM INFORMATION
PANTRY # 3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
UST ID
Number Product Capacity
(gallons)
Date
Installed
Date taken out of
Use
Date
Permanently
Closed
Was Release
Associated With
UST System?
1 Gasoline 15,000 12/18/1996 Currently in Use Not Applicable Unknown
2 Gasoline 12,000 12/18/1996 Currently in Use Not Applicable Unknown
3 Kerosene 10,000 12/18/1996 Currently in Use Not Applicable Unknown
4 Diesel 15,000 12/18/1996 Currently in Use Not Applicable Unknown
5 Diesel 15,000 12/18/1996 Currently in Use Not Applicable Unknown
Facility ID
No.
Owner or
Operator?
0-035356 Owner
Name of Owner or OperatorDates of Ownership / Operation
The Pantry, Inc.2001 to Present
Sanford, North Carolina 27330
Address Telephone Number
1801 Douglas Drive [phone]
TABLE 2
WATER SUPPLY WELL INFORMATION
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
Well ID
Last 6
digits of
PIN
Property Owner and Address Property Address Property Use/Tenant Well Use
Distance
from
Source
(feet)
Connected to
Municipal
Water
Virginia Hayes
4957 Raleigh Road Parkway
Wilson, NC
PW-2 74-7531 Beulah and Hazel Finch
5730 Lamm Road Wilson, NC
Raleigh Road
Parkway
Agricultural with
Abandoned/Delapitated
Residence
Not used due
to abandoned
house
1,500 No
Location of water supply well PW-1 can be referenced on Figure 3.
PW-1 4957 Raleigh Road
Parkway Residential Drinking 550 No41-5379
TABLE 3
SOIL ANALYTICAL DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
BenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthaleneAcetone1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenep-IsopropyltolueneIsopropylbenzenen-Butylbenzenesec-Butylbenzenen-PropylbenzeneMethylene ChlorideSD-10 7 11/30/15 74.1 <0.100 <0.113 0.12J <0.226 <0.0941 0.956 <0.627 1.67 0.269J 0.407 0.222J 0.95 0.589 0.429 <0.188
SD-11 7 11/30/15 26.7 <0.0019 <0.0022 <0.0022 <0.0043 <0.0018 <0.0014 <0.0121 <0.0024 <0.0022 <0.0020 <0.0023 <0.0022 <0.0019 <0.0020 0.0087J
SD-13 7 11/30/15 12.6 <0.0022 <0.0024 <0.0024 <0.0049 <0.0020 0.004J <0.0135 <0.0027 <0.0024 <0.0023 <0.0026 <0.0024 <0.0022 <0.0023 0.0065J
SD-17 7 11/30/15 N/A <0.0020 <0.0022 <0.0022 <0.0044 <0.0018 <0.0015 0.0517J <0.0024 <0.0022 <0.0021 <0.0023 <0.0022 <0.0020 <0.0021 0.0126J
SD-19 4 11/30/15 0.1 <0.0020 <0.0023 <0.0023 <0.0046 <0.0019 <0.0015 0.0317J <0.0026 <0.0023 <0.0022 <0.0024 <0.0023 <0.0020 <0.0022 0.0043J
SD-25 5 11/30/15 0.8 <0.0016 <0.0017 <0.0017 <0.0035 <0.0015 <0.0012 0.0278J <0.0019 <0.0017 <0.0016 <0.0018 <0.0017 <0.0016 <0.0016 <0.0029
SD-26 5.5 11/30/15 5.6 <0.0018 <0.002 <0.002 <0.0039 <0.0016 <0.0013 0.0131J <0.0022 <0.0020 <0.0019 <0.0021 <0.0020 <0.0018 <0.0019 <0.0033
SK-25 7 11/30/15 1.4 <0.0022 <0.0025 <0.0025 <0.0049 <0.0020 <0.0016 0.0177J <0.0027 <0.0025 <0.0023 <0.0026 <0.0025 <0.0022 <0.0023 0.0083J
SK-30 7 11/30/15 3.7 <0.0021 <0.0024 <0.0024 <0.0048 <0.0020 <0.0016 0.0249J <0.0027 <0.0024 <0.0023 <0.0025 <0.0024 <0.0021 <0.0023 0.0128J
0.0056 4.3 4.9 4.6 0.091 0.16 24 8.5 8.3 0.12 1.7 4.3 3.3 1.7 0.02
18 1,200 1,560 3,129 350 313 14,000 782 782 100 1,564 626 626 626 85
164 32,000 40,000 81,760 3,100 8,176 360,000 20,440 20,440 4,000 40,880 16,350 16,350 16,350 763
Benzo(a) anthraceneBenzo(a) pyreneBenzo(b) fluorantheneChryseneFluor-anthenePhenanthrenePyrene1-Methylnaphthalene2-MethylnaphthaleneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsSD-10 7 11/30/15 74.1 <0.0797 <0.0823 <0.0745 <0.0575 <0.0627 <0.0719 <0.0732 0.149J 0.228J 10.9 318.6 <105 184.3
SD-11 7 11/30/15 26.7 <0.0783 <0.0808 <0.0731 <0.0565 <0.0616 <0.0706 <0.0719 <0.110 <0.0911 <3.5 <16.3 <12.8 <16.3
SD-13 7 11/30/15 12.6 <0.0857 <0.0885 <0.0800 <0.0618 <0.0674 <0.0772 <0.0786 <0.121 <0.0997 <3.8 <17.8 <14.0 <17.8
SD-17 7 11/30/15 N/A <0.0701 <0.0724 <0.0655 <0.0506 <0.0552 <0.0632 <0.0643 <0.0988 <0.0816 <2.6 44.9 <11.5 22.4
SD-19 4 11/30/15 0.1 <0.0641 <0.0662 <0.0599 <0.0463 <0.0505 <0.0578 <0.0589 <0.0904 <0.0747 <4.1 <14.6 <10.5 <14.6
SD-25 5 11/30/15 0.8 <0.0634 <0.0655 <0.0593 <0.0457 0.0804J 0.0585J 0.0687J <0.0894 <0.0738 <4.1 <14.5 <10.4 <14.5
SD-26 5.5 11/30/15 5.6 <0.0644 <0.0665 <0.0601 <0.0464 <0.0506 <0.0580 <0.0591 <0.0907 <0.0749 <3.0 <13.6 <10.6 <13.6
SK-25 7 11/30/15 1.4 <0.0797 <0.0823 <0.0745 <0.0575 <0.0627 <0.0719 <0.0732 <0.112 <0.0928 <4.1 <17.2 <13.1 <17.2
SK-30 7 11/30/15 3.7 0.110J 0.090J 0.115J 0.117J 0.343J 0.175J 0.296J <0.119 <0.0985 <4.4 <18.3 <13.9 32
0.35 0.096 1.2 39 290 56 270 0.004 3.6 68 540 #31
0.88 0.088 0.88 88 620 469 469 20 63 939 1,500 31,000 469
8 0.78 8 780 16,400 12,264 12,264 100 1635 24,528 40,000 810,000 12,264
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. The MADEP VPH and EPH values were obtained from Table 10 in the "Guidelines for Assessment and corrective Action for UST Releases, dated July 15, 2008, updated October 2012.
3. MSCCs = Maximum Soil Contaminant Concentration
4. Bold concentrations equal or exceed Soil-to-Groundwater MSCCs.
5. # - Considered Immobile
6. "<" denotes compound not detected above laboratory method detection limit.
7. J value denotes estimated concentration by the laboratory.
PID
Reading
(ppm)
Industrial/Commercial MSCCs
Soil-to-Groundwater MSCCs
Residential MSCCs
EPA Method 8260
Soil
Sample
ID
Sample
Depth
(feet)
Soil-to-Groundwater MSCCs
Residential MSCCs
Industrial/Commercial MSCCs
EPA Method 8270 MADEP Methods for VPH and EPH
Sampling
Date
PID
Reading
(ppm)
Soil
Sample
ID
Sample
Depth
(feet)
Sampling
Date
TABLE 4
MONITORING WELL CONSTRUCTION DETAILS
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
Monitoring
Well ID
Date of
Construction
Well
Diameter
(inches)
Screen
Slot Size
(inches)
Total Well
Depth (ft)
Screen
Interval
(feet)Comments
MW-1 1/20/2010 2 0.01 13 3-13 Active
MW-2 11/9/2010 2 0.01 12 4-12 Active
MW-3 8/2/2013 2 0.01 14 4-15 Active
MW-4 8/2/2013 2 0.01 15 5-15 Active
MW-5 8/2/2013 2 0.01 15 5-15 Active
MW-6 2/12/2015 2 0.01 25 5.5-25 Active
MW-7 2/12/2015 2 0.01 25 5.5-25 Active
MW-8 2/12/2015 2 0.01 25 5.5-25 Active
MW-9 2/12/2015 2 0.01 20 5.5-20 Active
MW-10 2/12/2015 2 0.01 20 5.5-20 Active
DW-1 2/13/2015 2 0.01 40 35-40 Active
DW-2 11/20/2015 2 0.01 80 75-80 Active
TABLE 5
GROUNDWATER ELEVATION DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
WELL I.D.Date
Measured
TOC Elevation
(ft)
Depth to
Product (ft)
Depth to
Groundwater (ft)
Groundwater
Elevations (ft)
MW-1 --100.00
MW-2 --94.08
MW-3 --100.78
MW-4 --102.99
MW-5 --102.27
MW-6 --101.96
MW-7 --100.17
MW-8 --85.82
MW-9 --93.50
MW-10 --95.32
DW-1 --101.24
11/24/2015 --8.46 92.44
1/26/2016 --7.22 93.68
Note:
1. Top of Casing elevation is based on an arbitrary benchmark of 100.00 feet.
DW-2 100.90
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
Not Measured
TABLE 6
HISTORICAL GROUNDWATER ELEVATION DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
WELL I.D. Date TOC Elevation
(ft)
Depth to
Product (ft)
Depth to
Groundwater (ft)
Product Thickness
(ft)
Groundwater
Elevations (ft)
8/5/2013 5.53 6.38 0.85 94.27
3/4/2015 --4.70 --95.30
8/5/2013
3/4/2015 --6.93 --87.15
8/5/2013 5.50 6.08 0.58 95.14
3/4/2015 --3.95 --96.83
8/5/2013 --8.10 --94.89
3/4/2015 --6.39 --96.60
8/5/2013 --9.41 --92.86
3/4/2015 --7.05 --95.22
MW-6 3/4/2015 101.96 --7.36 --94.60
MW-7 3/4/2015 100.17 --8.28 --91.89
MW-8 3/4/2015 85.82 --4.10 --81.72
MW-9 3/4/2015 93.50 --9.21 --84.29
MW-10 3/4/2015 95.32 --7.52 --87.80
DW-1 3/4/2015 101.24 --7.12 --94.12
11/24/15 --8.46 --92.44
1/26/2016 --7.22 --93.68
Notes:
1. TOC = Top of well casing.
2. Groundwater elevation corrected for presence of free product calculated by:
[(TOC Elevation-Depth to Groundwater)+(0.76*Product thickness)]
94.08
100.78
102.99
102.27
DW-2 100.90
MW-5
Well Not Measured
MW-1
MW-2
MW-3
MW-4
100.00
TABLE 7
GROUNDWATER ANALYTICAL DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
EPA Method 625
EPA
Method
6010
Benzene Toluene Ethylbenzene Total
Xylenes MTBE Naphthalene IPE Bis(2-Ethylhexyl)-
phthalate
C5-C8
Aliphatics
C9-C18
Aliphatics
C19-C36
Aliphatics
C9-C22
Aromatics Lead
DW-2 11/24/15 3.1 <0.25 <0.25 <0.5 14.7 <1 <0.25 1.5J <50 <150 <100 <150 <2.5
DW-2 1/26/16 <0.5 <0.5 <0.5 <1 1.2 <0.5 <0.5 ------------
1 600 600 500 20 6 70 3 400 700 10,000 200 15
5,000 260,000 84,500 85,500 20,000 6,000 70,000 170 NE NE NE NE 15,000
Notes:
1. "<" denotes compound not detected above laboratory method detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDEQ 2L Standard (2L).
4. NCDEQ = North Carolina Department of Environmental Quality.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the
"Guidelines for Assessment and Corrective Action for UST Releases", November 2008, updated January 2010.
8. NE denotes not established.
9. J denotes estimated concentration by the laboratory.
Well
MADEP Methods for VPH and EPH
NCDEQ 2L Standard
GCLs
EPA Method 6200B
Sampling
Date
TABLE 8
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
Benzene Toluene Ethylbenzene Total
Xylenes MTBE Naphthalene
01/20/10 810 13 470 1,710 <40 --
02/19/10 940 61 610 2,493 7.3 890
08/05/13
3/4/15 38.6 21.4 133 9.3 0.31J 166
11/16/10 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1
3/4/15 1.8 <0.5 <0.5 <1.5 <0.5 0.27J
8/5/13
3/4/15 33 <25 1,840 6,830 <25 1,500
8/5/13 6.5 23 2.1 12.1 43 0.61
3/4/15 0.46J <0.5 <0.5 <1.5 8.5 <0.5
8/5/13 6.5 27 2.4 14.5 52 0.65
3/4/15 0.99 <0.5 <0.5 <1.5 39.4 0.29J
MW-6 3/4/15 <0.5 <0.5 0.22J 0.83J <0.5 <0.5
MW-7 3/4/15 0.83 <0.5 <0.5 0.18J 87 <0.5
MW-8 3/4/15 <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
MW-9 3/4/15 <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
MW-10 3/4/15 <0.5 <0.5 <0.5 <1.5 1.8 <0.5
DW-1 3/4/15 1.6 <0.5 <0.5 <1.5 211 <0.5
11/24/15 3.1 <0.25 <0.25 <0.5 14.7 <1
1/26/16 <0.5 <0.5 <0.5 <1 1.2 <0.5
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" denotes compound not detected above laboratory method detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDEQ 2L Standard (2L).
4. NCDEQ = North Carolina Department of Environmental Quality.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the
"Guidelines for Assessment and Corrective Action for UST Releases", November 2008, updated January 2010.
8. J denotes estimated concentration by the laboratory.
EPA Method 6200B
0.58 feet Free Product
NCDEQ 2L Standards
Well I.D.Sampling
Date
0.85 feet Free Product
GCLs
MW-3
MW-4
MW-5
MW-2
MW-1
DW-2
TABLE 9
WATER SUPPLY WELL ANALYTICAL DATA
PANTRY #3471
4940 U.S. HIGHWAY 264 WEST
WILSON, NORTH CAROLINA
NCDEQ INCIDENT NO. 33892
Benzene Toluene Ethylbenzene Total
Xylenes MTBE Naphthalene
PW-1 11/24/15 <0.25 <0.25 <0.25 <0.5 <0.25 <1
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
Notes:
1. "<" denotes compound not detected above laboratory method detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDEQ 2L Standard (2L).
4. NCDEQ = North Carolina Department of Environmental Quality.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the
"Guidelines for Assessment and Corrective Action for UST Releases", November 2008, updated January 2010.
NCDEQ 2L Standards
GCLs
EPA Method 6200B
Sampling
DateWell I.D.

FIGURES
FIGURE 1
USGS TOPOGRAPHIC MAP
Pantry # 3471
4940 US Highway 264 West
Wilson, North Carolina
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.24639.3471
SCALE: 1” = 600’DATE: 7/7/2009
SITE
FIGURE 3
SITE VICINITY MAP
Pantry # 3471
4940 US Highway 264 West
Wilson, North Carolina
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.24639.3471
SCALE: 1” = 430’DATE: 12/1/13
SOURCE: WILSON COUNTY GIS
SITE
N
Water Supply Well
500 foot Radius
1,000 Foot Radius
PW-1

APPENDIX A
BORING LOGS AND MONITORING WELL
CONSTRUCTION RECORDS
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\DW-1.borPantry #3471
4940 US Highway 264 West
Wilson, Wilson County, North Carolina
ATC Project No. 45.42017.3471
Client: The Pantry
BORING LOG: DW-2
(Page 1 of 1)
Date(s) Drilled : 11/19/15 & 11/20/15
Drilling Conractor : GEX
Drilling Method : Hollow Stem Augers/Air Rotary
Boring Diameter : 8 Inches
Sampling Method : None
Sampling Interval : None
Logged By : Robert Winfield
Depth in Feet0
5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
80 USCSAR
SM
SM
GR GRAPHICDESCRIPTION
Asphalt
Gray SILT
Brown sandy CLAY, partially weathered rock encountered at 25 feet
Brown partially weathered rock, wet at 59 feet
End of boring
Boring terminated at 80 feet bgs.
Well: DW-2
Grout
Bentonite
Sand Pack
SurfaceCasing
Cover
2" Diameter Casing
Screen
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SK-25.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Boring terminated at 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SD-10
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
AR
CL GRAPHICDESCRIPTION
Concrete
Gravel with partially weathered rock
Brown and gray sandy CLAY
Boring terminated at 7 feet
PID
(ppm)
74.1
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-10.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Boring terminated at 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SD-11
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
AR
CL GRAPHICDESCRIPTION
Concrete
Gravel with partially weathered rock
Brown and gray sandy CLAY
Boring terminated at 7 feet
PID
(ppm)
26.7
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-11.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Boring terminated at 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SD-13
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
AR
CL GRAPHICDESCRIPTION
Concrete
Gravel with partially weathered rock
Brown and gray sandy CLAY
Boring terminated at 7 feet
PID
(ppm)
12.6
02-16-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-19.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
End of boring 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SD-17
Date(s) Drilled : 11/20/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
SM
SM GRAPHICDESCRIPTION
Asphalt
Gray SAND with gravel
Gray and brown SAND with gravel
End of boring
PID
(ppm)
30.7
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-19.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Refusal at 4 feet below ground surface (bgs).
Soil sample collected at 4 feet bgs.
BORING LOG: SD-19
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4 USCSGRAPHICDESCRIPTION PID
(ppm)
0.1
AR
SM
CL
Asphalt and gravel
Gray SAND with gravel
Brown sandy CLAY with partially weathered rock
Refusal at 4 feet
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-25.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Refusal at 5 feet below ground surface (bgs).
Soil sample collected at 5 feet bgs.
BORING LOG: SD-25
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5 USCSGRAPHICDESCRIPTION PID
(ppm)
0.8
AR
SM
CL
Asphalt and gravel
Gray SAND with gravel
Brown sandy CLAY with partially weathered rock encountered at 3.5 feet
Refusal at 5 feet
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SD-26.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Refusal at 5.5 feet below ground surface (bgs).
Soil sample collected at 5.5 feet bgs.
BORING LOG: SD-26
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5 USCSAR
SM
CL GRAPHICDESCRIPTION
Asphalt
Gray SAND with gravel
Brown sandy CLAY with partially weathered rock encountered at 4 feet
Refusal at 5.5 feet
PID
(ppm)
5.6
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SK-30.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Boring terminated at 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SK-25
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
AR
CL GRAPHICDESCRIPTION
Asphalt
Gravel with partially weathered rock
Brown sandy CLAY
Boring terminated at 7 feet
PID
(ppm)
1.4
02-02-2016 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SK-30.borClient: The Pantry
ATC Project No. 45.42017.3471
Wilson, Wilson County, North Carolina
4940 US Highway 264 West
Pantry #3471
Boring terminated at 7 feet below ground surface (bgs).
Soil sample collected at 7 feet bgs.
BORING LOG: SK-30
Date(s) Drilled : 11/30/15
Drilling Contractor : Geologic Exploration
Drilling Method : Direct-Push
Boring Diameter : 4.25 Inches
Sampling Method : Observed cuttings
Sampling Interval : 5'
Logged By : Robert Winfield
Depth In Feet0
1
2
3
4
5
6
7 USCSAR
SM
CL GRAPHICDESCRIPTION
Asphalt
Gray SAND with gravel
Brown sandy CLAY with partially weathered rock encountered at 4 feet
Boring terminated at 7 feet
PID
(ppm)
3.7

APPENDIX B
LABORATORY REPORTS AND
CHAIN-OF-CUSTODY DOCUMENTS

#=CL#
December 11, 2015
LIMS USE: FR - MAUREEN JACKSON
LIMS OBJECT ID: 92277685
92277685
Project:
Pace Project No.:
RE:
Maureen Jackson
Cardno AtC
2725 E. Millbrook Road
Suite 121
Raleigh, NC 27604
PANTRY #3471 GW
Dear Maureen Jackson:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 29
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Lab ID Sample ID Matrix Date Collected Date Received
92277685001 PW-1 Water 11/24/15 15:35 11/25/15 11:00
92277685002 DW-2 Water 11/24/15 14:40 11/25/15 11:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277685001 PW-1 SM 6200B 63 PASI-CCAH
92277685002 DW-2 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 6010 1 PASI-ACDF
EPA 625 60 PASI-CBPJ
SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92277685002 DW-2
bis(2-Ethylhexyl)phthalate 1.5J ug/L 12/04/15 02:395.0EPA 625
3.622:Methylene Chloride 13.4 ug/L 12/04/15 02:39 NEPA 625
12.181:Hexadecanoic acid 7.5 ug/L 12/04/15 02:39 NEPA 625
Benzene 3.1 ug/L 12/04/15 08:420.50SM 6200B
Methyl-tert-butyl ether 14.7 ug/L 12/04/15 08:420.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:PW-1 Lab ID:92277685001 Collected:11/24/15 15:35 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.25 ug/L 12/04/15 08:26 71-43-20.50 0.25 1
Bromobenzene <0.25 ug/L 12/04/15 08:26 108-86-10.50 0.25 1
Bromochloromethane <0.25 ug/L 12/04/15 08:26 74-97-50.50 0.25 1
Bromodichloromethane <0.25 ug/L 12/04/15 08:26 75-27-40.50 0.25 1
Bromoform <0.25 ug/L 12/04/15 08:26 75-25-20.50 0.25 1
Bromomethane <0.50 ug/L 12/04/15 08:26 74-83-95.0 0.50 1
n-Butylbenzene <0.25 ug/L 12/04/15 08:26 104-51-80.50 0.25 1
sec-Butylbenzene <0.25 ug/L 12/04/15 08:26 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/04/15 08:26 98-06-60.50 0.25 1
Carbon tetrachloride <0.25 ug/L 12/04/15 08:26 56-23-50.50 0.25 1
Chlorobenzene <0.25 ug/L 12/04/15 08:26 108-90-70.50 0.25 1
Chloroethane <0.50 ug/L 12/04/15 08:26 75-00-31.0 0.50 1
Chloroform <0.25 ug/L 12/04/15 08:26 67-66-30.50 0.25 1
Chloromethane <0.50 ug/L 12/04/15 08:26 74-87-31.0 0.50 1
2-Chlorotoluene <0.25 ug/L 12/04/15 08:26 95-49-80.50 0.25 1
4-Chlorotoluene <0.25 ug/L 12/04/15 08:26 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane <0.50 ug/L 12/04/15 08:26 96-12-81.0 0.50 1
Dibromochloromethane <0.25 ug/L 12/04/15 08:26 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)<0.25 ug/L 12/04/15 08:26 106-93-40.50 0.25 1
Dibromomethane <0.25 ug/L 12/04/15 08:26 74-95-30.50 0.25 1
1,2-Dichlorobenzene <0.25 ug/L 12/04/15 08:26 95-50-10.50 0.25 1
1,3-Dichlorobenzene <0.25 ug/L 12/04/15 08:26 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/04/15 08:26 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.25 ug/L 12/04/15 08:26 75-71-80.50 0.25 1
1,1-Dichloroethane <0.25 ug/L 12/04/15 08:26 75-34-30.50 0.25 1
1,2-Dichloroethane <0.25 ug/L 12/04/15 08:26 107-06-20.50 0.25 1
1,1-Dichloroethene <0.25 ug/L 12/04/15 08:26 75-35-40.50 0.25 1
cis-1,2-Dichloroethene <0.25 ug/L 12/04/15 08:26 156-59-20.50 0.25 1
trans-1,2-Dichloroethene <0.25 ug/L 12/04/15 08:26 156-60-50.50 0.25 1
1,2-Dichloropropane <0.25 ug/L 12/04/15 08:26 78-87-50.50 0.25 1
1,3-Dichloropropane <0.25 ug/L 12/04/15 08:26 142-28-90.50 0.25 1
2,2-Dichloropropane <0.25 ug/L 12/04/15 08:26 594-20-70.50 0.25 1
1,1-Dichloropropene <0.25 ug/L 12/04/15 08:26 563-58-60.50 0.25 1
cis-1,3-Dichloropropene <0.25 ug/L 12/04/15 08:26 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene <0.25 ug/L 12/04/15 08:26 10061-02-60.50 0.25 1
Diisopropyl ether <0.25 ug/L 12/04/15 08:26 108-20-30.50 0.25 1
Ethylbenzene <0.25 ug/L 12/04/15 08:26 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene <1.0 ug/L 12/04/15 08:26 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)<0.25 ug/L 12/04/15 08:26 98-82-80.50 0.25 1
Methylene Chloride <1.0 ug/L 12/04/15 08:26 75-09-22.0 1.0 1
Methyl-tert-butyl ether <0.25 ug/L 12/04/15 08:26 1634-04-40.50 0.25 1
Naphthalene <1.0 ug/L 12/04/15 08:26 91-20-32.0 1.0 1
n-Propylbenzene <0.25 ug/L 12/04/15 08:26 103-65-10.50 0.25 1
Styrene <0.25 ug/L 12/04/15 08:26 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane <0.25 ug/L 12/04/15 08:26 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane <0.25 ug/L 12/04/15 08:26 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:PW-1 Lab ID:92277685001 Collected:11/24/15 15:35 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene <0.25 ug/L 12/04/15 08:26 127-18-40.50 0.25 1
Toluene <0.25 ug/L 12/04/15 08:26 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene <1.0 ug/L 12/04/15 08:26 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 12/04/15 08:26 120-82-12.0 1.0 1
1,1,1-Trichloroethane <0.25 ug/L 12/04/15 08:26 71-55-60.50 0.25 1
1,1,2-Trichloroethane <0.25 ug/L 12/04/15 08:26 79-00-50.50 0.25 1
Trichloroethene <0.25 ug/L 12/04/15 08:26 79-01-60.50 0.25 1
Trichlorofluoromethane <0.50 ug/L 12/04/15 08:26 75-69-41.0 0.50 1
1,2,3-Trichloropropane <0.25 ug/L 12/04/15 08:26 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene <0.25 ug/L 12/04/15 08:26 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene <0.25 ug/L 12/04/15 08:26 108-67-80.50 0.25 1
Vinyl chloride <0.25 ug/L 12/04/15 08:26 75-01-41.0 0.25 1
m&p-Xylene <0.50 ug/L 12/04/15 08:26 179601-23-11.0 0.50 1
o-Xylene <0.25 ug/L 12/04/15 08:26 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %12/04/15 08:26 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/04/15 08:26 460-00-470-130 1
Toluene-d8 (S)100 %12/04/15 08:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:DW-2 Lab ID:92277685002 Collected:11/24/15 14:40 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)<100 ug/L 12/09/15 19:16 N212/07/15 14:531001001
Aliphatic (C19-C36)<100 ug/L 12/09/15 19:16 N212/07/15 14:531001001
Aromatic (C11-C22)<100 ug/L 12/09/15 19:16 N212/07/15 14:531001001
Surrogates
Nonatriacontane (S)69 %12/09/15 19:16 7194-86-712/07/15 14:5340-140 1
o-Terphenyl (S)80 %12/09/15 19:16 84-15-112/07/15 14:5340-140 1
2-Fluorobiphenyl (S)88 %12/09/15 19:16 321-60-812/07/15 14:5340-140 1
2-Bromonaphthalene (S)84 %12/09/15 19:16 580-13-212/07/15 14:5340-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)<50.0 ug/L 11/30/15 16:38 N250.0 50.0 1
Aliphatic (C09-C12)<50.0 ug/L 11/30/15 16:38 N250.0 50.0 1
Aromatic (C09-C10)<50.0 ug/L 11/30/15 16:38 N250.0 50.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)95 %11/30/15 16:38 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)88 %11/30/15 16:38 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead <2.5 ug/L 12/08/15 01:37 7439-92-112/04/15 19:305.0 2.5 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene <0.25 ug/L 12/04/15 02:39 83-32-912/01/15 16:405.0 0.25 1
Acenaphthylene <0.21 ug/L 12/04/15 02:39 208-96-812/01/15 16:405.0 0.21 1
Anthracene <0.14 ug/L 12/04/15 02:39 120-12-712/01/15 16:405.0 0.14 1
Benzo(a)anthracene <0.33 ug/L 12/04/15 02:39 56-55-312/01/15 16:405.0 0.33 1
Benzo(a)pyrene <0.30 ug/L 12/04/15 02:39 50-32-812/01/15 16:405.0 0.30 1
Benzo(b)fluoranthene <0.28 ug/L 12/04/15 02:39 205-99-212/01/15 16:405.0 0.28 1
Benzo(g,h,i)perylene <0.38 ug/L 12/04/15 02:39 191-24-212/01/15 16:405.0 0.38 1
Benzo(k)fluoranthene <0.43 ug/L 12/04/15 02:39 207-08-912/01/15 16:405.0 0.43 1
4-Bromophenylphenyl ether <0.82 ug/L 12/04/15 02:39 101-55-312/01/15 16:405.0 0.82 1
Butylbenzylphthalate <0.79 ug/L 12/04/15 02:39 85-68-712/01/15 16:405.0 0.79 1
4-Chloro-3-methylphenol <3.7 ug/L 12/04/15 02:39 59-50-712/01/15 16:405.0 3.7 1
bis(2-Chloroethoxy)methane <0.92 ug/L 12/04/15 02:39 111-91-112/01/15 16:4010.0 0.92 1
bis(2-Chloroethyl) ether <1.0 ug/L 12/04/15 02:39 111-44-412/01/15 16:405.0 1.0 1
bis(2-Chloroisopropyl) ether <0.95 ug/L 12/04/15 02:39 108-60-112/01/15 16:405.0 0.95 1
2-Chloronaphthalene <0.98 ug/L 12/04/15 02:39 91-58-712/01/15 16:405.0 0.98 1
2-Chlorophenol <1.3 ug/L 12/04/15 02:39 95-57-812/01/15 16:405.0 1.3 1
4-Chlorophenylphenyl ether <0.87 ug/L 12/04/15 02:39 7005-72-312/01/15 16:405.0 0.87 1
Chrysene <0.21 ug/L 12/04/15 02:39 218-01-912/01/15 16:405.0 0.21 1
Dibenz(a,h)anthracene <0.55 ug/L 12/04/15 02:39 53-70-312/01/15 16:405.0 0.55 1
3,3'-Dichlorobenzidine <2.1 ug/L 12/04/15 02:39 91-94-112/01/15 16:4025.0 2.1 1
2,4-Dichlorophenol <1.7 ug/L 12/04/15 02:39 120-83-212/01/15 16:405.0 1.7 1
Diethylphthalate <0.58 ug/L 12/04/15 02:39 84-66-212/01/15 16:405.0 0.58 1
2,4-Dimethylphenol <1.2 ug/L 12/04/15 02:39 105-67-912/01/15 16:4010.0 1.2 1
Dimethylphthalate <0.76 ug/L 12/04/15 02:39 131-11-312/01/15 16:405.0 0.76 1
Di-n-butylphthalate <0.75 ug/L 12/04/15 02:39 84-74-212/01/15 16:405.0 0.75 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
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Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:DW-2 Lab ID:92277685002 Collected:11/24/15 14:40 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
4,6-Dinitro-2-methylphenol <2.6 ug/L 12/04/15 02:39 534-52-112/01/15 16:4020.0 2.6 1
2,4-Dinitrophenol <9.0 ug/L 12/04/15 02:39 51-28-512/01/15 16:4050.0 9.0 1
2,4-Dinitrotoluene <0.90 ug/L 12/04/15 02:39 121-14-212/01/15 16:405.0 0.90 1
2,6-Dinitrotoluene <0.98 ug/L 12/04/15 02:39 606-20-212/01/15 16:405.0 0.98 1
Di-n-octylphthalate <0.66 ug/L 12/04/15 02:39 117-84-012/01/15 16:405.0 0.66 1
bis(2-Ethylhexyl)phthalate 1.5J ug/L 12/04/15 02:39 117-81-712/01/15 16:405.0 0.79 1
Fluoranthene <0.21 ug/L 12/04/15 02:39 206-44-012/01/15 16:405.0 0.21 1
Fluorene <0.21 ug/L 12/04/15 02:39 86-73-712/01/15 16:405.0 0.21 1
Hexachloro-1,3-butadiene <0.94 ug/L 12/04/15 02:39 87-68-312/01/15 16:405.0 0.94 1
Hexachlorobenzene <0.72 ug/L 12/04/15 02:39 118-74-112/01/15 16:405.0 0.72 1
Hexachlorocyclopentadiene <0.88 ug/L 12/04/15 02:39 77-47-4 L212/01/15 16:4010.0 0.88 1
Hexachloroethane <1.1 ug/L 12/04/15 02:39 67-72-1 L212/01/15 16:405.0 1.1 1
Indeno(1,2,3-cd)pyrene <0.29 ug/L 12/04/15 02:39 193-39-512/01/15 16:405.0 0.29 1
Isophorone <0.89 ug/L 12/04/15 02:39 78-59-112/01/15 16:4010.0 0.89 1
Naphthalene <0.34 ug/L 12/04/15 02:39 91-20-312/01/15 16:405.0 0.34 1
Nitrobenzene <1.1 ug/L 12/04/15 02:39 98-95-312/01/15 16:405.0 1.1 1
2-Nitrophenol <0.91 ug/L 12/04/15 02:39 88-75-512/01/15 16:405.0 0.91 1
4-Nitrophenol <4.1 ug/L 12/04/15 02:39 100-02-712/01/15 16:4050.0 4.1 1
N-Nitrosodimethylamine <0.91 ug/L 12/04/15 02:39 62-75-912/01/15 16:405.0 0.91 1
N-Nitroso-di-n-propylamine <0.99 ug/L 12/04/15 02:39 621-64-712/01/15 16:405.0 0.99 1
N-Nitrosodiphenylamine <1.0 ug/L 12/04/15 02:39 86-30-612/01/15 16:4010.0 1.0 1
Pentachlorophenol <4.6 ug/L 12/04/15 02:39 87-86-512/01/15 16:4010.0 4.6 1
Phenanthrene <0.22 ug/L 12/04/15 02:39 85-01-812/01/15 16:405.0 0.22 1
Phenol <1.9 ug/L 12/04/15 02:39 108-95-212/01/15 16:405.0 1.9 1
Pyrene <0.19 ug/L 12/04/15 02:39 129-00-012/01/15 16:405.0 0.19 1
1,2,4-Trichlorobenzene <0.98 ug/L 12/04/15 02:39 120-82-112/01/15 16:405.0 0.98 1
2,4,6-Trichlorophenol <1.3 ug/L 12/04/15 02:39 88-06-212/01/15 16:4010.0 1.3 1
Surrogates
Nitrobenzene-d5 (S)64 %12/04/15 02:39 4165-60-012/01/15 16:4010-120 1
2-Fluorobiphenyl (S)64 %12/04/15 02:39 321-60-812/01/15 16:4015-120 1
Terphenyl-d14 (S)90 %12/04/15 02:39 1718-51-012/01/15 16:4011-131 1
Phenol-d6 (S)20 %12/04/15 02:39 13127-88-312/01/15 16:4010-120 1
2-Fluorophenol (S)30 %12/04/15 02:39 367-12-412/01/15 16:4010-120 1
2,4,6-Tribromophenol (S)85 %12/04/15 02:39 118-79-612/01/15 16:4010-137 1
Tentatively Identified Compounds
Methylene Chloride 13.4 ug/L 12/04/15 02:39 75-09-2 N12/01/15 16:401
Hexadecanoic acid 7.5 ug/L 12/04/15 02:39 57-10-3 N12/01/15 16:401
Analytical Method: SM 6200B6200B MSV
Benzene 3.1 ug/L 12/04/15 08:42 71-43-20.50 0.25 1
Bromobenzene <0.25 ug/L 12/04/15 08:42 108-86-10.50 0.25 1
Bromochloromethane <0.25 ug/L 12/04/15 08:42 74-97-50.50 0.25 1
Bromodichloromethane <0.25 ug/L 12/04/15 08:42 75-27-40.50 0.25 1
Bromoform <0.25 ug/L 12/04/15 08:42 75-25-20.50 0.25 1
Bromomethane <0.50 ug/L 12/04/15 08:42 74-83-95.0 0.50 1
n-Butylbenzene <0.25 ug/L 12/04/15 08:42 104-51-80.50 0.25 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:DW-2 Lab ID:92277685002 Collected:11/24/15 14:40 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
sec-Butylbenzene <0.25 ug/L 12/04/15 08:42 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/04/15 08:42 98-06-60.50 0.25 1
Carbon tetrachloride <0.25 ug/L 12/04/15 08:42 56-23-50.50 0.25 1
Chlorobenzene <0.25 ug/L 12/04/15 08:42 108-90-70.50 0.25 1
Chloroethane <0.50 ug/L 12/04/15 08:42 75-00-31.0 0.50 1
Chloroform <0.25 ug/L 12/04/15 08:42 67-66-30.50 0.25 1
Chloromethane <0.50 ug/L 12/04/15 08:42 74-87-31.0 0.50 1
2-Chlorotoluene <0.25 ug/L 12/04/15 08:42 95-49-80.50 0.25 1
4-Chlorotoluene <0.25 ug/L 12/04/15 08:42 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane <0.50 ug/L 12/04/15 08:42 96-12-81.0 0.50 1
Dibromochloromethane <0.25 ug/L 12/04/15 08:42 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)<0.25 ug/L 12/04/15 08:42 106-93-40.50 0.25 1
