RA-1468_9329_CA_SAR_20041008_UNKNOWN

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October 8. 2004
Mr. Mickey Roberts
NCDENR
Division of Waste Management
UST Section
Raleigh Regional Oflicc
1628 Mail Service Center
Raleigh. NC 27699-1628
RE: Soil Assessment Report
RAM #5
HWY !58 East
Facility ID # 0-026626
Jackson, Northampton County. NC
Incident No. 9329
CES l'roject No. 01-105
Dear Mr. Roberts:
857 West Main Street
Murfreesboro, NC 27855
Phone: [phone]
Fox: 252.398.4768
Enclosed please lind a copy of the Soil Assessment Report for the above referenced site.
Please contact me at [phone] if you have any questions.
Sincerely yours,
CES ENGINEERING, PC
Leigh Sumner
Geologist
COMPLIANCE ASSESSMENT REMEDIATION
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Prepared by:
'-~-/
Leigh Sumner
Project Geologist
Soil Assessment Report
Red Apple Market #5
Highway 158
Jackson, Northampton County. NC
Facility ID # 0-026626
By:
CES Engineering, PC
857 W. Main Street
Murfreesboro, North Carolina
CES No. 08-240
October 8, 2004
Reviewed by:
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Soil A.ue.1·sment Report
Red Apple Market #5
I 01 West .Jefferson Street!NC I /11)' /58
Jackson. Northampton County, Nor!h Carolina
1.0 Site History
CES. Engineering, I'.C
October 8, 200./
Jncide111 # 9329
CE.\' # 01-105
This report is prepared for Eastern Fuels, Inc .. to summarize soil assessment activities
conducted at the Red Appk Market #5 Underground Storage Tank (UST) site. In
September I 992, Coastal Environmental Services, Inc .. (CES) conducted UST closure
and assessment activities in conjunction \Vith the removal of one 1000-gallon gasoline
and three 4.000-gallon gasoline USTs (Table 1 ). Soil in the immediate vicinity of tank
was analyzed for total petroleum hydrocarbons (TPH) by methods 3550/5030. The
contaminated soil was excavated vertically and horizontally until groundwater was
encountered and laterally until TPH concentrations were below the laboratory detection
limit. A new UST system was then installed.
CES conducted a Phase I Groundwater Quality Assessment in August 1993 to evaluate
the extent of groundwater contamination at the site. Three North Carolina Type II
monitoring wells were installed and sampled during this event. According to laboratory
results, levels of dissolved phase petroleum hydrocarbons were present above the NCAC
2L standards within groundwater sampled at this site. A Phase II Groundwater Quality
Assessment was conducted during October 1994 at the subject l~tcility to further assess
the extent of groundwater contamination at the site. Three North Carolina Type I I
monitoring wells along with one North Carolina Type Ill monitoring well were installed
and sampled during Phase II activitie:->. According to laboratory results, levels of
dissolved phase petroleum hydrocarbons were present above the NCAC 2L standards
within groundwater sampled at this site.
On Fchruary 26, 2004 the NCDENR issued a Notice of Regulatory Requirements
(NORR) to Eastern Fuels, Inc requesting a Phase II Limited Site Assessment (Phase II
LSA). Assessment activities included seven groundv,•atcr samples. one soil sample and an
updated receptor survey. According to laboratory results, levels of dissolved phase
petroleum hydrocarbons wcrc present abovc the NCAC 2L standards within groundwater
}'age 1
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.)'oil As.1essmen1 Repr1rl
Red Apple ,\4arket #5
I 01 We.~/ Jefferson ,\'rreer/NC 1/1!:\' /58
.Jack..wn. Northampum County. Norrh Carolina
CES. Engineering. P.C.
Octoher 8. 201J.I
fncidem # Y32Y
CES # 01-105
sampled at the site. A Light Non-Aqueous Phase LiquiJ (LNAPL) was recovered from
monitoring well MW-1. The one soil sample. based on laboratory results. did not contain
constituents above standards (Table 2). A Phase II LSA was submitted August 2004.
