RA-1939_11920_CA_RPTS_20211015_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

October 15, 2021

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
September 2021
Red Apple Market #9
100 West Jackson Street
Rich Square, Northampton County
North Carolina
Facility ID Number: 0-00-0000026624
Incident Number: 11920
GRI Project Number: 4497

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Bea Harrison, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Ground Water Monitoring Report
September 2021
Red Apple Market #9
100 West Jackson Street
Rich Square, Northampton County
North Carolina
Facility ID Number: 0-00-0000026624
Incident Number: 11920
GRI Project Number: 4497

Prepared for:

Red Apple Markets, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910

October 15, 2021

William Regenthal, P.G.
Project Manager
Brett Houghton
Staff Scientist

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
i
SITE INFORMATION
1. Site Identification
 Red Apple Market #9 (Facility ID 0-00-0000026624)
 Incident Number 11920 – Intermediate Risk (I175D)
 Location of Source Area: 100 West Jackson Street
Rich Square, NC 227869
Northampton County
36.2741410°N, 77.2842062°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

UST Operator
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Property Owner
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Property Occupant
Duck Thru Food Stores
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, Florida 32811
State Certification No. 573
[phone]
3. Information about Release
 Release was discovered on July 15, 1992
 An unknown amount of product was released from the leaking UST System
 One 8,000-gallon gasoline, one 5,000-gallon gasoline, two 3,000-gallon gasoline, two 3,000-gallon
#2 fuel oil and one 2,000-gallon kerosene USTs were removed and/or abandoned in place in July
1992. One 10,000-gallon and one 6,000-gallon gasoline and one 4,000-gallon kerosene USTs are
currently in use at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
ii
EXECUTIVE SUMMARY
The former Red Apple Market #9 is located at 100 West Jackson Street in Rich Square, Northampton
County, North Carolina. The site is currently owned by Jernigan Properties, Inc. and is operated by Duck
Thru Food Stores as a petroleum retail facility. One 8,000-gallon gasoline, one 5,000-gallon gasoline, two
3,000-gallon gasoline, two 3,000-gallon #2 fuel oil and one 2,000-gallon kerosene USTs were removed
and/or abandoned in place in July 1992 confirming the presence of a release. Currently, one 10,000-gallon
and one 6,000-gallon gasoline and one 4,000-gallon kerosene USTs are in use at the site. The adjoining
properties are a mixture of commercial and residential properties. According to the information
determined during receptor survey activities, no water supply wells were identified within 1,500 feet of
the site. Public water is available to the site and surrounding properties within a 1,500-foot radius of the
site.

A CAP has not been submitted for the site. Free product recovery events have been conducted at the site
beginning in August 2017.

On September 7, 2021, five Type II monitoring wells were gauged, purged and/or sampled in accordance
with the NCDEQ Guidelines. Free product was not observed in the monitoring wells in September 2021;
however, approximately 0.03 gallons of free product were recovered by an absorbent boom that was
removed from MW-1 prior to gauging. Concentrations of benzene and naphthalene that exceeded the
MACs were reported in the ground water samples collected from MW-13. All of the reported contaminant
concentrations were less than the Gross Contamination Levels (GCLs).

Upon completion of the September 2021 sampling event, an absorbent boom was installed in MW-1.

Based on this information, the risk classification for the site should remain intermediate risk. Free product
recovery events should continue to be conducted at the site until free product is no longer present and
contaminant concentrations are less than the GCLs. Semi-annual ground water monitoring should
continue at the site. The next sampling event is tentatively scheduled for March 2022.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................3
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................3
5.0 CONCLUSIONS .........................................................................................................................3
6.0 LIMITATIONS ...........................................................................................................................4
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Well Construction and Gauging Information
Table 5: Summary of Ground Water Sample Analytical Results
Table 6: Free Product Recovery Results
Table 7: Free Product Recovery Event Information
Table 8: Free Product Recovery Cost Summary

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
1
1.0 SITE HISTORY AND CHARACTERIZATION
Geological Resources, Inc. (GRI) presents the results of the September 2021 ground water sampling event
at the Red Apple Market #9 site located at 100 West Jackson Street in Rich Square, Northampton County,
North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 21-551,
which was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on August 27,
2021 and was approved as Task Authorization No. 11920-7 on September 1, 2020. State correspondence
has been included as Appendix A.

The site is currently owned by Jernigan Properties, Inc. and is operated by Duck Thru Food Stores as a
petroleum retail facility. One 8,000-gallon gasoline, one 5,000-gallon gasoline, two 3,000-gallon gasoline,
two 3,000-gallon #2 fuel oil and one 2,000-gallon kerosene USTs were removed and/or abandoned in
place in July 1992, confirming the presence of a release. Currently, one 10,000-gallon and one 6,000-
gallon gasoline and one 4,000-gallon kerosene USTs are in use at the site. UST owner/operator
information and UST system information are included as Tables 1 and 2, respectively. Please note that
the information presented in this report is based on information provided by the previous consultant and
does not match the NCDEQ Registered Tank Database. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of commercial and residential properties. The site contains
one building (the store) and is partially capped with concrete. The overall topography at the site is
relatively flat. No surface water bodies were identified within a 500-foot radius of the site. Thirteen Type
II monitoring wells (MW-1 through MW-5 and MW-7 through MW-14) and one Type III monitoring well

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
2
(MWD-6) were installed at the site during previous ground water assessment activities. A Site Map
showing the locations of the monitoring wells and the structures on-site has been included as Figure 2.