Dibromomethane <0.25 ug/L 12/04/15 08:42 74-95-30.50 0.25 1
1,2-Dichlorobenzene <0.25 ug/L 12/04/15 08:42 95-50-10.50 0.25 1
1,3-Dichlorobenzene <0.25 ug/L 12/04/15 08:42 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/04/15 08:42 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.25 ug/L 12/04/15 08:42 75-71-80.50 0.25 1
1,1-Dichloroethane <0.25 ug/L 12/04/15 08:42 75-34-30.50 0.25 1
1,2-Dichloroethane <0.25 ug/L 12/04/15 08:42 107-06-20.50 0.25 1
1,1-Dichloroethene <0.25 ug/L 12/04/15 08:42 75-35-40.50 0.25 1
cis-1,2-Dichloroethene <0.25 ug/L 12/04/15 08:42 156-59-20.50 0.25 1
trans-1,2-Dichloroethene <0.25 ug/L 12/04/15 08:42 156-60-50.50 0.25 1
1,2-Dichloropropane <0.25 ug/L 12/04/15 08:42 78-87-50.50 0.25 1
1,3-Dichloropropane <0.25 ug/L 12/04/15 08:42 142-28-90.50 0.25 1
2,2-Dichloropropane <0.25 ug/L 12/04/15 08:42 594-20-70.50 0.25 1
1,1-Dichloropropene <0.25 ug/L 12/04/15 08:42 563-58-60.50 0.25 1
cis-1,3-Dichloropropene <0.25 ug/L 12/04/15 08:42 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene <0.25 ug/L 12/04/15 08:42 10061-02-60.50 0.25 1
Diisopropyl ether <0.25 ug/L 12/04/15 08:42 108-20-30.50 0.25 1
Ethylbenzene <0.25 ug/L 12/04/15 08:42 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene <1.0 ug/L 12/04/15 08:42 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)<0.25 ug/L 12/04/15 08:42 98-82-80.50 0.25 1
Methylene Chloride <1.0 ug/L 12/04/15 08:42 75-09-22.0 1.0 1
Methyl-tert-butyl ether 14.7 ug/L 12/04/15 08:42 1634-04-40.50 0.25 1
Naphthalene <1.0 ug/L 12/04/15 08:42 91-20-32.0 1.0 1
n-Propylbenzene <0.25 ug/L 12/04/15 08:42 103-65-10.50 0.25 1
Styrene <0.25 ug/L 12/04/15 08:42 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane <0.25 ug/L 12/04/15 08:42 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane <0.25 ug/L 12/04/15 08:42 79-34-50.50 0.25 1
Tetrachloroethene <0.25 ug/L 12/04/15 08:42 127-18-40.50 0.25 1
Toluene <0.25 ug/L 12/04/15 08:42 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene <1.0 ug/L 12/04/15 08:42 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 12/04/15 08:42 120-82-12.0 1.0 1
1,1,1-Trichloroethane <0.25 ug/L 12/04/15 08:42 71-55-60.50 0.25 1
1,1,2-Trichloroethane <0.25 ug/L 12/04/15 08:42 79-00-50.50 0.25 1
Trichloroethene <0.25 ug/L 12/04/15 08:42 79-01-60.50 0.25 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Sample:DW-2 Lab ID:92277685002 Collected:11/24/15 14:40 Received:11/25/15 11:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane <0.50 ug/L 12/04/15 08:42 75-69-41.0 0.50 1
1,2,3-Trichloropropane <0.25 ug/L 12/04/15 08:42 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene <0.25 ug/L 12/04/15 08:42 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene <0.25 ug/L 12/04/15 08:42 108-67-80.50 0.25 1
Vinyl chloride <0.25 ug/L 12/04/15 08:42 75-01-41.0 0.25 1
m&p-Xylene <0.50 ug/L 12/04/15 08:42 179601-23-11.0 0.50 1
o-Xylene <0.25 ug/L 12/04/15 08:42 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %12/04/15 08:42 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %12/04/15 08:42 460-00-470-130 1
Toluene-d8 (S)101 %12/04/15 08:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
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[phone]
Page 11 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10139
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92277685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1616279
Associated Lab Samples:92277685002
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L <50.0 50.0 N211/30/15 13:0750.0
Aliphatic (C09-C12)ug/L <50.0 50.0 N211/30/15 13:0750.0
Aromatic (C09-C10)ug/L <50.0 50.0 N211/30/15 13:0750.0
4-Bromofluorobenzene (FID) (S)%100 70-130 11/30/15 13:07
4-Bromofluorobenzene (PID) (S)%94 70-130 11/30/15 13:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1616280LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1616281
Aliphatic (C05-C08)ug/L 321 N230010770-130105314 2 25
Aliphatic (C09-C12)ug/L 329 N230011030-130112335 2 25
Aromatic (C09-C10)ug/L 90.2 N21009070-1309089.6 1 25
4-Bromofluorobenzene (FID) (S)%103 70-13098
4-Bromofluorobenzene (PID) (S)%97 70-13093
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/20176
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92277685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1620436
Associated Lab Samples:92277685002
Matrix:Water
AnalyzedMDL
Lead ug/L <2.5 5.0 12/08/15 01:312.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1620437LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 469500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1620438MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277685002
1620439
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 89 75-12595 6 20500<2.5 448 477
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
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Huntersville, NC 28078
[phone]
Page 13 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34531
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92277685001, 92277685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1619376
Associated Lab Samples:92277685001, 92277685002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,1,1-Trichloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,1,2,2-Tetrachloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,1,2-Trichloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,1-Dichloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,1-Dichloroethene ug/L <0.25 0.50 12/04/15 03:420.25
1,1-Dichloropropene ug/L <0.25 0.50 12/04/15 03:420.25
1,2,3-Trichlorobenzene ug/L <1.0 2.0 12/04/15 03:421.0
1,2,3-Trichloropropane ug/L <0.25 0.50 12/04/15 03:420.25
1,2,4-Trichlorobenzene ug/L <1.0 2.0 12/04/15 03:421.0
1,2,4-Trimethylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
1,2-Dibromo-3-chloropropane ug/L <0.50 1.0 12/04/15 03:420.50
1,2-Dibromoethane (EDB)ug/L <0.25 0.50 12/04/15 03:420.25
1,2-Dichlorobenzene ug/L <0.25 0.50 12/04/15 03:420.25
1,2-Dichloroethane ug/L <0.25 0.50 12/04/15 03:420.25
1,2-Dichloropropane ug/L <0.25 0.50 12/04/15 03:420.25
1,3,5-Trimethylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
1,3-Dichlorobenzene ug/L <0.25 0.50 12/04/15 03:420.25
1,3-Dichloropropane ug/L <0.25 0.50 12/04/15 03:420.25
1,4-Dichlorobenzene ug/L <0.25 0.50 12/04/15 03:420.25
2,2-Dichloropropane ug/L <0.25 0.50 12/04/15 03:420.25
2-Chlorotoluene ug/L <0.25 0.50 12/04/15 03:420.25
4-Chlorotoluene ug/L <0.25 0.50 12/04/15 03:420.25
Benzene ug/L <0.25 0.50 12/04/15 03:420.25
Bromobenzene ug/L <0.25 0.50 12/04/15 03:420.25
Bromochloromethane ug/L <0.25 0.50 12/04/15 03:420.25
Bromodichloromethane ug/L <0.25 0.50 12/04/15 03:420.25
Bromoform ug/L <0.25 0.50 12/04/15 03:420.25
Bromomethane ug/L <0.50 5.0 12/04/15 03:420.50
Carbon tetrachloride ug/L <0.25 0.50 12/04/15 03:420.25
Chlorobenzene ug/L <0.25 0.50 12/04/15 03:420.25
Chloroethane ug/L <0.50 1.0 12/04/15 03:420.50
Chloroform ug/L <0.25 0.50 12/04/15 03:420.25
Chloromethane ug/L <0.50 1.0 12/04/15 03:420.50
cis-1,2-Dichloroethene ug/L <0.25 0.50 12/04/15 03:420.25
cis-1,3-Dichloropropene ug/L <0.25 0.50 12/04/15 03:420.25
Dibromochloromethane ug/L <0.25 0.50 12/04/15 03:420.25
Dibromomethane ug/L <0.25 0.50 12/04/15 03:420.25
Dichlorodifluoromethane ug/L <0.25 0.50 12/04/15 03:420.25
Diisopropyl ether ug/L <0.25 0.50 12/04/15 03:420.25
Ethylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1619376
Associated Lab Samples:92277685001, 92277685002
Matrix:Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L <1.0 2.0 12/04/15 03:421.0
Isopropylbenzene (Cumene)ug/L <0.25 0.50 12/04/15 03:420.25
m&p-Xylene ug/L <0.50 1.0 12/04/15 03:420.50
Methyl-tert-butyl ether ug/L <0.25 0.50 12/04/15 03:420.25
Methylene Chloride ug/L <1.0 2.0 12/04/15 03:421.0
n-Butylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
n-Propylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
Naphthalene ug/L <1.0 2.0 12/04/15 03:421.0
o-Xylene ug/L <0.25 0.50 12/04/15 03:420.25
sec-Butylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
Styrene ug/L <0.25 0.50 12/04/15 03:420.25
tert-Butylbenzene ug/L <0.25 0.50 12/04/15 03:420.25
Tetrachloroethene ug/L <0.25 0.50 12/04/15 03:420.25
Toluene ug/L <0.25 0.50 12/04/15 03:420.25
trans-1,2-Dichloroethene ug/L <0.25 0.50 12/04/15 03:420.25
trans-1,3-Dichloropropene ug/L <0.25 0.50 12/04/15 03:420.25
Trichloroethene ug/L <0.25 0.50 12/04/15 03:420.25
Trichlorofluoromethane ug/L <0.50 1.0 12/04/15 03:420.50
Vinyl chloride ug/L <0.25 1.0 12/04/15 03:420.25
1,2-Dichloroethane-d4 (S)%99 70-130 12/04/15 03:42
4-Bromofluorobenzene (S)%100 70-130 12/04/15 03:42
Toluene-d8 (S)%102 70-130 12/04/15 03:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1619377LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.150 110 60-140
1,1,1-Trichloroethane ug/L 54.650 109 60-140
1,1,2,2-Tetrachloroethane ug/L 47.950 96 60-140
1,1,2-Trichloroethane ug/L 48.450 97 60-140
1,1-Dichloroethane ug/L 51.650 103 60-140
1,1-Dichloroethene ug/L 60.450 121 60-140
1,1-Dichloropropene ug/L 55.950 112 60-140
1,2,3-Trichlorobenzene ug/L 46.150 92 60-140
1,2,3-Trichloropropane ug/L 46.850 94 60-140
1,2,4-Trichlorobenzene ug/L 48.350 97 60-140
1,2,4-Trimethylbenzene ug/L 56.950 114 60-140
1,2-Dibromo-3-chloropropane ug/L 48.750 97 60-140
1,2-Dibromoethane (EDB)ug/L 53.050 106 60-140
1,2-Dichlorobenzene ug/L 51.950 104 60-140
1,2-Dichloroethane ug/L 44.350 89 60-140
1,2-Dichloropropane ug/L 51.650 103 60-140
1,3,5-Trimethylbenzene ug/L 56.850 114 60-140
1,3-Dichlorobenzene ug/L 53.350 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1619377LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.650 97 60-140
1,4-Dichlorobenzene ug/L 51.250 102 60-140
2,2-Dichloropropane ug/L 53.450 107 60-140
2-Chlorotoluene ug/L 54.450 109 60-140
4-Chlorotoluene ug/L 54.350 109 60-140
Benzene ug/L 53.850 108 60-140
Bromobenzene ug/L 52.050 104 60-140
Bromochloromethane ug/L 53.550 107 60-140
Bromodichloromethane ug/L 55.550 111 60-140
Bromoform ug/L 37.650 75 60-140
Bromomethane ug/L 33.350 67 60-140
Carbon tetrachloride ug/L 59.350 119 60-140
Chlorobenzene ug/L 50.550 101 60-140
Chloroethane ug/L 49.850 100 60-140
Chloroform ug/L 51.750 103 60-140
Chloromethane ug/L 44.350 89 60-140
cis-1,2-Dichloroethene ug/L 53.350 107 60-140
cis-1,3-Dichloropropene ug/L 55.050 110 60-140
Dibromochloromethane ug/L 45.450 91 60-140
Dibromomethane ug/L 51.050 102 60-140
Dichlorodifluoromethane ug/L 63.450 127 60-140
Diisopropyl ether ug/L 54.950 110 60-140
Ethylbenzene ug/L 51.850 104 60-140
Hexachloro-1,3-butadiene ug/L 52.750 105 60-140
Isopropylbenzene (Cumene)ug/L 57.650 115 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 53.050 106 60-140
Methylene Chloride ug/L 55.650 111 60-140
n-Butylbenzene ug/L 55.050 110 60-140
n-Propylbenzene ug/L 55.150 110 60-140
Naphthalene ug/L 49.950 100 60-140
o-Xylene ug/L 53.250 106 60-140
sec-Butylbenzene ug/L 57.350 115 60-140
Styrene ug/L 58.250 116 60-140
tert-Butylbenzene ug/L 48.150 96 60-140
Tetrachloroethene ug/L 49.650 99 60-140
Toluene ug/L 50.650 101 60-140
trans-1,2-Dichloroethene ug/L 55.250 110 60-140
trans-1,3-Dichloropropene ug/L 47.250 94 60-140
Trichloroethene ug/L 49.050 98 60-140
Trichlorofluoromethane ug/L 48.250 96 60-140
Vinyl chloride ug/L 57.150 114 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1619378MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277847019
1619379
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 60-140112 1 3020ND22.1 22.4
1,1,1-Trichloroethane ug/L 20 120 60-140122 2 3020ND24.0 24.5
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140108 0 3020ND21.5 21.5
1,1,2-Trichloroethane ug/L 20 104 60-140103 1 3020ND20.8 20.5
1,1-Dichloroethane ug/L 20 113 60-140115 2 3020ND22.6 23.0
1,1-Dichloroethene ug/L 20 138 60-140140 1 3020ND27.6 27.9
1,1-Dichloropropene ug/L 20 125 60-140127 2 3020ND25.0 25.4
1,2,3-Trichlorobenzene ug/L 20 109 60-140109 0 3020ND21.8 21.7
1,2,3-Trichloropropane ug/L 20 105 60-140105 0 3020ND20.9 20.9
1,2,4-Trichlorobenzene ug/L 20 109 60-140107 2 3020ND21.7 21.4
1,2,4-Trimethylbenzene ug/L 20 123 60-140123 0 3020ND24.5 24.6
1,2-Dibromo-3-
chloropropane ug/L 20 103 60-140102 1 3020ND20.7 20.4
1,2-Dibromoethane (EDB)ug/L 20 112 60-140113 1 3020ND22.4 22.5
1,2-Dichlorobenzene ug/L 20 110 60-140110 0 3020ND22.0 22.1
1,2-Dichloroethane ug/L 20 96 60-14097 0 3020ND19.5 19.5
1,2-Dichloropropane ug/L 20 112 60-140111 1 3020ND22.3 22.2
1,3,5-Trimethylbenzene ug/L 20 124 60-140123 0 3020ND24.7 24.7
1,3-Dichlorobenzene ug/L 20 114 60-140115 1 3020ND22.8 22.9
1,3-Dichloropropane ug/L 20 105 60-140106 1 3020ND21.1 21.2
1,4-Dichlorobenzene ug/L 20 111 60-140110 1 3020ND22.1 22.0
2,2-Dichloropropane ug/L M12014060-140141 1 3020ND27.9 28.1
2-Chlorotoluene ug/L 20 117 60-140120 3 3020ND23.4 24.1
4-Chlorotoluene ug/L 20 118 60-140118 0 3020ND23.7 23.6
Benzene ug/L 20 119 60-140118 1 3020ND23.8 23.7
Bromobenzene ug/L 20 109 60-140112 2 3020ND21.8 22.3
Bromochloromethane ug/L 20 112 60-140114 2 3020ND22.4 22.8
Bromodichloromethane ug/L 20 110 60-140110 0 3020ND22.0 22.0
Bromoform ug/L 20 76 60-14075 1 3020ND15.2 15.0
Bromomethane ug/L 20 85 60-14084 1 3020ND17.0 16.8
Carbon tetrachloride ug/L 20 126 60-140126 0 3020ND25.3 25.2
Chlorobenzene ug/L 20 110 60-140111 1 3020ND21.9 22.1
Chloroethane ug/L 20 111 60-140118 6 3020ND22.2 23.6
Chloroform ug/L 20 111 60-140114 2 3020ND22.3 22.7
Chloromethane ug/L 20 122 60-140133 8 3020ND24.4 26.5
cis-1,2-Dichloroethene ug/L 20 117 60-140119 2 3020ND23.4 23.8
cis-1,3-Dichloropropene ug/L 20 113 60-140112 1 3020ND22.6 22.5
Dibromochloromethane ug/L 20 90 60-14090 1 3020ND18.1 17.9
Dibromomethane ug/L 20 109 60-140106 3 3020ND21.9 21.1
Dichlorodifluoromethane ug/L M12014860-140147 0 3020ND29.6 29.4
Diisopropyl ether ug/L 20 119 60-140121 2 3020ND23.7 24.3
Ethylbenzene ug/L 20 115 60-140115 0 3020ND22.9 23.0
Hexachloro-1,3-butadiene ug/L 20 132 60-140129 2 3020ND26.4 25.9
Isopropylbenzene (Cumene)ug/L 20 128 60-140128 0 3020ND25.6 25.6
m&p-Xylene ug/L 40 118 60-140119 0 3040ND47.3 47.5
Methyl-tert-butyl ether ug/L 20 113 60-140115 2 3020ND22.7 23.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1619378MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92277847019
1619379
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 115 60-140117 2 3020ND22.9 23.3
n-Butylbenzene ug/L 20 125 60-140123 1 3020ND24.9 24.6
n-Propylbenzene ug/L 20 123 60-140123 0 3020ND24.6 24.7
Naphthalene ug/L 20 120 60-140118 1 3020ND23.9 23.7
o-Xylene ug/L 20 115 60-140116 0 3020ND23.1 23.1
sec-Butylbenzene ug/L 20 129 60-140128 1 3020ND25.9 25.7
Styrene ug/L 20 119 60-140121 2 3020ND23.9 24.3
tert-Butylbenzene ug/L 20 105 60-140104 0 3020ND20.9 20.9
Tetrachloroethene ug/L 20 111 60-140112 1 3020ND22.2 22.3
Toluene ug/L 20 114 60-140112 2 3020ND22.8 22.3
trans-1,2-Dichloroethene ug/L 20 125 60-140127 1 3020ND25.1 25.4
trans-1,3-Dichloropropene ug/L 20 102 60-140101 1 3020ND20.3 20.1
Trichloroethene ug/L 20 108 60-140108 0 3020ND21.5 21.6
Trichlorofluoromethane ug/L 20 113 60-140113 1 3020ND22.5 22.7
Vinyl chloride ug/L 20 133 60-140135 1 3020ND26.6 27.0
1,2-Dichloroethane-d4 (S)%97 70-13098
4-Bromofluorobenzene (S)%102 70-130103
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39417
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92277685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1618490
Associated Lab Samples:92277685002
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L <0.98 5.0 12/03/15 22:040.98
2,4,6-Trichlorophenol ug/L <1.3 10.0 12/03/15 22:041.3
2,4-Dichlorophenol ug/L <1.7 5.0 12/03/15 22:041.7
2,4-Dimethylphenol ug/L <1.2 10.0 12/03/15 22:041.2
2,4-Dinitrophenol ug/L <9.0 50.0 12/03/15 22:049.0
2,4-Dinitrotoluene ug/L <0.90 5.0 12/03/15 22:040.90
2,6-Dinitrotoluene ug/L <0.98 5.0 12/03/15 22:040.98
2-Chloronaphthalene ug/L <0.98 5.0 12/03/15 22:040.98
2-Chlorophenol ug/L <1.3 5.0 12/03/15 22:041.3
2-Nitrophenol ug/L <0.91 5.0 12/03/15 22:040.91
3,3'-Dichlorobenzidine ug/L <2.1 25.0 12/03/15 22:042.1
4,6-Dinitro-2-methylphenol ug/L <2.6 20.0 12/03/15 22:042.6
4-Bromophenylphenyl ether ug/L <0.82 5.0 12/03/15 22:040.82
4-Chloro-3-methylphenol ug/L <3.7 5.0 12/03/15 22:043.7
4-Chlorophenylphenyl ether ug/L <0.87 5.0 12/03/15 22:040.87
4-Nitrophenol ug/L <4.1 50.0 12/03/15 22:044.1
Acenaphthene ug/L <0.25 5.0 12/03/15 22:040.25
Acenaphthylene ug/L <0.21 5.0 12/03/15 22:040.21
Anthracene ug/L <0.14 5.0 12/03/15 22:040.14
Benzo(a)anthracene ug/L <0.33 5.0 12/03/15 22:040.33
Benzo(a)pyrene ug/L <0.30 5.0 12/03/15 22:040.30
Benzo(b)fluoranthene ug/L <0.28 5.0 12/03/15 22:040.28
Benzo(g,h,i)perylene ug/L <0.38 5.0 12/03/15 22:040.38
Benzo(k)fluoranthene ug/L <0.43 5.0 12/03/15 22:040.43
bis(2-Chloroethoxy)methane ug/L <0.92 10.0 12/03/15 22:040.92
bis(2-Chloroethyl) ether ug/L <1.0 5.0 12/03/15 22:041.0
bis(2-Chloroisopropyl) ether ug/L <0.95 5.0 12/03/15 22:040.95
bis(2-Ethylhexyl)phthalate ug/L <0.79 5.0 12/03/15 22:040.79
Butylbenzylphthalate ug/L <0.79 5.0 12/03/15 22:040.79
Chrysene ug/L <0.21 5.0 12/03/15 22:040.21
Di-n-butylphthalate ug/L <0.75 5.0 12/03/15 22:040.75
Di-n-octylphthalate ug/L <0.66 5.0 12/03/15 22:040.66
Dibenz(a,h)anthracene ug/L <0.55 5.0 12/03/15 22:040.55
Diethylphthalate ug/L <0.58 5.0 12/03/15 22:040.58
Dimethylphthalate ug/L <0.76 5.0 12/03/15 22:040.76
Fluoranthene ug/L <0.21 5.0 12/03/15 22:040.21
Fluorene ug/L <0.21 5.0 12/03/15 22:040.21
Hexachloro-1,3-butadiene ug/L <0.94 5.0 12/03/15 22:040.94
Hexachlorobenzene ug/L <0.72 5.0 12/03/15 22:040.72
Hexachlorocyclopentadiene ug/L <0.88 10.0 12/03/15 22:040.88
Hexachloroethane ug/L <1.1 5.0 12/03/15 22:041.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/11/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1618490
Associated Lab Samples:92277685002
Matrix:Water
AnalyzedMDL
Indeno(1,2,3-cd)pyrene ug/L <0.29 5.0 12/03/15 22:040.29
Isophorone ug/L <0.89 10.0 12/03/15 22:040.89
N-Nitroso-di-n-propylamine ug/L <0.99 5.0 12/03/15 22:040.99
N-Nitrosodimethylamine ug/L <0.91 5.0 12/03/15 22:040.91
N-Nitrosodiphenylamine ug/L <1.0 10.0 12/03/15 22:041.0
Naphthalene ug/L <0.34 5.0 12/03/15 22:040.34
Nitrobenzene ug/L <1.1 5.0 12/03/15 22:041.1
Pentachlorophenol ug/L <4.6 10.0 12/03/15 22:044.6
Phenanthrene ug/L <0.22 5.0 12/03/15 22:040.22
Phenol ug/L <1.9 5.0 12/03/15 22:041.9
Pyrene ug/L <0.19 5.0 12/03/15 22:040.19
2,4,6-Tribromophenol (S)%61 10-137 12/03/15 22:04
2-Fluorobiphenyl (S)%44 15-120 12/03/15 22:04
2-Fluorophenol (S)%23 10-120 12/03/15 22:04
Nitrobenzene-d5 (S)%48 10-120 12/03/15 22:04
Phenol-d6 (S)%17 10-120 12/03/15 22:04
Terphenyl-d14 (S)%74 11-131 12/03/15 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1618491LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 23.150 46 44-142
2,4,6-Trichlorophenol ug/L 32.850 66 37-144
2,4-Dichlorophenol ug/L 28.450 57 1-191
2,4-Dimethylphenol ug/L 25.150 50 32-119
2,4-Dinitrophenol ug/L 42.8J250 17 1-181
2,4-Dinitrotoluene ug/L 35.050 70 39-139
2,6-Dinitrotoluene ug/L 34.250 68 50-158
2-Chloronaphthalene ug/L 31.050 62 60-118
2-Chlorophenol ug/L 27.050 54 23-134
2-Nitrophenol ug/L 25.450 51 29-182
3,3'-Dichlorobenzidine ug/L 72.9100 73 1-262
4,6-Dinitro-2-methylphenol ug/L 22.5100 23 1-181
4-Bromophenylphenyl ether ug/L 33.750 67 53-127
4-Chloro-3-methylphenol ug/L 56.4100 56 22-147
4-Chlorophenylphenyl ether ug/L 30.650 61 25-158
4-Nitrophenol ug/L 75.6250 30 1-132
Acenaphthene ug/L 33.850 68 47-145
Acenaphthylene ug/L 35.450 71 33-145
Anthracene ug/L 40.450 81 1-166
Benzo(a)anthracene ug/L 39.550 79 33-143
Benzo(a)pyrene ug/L 39.550 79 17-163
Benzo(b)fluoranthene ug/L 37.150 74 24-159
Benzo(g,h,i)perylene ug/L 34.850 70 1-219
REPORT OF LABORATORY ANALYSIS
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Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1618491LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(k)fluoranthene ug/L 48.250 96 11-162
bis(2-Chloroethoxy)methane ug/L 24.250 48 33-184
bis(2-Chloroethyl) ether ug/L 25.650 51 12-158
bis(2-Chloroisopropyl) ether ug/L 21.550 43 36-166
bis(2-Ethylhexyl)phthalate ug/L 48.550 97 8-158
Butylbenzylphthalate ug/L 50.050 100 1-152
Chrysene ug/L 39.650 79 17-168
Di-n-butylphthalate ug/L 45.050 90 1-118
Di-n-octylphthalate ug/L 46.350 93 4-146
Dibenz(a,h)anthracene ug/L 35.050 70 1-227
Diethylphthalate ug/L 38.250 76 1-114
Dimethylphthalate ug/L 36.250 72 1-112
Fluoranthene ug/L 41.150 82 26-137
Fluorene ug/L 36.950 74 59-121
Hexachloro-1,3-butadiene ug/L 22.050 44 24-116
Hexachlorobenzene ug/L 39.150 78 1-152
Hexachlorocyclopentadiene ug/L 5.6J L0501125-150
Hexachloroethane ug/L 19.3 L0503940-113
Indeno(1,2,3-cd)pyrene ug/L 34.950 70 1-171
Isophorone ug/L 26.950 54 21-196
N-Nitroso-di-n-propylamine ug/L 28.150 56 1-230
N-Nitrosodimethylamine ug/L 15.950 32 25-150
N-Nitrosodiphenylamine ug/L 35.750 71 25-150
Naphthalene ug/L 24.950 50 21-133
Nitrobenzene ug/L 24.850 50 35-180
Pentachlorophenol ug/L 62.4100 62 14-176
Phenanthrene ug/L 36.750 73 54-120
Phenol ug/L 12.450 25 5-112
Pyrene ug/L 43.350 87 52-115
2,4,6-Tribromophenol (S)%76 10-137
2-Fluorobiphenyl (S)%60 15-120
2-Fluorophenol (S)%33 10-120
Nitrobenzene-d5 (S)%52 10-120
Phenol-d6 (S)%22 10-120
Terphenyl-d14 (S)%78 11-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1618492MATRIX SPIKE SAMPLE:
MSSpike
Result
92277684002
1,2,4-Trichlorobenzene ug/L 27.750 55 44-142ND
2,4,6-Trichlorophenol ug/L 31.950 64 37-144ND
2,4-Dichlorophenol ug/L 28.850 58 1-191ND
2,4-Dimethylphenol ug/L 4.8J M150432-119ND
2,4-Dinitrophenol ug/L 82.8250 33 1-181ND
2,4-Dinitrotoluene ug/L 37.450 75 39-139ND
REPORT OF LABORATORY ANALYSIS
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Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1618492MATRIX SPIKE SAMPLE:
MSSpike
Result
92277684002
2,6-Dinitrotoluene ug/L 36.050 72 50-158ND
2-Chloronaphthalene ug/L 32.850 66 60-118ND
2-Chlorophenol ug/L 27.750 55 23-134ND
2-Nitrophenol ug/L 30.050 60 29-182ND
3,3'-Dichlorobenzidine ug/L <2.1 M110001-262ND
4,6-Dinitro-2-methylphenol ug/L 36.5100 36 1-181ND
4-Bromophenylphenyl ether ug/L 33.050 66 53-127ND
4-Chloro-3-methylphenol ug/L 52.8100 53 22-147ND
4-Chlorophenylphenyl ether ug/L 31.250 62 25-158ND
4-Nitrophenol ug/L 103250 41 1-132ND
Acenaphthene ug/L 34.150 68 47-145ND
Acenaphthylene ug/L 32.450 65 33-145ND
Anthracene ug/L 29.450 59 1-166ND
Benzo(a)anthracene ug/L 37.450 75 33-143ND
Benzo(a)pyrene ug/L 25.150 50 17-163ND
Benzo(b)fluoranthene ug/L 39.550 79 24-159ND
Benzo(g,h,i)perylene ug/L 35.250 70 1-219ND
Benzo(k)fluoranthene ug/L 51.350 103 11-162ND
bis(2-Chloroethoxy)methane ug/L 27.850 56 33-184ND
bis(2-Chloroethyl) ether ug/L 25.750 51 12-158ND
bis(2-Chloroisopropyl) ether ug/L 23.050 46 36-166ND
bis(2-Ethylhexyl)phthalate ug/L 45.450 91 8-158ND
Butylbenzylphthalate ug/L 46.750 93 1-152ND
Chrysene ug/L 39.750 79 17-168ND
Di-n-butylphthalate ug/L 46.550 93 1-118ND
Di-n-octylphthalate ug/L 45.650 91 4-146ND
Dibenz(a,h)anthracene ug/L 36.850 74 1-227ND
Diethylphthalate ug/L 37.550 75 1-114ND
Dimethylphthalate ug/L 35.350 71 1-112ND
Fluoranthene ug/L 46.250 92 26-137ND
Fluorene ug/L 38.050 76 59-121ND
Hexachloro-1,3-butadiene ug/L 27.850 56 24-116ND
Hexachlorobenzene ug/L 38.250 76 1-152ND
Hexachlorocyclopentadiene ug/L 12.750 25 25-150ND
Hexachloroethane ug/L 31.750 63 40-113ND
Indeno(1,2,3-cd)pyrene ug/L 36.550 73 1-171ND
Isophorone ug/L 26.150 52 21-196ND
N-Nitroso-di-n-propylamine ug/L 27.650 55 1-230ND
N-Nitrosodimethylamine ug/L 18.050 35 25-150ND
N-Nitrosodiphenylamine ug/L 28.850 58 25-150ND
Naphthalene ug/L 64.350 51 21-13339.0
Nitrobenzene ug/L 54.450 109 35-180ND
Pentachlorophenol ug/L 68.9100 69 14-176ND
Phenanthrene ug/L 37.250 74 54-120ND
Phenol ug/L 13.250 26 5-112ND
Pyrene ug/L 39.650 79 52-115ND
2,4,6-Tribromophenol (S)%70 10-137
REPORT OF LABORATORY ANALYSIS
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Page 22 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1618492MATRIX SPIKE SAMPLE:
MSSpike
Result
92277684002
2-Fluorobiphenyl (S)%61 15-120
2-Fluorophenol (S)%33 10-120
Nitrobenzene-d5 (S)%54 10-120
Phenol-d6 (S)%23 10-120
Terphenyl-d14 (S)%58 11-131
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277685002
1618493SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L <0.98 30<0.98
2,4,6-Trichlorophenol ug/L <1.3 30<1.3
2,4-Dichlorophenol ug/L <1.7 30<1.7
2,4-Dimethylphenol ug/L <1.2 30<1.2
2,4-Dinitrophenol ug/L <9.0 30<9.0
2,4-Dinitrotoluene ug/L <0.90 30<0.90
2,6-Dinitrotoluene ug/L <0.98 30<0.98
2-Chloronaphthalene ug/L <0.98 30<0.98
2-Chlorophenol ug/L <1.3 30<1.3
2-Nitrophenol ug/L <0.91 30<0.91
3,3'-Dichlorobenzidine ug/L <2.1 30<2.1
4,6-Dinitro-2-methylphenol ug/L <2.6 30<2.6
4-Bromophenylphenyl ether ug/L <0.82 30<0.82
4-Chloro-3-methylphenol ug/L <3.7 30<3.7
4-Chlorophenylphenyl ether ug/L <0.87 30<0.87
4-Nitrophenol ug/L <4.1 30<4.1
Acenaphthene ug/L <0.25 30<0.25
Acenaphthylene ug/L <0.21 30<0.21
Anthracene ug/L <0.14 30<0.14
Benzo(a)anthracene ug/L <0.33 30<0.33
Benzo(a)pyrene ug/L <0.30 30<0.30
Benzo(b)fluoranthene ug/L <0.28 30<0.28
Benzo(g,h,i)perylene ug/L <0.38 30<0.38
Benzo(k)fluoranthene ug/L <0.43 30<0.43
bis(2-Chloroethoxy)methane ug/L <0.92 30<0.92
bis(2-Chloroethyl) ether ug/L <1.0 30<1.0
bis(2-Chloroisopropyl) ether ug/L <0.95 30<0.95
bis(2-Ethylhexyl)phthalate ug/L 4.0J 301.5J
Butylbenzylphthalate ug/L <0.79 30<0.79
Chrysene ug/L <0.21 30<0.21
Di-n-butylphthalate ug/L <0.75 30<0.75
Di-n-octylphthalate ug/L <0.66 30<0.66
Dibenz(a,h)anthracene ug/L <0.55 30<0.55
Diethylphthalate ug/L <0.58 30<0.58
Dimethylphthalate ug/L <0.76 30<0.76
Fluoranthene ug/L <0.21 30<0.21
REPORT OF LABORATORY ANALYSIS
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Page 23 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277685002
1618493SAMPLE DUPLICATE:
Fluorene ug/L <0.21 30<0.21
Hexachloro-1,3-butadiene ug/L <0.94 30<0.94
Hexachlorobenzene ug/L <0.72 30<0.72
Hexachlorocyclopentadiene ug/L <0.88 30<0.88
Hexachloroethane ug/L <1.1 30<1.1
Indeno(1,2,3-cd)pyrene ug/L <0.29 30<0.29
Isophorone ug/L <0.89 30<0.89
N-Nitroso-di-n-propylamine ug/L <0.99 30<0.99
N-Nitrosodimethylamine ug/L <0.91 30<0.91
N-Nitrosodiphenylamine ug/L <1.0 30<1.0
Naphthalene ug/L <0.34 30<0.34
Nitrobenzene ug/L <1.1 30<1.1
Pentachlorophenol ug/L <4.6 30<4.6
Phenanthrene ug/L <0.22 30<0.22
Phenol ug/L <1.9 30<1.9
Pyrene ug/L <0.19 30<0.19
2,4,6-Tribromophenol (S)%90 585
2-Fluorobiphenyl (S)%79 2264
2-Fluorophenol (S)%37 2230
Nitrobenzene-d5 (S)%74 1464
Phenol-d6 (S)%24 1820
Terphenyl-d14 (S)%93 290
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 24 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39527
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92277685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1621734
Associated Lab Samples:92277685002
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L <100 100 N212/09/15 15:39100
Aliphatic (C19-C36)ug/L <100 100 N212/09/15 15:39100
Aromatic (C11-C22)ug/L <100 100 N212/09/15 15:39100
2-Bromonaphthalene (S)%80 40-140 12/09/15 15:39
2-Fluorobiphenyl (S)%82 40-140 12/09/15 15:39
Nonatriacontane (S)%88 40-140 12/09/15 15:39
o-Terphenyl (S)%80 40-140 12/09/15 15:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621735LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1621736
Aliphatic (C09-C18)ug/L 216 N23007240-14070209 3 50
Aliphatic (C19-C36)ug/L 323 N24008140-14089356 10 50
Aromatic (C11-C22)ug/L 752 N28508840-14085721 4 50
2-Bromonaphthalene (S)%87 40-14088
2-Fluorobiphenyl (S)%89 40-14088
Nonatriacontane (S)%92 40-14088
o-Terphenyl (S)%86 40-14080
REPORT OF LABORATORY ANALYSIS
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Page 25 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Tentatively identified compound (TIC) based on mass spectral library search. Result is estimated.N
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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Page 26 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277685
PANTRY #3471 GW
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277685002 OEXT/39527 GCSV/23492DW-2 MADEP EPH MADEP EPH
92277685002 GCV/10139DW-2 MADEP VPH
92277685002 MPRP/20176 ICP/18200DW-2 EPA 3010A EPA 6010
92277685002 OEXT/39417 MSSV/11596DW-2 EPA 625 EPA 625
92277685001 MSV/34531PW-1 SM 6200B
92277685002 MSV/34531DW-2 SM 6200B
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 27 of 29
Page 28 of 29
Page 29 of 29
#=CL#
December 22, 2015
LIMS USE: FR - MAUREEN JACKSON
LIMS OBJECT ID: 92278649
92278649
Project:
Pace Project No.:
RE:
Maureen Jackson
ATC Group Services LLC
2725 E. Millbrook Road
Suite 121
Raleigh, NC 27604
PANTRY #3471
Dear Maureen Jackson:
Enclosed are the analytical results for sample(s) received by the laboratory on December 07, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 64
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92278649
PANTRY #3471
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 64
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92278649
PANTRY #3471
Lab ID Sample ID Matrix Date Collected Date Received
92278649001 SD-19 Solid 11/30/15 11:00 12/07/15 08:40