Following review of the report the NCDENR issued a NORR requesting the assessment.
removal and cleanup of contaminated soil and free product (Appendix A). The site was
ranked as residential land use with intermediate risk class!fication. The following report
addresses soil assessment preformed on September 17,2004.
The Red Apple Market #5 has been dosed. the USTs have been pumped of contents and
the site is currently fOr sale.
2.0 Risk Assessment
Land usc in the area around the RAM #5 facility was reported in the Phase II LSA to
consist of residential. industrial. as well as commercial areas. The Northampton County
Courthouse and Sheriff Office along \Vith numerous law oflices surround the subject site.
Residential homes and local businesses are also located within a 1500' radius from the
source area.
The Town of Jackson receives its water from two water supply wells located outside the
1500 foot radius of the site. Water storage tanks arc located 200 and 1400 feet from the
tank bed. According to the NCDENR Public Water Supply Section, a Wellhead
Protedion Plan has not been established for the Town of Jackson. There are no domestic
supply wells within the 1.500' radius of this site. A copy of the Phase II Sensitive
Receptor Survey has been included as Appendix B. Table 3 provides a list of property
owners within a 1500 foot radius of the site.
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,)'oil Assessment Report
Red Apple 114arker #5
I 0 I West .Jejfi!r.\·on Street!NC J lwy /58
Jackson, Nnrtlwmpton Coullfy. North Carolina
3.0 Regional Geology
Ct~·s. Engineering, I'.C
Octoher 8. 200.J
Incident# 9329
C£,<.,'/1 01-105
The geology of North Carolina can be generally divided into two basic rock types-the
unconsolidah.:d sediments of the Coastal Plain lm:atcd east of the Fall Line, and the
crystalline ro~.:ks of the Blue Ridge and Piedmont Physiographk Provinces, located west
of the Fall Line. Northampton County is located in the northeastern part of the state. in
the Coastal Plain Physiographic Province. The Town of Jackson is situated on the central
cash:rn part of the county. within the Coastal Plain Province.
The Topography of the Coastal Plain can be described as mostly leveL with elevations
ranging Ji·om 400 feet ncar the Fall Line to sea level feet near the coast. Geologically. the
Jackson area is within the Coastal Plain. Crystalline bedrock in this area generally
consists of metamorphosed granitic rocks, which include granite, gneiss. and schist. The
crystalline bedrock is covered by many layers of sand and silty clays. which separate the
surficial aqui!Cr from deeper aquiJCrs in the region. Most municipal \Vater supplies are
drawn from these deeper aquifers for public water location. The groundv,:atcr from the
Woodland area occurs in the surficial aquifer as well as deeper aquifers. which are
separated by confining layers of clay and silty clay.
4.0 Site Geology
The facility is located within the Atlantic Coastal Plain physiographic province.
Regionally. the entire area is underlain with a thick Wl:dge of sedimentary deposits that
dip gently seaward. An extensive sequence of interbedded sands, clays and limestone's
of Cretaceous to Tertiary age underlie the surficial deposits.
In Northampton County, the surficial deposits arc predominantly arenaceous and have an
average thickness of forty JCet. These deposits arc underlain hy the Castle Hayne
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Soil Assc.1·snwnt Report
Red Apple Market #5
101 West .Jefferson ,\'tree/INC 1!11~1' /5r'J
Juchwn. NorthamptmJ County. North Carolina
(.'H,'I'. Engineering, P. C.
October 8, 200./
f11ciden1 # 9329
CES # 01-105
Formation of Tertiary age. The surlicial deposits arc a common source of domestic water
in the area.
5.0 Discussion of Soil Sampling Results
Twelve soil samples were taken at the RAM #5 site on September 7, 2004. The soil
samples were analyzed for total solids, volatile petroleum hydrocarbons (VPH) and
\'Oiatilc organics using Environmental Protection Agency (EPA) Method 8260. A
distribution map illustrating soil locations found as Figure 2. A summary of the soil
analytical data from the current soil sampling event is included in Table 2. A summary or
field activities is included in Table 4. A copy or the most recent laboratory analytical
report for the soil sample is included in Appendix C.