On May 2, 2017, GRI personnel conducted a receptor survey update at the site. The site lies within the
designated wellhead protection area for the Town of Rich Square. No water supply wells were identified
within a 1,500-foot radius of the site. Municipal water is available to the site and surrounding properties.
Adjacent property owner information is presented in Table 3. A Site Vicinity Map showing the adjacent
properties has been included as Figure 3.

A CAP has not yet been developed for the site. To date, two MMPE events have been conducted at the
site along with hand bailing and an aggressive fluid-vapor recovery (AFVR) event. Please note that no
projected milestones have been established for this site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On September 7, 2021, five Type II monitoring wells (MW-1 and MW-11 through MW-14) were gauged,
purged and sampled in accordance with NCDEQ Guidelines. Approximately 0.03 gallons of free product
were recovered by an absorbent boom that was removed from MW-1 prior to gauging. Free product was
not measured in any monitoring wells during the sampling event. Depths to ground water in the Type II
monitoring wells ranged from 3.23 to 6.06 feet below the tops of well casings. Ground water elevations
in the Type II monitoring wells ranged from 94.41 to 96.30 feet. Ground water flow was generally radial
outward from a hydraulic ridge in the vicinity of MW-1 and MW-13. The horizontal hydraulic gradient
was approximately 0.03 feet per foot. The vertical gradient could be calculated since no telescoping well
was gauged. Well construction and gauging information is presented in Table 4. A Water Table Surface
Map based on the Type II monitoring wells is included as Figure 4. A summary of the current ground
water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 8 – 18 18 100.00 3.83 --- 96.17
MW-11 2 - 17 17 100.47 6.06 --- 94.41
MW-12 2 - 17 17 99.82 4.60 --- 95.22
MW-13 2 - 17 17 99.53 3.23 --- 96.30
MW-14 2 - 17 17 99.59 4.88 --- 94.71

Ground water samples collected from the monitoring wells were submitted for laboratory analyses of
VOCs using EPA Method 6200B. Concentrations of benzene and naphthalene that exceeded the MACs
were reported in the ground water sample collected from MW-13. All of the reported contaminant
concentrations were less than the GCLs. A summary of the analytical results for ground water samples
collected on September 7, 2021, is presented in Table 5. A Ground Water Quality Map based on the
September 2021 data is included as Figure 5. A complete report of laboratory analyses of the ground

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
3

Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80000 85,500 20,000 6,000
MW-1 <0.13 0.19 J <0.13 <0.25 1.7 1.1
MW-11 <0.13 <0.13 0.58 0.40 J 0.88 1.9
MW-12 0.40 J <0.13 <0.13 1.4 J 0.55 3.7
MW-13 48.6 22.9 119 234 <0.63 50.1
MW-14 <0.13 <0.13 <0.13 <0.25 9.0 <0.13

The baseline contaminant mass at the site has not been determined due to the presence of free product
in MW-1. Since free product was not observed in the ground water sample collected from MW-1, the
September 2021 sampling event can be used at the baseline event in the future. Contaminant mass
calculations can be completed during the next sampling event if free product is not observed.

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 3 to 17 feet below ground surface (bgs).

Please note that while free product recovery events have been conducted, a CAP has not been developed
for the site; therefore, a baseline contaminant mass prior to CAP implementation has not been established
at the site. Please note that milestones have not been established for this site.
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in MW-1. While no free product was observed in MW-1 during
the September 2021 sampling event, a total of 0.03 gallons of free product was recovered by the
absorbent boom removed from the well prior to gauging. Free product recovery should continue at the
site until free product is no longer present. Past free product recovery events are summarized in Tables
6, 7 and 8. Upon completion of the September 2021 sampling event, an absorbent sock was reinstalled
in MW-1.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Free product recovery events are being conducted at the site as the primary method of corrective action.
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.
5.0 CONCLUSIONS
 On September 7, 2021, five Type II monitoring wells were gauged, purged, and sampled. Ground
water flow was generally radial outward from a hydraulic ridge in the vicinity of MW-1 and MW-
13 with a horizontal gradient of approximately 0.03 feet per foot.
included as Appendix B. A summary of the current ground water analytical data is shown below:
water samples collected from the monitoring wells during the September 2021 sampling event has been

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 15, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
4
 A total of 0.03 gallons of free product was recovered by an absorbent boom that was removed
from MW-1 prior to gauging.
 Free product was not observed in any of the monitoring wells during the September 2021
sampling event.
 Concentrations of benzene and naphthalene that exceeded the MACs were reported in the
ground water sample collected from MW-13. All of the reported contaminant concentrations
were less than the GCLs.
 Upon completion of the September 2021 sampling event, an absorbent boom was installed in
MW-1.
 Based on this information, the risk classification for the site should remain intermediate risk. Free
product recovery events should continue to be conducted at the site until free product is no
longer present and contaminant concentrations are below the GCLs. Semi-annual ground water
monitoring should be continued at the site. The next sampling event is tentatively scheduled for
March 2022.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Northampton County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO

FIGURES
Copyright (C) 2009 MyTopo, 2006-2017 TomTom
077.3000000° W
077.3000000° W
077.2833333° W
077.2833333° W
077.2666666° W
077.2666666° W36.300036.300036.2833333° N36.2833333° N36.2666666° N36.2666666° N6.2500000° N6.2500000° NName: Site Location Map Map Center Location: 036.2741410° N 077.2842062° W
Date: 05/16/17
Scale: 1 inch = 2,000 ft.
Generated by Geological Resources, Inc.
Declination
MN 10.12° WGN 1.35° W
MNGN
Figure 1
Red Apple Mart #9
100 W. Jackson Street
Rich Square, Northampton County
North Carolina
Incident No. 11920
GRI Project No. 4497
SCALE 1:24000
0 1000 2000 3000 4000 5000 6000
FEET
SITE
5902-53-7210
5902-52-5930 5902-53-60845902-53-8071
5902-52-7962
5902-52-7801
5902-52-89365902-52-8948
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan, Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand), NGCC, ©OpenStreetMap contributors, and the GIS User Community
FIGURE 3: SITE VICINITY MAPRAM #9100 W. JACKSON STREETRICH SQUARE, NORTHAMPTON COUNTYNORTH CAROLINAINCIDENT NO. 11920GRI PROJECT NO. 4497
PREPARED BY:GEOLOGICAL RESOURCES,INC.APRIL 28, 2017
³
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Adjacent Properties
ncrivers
nc_northampton_parcels_poly
C:\Users\darhoward\Desktop\4497\4497 BaseMap.dwg, Model, 9/30/2021 7:03:17 AM, DARHOWARD