92278649002 SD-25 Solid 11/30/15 11:45 12/07/15 08:40
92278649003 SD-26 Solid 11/30/15 12:10 12/07/15 08:40
92278649004 SK-30 Solid 11/30/15 12:45 12/07/15 08:40
92278649005 SK-25 Solid 11/30/15 13:45 12/07/15 08:40
92278649006 SD-10 Solid 11/30/15 14:30 12/07/15 08:40
92278649007 SD-11 Solid 11/30/15 15:15 12/07/15 08:40
92278649008 SD-13 Solid 11/30/15 16:00 12/07/15 08:40
REPORT OF LABORATORY ANALYSIS
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Page 3 of 64
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92278649
PANTRY #3471
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92278649001 SD-19 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649002 SD-25 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649003 SD-26 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649004 SK-30 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649005 SK-25 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649006 SD-10 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649007 SD-11 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92278649008 SD-13 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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Page 4 of 64
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92278649
PANTRY #3471
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 64
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92278649
PANTRY #3471
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92278649001 SD-19
Acetone 31.7J ug/kg 12/08/15 20:09128EPA 8260
Methylene Chloride 4.3J ug/kg 12/08/15 20:09 C925.5EPA 8260
Percent Moisture 4.9 %12/08/15 11:230.10ASTM D2974-87
92278649002 SD-25
Fluoranthene 80.4J ug/kg 12/14/15 18:49343EPA 8270
Phenanthrene 58.5J ug/kg 12/14/15 18:49343EPA 8270
Pyrene 68.7J ug/kg 12/14/15 18:49343EPA 8270
Acetone 27.8J ug/kg 12/08/15 20:2997.0EPA 8260
Percent Moisture 3.8 %12/08/15 11:230.10ASTM D2974-87
92278649003 SD-26
Acetone 13.1J ug/kg 12/08/15 20:49110EPA 8260
Percent Moisture 5.2 %12/08/15 11:230.10ASTM D2974-87
92278649004 SK-30
Aromatic (C11-C22)32.0 mg/kg 12/15/15 03:00 N213.9MADEP EPH
Benzo(a)anthracene 110J ug/kg 12/14/15 05:02458EPA 8270
Benzo(a)pyrene 90.0J ug/kg 12/14/15 05:02458EPA 8270
Benzo(b)fluoranthene 115J ug/kg 12/14/15 05:02458EPA 8270
Chrysene 117J ug/kg 12/14/15 05:02458EPA 8270
Fluoranthene 343J ug/kg 12/14/15 05:02458EPA 8270
Phenanthrene 175J ug/kg 12/14/15 05:02458EPA 8270
Pyrene 296J ug/kg 12/14/15 05:02458EPA 8270
Acetone 24.9J ug/kg 12/08/15 21:09133EPA 8260
Methylene Chloride 12.8J ug/kg 12/08/15 21:0926.6EPA 8260
Percent Moisture 27.9 %12/08/15 11:230.10ASTM D2974-87
92278649005 SK-25
Acetone 17.7J ug/kg 12/08/15 21:29136EPA 8260
Methylene Chloride 8.3J ug/kg 12/08/15 21:2927.3EPA 8260
Percent Moisture 23.5 %12/08/15 11:240.10ASTM D2974-87
92278649006 SD-10
Aliphatic (C09-C18)256 mg/kg 12/17/15 11:40 N2105MADEP EPH
Aromatic (C11-C22)83.3 mg/kg 12/15/15 03:55 N213.1MADEP EPH
Aliphatic (C05-C08)10.9 mg/kg 12/16/15 18:11 N23.3MADEP VPH
Aliphatic (C09-C12)62.6 mg/kg 12/16/15 18:11 N23.3MADEP VPH
Aromatic (C09-C10)101 mg/kg 12/16/15 18:11 N23.3MADEP VPH
1-Methylnaphthalene 149J ug/kg 12/14/15 20:11431EPA 8270
2-Methylnaphthalene 228J ug/kg 12/14/15 20:11431EPA 8270
n-Butylbenzene 950 ug/kg 12/08/15 21:48314EPA 8260
sec-Butylbenzene 589 ug/kg 12/08/15 21:48314EPA 8260
Ethylbenzene 120J ug/kg 12/08/15 21:48314EPA 8260
Isopropylbenzene (Cumene)222J ug/kg 12/08/15 21:48314EPA 8260
p-Isopropyltoluene 407 ug/kg 12/08/15 21:48314EPA 8260
Naphthalene 956 ug/kg 12/08/15 21:48314EPA 8260
n-Propylbenzene 429 ug/kg 12/08/15 21:48314EPA 8260
1,2,4-Trimethylbenzene 1670 ug/kg 12/08/15 21:48314EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 64
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92278649
PANTRY #3471
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92278649006 SD-10
1,3,5-Trimethylbenzene 269J ug/kg 12/08/15 21:48314EPA 8260
Percent Moisture 23.5 %12/08/15 11:240.10ASTM D2974-87
92278649007 SD-11
Methylene Chloride 8.7J ug/kg 12/08/15 22:0824.1EPA 8260
Percent Moisture 22.1 %12/08/15 11:240.10ASTM D2974-87
92278649008 SD-13
Methylene Chloride 6.5J ug/kg 12/09/15 22:0527.0EPA 8260
Naphthalene 4.0J ug/kg 12/09/15 22:05 B6.7EPA 8260
Percent Moisture 28.8 %12/08/15 11:240.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-19 Lab ID:92278649001 Collected:11/30/15 11:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<10.5 mg/kg 12/12/15 00:41 N212/10/15 10:1210.5 10.5 1
Aliphatic (C19-C36)<10.5 mg/kg 12/12/15 00:41 N212/10/15 10:1210.5 10.5 1
Aromatic (C11-C22)<10.5 mg/kg 12/15/15 01:39 N212/10/15 10:1210.5 10.5 1
Surrogates
Nonatriacontane (S)93 %12/12/15 00:41 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)71 %12/15/15 01:39 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)88 %12/15/15 01:39 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)76 %12/15/15 01:39 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<4.1 mg/kg 12/16/15 15:40 N212/16/15 14:154.1 4.1 1
Aliphatic (C09-C12)<4.1 mg/kg 12/16/15 15:40 N212/16/15 14:154.1 4.1 1
Aromatic (C09-C10)<4.1 mg/kg 12/16/15 15:40 N212/16/15 14:154.1 4.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)94 %12/16/15 15:40 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)93 %12/16/15 15:40 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <79.9 ug/kg 12/14/15 03:58 83-32-912/07/15 15:3034779.9 1
Acenaphthylene <82.0 ug/kg 12/14/15 03:58 208-96-812/07/15 15:3034782.0 1
Aniline <93.6 ug/kg 12/14/15 03:58 62-53-312/07/15 15:3034793.6 1
Anthracene <77.8 ug/kg 12/14/15 03:58 120-12-712/07/15 15:3034777.8 1
Benzo(a)anthracene <64.1 ug/kg 12/14/15 03:58 56-55-312/07/15 15:3034764.1 1
Benzo(a)pyrene <66.2 ug/kg 12/14/15 03:58 50-32-812/07/15 15:3034766.2 1
Benzo(b)fluoranthene <59.9 ug/kg 12/14/15 03:58 205-99-212/07/15 15:3034759.9 1
Benzo(g,h,i)perylene <88.3 ug/kg 12/14/15 03:58 191-24-212/07/15 15:3034788.3 1
Benzo(k)fluoranthene <68.4 ug/kg 12/14/15 03:58 207-08-912/07/15 15:3034768.4 1
Benzoic Acid <63.1 ug/kg 12/14/15 03:58 65-85-012/07/15 15:30174063.1 1
Benzyl alcohol <69.4 ug/kg 12/14/15 03:58 100-51-612/07/15 15:3069469.4 1
4-Bromophenylphenyl ether <63.1 ug/kg 12/14/15 03:58 101-55-312/07/15 15:3034763.1 1
Butylbenzylphthalate <73.6 ug/kg 12/14/15 03:58 85-68-712/07/15 15:3034773.6 1
4-Chloro-3-methylphenol <71.5 ug/kg 12/14/15 03:58 59-50-712/07/15 15:3069471.5 1
4-Chloroaniline <96.7 ug/kg 12/14/15 03:58 106-47-812/07/15 15:30174096.7 1
bis(2-Chloroethoxy)methane <81.0 ug/kg 12/14/15 03:58 111-91-112/07/15 15:3034781.0 1
bis(2-Chloroethyl) ether <88.3 ug/kg 12/14/15 03:58 111-44-412/07/15 15:3034788.3 1
bis(2-Chloroisopropyl) ether <92.5 ug/kg 12/14/15 03:58 108-60-112/07/15 15:3034792.5 1
2-Chloronaphthalene <68.4 ug/kg 12/14/15 03:58 91-58-712/07/15 15:3034768.4 1
2-Chlorophenol <94.6 ug/kg 12/14/15 03:58 95-57-812/07/15 15:3034794.6 1
4-Chlorophenylphenyl ether <71.5 ug/kg 12/14/15 03:58 7005-72-312/07/15 15:3034771.5 1
Chrysene <46.3 ug/kg 12/14/15 03:58 218-01-912/07/15 15:3034746.3 1
Dibenz(a,h)anthracene <73.6 ug/kg 12/14/15 03:58 53-70-312/07/15 15:3034773.6 1
Dibenzofuran <56.8 ug/kg 12/14/15 03:58 132-64-912/07/15 15:3034756.8 1
1,2-Dichlorobenzene <92.5 ug/kg 12/14/15 03:58 95-50-112/07/15 15:3034792.5 1
1,3-Dichlorobenzene <78.9 ug/kg 12/14/15 03:58 541-73-112/07/15 15:3034778.9 1
1,4-Dichlorobenzene <97.8 ug/kg 12/14/15 03:58 106-46-712/07/15 15:3034797.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-19 Lab ID:92278649001 Collected:11/30/15 11:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <75.7 ug/kg 12/14/15 03:58 91-94-112/07/15 15:30174075.7 1
2,4-Dichlorophenol <75.7 ug/kg 12/14/15 03:58 120-83-212/07/15 15:3034775.7 1
Diethylphthalate <53.6 ug/kg 12/14/15 03:58 84-66-212/07/15 15:3034753.6 1
2,4-Dimethylphenol <137 ug/kg 12/14/15 03:58 105-67-912/07/15 15:303471371
Dimethylphthalate <70.5 ug/kg 12/14/15 03:58 131-11-312/07/15 15:3034770.5 1
Di-n-butylphthalate <56.8 ug/kg 12/14/15 03:58 84-74-212/07/15 15:3034756.8 1
4,6-Dinitro-2-methylphenol <69.4 ug/kg 12/14/15 03:58 534-52-112/07/15 15:3069469.4 1
2,4-Dinitrophenol <56.8 ug/kg 12/14/15 03:58 51-28-512/07/15 15:30174056.8 1
2,4-Dinitrotoluene <65.2 ug/kg 12/14/15 03:58 121-14-212/07/15 15:3034765.2 1
2,6-Dinitrotoluene <72.6 ug/kg 12/14/15 03:58 606-20-212/07/15 15:3034772.6 1
Di-n-octylphthalate <72.6 ug/kg 12/14/15 03:58 117-84-012/07/15 15:3034772.6 1
bis(2-Ethylhexyl)phthalate <94.6 ug/kg 12/14/15 03:58 117-81-712/07/15 15:3034794.6 1
Fluoranthene <50.5 ug/kg 12/14/15 03:58 206-44-012/07/15 15:3034750.5 1
Fluorene <71.5 ug/kg 12/14/15 03:58 86-73-712/07/15 15:3034771.5 1
Hexachloro-1,3-butadiene <59.9 ug/kg 12/14/15 03:58 87-68-312/07/15 15:3034759.9 1
Hexachlorobenzene <44.2 ug/kg 12/14/15 03:58 118-74-112/07/15 15:3034744.2 1
Hexachlorocyclopentadiene <64.1 ug/kg 12/14/15 03:58 77-47-412/07/15 15:3034764.1 1
Hexachloroethane <91.5 ug/kg 12/14/15 03:58 67-72-112/07/15 15:3034791.5 1
Indeno(1,2,3-cd)pyrene <71.5 ug/kg 12/14/15 03:58 193-39-512/07/15 15:3034771.5 1
Isophorone <77.8 ug/kg 12/14/15 03:58 78-59-112/07/15 15:3034777.8 1
1-Methylnaphthalene <90.4 ug/kg 12/14/15 03:58 90-12-012/07/15 15:3034790.4 1
2-Methylnaphthalene <74.7 ug/kg 12/14/15 03:58 91-57-612/07/15 15:3034774.7 1
2-Methylphenol(o-Cresol)<105 ug/kg 12/14/15 03:58 95-48-712/07/15 15:303471051
3&4-Methylphenol(m&p Cresol)<137 ug/kg 12/14/15 03:5812/07/15 15:303471371
Naphthalene <85.2 ug/kg 12/14/15 03:58 91-20-312/07/15 15:3034785.2 1
2-Nitroaniline <107 ug/kg 12/14/15 03:58 88-74-412/07/15 15:3017401071
3-Nitroaniline <94.6 ug/kg 12/14/15 03:58 99-09-212/07/15 15:30174094.6 1
4-Nitroaniline <97.8 ug/kg 12/14/15 03:58 100-01-612/07/15 15:3069497.8 1
Nitrobenzene <94.6 ug/kg 12/14/15 03:58 98-95-312/07/15 15:3034794.6 1
2-Nitrophenol <84.1 ug/kg 12/14/15 03:58 88-75-512/07/15 15:3034784.1 1
4-Nitrophenol <62.0 ug/kg 12/14/15 03:58 100-02-712/07/15 15:30174062.0 1
N-Nitrosodimethylamine <113 ug/kg 12/14/15 03:58 62-75-912/07/15 15:303471131
N-Nitroso-di-n-propylamine <66.2 ug/kg 12/14/15 03:58 621-64-712/07/15 15:3034766.2 1
N-Nitrosodiphenylamine <103 ug/kg 12/14/15 03:58 86-30-612/07/15 15:303471031
Pentachlorophenol <63.1 ug/kg 12/14/15 03:58 87-86-512/07/15 15:30174063.1 1
Phenanthrene <57.8 ug/kg 12/14/15 03:58 85-01-812/07/15 15:3034757.8 1
Phenol <104 ug/kg 12/14/15 03:58 108-95-212/07/15 15:303471041
Pyrene <58.9 ug/kg 12/14/15 03:58 129-00-012/07/15 15:3034758.9 1
1,2,4-Trichlorobenzene <67.3 ug/kg 12/14/15 03:58 120-82-112/07/15 15:3034767.3 1
2,4,5-Trichlorophenol <107 ug/kg 12/14/15 03:58 95-95-412/07/15 15:303471071
2,4,6-Trichlorophenol <76.8 ug/kg 12/14/15 03:58 88-06-212/07/15 15:3034776.8 1
Surrogates
Nitrobenzene-d5 (S)63 %12/14/15 03:58 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)73 %12/14/15 03:58 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)80 %12/14/15 03:58 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-19 Lab ID:92278649001 Collected:11/30/15 11:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)61 %12/14/15 03:58 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)62 %12/14/15 03:58 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)78 %12/14/15 03:58 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 31.7J ug/kg 12/08/15 20:09 67-64-112812.8 1
Benzene <2.0 ug/kg 12/08/15 20:09 71-43-26.4 2.0 1
Bromobenzene <2.6 ug/kg 12/08/15 20:09 108-86-16.4 2.6 1
Bromochloromethane <2.2 ug/kg 12/08/15 20:09 74-97-56.4 2.2 1
Bromodichloromethane <2.4 ug/kg 12/08/15 20:09 75-27-46.4 2.4 1
Bromoform <2.9 ug/kg 12/08/15 20:09 75-25-26.4 2.9 1
Bromomethane <3.2 ug/kg 12/08/15 20:09 74-83-912.8 3.2 1
2-Butanone (MEK)<3.7 ug/kg 12/08/15 20:09 78-93-31283.7 1
n-Butylbenzene <2.3 ug/kg 12/08/15 20:09 104-51-86.4 2.3 1
sec-Butylbenzene <2.0 ug/kg 12/08/15 20:09 135-98-86.4 2.0 1
tert-Butylbenzene <2.6 ug/kg 12/08/15 20:09 98-06-66.4 2.6 1
Carbon tetrachloride <3.3 ug/kg 12/08/15 20:09 56-23-56.4 3.3 1
Chlorobenzene <2.4 ug/kg 12/08/15 20:09 108-90-76.4 2.4 1
Chloroethane <3.1 ug/kg 12/08/15 20:09 75-00-312.8 3.1 1
Chloroform <2.0 ug/kg 12/08/15 20:09 67-66-36.4 2.0 1
Chloromethane <3.1 ug/kg 12/08/15 20:09 74-87-312.8 3.1 1
2-Chlorotoluene <2.2 ug/kg 12/08/15 20:09 95-49-86.4 2.2 1
4-Chlorotoluene <2.3 ug/kg 12/08/15 20:09 106-43-46.4 2.3 1
1,2-Dibromo-3-chloropropane <4.6 ug/kg 12/08/15 20:09 96-12-86.4 4.6 1
Dibromochloromethane <2.3 ug/kg 12/08/15 20:09 124-48-16.4 2.3 1
1,2-Dibromoethane (EDB)<2.3 ug/kg 12/08/15 20:09 106-93-46.4 2.3 1
Dibromomethane <3.2 ug/kg 12/08/15 20:09 74-95-36.4 3.2 1
1,2-Dichlorobenzene <2.4 ug/kg 12/08/15 20:09 95-50-16.4 2.4 1
1,3-Dichlorobenzene <2.6 ug/kg 12/08/15 20:09 541-73-16.4 2.6 1
1,4-Dichlorobenzene <2.2 ug/kg 12/08/15 20:09 106-46-76.4 2.2 1
Dichlorodifluoromethane <4.6 ug/kg 12/08/15 20:09 75-71-812.8 4.6 1
1,1-Dichloroethane <1.9 ug/kg 12/08/15 20:09 75-34-36.4 1.9 1
1,2-Dichloroethane <2.8 ug/kg 12/08/15 20:09 107-06-26.4 2.8 1
1,1-Dichloroethene <2.3 ug/kg 12/08/15 20:09 75-35-46.4 2.3 1
cis-1,2-Dichloroethene <1.8 ug/kg 12/08/15 20:09 156-59-26.4 1.8 1
trans-1,2-Dichloroethene <2.4 ug/kg 12/08/15 20:09 156-60-56.4 2.4 1
1,2-Dichloropropane <2.2 ug/kg 12/08/15 20:09 78-87-56.4 2.2 1
1,3-Dichloropropane <2.4 ug/kg 12/08/15 20:09 142-28-96.4 2.4 1
2,2-Dichloropropane <2.2 ug/kg 12/08/15 20:09 594-20-76.4 2.2 1
1,1-Dichloropropene <1.9 ug/kg 12/08/15 20:09 563-58-66.4 1.9 1
cis-1,3-Dichloropropene <2.3 ug/kg 12/08/15 20:09 10061-01-56.4 2.3 1
trans-1,3-Dichloropropene <1.9 ug/kg 12/08/15 20:09 10061-02-66.4 1.9 1
Diisopropyl ether <2.2 ug/kg 12/08/15 20:09 108-20-36.4 2.2 1
Ethylbenzene <2.3 ug/kg 12/08/15 20:09 100-41-46.4 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-19 Lab ID:92278649001 Collected:11/30/15 11:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.6 ug/kg 12/08/15 20:09 87-68-36.4 2.6 1
2-Hexanone <5.0 ug/kg 12/08/15 20:09 591-78-663.8 5.0 1
Isopropylbenzene (Cumene)<2.4 ug/kg 12/08/15 20:09 98-82-86.4 2.4 1
p-Isopropyltoluene <2.2 ug/kg 12/08/15 20:09 99-87-66.4 2.2 1
Methylene Chloride 4.3J ug/kg 12/08/15 20:09 75-09-2 C925.5 3.8 1
4-Methyl-2-pentanone (MIBK)<4.7 ug/kg 12/08/15 20:09 108-10-163.8 4.7 1
Methyl-tert-butyl ether <1.9 ug/kg 12/08/15 20:09 1634-04-46.4 1.9 1
Naphthalene <1.5 ug/kg 12/08/15 20:09 91-20-36.4 1.5 1
n-Propylbenzene <2.2 ug/kg 12/08/15 20:09 103-65-16.4 2.2 1
Styrene <2.3 ug/kg 12/08/15 20:09 100-42-56.4 2.3 1
1,1,1,2-Tetrachloroethane <2.7 ug/kg 12/08/15 20:09 630-20-66.4 2.7 1
1,1,2,2-Tetrachloroethane <2.4 ug/kg 12/08/15 20:09 79-34-56.4 2.4 1
Tetrachloroethene <2.2 ug/kg 12/08/15 20:09 127-18-46.4 2.2 1
Toluene <2.3 ug/kg 12/08/15 20:09 108-88-36.4 2.3 1
1,2,3-Trichlorobenzene <2.8 ug/kg 12/08/15 20:09 87-61-66.4 2.8 1
1,2,4-Trichlorobenzene <2.0 ug/kg 12/08/15 20:09 120-82-16.4 2.0 1
1,1,1-Trichloroethane <2.3 ug/kg 12/08/15 20:09 71-55-66.4 2.3 1
1,1,2-Trichloroethane <2.7 ug/kg 12/08/15 20:09 79-00-56.4 2.7 1
Trichloroethene <2.7 ug/kg 12/08/15 20:09 79-01-66.4 2.7 1
Trichlorofluoromethane <2.8 ug/kg 12/08/15 20:09 75-69-46.4 2.8 1
1,2,3-Trichloropropane <2.0 ug/kg 12/08/15 20:09 96-18-46.4 2.0 1
1,2,4-Trimethylbenzene <2.6 ug/kg 12/08/15 20:09 95-63-66.4 2.6 1
1,3,5-Trimethylbenzene <2.3 ug/kg 12/08/15 20:09 108-67-86.4 2.3 1
Vinyl acetate <11.2 ug/kg 12/08/15 20:09 108-05-463.8 11.2 1
Vinyl chloride <2.3 ug/kg 12/08/15 20:09 75-01-412.8 2.3 1
Xylene (Total)<4.6 ug/kg 12/08/15 20:09 1330-20-712.8 4.6 1
m&p-Xylene <4.6 ug/kg 12/08/15 20:09 179601-23-112.8 4.6 1
o-Xylene <2.4 ug/kg 12/08/15 20:09 95-47-66.4 2.4 1
Surrogates
Toluene-d8 (S)98 %12/08/15 20:09 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %12/08/15 20:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/08/15 20:09 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 4.9 %12/08/15 11:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-25 Lab ID:92278649002 Collected:11/30/15 11:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<10.4 mg/kg 12/12/15 01:09 N212/10/15 10:1210.4 10.4 1
Aliphatic (C19-C36)<10.4 mg/kg 12/12/15 01:09 N212/10/15 10:1210.4 10.4 1
Aromatic (C11-C22)<10.4 mg/kg 12/15/15 02:06 N212/10/15 10:1210.4 10.4 1
Surrogates
Nonatriacontane (S)73 %12/12/15 01:09 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)65 %12/15/15 02:06 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)86 %12/15/15 02:06 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)81 %12/15/15 02:06 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<4.1 mg/kg 12/16/15 16:10 N212/16/15 14:154.1 4.1 1
Aliphatic (C09-C12)<4.1 mg/kg 12/16/15 16:10 N212/16/15 14:154.1 4.1 1
Aromatic (C09-C10)<4.1 mg/kg 12/16/15 16:10 N212/16/15 14:154.1 4.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)95 %12/16/15 16:10 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)94 %12/16/15 16:10 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <79.0 ug/kg 12/14/15 18:49 83-32-912/07/15 15:3034379.0 1
Acenaphthylene <81.1 ug/kg 12/14/15 18:49 208-96-812/07/15 15:3034381.1 1
Aniline <92.5 ug/kg 12/14/15 18:49 62-53-312/07/15 15:3034392.5 1
Anthracene <76.9 ug/kg 12/14/15 18:49 120-12-712/07/15 15:3034376.9 1
Benzo(a)anthracene <63.4 ug/kg 12/14/15 18:49 56-55-312/07/15 15:3034363.4 1
Benzo(a)pyrene <65.5 ug/kg 12/14/15 18:49 50-32-812/07/15 15:3034365.5 1
Benzo(b)fluoranthene <59.3 ug/kg 12/14/15 18:49 205-99-212/07/15 15:3034359.3 1
Benzo(g,h,i)perylene <87.3 ug/kg 12/14/15 18:49 191-24-212/07/15 15:3034387.3 1
Benzo(k)fluoranthene <67.6 ug/kg 12/14/15 18:49 207-08-912/07/15 15:3034367.6 1
Benzoic Acid <62.4 ug/kg 12/14/15 18:49 65-85-012/07/15 15:30172062.4 1
Benzyl alcohol <68.6 ug/kg 12/14/15 18:49 100-51-612/07/15 15:3068668.6 1
4-Bromophenylphenyl ether <62.4 ug/kg 12/14/15 18:49 101-55-312/07/15 15:3034362.4 1
Butylbenzylphthalate <72.8 ug/kg 12/14/15 18:49 85-68-712/07/15 15:3034372.8 1
4-Chloro-3-methylphenol <70.7 ug/kg 12/14/15 18:49 59-50-712/07/15 15:3068670.7 1
4-Chloroaniline <95.7 ug/kg 12/14/15 18:49 106-47-812/07/15 15:30172095.7 1
bis(2-Chloroethoxy)methane <80.1 ug/kg 12/14/15 18:49 111-91-112/07/15 15:3034380.1 1
bis(2-Chloroethyl) ether <87.3 ug/kg 12/14/15 18:49 111-44-412/07/15 15:3034387.3 1
bis(2-Chloroisopropyl) ether <91.5 ug/kg 12/14/15 18:49 108-60-112/07/15 15:3034391.5 1
2-Chloronaphthalene <67.6 ug/kg 12/14/15 18:49 91-58-712/07/15 15:3034367.6 1
2-Chlorophenol <93.6 ug/kg 12/14/15 18:49 95-57-812/07/15 15:3034393.6 1
4-Chlorophenylphenyl ether <70.7 ug/kg 12/14/15 18:49 7005-72-312/07/15 15:3034370.7 1
Chrysene <45.7 ug/kg 12/14/15 18:49 218-01-912/07/15 15:3034345.7 1
Dibenz(a,h)anthracene <72.8 ug/kg 12/14/15 18:49 53-70-312/07/15 15:3034372.8 1
Dibenzofuran <56.1 ug/kg 12/14/15 18:49 132-64-912/07/15 15:3034356.1 1
1,2-Dichlorobenzene <91.5 ug/kg 12/14/15 18:49 95-50-112/07/15 15:3034391.5 1
1,3-Dichlorobenzene <78.0 ug/kg 12/14/15 18:49 541-73-112/07/15 15:3034378.0 1
1,4-Dichlorobenzene <96.7 ug/kg 12/14/15 18:49 106-46-712/07/15 15:3034396.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-25 Lab ID:92278649002 Collected:11/30/15 11:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <74.9 ug/kg 12/14/15 18:49 91-94-112/07/15 15:30172074.9 1
2,4-Dichlorophenol <74.9 ug/kg 12/14/15 18:49 120-83-212/07/15 15:3034374.9 1
Diethylphthalate <53.0 ug/kg 12/14/15 18:49 84-66-212/07/15 15:3034353.0 1
2,4-Dimethylphenol <135 ug/kg 12/14/15 18:49 105-67-912/07/15 15:303431351
Dimethylphthalate <69.7 ug/kg 12/14/15 18:49 131-11-312/07/15 15:3034369.7 1
Di-n-butylphthalate <56.1 ug/kg 12/14/15 18:49 84-74-212/07/15 15:3034356.1 1
4,6-Dinitro-2-methylphenol <68.6 ug/kg 12/14/15 18:49 534-52-112/07/15 15:3068668.6 1
2,4-Dinitrophenol <56.1 ug/kg 12/14/15 18:49 51-28-512/07/15 15:30172056.1 1
2,4-Dinitrotoluene <64.5 ug/kg 12/14/15 18:49 121-14-212/07/15 15:3034364.5 1
2,6-Dinitrotoluene <71.7 ug/kg 12/14/15 18:49 606-20-212/07/15 15:3034371.7 1
Di-n-octylphthalate <71.7 ug/kg 12/14/15 18:49 117-84-012/07/15 15:3034371.7 1
bis(2-Ethylhexyl)phthalate <93.6 ug/kg 12/14/15 18:49 117-81-712/07/15 15:3034393.6 1
Fluoranthene 80.4J ug/kg 12/14/15 18:49 206-44-012/07/15 15:3034349.9 1
Fluorene <70.7 ug/kg 12/14/15 18:49 86-73-712/07/15 15:3034370.7 1
Hexachloro-1,3-butadiene <59.3 ug/kg 12/14/15 18:49 87-68-312/07/15 15:3034359.3 1
Hexachlorobenzene <43.7 ug/kg 12/14/15 18:49 118-74-112/07/15 15:3034343.7 1
Hexachlorocyclopentadiene <63.4 ug/kg 12/14/15 18:49 77-47-412/07/15 15:3034363.4 1
Hexachloroethane <90.5 ug/kg 12/14/15 18:49 67-72-112/07/15 15:3034390.5 1
Indeno(1,2,3-cd)pyrene <70.7 ug/kg 12/14/15 18:49 193-39-512/07/15 15:3034370.7 1
Isophorone <76.9 ug/kg 12/14/15 18:49 78-59-112/07/15 15:3034376.9 1
1-Methylnaphthalene <89.4 ug/kg 12/14/15 18:49 90-12-012/07/15 15:3034389.4 1
2-Methylnaphthalene <73.8 ug/kg 12/14/15 18:49 91-57-612/07/15 15:3034373.8 1
2-Methylphenol(o-Cresol)<104 ug/kg 12/14/15 18:49 95-48-712/07/15 15:303431041
3&4-Methylphenol(m&p Cresol)<135 ug/kg 12/14/15 18:4912/07/15 15:303431351
Naphthalene <84.2 ug/kg 12/14/15 18:49 91-20-312/07/15 15:3034384.2 1
2-Nitroaniline <106 ug/kg 12/14/15 18:49 88-74-412/07/15 15:3017201061
3-Nitroaniline <93.6 ug/kg 12/14/15 18:49 99-09-212/07/15 15:30172093.6 1
4-Nitroaniline <96.7 ug/kg 12/14/15 18:49 100-01-612/07/15 15:3068696.7 1
Nitrobenzene <93.6 ug/kg 12/14/15 18:49 98-95-312/07/15 15:3034393.6 1
2-Nitrophenol <83.2 ug/kg 12/14/15 18:49 88-75-512/07/15 15:3034383.2 1
4-Nitrophenol <61.3 ug/kg 12/14/15 18:49 100-02-712/07/15 15:30172061.3 1
N-Nitrosodimethylamine <111 ug/kg 12/14/15 18:49 62-75-912/07/15 15:303431111
N-Nitroso-di-n-propylamine <65.5 ug/kg 12/14/15 18:49 621-64-712/07/15 15:3034365.5 1
N-Nitrosodiphenylamine <102 ug/kg 12/14/15 18:49 86-30-612/07/15 15:303431021
Pentachlorophenol <62.4 ug/kg 12/14/15 18:49 87-86-512/07/15 15:30172062.4 1
Phenanthrene 58.5J ug/kg 12/14/15 18:49 85-01-812/07/15 15:3034357.2 1
Phenol <103 ug/kg 12/14/15 18:49 108-95-212/07/15 15:303431031
Pyrene 68.7J ug/kg 12/14/15 18:49 129-00-012/07/15 15:3034358.2 1
1,2,4-Trichlorobenzene <66.5 ug/kg 12/14/15 18:49 120-82-112/07/15 15:3034366.5 1
2,4,5-Trichlorophenol <106 ug/kg 12/14/15 18:49 95-95-412/07/15 15:303431061
2,4,6-Trichlorophenol <75.9 ug/kg 12/14/15 18:49 88-06-212/07/15 15:3034375.9 1
Surrogates
Nitrobenzene-d5 (S)82 %12/14/15 18:49 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)83 %12/14/15 18:49 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)94 %12/14/15 18:49 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-25 Lab ID:92278649002 Collected:11/30/15 11:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)73 %12/14/15 18:49 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)73 %12/14/15 18:49 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)86 %12/14/15 18:49 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 27.8J ug/kg 12/08/15 20:29 67-64-197.0 9.7 1
Benzene <1.6 ug/kg 12/08/15 20:29 71-43-24.8 1.6 1
Bromobenzene <1.9 ug/kg 12/08/15 20:29 108-86-14.8 1.9 1
Bromochloromethane <1.6 ug/kg 12/08/15 20:29 74-97-54.8 1.6 1
Bromodichloromethane <1.8 ug/kg 12/08/15 20:29 75-27-44.8 1.8 1
Bromoform <2.2 ug/kg 12/08/15 20:29 75-25-24.8 2.2 1
Bromomethane <2.4 ug/kg 12/08/15 20:29 74-83-99.7 2.4 1
2-Butanone (MEK)<2.8 ug/kg 12/08/15 20:29 78-93-397.0 2.8 1
n-Butylbenzene <1.7 ug/kg 12/08/15 20:29 104-51-84.8 1.7 1
sec-Butylbenzene <1.6 ug/kg 12/08/15 20:29 135-98-84.8 1.6 1
tert-Butylbenzene <1.9 ug/kg 12/08/15 20:29 98-06-64.8 1.9 1
Carbon tetrachloride <2.5 ug/kg 12/08/15 20:29 56-23-54.8 2.5 1
Chlorobenzene <1.8 ug/kg 12/08/15 20:29 108-90-74.8 1.8 1
Chloroethane <2.3 ug/kg 12/08/15 20:29 75-00-39.7 2.3 1
Chloroform <1.6 ug/kg 12/08/15 20:29 67-66-34.8 1.6 1
Chloromethane <2.3 ug/kg 12/08/15 20:29 74-87-39.7 2.3 1
2-Chlorotoluene <1.6 ug/kg 12/08/15 20:29 95-49-84.8 1.6 1
4-Chlorotoluene <1.7 ug/kg 12/08/15 20:29 106-43-44.8 1.7 1
1,2-Dibromo-3-chloropropane <3.5 ug/kg 12/08/15 20:29 96-12-84.8 3.5 1
Dibromochloromethane <1.7 ug/kg 12/08/15 20:29 124-48-14.8 1.7 1
1,2-Dibromoethane (EDB)<1.7 ug/kg 12/08/15 20:29 106-93-44.8 1.7 1
Dibromomethane <2.4 ug/kg 12/08/15 20:29 74-95-34.8 2.4 1
1,2-Dichlorobenzene <1.8 ug/kg 12/08/15 20:29 95-50-14.8 1.8 1
1,3-Dichlorobenzene <1.9 ug/kg 12/08/15 20:29 541-73-14.8 1.9 1
1,4-Dichlorobenzene <1.6 ug/kg 12/08/15 20:29 106-46-74.8 1.6 1
Dichlorodifluoromethane <3.5 ug/kg 12/08/15 20:29 75-71-89.7 3.5 1
1,1-Dichloroethane <1.5 ug/kg 12/08/15 20:29 75-34-34.8 1.5 1
1,2-Dichloroethane <2.1 ug/kg 12/08/15 20:29 107-06-24.8 2.1 1
1,1-Dichloroethene <1.7 ug/kg 12/08/15 20:29 75-35-44.8 1.7 1
cis-1,2-Dichloroethene <1.4 ug/kg 12/08/15 20:29 156-59-24.8 1.4 1
trans-1,2-Dichloroethene <1.8 ug/kg 12/08/15 20:29 156-60-54.8 1.8 1
1,2-Dichloropropane <1.6 ug/kg 12/08/15 20:29 78-87-54.8 1.6 1
1,3-Dichloropropane <1.8 ug/kg 12/08/15 20:29 142-28-94.8 1.8 1
2,2-Dichloropropane <1.6 ug/kg 12/08/15 20:29 594-20-74.8 1.6 1
1,1-Dichloropropene <1.5 ug/kg 12/08/15 20:29 563-58-64.8 1.5 1
cis-1,3-Dichloropropene <1.7 ug/kg 12/08/15 20:29 10061-01-54.8 1.7 1
trans-1,3-Dichloropropene <1.5 ug/kg 12/08/15 20:29 10061-02-64.8 1.5 1
Diisopropyl ether <1.6 ug/kg 12/08/15 20:29 108-20-34.8 1.6 1
Ethylbenzene <1.7 ug/kg 12/08/15 20:29 100-41-44.8 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-25 Lab ID:92278649002 Collected:11/30/15 11:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <1.9 ug/kg 12/08/15 20:29 87-68-34.8 1.9 1
2-Hexanone <3.8 ug/kg 12/08/15 20:29 591-78-648.5 3.8 1
Isopropylbenzene (Cumene)<1.8 ug/kg 12/08/15 20:29 98-82-84.8 1.8 1
p-Isopropyltoluene <1.6 ug/kg 12/08/15 20:29 99-87-64.8 1.6 1
Methylene Chloride <2.9 ug/kg 12/08/15 20:29 75-09-219.4 2.9 1
4-Methyl-2-pentanone (MIBK)<3.6 ug/kg 12/08/15 20:29 108-10-148.5 3.6 1
Methyl-tert-butyl ether <1.5 ug/kg 12/08/15 20:29 1634-04-44.8 1.5 1
Naphthalene <1.2 ug/kg 12/08/15 20:29 91-20-34.8 1.2 1
n-Propylbenzene <1.6 ug/kg 12/08/15 20:29 103-65-14.8 1.6 1
Styrene <1.7 ug/kg 12/08/15 20:29 100-42-54.8 1.7 1
1,1,1,2-Tetrachloroethane <2.0 ug/kg 12/08/15 20:29 630-20-64.8 2.0 1
1,1,2,2-Tetrachloroethane <1.8 ug/kg 12/08/15 20:29 79-34-54.8 1.8 1
Tetrachloroethene <1.6 ug/kg 12/08/15 20:29 127-18-44.8 1.6 1
Toluene <1.7 ug/kg 12/08/15 20:29 108-88-34.8 1.7 1
1,2,3-Trichlorobenzene <2.1 ug/kg 12/08/15 20:29 87-61-64.8 2.1 1
1,2,4-Trichlorobenzene <1.6 ug/kg 12/08/15 20:29 120-82-14.8 1.6 1
1,1,1-Trichloroethane <1.7 ug/kg 12/08/15 20:29 71-55-64.8 1.7 1
1,1,2-Trichloroethane <2.0 ug/kg 12/08/15 20:29 79-00-54.8 2.0 1
Trichloroethene <2.0 ug/kg 12/08/15 20:29 79-01-64.8 2.0 1
Trichlorofluoromethane <2.1 ug/kg 12/08/15 20:29 75-69-44.8 2.1 1
1,2,3-Trichloropropane <1.6 ug/kg 12/08/15 20:29 96-18-44.8 1.6 1
1,2,4-Trimethylbenzene <1.9 ug/kg 12/08/15 20:29 95-63-64.8 1.9 1
1,3,5-Trimethylbenzene <1.7 ug/kg 12/08/15 20:29 108-67-84.8 1.7 1
Vinyl acetate <8.5 ug/kg 12/08/15 20:29 108-05-448.5 8.5 1
Vinyl chloride <1.7 ug/kg 12/08/15 20:29 75-01-49.7 1.7 1
Xylene (Total)<3.5 ug/kg 12/08/15 20:29 1330-20-79.7 3.5 1
m&p-Xylene <3.5 ug/kg 12/08/15 20:29 179601-23-19.7 3.5 1
o-Xylene <1.8 ug/kg 12/08/15 20:29 95-47-64.8 1.8 1
Surrogates
Toluene-d8 (S)100 %12/08/15 20:29 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %12/08/15 20:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %12/08/15 20:29 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 3.8 %12/08/15 11:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-26 Lab ID:92278649003 Collected:11/30/15 12:10 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<10.6 mg/kg 12/12/15 01:36 N212/10/15 10:1210.6 10.6 1
Aliphatic (C19-C36)<10.6 mg/kg 12/12/15 01:36 N212/10/15 10:1210.6 10.6 1
Aromatic (C11-C22)<10.6 mg/kg 12/15/15 02:33 N212/10/15 10:1210.6 10.6 1
Surrogates
Nonatriacontane (S)80 %12/12/15 01:36 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)77 %12/15/15 02:33 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)94 %12/15/15 02:33 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)90 %12/15/15 02:33 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<3.0 mg/kg 12/16/15 16:41 N212/16/15 14:153.0 3.0 1
Aliphatic (C09-C12)<3.0 mg/kg 12/16/15 16:41 N212/16/15 14:153.0 3.0 1
Aromatic (C09-C10)<3.0 mg/kg 12/16/15 16:41 N212/16/15 14:153.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)91 %12/16/15 16:41 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)91 %12/16/15 16:41 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <80.2 ug/kg 12/14/15 18:21 83-32-912/07/15 15:3034880.2 1
Acenaphthylene <82.3 ug/kg 12/14/15 18:21 208-96-812/07/15 15:3034882.3 1
Aniline <93.9 ug/kg 12/14/15 18:21 62-53-312/07/15 15:3034893.9 1
Anthracene <78.1 ug/kg 12/14/15 18:21 120-12-712/07/15 15:3034878.1 1
Benzo(a)anthracene <64.4 ug/kg 12/14/15 18:21 56-55-312/07/15 15:3034864.4 1
Benzo(a)pyrene <66.5 ug/kg 12/14/15 18:21 50-32-812/07/15 15:3034866.5 1
Benzo(b)fluoranthene <60.1 ug/kg 12/14/15 18:21 205-99-212/07/15 15:3034860.1 1
Benzo(g,h,i)perylene <88.6 ug/kg 12/14/15 18:21 191-24-212/07/15 15:3034888.6 1
Benzo(k)fluoranthene <68.6 ug/kg 12/14/15 18:21 207-08-912/07/15 15:3034868.6 1
Benzoic Acid <63.3 ug/kg 12/14/15 18:21 65-85-012/07/15 15:30174063.3 1
Benzyl alcohol <69.6 ug/kg 12/14/15 18:21 100-51-612/07/15 15:3069669.6 1