5. I Field Activities
Field personnel met on site at approximately 9 am on September 7, 2004. After
soil locations and utilities were flagged, drilling activities began via geoprobe
methodology. The following is an account of field activities:
I. Alh:r recovery of each of the eight foot cores. the entire core was logged
in respect to lithology and overall observation of the soil.
2. Soil samples for laboratory testing wen: acquired at approximately eight
feet below land surface.
3. Each soil sample was screened for total volatiles using a handheld OVA
meter and then stored in the appropriate laboratory containers.
4. The soil laboratory containers were packaged in iced coolers with
appropriate chains of custody and sent to an approved laboratory v1a
Fed Ex.
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Soil Assessme/11 Report
Ned Apple Market #5
CES. Engineering, I'. C.
Octoher 8. 200-1
Incident # 9329
CE'I # Ol-105
I 0 I West Jefferson Street!A'C //11~\' /58
Jackson. Nonhamp/1!11 Crmmy, North Carolina
6.0
5.2 LahomiOIT Ana!J'Ikai Res1tlts
Comparing the results of the analytical hydrocarbon fractions to the Maximum
Soil Contaminant Concentrations (MSCC) for the toxicologically delined. the
hydrocarbon fractions show contamination levels above the Soil lo Wafer
,)'tandard\· for C5-C8 Aliphatic and Benzene. A summary of the soil analytical data
from the current soil sampling event is included in Table 2.
Conclusions and Recommendations
Based on a rcv1cw of the infonnation gathered during this Soil Assessment. CES
Engineering concludes the following:
• Soil apparently has been impacted due to the release at this site.
• LNAPL was found within one of the monitoring wells on site during the previous
groundwater sampling event. Although a soil sample was recovered in
approximate location to this monitoring welL contaminant concentrations within
the soil appear below laboratory quantitati\'e limits.
• The Town of Jackson receives its water from two water supply wells located
outside the 1500 foot radius of the site.
• The soil and groundwater at this site is capped by the former Red Apple Markel I # 5 building and pavement for most of the area. The Red Apple Market #5 has
been closed and the site is currently for sale.
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• CES Engineering, P.C. nx:ommends the submittal of a Soil Cleanup Plan.
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.'loi/ Asses.l'me/11 Report
Red Apple Market #5
I 0 I West .!e,fferson .'·!treetiNC HIIJ' /58
Jackson. Northampton County, Nonh Carofina
6.0 Limitations
CES, Engineering, I'. C.
Ocrober 8, 2(}().1
lncidellf ii 9329
CES # 01-105
This report is based on a limited number of samples and chemical analyses. The
conclusions presented in this report arc based only on thl: observations made during this
investigation and data provided by others. The report presents a dcscription of the soil
subsurl'ucc conditions observed during this investigation. Subsurface conditions may
vary significantly \Vith time. particularly with respect to groundwater elevations and
quality. Conclusions and recommendations set forth herein arc applicable only to the
facts and conditions described at the time of this rcporl.
In performing its professional .services, CES Engineering. PC uses that degree of care and
skill exercised under similar circumstances by members of the environmental profC.ssion
practicing in the .same or similar locality under similar conditions. The standard of care
shall be judged exclusively as of the time these services arc rendered and not according to
later standards. CES Engineering, PC makes no express or implied warranty beyond its
conformance to this standard. CES Engineering, PC shall not be responsible for
conditions or consequences arising from rdevant facts that were concealed withheld or
not fully disclosed for this report. CES Engineering, PC believes that all information
contained in this report is factual. but no guarantee is made or implied.
Paj!,e 6
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Tank
No.
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2
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4
Tank
No.