TABLES
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
Red Apple Markets, Inc./Eastern Fuels, Inc.08/26/1992 - 03/28/2002
Red Apple Markets, Inc./Eastern Fuels, Inc.12/30/1988 - 07/16/1992
Address Telephone Number
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
804-590-3555
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Name of Owner or Operator Dates of Ownership / Operation
Eastern Fuels, Inc.08/26/1992 - 10/26/2006
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
443-393-6270
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Classic Ventures, LLC 10/26/2006 - 10/27/2006
Address Telephone Number
710 North Hamilton Street, #200, Richmond, VA 23221
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Jernigan Oil Company, Inc.01/10/2012 - Current
Address
SDA Ventures, LLC 10/27/2006 - 01/10/2012
10211 Wincopin Circle, Suite 300, Columbia MD, 21044
P.O. Box 688, Ahoskie, NC 29710 252-332-2131
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Page 1 of 2
TABLE 1
UST OWNER/OPERATOR INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
UST ID Number 1 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 2 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Unknown 10/09/1982 - 12/30/1988
Telephone Number
0-026624
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
Unknown 08/01/1975 - 10/09/1982
Name of Owner or Operator Dates of Ownership / Operation
Address
Page 2 of 2
Date: 01/16/20
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 8,000 10/9/1982 Single Wall Steel 8 x 21' 4"Single Wall Steel Removed
(07/16/92)Yes
2 Gasoline 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
3 Gasoline 5,000 8/1/1975 Single Wall Steel 8' x 13' 5"Single Wall FRP Removed
(07/16/92)Yes
4 Gasoline 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
5 #2 Fuel Oil 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
6 #2 Fuel Oil 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
7 Kerosene 2,000 8/1/1975 Single Wall Steel 64" x 12'Single Wall Steel Removed
(07/16/92)Yes
A1 Gasoline 10,000 8/26/1992 Single Wall Steel 8' x 26' 7"Single Wall Flex Current No
A2 Gasoline 6,000 8/26/1992 Single Wall Steel 8' x 16'Single Wall Flex Current No
A3 Kerosene 4,000 8/26/1992 Single Wall Steel 64" x 24'Single Wall Flex Current No
Notes:
• FRP: Fiberglass reinforced plastic.
• This table is based off of historical information provided by a previous consultant and does not match the Resistered Tank Database.
TABLE 2
UST SYSTEM INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Date: 01/16/20 Facility ID # : 0-025344
Parcel Number Owner Name Address
0604542 Jernigan Properties, Inc.Post Office Box 688
Ahoskie, NC 27910
0605367 Town of Rich Square
c/o Vernice B Long, Clerk
Post Office Box 336
Rich Square, NC 27869
1301125 Wayne Ray Parker &
Lisa Parker Evans
100 S. Main Street
Littleton, NC 27850
0600629 Themistoklis Zacharopoulous 209 S. Main Street
Rich Square, NC 27869
1300360 Darlene M. Zacharoloulos Post Office Box 1
Rich Square, NC 27869
0601555 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
0601556 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
0601561 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
Note:
• Properties are keyed to Figure 3.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920))
Page 1 of 1
Date: 09/28/2021
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
05/02/17 7.56 4.35 96.17
08/16/17 6.69 4.08 96.81
05/21/18 7.10 3.89 96.24 Before MMPE
05/25/18 13.56 ---86.44 After MMPE
07/18/18 4.60 0.08 95.47
02/25/19 1.82 0.06 98.23 Before MMPE
03/01/19 11.20 ---88.80 After MMPE
04/15/19 2.25 0.07 97.81
11/26/19 6.27 0.02 93.75 Before AFVR
11/26/19 13.28 ---86.72 After AFVR
01/07/20 2.28 0.05 97.76
01/06/21 3.31 0.26 96.91
09/07/21 3.83 ---96.17
05/02/17 5.23 ---94.88
05/21/18 4.54 ---95.57 Before MMPE
05/25/18 4.25 ---95.86 After MMPE
07/18/18 6.65 ---93.46
02/25/19 1.96 ---98.15
04/15/19 2.56 ---97.55
01/07/20 8.09 ---92.02
01/06/21 4.42 ---95.69
05/02/17 4.66 ---96.24
05/21/18 4.84 ---96.06 Before MMPE
05/25/18 4.35 ---96.55 After MMPE
07/18/18 7.07 ---93.83
04/15/19 2.17 ---98.73
01/07/20 7.75 ---93.15
01/06/21 5.63 ---95.27
05/02/17 4.21 ---96.31
07/18/18 7.00 ---93.52
04/15/19 3.63 ---96.89
01/07/20 7.72 ---92.80
01/06/21 5.28 ---95.24
05/02/17 2.32 ---98.75
07/18/18 5.17 ---95.90
02/25/19 0.70 ---100.37
04/15/19 0.95 ---100.12
01/07/20 1.14 ---99.93
01/06/21 1.23 ---99.84
05/02/17 9.54 ---91.37
07/18/18 10.49 ---90.42
04/15/19 6.89 ---94.02
01/07/20 12.14 ---88.77
01/06/21 9.47 ---91.44
05/02/17 5.07 ---94.54
07/18/18 5.21 ---94.40
04/15/19 3.93 ---95.68
01/07/20 6.03 ---93.58
01/06/21 3.47 ---96.14
05/02/17 6.14 ---94.07
05/21/18 6.01 ---94.20 Before MMPE
05/25/18 9.53 ---90.68 After MMPE
07/18/18 7.04 ---93.17
02/25/19 0.87 ---99.34
04/15/19 4.18 ---96.03
01/07/20 7.03 ---93.18
01/06/21 6.24 ---93.97
05/02/17 6.07 ---94.56
07/18/18 7.65 ---92.98
04/15/19 3.32 ---97.31
01/07/20 8.69 ---91.94
01/06/21 5.34 ---95.29
05/02/17 8.56 ---92.50
07/18/18 9.16 ---91.90
04/15/19 5.54 ---95.52
01/07/20 10.77 ---90.29
01/06/21 8.32 ---92.74
01/06/21 6.70 ---93.77
09/07/21 6.06 ---94.41
01/06/21 12.21 ---87.61
09/07/21 4.60 ---95.22MW-12
100.47172-17201/06/21MW-11
99.82172-17201/06/21
100.90177-1706/23/93
100.63166-16608/26/94
6-16606/24/93MW-4
7
MW-5
100.00188-188MW-1 06/23/93
706/23/93MW-2 100.11177-17
MW-3
100.5216
3530-353008/25/94
706/24/93
MW-8
MW-9
99.61166-16
MW-10 101.06166-16608/26/94
TABLE 4
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
100.21166-16608/26/94
MWD-6
608/26/94MW-7
101.07177-17
100.91
Page 1 of 2
Date: 09/28/2021
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
TABLE 4
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
01/06/21 15.72 ---83.81
09/07/21 3.23 ---96.30
01/06/21 17.05 ---82.54
09/07/21 4.88 ---94.71
Notes:
2-17201/06/21MW-13
99.59172-17201/06/21
• NM : Not measured.
• Elevation relative to mean sea level.
MW-14
99.5317
• ft BGS : feet below ground surface.
Page 2 of 2
Date : 09/28/2021 Facility ID #: 0-026624
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 1
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 12,000
05/02/17 FP FP FP FP FP FP FP FP FP FP FP FP FP
05/21/18 FP FP FP FP FP FP FP FP FP FP FP FP FP
07/18/18 FP FP FP FP FP FP FP FP FP FP FP FP FP
04/15/19 FP FP FP FP FP FP FP FP FP FP FP FP FP
01/07/20 FP FP FP FP FP FP FP FP FP FP FP FP FP
01/06/21 FP FP FP FP FP FP FP FP FP FP FP FP FP
09/07/21 <0.13 0.19 J <0.13 <0.25 1.7 1.1 <0.13 2.1 <0.13 0.74 <0.13 <0.13 NR
05/02/17 452 8.3 12.2 13.0 18.4 67.2 <0.13 21.9 4.4 44.9 0.54 0.66 13.4
07/18/18 938 21.1 14.7 71.2 34.5 234 <1.3 29.5 39.8 56.1 <1.3 3.2 J NR
04/15/19 1,930 33.1 36.7 64.9 J 37.2 425 <6.3 34.7 9.6 J 104 <6.3 <6.3 NR