4-Bromophenylphenyl ether <63.3 ug/kg 12/14/15 18:21 101-55-312/07/15 15:3034863.3 1
Butylbenzylphthalate <73.9 ug/kg 12/14/15 18:21 85-68-712/07/15 15:3034873.9 1
4-Chloro-3-methylphenol <71.7 ug/kg 12/14/15 18:21 59-50-712/07/15 15:3069671.7 1
4-Chloroaniline <97.1 ug/kg 12/14/15 18:21 106-47-812/07/15 15:30174097.1 1
bis(2-Chloroethoxy)methane <81.2 ug/kg 12/14/15 18:21 111-91-112/07/15 15:3034881.2 1
bis(2-Chloroethyl) ether <88.6 ug/kg 12/14/15 18:21 111-44-412/07/15 15:3034888.6 1
bis(2-Chloroisopropyl) ether <92.9 ug/kg 12/14/15 18:21 108-60-112/07/15 15:3034892.9 1
2-Chloronaphthalene <68.6 ug/kg 12/14/15 18:21 91-58-712/07/15 15:3034868.6 1
2-Chlorophenol <95.0 ug/kg 12/14/15 18:21 95-57-812/07/15 15:3034895.0 1
4-Chlorophenylphenyl ether <71.7 ug/kg 12/14/15 18:21 7005-72-312/07/15 15:3034871.7 1
Chrysene <46.4 ug/kg 12/14/15 18:21 218-01-912/07/15 15:3034846.4 1
Dibenz(a,h)anthracene <73.9 ug/kg 12/14/15 18:21 53-70-312/07/15 15:3034873.9 1
Dibenzofuran <57.0 ug/kg 12/14/15 18:21 132-64-912/07/15 15:3034857.0 1
1,2-Dichlorobenzene <92.9 ug/kg 12/14/15 18:21 95-50-112/07/15 15:3034892.9 1
1,3-Dichlorobenzene <79.1 ug/kg 12/14/15 18:21 541-73-112/07/15 15:3034879.1 1
1,4-Dichlorobenzene <98.1 ug/kg 12/14/15 18:21 106-46-712/07/15 15:3034898.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-26 Lab ID:92278649003 Collected:11/30/15 12:10 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <76.0 ug/kg 12/14/15 18:21 91-94-112/07/15 15:30174076.0 1
2,4-Dichlorophenol <76.0 ug/kg 12/14/15 18:21 120-83-212/07/15 15:3034876.0 1
Diethylphthalate <53.8 ug/kg 12/14/15 18:21 84-66-212/07/15 15:3034853.8 1
2,4-Dimethylphenol <137 ug/kg 12/14/15 18:21 105-67-912/07/15 15:303481371
Dimethylphthalate <70.7 ug/kg 12/14/15 18:21 131-11-312/07/15 15:3034870.7 1
Di-n-butylphthalate <57.0 ug/kg 12/14/15 18:21 84-74-212/07/15 15:3034857.0 1
4,6-Dinitro-2-methylphenol <69.6 ug/kg 12/14/15 18:21 534-52-112/07/15 15:3069669.6 1
2,4-Dinitrophenol <57.0 ug/kg 12/14/15 18:21 51-28-512/07/15 15:30174057.0 1
2,4-Dinitrotoluene <65.4 ug/kg 12/14/15 18:21 121-14-212/07/15 15:3034865.4 1
2,6-Dinitrotoluene <72.8 ug/kg 12/14/15 18:21 606-20-212/07/15 15:3034872.8 1
Di-n-octylphthalate <72.8 ug/kg 12/14/15 18:21 117-84-012/07/15 15:3034872.8 1
bis(2-Ethylhexyl)phthalate <95.0 ug/kg 12/14/15 18:21 117-81-712/07/15 15:3034895.0 1
Fluoranthene <50.6 ug/kg 12/14/15 18:21 206-44-012/07/15 15:3034850.6 1
Fluorene <71.7 ug/kg 12/14/15 18:21 86-73-712/07/15 15:3034871.7 1
Hexachloro-1,3-butadiene <60.1 ug/kg 12/14/15 18:21 87-68-312/07/15 15:3034860.1 1
Hexachlorobenzene <44.3 ug/kg 12/14/15 18:21 118-74-112/07/15 15:3034844.3 1
Hexachlorocyclopentadiene <64.4 ug/kg 12/14/15 18:21 77-47-412/07/15 15:3034864.4 1
Hexachloroethane <91.8 ug/kg 12/14/15 18:21 67-72-112/07/15 15:3034891.8 1
Indeno(1,2,3-cd)pyrene <71.7 ug/kg 12/14/15 18:21 193-39-512/07/15 15:3034871.7 1
Isophorone <78.1 ug/kg 12/14/15 18:21 78-59-112/07/15 15:3034878.1 1
1-Methylnaphthalene <90.7 ug/kg 12/14/15 18:21 90-12-012/07/15 15:3034890.7 1
2-Methylnaphthalene <74.9 ug/kg 12/14/15 18:21 91-57-612/07/15 15:3034874.9 1
2-Methylphenol(o-Cresol)<106 ug/kg 12/14/15 18:21 95-48-712/07/15 15:303481061
3&4-Methylphenol(m&p Cresol)<137 ug/kg 12/14/15 18:2112/07/15 15:303481371
Naphthalene <85.5 ug/kg 12/14/15 18:21 91-20-312/07/15 15:3034885.5 1
2-Nitroaniline <108 ug/kg 12/14/15 18:21 88-74-412/07/15 15:3017401081
3-Nitroaniline <95.0 ug/kg 12/14/15 18:21 99-09-212/07/15 15:30174095.0 1
4-Nitroaniline <98.1 ug/kg 12/14/15 18:21 100-01-612/07/15 15:3069698.1 1
Nitrobenzene <95.0 ug/kg 12/14/15 18:21 98-95-312/07/15 15:3034895.0 1
2-Nitrophenol <84.4 ug/kg 12/14/15 18:21 88-75-512/07/15 15:3034884.4 1
4-Nitrophenol <62.3 ug/kg 12/14/15 18:21 100-02-712/07/15 15:30174062.3 1
N-Nitrosodimethylamine <113 ug/kg 12/14/15 18:21 62-75-912/07/15 15:303481131
N-Nitroso-di-n-propylamine <66.5 ug/kg 12/14/15 18:21 621-64-712/07/15 15:3034866.5 1
N-Nitrosodiphenylamine <103 ug/kg 12/14/15 18:21 86-30-612/07/15 15:303481031
Pentachlorophenol <63.3 ug/kg 12/14/15 18:21 87-86-512/07/15 15:30174063.3 1
Phenanthrene <58.0 ug/kg 12/14/15 18:21 85-01-812/07/15 15:3034858.0 1
Phenol <104 ug/kg 12/14/15 18:21 108-95-212/07/15 15:303481041
Pyrene <59.1 ug/kg 12/14/15 18:21 129-00-012/07/15 15:3034859.1 1
1,2,4-Trichlorobenzene <67.5 ug/kg 12/14/15 18:21 120-82-112/07/15 15:3034867.5 1
2,4,5-Trichlorophenol <108 ug/kg 12/14/15 18:21 95-95-412/07/15 15:303481081
2,4,6-Trichlorophenol <77.0 ug/kg 12/14/15 18:21 88-06-212/07/15 15:3034877.0 1
Surrogates
Nitrobenzene-d5 (S)83 %12/14/15 18:21 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)83 %12/14/15 18:21 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)93 %12/14/15 18:21 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-26 Lab ID:92278649003 Collected:11/30/15 12:10 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)75 %12/14/15 18:21 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)74 %12/14/15 18:21 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)84 %12/14/15 18:21 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 13.1J ug/kg 12/08/15 20:49 67-64-111011.0 1
Benzene <1.8 ug/kg 12/08/15 20:49 71-43-25.5 1.8 1
Bromobenzene <2.2 ug/kg 12/08/15 20:49 108-86-15.5 2.2 1
Bromochloromethane <1.9 ug/kg 12/08/15 20:49 74-97-55.5 1.9 1
Bromodichloromethane <2.1 ug/kg 12/08/15 20:49 75-27-45.5 2.1 1
Bromoform <2.5 ug/kg 12/08/15 20:49 75-25-25.5 2.5 1
Bromomethane <2.7 ug/kg 12/08/15 20:49 74-83-911.0 2.7 1
2-Butanone (MEK)<3.2 ug/kg 12/08/15 20:49 78-93-31103.2 1
n-Butylbenzene <2.0 ug/kg 12/08/15 20:49 104-51-85.5 2.0 1
sec-Butylbenzene <1.8 ug/kg 12/08/15 20:49 135-98-85.5 1.8 1
tert-Butylbenzene <2.2 ug/kg 12/08/15 20:49 98-06-65.5 2.2 1
Carbon tetrachloride <2.9 ug/kg 12/08/15 20:49 56-23-55.5 2.9 1
Chlorobenzene <2.1 ug/kg 12/08/15 20:49 108-90-75.5 2.1 1
Chloroethane <2.6 ug/kg 12/08/15 20:49 75-00-311.0 2.6 1
Chloroform <1.8 ug/kg 12/08/15 20:49 67-66-35.5 1.8 1
Chloromethane <2.6 ug/kg 12/08/15 20:49 74-87-311.0 2.6 1
2-Chlorotoluene <1.9 ug/kg 12/08/15 20:49 95-49-85.5 1.9 1
4-Chlorotoluene <2.0 ug/kg 12/08/15 20:49 106-43-45.5 2.0 1
1,2-Dibromo-3-chloropropane <3.9 ug/kg 12/08/15 20:49 96-12-85.5 3.9 1
Dibromochloromethane <2.0 ug/kg 12/08/15 20:49 124-48-15.5 2.0 1
1,2-Dibromoethane (EDB)<2.0 ug/kg 12/08/15 20:49 106-93-45.5 2.0 1
Dibromomethane <2.7 ug/kg 12/08/15 20:49 74-95-35.5 2.7 1
1,2-Dichlorobenzene <2.1 ug/kg 12/08/15 20:49 95-50-15.5 2.1 1
1,3-Dichlorobenzene <2.2 ug/kg 12/08/15 20:49 541-73-15.5 2.2 1
1,4-Dichlorobenzene <1.9 ug/kg 12/08/15 20:49 106-46-75.5 1.9 1
Dichlorodifluoromethane <3.9 ug/kg 12/08/15 20:49 75-71-811.0 3.9 1
1,1-Dichloroethane <1.6 ug/kg 12/08/15 20:49 75-34-35.5 1.6 1
1,2-Dichloroethane <2.4 ug/kg 12/08/15 20:49 107-06-25.5 2.4 1
1,1-Dichloroethene <2.0 ug/kg 12/08/15 20:49 75-35-45.5 2.0 1
cis-1,2-Dichloroethene <1.5 ug/kg 12/08/15 20:49 156-59-25.5 1.5 1
trans-1,2-Dichloroethene <2.1 ug/kg 12/08/15 20:49 156-60-55.5 2.1 1
1,2-Dichloropropane <1.9 ug/kg 12/08/15 20:49 78-87-55.5 1.9 1
1,3-Dichloropropane <2.1 ug/kg 12/08/15 20:49 142-28-95.5 2.1 1
2,2-Dichloropropane <1.9 ug/kg 12/08/15 20:49 594-20-75.5 1.9 1
1,1-Dichloropropene <1.6 ug/kg 12/08/15 20:49 563-58-65.5 1.6 1
cis-1,3-Dichloropropene <2.0 ug/kg 12/08/15 20:49 10061-01-55.5 2.0 1
trans-1,3-Dichloropropene <1.6 ug/kg 12/08/15 20:49 10061-02-65.5 1.6 1
Diisopropyl ether <1.9 ug/kg 12/08/15 20:49 108-20-35.5 1.9 1
Ethylbenzene <2.0 ug/kg 12/08/15 20:49 100-41-45.5 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-26 Lab ID:92278649003 Collected:11/30/15 12:10 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.2 ug/kg 12/08/15 20:49 87-68-35.5 2.2 1
2-Hexanone <4.3 ug/kg 12/08/15 20:49 591-78-654.8 4.3 1
Isopropylbenzene (Cumene)<2.1 ug/kg 12/08/15 20:49 98-82-85.5 2.1 1
p-Isopropyltoluene <1.9 ug/kg 12/08/15 20:49 99-87-65.5 1.9 1
Methylene Chloride <3.3 ug/kg 12/08/15 20:49 75-09-221.9 3.3 1
4-Methyl-2-pentanone (MIBK)<4.1 ug/kg 12/08/15 20:49 108-10-154.8 4.1 1
Methyl-tert-butyl ether <1.6 ug/kg 12/08/15 20:49 1634-04-45.5 1.6 1
Naphthalene <1.3 ug/kg 12/08/15 20:49 91-20-35.5 1.3 1
n-Propylbenzene <1.9 ug/kg 12/08/15 20:49 103-65-15.5 1.9 1
Styrene <2.0 ug/kg 12/08/15 20:49 100-42-55.5 2.0 1
1,1,1,2-Tetrachloroethane <2.3 ug/kg 12/08/15 20:49 630-20-65.5 2.3 1
1,1,2,2-Tetrachloroethane <2.1 ug/kg 12/08/15 20:49 79-34-55.5 2.1 1
Tetrachloroethene <1.9 ug/kg 12/08/15 20:49 127-18-45.5 1.9 1
Toluene <2.0 ug/kg 12/08/15 20:49 108-88-35.5 2.0 1
1,2,3-Trichlorobenzene <2.4 ug/kg 12/08/15 20:49 87-61-65.5 2.4 1
1,2,4-Trichlorobenzene <1.8 ug/kg 12/08/15 20:49 120-82-15.5 1.8 1
1,1,1-Trichloroethane <2.0 ug/kg 12/08/15 20:49 71-55-65.5 2.0 1
1,1,2-Trichloroethane <2.3 ug/kg 12/08/15 20:49 79-00-55.5 2.3 1
Trichloroethene <2.3 ug/kg 12/08/15 20:49 79-01-65.5 2.3 1
Trichlorofluoromethane <2.4 ug/kg 12/08/15 20:49 75-69-45.5 2.4 1
1,2,3-Trichloropropane <1.8 ug/kg 12/08/15 20:49 96-18-45.5 1.8 1
1,2,4-Trimethylbenzene <2.2 ug/kg 12/08/15 20:49 95-63-65.5 2.2 1
1,3,5-Trimethylbenzene <2.0 ug/kg 12/08/15 20:49 108-67-85.5 2.0 1
Vinyl acetate <9.7 ug/kg 12/08/15 20:49 108-05-454.8 9.7 1
Vinyl chloride <2.0 ug/kg 12/08/15 20:49 75-01-411.0 2.0 1
Xylene (Total)<3.9 ug/kg 12/08/15 20:49 1330-20-711.0 3.9 1
m&p-Xylene <3.9 ug/kg 12/08/15 20:49 179601-23-111.0 3.9 1
o-Xylene <2.1 ug/kg 12/08/15 20:49 95-47-65.5 2.1 1
Surrogates
Toluene-d8 (S)98 %12/08/15 20:49 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %12/08/15 20:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %12/08/15 20:49 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 5.2 %12/08/15 11:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-30 Lab ID:92278649004 Collected:11/30/15 12:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<13.9 mg/kg 12/12/15 02:03 N212/10/15 10:1213.9 13.9 1
Aliphatic (C19-C36)<13.9 mg/kg 12/12/15 02:03 N212/10/15 10:1213.9 13.9 1
Aromatic (C11-C22)32.0 mg/kg 12/15/15 03:00 N212/10/15 10:1213.9 13.9 1
Surrogates
Nonatriacontane (S)73 %12/12/15 02:03 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)68 %12/15/15 03:00 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)98 %12/15/15 03:00 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)97 %12/15/15 03:00 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<4.4 mg/kg 12/16/15 17:11 N212/16/15 14:154.4 4.4 1
Aliphatic (C09-C12)<4.4 mg/kg 12/16/15 17:11 N212/16/15 14:154.4 4.4 1
Aromatic (C09-C10)<4.4 mg/kg 12/16/15 17:11 N212/16/15 14:154.4 4.4 1
Surrogates
4-Bromofluorobenzene (FID) (S)91 %12/16/15 17:11 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)90 %12/16/15 17:11 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <105 ug/kg 12/14/15 05:02 83-32-912/07/15 15:304581051
Acenaphthylene <108 ug/kg 12/14/15 05:02 208-96-812/07/15 15:304581081
Aniline <123 ug/kg 12/14/15 05:02 62-53-312/07/15 15:304581231
Anthracene <103 ug/kg 12/14/15 05:02 120-12-712/07/15 15:304581031
Benzo(a)anthracene 110J ug/kg 12/14/15 05:02 56-55-312/07/15 15:3045884.6 1
Benzo(a)pyrene 90.0J ug/kg 12/14/15 05:02 50-32-812/07/15 15:3045887.4 1
Benzo(b)fluoranthene 115J ug/kg 12/14/15 05:02 205-99-212/07/15 15:3045879.1 1
Benzo(g,h,i)perylene <117 ug/kg 12/14/15 05:02 191-24-212/07/15 15:304581171
Benzo(k)fluoranthene <90.2 ug/kg 12/14/15 05:02 207-08-912/07/15 15:3045890.2 1
Benzoic Acid <83.2 ug/kg 12/14/15 05:02 65-85-012/07/15 15:30229083.2 1
Benzyl alcohol <91.5 ug/kg 12/14/15 05:02 100-51-612/07/15 15:3091591.5 1
4-Bromophenylphenyl ether <83.2 ug/kg 12/14/15 05:02 101-55-312/07/15 15:3045883.2 1
Butylbenzylphthalate <97.1 ug/kg 12/14/15 05:02 85-68-712/07/15 15:3045897.1 1
4-Chloro-3-methylphenol <94.3 ug/kg 12/14/15 05:02 59-50-712/07/15 15:3091594.3 1
4-Chloroaniline <128 ug/kg 12/14/15 05:02 106-47-812/07/15 15:3022901281
bis(2-Chloroethoxy)methane <107 ug/kg 12/14/15 05:02 111-91-112/07/15 15:304581071
bis(2-Chloroethyl) ether <117 ug/kg 12/14/15 05:02 111-44-412/07/15 15:304581171
bis(2-Chloroisopropyl) ether <122 ug/kg 12/14/15 05:02 108-60-112/07/15 15:304581221
2-Chloronaphthalene <90.2 ug/kg 12/14/15 05:02 91-58-712/07/15 15:3045890.2 1
2-Chlorophenol <125 ug/kg 12/14/15 05:02 95-57-812/07/15 15:304581251
4-Chlorophenylphenyl ether <94.3 ug/kg 12/14/15 05:02 7005-72-312/07/15 15:3045894.3 1
Chrysene 117J ug/kg 12/14/15 05:02 218-01-912/07/15 15:3045861.0 1
Dibenz(a,h)anthracene <97.1 ug/kg 12/14/15 05:02 53-70-312/07/15 15:3045897.1 1
Dibenzofuran <74.9 ug/kg 12/14/15 05:02 132-64-912/07/15 15:3045874.9 1
1,2-Dichlorobenzene <122 ug/kg 12/14/15 05:02 95-50-112/07/15 15:304581221
1,3-Dichlorobenzene <104 ug/kg 12/14/15 05:02 541-73-112/07/15 15:304581041
1,4-Dichlorobenzene <129 ug/kg 12/14/15 05:02 106-46-712/07/15 15:304581291
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-30 Lab ID:92278649004 Collected:11/30/15 12:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <99.9 ug/kg 12/14/15 05:02 91-94-112/07/15 15:30229099.9 1
2,4-Dichlorophenol <99.9 ug/kg 12/14/15 05:02 120-83-212/07/15 15:3045899.9 1
Diethylphthalate <70.7 ug/kg 12/14/15 05:02 84-66-212/07/15 15:3045870.7 1
2,4-Dimethylphenol <180 ug/kg 12/14/15 05:02 105-67-912/07/15 15:304581801
Dimethylphthalate <92.9 ug/kg 12/14/15 05:02 131-11-312/07/15 15:3045892.9 1
Di-n-butylphthalate <74.9 ug/kg 12/14/15 05:02 84-74-212/07/15 15:3045874.9 1
4,6-Dinitro-2-methylphenol <91.5 ug/kg 12/14/15 05:02 534-52-112/07/15 15:3091591.5 1
2,4-Dinitrophenol <74.9 ug/kg 12/14/15 05:02 51-28-512/07/15 15:30229074.9 1
2,4-Dinitrotoluene <86.0 ug/kg 12/14/15 05:02 121-14-212/07/15 15:3045886.0 1
2,6-Dinitrotoluene <95.7 ug/kg 12/14/15 05:02 606-20-212/07/15 15:3045895.7 1
Di-n-octylphthalate <95.7 ug/kg 12/14/15 05:02 117-84-012/07/15 15:3045895.7 1
bis(2-Ethylhexyl)phthalate <125 ug/kg 12/14/15 05:02 117-81-712/07/15 15:304581251
Fluoranthene 343J ug/kg 12/14/15 05:02 206-44-012/07/15 15:3045866.6 1
Fluorene <94.3 ug/kg 12/14/15 05:02 86-73-712/07/15 15:3045894.3 1
Hexachloro-1,3-butadiene <79.1 ug/kg 12/14/15 05:02 87-68-312/07/15 15:3045879.1 1
Hexachlorobenzene <58.3 ug/kg 12/14/15 05:02 118-74-112/07/15 15:3045858.3 1
Hexachlorocyclopentadiene <84.6 ug/kg 12/14/15 05:02 77-47-412/07/15 15:3045884.6 1
Hexachloroethane <121 ug/kg 12/14/15 05:02 67-72-112/07/15 15:304581211
Indeno(1,2,3-cd)pyrene <94.3 ug/kg 12/14/15 05:02 193-39-512/07/15 15:3045894.3 1
Isophorone <103 ug/kg 12/14/15 05:02 78-59-112/07/15 15:304581031
1-Methylnaphthalene <119 ug/kg 12/14/15 05:02 90-12-012/07/15 15:304581191
2-Methylnaphthalene <98.5 ug/kg 12/14/15 05:02 91-57-612/07/15 15:3045898.5 1
2-Methylphenol(o-Cresol)<139 ug/kg 12/14/15 05:02 95-48-712/07/15 15:304581391
3&4-Methylphenol(m&p Cresol)<180 ug/kg 12/14/15 05:0212/07/15 15:304581801
Naphthalene <112 ug/kg 12/14/15 05:02 91-20-312/07/15 15:304581121
2-Nitroaniline <141 ug/kg 12/14/15 05:02 88-74-412/07/15 15:3022901411
3-Nitroaniline <125 ug/kg 12/14/15 05:02 99-09-212/07/15 15:3022901251
4-Nitroaniline <129 ug/kg 12/14/15 05:02 100-01-612/07/15 15:309151291
Nitrobenzene <125 ug/kg 12/14/15 05:02 98-95-312/07/15 15:304581251
2-Nitrophenol <111 ug/kg 12/14/15 05:02 88-75-512/07/15 15:304581111
4-Nitrophenol <81.8 ug/kg 12/14/15 05:02 100-02-712/07/15 15:30229081.8 1
N-Nitrosodimethylamine <148 ug/kg 12/14/15 05:02 62-75-912/07/15 15:304581481
N-Nitroso-di-n-propylamine <87.4 ug/kg 12/14/15 05:02 621-64-712/07/15 15:3045887.4 1
N-Nitrosodiphenylamine <136 ug/kg 12/14/15 05:02 86-30-612/07/15 15:304581361
Pentachlorophenol <83.2 ug/kg 12/14/15 05:02 87-86-512/07/15 15:30229083.2 1
Phenanthrene 175J ug/kg 12/14/15 05:02 85-01-812/07/15 15:3045876.3 1
Phenol <137 ug/kg 12/14/15 05:02 108-95-212/07/15 15:304581371
Pyrene 296J ug/kg 12/14/15 05:02 129-00-012/07/15 15:3045877.7 1
1,2,4-Trichlorobenzene <88.8 ug/kg 12/14/15 05:02 120-82-112/07/15 15:3045888.8 1
2,4,5-Trichlorophenol <141 ug/kg 12/14/15 05:02 95-95-412/07/15 15:304581411
2,4,6-Trichlorophenol <101 ug/kg 12/14/15 05:02 88-06-212/07/15 15:304581011
Surrogates
Nitrobenzene-d5 (S)85 %12/14/15 05:02 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)82 %12/14/15 05:02 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)89 %12/14/15 05:02 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-30 Lab ID:92278649004 Collected:11/30/15 12:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)79 %12/14/15 05:02 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)76 %12/14/15 05:02 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)90 %12/14/15 05:02 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 24.9J ug/kg 12/08/15 21:09 67-64-113313.3 1
Benzene <2.1 ug/kg 12/08/15 21:09 71-43-26.6 2.1 1
Bromobenzene <2.7 ug/kg 12/08/15 21:09 108-86-16.6 2.7 1
Bromochloromethane <2.3 ug/kg 12/08/15 21:09 74-97-56.6 2.3 1
Bromodichloromethane <2.5 ug/kg 12/08/15 21:09 75-27-46.6 2.5 1
Bromoform <3.1 ug/kg 12/08/15 21:09 75-25-26.6 3.1 1
Bromomethane <3.3 ug/kg 12/08/15 21:09 74-83-913.3 3.3 1
2-Butanone (MEK)<3.9 ug/kg 12/08/15 21:09 78-93-31333.9 1
n-Butylbenzene <2.4 ug/kg 12/08/15 21:09 104-51-86.6 2.4 1
sec-Butylbenzene <2.1 ug/kg 12/08/15 21:09 135-98-86.6 2.1 1
tert-Butylbenzene <2.7 ug/kg 12/08/15 21:09 98-06-66.6 2.7 1
Carbon tetrachloride <3.5 ug/kg 12/08/15 21:09 56-23-56.6 3.5 1
Chlorobenzene <2.5 ug/kg 12/08/15 21:09 108-90-76.6 2.5 1
Chloroethane <3.2 ug/kg 12/08/15 21:09 75-00-313.3 3.2 1
Chloroform <2.1 ug/kg 12/08/15 21:09 67-66-36.6 2.1 1
Chloromethane <3.2 ug/kg 12/08/15 21:09 74-87-313.3 3.2 1
2-Chlorotoluene <2.3 ug/kg 12/08/15 21:09 95-49-86.6 2.3 1
4-Chlorotoluene <2.4 ug/kg 12/08/15 21:09 106-43-46.6 2.4 1
1,2-Dibromo-3-chloropropane <4.8 ug/kg 12/08/15 21:09 96-12-86.6 4.8 1
Dibromochloromethane <2.4 ug/kg 12/08/15 21:09 124-48-16.6 2.4 1
1,2-Dibromoethane (EDB)<2.4 ug/kg 12/08/15 21:09 106-93-46.6 2.4 1
Dibromomethane <3.3 ug/kg 12/08/15 21:09 74-95-36.6 3.3 1
1,2-Dichlorobenzene <2.5 ug/kg 12/08/15 21:09 95-50-16.6 2.5 1
1,3-Dichlorobenzene <2.7 ug/kg 12/08/15 21:09 541-73-16.6 2.7 1
1,4-Dichlorobenzene <2.3 ug/kg 12/08/15 21:09 106-46-76.6 2.3 1
Dichlorodifluoromethane <4.8 ug/kg 12/08/15 21:09 75-71-813.3 4.8 1
1,1-Dichloroethane <2.0 ug/kg 12/08/15 21:09 75-34-36.6 2.0 1
1,2-Dichloroethane <2.9 ug/kg 12/08/15 21:09 107-06-26.6 2.9 1
1,1-Dichloroethene <2.4 ug/kg 12/08/15 21:09 75-35-46.6 2.4 1
cis-1,2-Dichloroethene <1.9 ug/kg 12/08/15 21:09 156-59-26.6 1.9 1
trans-1,2-Dichloroethene <2.5 ug/kg 12/08/15 21:09 156-60-56.6 2.5 1
1,2-Dichloropropane <2.3 ug/kg 12/08/15 21:09 78-87-56.6 2.3 1
1,3-Dichloropropane <2.5 ug/kg 12/08/15 21:09 142-28-96.6 2.5 1
2,2-Dichloropropane <2.3 ug/kg 12/08/15 21:09 594-20-76.6 2.3 1
1,1-Dichloropropene <2.0 ug/kg 12/08/15 21:09 563-58-66.6 2.0 1
cis-1,3-Dichloropropene <2.4 ug/kg 12/08/15 21:09 10061-01-56.6 2.4 1
trans-1,3-Dichloropropene <2.0 ug/kg 12/08/15 21:09 10061-02-66.6 2.0 1
Diisopropyl ether <2.3 ug/kg 12/08/15 21:09 108-20-36.6 2.3 1
Ethylbenzene <2.4 ug/kg 12/08/15 21:09 100-41-46.6 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-30 Lab ID:92278649004 Collected:11/30/15 12:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.7 ug/kg 12/08/15 21:09 87-68-36.6 2.7 1
2-Hexanone <5.2 ug/kg 12/08/15 21:09 591-78-666.4 5.2 1
Isopropylbenzene (Cumene)<2.5 ug/kg 12/08/15 21:09 98-82-86.6 2.5 1
p-Isopropyltoluene <2.3 ug/kg 12/08/15 21:09 99-87-66.6 2.3 1
Methylene Chloride 12.8J ug/kg 12/08/15 21:09 75-09-226.6 4.0 1
4-Methyl-2-pentanone (MIBK)<4.9 ug/kg 12/08/15 21:09 108-10-166.4 4.9 1
Methyl-tert-butyl ether <2.0 ug/kg 12/08/15 21:09 1634-04-46.6 2.0 1
Naphthalene <1.6 ug/kg 12/08/15 21:09 91-20-36.6 1.6 1
n-Propylbenzene <2.3 ug/kg 12/08/15 21:09 103-65-16.6 2.3 1
Styrene <2.4 ug/kg 12/08/15 21:09 100-42-56.6 2.4 1
1,1,1,2-Tetrachloroethane <2.8 ug/kg 12/08/15 21:09 630-20-66.6 2.8 1
1,1,2,2-Tetrachloroethane <2.5 ug/kg 12/08/15 21:09 79-34-56.6 2.5 1
Tetrachloroethene <2.3 ug/kg 12/08/15 21:09 127-18-46.6 2.3 1
Toluene <2.4 ug/kg 12/08/15 21:09 108-88-36.6 2.4 1
1,2,3-Trichlorobenzene <2.9 ug/kg 12/08/15 21:09 87-61-66.6 2.9 1
1,2,4-Trichlorobenzene <2.1 ug/kg 12/08/15 21:09 120-82-16.6 2.1 1
1,1,1-Trichloroethane <2.4 ug/kg 12/08/15 21:09 71-55-66.6 2.4 1
1,1,2-Trichloroethane <2.8 ug/kg 12/08/15 21:09 79-00-56.6 2.8 1
Trichloroethene <2.8 ug/kg 12/08/15 21:09 79-01-66.6 2.8 1
Trichlorofluoromethane <2.9 ug/kg 12/08/15 21:09 75-69-46.6 2.9 1
1,2,3-Trichloropropane <2.1 ug/kg 12/08/15 21:09 96-18-46.6 2.1 1
1,2,4-Trimethylbenzene <2.7 ug/kg 12/08/15 21:09 95-63-66.6 2.7 1
1,3,5-Trimethylbenzene <2.4 ug/kg 12/08/15 21:09 108-67-86.6 2.4 1
Vinyl acetate <11.7 ug/kg 12/08/15 21:09 108-05-466.4 11.7 1
Vinyl chloride <2.4 ug/kg 12/08/15 21:09 75-01-413.3 2.4 1
Xylene (Total)<4.8 ug/kg 12/08/15 21:09 1330-20-713.3 4.8 1
m&p-Xylene <4.8 ug/kg 12/08/15 21:09 179601-23-113.3 4.8 1
o-Xylene <2.5 ug/kg 12/08/15 21:09 95-47-66.6 2.5 1
Surrogates
Toluene-d8 (S)97 %12/08/15 21:09 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %12/08/15 21:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %12/08/15 21:09 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.9 %12/08/15 11:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-25 Lab ID:92278649005 Collected:11/30/15 13:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<13.1 mg/kg 12/12/15 02:30 N212/10/15 10:1213.1 13.1 1
Aliphatic (C19-C36)<13.1 mg/kg 12/12/15 02:30 N212/10/15 10:1213.1 13.1 1
Aromatic (C11-C22)<13.1 mg/kg 12/15/15 03:28 N212/10/15 10:1213.1 13.1 1
Surrogates
Nonatriacontane (S)70 %12/12/15 02:30 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)49 %12/15/15 03:28 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)86 %12/15/15 03:28 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)83 %12/15/15 03:28 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<4.1 mg/kg 12/16/15 17:41 N212/16/15 14:154.1 4.1 1
Aliphatic (C09-C12)<4.1 mg/kg 12/16/15 17:41 N212/16/15 14:154.1 4.1 1
Aromatic (C09-C10)<4.1 mg/kg 12/16/15 17:41 N212/16/15 14:154.1 4.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)93 %12/16/15 17:41 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)92 %12/16/15 17:41 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <99.3 ug/kg 12/14/15 19:44 83-32-912/07/15 15:3043199.3 1
Acenaphthylene <102 ug/kg 12/14/15 19:44 208-96-812/07/15 15:304311021
Aniline <116 ug/kg 12/14/15 19:44 62-53-312/07/15 15:304311161
Anthracene <96.7 ug/kg 12/14/15 19:44 120-12-712/07/15 15:3043196.7 1
Benzo(a)anthracene <79.7 ug/kg 12/14/15 19:44 56-55-312/07/15 15:3043179.7 1
Benzo(a)pyrene <82.3 ug/kg 12/14/15 19:44 50-32-812/07/15 15:3043182.3 1
Benzo(b)fluoranthene <74.5 ug/kg 12/14/15 19:44 205-99-212/07/15 15:3043174.5 1
Benzo(g,h,i)perylene <110 ug/kg 12/14/15 19:44 191-24-212/07/15 15:304311101
Benzo(k)fluoranthene <84.9 ug/kg 12/14/15 19:44 207-08-912/07/15 15:3043184.9 1
Benzoic Acid <78.4 ug/kg 12/14/15 19:44 65-85-012/07/15 15:30216078.4 1
Benzyl alcohol <86.2 ug/kg 12/14/15 19:44 100-51-612/07/15 15:3086286.2 1
4-Bromophenylphenyl ether <78.4 ug/kg 12/14/15 19:44 101-55-312/07/15 15:3043178.4 1
Butylbenzylphthalate <91.5 ug/kg 12/14/15 19:44 85-68-712/07/15 15:3043191.5 1
4-Chloro-3-methylphenol <88.8 ug/kg 12/14/15 19:44 59-50-712/07/15 15:3086288.8 1
4-Chloroaniline <120 ug/kg 12/14/15 19:44 106-47-812/07/15 15:3021601201
bis(2-Chloroethoxy)methane <101 ug/kg 12/14/15 19:44 111-91-112/07/15 15:304311011
bis(2-Chloroethyl) ether <110 ug/kg 12/14/15 19:44 111-44-412/07/15 15:304311101
bis(2-Chloroisopropyl) ether <115 ug/kg 12/14/15 19:44 108-60-112/07/15 15:304311151
2-Chloronaphthalene <84.9 ug/kg 12/14/15 19:44 91-58-712/07/15 15:3043184.9 1
2-Chlorophenol <118 ug/kg 12/14/15 19:44 95-57-812/07/15 15:304311181
4-Chlorophenylphenyl ether <88.8 ug/kg 12/14/15 19:44 7005-72-312/07/15 15:3043188.8 1
Chrysene <57.5 ug/kg 12/14/15 19:44 218-01-912/07/15 15:3043157.5 1
Dibenz(a,h)anthracene <91.5 ug/kg 12/14/15 19:44 53-70-312/07/15 15:3043191.5 1
Dibenzofuran <70.6 ug/kg 12/14/15 19:44 132-64-912/07/15 15:3043170.6 1
1,2-Dichlorobenzene <115 ug/kg 12/14/15 19:44 95-50-112/07/15 15:304311151
1,3-Dichlorobenzene <98.0 ug/kg 12/14/15 19:44 541-73-112/07/15 15:3043198.0 1
1,4-Dichlorobenzene <122 ug/kg 12/14/15 19:44 106-46-712/07/15 15:304311221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-25 Lab ID:92278649005 Collected:11/30/15 13:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <94.1 ug/kg 12/14/15 19:44 91-94-112/07/15 15:30216094.1 1
2,4-Dichlorophenol <94.1 ug/kg 12/14/15 19:44 120-83-212/07/15 15:3043194.1 1
Diethylphthalate <66.6 ug/kg 12/14/15 19:44 84-66-212/07/15 15:3043166.6 1
2,4-Dimethylphenol <170 ug/kg 12/14/15 19:44 105-67-912/07/15 15:304311701
Dimethylphthalate <87.5 ug/kg 12/14/15 19:44 131-11-312/07/15 15:3043187.5 1
Di-n-butylphthalate <70.6 ug/kg 12/14/15 19:44 84-74-212/07/15 15:3043170.6 1
4,6-Dinitro-2-methylphenol <86.2 ug/kg 12/14/15 19:44 534-52-112/07/15 15:3086286.2 1
2,4-Dinitrophenol <70.6 ug/kg 12/14/15 19:44 51-28-512/07/15 15:30216070.6 1
2,4-Dinitrotoluene <81.0 ug/kg 12/14/15 19:44 121-14-212/07/15 15:3043181.0 1
2,6-Dinitrotoluene <90.2 ug/kg 12/14/15 19:44 606-20-212/07/15 15:3043190.2 1
Di-n-octylphthalate <90.2 ug/kg 12/14/15 19:44 117-84-012/07/15 15:3043190.2 1
bis(2-Ethylhexyl)phthalate <118 ug/kg 12/14/15 19:44 117-81-712/07/15 15:304311181
Fluoranthene <62.7 ug/kg 12/14/15 19:44 206-44-012/07/15 15:3043162.7 1
Fluorene <88.8 ug/kg 12/14/15 19:44 86-73-712/07/15 15:3043188.8 1
Hexachloro-1,3-butadiene <74.5 ug/kg 12/14/15 19:44 87-68-312/07/15 15:3043174.5 1
Hexachlorobenzene <54.9 ug/kg 12/14/15 19:44 118-74-112/07/15 15:3043154.9 1
Hexachlorocyclopentadiene <79.7 ug/kg 12/14/15 19:44 77-47-412/07/15 15:3043179.7 1
Hexachloroethane <114 ug/kg 12/14/15 19:44 67-72-112/07/15 15:304311141
Indeno(1,2,3-cd)pyrene <88.8 ug/kg 12/14/15 19:44 193-39-512/07/15 15:3043188.8 1
Isophorone <96.7 ug/kg 12/14/15 19:44 78-59-112/07/15 15:3043196.7 1
1-Methylnaphthalene <112 ug/kg 12/14/15 19:44 90-12-012/07/15 15:304311121
2-Methylnaphthalene <92.8 ug/kg 12/14/15 19:44 91-57-612/07/15 15:3043192.8 1
2-Methylphenol(o-Cresol)<131 ug/kg 12/14/15 19:44 95-48-712/07/15 15:304311311
3&4-Methylphenol(m&p Cresol)<170 ug/kg 12/14/15 19:4412/07/15 15:304311701
Naphthalene <106 ug/kg 12/14/15 19:44 91-20-312/07/15 15:304311061
2-Nitroaniline <133 ug/kg 12/14/15 19:44 88-74-412/07/15 15:3021601331
3-Nitroaniline <118 ug/kg 12/14/15 19:44 99-09-212/07/15 15:3021601181
4-Nitroaniline <122 ug/kg 12/14/15 19:44 100-01-612/07/15 15:308621221
Nitrobenzene <118 ug/kg 12/14/15 19:44 98-95-312/07/15 15:304311181
2-Nitrophenol <105 ug/kg 12/14/15 19:44 88-75-512/07/15 15:304311051
4-Nitrophenol <77.1 ug/kg 12/14/15 19:44 100-02-712/07/15 15:30216077.1 1
N-Nitrosodimethylamine <140 ug/kg 12/14/15 19:44 62-75-912/07/15 15:304311401
N-Nitroso-di-n-propylamine <82.3 ug/kg 12/14/15 19:44 621-64-712/07/15 15:3043182.3 1
N-Nitrosodiphenylamine <128 ug/kg 12/14/15 19:44 86-30-612/07/15 15:304311281
Pentachlorophenol <78.4 ug/kg 12/14/15 19:44 87-86-512/07/15 15:30216078.4 1
Phenanthrene <71.9 ug/kg 12/14/15 19:44 85-01-812/07/15 15:3043171.9 1
Phenol <129 ug/kg 12/14/15 19:44 108-95-212/07/15 15:304311291
Pyrene <73.2 ug/kg 12/14/15 19:44 129-00-012/07/15 15:3043173.2 1
1,2,4-Trichlorobenzene <83.6 ug/kg 12/14/15 19:44 120-82-112/07/15 15:3043183.6 1
2,4,5-Trichlorophenol <133 ug/kg 12/14/15 19:44 95-95-412/07/15 15:304311331
2,4,6-Trichlorophenol <95.4 ug/kg 12/14/15 19:44 88-06-212/07/15 15:3043195.4 1
Surrogates
Nitrobenzene-d5 (S)88 %12/14/15 19:44 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)86 %12/14/15 19:44 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)62 %12/14/15 19:44 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-25 Lab ID:92278649005 Collected:11/30/15 13:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)74 %12/14/15 19:44 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)74 %12/14/15 19:44 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)90 %12/14/15 19:44 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 17.7J ug/kg 12/08/15 21:29 67-64-113613.6 1
Benzene <2.2 ug/kg 12/08/15 21:29 71-43-26.8 2.2 1
Bromobenzene <2.7 ug/kg 12/08/15 21:29 108-86-16.8 2.7 1
Bromochloromethane <2.3 ug/kg 12/08/15 21:29 74-97-56.8 2.3 1
Bromodichloromethane <2.6 ug/kg 12/08/15 21:29 75-27-46.8 2.6 1
Bromoform <3.1 ug/kg 12/08/15 21:29 75-25-26.8 3.1 1
Bromomethane <3.4 ug/kg 12/08/15 21:29 74-83-913.6 3.4 1
2-Butanone (MEK)<4.0 ug/kg 12/08/15 21:29 78-93-31364.0 1
n-Butylbenzene <2.5 ug/kg 12/08/15 21:29 104-51-86.8 2.5 1
sec-Butylbenzene <2.2 ug/kg 12/08/15 21:29 135-98-86.8 2.2 1
tert-Butylbenzene <2.7 ug/kg 12/08/15 21:29 98-06-66.8 2.7 1
Carbon tetrachloride <3.5 ug/kg 12/08/15 21:29 56-23-56.8 3.5 1
Chlorobenzene <2.6 ug/kg 12/08/15 21:29 108-90-76.8 2.6 1
Chloroethane <3.3 ug/kg 12/08/15 21:29 75-00-313.6 3.3 1
Chloroform <2.2 ug/kg 12/08/15 21:29 67-66-36.8 2.2 1
Chloromethane <3.3 ug/kg 12/08/15 21:29 74-87-313.6 3.3 1
2-Chlorotoluene <2.3 ug/kg 12/08/15 21:29 95-49-86.8 2.3 1
4-Chlorotoluene <2.5 ug/kg 12/08/15 21:29 106-43-46.8 2.5 1
1,2-Dibromo-3-chloropropane <4.9 ug/kg 12/08/15 21:29 96-12-86.8 4.9 1
Dibromochloromethane <2.5 ug/kg 12/08/15 21:29 124-48-16.8 2.5 1