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2
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Size
(gallons)
1.000
4.000
4.000
4.000
Size
(gallons)
4.000
6.000
10.000
Table I
UST Information
Red Apple Market #5
NC Highway 158
Jackson, Northampton County NC
Date
Installed
UnknO\•m
Unknown
Unknown
Unknown
Date
Installed
1992
1992
1992
Date Removed Tank Or Closed In
Place Construction
\992 Steel
1992 Steel
1992 Steel
1992 Steel
UST Information
Red Apple Market #5
NC Highway 158
Jackson, Northampton NC
Date Removed Tank Or Closed In
Place Construction
N/A Fihcrstccl
N/A Fihcrstecl
N/A Fiberstecl
Last Previous
Contents (if Contents anv)
Gasoline N/A
Gasoline N/A
Gasoline N/A
Gasoline NIA
Last Previous
Contents (if Contents anvl
Kerosene N/A
Gasoline N/A
Gasoline N/A
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Samp/e!D
GP-1@ 8-10·
GP-1@ 8-10'
GP-2@ 8-\0'
GP-3@ 8-10'
GP-4@ 8-10'
GP-5@ 8-10'
GP-6@ 8-10·
GP-7@ 8-10"
GP-8@ 8-10'
GP-9@ 8-10'
GP-\0@ 8-10'
GP-11@ 8-10·
GP-12@8-10'
Date Acetone
H(lkg
06/16/04 <0.032
09/09/04 <0.030
09/09/04 <0.030
09/09/04 <0.030
09/09/04 <3.0
09/09/04 1.5
09/09/04 <\.5
09/09/04 <3.1
09/09/04 <0.030
09/09/04 0.043
09/09/04 <0.031
09/09/04 <0.030
09/09/04 0.036
156-1
-10880
3
4-Chloro-Cs-C8 Benzene toluene Aliphatic H(!kg pg/kg H(lkg
<0.013 <0.0013 <6.5
<0.00\2 <0.0012 <8.7
<0.0012 <0.0012 <7.7
<0.0012 <0.0012 <3.5
<0.0012 <0.12 8.6
<0.060 <0.060 <7.8
<0.0012 <0.062 <8.0
"CO~i32 <0.12 C7?
<0.0012 <0.0012 <6.7
<0.0012 <0.0012 <8.8
<0.0012 <0.0012 <9.6
<0.0012 <0.0012 <4.4
<0.0012 <0.0012 <5.0
22 -939
200 -2-1528
0. 0056 -71
C,-Cn
Aliphatic
pglkg
47
<8.7
<7.7
<3.5
11
<7.8
<8.0
58
<6.7
<8.8
<9.6
<4.4
<5.0
9386
J./5,280
3255
Table 2
Summary of Soil Sample Results
Red Apple Market #5
400 West Jackson Street
Rich Square. Northampton County, NC
c,...c10 Ethyl-Isopropyl-Sec-
Aromatics benzene benzene Butyl-
benzene pg/kg H(lkg pg/kg !k.
38 <0.0013 0.011 0.064
<8.7 <0.0012 0.0049 0.0039
<7.7 <0.0012 0.011 0.014
<3.5 <0.0012 <0.0012 <0.0012
7.2 lfu' 0.36 0.15
<7.8 0.084 <0.060 <0.060
<8.0 0.065 0.062 <0.062
25 0.13 <0.12
<6.7 <0.0012 <0.0012 <0.0012
<8.8 <0.0012 <0.0012 <0.0012
<9.6 <0.0012 <0.0012 <0.0012
<4.4 <0.0012 <0.0012 <0.0012
<5.0 <0.0012 <0.0012 <0.0012
9386 1560 156-1 156
2-15,280 41/000 -10880 4088
3255 0.2-1 1 3
Tert-·-Tri~;t~yl-Tri~t!yt-p-
Butyl-Propyl-MTBE Naphthalene Isopropyl-Xylenes
benzene benzene benzene benzene H(!kg H(!kg toluene H:lkg
""/kp /k, UI!Ik• l11! lk• ~.