01/07/20 846 30.6 30.5 102 27.7 430 <3.1 51.8 16.6 100 <3.1 5.3 J NR
01/06/21 652 29.1 25.4 82.4 22.6 453 <2.5 44.0 16.0 87.7 <2.5 4.8 J NR
05/02/17 <0.13 <0.13 <0.13 <0.25 0.55 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 0.88 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 0.48 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 0.69 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 0.47 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 0.18 J <0.13 <0.13 <0.13 0.64 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 0.16 J <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 9.3 0.44 J 0.63 <0.13 63.0 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 8.0 <0.13 0.68 <0.13 69.3 <0.13 <0.13 <0.13 NR
04/15/19 <0.25 <0.25 <0.25 <0.50 6.1 <0.25 0.73 J <0.25 86.4 <0.25 <0.25 <0.25 NR
01/07/20 <0.31 <0.31 <0.31 <0.63 8.6 <0.31 0.70 J <0.31 101 <0.31 <0.31 <0.31 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 4.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.40
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.40
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 0.95 <0.13 1.3 1.6 0.43 J NR
05/02/17 0.17 J <0.13 0.27 J 0.78 J <0.13 0.58 <0.13 0.68 <0.13 1.7 23.0 7.5 2.3
07/18/18 15.0 47.0 40.6 46.1 <0.63 8.8 <0.63 25.2 <0.63 87.6 655 224 NR
04/15/19 <0.13 <0.13 0.70 <0.25 <0.13 0.18 J <0.13 0.23 J <0.13 0.56 3.4 0.74 NR
01/07/20 61.4 45.8 65.8 17.3 <0.31 4.5 <0.31 21.7 0.39 J 62.7 72.7 13.6 NR
01/06/21 <0.13 <0.13 0.57 0.36 J <0.13 <0.13 0.33 J <0.13 61.7 <0.13 <0.13 <0.13 NR
05/02/17 498 171 84.0 121 237 114 0.47 J 14.8 22.5 29.3 12.9 3.1 19.6
07/18/18 16.8 0.25 J 0.71 0.55 J 7.9 1.8 <0.13 0.20 J 0.71 0.20 J <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 1.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 16.6 0.27 J <0.13 <0.25 9.5 0.95 <0.13 <0.13 0.82 <0.13 0.15 J <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 0.14 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 4.9 4.5 30.0 11.6 8.9 <0.13 2.0 0.22 J 4.0 16.1 5.3 NR
09/07/21 <0.13 <0.13 0.58 0.40 J 0.88 1.9 <0.13 11.0 <0.13 0.87 <0.13 <0.13 NR
01/06/21 <0.13 0.62 0.50 2.5 3.8 0.45 J <0.13 0.22 J 0.59 0.78 1.6 0.45 J NR
09/07/21 0.40 J <0.13 <0.13 1.4 J 0.55 3.7 <0.13 0.85 <0.13 0.66 2.0 0.26 J NR
01/06/21 58.6 41.5 160 407 37.6 101 <0.63 20.4 4.8 60.6 207 72.6 NR
09/07/21 48.6 22.9 119 234 <0.63 50.1 <0.63 8.9 1.8 J 23.1 149 45.4 NRMW-13
MW-12
MW-11
TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Analytical Method
→ EPA Methods 6200B & 610
1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1-MethylnaphthaleneMAC (µg/l)
GCL (µg/l)MTBENaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-PropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneXylenesMW-1
MW-8
MW-9
MW-10
MW-2
MW-3
MW-4
MW-5
MWD-6
MW-7
Page 1 of 2
Date : 09/28/2021 Facility ID #: 0-026624
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 1
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 70,000 26,100 28,500 24,100 12,000
TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Analytical Method
→ EPA Methods 6200B & 610
1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1-MethylnaphthaleneMAC (µg/l)
GCL (µg/l)MTBENaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-PropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes01/06/21 0.15 J 2.2 1.0 5.2 61.7 0.42 J <0.13 0.16 J 0.36 J 0.41 J 2.8 0.95 NR
09/07/21 <0.13 <0.13 <0.13 <0.25 9.0 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
Notes:
• Results reported in µg/l (micrograms per liter).
• MAC: Maximum allowable concentrations also known as the 2L Standards specified in T15A NCAC 2L.0202.
• GCL : Gross contamination level.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards; concentration in italics exceeded the GCLs.
• NS: Not Sampled, well not located and assumed to be destroyed.
• FP: Free Product.
• Please refer to the lab report for detectable concentrations which did not exceed the 2L Standards, or for which no standard has been established.
MW-14
Page 2 of 2
Date: 10/14/2021
Method of Measurement:
Well ID
Product Type
(gas, diesel,
etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before
Recovery
(feet)
Product
Thickness
after
Recovery
(feet)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
08/16/17 Hand Bailing 4.08 0.00 7 5.3
05/21/18 - 05/26/18 MMPE 3.89 0.00 1,811 0.00
02/25/19 - 03/01/19 MMPE 0.06 0.00 1,968 0.00
11/26/19 AFVR 0.02 0.00 160 0.00
01/06/21 - 09/07/21 Boom 0.26 0.00 0.30 0.30
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• **: No free product was observed during initial gauging event; however, free product entered the well during purging activities.
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
TABLE 6
FREE PRODUCT RECOVERY RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID#: 0-026624
Interface probe at top-of-casing
2OilMW-1
Page 1 of 1
Date: 10/14/21
08/16/17 Hand Bailing ------------7 5.25 5.25
05/21/18 - 05/26/18 MMPE 54.72 85.37 577.16 2.17 1,811 0 2.17
02/25/19 - 03/01/19 MMPE 521 58.6 24.3 2.27 1,968 0 2.27
11/26/19 AFVR 1,459 77.8 13.9 0.42 160 0 0.42
01/06/21 - 09/07/21 Boom ------------0.03 0.03 0.03
4.86 3,946 5.28 10.14
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.15
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Total To Date 3,951.14 10.14
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Current Event 0.03 0.03
Totals
SUMMARY OF FLUID REMOVAL
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
MW-1
TABLE 7
FREE PRODUCT RECOVERY EVENT INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID #: 0-026624
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Page 1 of 1
Date: 01/16/20 Facility ID #: 0-026624
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered
(gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total fluids)Comments
MMPE 05/21/18 -
05/26/18 1,813.17 $8,142.85 $4.49 Cost per gallon for the event is based on a total volume of
1,813.17 gallons of free product and water.
MMPE 02/25/19 -
03/01/19 1,970.27 $7,977.80 $4.05 Cost per gallon for the event is based on a total volume of
1,970.27 gallons of free product and water.
AFVR 11/26/2019 160.42 $2,070.00 $12.90 Cost per gallon for the event is based on a total volume of
160.42 gallons of free product and water.
Boom 01/06/21 -
09/07/21 0.03 $37.09 $1,236.33 Cost per gallon for the event is based on a total volume of
0.03 gallons of free product and water.
3,943.89 $18,227.74 $4.62
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, MMPE sampling, MMPE sampling analytical and project
management.
MW-1
TOTAL (to date)
TABLE 8
FREE PRODUCT RECOVERY COST SUMMARY
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence
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4497 Received SEP 01 2021