1,2-Dibromoethane (EDB)<2.5 ug/kg 12/08/15 21:29 106-93-46.8 2.5 1
Dibromomethane <3.4 ug/kg 12/08/15 21:29 74-95-36.8 3.4 1
1,2-Dichlorobenzene <2.6 ug/kg 12/08/15 21:29 95-50-16.8 2.6 1
1,3-Dichlorobenzene <2.7 ug/kg 12/08/15 21:29 541-73-16.8 2.7 1
1,4-Dichlorobenzene <2.3 ug/kg 12/08/15 21:29 106-46-76.8 2.3 1
Dichlorodifluoromethane <4.9 ug/kg 12/08/15 21:29 75-71-813.6 4.9 1
1,1-Dichloroethane <2.0 ug/kg 12/08/15 21:29 75-34-36.8 2.0 1
1,2-Dichloroethane <3.0 ug/kg 12/08/15 21:29 107-06-26.8 3.0 1
1,1-Dichloroethene <2.5 ug/kg 12/08/15 21:29 75-35-46.8 2.5 1
cis-1,2-Dichloroethene <1.9 ug/kg 12/08/15 21:29 156-59-26.8 1.9 1
trans-1,2-Dichloroethene <2.6 ug/kg 12/08/15 21:29 156-60-56.8 2.6 1
1,2-Dichloropropane <2.3 ug/kg 12/08/15 21:29 78-87-56.8 2.3 1
1,3-Dichloropropane <2.6 ug/kg 12/08/15 21:29 142-28-96.8 2.6 1
2,2-Dichloropropane <2.3 ug/kg 12/08/15 21:29 594-20-76.8 2.3 1
1,1-Dichloropropene <2.0 ug/kg 12/08/15 21:29 563-58-66.8 2.0 1
cis-1,3-Dichloropropene <2.5 ug/kg 12/08/15 21:29 10061-01-56.8 2.5 1
trans-1,3-Dichloropropene <2.0 ug/kg 12/08/15 21:29 10061-02-66.8 2.0 1
Diisopropyl ether <2.3 ug/kg 12/08/15 21:29 108-20-36.8 2.3 1
Ethylbenzene <2.5 ug/kg 12/08/15 21:29 100-41-46.8 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SK-25 Lab ID:92278649005 Collected:11/30/15 13:45 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.7 ug/kg 12/08/15 21:29 87-68-36.8 2.7 1
2-Hexanone <5.3 ug/kg 12/08/15 21:29 591-78-668.2 5.3 1
Isopropylbenzene (Cumene)<2.6 ug/kg 12/08/15 21:29 98-82-86.8 2.6 1
p-Isopropyltoluene <2.3 ug/kg 12/08/15 21:29 99-87-66.8 2.3 1
Methylene Chloride 8.3J ug/kg 12/08/15 21:29 75-09-227.3 4.1 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/kg 12/08/15 21:29 108-10-168.2 5.0 1
Methyl-tert-butyl ether <2.0 ug/kg 12/08/15 21:29 1634-04-46.8 2.0 1
Naphthalene <1.6 ug/kg 12/08/15 21:29 91-20-36.8 1.6 1
n-Propylbenzene <2.3 ug/kg 12/08/15 21:29 103-65-16.8 2.3 1
Styrene <2.5 ug/kg 12/08/15 21:29 100-42-56.8 2.5 1
1,1,1,2-Tetrachloroethane <2.9 ug/kg 12/08/15 21:29 630-20-66.8 2.9 1
1,1,2,2-Tetrachloroethane <2.6 ug/kg 12/08/15 21:29 79-34-56.8 2.6 1
Tetrachloroethene <2.3 ug/kg 12/08/15 21:29 127-18-46.8 2.3 1
Toluene <2.5 ug/kg 12/08/15 21:29 108-88-36.8 2.5 1
1,2,3-Trichlorobenzene <3.0 ug/kg 12/08/15 21:29 87-61-66.8 3.0 1
1,2,4-Trichlorobenzene <2.2 ug/kg 12/08/15 21:29 120-82-16.8 2.2 1
1,1,1-Trichloroethane <2.5 ug/kg 12/08/15 21:29 71-55-66.8 2.5 1
1,1,2-Trichloroethane <2.9 ug/kg 12/08/15 21:29 79-00-56.8 2.9 1
Trichloroethene <2.9 ug/kg 12/08/15 21:29 79-01-66.8 2.9 1
Trichlorofluoromethane <3.0 ug/kg 12/08/15 21:29 75-69-46.8 3.0 1
1,2,3-Trichloropropane <2.2 ug/kg 12/08/15 21:29 96-18-46.8 2.2 1
1,2,4-Trimethylbenzene <2.7 ug/kg 12/08/15 21:29 95-63-66.8 2.7 1
1,3,5-Trimethylbenzene <2.5 ug/kg 12/08/15 21:29 108-67-86.8 2.5 1
Vinyl acetate <12.0 ug/kg 12/08/15 21:29 108-05-468.2 12.0 1
Vinyl chloride <2.5 ug/kg 12/08/15 21:29 75-01-413.6 2.5 1
Xylene (Total)<4.9 ug/kg 12/08/15 21:29 1330-20-713.6 4.9 1
m&p-Xylene <4.9 ug/kg 12/08/15 21:29 179601-23-113.6 4.9 1
o-Xylene <2.6 ug/kg 12/08/15 21:29 95-47-66.8 2.6 1
Surrogates
Toluene-d8 (S)100 %12/08/15 21:29 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %12/08/15 21:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %12/08/15 21:29 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.5 %12/08/15 11:240.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-10 Lab ID:92278649006 Collected:11/30/15 14:30 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)256 mg/kg 12/17/15 11:40 N212/10/15 10:121051058
Aliphatic (C19-C36)<105 mg/kg 12/17/15 11:40 N212/10/15 10:121051058
Aromatic (C11-C22)83.3 mg/kg 12/15/15 03:55 N212/10/15 10:1213.1 13.1 1
Surrogates
Nonatriacontane (S)100 %12/17/15 11:40 7194-86-712/10/15 10:1240-140 8
o-Terphenyl (S)115 %12/15/15 03:55 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)127 %12/15/15 03:55 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)177 %12/15/15 03:55 580-13-2 S512/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)10.9 mg/kg 12/16/15 18:11 N212/16/15 14:153.3 3.3 1
Aliphatic (C09-C12)62.6 mg/kg 12/16/15 18:11 N212/16/15 14:153.3 3.3 1
Aromatic (C09-C10)101 mg/kg 12/16/15 18:11 N212/16/15 14:153.3 3.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)122 %12/16/15 18:11 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)98 %12/16/15 18:11 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <99.3 ug/kg 12/14/15 20:11 83-32-912/07/15 15:3043199.3 1
Acenaphthylene <102 ug/kg 12/14/15 20:11 208-96-812/07/15 15:304311021
Aniline <116 ug/kg 12/14/15 20:11 62-53-312/07/15 15:304311161
Anthracene <96.7 ug/kg 12/14/15 20:11 120-12-712/07/15 15:3043196.7 1
Benzo(a)anthracene <79.7 ug/kg 12/14/15 20:11 56-55-312/07/15 15:3043179.7 1
Benzo(a)pyrene <82.3 ug/kg 12/14/15 20:11 50-32-812/07/15 15:3043182.3 1
Benzo(b)fluoranthene <74.5 ug/kg 12/14/15 20:11 205-99-212/07/15 15:3043174.5 1
Benzo(g,h,i)perylene <110 ug/kg 12/14/15 20:11 191-24-212/07/15 15:304311101
Benzo(k)fluoranthene <84.9 ug/kg 12/14/15 20:11 207-08-912/07/15 15:3043184.9 1
Benzoic Acid <78.4 ug/kg 12/14/15 20:11 65-85-012/07/15 15:30216078.4 1
Benzyl alcohol <86.2 ug/kg 12/14/15 20:11 100-51-612/07/15 15:3086286.2 1
4-Bromophenylphenyl ether <78.4 ug/kg 12/14/15 20:11 101-55-312/07/15 15:3043178.4 1
Butylbenzylphthalate <91.5 ug/kg 12/14/15 20:11 85-68-712/07/15 15:3043191.5 1
4-Chloro-3-methylphenol <88.9 ug/kg 12/14/15 20:11 59-50-712/07/15 15:3086288.9 1
4-Chloroaniline <120 ug/kg 12/14/15 20:11 106-47-812/07/15 15:3021601201
bis(2-Chloroethoxy)methane <101 ug/kg 12/14/15 20:11 111-91-112/07/15 15:304311011
bis(2-Chloroethyl) ether <110 ug/kg 12/14/15 20:11 111-44-412/07/15 15:304311101
bis(2-Chloroisopropyl) ether <115 ug/kg 12/14/15 20:11 108-60-112/07/15 15:304311151
2-Chloronaphthalene <84.9 ug/kg 12/14/15 20:11 91-58-712/07/15 15:3043184.9 1
2-Chlorophenol <118 ug/kg 12/14/15 20:11 95-57-812/07/15 15:304311181
4-Chlorophenylphenyl ether <88.9 ug/kg 12/14/15 20:11 7005-72-312/07/15 15:3043188.9 1
Chrysene <57.5 ug/kg 12/14/15 20:11 218-01-912/07/15 15:3043157.5 1
Dibenz(a,h)anthracene <91.5 ug/kg 12/14/15 20:11 53-70-312/07/15 15:3043191.5 1
Dibenzofuran <70.6 ug/kg 12/14/15 20:11 132-64-912/07/15 15:3043170.6 1
1,2-Dichlorobenzene <115 ug/kg 12/14/15 20:11 95-50-112/07/15 15:304311151
1,3-Dichlorobenzene <98.0 ug/kg 12/14/15 20:11 541-73-112/07/15 15:3043198.0 1
1,4-Dichlorobenzene <122 ug/kg 12/14/15 20:11 106-46-712/07/15 15:304311221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-10 Lab ID:92278649006 Collected:11/30/15 14:30 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <94.1 ug/kg 12/14/15 20:11 91-94-112/07/15 15:30216094.1 1
2,4-Dichlorophenol <94.1 ug/kg 12/14/15 20:11 120-83-212/07/15 15:3043194.1 1
Diethylphthalate <66.6 ug/kg 12/14/15 20:11 84-66-212/07/15 15:3043166.6 1
2,4-Dimethylphenol <170 ug/kg 12/14/15 20:11 105-67-912/07/15 15:304311701
Dimethylphthalate <87.6 ug/kg 12/14/15 20:11 131-11-312/07/15 15:3043187.6 1
Di-n-butylphthalate <70.6 ug/kg 12/14/15 20:11 84-74-212/07/15 15:3043170.6 1
4,6-Dinitro-2-methylphenol <86.2 ug/kg 12/14/15 20:11 534-52-112/07/15 15:3086286.2 1
2,4-Dinitrophenol <70.6 ug/kg 12/14/15 20:11 51-28-512/07/15 15:30216070.6 1
2,4-Dinitrotoluene <81.0 ug/kg 12/14/15 20:11 121-14-212/07/15 15:3043181.0 1
2,6-Dinitrotoluene <90.2 ug/kg 12/14/15 20:11 606-20-212/07/15 15:3043190.2 1
Di-n-octylphthalate <90.2 ug/kg 12/14/15 20:11 117-84-012/07/15 15:3043190.2 1
bis(2-Ethylhexyl)phthalate <118 ug/kg 12/14/15 20:11 117-81-712/07/15 15:304311181
Fluoranthene <62.7 ug/kg 12/14/15 20:11 206-44-012/07/15 15:3043162.7 1
Fluorene <88.9 ug/kg 12/14/15 20:11 86-73-712/07/15 15:3043188.9 1
Hexachloro-1,3-butadiene <74.5 ug/kg 12/14/15 20:11 87-68-312/07/15 15:3043174.5 1
Hexachlorobenzene <54.9 ug/kg 12/14/15 20:11 118-74-112/07/15 15:3043154.9 1
Hexachlorocyclopentadiene <79.7 ug/kg 12/14/15 20:11 77-47-412/07/15 15:3043179.7 1
Hexachloroethane <114 ug/kg 12/14/15 20:11 67-72-112/07/15 15:304311141
Indeno(1,2,3-cd)pyrene <88.9 ug/kg 12/14/15 20:11 193-39-512/07/15 15:3043188.9 1
Isophorone <96.7 ug/kg 12/14/15 20:11 78-59-112/07/15 15:3043196.7 1
1-Methylnaphthalene 149J ug/kg 12/14/15 20:11 90-12-012/07/15 15:304311121
2-Methylnaphthalene 228J ug/kg 12/14/15 20:11 91-57-612/07/15 15:3043192.8 1
2-Methylphenol(o-Cresol)<131 ug/kg 12/14/15 20:11 95-48-712/07/15 15:304311311
3&4-Methylphenol(m&p Cresol)<170 ug/kg 12/14/15 20:1112/07/15 15:304311701
Naphthalene <106 ug/kg 12/14/15 20:11 91-20-312/07/15 15:304311061
2-Nitroaniline <133 ug/kg 12/14/15 20:11 88-74-412/07/15 15:3021601331
3-Nitroaniline <118 ug/kg 12/14/15 20:11 99-09-212/07/15 15:3021601181
4-Nitroaniline <122 ug/kg 12/14/15 20:11 100-01-612/07/15 15:308621221
Nitrobenzene <118 ug/kg 12/14/15 20:11 98-95-312/07/15 15:304311181
2-Nitrophenol <105 ug/kg 12/14/15 20:11 88-75-512/07/15 15:304311051
4-Nitrophenol <77.1 ug/kg 12/14/15 20:11 100-02-712/07/15 15:30216077.1 1
N-Nitrosodimethylamine <140 ug/kg 12/14/15 20:11 62-75-912/07/15 15:304311401
N-Nitroso-di-n-propylamine <82.3 ug/kg 12/14/15 20:11 621-64-712/07/15 15:3043182.3 1
N-Nitrosodiphenylamine <128 ug/kg 12/14/15 20:11 86-30-612/07/15 15:304311281
Pentachlorophenol <78.4 ug/kg 12/14/15 20:11 87-86-512/07/15 15:30216078.4 1
Phenanthrene <71.9 ug/kg 12/14/15 20:11 85-01-812/07/15 15:3043171.9 1
Phenol <129 ug/kg 12/14/15 20:11 108-95-212/07/15 15:304311291
Pyrene <73.2 ug/kg 12/14/15 20:11 129-00-012/07/15 15:3043173.2 1
1,2,4-Trichlorobenzene <83.6 ug/kg 12/14/15 20:11 120-82-112/07/15 15:3043183.6 1
2,4,5-Trichlorophenol <133 ug/kg 12/14/15 20:11 95-95-412/07/15 15:304311331
2,4,6-Trichlorophenol <95.4 ug/kg 12/14/15 20:11 88-06-212/07/15 15:3043195.4 1
Surrogates
Nitrobenzene-d5 (S)86 %12/14/15 20:11 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)81 %12/14/15 20:11 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)69 %12/14/15 20:11 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-10 Lab ID:92278649006 Collected:11/30/15 14:30 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)74 %12/14/15 20:11 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)75 %12/14/15 20:11 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)91 %12/14/15 20:11 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone <627 ug/kg 12/08/15 21:48 67-64-1627062750
Benzene <100 ug/kg 12/08/15 21:48 71-43-231410050
Bromobenzene <125 ug/kg 12/08/15 21:48 108-86-131412550
Bromochloromethane <107 ug/kg 12/08/15 21:48 74-97-531410750
Bromodichloromethane <119 ug/kg 12/08/15 21:48 75-27-431411950
Bromoform <144 ug/kg 12/08/15 21:48 75-25-231414450
Bromomethane <157 ug/kg 12/08/15 21:48 74-83-962715750
2-Butanone (MEK)<182 ug/kg 12/08/15 21:48 78-93-3627018250
n-Butylbenzene 950 ug/kg 12/08/15 21:48 104-51-831411350
sec-Butylbenzene 589 ug/kg 12/08/15 21:48 135-98-831410050
tert-Butylbenzene <125 ug/kg 12/08/15 21:48 98-06-631412550
Carbon tetrachloride <163 ug/kg 12/08/15 21:48 56-23-531416350
Chlorobenzene <119 ug/kg 12/08/15 21:48 108-90-731411950
Chloroethane <150 ug/kg 12/08/15 21:48 75-00-362715050
Chloroform <100 ug/kg 12/08/15 21:48 67-66-331410050
Chloromethane <150 ug/kg 12/08/15 21:48 74-87-362715050
2-Chlorotoluene <107 ug/kg 12/08/15 21:48 95-49-831410750
4-Chlorotoluene <113 ug/kg 12/08/15 21:48 106-43-431411350
1,2-Dibromo-3-chloropropane <226 ug/kg 12/08/15 21:48 96-12-831422650
Dibromochloromethane <113 ug/kg 12/08/15 21:48 124-48-131411350
1,2-Dibromoethane (EDB)<113 ug/kg 12/08/15 21:48 106-93-431411350
Dibromomethane <157 ug/kg 12/08/15 21:48 74-95-331415750
1,2-Dichlorobenzene <119 ug/kg 12/08/15 21:48 95-50-131411950
1,3-Dichlorobenzene <125 ug/kg 12/08/15 21:48 541-73-131412550
1,4-Dichlorobenzene <107 ug/kg 12/08/15 21:48 106-46-731410750
Dichlorodifluoromethane <226 ug/kg 12/08/15 21:48 75-71-862722650
1,1-Dichloroethane <94.1 ug/kg 12/08/15 21:48 75-34-331494.1 50
1,2-Dichloroethane <138 ug/kg 12/08/15 21:48 107-06-231413850
1,1-Dichloroethene <113 ug/kg 12/08/15 21:48 75-35-431411350
cis-1,2-Dichloroethene <87.8 ug/kg 12/08/15 21:48 156-59-231487.8 50
trans-1,2-Dichloroethene <119 ug/kg 12/08/15 21:48 156-60-531411950
1,2-Dichloropropane <107 ug/kg 12/08/15 21:48 78-87-531410750
1,3-Dichloropropane <119 ug/kg 12/08/15 21:48 142-28-931411950
2,2-Dichloropropane <107 ug/kg 12/08/15 21:48 594-20-731410750
1,1-Dichloropropene <94.1 ug/kg 12/08/15 21:48 563-58-631494.1 50
cis-1,3-Dichloropropene <113 ug/kg 12/08/15 21:48 10061-01-531411350
trans-1,3-Dichloropropene <94.1 ug/kg 12/08/15 21:48 10061-02-631494.1 50
Diisopropyl ether <107 ug/kg 12/08/15 21:48 108-20-331410750
Ethylbenzene 120J ug/kg 12/08/15 21:48 100-41-431411350
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-10 Lab ID:92278649006 Collected:11/30/15 14:30 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <125 ug/kg 12/08/15 21:48 87-68-331412550
2-Hexanone <245 ug/kg 12/08/15 21:48 591-78-6314024550
Isopropylbenzene (Cumene)222J ug/kg 12/08/15 21:48 98-82-831411950
p-Isopropyltoluene 407 ug/kg 12/08/15 21:48 99-87-631410750
Methylene Chloride <188 ug/kg 12/08/15 21:48 75-09-2125018850
4-Methyl-2-pentanone (MIBK)<232 ug/kg 12/08/15 21:48 108-10-1314023250
Methyl-tert-butyl ether <94.1 ug/kg 12/08/15 21:48 1634-04-431494.1 50
Naphthalene 956 ug/kg 12/08/15 21:48 91-20-331475.2 50
n-Propylbenzene 429 ug/kg 12/08/15 21:48 103-65-131410750
Styrene <113 ug/kg 12/08/15 21:48 100-42-531411350
1,1,1,2-Tetrachloroethane <132 ug/kg 12/08/15 21:48 630-20-631413250
1,1,2,2-Tetrachloroethane <119 ug/kg 12/08/15 21:48 79-34-531411950
Tetrachloroethene <107 ug/kg 12/08/15 21:48 127-18-431410750
Toluene <113 ug/kg 12/08/15 21:48 108-88-331411350
1,2,3-Trichlorobenzene <138 ug/kg 12/08/15 21:48 87-61-631413850
1,2,4-Trichlorobenzene <100 ug/kg 12/08/15 21:48 120-82-131410050
1,1,1-Trichloroethane <113 ug/kg 12/08/15 21:48 71-55-631411350
1,1,2-Trichloroethane <132 ug/kg 12/08/15 21:48 79-00-531413250
Trichloroethene <132 ug/kg 12/08/15 21:48 79-01-631413250
Trichlorofluoromethane <138 ug/kg 12/08/15 21:48 75-69-431413850
1,2,3-Trichloropropane <100 ug/kg 12/08/15 21:48 96-18-431410050
1,2,4-Trimethylbenzene 1670 ug/kg 12/08/15 21:48 95-63-631412550
1,3,5-Trimethylbenzene 269J ug/kg 12/08/15 21:48 108-67-831411350
Vinyl acetate <552 ug/kg 12/08/15 21:48 108-05-4314055250
Vinyl chloride <113 ug/kg 12/08/15 21:48 75-01-462711350
Xylene (Total)<226 ug/kg 12/08/15 21:48 1330-20-762722650
m&p-Xylene <226 ug/kg 12/08/15 21:48 179601-23-162722650
o-Xylene <119 ug/kg 12/08/15 21:48 95-47-631411950
Surrogates
Toluene-d8 (S)99 %12/08/15 21:48 2037-26-5 D370-130 50
4-Bromofluorobenzene (S)98 %12/08/15 21:48 460-00-470-130 50
1,2-Dichloroethane-d4 (S)83 %12/08/15 21:48 17060-07-070-132 50
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.5 %12/08/15 11:240.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-11 Lab ID:92278649007 Collected:11/30/15 15:15 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<12.8 mg/kg 12/12/15 03:24 N212/10/15 10:1212.8 12.8 1
Aliphatic (C19-C36)<12.8 mg/kg 12/12/15 03:24 N212/10/15 10:1212.8 12.8 1
Aromatic (C11-C22)<12.8 mg/kg 12/15/15 04:22 N212/10/15 10:1212.8 12.8 1
Surrogates
Nonatriacontane (S)60 %12/12/15 03:24 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)54 %12/15/15 04:22 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)91 %12/15/15 04:22 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)84 %12/15/15 04:22 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<3.5 mg/kg 12/17/15 10:25 N212/16/15 14:153.5 3.5 1
Aliphatic (C09-C12)<3.5 mg/kg 12/17/15 10:25 N212/16/15 14:153.5 3.5 1
Aromatic (C09-C10)<3.5 mg/kg 12/17/15 10:25 N212/16/15 14:153.5 3.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)89 %12/17/15 10:25 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)89 %12/17/15 10:25 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <97.5 ug/kg 12/14/15 20:39 83-32-912/07/15 15:3042397.5 1
Acenaphthylene <100 ug/kg 12/14/15 20:39 208-96-812/07/15 15:304231001
Aniline <114 ug/kg 12/14/15 20:39 62-53-312/07/15 15:304231141
Anthracene <94.9 ug/kg 12/14/15 20:39 120-12-712/07/15 15:3042394.9 1
Benzo(a)anthracene <78.3 ug/kg 12/14/15 20:39 56-55-312/07/15 15:3042378.3 1
Benzo(a)pyrene <80.8 ug/kg 12/14/15 20:39 50-32-812/07/15 15:3042380.8 1
Benzo(b)fluoranthene <73.1 ug/kg 12/14/15 20:39 205-99-212/07/15 15:3042373.1 1
Benzo(g,h,i)perylene <108 ug/kg 12/14/15 20:39 191-24-212/07/15 15:304231081
Benzo(k)fluoranthene <83.4 ug/kg 12/14/15 20:39 207-08-912/07/15 15:3042383.4 1
Benzoic Acid <77.0 ug/kg 12/14/15 20:39 65-85-012/07/15 15:30212077.0 1
Benzyl alcohol <84.7 ug/kg 12/14/15 20:39 100-51-612/07/15 15:3084784.7 1
4-Bromophenylphenyl ether <77.0 ug/kg 12/14/15 20:39 101-55-312/07/15 15:3042377.0 1
Butylbenzylphthalate <89.8 ug/kg 12/14/15 20:39 85-68-712/07/15 15:3042389.8 1
4-Chloro-3-methylphenol <87.2 ug/kg 12/14/15 20:39 59-50-712/07/15 15:3084787.2 1
4-Chloroaniline <118 ug/kg 12/14/15 20:39 106-47-812/07/15 15:3021201181
bis(2-Chloroethoxy)methane <98.8 ug/kg 12/14/15 20:39 111-91-112/07/15 15:3042398.8 1
bis(2-Chloroethyl) ether <108 ug/kg 12/14/15 20:39 111-44-412/07/15 15:304231081
bis(2-Chloroisopropyl) ether <113 ug/kg 12/14/15 20:39 108-60-112/07/15 15:304231131
2-Chloronaphthalene <83.4 ug/kg 12/14/15 20:39 91-58-712/07/15 15:3042383.4 1
2-Chlorophenol <115 ug/kg 12/14/15 20:39 95-57-812/07/15 15:304231151
4-Chlorophenylphenyl ether <87.2 ug/kg 12/14/15 20:39 7005-72-312/07/15 15:3042387.2 1
Chrysene <56.5 ug/kg 12/14/15 20:39 218-01-912/07/15 15:3042356.5 1
Dibenz(a,h)anthracene <89.8 ug/kg 12/14/15 20:39 53-70-312/07/15 15:3042389.8 1
Dibenzofuran <69.3 ug/kg 12/14/15 20:39 132-64-912/07/15 15:3042369.3 1
1,2-Dichlorobenzene <113 ug/kg 12/14/15 20:39 95-50-112/07/15 15:304231131
1,3-Dichlorobenzene <96.2 ug/kg 12/14/15 20:39 541-73-112/07/15 15:3042396.2 1
1,4-Dichlorobenzene <119 ug/kg 12/14/15 20:39 106-46-712/07/15 15:304231191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-11 Lab ID:92278649007 Collected:11/30/15 15:15 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <92.4 ug/kg 12/14/15 20:39 91-94-112/07/15 15:30212092.4 1
2,4-Dichlorophenol <92.4 ug/kg 12/14/15 20:39 120-83-212/07/15 15:3042392.4 1
Diethylphthalate <65.4 ug/kg 12/14/15 20:39 84-66-212/07/15 15:3042365.4 1
2,4-Dimethylphenol <167 ug/kg 12/14/15 20:39 105-67-912/07/15 15:304231671
Dimethylphthalate <86.0 ug/kg 12/14/15 20:39 131-11-312/07/15 15:3042386.0 1
Di-n-butylphthalate <69.3 ug/kg 12/14/15 20:39 84-74-212/07/15 15:3042369.3 1
4,6-Dinitro-2-methylphenol <84.7 ug/kg 12/14/15 20:39 534-52-112/07/15 15:3084784.7 1
2,4-Dinitrophenol <69.3 ug/kg 12/14/15 20:39 51-28-512/07/15 15:30212069.3 1
2,4-Dinitrotoluene <79.5 ug/kg 12/14/15 20:39 121-14-212/07/15 15:3042379.5 1
2,6-Dinitrotoluene <88.5 ug/kg 12/14/15 20:39 606-20-212/07/15 15:3042388.5 1
Di-n-octylphthalate <88.5 ug/kg 12/14/15 20:39 117-84-012/07/15 15:3042388.5 1
bis(2-Ethylhexyl)phthalate <115 ug/kg 12/14/15 20:39 117-81-712/07/15 15:304231151
Fluoranthene <61.6 ug/kg 12/14/15 20:39 206-44-012/07/15 15:3042361.6 1
Fluorene <87.2 ug/kg 12/14/15 20:39 86-73-712/07/15 15:3042387.2 1
Hexachloro-1,3-butadiene <73.1 ug/kg 12/14/15 20:39 87-68-312/07/15 15:3042373.1 1
Hexachlorobenzene <53.9 ug/kg 12/14/15 20:39 118-74-112/07/15 15:3042353.9 1
Hexachlorocyclopentadiene <78.3 ug/kg 12/14/15 20:39 77-47-412/07/15 15:3042378.3 1
Hexachloroethane <112 ug/kg 12/14/15 20:39 67-72-112/07/15 15:304231121
Indeno(1,2,3-cd)pyrene <87.2 ug/kg 12/14/15 20:39 193-39-512/07/15 15:3042387.2 1
Isophorone <94.9 ug/kg 12/14/15 20:39 78-59-112/07/15 15:3042394.9 1
1-Methylnaphthalene <110 ug/kg 12/14/15 20:39 90-12-012/07/15 15:304231101
2-Methylnaphthalene <91.1 ug/kg 12/14/15 20:39 91-57-612/07/15 15:3042391.1 1
2-Methylphenol(o-Cresol)<128 ug/kg 12/14/15 20:39 95-48-712/07/15 15:304231281
3&4-Methylphenol(m&p Cresol)<167 ug/kg 12/14/15 20:3912/07/15 15:304231671
Naphthalene <104 ug/kg 12/14/15 20:39 91-20-312/07/15 15:304231041
2-Nitroaniline <131 ug/kg 12/14/15 20:39 88-74-412/07/15 15:3021201311
3-Nitroaniline <115 ug/kg 12/14/15 20:39 99-09-212/07/15 15:3021201151
4-Nitroaniline <119 ug/kg 12/14/15 20:39 100-01-612/07/15 15:308471191
Nitrobenzene <115 ug/kg 12/14/15 20:39 98-95-312/07/15 15:304231151
2-Nitrophenol <103 ug/kg 12/14/15 20:39 88-75-512/07/15 15:304231031
4-Nitrophenol <75.7 ug/kg 12/14/15 20:39 100-02-712/07/15 15:30212075.7 1
N-Nitrosodimethylamine <137 ug/kg 12/14/15 20:39 62-75-912/07/15 15:304231371
N-Nitroso-di-n-propylamine <80.8 ug/kg 12/14/15 20:39 621-64-712/07/15 15:3042380.8 1
N-Nitrosodiphenylamine <126 ug/kg 12/14/15 20:39 86-30-612/07/15 15:304231261
Pentachlorophenol <77.0 ug/kg 12/14/15 20:39 87-86-512/07/15 15:30212077.0 1
Phenanthrene <70.6 ug/kg 12/14/15 20:39 85-01-812/07/15 15:3042370.6 1
Phenol <127 ug/kg 12/14/15 20:39 108-95-212/07/15 15:304231271
Pyrene <71.9 ug/kg 12/14/15 20:39 129-00-012/07/15 15:3042371.9 1
1,2,4-Trichlorobenzene <82.1 ug/kg 12/14/15 20:39 120-82-112/07/15 15:3042382.1 1
2,4,5-Trichlorophenol <131 ug/kg 12/14/15 20:39 95-95-412/07/15 15:304231311
2,4,6-Trichlorophenol <93.7 ug/kg 12/14/15 20:39 88-06-212/07/15 15:3042393.7 1
Surrogates
Nitrobenzene-d5 (S)87 %12/14/15 20:39 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)85 %12/14/15 20:39 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)63 %12/14/15 20:39 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-11 Lab ID:92278649007 Collected:11/30/15 15:15 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)78 %12/14/15 20:39 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)77 %12/14/15 20:39 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)90 %12/14/15 20:39 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone <12.1 ug/kg 12/08/15 22:08 67-64-112112.1 1
Benzene <1.9 ug/kg 12/08/15 22:08 71-43-26.0 1.9 1
Bromobenzene <2.4 ug/kg 12/08/15 22:08 108-86-16.0 2.4 1
Bromochloromethane <2.0 ug/kg 12/08/15 22:08 74-97-56.0 2.0 1
Bromodichloromethane <2.3 ug/kg 12/08/15 22:08 75-27-46.0 2.3 1
Bromoform <2.8 ug/kg 12/08/15 22:08 75-25-26.0 2.8 1
Bromomethane <3.0 ug/kg 12/08/15 22:08 74-83-912.1 3.0 1
2-Butanone (MEK)<3.5 ug/kg 12/08/15 22:08 78-93-31213.5 1
n-Butylbenzene <2.2 ug/kg 12/08/15 22:08 104-51-86.0 2.2 1
sec-Butylbenzene <1.9 ug/kg 12/08/15 22:08 135-98-86.0 1.9 1
tert-Butylbenzene <2.4 ug/kg 12/08/15 22:08 98-06-66.0 2.4 1
Carbon tetrachloride <3.1 ug/kg 12/08/15 22:08 56-23-56.0 3.1 1
Chlorobenzene <2.3 ug/kg 12/08/15 22:08 108-90-76.0 2.3 1
Chloroethane <2.9 ug/kg 12/08/15 22:08 75-00-312.1 2.9 1
Chloroform <1.9 ug/kg 12/08/15 22:08 67-66-36.0 1.9 1
Chloromethane <2.9 ug/kg 12/08/15 22:08 74-87-312.1 2.9 1
2-Chlorotoluene <2.0 ug/kg 12/08/15 22:08 95-49-86.0 2.0 1
4-Chlorotoluene <2.2 ug/kg 12/08/15 22:08 106-43-46.0 2.2 1
1,2-Dibromo-3-chloropropane <4.3 ug/kg 12/08/15 22:08 96-12-86.0 4.3 1
Dibromochloromethane <2.2 ug/kg 12/08/15 22:08 124-48-16.0 2.2 1
1,2-Dibromoethane (EDB)<2.2 ug/kg 12/08/15 22:08 106-93-46.0 2.2 1
Dibromomethane <3.0 ug/kg 12/08/15 22:08 74-95-36.0 3.0 1
1,2-Dichlorobenzene <2.3 ug/kg 12/08/15 22:08 95-50-16.0 2.3 1
1,3-Dichlorobenzene <2.4 ug/kg 12/08/15 22:08 541-73-16.0 2.4 1
1,4-Dichlorobenzene <2.0 ug/kg 12/08/15 22:08 106-46-76.0 2.0 1
Dichlorodifluoromethane <4.3 ug/kg 12/08/15 22:08 75-71-812.1 4.3 1
1,1-Dichloroethane <1.8 ug/kg 12/08/15 22:08 75-34-36.0 1.8 1
1,2-Dichloroethane <2.7 ug/kg 12/08/15 22:08 107-06-26.0 2.7 1
1,1-Dichloroethene <2.2 ug/kg 12/08/15 22:08 75-35-46.0 2.2 1
cis-1,2-Dichloroethene <1.7 ug/kg 12/08/15 22:08 156-59-26.0 1.7 1
trans-1,2-Dichloroethene <2.3 ug/kg 12/08/15 22:08 156-60-56.0 2.3 1
1,2-Dichloropropane <2.0 ug/kg 12/08/15 22:08 78-87-56.0 2.0 1
1,3-Dichloropropane <2.3 ug/kg 12/08/15 22:08 142-28-96.0 2.3 1
2,2-Dichloropropane <2.0 ug/kg 12/08/15 22:08 594-20-76.0 2.0 1
1,1-Dichloropropene <1.8 ug/kg 12/08/15 22:08 563-58-66.0 1.8 1
cis-1,3-Dichloropropene <2.2 ug/kg 12/08/15 22:08 10061-01-56.0 2.2 1
trans-1,3-Dichloropropene <1.8 ug/kg 12/08/15 22:08 10061-02-66.0 1.8 1
Diisopropyl ether <2.0 ug/kg 12/08/15 22:08 108-20-36.0 2.0 1
Ethylbenzene <2.2 ug/kg 12/08/15 22:08 100-41-46.0 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-11 Lab ID:92278649007 Collected:11/30/15 15:15 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.4 ug/kg 12/08/15 22:08 87-68-36.0 2.4 1
2-Hexanone <4.7 ug/kg 12/08/15 22:08 591-78-660.3 4.7 1
Isopropylbenzene (Cumene)<2.3 ug/kg 12/08/15 22:08 98-82-86.0 2.3 1
p-Isopropyltoluene <2.0 ug/kg 12/08/15 22:08 99-87-66.0 2.0 1
Methylene Chloride 8.7J ug/kg 12/08/15 22:08 75-09-224.1 3.6 1
4-Methyl-2-pentanone (MIBK)<4.5 ug/kg 12/08/15 22:08 108-10-160.3 4.5 1
Methyl-tert-butyl ether <1.8 ug/kg 12/08/15 22:08 1634-04-46.0 1.8 1
Naphthalene <1.4 ug/kg 12/08/15 22:08 91-20-36.0 1.4 1
n-Propylbenzene <2.0 ug/kg 12/08/15 22:08 103-65-16.0 2.0 1
Styrene <2.2 ug/kg 12/08/15 22:08 100-42-56.0 2.2 1
1,1,1,2-Tetrachloroethane <2.5 ug/kg 12/08/15 22:08 630-20-66.0 2.5 1
1,1,2,2-Tetrachloroethane <2.3 ug/kg 12/08/15 22:08 79-34-56.0 2.3 1
Tetrachloroethene <2.0 ug/kg 12/08/15 22:08 127-18-46.0 2.0 1
Toluene <2.2 ug/kg 12/08/15 22:08 108-88-36.0 2.2 1
1,2,3-Trichlorobenzene <2.7 ug/kg 12/08/15 22:08 87-61-66.0 2.7 1
1,2,4-Trichlorobenzene <1.9 ug/kg 12/08/15 22:08 120-82-16.0 1.9 1
1,1,1-Trichloroethane <2.2 ug/kg 12/08/15 22:08 71-55-66.0 2.2 1
1,1,2-Trichloroethane <2.5 ug/kg 12/08/15 22:08 79-00-56.0 2.5 1
Trichloroethene <2.5 ug/kg 12/08/15 22:08 79-01-66.0 2.5 1
Trichlorofluoromethane <2.7 ug/kg 12/08/15 22:08 75-69-46.0 2.7 1
1,2,3-Trichloropropane <1.9 ug/kg 12/08/15 22:08 96-18-46.0 1.9 1
1,2,4-Trimethylbenzene <2.4 ug/kg 12/08/15 22:08 95-63-66.0 2.4 1
1,3,5-Trimethylbenzene <2.2 ug/kg 12/08/15 22:08 108-67-86.0 2.2 1
Vinyl acetate <10.6 ug/kg 12/08/15 22:08 108-05-460.3 10.6 1
Vinyl chloride <2.2 ug/kg 12/08/15 22:08 75-01-412.1 2.2 1
Xylene (Total)<4.3 ug/kg 12/08/15 22:08 1330-20-712.1 4.3 1
m&p-Xylene <4.3 ug/kg 12/08/15 22:08 179601-23-112.1 4.3 1
o-Xylene <2.3 ug/kg 12/08/15 22:08 95-47-66.0 2.3 1
Surrogates
Toluene-d8 (S)100 %12/08/15 22:08 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %12/08/15 22:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %12/08/15 22:08 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.1 %12/08/15 11:240.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-13 Lab ID:92278649008 Collected:11/30/15 16:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)<14.0 mg/kg 12/12/15 03:51 N212/10/15 10:1214.0 14.0 1
Aliphatic (C19-C36)<14.0 mg/kg 12/12/15 03:51 N212/10/15 10:1214.0 14.0 1
Aromatic (C11-C22)<14.0 mg/kg 12/15/15 04:49 N212/10/15 10:1214.0 14.0 1
Surrogates
Nonatriacontane (S)56 %12/12/15 03:51 7194-86-712/10/15 10:1240-140 1
o-Terphenyl (S)71 %12/15/15 04:49 84-15-112/10/15 10:1240-140 1
2-Fluorobiphenyl (S)104 %12/15/15 04:49 321-60-812/10/15 10:1240-140 1
2-Bromonaphthalene (S)87 %12/15/15 04:49 580-13-212/10/15 10:1240-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<3.8 mg/kg 12/16/15 19:12 N212/16/15 14:153.8 3.8 1
Aliphatic (C09-C12)<3.8 mg/kg 12/16/15 19:12 N212/16/15 14:153.8 3.8 1
Aromatic (C09-C10)<3.8 mg/kg 12/16/15 19:12 N212/16/15 14:153.8 3.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %12/16/15 19:12 460-00-412/16/15 14:1570-130 1
4-Bromofluorobenzene (PID) (S)97 %12/16/15 19:12 460-00-412/16/15 14:1570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <107 ug/kg 12/14/15 21:07 83-32-912/07/15 15:304631071
Acenaphthylene <110 ug/kg 12/14/15 21:07 208-96-812/07/15 15:304631101
Aniline <125 ug/kg 12/14/15 21:07 62-53-312/07/15 15:304631251
Anthracene <104 ug/kg 12/14/15 21:07 120-12-712/07/15 15:304631041
Benzo(a)anthracene <85.7 ug/kg 12/14/15 21:07 56-55-312/07/15 15:3046385.7 1
Benzo(a)pyrene <88.5 ug/kg 12/14/15 21:07 50-32-812/07/15 15:3046388.5 1
Benzo(b)fluoranthene <80.0 ug/kg 12/14/15 21:07 205-99-212/07/15 15:3046380.0 1
Benzo(g,h,i)perylene <118 ug/kg 12/14/15 21:07 191-24-212/07/15 15:304631181
Benzo(k)fluoranthene <91.3 ug/kg 12/14/15 21:07 207-08-912/07/15 15:3046391.3 1
Benzoic Acid <84.3 ug/kg 12/14/15 21:07 65-85-012/07/15 15:30232084.3 1
Benzyl alcohol <92.7 ug/kg 12/14/15 21:07 100-51-612/07/15 15:3092792.7 1
4-Bromophenylphenyl ether <84.3 ug/kg 12/14/15 21:07 101-55-312/07/15 15:3046384.3 1
Butylbenzylphthalate <98.3 ug/kg 12/14/15 21:07 85-68-712/07/15 15:3046398.3 1
4-Chloro-3-methylphenol <95.5 ug/kg 12/14/15 21:07 59-50-712/07/15 15:3092795.5 1
4-Chloroaniline <129 ug/kg 12/14/15 21:07 106-47-812/07/15 15:3023201291
bis(2-Chloroethoxy)methane <108 ug/kg 12/14/15 21:07 111-91-112/07/15 15:304631081
bis(2-Chloroethyl) ether <118 ug/kg 12/14/15 21:07 111-44-412/07/15 15:304631181
bis(2-Chloroisopropyl) ether <124 ug/kg 12/14/15 21:07 108-60-112/07/15 15:304631241
2-Chloronaphthalene <91.3 ug/kg 12/14/15 21:07 91-58-712/07/15 15:3046391.3 1
2-Chlorophenol <126 ug/kg 12/14/15 21:07 95-57-812/07/15 15:304631261
4-Chlorophenylphenyl ether <95.5 ug/kg 12/14/15 21:07 7005-72-312/07/15 15:3046395.5 1
Chrysene <61.8 ug/kg 12/14/15 21:07 218-01-912/07/15 15:3046361.8 1
Dibenz(a,h)anthracene <98.3 ug/kg 12/14/15 21:07 53-70-312/07/15 15:3046398.3 1