<0.0013 0.014 <0.0013 <0.0013 <0.0013 <0.0065 0.012 <0.0039
0.0014 0.0081 <0.0012 <0.0012 <0.00\2 <0.0061 <0.0012 <0.0037
0.0026 0.023 <0.0012 <0.0012 <0.00\2 <0.0059 0.0054 <0.0036
<0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0060 <0.0012 <0.0036
<0.12 0.72 1.4 0.91 <0.12 <0.60 0.20 <0.36
<0.060 <0.060 0.26 0.10 <0.060 0.30 <0.060 0.37
<0.062 <0.062 0.13 <0.062 <0.062 <0.31 <0.062 0.27
<0.12 0.24 1.6 0.62 <0.12 <0.62 <0.12 2.4
<0.0012 <0.0012 <0.0012 <0.0012 0.0020 <0.0061 <0.0012 <0.0036
<0.0012 <0.0012 <0.0012 <0.0012 0.017 <0.0062 <0.0012 <0.0037
<0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0062 <0.0012 <0.0037
<0.0012 <0.0012 <0.0012 <0.0012 <0.0012 <0.0059 <0.0012 <0.0036
<0.0012 <0.0012 <0.0012 <0.0012 0.036 <0.0061 <0.0012 <0.0037
!56 /56 782 782 !56 63 -32.000
-1088 -1088 20-1-10 20-1-10 4088 1635 -200,000
3 1 8 7 0.92 0.58 -5
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GIS Pin Number
4966-54-3431
4966-54-070 I
4966-54-0607
4966-54-0604
4966-54-0640
4966-54-0516
4966-54-5806
4966-54-5713
4966-54-5615
4966-54-4670
4966-54-4545
Table3
Adjacent Property Owners
Red Apple Market #5
NC Hwy 158
Jackson, Northampton County NC
Property Owner Name Mailing Address
Eastern Fuels. Inc. PO Box 1386
Ahoskie, NC 27910
David and Mary Bridger PO Box 592
Ahoskie, NC 27910
John McKellar PO Box 868
Jackson, NC 27845
RJ White. Ill 1599 Vaughan Creek
Pendleton. NC 27862
Northampton Co. PO Box 637
Jackson, NC 27845
Frank White PO Box 446
Jackson. NC 27845
Janie Lewis POBox37
Jackson. NC 27845
Janie Lewis PO Box 37
Jackson, NC 27845
John R. Mitchell 54 Pine Lane
Windsor. Va. 23487
Northampton Co. PO Box 63
Jackson, NC 27845
P0Box614 Town of Jackson Jackson. NC 27845
Distance from
Water Siie to
Source Domestic
Well
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
City Water N/A
N/A
City Water
-------------------
Distance from
GIS Pin Number Property Owner Name Mailing Address Water Site to
Source Domestic
Well
4966-54-5505 Felton Turner Jr. PO Box 398 City Water NIA Jackson. NC '7845
4966-54-5545 Felton Turner Jr. PO Box 398 City Water N/A Jackson, NC 27845
4966-54-5587 Alice M. Warner PO Box 201 City Water NIA Jackson. NC 27845
4966-54-6884 William Cooley PO Box4l6 Citv Water N/A Jackson. NC 27845
4966-54-6671 JC and Winston Callahan Ill POBox412 City Water N/A Jackson. NC '7845
4966-54-8844 BH Harrell PO Box 365 City Water N/A Jackson. NC 27845
4966-54-8631 Brodie Harrell Jr. PO Box 96 City Water N/A Jackson. NC 1 7845
4966-54-0329 Lawrence Vaughan PO Box 26 City Water N/A Jackson. NC 27845
4966-54-0379 Lawrence Vaughan PO Box 26 City Water N/A Jackson. NC 27845
4966-54-14 72 Northampton Co. PO Box 637 City Water N/A Jackson, NC 27845
4966-54-1430 Northampton Co. PO Box 637 City Water N/A Jackson, NC 27845
4966-54-1398 Northampton Co. PO Box 637 City Water N/A Jackson, NC 27845