APPENDIX B
Laboratory Report – Ground Water Samples
09/14/21
Technical Report for
GRI (Geological Resources Inc.)
RAM 9; 100 Jackson St, Rich Square, NC
2757
SGS Job Number: FA88686
Sampling Date: 09/07/21
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 09/14/21
e-Hardcopy 2.0
Automated Report
26
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1 of 26
FA88686
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA88686-1: MW-1 ........................................................................................................7
3.2: FA88686-2: MW-11 ......................................................................................................9
3.3: FA88686-3: MW-12 ......................................................................................................11
3.4: FA88686-4: MW-13 ......................................................................................................13
3.5: FA88686-5: MW-14 ......................................................................................................15
Section 4: Misc. Forms ............................................................................................................17
4.1: Chain of Custody ...........................................................................................................18
Section 5: MS Volatiles - QC Data Summaries .....................................................................20
5.1: Method Blank Summary ................................................................................................21
5.2: Blank Spike Summary ...................................................................................................23
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................25 123452 of 26
FA88686
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA88686
RAM 9; 100 Jackson St, Rich Square, NC
Project No: 2757
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA88686-1 09/07/21 11:40 JH 09/08/21 AQ Ground Water MW-1
FA88686-2 09/07/21 10:31 JH 09/08/21 AQ Ground Water MW-11
FA88686-3 09/07/21 10:42 JH 09/08/21 AQ Ground Water MW-12
FA88686-4 09/07/21 10:53 JH 09/08/21 AQ Ground Water MW-13
FA88686-5 09/07/21 11:04 JH 09/08/21 AQ Ground Water MW-14
3 of 26
FA886861
Summary of Hits Page 1 of 2
Job Number:FA88686
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:09/07/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88686-1 MW-1
n-Butylbenzene 0.25 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 2.4 0.50 0.13 ug/l SM 6200B
2,2-Dichloropropane 0.15 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 2.1 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 1.7 0.50 0.13 ug/l SM 6200B
Naphthalene 1.1 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.74 0.50 0.13 ug/l SM 6200B
Toluene 0.19 J 0.50 0.13 ug/l SM 6200B
FA88686-2 MW-11
n-Butylbenzene 0.17 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 6.0 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 4.1 0.50 0.13 ug/l SM 6200B
1,2-Dichlorobenzene 0.20 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.58 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 11.0 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.14 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.88 0.50 0.13 ug/l SM 6200B
Naphthalene 1.9 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.87 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.16 J 1.0 0.13 ug/l SM 6200B
o-Xylene 0.24 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.40 J 1.5 0.25 ug/l SM 6200B
FA88686-3 MW-12
Benzene 0.40 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.85 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.55 0.50 0.13 ug/l SM 6200B
Naphthalene 3.7 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.66 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2.0 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.26 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.4 1.0 0.13 ug/l SM 6200B
Xylene (total)1.4 J 1.5 0.25 ug/l SM 6200B
FA88686-4 MW-13
Benzene 48.6 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 2.7 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 2.3 J 2.5 0.63 ug/l SM 6200B
tert-Butylbenzene 0.67 J 2.5 0.63 ug/l SM 6200B
4 of 26
FA886862
Summary of Hits Page 2 of 2
Job Number:FA88686
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:09/07/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Di-Isopropyl Ether 1.8 J 2.5 0.63 ug/l SM 6200B
Ethylbenzene 119 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 8.9 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 2.8 2.5 0.63 ug/l SM 6200B
Methylene Chloride a 20.8 10 5.0 ug/l SM 6200B
Naphthalene 50.1 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 23.1 2.5 0.63 ug/l SM 6200B
Styrene 0.94 J 2.5 0.63 ug/l SM 6200B
Toluene 22.9 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 149 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 45.4 2.5 0.63 ug/l SM 6200B
m,p-Xylene 158 5.0 0.63 ug/l SM 6200B
o-Xylene 75.3 2.5 0.63 ug/l SM 6200B
Xylene (total)234 7.5 1.3 ug/l SM 6200B
FA88686-5 MW-14
sec-Butylbenzene 0.30 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 9.0 0.50 0.13 ug/l SM 6200B
(a) Suspected laboratory contaminant.
5 of 26
FA886862
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 26
FA886863
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA88686-1 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E108512.D 1 09/10/21 14:13 JL n/a n/a VE2540
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.25 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 2.4 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene a ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane 0.15 0.50 0.13 ug/l J
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 26
FA8868633.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA88686-1 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 2.1 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.7 0.50 0.13 ug/l
91-20-3 Naphthalene 1.1 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.74 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.19 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 26
FA8868633.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA88686-2 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E108513.D 1 09/10/21 14:36 JL n/a n/a VE2540
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.17 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 6.0 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 4.1 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene 0.20 0.50 0.13 ug/l J