Dibenzofuran <75.8 ug/kg 12/14/15 21:07 132-64-912/07/15 15:3046375.8 1
1,2-Dichlorobenzene <124 ug/kg 12/14/15 21:07 95-50-112/07/15 15:304631241
1,3-Dichlorobenzene <105 ug/kg 12/14/15 21:07 541-73-112/07/15 15:304631051
1,4-Dichlorobenzene <131 ug/kg 12/14/15 21:07 106-46-712/07/15 15:304631311
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-13 Lab ID:92278649008 Collected:11/30/15 16:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <101 ug/kg 12/14/15 21:07 91-94-112/07/15 15:3023201011
2,4-Dichlorophenol <101 ug/kg 12/14/15 21:07 120-83-212/07/15 15:304631011
Diethylphthalate <71.6 ug/kg 12/14/15 21:07 84-66-212/07/15 15:3046371.6 1
2,4-Dimethylphenol <183 ug/kg 12/14/15 21:07 105-67-912/07/15 15:304631831
Dimethylphthalate <94.1 ug/kg 12/14/15 21:07 131-11-312/07/15 15:3046394.1 1
Di-n-butylphthalate <75.8 ug/kg 12/14/15 21:07 84-74-212/07/15 15:3046375.8 1
4,6-Dinitro-2-methylphenol <92.7 ug/kg 12/14/15 21:07 534-52-112/07/15 15:3092792.7 1
2,4-Dinitrophenol <75.8 ug/kg 12/14/15 21:07 51-28-512/07/15 15:30232075.8 1
2,4-Dinitrotoluene <87.1 ug/kg 12/14/15 21:07 121-14-212/07/15 15:3046387.1 1
2,6-Dinitrotoluene <96.9 ug/kg 12/14/15 21:07 606-20-212/07/15 15:3046396.9 1
Di-n-octylphthalate <96.9 ug/kg 12/14/15 21:07 117-84-012/07/15 15:3046396.9 1
bis(2-Ethylhexyl)phthalate <126 ug/kg 12/14/15 21:07 117-81-712/07/15 15:304631261
Fluoranthene <67.4 ug/kg 12/14/15 21:07 206-44-012/07/15 15:3046367.4 1
Fluorene <95.5 ug/kg 12/14/15 21:07 86-73-712/07/15 15:3046395.5 1
Hexachloro-1,3-butadiene <80.0 ug/kg 12/14/15 21:07 87-68-312/07/15 15:3046380.0 1
Hexachlorobenzene <59.0 ug/kg 12/14/15 21:07 118-74-112/07/15 15:3046359.0 1
Hexachlorocyclopentadiene <85.7 ug/kg 12/14/15 21:07 77-47-412/07/15 15:3046385.7 1
Hexachloroethane <122 ug/kg 12/14/15 21:07 67-72-112/07/15 15:304631221
Indeno(1,2,3-cd)pyrene <95.5 ug/kg 12/14/15 21:07 193-39-512/07/15 15:3046395.5 1
Isophorone <104 ug/kg 12/14/15 21:07 78-59-112/07/15 15:304631041
1-Methylnaphthalene <121 ug/kg 12/14/15 21:07 90-12-012/07/15 15:304631211
2-Methylnaphthalene <99.7 ug/kg 12/14/15 21:07 91-57-612/07/15 15:3046399.7 1
2-Methylphenol(o-Cresol)<140 ug/kg 12/14/15 21:07 95-48-712/07/15 15:304631401
3&4-Methylphenol(m&p Cresol)<183 ug/kg 12/14/15 21:0712/07/15 15:304631831
Naphthalene <114 ug/kg 12/14/15 21:07 91-20-312/07/15 15:304631141
2-Nitroaniline <143 ug/kg 12/14/15 21:07 88-74-412/07/15 15:3023201431
3-Nitroaniline <126 ug/kg 12/14/15 21:07 99-09-212/07/15 15:3023201261
4-Nitroaniline <131 ug/kg 12/14/15 21:07 100-01-612/07/15 15:309271311
Nitrobenzene <126 ug/kg 12/14/15 21:07 98-95-312/07/15 15:304631261
2-Nitrophenol <112 ug/kg 12/14/15 21:07 88-75-512/07/15 15:304631121
4-Nitrophenol <82.9 ug/kg 12/14/15 21:07 100-02-712/07/15 15:30232082.9 1
N-Nitrosodimethylamine <150 ug/kg 12/14/15 21:07 62-75-912/07/15 15:304631501
N-Nitroso-di-n-propylamine <88.5 ug/kg 12/14/15 21:07 621-64-712/07/15 15:3046388.5 1
N-Nitrosodiphenylamine <138 ug/kg 12/14/15 21:07 86-30-612/07/15 15:304631381
Pentachlorophenol <84.3 ug/kg 12/14/15 21:07 87-86-512/07/15 15:30232084.3 1
Phenanthrene <77.2 ug/kg 12/14/15 21:07 85-01-812/07/15 15:3046377.2 1
Phenol <139 ug/kg 12/14/15 21:07 108-95-212/07/15 15:304631391
Pyrene <78.6 ug/kg 12/14/15 21:07 129-00-012/07/15 15:3046378.6 1
1,2,4-Trichlorobenzene <89.9 ug/kg 12/14/15 21:07 120-82-112/07/15 15:3046389.9 1
2,4,5-Trichlorophenol <143 ug/kg 12/14/15 21:07 95-95-412/07/15 15:304631431
2,4,6-Trichlorophenol <103 ug/kg 12/14/15 21:07 88-06-212/07/15 15:304631031
Surrogates
Nitrobenzene-d5 (S)83 %12/14/15 21:07 4165-60-012/07/15 15:3023-110 1
2-Fluorobiphenyl (S)88 %12/14/15 21:07 321-60-812/07/15 15:3030-110 1
Terphenyl-d14 (S)75 %12/14/15 21:07 1718-51-012/07/15 15:3028-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-13 Lab ID:92278649008 Collected:11/30/15 16:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)72 %12/14/15 21:07 13127-88-312/07/15 15:3022-110 1
2-Fluorophenol (S)72 %12/14/15 21:07 367-12-412/07/15 15:3013-110 1
2,4,6-Tribromophenol (S)85 %12/14/15 21:07 118-79-612/07/15 15:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone <13.5 ug/kg 12/09/15 22:05 67-64-113513.5 1
Benzene <2.2 ug/kg 12/09/15 22:05 71-43-26.7 2.2 1
Bromobenzene <2.7 ug/kg 12/09/15 22:05 108-86-16.7 2.7 1
Bromochloromethane <2.3 ug/kg 12/09/15 22:05 74-97-56.7 2.3 1
Bromodichloromethane <2.6 ug/kg 12/09/15 22:05 75-27-46.7 2.6 1
Bromoform <3.1 ug/kg 12/09/15 22:05 75-25-26.7 3.1 1
Bromomethane <3.4 ug/kg 12/09/15 22:05 74-83-913.5 3.4 1
2-Butanone (MEK)<3.9 ug/kg 12/09/15 22:05 78-93-31353.9 1
n-Butylbenzene <2.4 ug/kg 12/09/15 22:05 104-51-86.7 2.4 1
sec-Butylbenzene <2.2 ug/kg 12/09/15 22:05 135-98-86.7 2.2 1
tert-Butylbenzene <2.7 ug/kg 12/09/15 22:05 98-06-66.7 2.7 1
Carbon tetrachloride <3.5 ug/kg 12/09/15 22:05 56-23-56.7 3.5 1
Chlorobenzene <2.6 ug/kg 12/09/15 22:05 108-90-76.7 2.6 1
Chloroethane <3.2 ug/kg 12/09/15 22:05 75-00-313.5 3.2 1
Chloroform <2.2 ug/kg 12/09/15 22:05 67-66-36.7 2.2 1
Chloromethane <3.2 ug/kg 12/09/15 22:05 74-87-313.5 3.2 1
2-Chlorotoluene <2.3 ug/kg 12/09/15 22:05 95-49-86.7 2.3 1
4-Chlorotoluene <2.4 ug/kg 12/09/15 22:05 106-43-46.7 2.4 1
1,2-Dibromo-3-chloropropane <4.9 ug/kg 12/09/15 22:05 96-12-86.7 4.9 1
Dibromochloromethane <2.4 ug/kg 12/09/15 22:05 124-48-16.7 2.4 1
1,2-Dibromoethane (EDB)<2.4 ug/kg 12/09/15 22:05 106-93-46.7 2.4 1
Dibromomethane <3.4 ug/kg 12/09/15 22:05 74-95-36.7 3.4 1
1,2-Dichlorobenzene <2.6 ug/kg 12/09/15 22:05 95-50-16.7 2.6 1
1,3-Dichlorobenzene <2.7 ug/kg 12/09/15 22:05 541-73-16.7 2.7 1
1,4-Dichlorobenzene <2.3 ug/kg 12/09/15 22:05 106-46-76.7 2.3 1
Dichlorodifluoromethane <4.9 ug/kg 12/09/15 22:05 75-71-813.5 4.9 1
1,1-Dichloroethane <2.0 ug/kg 12/09/15 22:05 75-34-36.7 2.0 1
1,2-Dichloroethane <3.0 ug/kg 12/09/15 22:05 107-06-26.7 3.0 1
1,1-Dichloroethene <2.4 ug/kg 12/09/15 22:05 75-35-46.7 2.4 1
cis-1,2-Dichloroethene <1.9 ug/kg 12/09/15 22:05 156-59-26.7 1.9 1
trans-1,2-Dichloroethene <2.6 ug/kg 12/09/15 22:05 156-60-56.7 2.6 1
1,2-Dichloropropane <2.3 ug/kg 12/09/15 22:05 78-87-56.7 2.3 1
1,3-Dichloropropane <2.6 ug/kg 12/09/15 22:05 142-28-96.7 2.6 1
2,2-Dichloropropane <2.3 ug/kg 12/09/15 22:05 594-20-76.7 2.3 1
1,1-Dichloropropene <2.0 ug/kg 12/09/15 22:05 563-58-66.7 2.0 1
cis-1,3-Dichloropropene <2.4 ug/kg 12/09/15 22:05 10061-01-56.7 2.4 1
trans-1,3-Dichloropropene <2.0 ug/kg 12/09/15 22:05 10061-02-66.7 2.0 1
Diisopropyl ether <2.3 ug/kg 12/09/15 22:05 108-20-36.7 2.3 1
Ethylbenzene <2.4 ug/kg 12/09/15 22:05 100-41-46.7 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 64
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92278649
PANTRY #3471
Sample:SD-13 Lab ID:92278649008 Collected:11/30/15 16:00 Received:12/07/15 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.7 ug/kg 12/09/15 22:05 87-68-36.7 2.7 1
2-Hexanone <5.3 ug/kg 12/09/15 22:05 591-78-667.4 5.3 1
Isopropylbenzene (Cumene)<2.6 ug/kg 12/09/15 22:05 98-82-86.7 2.6 1
p-Isopropyltoluene <2.3 ug/kg 12/09/15 22:05 99-87-66.7 2.3 1
Methylene Chloride 6.5J ug/kg 12/09/15 22:05 75-09-227.0 4.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/kg 12/09/15 22:05 108-10-167.4 5.0 1
Methyl-tert-butyl ether <2.0 ug/kg 12/09/15 22:05 1634-04-46.7 2.0 1
Naphthalene 4.0J ug/kg 12/09/15 22:05 91-20-3 B6.7 1.6 1
n-Propylbenzene <2.3 ug/kg 12/09/15 22:05 103-65-16.7 2.3 1
Styrene <2.4 ug/kg 12/09/15 22:05 100-42-56.7 2.4 1
1,1,1,2-Tetrachloroethane <2.8 ug/kg 12/09/15 22:05 630-20-66.7 2.8 1
1,1,2,2-Tetrachloroethane <2.6 ug/kg 12/09/15 22:05 79-34-56.7 2.6 1
Tetrachloroethene <2.3 ug/kg 12/09/15 22:05 127-18-46.7 2.3 1
Toluene <2.4 ug/kg 12/09/15 22:05 108-88-36.7 2.4 1
1,2,3-Trichlorobenzene <3.0 ug/kg 12/09/15 22:05 87-61-66.7 3.0 1
1,2,4-Trichlorobenzene <2.2 ug/kg 12/09/15 22:05 120-82-16.7 2.2 1
1,1,1-Trichloroethane <2.4 ug/kg 12/09/15 22:05 71-55-66.7 2.4 1
1,1,2-Trichloroethane <2.8 ug/kg 12/09/15 22:05 79-00-56.7 2.8 1
Trichloroethene <2.8 ug/kg 12/09/15 22:05 79-01-6 L36.7 2.8 1
Trichlorofluoromethane <3.0 ug/kg 12/09/15 22:05 75-69-46.7 3.0 1
1,2,3-Trichloropropane <2.2 ug/kg 12/09/15 22:05 96-18-46.7 2.2 1
1,2,4-Trimethylbenzene <2.7 ug/kg 12/09/15 22:05 95-63-66.7 2.7 1
1,3,5-Trimethylbenzene <2.4 ug/kg 12/09/15 22:05 108-67-86.7 2.4 1
Vinyl acetate <11.9 ug/kg 12/09/15 22:05 108-05-4 L267.4 11.9 1
Vinyl chloride <2.4 ug/kg 12/09/15 22:05 75-01-413.5 2.4 1
Xylene (Total)<4.9 ug/kg 12/09/15 22:05 1330-20-713.5 4.9 1
m&p-Xylene <4.9 ug/kg 12/09/15 22:05 179601-23-113.5 4.9 1
o-Xylene <2.6 ug/kg 12/09/15 22:05 95-47-66.7 2.6 1
Surrogates
Toluene-d8 (S)99 %12/09/15 22:05 2037-26-570-130 1
4-Bromofluorobenzene (S)102 %12/09/15 22:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %12/09/15 22:05 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.8 %12/08/15 11:240.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
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Page 39 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10195
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1630390
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg <2.5 2.5 N212/16/15 14:102.5
Aliphatic (C09-C12)mg/kg <2.5 2.5 N212/16/15 14:102.5
Aromatic (C09-C10)mg/kg <2.5 2.5 N212/16/15 14:102.5
4-Bromofluorobenzene (FID) (S)%98 70-130 12/16/15 14:10
4-Bromofluorobenzene (PID) (S)%97 70-130 12/16/15 14:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1630391LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1630392
Aliphatic (C05-C08)mg/kg 13.4 N2159070-1308913.3 1 25
Aliphatic (C09-C12)mg/kg 12.8 N2158530-1308813.3 4 25
Aromatic (C09-C10)mg/kg 4.9 N259770-130964.8 1 25
4-Bromofluorobenzene (FID) (S)%94 70-130101
4-Bromofluorobenzene (PID) (S)%95 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34588
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1622305
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg <1.9 4.6 12/08/15 12:341.9
1,1,1-Trichloroethane ug/kg <1.7 4.6 12/08/15 12:341.7
1,1,2,2-Tetrachloroethane ug/kg <1.8 4.6 12/08/15 12:341.8
1,1,2-Trichloroethane ug/kg <1.9 4.6 12/08/15 12:341.9
1,1-Dichloroethane ug/kg <1.4 4.6 12/08/15 12:341.4
1,1-Dichloroethene ug/kg <1.7 4.6 12/08/15 12:341.7
1,1-Dichloropropene ug/kg <1.4 4.6 12/08/15 12:341.4
1,2,3-Trichlorobenzene ug/kg <2.0 4.6 12/08/15 12:342.0
1,2,3-Trichloropropane ug/kg <1.5 4.6 12/08/15 12:341.5
1,2,4-Trichlorobenzene ug/kg <1.5 4.6 12/08/15 12:341.5
1,2,4-Trimethylbenzene ug/kg <1.8 4.6 12/08/15 12:341.8
1,2-Dibromo-3-chloropropane ug/kg <3.3 4.6 12/08/15 12:343.3
1,2-Dibromoethane (EDB)ug/kg <1.7 4.6 12/08/15 12:341.7
1,2-Dichlorobenzene ug/kg <1.8 4.6 12/08/15 12:341.8
1,2-Dichloroethane ug/kg <2.0 4.6 12/08/15 12:342.0
1,2-Dichloropropane ug/kg <1.6 4.6 12/08/15 12:341.6
1,3,5-Trimethylbenzene ug/kg <1.7 4.6 12/08/15 12:341.7
1,3-Dichlorobenzene ug/kg <1.8 4.6 12/08/15 12:341.8
1,3-Dichloropropane ug/kg <1.8 4.6 12/08/15 12:341.8
1,4-Dichlorobenzene ug/kg <1.6 4.6 12/08/15 12:341.6
2,2-Dichloropropane ug/kg <1.6 4.6 12/08/15 12:341.6
2-Butanone (MEK)ug/kg <2.7 92.4 12/08/15 12:342.7
2-Chlorotoluene ug/kg <1.6 4.6 12/08/15 12:341.6
2-Hexanone ug/kg <3.6 46.2 12/08/15 12:343.6
4-Chlorotoluene ug/kg <1.7 4.6 12/08/15 12:341.7
4-Methyl-2-pentanone (MIBK)ug/kg <3.4 46.2 12/08/15 12:343.4
Acetone ug/kg <9.2 92.4 12/08/15 12:349.2
Benzene ug/kg <1.5 4.6 12/08/15 12:341.5
Bromobenzene ug/kg <1.8 4.6 12/08/15 12:341.8
Bromochloromethane ug/kg <1.6 4.6 12/08/15 12:341.6
Bromodichloromethane ug/kg <1.8 4.6 12/08/15 12:341.8
Bromoform ug/kg <2.1 4.6 12/08/15 12:342.1
Bromomethane ug/kg <2.3 9.2 12/08/15 12:342.3
Carbon tetrachloride ug/kg <2.4 4.6 12/08/15 12:342.4
Chlorobenzene ug/kg <1.8 4.6 12/08/15 12:341.8
Chloroethane ug/kg <2.2 9.2 12/08/15 12:342.2
Chloroform ug/kg <1.5 4.6 12/08/15 12:341.5
Chloromethane ug/kg <2.2 9.2 12/08/15 12:342.2
cis-1,2-Dichloroethene ug/kg <1.3 4.6 12/08/15 12:341.3
cis-1,3-Dichloropropene ug/kg <1.7 4.6 12/08/15 12:341.7
Dibromochloromethane ug/kg <1.7 4.6 12/08/15 12:341.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1622305
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg <2.3 4.6 12/08/15 12:342.3
Dichlorodifluoromethane ug/kg <3.3 9.2 12/08/15 12:343.3
Diisopropyl ether ug/kg <1.6 4.6 12/08/15 12:341.6
Ethylbenzene ug/kg <1.7 4.6 12/08/15 12:341.7
Hexachloro-1,3-butadiene ug/kg <1.8 4.6 12/08/15 12:341.8
Isopropylbenzene (Cumene)ug/kg <1.8 4.6 12/08/15 12:341.8
m&p-Xylene ug/kg <3.3 9.2 12/08/15 12:343.3
Methyl-tert-butyl ether ug/kg <1.4 4.6 12/08/15 12:341.4
Methylene Chloride ug/kg <2.8 18.5 12/08/15 12:342.8
n-Butylbenzene ug/kg <1.7 4.6 12/08/15 12:341.7
n-Propylbenzene ug/kg <1.6 4.6 12/08/15 12:341.6
Naphthalene ug/kg 1.2J 4.6 12/08/15 12:341.1
o-Xylene ug/kg <1.8 4.6 12/08/15 12:341.8
p-Isopropyltoluene ug/kg <1.6 4.6 12/08/15 12:341.6
sec-Butylbenzene ug/kg <1.5 4.6 12/08/15 12:341.5
Styrene ug/kg <1.7 4.6 12/08/15 12:341.7
tert-Butylbenzene ug/kg <1.8 4.6 12/08/15 12:341.8
Tetrachloroethene ug/kg <1.6 4.6 12/08/15 12:341.6
Toluene ug/kg <1.7 4.6 12/08/15 12:341.7
trans-1,2-Dichloroethene ug/kg <1.8 4.6 12/08/15 12:341.8
trans-1,3-Dichloropropene ug/kg <1.4 4.6 12/08/15 12:341.4
Trichloroethene ug/kg <1.9 4.6 12/08/15 12:341.9
Trichlorofluoromethane ug/kg <2.0 4.6 12/08/15 12:342.0
Vinyl acetate ug/kg <8.1 46.2 12/08/15 12:348.1
Vinyl chloride ug/kg <1.7 9.2 12/08/15 12:341.7
Xylene (Total)ug/kg <3.3 9.2 12/08/15 12:343.3
1,2-Dichloroethane-d4 (S)%89 70-132 12/08/15 12:34
4-Bromofluorobenzene (S)%99 70-130 12/08/15 12:34
Toluene-d8 (S)%100 70-130 12/08/15 12:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1622306LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 53.955.1 98 74-137
1,1,1-Trichloroethane ug/kg 53.055.1 96 67-140
1,1,2,2-Tetrachloroethane ug/kg 56.655.1 103 72-141
1,1,2-Trichloroethane ug/kg 58.055.1 105 78-138
1,1-Dichloroethane ug/kg 55.955.1 102 69-134
1,1-Dichloroethene ug/kg 56.255.1 102 67-138
1,1-Dichloropropene ug/kg 59.455.1 108 69-139
1,2,3-Trichlorobenzene ug/kg 60.955.1 111 70-146
1,2,3-Trichloropropane ug/kg 63.355.1 115 69-144
1,2,4-Trichlorobenzene ug/kg 58.655.1 106 68-148
1,2,4-Trimethylbenzene ug/kg 58.355.1 106 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1622306LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 56.055.1 102 65-140
1,2-Dibromoethane (EDB)ug/kg 63.055.1 114 77-135
1,2-Dichlorobenzene ug/kg 59.255.1 108 77-141
1,2-Dichloroethane ug/kg 51.155.1 93 65-137
1,2-Dichloropropane ug/kg 56.655.1 103 72-136
1,3,5-Trimethylbenzene ug/kg 57.655.1 105 76-133
1,3-Dichlorobenzene ug/kg 60.655.1 110 74-138
1,3-Dichloropropane ug/kg 57.355.1 104 71-139
1,4-Dichlorobenzene ug/kg 59.455.1 108 76-138
2,2-Dichloropropane ug/kg 53.655.1 97 68-137
2-Butanone (MEK)ug/kg 103J110 94 58-147
2-Chlorotoluene ug/kg 57.755.1 105 73-139
2-Hexanone ug/kg 109110 99 62-145
4-Chlorotoluene ug/kg 57.055.1 103 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 112110 101 64-149
Acetone ug/kg 86.1J110 78 53-153
Benzene ug/kg 60.555.1 110 73-135
Bromobenzene ug/kg 55.655.1 101 75-133
Bromochloromethane ug/kg 51.955.1 94 73-134
Bromodichloromethane ug/kg 54.955.1 100 71-135
Bromoform ug/kg 52.855.1 96 66-141
Bromomethane ug/kg 63.155.1 115 53-160
Carbon tetrachloride ug/kg 54.555.1 99 60-145
Chlorobenzene ug/kg 60.055.1 109 78-130
Chloroethane ug/kg 60.155.1 109 64-149
Chloroform ug/kg 55.455.1 101 70-134
Chloromethane ug/kg 55.255.1 100 52-150
cis-1,2-Dichloroethene ug/kg 56.755.1 103 70-133
cis-1,3-Dichloropropene ug/kg 55.555.1 101 68-134
Dibromochloromethane ug/kg 58.255.1 106 71-138
Dibromomethane ug/kg 54.755.1 99 74-130
Dichlorodifluoromethane ug/kg 60.555.1 110 40-160
Diisopropyl ether ug/kg 53.655.1 97 69-141
Ethylbenzene ug/kg 57.455.1 104 75-133
Hexachloro-1,3-butadiene ug/kg 55.155.1 100 68-143
Isopropylbenzene (Cumene)ug/kg 63.155.1 115 76-143
m&p-Xylene ug/kg 112110 102 75-136
Methyl-tert-butyl ether ug/kg 54.455.1 99 68-144
Methylene Chloride ug/kg 55.355.1 100 45-154
n-Butylbenzene ug/kg 58.655.1 106 72-137
n-Propylbenzene ug/kg 57.155.1 104 76-136
Naphthalene ug/kg 63.855.1 116 68-151
o-Xylene ug/kg 57.655.1 105 76-141
p-Isopropyltoluene ug/kg 58.655.1 106 76-140
sec-Butylbenzene ug/kg 59.955.1 109 79-139
Styrene ug/kg 60.155.1 109 79-137
tert-Butylbenzene ug/kg 51.755.1 94 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1622306LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 57.255.1 104 71-138
Toluene ug/kg 58.855.1 107 74-131
trans-1,2-Dichloroethene ug/kg 57.955.1 105 67-135
trans-1,3-Dichloropropene ug/kg 52.855.1 96 65-146
Trichloroethene ug/kg 60.155.1 109 67-135
Trichlorofluoromethane ug/kg 52.255.1 95 59-144
Vinyl acetate ug/kg 96.1 F31108740-160
Vinyl chloride ug/kg 63.755.1 116 56-141
Xylene (Total)ug/kg 170165 103 76-137
1,2-Dichloroethane-d4 (S)%90 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1623588MATRIX SPIKE SAMPLE:
MSSpike
Result
92278649001
1,1,1,2-Tetrachloroethane ug/kg 22.522.6 100 70-130<2.7
1,1,1-Trichloroethane ug/kg 21.322.6 94 70-130<2.3
1,1,2,2-Tetrachloroethane ug/kg 25.822.6 114 70-130<2.4
1,1,2-Trichloroethane ug/kg 25.522.6 113 70-130<2.7
1,1-Dichloroethane ug/kg 21.822.6 96 70-130<1.9
1,1-Dichloroethene ug/kg 20.822.6 92 49-180<2.3
1,1-Dichloropropene ug/kg 24.322.6 108 70-130<1.9
1,2,3-Trichlorobenzene ug/kg 25.722.6 114 70-130<2.8
1,2,3-Trichloropropane ug/kg 25.422.6 112 70-130<2.0
1,2,4-Trichlorobenzene ug/kg 23.722.6 105 70-130<2.0
1,2,4-Trimethylbenzene ug/kg 24.222.6 107 70-130<2.6
1,2-Dibromo-3-chloropropane ug/kg 22.622.6 100 70-130<4.6
1,2-Dibromoethane (EDB)ug/kg 26.622.6 118 70-130<2.3
1,2-Dichlorobenzene ug/kg 25.522.6 113 70-130<2.4
1,2-Dichloroethane ug/kg 20.022.6 89 70-130<2.8
1,2-Dichloropropane ug/kg 24.022.6 106 70-130<2.2
1,3,5-Trimethylbenzene ug/kg 24.322.6 107 70-130<2.3
1,3-Dichlorobenzene ug/kg 24.922.6 110 70-130<2.6
1,3-Dichloropropane ug/kg 24.822.6 110 70-130<2.4
1,4-Dichlorobenzene ug/kg 25.122.6 111 70-130<2.2
2,2-Dichloropropane ug/kg 20.722.6 92 70-130<2.2
2-Butanone (MEK)ug/kg 44.5J45.2 98 70-130<3.7
2-Chlorotoluene ug/kg 23.422.6 104 70-130<2.2
2-Hexanone ug/kg 44.5J45.2 98 70-130<5.0
4-Chlorotoluene ug/kg 23.722.6 105 70-130<2.3
4-Methyl-2-pentanone (MIBK)ug/kg 47.3J45.2 105 70-130<4.7
Acetone ug/kg 68.2J45.2 81 70-13031.7J
Benzene ug/kg 25.122.6 111 50-166<2.0
Bromobenzene ug/kg 22.922.6 101 70-130<2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1623588MATRIX SPIKE SAMPLE:
MSSpike
Result
92278649001
Bromochloromethane ug/kg 22.522.6 99 70-130<2.2
Bromodichloromethane ug/kg 22.322.6 99 70-130<2.4
Bromoform ug/kg 21.922.6 97 70-130<2.9
Bromomethane ug/kg 25.322.6 112 70-130<3.2
Carbon tetrachloride ug/kg 21.922.6 97 70-130<3.3
Chlorobenzene ug/kg 25.322.6 112 43-169<2.4
Chloroethane ug/kg 23.722.6 105 70-130<3.1
Chloroform ug/kg 22.022.6 97 70-130<2.0
Chloromethane ug/kg 21.022.6 93 70-130<3.1
cis-1,2-Dichloroethene ug/kg 22.922.6 101 70-130<1.8
cis-1,3-Dichloropropene ug/kg 23.522.6 104 70-130<2.3
Dibromochloromethane ug/kg 22.822.6 101 70-130<2.3
Dibromomethane ug/kg 23.422.6 103 70-130<3.2
Dichlorodifluoromethane ug/kg 19.622.6 87 70-130<4.6
Diisopropyl ether ug/kg 22.222.6 98 70-130<2.2
Ethylbenzene ug/kg 24.422.6 108 70-130<2.3
Hexachloro-1,3-butadiene ug/kg 22.522.6 99 70-130<2.6
Isopropylbenzene (Cumene)ug/kg 27.422.6 121 70-130<2.4
m&p-Xylene ug/kg 49.145.2 108 70-130<4.6
Methyl-tert-butyl ether ug/kg 22.222.6 98 70-130<1.9
Methylene Chloride ug/kg 29.122.6 110 70-1304.3J
n-Butylbenzene ug/kg 25.522.6 113 70-130<2.3
n-Propylbenzene ug/kg 24.622.6 109 70-130<2.2
Naphthalene ug/kg 27.022.6 120 70-130<1.5
o-Xylene ug/kg 23.922.6 106 70-130<2.4
p-Isopropyltoluene ug/kg 24.922.6 110 70-130<2.2
sec-Butylbenzene ug/kg 26.122.6 116 70-130<2.0
Styrene ug/kg 25.422.6 112 70-130<2.3
tert-Butylbenzene ug/kg 21.622.6 96 70-130<2.6
Tetrachloroethene ug/kg 23.822.6 105 70-130<2.2
Toluene ug/kg 25.822.6 111 52-163<2.3
trans-1,2-Dichloroethene ug/kg 23.122.6 102 70-130<2.4
trans-1,3-Dichloropropene ug/kg 21.122.6 94 70-130<1.9
Trichloroethene ug/kg 25.222.6 111 49-167<2.7
Trichlorofluoromethane ug/kg 19.222.6 85 70-130<2.8
Vinyl acetate ug/kg 49.2J45.2 109 70-130<11.2
Vinyl chloride ug/kg 24.822.6 110 70-130<2.3
1,2-Dichloroethane-d4 (S)%90 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278215008
1623587SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg <1.7 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278215008
1623587SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg <1.4 30ND
1,1,2,2-Tetrachloroethane ug/kg <1.5 30ND
1,1,2-Trichloroethane ug/kg <1.7 30ND
1,1-Dichloroethane ug/kg <1.2 30ND
1,1-Dichloroethene ug/kg <1.4 30ND
1,1-Dichloropropene ug/kg <1.2 30ND
1,2,3-Trichlorobenzene ug/kg <1.7 30ND
1,2,3-Trichloropropane ug/kg <1.3 30ND
1,2,4-Trichlorobenzene ug/kg <1.3 30ND
1,2,4-Trimethylbenzene ug/kg <1.6 30ND
1,2-Dibromo-3-chloropropane ug/kg <2.8 30ND
1,2-Dibromoethane (EDB)ug/kg <1.4 30ND
1,2-Dichlorobenzene ug/kg <1.5 30ND
1,2-Dichloroethane ug/kg <1.7 30ND
1,2-Dichloropropane ug/kg <1.3 30ND
1,3,5-Trimethylbenzene ug/kg <1.4 30ND
1,3-Dichlorobenzene ug/kg <1.6 30ND
1,3-Dichloropropane ug/kg <1.5 30ND
1,4-Dichlorobenzene ug/kg <1.3 30ND
2,2-Dichloropropane ug/kg <1.3 30ND
2-Butanone (MEK)ug/kg <2.3 30ND
2-Chlorotoluene ug/kg <1.3 30ND
2-Hexanone ug/kg <3.1 30ND
4-Chlorotoluene ug/kg <1.4 30ND
4-Methyl-2-pentanone (MIBK)ug/kg <2.9 30ND
Acetone ug/kg <7.9 30ND
Benzene ug/kg <1.3 30ND
Bromobenzene ug/kg <1.6 30ND
Bromochloromethane ug/kg <1.3 30ND
Bromodichloromethane ug/kg <1.5 30ND
Bromoform ug/kg <1.8 30ND
Bromomethane ug/kg <2.0 30ND
Carbon tetrachloride ug/kg <2.1 30ND
Chlorobenzene ug/kg <1.5 30ND
Chloroethane ug/kg <1.9 30ND
Chloroform ug/kg <1.3 30ND
Chloromethane ug/kg <1.9 30ND
cis-1,2-Dichloroethene ug/kg <1.1 30ND
cis-1,3-Dichloropropene ug/kg <1.4 30ND
Dibromochloromethane ug/kg <1.4 30ND
Dibromomethane ug/kg <2.0 30ND
Dichlorodifluoromethane ug/kg <2.8 30ND
Diisopropyl ether ug/kg <1.3 30ND
Ethylbenzene ug/kg <1.4 30ND
Hexachloro-1,3-butadiene ug/kg <1.6 30ND
Isopropylbenzene (Cumene)ug/kg <1.5 30ND
m&p-Xylene ug/kg <2.8 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
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[phone]
Page 46 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278215008
1623587SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg <1.2 30ND
Methylene Chloride ug/kg <2.4 30ND
n-Butylbenzene ug/kg <1.4 30ND
n-Propylbenzene ug/kg <1.3 30ND
Naphthalene ug/kg <0.95 30ND
o-Xylene ug/kg <1.5 30ND
p-Isopropyltoluene ug/kg <1.3 30ND
sec-Butylbenzene ug/kg <1.3 30ND
Styrene ug/kg <1.4 30ND
tert-Butylbenzene ug/kg <1.6 30ND
Tetrachloroethene ug/kg <1.3 30ND
Toluene ug/kg <1.4 30ND
trans-1,2-Dichloroethene ug/kg <1.5 30ND
trans-1,3-Dichloropropene ug/kg <1.2 30ND
Trichloroethene ug/kg <1.7 30ND
Trichlorofluoromethane ug/kg <1.7 30ND
Vinyl acetate ug/kg <7.0 30ND
Vinyl chloride ug/kg <1.4 30ND
Xylene (Total)ug/kg <2.8 30ND
1,2-Dichloroethane-d4 (S)%86 491
4-Bromofluorobenzene (S)%92 396
Toluene-d8 (S)%99 199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34610
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92278649008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1623905
Associated Lab Samples:92278649008
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg <2.4 5.8 12/09/15 21:062.4
1,1,1-Trichloroethane ug/kg <2.1 5.8 12/09/15 21:062.1
1,1,2,2-Tetrachloroethane ug/kg <2.2 5.8 12/09/15 21:062.2
1,1,2-Trichloroethane ug/kg <2.4 5.8 12/09/15 21:062.4
1,1-Dichloroethane ug/kg <1.7 5.8 12/09/15 21:061.7
1,1-Dichloroethene ug/kg <2.1 5.8 12/09/15 21:062.1
1,1-Dichloropropene ug/kg <1.7 5.8 12/09/15 21:061.7
1,2,3-Trichlorobenzene ug/kg <2.6 5.8 12/09/15 21:062.6
1,2,3-Trichloropropane ug/kg <1.9 5.8 12/09/15 21:061.9
1,2,4-Trichlorobenzene ug/kg <1.9 5.8 12/09/15 21:061.9
1,2,4-Trimethylbenzene ug/kg <2.3 5.8 12/09/15 21:062.3
1,2-Dibromo-3-chloropropane ug/kg <4.2 5.8 12/09/15 21:064.2
1,2-Dibromoethane (EDB)ug/kg <2.1 5.8 12/09/15 21:062.1
1,2-Dichlorobenzene ug/kg <2.2 5.8 12/09/15 21:062.2
1,2-Dichloroethane ug/kg <2.6 5.8 12/09/15 21:062.6
1,2-Dichloropropane ug/kg <2.0 5.8 12/09/15 21:062.0
1,3,5-Trimethylbenzene ug/kg <2.1 5.8 12/09/15 21:062.1
1,3-Dichlorobenzene ug/kg <2.3 5.8 12/09/15 21:062.3
1,3-Dichloropropane ug/kg <2.2 5.8 12/09/15 21:062.2
1,4-Dichlorobenzene ug/kg <2.0 5.8 12/09/15 21:062.0
2,2-Dichloropropane ug/kg <2.0 5.8 12/09/15 21:062.0
2-Butanone (MEK)ug/kg <3.4 116 12/09/15 21:063.4
2-Chlorotoluene ug/kg <2.0 5.8 12/09/15 21:062.0
2-Hexanone ug/kg <4.5 58.0 12/09/15 21:064.5
4-Chlorotoluene ug/kg <2.1 5.8 12/09/15 21:062.1
4-Methyl-2-pentanone (MIBK)ug/kg <4.3 58.0 12/09/15 21:064.3
Acetone ug/kg <11.6 116 12/09/15 21:0611.6
Benzene ug/kg <1.9 5.8 12/09/15 21:061.9
Bromobenzene ug/kg <2.3 5.8 12/09/15 21:062.3
Bromochloromethane ug/kg <2.0 5.8 12/09/15 21:062.0
Bromodichloromethane ug/kg <2.2 5.8 12/09/15 21:062.2
Bromoform ug/kg <2.7 5.8 12/09/15 21:062.7
Bromomethane ug/kg <2.9 11.6 12/09/15 21:062.9
Carbon tetrachloride ug/kg <3.0 5.8 12/09/15 21:063.0
Chlorobenzene ug/kg <2.2 5.8 12/09/15 21:062.2
Chloroethane ug/kg <2.8 11.6 12/09/15 21:062.8
Chloroform ug/kg <1.9 5.8 12/09/15 21:061.9
Chloromethane ug/kg <2.8 11.6 12/09/15 21:062.8
cis-1,2-Dichloroethene ug/kg <1.6 5.8 12/09/15 21:061.6
cis-1,3-Dichloropropene ug/kg <2.1 5.8 12/09/15 21:062.1
Dibromochloromethane ug/kg <2.1 5.8 12/09/15 21:062.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1623905
Associated Lab Samples:92278649008
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg <2.9 5.8 12/09/15 21:062.9
Dichlorodifluoromethane ug/kg <4.2 11.6 12/09/15 21:064.2
Diisopropyl ether ug/kg <2.0 5.8 12/09/15 21:062.0
Ethylbenzene ug/kg <2.1 5.8 12/09/15 21:062.1
Hexachloro-1,3-butadiene ug/kg <2.3 5.8 12/09/15 21:062.3
Isopropylbenzene (Cumene)ug/kg <2.2 5.8 12/09/15 21:062.2
m&p-Xylene ug/kg <4.2 11.6 12/09/15 21:064.2
Methyl-tert-butyl ether ug/kg <1.7 5.8 12/09/15 21:061.7
Methylene Chloride ug/kg <3.5 23.2 12/09/15 21:063.5
n-Butylbenzene ug/kg <2.1 5.8 12/09/15 21:062.1
n-Propylbenzene ug/kg <2.0 5.8 12/09/15 21:062.0
Naphthalene ug/kg 2.1J 5.8 12/09/15 21:061.4
o-Xylene ug/kg <2.2 5.8 12/09/15 21:062.2
p-Isopropyltoluene ug/kg <2.0 5.8 12/09/15 21:062.0
sec-Butylbenzene ug/kg <1.9 5.8 12/09/15 21:061.9
Styrene ug/kg <2.1 5.8 12/09/15 21:062.1
tert-Butylbenzene ug/kg <2.3 5.8 12/09/15 21:062.3
Tetrachloroethene ug/kg <2.0 5.8 12/09/15 21:062.0
Toluene ug/kg <2.1 5.8 12/09/15 21:062.1
trans-1,2-Dichloroethene ug/kg <2.2 5.8 12/09/15 21:062.2
trans-1,3-Dichloropropene ug/kg <1.7 5.8 12/09/15 21:061.7
Trichloroethene ug/kg <2.4 5.8 12/09/15 21:062.4
Trichlorofluoromethane ug/kg <2.6 5.8 12/09/15 21:062.6
Vinyl acetate ug/kg <10.2 58.0 12/09/15 21:0610.2
Vinyl chloride ug/kg <2.1 11.6 12/09/15 21:062.1
Xylene (Total)ug/kg <4.2 11.6 12/09/15 21:064.2
1,2-Dichloroethane-d4 (S)%89 70-132 12/09/15 21:06
4-Bromofluorobenzene (S)%97 70-130 12/09/15 21:06
Toluene-d8 (S)%99 70-130 12/09/15 21:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1623906LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 58.650.5 116 74-137
1,1,1-Trichloroethane ug/kg 49.650.5 98 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.350.5 92 72-141
1,1,2-Trichloroethane ug/kg 60.150.5 119 78-138
1,1-Dichloroethane ug/kg 51.550.5 102 69-134
1,1-Dichloroethene ug/kg 54.150.5 107 67-138
1,1-Dichloropropene ug/kg 56.050.5 111 69-139
1,2,3-Trichlorobenzene ug/kg 62.250.5 123 70-146
1,2,3-Trichloropropane ug/kg 61.750.5 122 69-144
1,2,4-Trichlorobenzene ug/kg 56.150.5 111 68-148
1,2,4-Trimethylbenzene ug/kg 58.450.5 116 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1623906LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 57.050.5 113 65-140
1,2-Dibromoethane (EDB)ug/kg 62.450.5 123 77-135
1,2-Dichlorobenzene ug/kg 62.850.5 124 77-141
1,2-Dichloroethane ug/kg 48.150.5 95 65-137
1,2-Dichloropropane ug/kg 56.550.5 112 72-136
1,3,5-Trimethylbenzene ug/kg 57.950.5 115 76-133
1,3-Dichlorobenzene ug/kg 60.450.5 120 74-138
1,3-Dichloropropane ug/kg 59.450.5 118 71-139
1,4-Dichlorobenzene ug/kg 60.850.5 120 76-138
2,2-Dichloropropane ug/kg 48.350.5 96 68-137
2-Butanone (MEK)ug/kg 103101 102 58-147
2-Chlorotoluene ug/kg 57.950.5 115 73-139
2-Hexanone ug/kg 116101 115 62-145
4-Chlorotoluene ug/kg 56.950.5 113 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 118101 117 64-149
Acetone ug/kg 88.0J101 87 53-153
Benzene ug/kg 57.650.5 114 73-135
Bromobenzene ug/kg 56.850.5 112 75-133
Bromochloromethane ug/kg 56.550.5 112 73-134
Bromodichloromethane ug/kg 53.950.5 107 71-135
Bromoform ug/kg 55.550.5 110 66-141
Bromomethane ug/kg 58.550.5 116 53-160
Carbon tetrachloride ug/kg 50.650.5 100 60-145
Chlorobenzene ug/kg 60.050.5 119 78-130
Chloroethane ug/kg 54.750.5 108 64-149
Chloroform ug/kg 52.550.5 104 70-134
Chloromethane ug/kg 51.550.5 102 52-150
cis-1,2-Dichloroethene ug/kg 53.550.5 106 70-133
cis-1,3-Dichloropropene ug/kg 55.250.5 109 68-134
Dibromochloromethane ug/kg 60.250.5 119 71-138
Dibromomethane ug/kg 54.850.5 108 74-130
Dichlorodifluoromethane ug/kg 53.550.5 106 40-160
Diisopropyl ether ug/kg 51.850.5 103 69-141
Ethylbenzene ug/kg 56.050.5 111 75-133