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene a ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 26
FA8868633.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA88686-2 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.58 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 11.0 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.14 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.88 0.50 0.13 ug/l
91-20-3 Naphthalene 1.9 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.87 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.16 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.24 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.40 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 26
FA8868633.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA88686-3 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E108514.D 1 09/10/21 14:59 JL n/a n/a VE2540
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.40 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene a ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 26
FA8868633.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA88686-3 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.85 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.55 0.50 0.13 ug/l
91-20-3 Naphthalene 3.7 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.66 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2.0 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.26 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.4 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.4 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 26
FA8868633.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA88686-4 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E108519.D 5 09/10/21 16:52 JL n/a n/a VE2540
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 48.6 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 2.7 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 2.3 2.5 0.63 ug/l J
98-06-6 tert-Butylbenzene 0.67 2.5 0.63 ug/l J
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene a ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA8868633.4
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Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA88686-4 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.8 2.5 0.63 ug/l J
100-41-4 Ethylbenzene 119 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 8.9 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 2.8 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride b 20.8 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.63 ug/l
91-20-3 Naphthalene 50.1 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 23.1 2.5 0.63 ug/l
100-42-5 Styrene 0.94 2.5 0.63 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene 22.9 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 149 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 45.4 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 158 5.0 0.63 ug/l
95-47-6 o-Xylene 75.3 2.5 0.63 ug/l
1330-20-7 Xylene (total)234 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA8868633.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA88686-5 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E108515.D 1 09/10/21 15:21 JL n/a n/a VE2540
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.30 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene a ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 26
FA8868633.5
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Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA88686-5 Date Sampled:09/07/21
Matrix:AQ - Ground Water Date Received:09/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 9.0 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 26
FA8868633.5
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
17 of 26
FA886864
FA88686: Chain of Custody
Page 1 of 2
18 of 26
FA8868644.1
Job Number:FA88686 Client:GRI
Date / Time Received:9/8/2021 10:00:00 AM Delivery Method:FEDEX
Project:RAM #9
Airbill #'s:100963788812
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments SAMPLES 2 AND 3 RECEIVED WITHOUT TIME/DATE ON LABELS.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.4);
Cooler 1: (3.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:BRYANG Date:Date:9/8/2021 10:00:00 AM
FA88686: Chain of Custody
Page 2 of 2
19 of 26
FA8868644.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
20 of 26
FA886865
Method Blank Summary Page 1 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2540-MB E108511.D 1 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
21 of 26
FA8868655.1.1
Method Blank Summary Page 2 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2540-MB E108511.D 1 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
22 of 26
FA8868655.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2540-BS E108509.D 1 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.4 84 70-130
108-86-1 Bromobenzene 10 8.5 85 70-130
74-97-5 Bromochloromethane 10 7.6 76 70-130
75-27-4 Bromodichloromethane 10 8.3 83 70-130
75-25-2 Bromoform 10 8.2 82 70-130
104-51-8 n-Butylbenzene 10 8.8 88 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 8.9 89 70-130
56-23-5 Carbon Tetrachloride 10 8.7 87 70-130
108-90-7 Chlorobenzene 10 8.7 87 70-130
75-00-3 Chloroethane 10 9.9 99 60-140
67-66-3 Chloroform 10 8.5 85 70-130
95-49-8 o-Chlorotoluene 10 8.7 87 70-130
106-43-4 p-Chlorotoluene 10 8.8 88 70-130
124-48-1 Dibromochloromethane 10 8.0 80 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.6 76 70-130
106-93-4 1,2-Dibromoethane 10 8.2 82 70-130
75-71-8 Dichlorodifluoromethane 10 6.5 65 60-140
95-50-1 1,2-Dichlorobenzene 10 8.5 85 70-130
541-73-1 1,3-Dichlorobenzene 10 8.9 89 70-130
106-46-7 1,4-Dichlorobenzene 10 8.6 86 70-130
75-34-3 1,1-Dichloroethane 10 8.7 87 70-130
107-06-2 1,2-Dichloroethane 10 8.3 83 70-130
75-35-4 1,1-Dichloroethylene 10 10.3 103 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.6 86 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.3 83 70-130
78-87-5 1,2-Dichloropropane 10 8.5 85 70-130
142-28-9 1,3-Dichloropropane 10 8.1 81 70-130
594-20-7 2,2-Dichloropropane 10 9.2 92 70-130
563-58-6 1,1-Dichloropropene 10 8.5 85 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.2 82 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.8 88 70-130
108-20-3 Di-Isopropyl Ether 10 8.3 83 70-130
100-41-4 Ethylbenzene 10 8.8 88 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 9.1 91 70-130
* = Outside of Control Limits.
23 of 26