Hexachloro-1,3-butadiene ug/kg 53.550.5 106 68-143
Isopropylbenzene (Cumene)ug/kg 63.550.5 126 76-143
m&p-Xylene ug/kg 111101 110 75-136
Methyl-tert-butyl ether ug/kg 53.650.5 106 68-144
Methylene Chloride ug/kg 50.750.5 100 45-154
n-Butylbenzene ug/kg 58.250.5 115 72-137
n-Propylbenzene ug/kg 56.850.5 113 76-136
Naphthalene ug/kg 67.250.5 133 68-151
o-Xylene ug/kg 57.750.5 114 76-141
p-Isopropyltoluene ug/kg 59.150.5 117 76-140
sec-Butylbenzene ug/kg 61.150.5 121 79-139
Styrene ug/kg 63.050.5 125 79-137
tert-Butylbenzene ug/kg 53.050.5 105 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1623906LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 52.650.5 104 71-138
Toluene ug/kg 56.650.5 112 74-131
trans-1,2-Dichloroethene ug/kg 53.850.5 107 67-135
trans-1,3-Dichloropropene ug/kg 53.750.5 106 65-146
Trichloroethene ug/kg 69.8 L050.5 138 67-135
Trichlorofluoromethane ug/kg 47.450.5 94 59-144
Vinyl acetate ug/kg 27.2J F3,L01012740-160
Vinyl chloride ug/kg 60.650.5 120 56-141
Xylene (Total)ug/kg 169152 112 76-137
1,2-Dichloroethane-d4 (S)%89 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39529
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1621770
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg <64.0 330 12/08/15 20:5264.0
1,2-Dichlorobenzene ug/kg <88.0 330 12/08/15 20:5288.0
1,3-Dichlorobenzene ug/kg <75.0 330 12/08/15 20:5275.0
1,4-Dichlorobenzene ug/kg <93.0 330 12/08/15 20:5293.0
1-Methylnaphthalene ug/kg <86.0 330 12/08/15 20:5286.0
2,4,5-Trichlorophenol ug/kg <102 330 12/08/15 20:52102
2,4,6-Trichlorophenol ug/kg <73.0 330 12/08/15 20:5273.0
2,4-Dichlorophenol ug/kg <72.0 330 12/08/15 20:5272.0
2,4-Dimethylphenol ug/kg <130 330 12/08/15 20:52130
2,4-Dinitrophenol ug/kg <54.0 1650 12/08/15 20:5254.0
2,4-Dinitrotoluene ug/kg <62.0 330 12/08/15 20:5262.0
2,6-Dinitrotoluene ug/kg <69.0 330 12/08/15 20:5269.0
2-Chloronaphthalene ug/kg <65.0 330 12/08/15 20:5265.0
2-Chlorophenol ug/kg <90.0 330 12/08/15 20:5290.0
2-Methylnaphthalene ug/kg <71.0 330 12/08/15 20:5271.0
2-Methylphenol(o-Cresol)ug/kg <100 330 12/08/15 20:52100
2-Nitroaniline ug/kg <102 1650 12/08/15 20:52102
2-Nitrophenol ug/kg <80.0 330 12/08/15 20:5280.0
3&4-Methylphenol(m&p Cresol)ug/kg <130 330 12/08/15 20:52130
3,3'-Dichlorobenzidine ug/kg <72.0 1650 12/08/15 20:5272.0
3-Nitroaniline ug/kg <90.0 1650 12/08/15 20:5290.0
4,6-Dinitro-2-methylphenol ug/kg <66.0 660 12/08/15 20:5266.0
4-Bromophenylphenyl ether ug/kg <60.0 330 12/08/15 20:5260.0
4-Chloro-3-methylphenol ug/kg <68.0 660 12/08/15 20:5268.0
4-Chloroaniline ug/kg <92.0 1650 12/08/15 20:5292.0
4-Chlorophenylphenyl ether ug/kg <68.0 330 12/08/15 20:5268.0
4-Nitroaniline ug/kg <93.0 660 12/08/15 20:5293.0
4-Nitrophenol ug/kg <59.0 1650 12/08/15 20:5259.0
Acenaphthene ug/kg <76.0 330 12/08/15 20:5276.0
Acenaphthylene ug/kg <78.0 330 12/08/15 20:5278.0
Aniline ug/kg <89.0 330 12/08/15 20:5289.0
Anthracene ug/kg <74.0 330 12/08/15 20:5274.0
Benzo(a)anthracene ug/kg <61.0 330 12/08/15 20:5261.0
Benzo(a)pyrene ug/kg <63.0 330 12/08/15 20:5263.0
Benzo(b)fluoranthene ug/kg <57.0 330 12/08/15 20:5257.0
Benzo(g,h,i)perylene ug/kg <84.0 330 12/08/15 20:5284.0
Benzo(k)fluoranthene ug/kg <65.0 330 12/08/15 20:5265.0
Benzoic Acid ug/kg <60.0 1650 12/08/15 20:5260.0
Benzyl alcohol ug/kg <66.0 660 12/08/15 20:5266.0
bis(2-Chloroethoxy)methane ug/kg <77.0 330 12/08/15 20:5277.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1621770
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg <84.0 330 12/08/15 20:5284.0
bis(2-Chloroisopropyl) ether ug/kg <88.0 330 12/08/15 20:5288.0
bis(2-Ethylhexyl)phthalate ug/kg <90.0 330 12/08/15 20:5290.0
Butylbenzylphthalate ug/kg <70.0 330 12/08/15 20:5270.0
Chrysene ug/kg <44.0 330 12/08/15 20:5244.0
Di-n-butylphthalate ug/kg <54.0 330 12/08/15 20:5254.0
Di-n-octylphthalate ug/kg <69.0 330 12/08/15 20:5269.0
Dibenz(a,h)anthracene ug/kg <70.0 330 12/08/15 20:5270.0
Dibenzofuran ug/kg <54.0 330 12/08/15 20:5254.0
Diethylphthalate ug/kg <51.0 330 12/08/15 20:5251.0
Dimethylphthalate ug/kg <67.0 330 12/08/15 20:5267.0
Fluoranthene ug/kg <48.0 330 12/08/15 20:5248.0
Fluorene ug/kg <68.0 330 12/08/15 20:5268.0
Hexachloro-1,3-butadiene ug/kg <57.0 330 12/08/15 20:5257.0
Hexachlorobenzene ug/kg <42.0 330 12/08/15 20:5242.0
Hexachlorocyclopentadiene ug/kg <61.0 330 12/08/15 20:5261.0
Hexachloroethane ug/kg <87.0 330 12/08/15 20:5287.0
Indeno(1,2,3-cd)pyrene ug/kg <68.0 330 12/08/15 20:5268.0
Isophorone ug/kg <74.0 330 12/08/15 20:5274.0
N-Nitroso-di-n-propylamine ug/kg <63.0 330 12/08/15 20:5263.0
N-Nitrosodimethylamine ug/kg <107 330 12/08/15 20:52107
N-Nitrosodiphenylamine ug/kg <98.0 330 12/08/15 20:5298.0
Naphthalene ug/kg <81.0 330 12/08/15 20:5281.0
Nitrobenzene ug/kg <90.0 330 12/08/15 20:5290.0
Pentachlorophenol ug/kg <60.0 1650 12/08/15 20:5260.0
Phenanthrene ug/kg <55.0 330 12/08/15 20:5255.0
Phenol ug/kg <99.0 330 12/08/15 20:5299.0
Pyrene ug/kg <56.0 330 12/08/15 20:5256.0
2,4,6-Tribromophenol (S)%83 27-110 12/08/15 20:52
2-Fluorobiphenyl (S)%81 30-110 12/08/15 20:52
2-Fluorophenol (S)%68 13-110 12/08/15 20:52
Nitrobenzene-d5 (S)%77 23-110 12/08/15 20:52
Phenol-d6 (S)%72 22-110 12/08/15 20:52
Terphenyl-d14 (S)%91 28-110 12/08/15 20:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621771LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12701670 76 36-120
1,2-Dichlorobenzene ug/kg 13301670 80 41-120
1,3-Dichlorobenzene ug/kg 12801670 77 66-120
1,4-Dichlorobenzene ug/kg 12901670 78 42-120
1-Methylnaphthalene ug/kg 14301670 86 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621771LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/kg 15501670 93 37-120
2,4,6-Trichlorophenol ug/kg 14601670 88 40-120
2,4-Dichlorophenol ug/kg 14701670 88 33-120
2,4-Dimethylphenol ug/kg 14001670 84 36-120
2,4-Dinitrophenol ug/kg 78408330 94 22-121
2,4-Dinitrotoluene ug/kg 16201670 97 60-120
2,6-Dinitrotoluene ug/kg 15901670 95 54-120
2-Chloronaphthalene ug/kg 14001670 84 41-120
2-Chlorophenol ug/kg 14301670 86 39-120
2-Methylnaphthalene ug/kg 13701670 82 26-120
2-Methylphenol(o-Cresol)ug/kg 16901670 101 41-120
2-Nitroaniline ug/kg 26403330 79 45-120
2-Nitrophenol ug/kg 14601670 87 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 16001670 96 35-120
3,3'-Dichlorobenzidine ug/kg 26203330 79 16-125
3-Nitroaniline ug/kg 27703330 83 45-120
4,6-Dinitro-2-methylphenol ug/kg 30703330 92 46-120
4-Bromophenylphenyl ether ug/kg 13801670 83 36-120
4-Chloro-3-methylphenol ug/kg 30803330 92 37-120
4-Chloroaniline ug/kg 24103330 72 35-120
4-Chlorophenylphenyl ether ug/kg 13001670 78 30-120
4-Nitroaniline ug/kg 31503330 95 48-120
4-Nitrophenol ug/kg 75208330 90 43-120
Acenaphthene ug/kg 14801670 89 46-120
Acenaphthylene ug/kg 15501670 93 46-120
Aniline ug/kg 11801670 71 33-120
Anthracene ug/kg 15701670 94 63-120
Benzo(a)anthracene ug/kg 15001670 90 61-120
Benzo(a)pyrene ug/kg 15301670 92 59-120
Benzo(b)fluoranthene ug/kg 14601670 88 55-120
Benzo(g,h,i)perylene ug/kg 13401670 81 57-120
Benzo(k)fluoranthene ug/kg 17701670 106 56-120
Benzoic Acid ug/kg 66808330 80 13-120
Benzyl alcohol ug/kg 29703330 89 34-120
bis(2-Chloroethoxy)methane ug/kg 12401670 74 21-120
bis(2-Chloroethyl) ether ug/kg 11901670 72 25-120
bis(2-Chloroisopropyl) ether ug/kg 10301670 62 13-120
bis(2-Ethylhexyl)phthalate ug/kg 17001670 102 56-123
Butylbenzylphthalate ug/kg 17401670 105 57-120
Chrysene ug/kg 14701670 88 64-120
Di-n-butylphthalate ug/kg 17601670 105 58-120
Di-n-octylphthalate ug/kg 14901670 89 47-121
Dibenz(a,h)anthracene ug/kg 13501670 81 56-120
Dibenzofuran ug/kg 14401670 86 43-120
Diethylphthalate ug/kg 15501670 93 55-120
Dimethylphthalate ug/kg 14901670 89 54-120
Fluoranthene ug/kg 15901670 96 61-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1621771LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 15701670 94 51-120
Hexachloro-1,3-butadiene ug/kg 12501670 75 22-120
Hexachlorobenzene ug/kg 15401670 92 53-120
Hexachlorocyclopentadiene ug/kg 10301670 62 18-150
Hexachloroethane ug/kg 13301670 80 39-120
Indeno(1,2,3-cd)pyrene ug/kg 13701670 82 58-120
Isophorone ug/kg 13301670 80 38-120
N-Nitroso-di-n-propylamine ug/kg 13801670 83 30-120
N-Nitrosodimethylamine ug/kg 11601670 70 32-120
N-Nitrosodiphenylamine ug/kg 14301670 86 50-120
Naphthalene ug/kg 13501670 81 38-120
Nitrobenzene ug/kg 12301670 74 37-120
Pentachlorophenol ug/kg 27603330 83 10-120
Phenanthrene ug/kg 14401670 86 62-120
Phenol ug/kg 15101670 91 37-120
Pyrene ug/kg 16201670 97 63-120
2,4,6-Tribromophenol (S)%91 27-110
2-Fluorobiphenyl (S)%82 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%77 23-110
Phenol-d6 (S)%86 22-110
Terphenyl-d14 (S)%87 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621772MATRIX SPIKE SAMPLE:
MSSpike
Result
92278649001
1,2,4-Trichlorobenzene ug/kg 13301760 76 18-119<67.3
1,2-Dichlorobenzene ug/kg 12601760 72 50-110<92.5
1,3-Dichlorobenzene ug/kg 12301760 70 27-110<78.9
1,4-Dichlorobenzene ug/kg 12101760 69 28-110<97.8
1-Methylnaphthalene ug/kg 13301760 76 24-116<90.4
2,4,5-Trichlorophenol ug/kg 13901760 79 28-110<107
2,4,6-Trichlorophenol ug/kg 14101760 81 17-117<76.8
2,4-Dichlorophenol ug/kg 13301760 76 21-128<75.7
2,4-Dimethylphenol ug/kg 13301760 76 10-120<137
2,4-Dinitrophenol ug/kg 61208760 70 10-107<56.8
2,4-Dinitrotoluene ug/kg 12801760 73 36-109<65.2
2,6-Dinitrotoluene ug/kg 12601760 72 32-110<72.6
2-Chloronaphthalene ug/kg 13101760 75 30-107<68.4
2-Chlorophenol ug/kg 12801760 73 14-106<94.6
2-Methylnaphthalene ug/kg 12901760 74 10-135<74.7
2-Methylphenol(o-Cresol)ug/kg 12701760 72 10-124<105
2-Nitroaniline ug/kg 1720J3500 49 26-116<107
2-Nitrophenol ug/kg 12801760 73 28-103<84.1
3&4-Methylphenol(m&p Cresol)ug/kg 11501760 66 10-109<137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621772MATRIX SPIKE SAMPLE:
MSSpike
Result
92278649001
3,3'-Dichlorobenzidine ug/kg 25003500 71 10-150<75.7
3-Nitroaniline ug/kg 22303500 64 22-110<94.6
4,6-Dinitro-2-methylphenol ug/kg 27303500 78 13-121<69.4
4-Bromophenylphenyl ether ug/kg 12801760 73 31-109<63.1
4-Chloro-3-methylphenol ug/kg 26003500 74 13-128<71.5
4-Chloroaniline ug/kg 21603500 62 18-102<96.7
4-Chlorophenylphenyl ether ug/kg 12901760 74 29-112<71.5
4-Nitroaniline ug/kg 22603500 64 16-111<97.8
4-Nitrophenol ug/kg 51608760 59 14-135<62.0
Acenaphthene ug/kg 12401760 71 26-114<79.9
Acenaphthylene ug/kg 13301760 76 32-108<82.0
Aniline ug/kg 8721760 50 10-107<93.6
Anthracene ug/kg 13501760 77 32-111<77.8
Benzo(a)anthracene ug/kg 14501760 83 25-117<64.1
Benzo(a)pyrene ug/kg 13401760 76 25-106<66.2
Benzo(b)fluoranthene ug/kg 13501760 77 24-110<59.9
Benzo(g,h,i)perylene ug/kg 13201760 76 19-112<88.3
Benzo(k)fluoranthene ug/kg 15801760 90 24-114<68.4
Benzoic Acid ug/kg 50708760 58 10-110<63.1
Benzyl alcohol ug/kg 21703500 62 24-106<69.4
bis(2-Chloroethoxy)methane ug/kg 10401760 59 13-119<81.0
bis(2-Chloroethyl) ether ug/kg 9991760 57 10-134<88.3
bis(2-Chloroisopropyl) ether ug/kg 5721760 33 10-113<92.5
bis(2-Ethylhexyl)phthalate ug/kg 15001760 86 10-125<94.6
Butylbenzylphthalate ug/kg 15301760 87 18-110<73.6
Chrysene ug/kg 13601760 78 30-110<46.3
Di-n-butylphthalate ug/kg 13801760 79 19-112<56.8
Di-n-octylphthalate ug/kg 16601760 94 17-105<72.6
Dibenz(a,h)anthracene ug/kg 13701760 78 23-111<73.6
Dibenzofuran ug/kg 12301760 70 35-103<56.8
Diethylphthalate ug/kg 12901760 74 27-113<53.6
Dimethylphthalate ug/kg 12801760 73 26-111<70.5
Fluoranthene ug/kg 13601760 78 33-109<50.5
Fluorene ug/kg 13301760 76 32-113<71.5
Hexachloro-1,3-butadiene ug/kg 13601760 78 16-116<59.9
Hexachlorobenzene ug/kg 14501760 83 27-120<44.2
Hexachlorocyclopentadiene ug/kg 11701760 67 10-108<64.1
Hexachloroethane ug/kg 12001760 68 10-117<91.5
Indeno(1,2,3-cd)pyrene ug/kg 13501760 77 10-122<71.5
Isophorone ug/kg 9661760 55 28-114<77.8
N-Nitroso-di-n-propylamine ug/kg 9341760 53 27-113<66.2
N-Nitrosodimethylamine ug/kg 8931760 51 10-109<113
N-Nitrosodiphenylamine ug/kg 12201760 69 10-128<103
Naphthalene ug/kg 12501760 71 25-110<85.2
Nitrobenzene ug/kg 9601760 55 18-114<94.6
Pentachlorophenol ug/kg 23103500 66 10-122<63.1
Phenanthrene ug/kg 12601760 72 30-114<57.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1621772MATRIX SPIKE SAMPLE:
MSSpike
Result
92278649001
Phenol ug/kg 11801760 68 11-102<104
Pyrene ug/kg 13601760 78 25-116<58.9
2,4,6-Tribromophenol (S)%77 27-110
2-Fluorobiphenyl (S)%70 30-110
2-Fluorophenol (S)%63 13-110
Nitrobenzene-d5 (S)%59 23-110
Phenol-d6 (S)%66 22-110
Terphenyl-d14 (S)%75 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278649002
1621773SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg <66.5 30<66.5
1,2-Dichlorobenzene ug/kg <91.5 30<91.5
1,3-Dichlorobenzene ug/kg <78.0 30<78.0
1,4-Dichlorobenzene ug/kg <96.7 30<96.7
1-Methylnaphthalene ug/kg <89.4 30<89.4
2,4,5-Trichlorophenol ug/kg <106 30<106
2,4,6-Trichlorophenol ug/kg <75.9 30<75.9
2,4-Dichlorophenol ug/kg <74.9 30<74.9
2,4-Dimethylphenol ug/kg <135 30<135
2,4-Dinitrophenol ug/kg <56.1 30<56.1
2,4-Dinitrotoluene ug/kg <64.5 30<64.5
2,6-Dinitrotoluene ug/kg <71.7 30<71.7
2-Chloronaphthalene ug/kg <67.6 30<67.6
2-Chlorophenol ug/kg <93.6 30<93.6
2-Methylnaphthalene ug/kg <73.8 30<73.8
2-Methylphenol(o-Cresol)ug/kg <104 30<104
2-Nitroaniline ug/kg <106 30<106
2-Nitrophenol ug/kg <83.2 30<83.2
3&4-Methylphenol(m&p Cresol)ug/kg <135 30<135
3,3'-Dichlorobenzidine ug/kg <74.9 30<74.9
3-Nitroaniline ug/kg <93.6 30<93.6
4,6-Dinitro-2-methylphenol ug/kg <68.6 30<68.6
4-Bromophenylphenyl ether ug/kg <62.4 30<62.4
4-Chloro-3-methylphenol ug/kg <70.7 30<70.7
4-Chloroaniline ug/kg <95.7 30<95.7
4-Chlorophenylphenyl ether ug/kg <70.7 30<70.7
4-Nitroaniline ug/kg <96.7 30<96.7
4-Nitrophenol ug/kg <61.3 30<61.3
Acenaphthene ug/kg <79.0 30<79.0
Acenaphthylene ug/kg <81.1 30<81.1
Aniline ug/kg <92.5 30<92.5
Anthracene ug/kg <76.9 30<76.9
Benzo(a)anthracene ug/kg <63.4 30<63.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278649002
1621773SAMPLE DUPLICATE:
Benzo(a)pyrene ug/kg <65.5 30<65.5
Benzo(b)fluoranthene ug/kg <59.3 30<59.3
Benzo(g,h,i)perylene ug/kg <87.3 30<87.3
Benzo(k)fluoranthene ug/kg <67.6 30<67.6
Benzoic Acid ug/kg <62.4 30<62.4
Benzyl alcohol ug/kg <68.6 30<68.6
bis(2-Chloroethoxy)methane ug/kg <80.1 30<80.1
bis(2-Chloroethyl) ether ug/kg <87.3 30<87.3
bis(2-Chloroisopropyl) ether ug/kg <91.5 30<91.5
bis(2-Ethylhexyl)phthalate ug/kg <93.6 30<93.6
Butylbenzylphthalate ug/kg <72.8 30<72.8
Chrysene ug/kg <45.7 30<45.7
Di-n-butylphthalate ug/kg <56.1 30<56.1
Di-n-octylphthalate ug/kg <71.7 30<71.7
Dibenz(a,h)anthracene ug/kg <72.8 30<72.8
Dibenzofuran ug/kg <56.1 30<56.1
Diethylphthalate ug/kg <53.0 30<53.0
Dimethylphthalate ug/kg <69.7 30<69.7
Fluoranthene ug/kg 70.1J 3080.4J
Fluorene ug/kg <70.7 30<70.7
Hexachloro-1,3-butadiene ug/kg <59.3 30<59.3
Hexachlorobenzene ug/kg <43.7 30<43.7
Hexachlorocyclopentadiene ug/kg <63.4 30<63.4
Hexachloroethane ug/kg <90.5 30<90.5
Indeno(1,2,3-cd)pyrene ug/kg <70.7 30<70.7
Isophorone ug/kg <76.9 30<76.9
N-Nitroso-di-n-propylamine ug/kg <65.5 30<65.5
N-Nitrosodimethylamine ug/kg <111 30<111
N-Nitrosodiphenylamine ug/kg <102 30<102
Naphthalene ug/kg <84.2 30<84.2
Nitrobenzene ug/kg <93.6 30<93.6
Pentachlorophenol ug/kg <62.4 30<62.4
Phenanthrene ug/kg <57.2 3058.5J
Phenol ug/kg <103 30<103
Pyrene ug/kg 60.4J 3068.7J
2,4,6-Tribromophenol (S)%80 786
2-Fluorobiphenyl (S)%78 783
2-Fluorophenol (S)%69 673
Nitrobenzene-d5 (S)%75 982
Phenol-d6 (S)%73 073
Terphenyl-d14 (S)%89 694
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39607
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1625001
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg <10.0 10.0 N212/11/15 21:3110.0
Aliphatic (C19-C36)mg/kg <10.0 10.0 N212/11/15 21:3110.0
Aromatic (C11-C22)mg/kg <10.0 10.0 N212/14/15 23:2310.0
2-Bromonaphthalene (S)%83 40-140 12/14/15 23:23
2-Fluorobiphenyl (S)%85 40-140 12/14/15 23:23
Nonatriacontane (S)%104 40-140 12/11/15 21:31
o-Terphenyl (S)%77 40-140 12/14/15 23:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1625002LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1625003
Aliphatic (C09-C18)mg/kg <10.0 N2108140-14071<10.0 50
Aliphatic (C19-C36)mg/kg 13.1 N213.3 98 40-1408611.5 13 50
Aromatic (C11-C22)mg/kg 20.4 N228.3 72 40-1408925.2 21 50
2-Bromonaphthalene (S)%83 40-140100
2-Fluorobiphenyl (S)%85 40-14099
Nonatriacontane (S)%S014240-14091
o-Terphenyl (S)%77 40-14089
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 64
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92278649
PANTRY #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8630
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92278649001, 92278649002, 92278649003, 92278649004, 92278649005, 92278649006, 92278649007,
92278649008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278337001
1621776SAMPLE DUPLICATE:
Percent Moisture %11.7 6 2512.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92278651001
1621777SAMPLE DUPLICATE:
Percent Moisture %26.5 0 2526.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 64
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92278649
PANTRY #3471
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
The lab does not hold TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
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Page 61 of 64
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92278649
PANTRY #3471
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92278649001 OEXT/39607 GCSV/23518SD-19 MADEP EPH MADEP EPH
92278649002 OEXT/39607 GCSV/23518SD-25 MADEP EPH MADEP EPH
92278649003 OEXT/39607 GCSV/23518SD-26 MADEP EPH MADEP EPH
92278649004 OEXT/39607 GCSV/23518SK-30 MADEP EPH MADEP EPH
92278649005 OEXT/39607 GCSV/23518SK-25 MADEP EPH MADEP EPH
92278649006 OEXT/39607 GCSV/23518SD-10 MADEP EPH MADEP EPH
92278649007 OEXT/39607 GCSV/23518SD-11 MADEP EPH MADEP EPH
92278649008 OEXT/39607 GCSV/23518SD-13 MADEP EPH MADEP EPH
92278649001 GCV/10195 GCV/10197SD-19 MADEP VPH MADEP VPH
92278649002 GCV/10195 GCV/10197SD-25 MADEP VPH MADEP VPH
92278649003 GCV/10195 GCV/10197SD-26 MADEP VPH MADEP VPH
92278649004 GCV/10195 GCV/10197SK-30 MADEP VPH MADEP VPH
92278649005 GCV/10195 GCV/10197SK-25 MADEP VPH MADEP VPH
92278649006 GCV/10195 GCV/10197SD-10 MADEP VPH MADEP VPH
92278649007 GCV/10195 GCV/10197SD-11 MADEP VPH MADEP VPH
92278649008 GCV/10195 GCV/10197SD-13 MADEP VPH MADEP VPH
92278649001 OEXT/39529 MSSV/11615SD-19 EPA 3546 EPA 8270
92278649002 OEXT/39529 MSSV/11615SD-25 EPA 3546 EPA 8270
92278649003 OEXT/39529 MSSV/11615SD-26 EPA 3546 EPA 8270
92278649004 OEXT/39529 MSSV/11615SK-30 EPA 3546 EPA 8270
92278649005 OEXT/39529 MSSV/11615SK-25 EPA 3546 EPA 8270
92278649006 OEXT/39529 MSSV/11615SD-10 EPA 3546 EPA 8270
92278649007 OEXT/39529 MSSV/11615SD-11 EPA 3546 EPA 8270
92278649008 OEXT/39529 MSSV/11615SD-13 EPA 3546 EPA 8270
92278649001 MSV/34588SD-19 EPA 8260
92278649002 MSV/34588SD-25 EPA 8260
92278649003 MSV/34588SD-26 EPA 8260
92278649004 MSV/34588SK-30 EPA 8260
92278649005 MSV/34588SK-25 EPA 8260
92278649006 MSV/34588SD-10 EPA 8260
92278649007 MSV/34588SD-11 EPA 8260
92278649008 MSV/34610SD-13 EPA 8260
92278649001 PMST/8630SD-19 ASTM D2974-87
92278649002 PMST/8630SD-25 ASTM D2974-87
92278649003 PMST/8630SD-26 ASTM D2974-87
92278649004 PMST/8630SK-30 ASTM D2974-87
92278649005 PMST/8630SK-25 ASTM D2974-87
92278649006 PMST/8630SD-10 ASTM D2974-87
92278649007 PMST/8630SD-11 ASTM D2974-87
92278649008 PMST/8630SD-13 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/22/2015 08:14 AM
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Page 62 of 64
Page 63 of 64
Page 64 of 64
Page 1 of 15
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
16A1082-01 5
Sample Preparation Information 7
QC Data 8
Volatile Organic Compounds by GC/MS 8
B141130 8
Flag/Qualifier Summary 12
Certifications 13
Chain of Custody/Sample Receipt 15
Page 2 of 15
Table of Contents
Page 3 of 15
Table of Contents
Page 4 of 15
Table of Contents
Page 5 of 15
Table of Contents
Page 6 of 15
Table of Contents
Page 7 of 15
Table of Contents
Page 8 of 15
Table of Contents
Page 9 of 15
Table of Contents
Page 10 of 15
Table of Contents
Page 11 of 15
Table of Contents
Page 12 of 15
Table of Contents
Page 13 of 15
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Table of Contents
#=CL#
December 15, 2015
LIMS USE: FR - MAUREEN JACKSON
LIMS OBJECT ID: 92277686
92277686
Project:
Pace Project No.:
RE:
Maureen Jackson
Cardno AtC
2725 E. Millbrook Road
Suite 121
Raleigh, NC 27604
Pantry #3471
Dear Maureen Jackson:
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92277686
Pantry #3471
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 2 of 27
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92277686
Pantry #3471
Lab ID Sample ID Matrix Date Collected Date Received
92277686001 SD-17 Solid 11/20/15 17:00 11/25/15 11:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92277686
Pantry #3471
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92277686001 SD-17 MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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Page 4 of 27
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92277686
Pantry #3471
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92277686001 SD-17
Aliphatic (C09-C18)44.9 mg/kg 12/07/15 19:03 N211.5MADEP EPH
Aromatic (C11-C22)22.4 mg/kg 12/07/15 19:03 N211.5MADEP EPH
Acetone 51.7J ug/kg 12/01/15 23:47122EPA 8260
Methylene Chloride 12.6J ug/kg 12/01/15 23:4724.4EPA 8260
Percent Moisture 13.0 %12/01/15 11:470.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277686
Pantry #3471
Sample:SD-17 Lab ID:92277686001 Collected:11/20/15 17:00 Received:11/25/15 11:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)44.9 mg/kg 12/07/15 19:03 N212/04/15 09:0011.5 11.5 1
Aliphatic (C19-C36)<11.5 mg/kg 12/07/15 19:03 N212/04/15 09:0011.5 11.5 1
Aromatic (C11-C22)22.4 mg/kg 12/07/15 19:03 N212/04/15 09:0011.5 11.5 1
Surrogates
Nonatriacontane (S)62 %12/07/15 19:03 7194-86-712/04/15 09:0040-140 1
o-Terphenyl (S)76 %12/07/15 19:03 84-15-112/04/15 09:0040-140 1
2-Fluorobiphenyl (S)99 %12/07/15 19:03 321-60-812/04/15 09:0040-140 1
2-Bromonaphthalene (S)122 %12/07/15 19:03 580-13-212/04/15 09:0040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)<2.6 mg/kg 12/15/15 04:40 N212/14/15 17:402.6 2.6 1
Aliphatic (C09-C12)<2.6 mg/kg 12/15/15 04:40 N212/14/15 17:402.6 2.6 1
Aromatic (C09-C10)<2.6 mg/kg 12/15/15 04:40 N212/14/15 17:402.6 2.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)94 %12/15/15 04:40 460-00-412/14/15 17:4070-130 1
4-Bromofluorobenzene (PID) (S)89 %12/15/15 04:40 460-00-412/14/15 17:4070-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene <87.3 ug/kg 12/02/15 13:35 83-32-912/02/15 07:0537987.3 1
Acenaphthylene <89.6 ug/kg 12/02/15 13:35 208-96-812/02/15 07:0537989.6 1
Aniline <102 ug/kg 12/02/15 13:35 62-53-312/02/15 07:053791021
Anthracene <85.0 ug/kg 12/02/15 13:35 120-12-712/02/15 07:0537985.0 1
Benzo(a)anthracene <70.1 ug/kg 12/02/15 13:35 56-55-312/02/15 07:0537970.1 1
Benzo(a)pyrene <72.4 ug/kg 12/02/15 13:35 50-32-812/02/15 07:0537972.4 1
Benzo(b)fluoranthene <65.5 ug/kg 12/02/15 13:35 205-99-212/02/15 07:0537965.5 1
Benzo(g,h,i)perylene <96.5 ug/kg 12/02/15 13:35 191-24-212/02/15 07:0537996.5 1
Benzo(k)fluoranthene <74.7 ug/kg 12/02/15 13:35 207-08-912/02/15 07:0537974.7 1
Benzoic Acid <68.9 ug/kg 12/02/15 13:35 65-85-012/02/15 07:05190068.9 1
Benzyl alcohol <75.8 ug/kg 12/02/15 13:35 100-51-612/02/15 07:0575875.8 1
4-Bromophenylphenyl ether <68.9 ug/kg 12/02/15 13:35 101-55-312/02/15 07:0537968.9 1
Butylbenzylphthalate <80.4 ug/kg 12/02/15 13:35 85-68-712/02/15 07:0537980.4 1
4-Chloro-3-methylphenol <78.1 ug/kg 12/02/15 13:35 59-50-712/02/15 07:0575878.1 1
4-Chloroaniline <106 ug/kg 12/02/15 13:35 106-47-812/02/15 07:0519001061
bis(2-Chloroethoxy)methane <88.5 ug/kg 12/02/15 13:35 111-91-112/02/15 07:0537988.5 1
bis(2-Chloroethyl) ether <96.5 ug/kg 12/02/15 13:35 111-44-412/02/15 07:0537996.5 1
bis(2-Chloroisopropyl) ether <101 ug/kg 12/02/15 13:35 108-60-112/02/15 07:053791011
2-Chloronaphthalene <74.7 ug/kg 12/02/15 13:35 91-58-712/02/15 07:0537974.7 1
2-Chlorophenol <103 ug/kg 12/02/15 13:35 95-57-812/02/15 07:053791031
4-Chlorophenylphenyl ether <78.1 ug/kg 12/02/15 13:35 7005-72-312/02/15 07:0537978.1 1
Chrysene <50.6 ug/kg 12/02/15 13:35 218-01-912/02/15 07:0537950.6 1
Dibenz(a,h)anthracene <80.4 ug/kg 12/02/15 13:35 53-70-312/02/15 07:0537980.4 1
Dibenzofuran <62.0 ug/kg 12/02/15 13:35 132-64-912/02/15 07:0537962.0 1
1,2-Dichlorobenzene <101 ug/kg 12/02/15 13:35 95-50-112/02/15 07:053791011
1,3-Dichlorobenzene <86.2 ug/kg 12/02/15 13:35 541-73-112/02/15 07:0537986.2 1
1,4-Dichlorobenzene <107 ug/kg 12/02/15 13:35 106-46-712/02/15 07:053791071
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 6 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277686
Pantry #3471
Sample:SD-17 Lab ID:92277686001 Collected:11/20/15 17:00 Received:11/25/15 11:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine <82.7 ug/kg 12/02/15 13:35 91-94-112/02/15 07:05190082.7 1
2,4-Dichlorophenol <82.7 ug/kg 12/02/15 13:35 120-83-212/02/15 07:0537982.7 1
Diethylphthalate <58.6 ug/kg 12/02/15 13:35 84-66-212/02/15 07:0537958.6 1
2,4-Dimethylphenol <149 ug/kg 12/02/15 13:35 105-67-912/02/15 07:053791491
Dimethylphthalate <77.0 ug/kg 12/02/15 13:35 131-11-312/02/15 07:0537977.0 1
Di-n-butylphthalate <62.0 ug/kg 12/02/15 13:35 84-74-212/02/15 07:0537962.0 1
4,6-Dinitro-2-methylphenol <75.8 ug/kg 12/02/15 13:35 534-52-112/02/15 07:0575875.8 1
2,4-Dinitrophenol <62.0 ug/kg 12/02/15 13:35 51-28-512/02/15 07:05190062.0 1
2,4-Dinitrotoluene <71.2 ug/kg 12/02/15 13:35 121-14-212/02/15 07:0537971.2 1
2,6-Dinitrotoluene <79.3 ug/kg 12/02/15 13:35 606-20-212/02/15 07:0537979.3 1
Di-n-octylphthalate <79.3 ug/kg 12/02/15 13:35 117-84-012/02/15 07:0537979.3 1
bis(2-Ethylhexyl)phthalate <103 ug/kg 12/02/15 13:35 117-81-712/02/15 07:053791031
Fluoranthene <55.2 ug/kg 12/02/15 13:35 206-44-012/02/15 07:0537955.2 1
Fluorene <78.1 ug/kg 12/02/15 13:35 86-73-712/02/15 07:0537978.1 1
Hexachloro-1,3-butadiene <65.5 ug/kg 12/02/15 13:35 87-68-312/02/15 07:0537965.5 1
Hexachlorobenzene <48.3 ug/kg 12/02/15 13:35 118-74-112/02/15 07:0537948.3 1
Hexachlorocyclopentadiene <70.1 ug/kg 12/02/15 13:35 77-47-412/02/15 07:0537970.1 1
Hexachloroethane <100 ug/kg 12/02/15 13:35 67-72-112/02/15 07:053791001
Indeno(1,2,3-cd)pyrene <78.1 ug/kg 12/02/15 13:35 193-39-512/02/15 07:0537978.1 1
Isophorone <85.0 ug/kg 12/02/15 13:35 78-59-112/02/15 07:0537985.0 1
1-Methylnaphthalene <98.8 ug/kg 12/02/15 13:35 90-12-012/02/15 07:0537998.8 1
2-Methylnaphthalene <81.6 ug/kg 12/02/15 13:35 91-57-612/02/15 07:0537981.6 1
2-Methylphenol(o-Cresol)<115 ug/kg 12/02/15 13:35 95-48-712/02/15 07:053791151
3&4-Methylphenol(m&p Cresol)<149 ug/kg 12/02/15 13:3512/02/15 07:053791491
Naphthalene <93.1 ug/kg 12/02/15 13:35 91-20-312/02/15 07:0537993.1 1
2-Nitroaniline <117 ug/kg 12/02/15 13:35 88-74-412/02/15 07:0519001171
3-Nitroaniline <103 ug/kg 12/02/15 13:35 99-09-212/02/15 07:0519001031
4-Nitroaniline <107 ug/kg 12/02/15 13:35 100-01-612/02/15 07:057581071
Nitrobenzene <103 ug/kg 12/02/15 13:35 98-95-312/02/15 07:053791031
2-Nitrophenol <91.9 ug/kg 12/02/15 13:35 88-75-512/02/15 07:0537991.9 1
4-Nitrophenol <67.8 ug/kg 12/02/15 13:35 100-02-712/02/15 07:05190067.8 1
N-Nitrosodimethylamine <123 ug/kg 12/02/15 13:35 62-75-912/02/15 07:053791231
N-Nitroso-di-n-propylamine <72.4 ug/kg 12/02/15 13:35 621-64-712/02/15 07:0537972.4 1
N-Nitrosodiphenylamine <113 ug/kg 12/02/15 13:35 86-30-612/02/15 07:053791131
Pentachlorophenol <68.9 ug/kg 12/02/15 13:35 87-86-512/02/15 07:05190068.9 1
Phenanthrene <63.2 ug/kg 12/02/15 13:35 85-01-812/02/15 07:0537963.2 1
Phenol <114 ug/kg 12/02/15 13:35 108-95-212/02/15 07:053791141
Pyrene <64.3 ug/kg 12/02/15 13:35 129-00-012/02/15 07:0537964.3 1
1,2,4-Trichlorobenzene <73.5 ug/kg 12/02/15 13:35 120-82-112/02/15 07:0537973.5 1
2,4,5-Trichlorophenol <117 ug/kg 12/02/15 13:35 95-95-412/02/15 07:053791171
2,4,6-Trichlorophenol <83.9 ug/kg 12/02/15 13:35 88-06-212/02/15 07:0537983.9 1
Surrogates
Nitrobenzene-d5 (S)79 %12/02/15 13:35 4165-60-012/02/15 07:0523-110 1
2-Fluorobiphenyl (S)75 %12/02/15 13:35 321-60-812/02/15 07:0530-110 1
Terphenyl-d14 (S)81 %12/02/15 13:35 1718-51-012/02/15 07:0528-110 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277686
Pantry #3471
Sample:SD-17 Lab ID:92277686001 Collected:11/20/15 17:00 Received:11/25/15 11:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)67 %12/02/15 13:35 13127-88-312/02/15 07:0522-110 1
2-Fluorophenol (S)65 %12/02/15 13:35 367-12-412/02/15 07:0513-110 1
2,4,6-Tribromophenol (S)86 %12/02/15 13:35 118-79-612/02/15 07:0527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 51.7J ug/kg 12/01/15 23:47 67-64-112212.2 1
Benzene <2.0 ug/kg 12/01/15 23:47 71-43-26.1 2.0 1
Bromobenzene <2.4 ug/kg 12/01/15 23:47 108-86-16.1 2.4 1
Bromochloromethane <2.1 ug/kg 12/01/15 23:47 74-97-56.1 2.1 1
Bromodichloromethane <2.3 ug/kg 12/01/15 23:47 75-27-46.1 2.3 1
Bromoform <2.8 ug/kg 12/01/15 23:47 75-25-26.1 2.8 1
Bromomethane <3.1 ug/kg 12/01/15 23:47 74-83-912.2 3.1 1
2-Butanone (MEK)<3.5 ug/kg 12/01/15 23:47 78-93-31223.5 1
n-Butylbenzene <2.2 ug/kg 12/01/15 23:47 104-51-86.1 2.2 1
sec-Butylbenzene <2.0 ug/kg 12/01/15 23:47 135-98-86.1 2.0 1
tert-Butylbenzene <2.4 ug/kg 12/01/15 23:47 98-06-66.1 2.4 1
Carbon tetrachloride <3.2 ug/kg 12/01/15 23:47 56-23-56.1 3.2 1
Chlorobenzene <2.3 ug/kg 12/01/15 23:47 108-90-76.1 2.3 1
Chloroethane <2.9 ug/kg 12/01/15 23:47 75-00-312.2 2.9 1
Chloroform <2.0 ug/kg 12/01/15 23:47 67-66-36.1 2.0 1
Chloromethane <2.9 ug/kg 12/01/15 23:47 74-87-312.2 2.9 1
2-Chlorotoluene <2.1 ug/kg 12/01/15 23:47 95-49-86.1 2.1 1
4-Chlorotoluene <2.2 ug/kg 12/01/15 23:47 106-43-46.1 2.2 1
1,2-Dibromo-3-chloropropane <4.4 ug/kg 12/01/15 23:47 96-12-86.1 4.4 1
Dibromochloromethane <2.2 ug/kg 12/01/15 23:47 124-48-16.1 2.2 1
1,2-Dibromoethane (EDB)<2.2 ug/kg 12/01/15 23:47 106-93-46.1 2.2 1
Dibromomethane <3.1 ug/kg 12/01/15 23:47 74-95-36.1 3.1 1
1,2-Dichlorobenzene <2.3 ug/kg 12/01/15 23:47 95-50-16.1 2.3 1
1,3-Dichlorobenzene <2.4 ug/kg 12/01/15 23:47 541-73-16.1 2.4 1
1,4-Dichlorobenzene <2.1 ug/kg 12/01/15 23:47 106-46-76.1 2.1 1
Dichlorodifluoromethane <4.4 ug/kg 12/01/15 23:47 75-71-812.2 4.4 1
1,1-Dichloroethane <1.8 ug/kg 12/01/15 23:47 75-34-36.1 1.8 1
1,2-Dichloroethane <2.7 ug/kg 12/01/15 23:47 107-06-26.1 2.7 1
1,1-Dichloroethene <2.2 ug/kg 12/01/15 23:47 75-35-46.1 2.2 1
cis-1,2-Dichloroethene <1.7 ug/kg 12/01/15 23:47 156-59-26.1 1.7 1
trans-1,2-Dichloroethene <2.3 ug/kg 12/01/15 23:47 156-60-56.1 2.3 1
1,2-Dichloropropane <2.1 ug/kg 12/01/15 23:47 78-87-56.1 2.1 1
1,3-Dichloropropane <2.3 ug/kg 12/01/15 23:47 142-28-96.1 2.3 1
2,2-Dichloropropane <2.1 ug/kg 12/01/15 23:47 594-20-76.1 2.1 1
1,1-Dichloropropene <1.8 ug/kg 12/01/15 23:47 563-58-66.1 1.8 1
cis-1,3-Dichloropropene <2.2 ug/kg 12/01/15 23:47 10061-01-56.1 2.2 1
trans-1,3-Dichloropropene <1.8 ug/kg 12/01/15 23:47 10061-02-66.1 1.8 1
Diisopropyl ether <2.1 ug/kg 12/01/15 23:47 108-20-36.1 2.1 1
Ethylbenzene <2.2 ug/kg 12/01/15 23:47 100-41-46.1 2.2 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92277686
Pantry #3471
Sample:SD-17 Lab ID:92277686001 Collected:11/20/15 17:00 Received:11/25/15 11:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene <2.4 ug/kg 12/01/15 23:47 87-68-36.1 2.4 1
2-Hexanone <4.8 ug/kg 12/01/15 23:47 591-78-661.1 4.8 1
Isopropylbenzene (Cumene)<2.3 ug/kg 12/01/15 23:47 98-82-86.1 2.3 1
p-Isopropyltoluene <2.1 ug/kg 12/01/15 23:47 99-87-66.1 2.1 1
Methylene Chloride 12.6J ug/kg 12/01/15 23:47 75-09-224.4 3.7 1
4-Methyl-2-pentanone (MIBK)<4.5 ug/kg 12/01/15 23:47 108-10-161.1 4.5 1
Methyl-tert-butyl ether <1.8 ug/kg 12/01/15 23:47 1634-04-46.1 1.8 1
Naphthalene <1.5 ug/kg 12/01/15 23:47 91-20-36.1 1.5 1
n-Propylbenzene <2.1 ug/kg 12/01/15 23:47 103-65-16.1 2.1 1
Styrene <2.2 ug/kg 12/01/15 23:47 100-42-56.1 2.2 1
1,1,1,2-Tetrachloroethane <2.6 ug/kg 12/01/15 23:47 630-20-66.1 2.6 1
1,1,2,2-Tetrachloroethane <2.3 ug/kg 12/01/15 23:47 79-34-56.1 2.3 1
Tetrachloroethene <2.1 ug/kg 12/01/15 23:47 127-18-46.1 2.1 1
Toluene <2.2 ug/kg 12/01/15 23:47 108-88-36.1 2.2 1
1,2,3-Trichlorobenzene <2.7 ug/kg 12/01/15 23:47 87-61-66.1 2.7 1
1,2,4-Trichlorobenzene <2.0 ug/kg 12/01/15 23:47 120-82-16.1 2.0 1
1,1,1-Trichloroethane <2.2 ug/kg 12/01/15 23:47 71-55-66.1 2.2 1
1,1,2-Trichloroethane <2.6 ug/kg 12/01/15 23:47 79-00-56.1 2.6 1
Trichloroethene <2.6 ug/kg 12/01/15 23:47 79-01-66.1 2.6 1
Trichlorofluoromethane <2.7 ug/kg 12/01/15 23:47 75-69-46.1 2.7 1
1,2,3-Trichloropropane <2.0 ug/kg 12/01/15 23:47 96-18-46.1 2.0 1
1,2,4-Trimethylbenzene <2.4 ug/kg 12/01/15 23:47 95-63-66.1 2.4 1
1,3,5-Trimethylbenzene <2.2 ug/kg 12/01/15 23:47 108-67-86.1 2.2 1
Vinyl acetate <10.8 ug/kg 12/01/15 23:47 108-05-461.1 10.8 1
Vinyl chloride <2.2 ug/kg 12/01/15 23:47 75-01-412.2 2.2 1
Xylene (Total)<4.4 ug/kg 12/01/15 23:47 1330-20-712.2 4.4 1
m&p-Xylene <4.4 ug/kg 12/01/15 23:47 179601-23-112.2 4.4 1
o-Xylene <2.3 ug/kg 12/01/15 23:47 95-47-66.1 2.3 1
Surrogates
Toluene-d8 (S)113 %12/01/15 23:47 2037-26-570-130 1
4-Bromofluorobenzene (S)102 %12/01/15 23:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)115 %12/01/15 23:47 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.0 %12/01/15 11:470.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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Page 9 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10183
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92277686001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1628781
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg <2.5 2.5 N212/14/15 19:362.5
Aliphatic (C09-C12)mg/kg <2.5 2.5 N212/14/15 19:362.5
Aromatic (C09-C10)mg/kg <2.5 2.5 N212/14/15 19:362.5
4-Bromofluorobenzene (FID) (S)%92 70-130 12/14/15 19:36
4-Bromofluorobenzene (PID) (S)%89 70-130 12/14/15 19:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1628782LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1628783
Aliphatic (C05-C08)mg/kg 13.2 N2158870-1308713.1 1 25
Aliphatic (C09-C12)mg/kg 13.8 N2159230-1309013.5 2 25
Aromatic (C09-C10)mg/kg 4.8 N259670-130954.7 1 25
4-Bromofluorobenzene (FID) (S)%97 70-13096
4-Bromofluorobenzene (PID) (S)%96 70-13095
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 10 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34494
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92277686001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617170
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg <2.5 5.9 12/01/15 13:162.5
1,1,1-Trichloroethane ug/kg <2.1 5.9 12/01/15 13:162.1
1,1,2,2-Tetrachloroethane ug/kg <2.2 5.9 12/01/15 13:162.2
1,1,2-Trichloroethane ug/kg <2.5 5.9 12/01/15 13:162.5
1,1-Dichloroethane ug/kg <1.8 5.9 12/01/15 13:161.8
1,1-Dichloroethene ug/kg <2.1 5.9 12/01/15 13:162.1
1,1-Dichloropropene ug/kg <1.8 5.9 12/01/15 13:161.8
1,2,3-Trichlorobenzene ug/kg <2.6 5.9 12/01/15 13:162.6
1,2,3-Trichloropropane ug/kg <1.9 5.9 12/01/15 13:161.9
1,2,4-Trichlorobenzene ug/kg <1.9 5.9 12/01/15 13:161.9
1,2,4-Trimethylbenzene ug/kg <2.3 5.9 12/01/15 13:162.3
1,2-Dibromo-3-chloropropane ug/kg <4.2 5.9 12/01/15 13:164.2
1,2-Dibromoethane (EDB)ug/kg <2.1 5.9 12/01/15 13:162.1
1,2-Dichlorobenzene ug/kg <2.2 5.9 12/01/15 13:162.2
1,2-Dichloroethane ug/kg <2.6 5.9 12/01/15 13:162.6
1,2-Dichloropropane ug/kg <2.0 5.9 12/01/15 13:162.0
1,3,5-Trimethylbenzene ug/kg <2.1 5.9 12/01/15 13:162.1
1,3-Dichlorobenzene ug/kg <2.3 5.9 12/01/15 13:162.3
1,3-Dichloropropane ug/kg <2.2 5.9 12/01/15 13:162.2
1,4-Dichlorobenzene ug/kg <2.0 5.9 12/01/15 13:162.0
2,2-Dichloropropane ug/kg <2.0 5.9 12/01/15 13:162.0
2-Butanone (MEK)ug/kg <3.4 117 12/01/15 13:163.4
2-Chlorotoluene ug/kg <2.0 5.9 12/01/15 13:162.0
2-Hexanone ug/kg <4.6 58.5 12/01/15 13:164.6
4-Chlorotoluene ug/kg <2.1 5.9 12/01/15 13:162.1
4-Methyl-2-pentanone (MIBK)ug/kg <4.3 58.5 12/01/15 13:164.3
Acetone ug/kg <11.7 117 12/01/15 13:1611.7
Benzene ug/kg <1.9 5.9 12/01/15 13:161.9
Bromobenzene ug/kg <2.3 5.9 12/01/15 13:162.3
Bromochloromethane ug/kg <2.0 5.9 12/01/15 13:162.0
Bromodichloromethane ug/kg <2.2 5.9 12/01/15 13:162.2
Bromoform ug/kg <2.7 5.9 12/01/15 13:162.7
Bromomethane ug/kg <2.9 11.7 12/01/15 13:162.9
Carbon tetrachloride ug/kg <3.0 5.9 12/01/15 13:163.0
Chlorobenzene ug/kg <2.2 5.9 12/01/15 13:162.2
Chloroethane ug/kg <2.8 11.7 12/01/15 13:162.8
Chloroform ug/kg <1.9 5.9 12/01/15 13:161.9
Chloromethane ug/kg <2.8 11.7 12/01/15 13:162.8
cis-1,2-Dichloroethene ug/kg <1.6 5.9 12/01/15 13:161.6
cis-1,3-Dichloropropene ug/kg <2.1 5.9 12/01/15 13:162.1
Dibromochloromethane ug/kg <2.1 5.9 12/01/15 13:162.1
REPORT OF LABORATORY ANALYSIS
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Page 11 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617170
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg <2.9 5.9 12/01/15 13:162.9
Dichlorodifluoromethane ug/kg <4.2 11.7 12/01/15 13:164.2
Diisopropyl ether ug/kg <2.0 5.9 12/01/15 13:162.0
Ethylbenzene ug/kg <2.1 5.9 12/01/15 13:162.1
Hexachloro-1,3-butadiene ug/kg <2.3 5.9 12/01/15 13:162.3
Isopropylbenzene (Cumene)ug/kg <2.2 5.9 12/01/15 13:162.2
m&p-Xylene ug/kg <4.2 11.7 12/01/15 13:164.2
Methyl-tert-butyl ether ug/kg <1.8 5.9 12/01/15 13:161.8
Methylene Chloride ug/kg <3.5 23.4 12/01/15 13:163.5
n-Butylbenzene ug/kg <2.1 5.9 12/01/15 13:162.1
n-Propylbenzene ug/kg <2.0 5.9 12/01/15 13:162.0
Naphthalene ug/kg <1.4 5.9 12/01/15 13:161.4
o-Xylene ug/kg <2.2 5.9 12/01/15 13:162.2
p-Isopropyltoluene ug/kg <2.0 5.9 12/01/15 13:162.0
sec-Butylbenzene ug/kg <1.9 5.9 12/01/15 13:161.9
Styrene ug/kg <2.1 5.9 12/01/15 13:162.1
tert-Butylbenzene ug/kg <2.3 5.9 12/01/15 13:162.3
Tetrachloroethene ug/kg <2.0 5.9 12/01/15 13:162.0
Toluene ug/kg <2.1 5.9 12/01/15 13:162.1
trans-1,2-Dichloroethene ug/kg <2.2 5.9 12/01/15 13:162.2
trans-1,3-Dichloropropene ug/kg <1.8 5.9 12/01/15 13:161.8
Trichloroethene ug/kg <2.5 5.9 12/01/15 13:162.5
Trichlorofluoromethane ug/kg <2.6 5.9 12/01/15 13:162.6
Vinyl acetate ug/kg <10.3 58.5 12/01/15 13:1610.3
Vinyl chloride ug/kg <2.1 11.7 12/01/15 13:162.1
Xylene (Total)ug/kg <4.2 11.7 12/01/15 13:164.2
1,2-Dichloroethane-d4 (S)%84 70-132 12/01/15 13:16
4-Bromofluorobenzene (S)%105 70-130 12/01/15 13:16
Toluene-d8 (S)%107 70-130 12/01/15 13:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617171LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 46.852.6 89 74-137
1,1,1-Trichloroethane ug/kg 45.452.6 86 67-140
1,1,2,2-Tetrachloroethane ug/kg 40.852.6 78 72-141
1,1,2-Trichloroethane ug/kg 45.652.6 87 78-138
1,1-Dichloroethane ug/kg 43.452.6 82 69-134
1,1-Dichloroethene ug/kg 50.852.6 97 67-138
1,1-Dichloropropene ug/kg 49.652.6 94 69-139
1,2,3-Trichlorobenzene ug/kg 45.452.6 86 70-146
1,2,3-Trichloropropane ug/kg 43.652.6 83 69-144
1,2,4-Trichlorobenzene ug/kg 45.552.6 86 68-148
1,2,4-Trimethylbenzene ug/kg 45.952.6 87 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 12 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617171LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 40.452.6 77 65-140
1,2-Dibromoethane (EDB)ug/kg 47.552.6 90 77-135
1,2-Dichlorobenzene ug/kg 46.652.6 89 77-141
1,2-Dichloroethane ug/kg 41.852.6 79 65-137
1,2-Dichloropropane ug/kg 45.952.6 87 72-136
1,3,5-Trimethylbenzene ug/kg 46.252.6 88 76-133
1,3-Dichlorobenzene ug/kg 46.952.6 89 74-138
1,3-Dichloropropane ug/kg 45.652.6 87 71-139
1,4-Dichlorobenzene ug/kg 45.552.6 86 76-138
2,2-Dichloropropane ug/kg 47.552.6 90 68-137
2-Butanone (MEK)ug/kg 79.8J105 76 58-147
2-Chlorotoluene ug/kg 44.252.6 84 73-139
2-Hexanone ug/kg 88.1105 84 62-145
4-Chlorotoluene ug/kg 45.152.6 86 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 90.6105 86 64-149
Acetone ug/kg 74.4J105 71 53-153
Benzene ug/kg 50.552.6 96 73-135
Bromobenzene ug/kg 43.152.6 82 75-133
Bromochloromethane ug/kg 47.752.6 91 73-134
Bromodichloromethane ug/kg 46.152.6 88 71-135
Bromoform ug/kg 38.152.6 72 66-141
Bromomethane ug/kg 55.152.6 105 53-160
Carbon tetrachloride ug/kg 49.252.6 93 60-145
Chlorobenzene ug/kg 46.552.6 88 78-130
Chloroethane ug/kg 51.652.6 98 64-149
Chloroform ug/kg 45.452.6 86 70-134
Chloromethane ug/kg 47.652.6 91 52-150
cis-1,2-Dichloroethene ug/kg 45.352.6 86 70-133
cis-1,3-Dichloropropene ug/kg 48.152.6 91 68-134
Dibromochloromethane ug/kg 45.152.6 86 71-138
Dibromomethane ug/kg 48.952.6 93 74-130
Dichlorodifluoromethane ug/kg 48.052.6 91 40-160
Diisopropyl ether ug/kg 44.952.6 85 69-141
Ethylbenzene ug/kg 46.452.6 88 75-133
Hexachloro-1,3-butadiene ug/kg 46.552.6 88 68-143
Isopropylbenzene (Cumene)ug/kg 52.052.6 99 76-143
m&p-Xylene ug/kg 92.3105 88 75-136
Methyl-tert-butyl ether ug/kg 49.352.6 94 68-144
Methylene Chloride ug/kg 42.552.6 81 45-154
n-Butylbenzene ug/kg 45.252.6 86 72-137
n-Propylbenzene ug/kg 44.852.6 85 76-136
Naphthalene ug/kg 45.552.6 86 68-151
o-Xylene ug/kg 47.252.6 90 76-141
p-Isopropyltoluene ug/kg 46.052.6 87 76-140
sec-Butylbenzene ug/kg 47.652.6 90 79-139
Styrene ug/kg 49.152.6 93 79-137
tert-Butylbenzene ug/kg 41.652.6 79 74-143
REPORT OF LABORATORY ANALYSIS
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Page 13 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617171LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 47.152.6 90 71-138
Toluene ug/kg 46.952.6 89 74-131
trans-1,2-Dichloroethene ug/kg 49.852.6 95 67-135
trans-1,3-Dichloropropene ug/kg 48.352.6 92 65-146
Trichloroethene ug/kg 49.252.6 94 67-135
Trichlorofluoromethane ug/kg 47.052.6 89 59-144
Vinyl acetate ug/kg 82.6 F31057840-160
Vinyl chloride ug/kg 49.152.6 93 56-141
Xylene (Total)ug/kg 139158 88 76-137
1,2-Dichloroethane-d4 (S)%91 70-132
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1617778MATRIX SPIKE SAMPLE:
MSSpike
Result
92277134005
1,1,1,2-Tetrachloroethane ug/kg 23.729.5 80 70-130ND
1,1,1-Trichloroethane ug/kg 25.429.5 86 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 24.129.5 82 70-130ND
1,1,2-Trichloroethane ug/kg 24.229.5 82 70-130ND
1,1-Dichloroethane ug/kg 29.229.5 99 70-130ND
1,1-Dichloroethene ug/kg 31.229.5 106 49-180ND
1,1-Dichloropropene ug/kg 28.329.5 96 70-130ND
1,2,3-Trichlorobenzene ug/kg 19.5 M129.5 66 70-130ND
1,2,3-Trichloropropane ug/kg 23.829.5 81 70-130ND
1,2,4-Trichlorobenzene ug/kg 18.7 M129.5 63 70-130ND
1,2,4-Trimethylbenzene ug/kg 26.029.5 88 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 22.329.5 76 70-130ND
1,2-Dibromoethane (EDB)ug/kg 26.429.5 89 70-130ND
1,2-Dichlorobenzene ug/kg 23.029.5 78 70-130ND
1,2-Dichloroethane ug/kg 26.529.5 90 70-130ND
1,2-Dichloropropane ug/kg 26.429.5 89 70-130ND
1,3,5-Trimethylbenzene ug/kg 26.129.5 88 70-130ND
1,3-Dichlorobenzene ug/kg 23.429.5 79 70-130ND
1,3-Dichloropropane ug/kg 26.129.5 88 70-130ND
1,4-Dichlorobenzene ug/kg 23.529.5 80 70-130ND
2,2-Dichloropropane ug/kg 25.929.5 88 70-130ND
2-Butanone (MEK)ug/kg 50.2J59.1 85 70-130ND
2-Chlorotoluene ug/kg 25.129.5 85 70-130ND
2-Hexanone ug/kg 50.7J59.1 86 70-130ND
4-Chlorotoluene ug/kg 25.229.5 85 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 53.3J59.1 90 70-130ND
Acetone ug/kg 52.1J M159.1 20 70-1300.040J mg/kg
Benzene ug/kg 27.729.5 94 50-166ND
Bromobenzene ug/kg 24.829.5 84 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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Page 14 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1617778MATRIX SPIKE SAMPLE:
MSSpike
Result
92277134005
Bromochloromethane ug/kg 24.629.5 83 70-130ND
Bromodichloromethane ug/kg 25.129.5 85 70-130ND
Bromoform ug/kg 24.329.5 82 70-130ND
Bromomethane ug/kg 32.829.5 111 70-130ND
Carbon tetrachloride ug/kg 27.429.5 93 70-130ND
Chlorobenzene ug/kg 25.629.5 87 43-169ND
Chloroethane ug/kg 27.929.5 94 70-130ND
Chloroform ug/kg 26.629.5 90 70-130ND
Chloromethane ug/kg 28.029.5 95 70-130ND
cis-1,2-Dichloroethene ug/kg 27.029.5 91 70-130ND
cis-1,3-Dichloropropene ug/kg 24.729.5 83 70-130ND
Dibromochloromethane ug/kg 22.329.5 75 70-130ND
Dibromomethane ug/kg 25.929.5 88 70-130ND
Dichlorodifluoromethane ug/kg 27.429.5 93 70-130ND
Diisopropyl ether ug/kg 26.929.5 91 70-130ND
Ethylbenzene ug/kg 26.629.5 90 70-130ND
Hexachloro-1,3-butadiene ug/kg 22.329.5 76 70-130ND
Isopropylbenzene (Cumene)ug/kg 28.529.5 96 70-130ND
m&p-Xylene ug/kg 52.459.1 89 70-130ND
Methyl-tert-butyl ether ug/kg 28.029.5 95 70-130ND
Methylene Chloride ug/kg 43.329.5 126 70-1300.0060J mg/kg
n-Butylbenzene ug/kg 24.629.5 83 70-130ND
n-Propylbenzene ug/kg 26.229.5 89 70-130ND
Naphthalene ug/kg 20.3 M129.5 69 70-130ND
o-Xylene ug/kg 25.829.5 87 70-130ND
p-Isopropyltoluene ug/kg 24.629.5 83 70-130ND
sec-Butylbenzene ug/kg 26.329.5 89 70-130ND
Styrene ug/kg 24.329.5 82 70-130ND
tert-Butylbenzene ug/kg 22.629.5 76 70-130ND
Tetrachloroethene ug/kg 38.3 M129.5 40 70-1300.026 mg/kg
Toluene ug/kg 26.429.5 89 52-163ND
trans-1,2-Dichloroethene ug/kg 27.729.5 94 70-130ND
trans-1,3-Dichloropropene ug/kg 25.229.5 85 70-130ND
Trichloroethene ug/kg 25.229.5 85 49-167ND
Trichlorofluoromethane ug/kg 28.329.5 96 70-130ND
Vinyl acetate ug/kg 22.8J M159.1 39 70-130ND
Vinyl chloride ug/kg 28.429.5 96 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277579001
1617777SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg <2.0 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277579001
1617777SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg <1.7 30ND
1,1,2,2-Tetrachloroethane ug/kg <1.8 30ND
1,1,2-Trichloroethane ug/kg <2.0 30ND
1,1-Dichloroethane ug/kg <1.5 30ND
1,1-Dichloroethene ug/kg <1.7 30ND
1,1-Dichloropropene ug/kg <1.5 30ND
1,2,3-Trichlorobenzene ug/kg <2.1 30ND
1,2,3-Trichloropropane ug/kg <1.6 30ND
1,2,4-Trichlorobenzene ug/kg <1.6 30ND
1,2,4-Trimethylbenzene ug/kg <1.9 30ND
1,2-Dibromo-3-chloropropane ug/kg <3.5 30ND
1,2-Dibromoethane (EDB)ug/kg <1.7 30ND
1,2-Dichlorobenzene ug/kg <1.8 30ND
1,2-Dichloroethane ug/kg <2.1 30ND
1,2-Dichloropropane ug/kg <1.6 30ND
1,3,5-Trimethylbenzene ug/kg <1.7 30ND
1,3-Dichlorobenzene ug/kg <1.9 30ND
1,3-Dichloropropane ug/kg <1.8 30ND
1,4-Dichlorobenzene ug/kg <1.6 30ND
2,2-Dichloropropane ug/kg <1.6 30ND
2-Butanone (MEK)ug/kg 19.8J 30ND
2-Chlorotoluene ug/kg <1.6 30ND
2-Hexanone ug/kg <3.8 30ND
4-Chlorotoluene ug/kg <1.7 30ND
4-Methyl-2-pentanone (MIBK)ug/kg <3.6 30ND
Acetone ug/kg 165 D6543094.5
Benzene ug/kg <1.6 30ND
Bromobenzene ug/kg <1.9 30ND
Bromochloromethane ug/kg <1.6 30ND
Bromodichloromethane ug/kg <1.8 30ND
Bromoform ug/kg <2.2 30ND
Bromomethane ug/kg <2.4 30ND
Carbon tetrachloride ug/kg <2.5 30ND
Chlorobenzene ug/kg <1.8 30ND
Chloroethane ug/kg <2.3 30ND
Chloroform ug/kg <1.6 30ND
Chloromethane ug/kg <2.3 30ND
cis-1,2-Dichloroethene ug/kg <1.4 30ND
cis-1,3-Dichloropropene ug/kg <1.7 30ND
Dibromochloromethane ug/kg <1.7 30ND
Dibromomethane ug/kg <2.4 30ND
Dichlorodifluoromethane ug/kg <3.5 30ND
Diisopropyl ether ug/kg <1.6 30ND
Ethylbenzene ug/kg <1.7 30ND
Hexachloro-1,3-butadiene ug/kg <1.9 30ND
Isopropylbenzene (Cumene)ug/kg <1.8 30ND
m&p-Xylene ug/kg <3.5 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277579001
1617777SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg <1.5 30ND
Methylene Chloride ug/kg <2.9 30ND
n-Butylbenzene ug/kg <1.7 30ND
n-Propylbenzene ug/kg <1.6 30ND
Naphthalene ug/kg <1.2 30ND
o-Xylene ug/kg <1.8 30ND
p-Isopropyltoluene ug/kg <1.6 30ND
sec-Butylbenzene ug/kg <1.6 30ND
Styrene ug/kg <1.7 30ND
tert-Butylbenzene ug/kg <1.9 30ND
Tetrachloroethene ug/kg <1.6 30ND
Toluene ug/kg <1.7 30ND
trans-1,2-Dichloroethene ug/kg <1.8 30ND
trans-1,3-Dichloropropene ug/kg <1.5 30ND
Trichloroethene ug/kg <2.0 30ND
Trichlorofluoromethane ug/kg <2.1 30ND
Vinyl acetate ug/kg <8.5 30ND
Vinyl chloride ug/kg <1.7 30ND
Xylene (Total)ug/kg <3.5 30ND
1,2-Dichloroethane-d4 (S)%103 5693
4-Bromofluorobenzene (S)%94 39103
Toluene-d8 (S)%112 47113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39393
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92277686001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617725
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg <64.0 330 12/02/15 10:5064.0
1,2-Dichlorobenzene ug/kg <88.0 330 12/02/15 10:5088.0
1,3-Dichlorobenzene ug/kg <75.0 330 12/02/15 10:5075.0
1,4-Dichlorobenzene ug/kg <93.0 330 12/02/15 10:5093.0
1-Methylnaphthalene ug/kg <86.0 330 12/02/15 10:5086.0
2,4,5-Trichlorophenol ug/kg <102 330 12/02/15 10:50102
2,4,6-Trichlorophenol ug/kg <73.0 330 12/02/15 10:5073.0
2,4-Dichlorophenol ug/kg <72.0 330 12/02/15 10:5072.0
2,4-Dimethylphenol ug/kg <130 330 12/02/15 10:50130
2,4-Dinitrophenol ug/kg <54.0 1650 12/02/15 10:5054.0
2,4-Dinitrotoluene ug/kg <62.0 330 12/02/15 10:5062.0
2,6-Dinitrotoluene ug/kg <69.0 330 12/02/15 10:5069.0
2-Chloronaphthalene ug/kg <65.0 330 12/02/15 10:5065.0
2-Chlorophenol ug/kg <90.0 330 12/02/15 10:5090.0
2-Methylnaphthalene ug/kg <71.0 330 12/02/15 10:5071.0
2-Methylphenol(o-Cresol)ug/kg <100 330 12/02/15 10:50100
2-Nitroaniline ug/kg <102 1650 12/02/15 10:50102
2-Nitrophenol ug/kg <80.0 330 12/02/15 10:5080.0
3&4-Methylphenol(m&p Cresol)ug/kg <130 330 12/02/15 10:50130
3,3'-Dichlorobenzidine ug/kg <72.0 1650 12/02/15 10:5072.0
3-Nitroaniline ug/kg <90.0 1650 12/02/15 10:5090.0
4,6-Dinitro-2-methylphenol ug/kg <66.0 660 12/02/15 10:5066.0
4-Bromophenylphenyl ether ug/kg <60.0 330 12/02/15 10:5060.0
4-Chloro-3-methylphenol ug/kg <68.0 660 12/02/15 10:5068.0
4-Chloroaniline ug/kg <92.0 1650 12/02/15 10:5092.0
4-Chlorophenylphenyl ether ug/kg <68.0 330 12/02/15 10:5068.0
4-Nitroaniline ug/kg <93.0 660 12/02/15 10:5093.0
4-Nitrophenol ug/kg <59.0 1650 12/02/15 10:5059.0
Acenaphthene ug/kg <76.0 330 12/02/15 10:5076.0
Acenaphthylene ug/kg <78.0 330 12/02/15 10:5078.0
Aniline ug/kg <89.0 330 12/02/15 10:5089.0
Anthracene ug/kg <74.0 330 12/02/15 10:5074.0
Benzo(a)anthracene ug/kg <61.0 330 12/02/15 10:5061.0
Benzo(a)pyrene ug/kg <63.0 330 12/02/15 10:5063.0
Benzo(b)fluoranthene ug/kg <57.0 330 12/02/15 10:5057.0
Benzo(g,h,i)perylene ug/kg <84.0 330 12/02/15 10:5084.0
Benzo(k)fluoranthene ug/kg <65.0 330 12/02/15 10:5065.0
Benzoic Acid ug/kg <60.0 1650 12/02/15 10:5060.0
Benzyl alcohol ug/kg <66.0 660 12/02/15 10:5066.0
bis(2-Chloroethoxy)methane ug/kg <77.0 330 12/02/15 10:5077.0
bis(2-Chloroethyl) ether ug/kg <84.0 330 12/02/15 10:5084.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1617725
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroisopropyl) ether ug/kg <88.0 330 12/02/15 10:5088.0
bis(2-Ethylhexyl)phthalate ug/kg <90.0 330 12/02/15 10:5090.0
Butylbenzylphthalate ug/kg <70.0 330 12/02/15 10:5070.0
Chrysene ug/kg <44.0 330 12/02/15 10:5044.0
Di-n-butylphthalate ug/kg <54.0 330 12/02/15 10:5054.0
Di-n-octylphthalate ug/kg <69.0 330 12/02/15 10:5069.0
Dibenz(a,h)anthracene ug/kg <70.0 330 12/02/15 10:5070.0
Dibenzofuran ug/kg <54.0 330 12/02/15 10:5054.0
Diethylphthalate ug/kg <51.0 330 12/02/15 10:5051.0
Dimethylphthalate ug/kg <67.0 330 12/02/15 10:5067.0
Fluoranthene ug/kg <48.0 330 12/02/15 10:5048.0
Fluorene ug/kg <68.0 330 12/02/15 10:5068.0
Hexachloro-1,3-butadiene ug/kg <57.0 330 12/02/15 10:5057.0
Hexachlorobenzene ug/kg <42.0 330 12/02/15 10:5042.0
Hexachlorocyclopentadiene ug/kg <61.0 330 12/02/15 10:5061.0
Hexachloroethane ug/kg <87.0 330 12/02/15 10:5087.0
Indeno(1,2,3-cd)pyrene ug/kg <68.0 330 12/02/15 10:5068.0
Isophorone ug/kg <74.0 330 12/02/15 10:5074.0
N-Nitroso-di-n-propylamine ug/kg <63.0 330 12/02/15 10:5063.0
N-Nitrosodimethylamine ug/kg <107 330 12/02/15 10:50107
N-Nitrosodiphenylamine ug/kg <98.0 330 12/02/15 10:5098.0
Naphthalene ug/kg <81.0 330 12/02/15 10:5081.0
Nitrobenzene ug/kg <90.0 330 12/02/15 10:5090.0
Pentachlorophenol ug/kg <60.0 1650 12/02/15 10:5060.0
Phenanthrene ug/kg <55.0 330 12/02/15 10:5055.0
Phenol ug/kg <99.0 330 12/02/15 10:5099.0
Pyrene ug/kg <56.0 330 12/02/15 10:5056.0
2,4,6-Tribromophenol (S)%93 27-110 12/02/15 10:50
2-Fluorobiphenyl (S)%84 30-110 12/02/15 10:50
2-Fluorophenol (S)%72 13-110 12/02/15 10:50
Nitrobenzene-d5 (S)%83 23-110 12/02/15 10:50
Phenol-d6 (S)%71 22-110 12/02/15 10:50
Terphenyl-d14 (S)%101 28-110 12/02/15 10:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617726LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1617727
1,2,4-Trichlorobenzene ug/kg 16701670 100 36-1201001670 0 30
1,2-Dichlorobenzene ug/kg 14201670 85 41-120851420 0 30
1,3-Dichlorobenzene ug/kg 14401670 86 66-120841410 2 30
1,4-Dichlorobenzene ug/kg 14201670 85 42-120841400 1 30
1-Methylnaphthalene ug/kg 14301670 86 40-120811350 6 30
2,4,5-Trichlorophenol ug/kg 18301670 110 37-1201051750 4 30
2,4,6-Trichlorophenol ug/kg 17901670 107 40-1201111840 3 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617726LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1617727
2,4-Dichlorophenol ug/kg 16201670 97 33-120941570 3 30
2,4-Dimethylphenol ug/kg 15401670 92 36-120881460 5 30
2,4-Dinitrophenol ug/kg 77108330 93 22-121847000 10 30
2,4-Dinitrotoluene ug/kg 15601670 94 60-120901500 4 30
2,6-Dinitrotoluene ug/kg 15701670 94 54-120901500 4 30
2-Chloronaphthalene ug/kg 15301670 92 41-120911510 2 30
2-Chlorophenol ug/kg 13701670 82 39-120801330 3 30
2-Methylnaphthalene ug/kg 13501670 81 26-120791320 2 30
2-Methylphenol(o-Cresol)ug/kg 14801670 89 41-120841400 6 30
2-Nitroaniline ug/kg 24703330 74 45-120742450 1 30
2-Nitrophenol ug/kg 15001670 90 35-120891480 2 30
3&4-Methylphenol(m&p Cresol)ug/kg 13001670 78 35-120741240 5 30
3,3'-Dichlorobenzidine ug/kg 30003330 90 16-125913020 1 30
3-Nitroaniline ug/kg 25403330 76 45-120732450 4 30
4,6-Dinitro-2-methylphenol ug/kg 32303330 97 46-120963200 1 30
4-Bromophenylphenyl ether ug/kg 15801670 95 36-120991640 4 30
4-Chloro-3-methylphenol ug/kg 30603330 92 37-120872900 5 30
4-Chloroaniline ug/kg 24703330 74 35-120702320 7 30
4-Chlorophenylphenyl ether ug/kg 15101670 91 30-120871450 4 30
4-Nitroaniline ug/kg 23803330 71 48-120672230 6 30
4-Nitrophenol ug/kg 82408330 99 43-120917590 8 30
Acenaphthene ug/kg 14801670 89 46-120861430 4 30
Acenaphthylene ug/kg 15801670 95 46-120921530 3 30
Aniline ug/kg 11801670 71 33-120671110 6 30
Anthracene ug/kg 16001670 96 63-120991650 3 30
Benzo(a)anthracene ug/kg 17101670 102 61-1201061770 4 30
Benzo(a)pyrene ug/kg 15801670 95 59-120971620 2 30
Benzo(b)fluoranthene ug/kg 16301670 98 55-1201001660 2 30
Benzo(g,h,i)perylene ug/kg 15601670 94 57-120951590 1 30
Benzo(k)fluoranthene ug/kg 18201670 109 56-1201131880 3 30
Benzoic Acid ug/kg 61108330 73 13-120665520 10 30
Benzyl alcohol ug/kg 25103330 75 34-120712360 6 30
bis(2-Chloroethoxy)methane ug/kg 12801670 77 21-120751250 2 30
bis(2-Chloroethyl) ether ug/kg 11701670 70 25-120701170 0 30
bis(2-Chloroisopropyl) ether ug/kg 8931670 54 13-12051852 5 30
bis(2-Ethylhexyl)phthalate ug/kg 16101670 97 56-1231021710 6 30
Butylbenzylphthalate ug/kg 16301670 98 57-1201071780 8 30
Chrysene ug/kg 15801670 95 64-1201021690 7 30
Di-n-butylphthalate ug/kg 15701670 94 58-120961590 2 30
Di-n-octylphthalate ug/kg 17401670 105 47-1211071780 2 30
Dibenz(a,h)anthracene ug/kg 15801670 95 56-120941570 0 30
Dibenzofuran ug/kg 14801670 89 43-120861440 3 30
Diethylphthalate ug/kg 15401670 92 55-120881470 4 30
Dimethylphthalate ug/kg 15601670 94 54-120901500 4 30
Fluoranthene ug/kg 16401670 98 61-120981640 0 30
Fluorene ug/kg 15601670 94 51-120901500 4 30
Hexachloro-1,3-butadiene ug/kg 18001670 108 22-1201081800 0 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1617726LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1617727
Hexachlorobenzene ug/kg 18301670 110 53-1201151920 5 30
Hexachlorocyclopentadiene ug/kg 16201670 97 18-150981630 1 30
Hexachloroethane ug/kg 14601670 87 39-120861430 2 30
Indeno(1,2,3-cd)pyrene ug/kg 16401670 98 58-120981630 0 30
Isophorone ug/kg 13201670 79 38-120741240 7 30
N-Nitroso-di-n-propylamine ug/kg 11501670 69 30-120621030 11 30
N-Nitrosodimethylamine ug/kg 13101670 78 32-120721200 8 30
N-Nitrosodiphenylamine ug/kg 14101670 84 50-120881460 4 30
Naphthalene ug/kg 14501670 87 38-120851420 3 30
Nitrobenzene ug/kg 14201670 85 37-120811350 5 30
Pentachlorophenol ug/kg 26703330 80 10-120802660 1 30
Phenanthrene ug/kg 15001670 90 62-120941560 4 30
Phenol ug/kg 14501670 87 37-120841400 3 30
Pyrene ug/kg 16401670 98 63-1201091820 10 30
2,4,6-Tribromophenol (S)%96 27-110101
2-Fluorobiphenyl (S)%92 30-11089
2-Fluorophenol (S)%79 13-11078
Nitrobenzene-d5 (S)%86 23-11084
Phenol-d6 (S)%81 22-11077
Terphenyl-d14 (S)%97 28-110106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39463
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92277686001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1619772
Associated Lab Samples:92277686001
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg <10.0 10.0 N212/06/15 05:3110.0
Aliphatic (C19-C36)mg/kg <10.0 10.0 N212/06/15 05:3110.0
Aromatic (C11-C22)mg/kg <10.0 10.0 N212/06/15 05:3110.0
2-Bromonaphthalene (S)%94 40-140 12/06/15 05:31
2-Fluorobiphenyl (S)%94 40-140 12/06/15 05:31
Nonatriacontane (S)%77 40-140 12/06/15 05:31
o-Terphenyl (S)%86 40-140 12/06/15 05:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1619773LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1619774
Aliphatic (C09-C18)mg/kg <10.0 N2107240-14060<10.0 50
Aliphatic (C19-C36)mg/kg <10.0 N213.3 67 40-14057<10.0 50
Aromatic (C11-C22)mg/kg 23.1 N228.3 82 40-1408524.1 4 50
2-Bromonaphthalene (S)%84 40-14088
2-Fluorobiphenyl (S)%85 40-14089
Nonatriacontane (S)%78 40-14077
o-Terphenyl (S)%82 40-14083
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92277686
Pantry #3471
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8619
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92277686001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277605010
1616491SAMPLE DUPLICATE:
Percent Moisture %18.5 2 2518.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92277690013
1616492SAMPLE DUPLICATE:
Percent Moisture %15.7 0 2515.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92277686
Pantry #3471
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92277686
Pantry #3471
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92277686001 OEXT/39463 GCSV/23457SD-17 MADEP EPH MADEP EPH
92277686001 GCV/10183 GCV/10185SD-17 MADEP VPH MADEP VPH
92277686001 OEXT/39393 MSSV/11590SD-17 EPA 3546 EPA 8270
92277686001 MSV/34494SD-17 EPA 8260
92277686001 PMST/8619SD-17 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/15/2015 04:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 27
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