FA8868655.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2540-BS E108509.D 1 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 8.3 83 60-140
74-87-3 Methyl Chloride 10 8.0 80 60-140
74-95-3 Methylene Bromide 10 8.0 80 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.1 81 70-130
91-20-3 Naphthalene 10 8.7 87 70-130
103-65-1 n-Propylbenzene 10 8.9 89 70-130
100-42-5 Styrene 10 8.7 87 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.2 82 70-130
127-18-4 Tetrachloroethylene 10 8.7 87 70-130
108-88-3 Toluene 10 8.4 84 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.2 82 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.4 84 70-130
71-55-6 1,1,1-Trichloroethane 10 8.4 84 70-130
79-00-5 1,1,2-Trichloroethane 10 8.6 86 70-130
79-01-6 Trichloroethylene 10 8.4 84 70-130
75-69-4 Trichlorofluoromethane 10 9.1 91 60-140
96-18-4 1,2,3-Trichloropropane 10 8.3 83 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.5 85 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.6 86 70-130
75-01-4 Vinyl Chloride 10 8.2 82 60-140
m,p-Xylene 20 17.8 89 70-130
95-47-6 o-Xylene 10 8.8 88 70-130
1330-20-7 Xylene (total)30 26.6 89 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
24 of 26
FA8868655.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA88695-1MS E108534.D 100 09/10/21 JL n/a n/a VE2540
FA88695-1MSD E108535.D 100 09/10/21 JL n/a n/a VE2540
FA88695-1 E108533.D 100 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
FA88695-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 93.2 1000 1000 91 1000 997 90 0 70-130/20
108-86-1 Bromobenzene ND 1000 860 86 1000 896 90 4 70-130/20
74-97-5 Bromochloromethane ND 1000 808 81 1000 789 79 2 70-130/20
75-27-4 Bromodichloromethane ND 1000 845 85 1000 860 86 2 70-130/20
75-25-2 Bromoform ND 1000 814 81 1000 830 83 2 70-130/20
104-51-8 n-Butylbenzene 29.8 J 1000 894 86 1000 883 85 1 70-130/20
135-98-8 sec-Butylbenzene 27.3 J 1000 980 95 1000 989 96 1 70-130/20
98-06-6 tert-Butylbenzene ND 1000 901 90 1000 917 92 2 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 960 96 1000 928 93 3 70-130/20
108-90-7 Chlorobenzene ND 1000 894 89 1000 889 89 1 70-130/20
75-00-3 Chloroethane ND 1000 1450 145*1000 1350 135 7 60-140/20
67-66-3 Chloroform ND 1000 920 92 1000 904 90 2 70-130/20
95-49-8 o-Chlorotoluene ND 1000 927 93 1000 958 96 3 70-130/20
106-43-4 p-Chlorotoluene ND 1000 884 88 1000 914 91 3 70-130/20
124-48-1 Dibromochloromethane ND 1000 814 81 1000 825 83 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 760 76 1000 776 78 2 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 837 84 1000 848 85 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 835 84 1000 796 80 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 888 89 1000 897 90 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 925 93 1000 926 93 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 884 88 1000 893 89 1 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 954 95 1000 933 93 2 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 865 87 1000 856 86 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1260 126 1000 1180 118 7 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 936 94 1000 924 92 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 915 92 1000 898 90 2 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 884 88 1000 897 90 1 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 821 82 1000 840 84 2 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 841 84 1000 841 84 0 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 886 89 1000 866 87 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 784 78 1000 803 80 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 839 84 1000 864 86 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 888 89 1000 878 88 1 70-130/20
100-41-4 Ethylbenzene 2830 1000 3870 104 1000 3640 81 6 70-130/20
87-68-3 Hexachlorobutadiene 16.8 J 1000 859 84 1000 829 81 4 70-130/20
98-82-8 Isopropylbenzene 141 1000 1140 100 1000 1100 96 4 70-130/20
* = Outside of Control Limits.
25 of 26
FA8868655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA88686
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA88695-1MS E108534.D 100 09/10/21 JL n/a n/a VE2540
FA88695-1MSD E108535.D 100 09/10/21 JL n/a n/a VE2540
FA88695-1 E108533.D 100 09/10/21 JL n/a n/a VE2540
The QC reported here applies to the following samples:Method: SM 6200B
FA88686-1, FA88686-2, FA88686-3, FA88686-4, FA88686-5
FA88695-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 13.9 J 1000 915 90 1000 919 91 0 70-130/20
74-83-9 Methyl Bromide ND 1000 1150 115 1000 1260 126 9 60-140/20
74-87-3 Methyl Chloride ND 1000 1040 104 1000 950 95 9 60-140/20
74-95-3 Methylene Bromide ND 1000 809 81 1000 822 82 2 70-130/20
75-09-2 Methylene Chloride 277 1000 1160 88 1000 1250 97 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 1000 877 88 1000 854 85 3 70-130/20
91-20-3 Naphthalene 392 1000 1360 97 1000 1240 85 9 70-130/20
103-65-1 n-Propylbenzene 402 1000 1360 96 1000 1350 95 1 70-130/20
100-42-5 Styrene ND 1000 922 92 1000 909 91 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 872 87 1000 847 85 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 862 86 1000 879 88 2 70-130/20
127-18-4 Tetrachloroethylene ND 1000 914 91 1000 894 89 2 70-130/20
108-88-3 Toluene 40.3 J 1000 935 89 1000 928 89 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene 21.5 J 1000 878 86 1000 804 78 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene 17.5 J 1000 880 86 1000 824 81 7 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 936 94 1000 912 91 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 906 91 1000 870 87 4 70-130/20
79-01-6 Trichloroethylene ND 1000 903 90 1000 869 87 4 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 1290 129 1000 1200 120 7 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 883 88 1000 888 89 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1570 1000 2560 99 1000 2490 92 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 274 1000 1180 91 1000 1180 91 0 70-130/20
75-01-4 Vinyl Chloride ND 1000 1180 118 1000 1090 109 8 60-140/20
m,p-Xylene 3840 2000 5840 100 2000 5580 87 5 70-130/20
95-47-6 o-Xylene 40.3 J 1000 999 96 1000 963 92 4 70-130/20
1330-20-7 Xylene (total)3880 3000 6840 99 3000 6540 89 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA88695-1 Limits
1868-53-7 Dibromofluoromethane 102%99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%101%99%70-130%
2037-26-5 Toluene-D8 100%98%97%70-130%
460-00-4 4-Bromofluorobenzene 95%99%96%70-130%
* = Outside of Control Limits.
26 of 26
FA8868655.3.1