4966-54-123 7 Northampton Co. PO Box 637 City Water NIA Jackson, NC 27845
4966-54-0207 Fanners Gin Co. Inc. PO Box 703 City Water NIA Jackson. NC 27845
-------------------
Distance
GIS Pin Property Owner Name Mailing Address Water from Site to
Number Source Domestic
Well
4966-54-0256 Northampton Co. PO Box 637 City Water NIA Jackson. NC 27845
4966-54-0031 Lawrence Vaughan PO Box 25 City Water N/A Jackson. NC 27845
4966-54-3324 Town of Jackson POBox614 City Water N/A Jackson, NC 27845
PO Box 614 Water Approximately 4966-54-4304 Town of Jackson Storage Jackson, NC 27845 Tower 200 feet
4966-54-3340 Jackson Vol. Fire Department PO Box 545 City Water N/A Jackson. NC 27845
4966-54-4410 Carolina Telephone and Telegraph 6100 Sprint Parkway City Water N/A Ahoskie. NC 27910
4966-54-3246 Vcmice Long PO Box 230 City Water N/A Rich Square. NC 27869
4966-54-3129 Viola Doles 2330 sm Ave. Apartments Citv Water NIA New York. NY 10037
4966-54-2072 Robert Keer PO Box 691 City Water N/A Jackson, NC 27845
4966-54-4392 Larry Moses PO Box 805 City Water N/A Jackson. NC 27845
4966-54-5390 Lloyd Martin P0Box651 City Water N/A Jackson, NC 27845
4966-54-6249 Harold Miller 567 Miller Trail City Water N/A Jackson, NC 27845
4966-54-730 I Wilbur Crawley PO Box 506 City Water N/A Jackson, NC 27845
4966-54-8306 Paul Calvert 51 00 Dorsett Ave. City Water N/A Cherrv Chase. MD 20815
-------------------
Distance
GIS Pin Property Owner Name Mailing Address Water from Site to
Number Source Domestic
WeD
4966-53-4613 Bain Cotton Co. PO Box 632 City Water N/A Jackson. NC 27845
4966-53-1691 Bain Cotton Co. PO Box 632 City Water N/A Jackson, NC 27845
City
4966-53-2387 Bain Cotton Co. PO Box 632 Water/Water Approximately
Jackson, NC 27845 Storage 1400 feet
Tank
4966-53-2091 Boones Fann Supply PO Box 428 City Water N/A Jackson. NC 27845
4966-53-7569 Bain Cotton Co. PO Box 632 City Water N/A Jackson. NC 27845
4966-64-1387 Northampton Co. ABC Board PO Box 277 City Water N/A Jackson, NC 27845
4966-64-3317 James Barnes 6864 NC IIWY 305 City Water N/A Jackson, NC 27845
4966-64-5314 Amicus Investments. LLC PO Box 3425 City Water N/A Greenville, NC 27836
4966-64-5213 Farrow & Sons, LTD PO Box 807 City Water N/A Jackson. NC 27845
4966-64-5384 Amicus Investments. LLC PO Box 3425 City Water N/A Greenville. NC 27836
4966-64-7368 Eddie Mason PO Box 233 City Water N/A Jackson, NC 27845
4966-64-7302 Town of Jackson POBox614 City Water NIA Jackson, NC 27845
4966-64-7258 Eddie Mason PO Box 233 City Water N/A Jackson, NC '7845
4966-64-7139 Buster Faison PO Box 361 City Water N/A Jackson, NC 27845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-64-7173 Buster Faison PO Box 361 City Water N/A Jackson, NC 27845
4966-64-8014 Buster Faison P0Box361 City Water N/A Jackson, NC 27845
4966-63-7933 Percy and Althea Henderson 44 Hillcrest Terrace City Water N/A East Orange, NJ 07018
4966-63-5000 Percy and Althea Henderson 44 Hillcrest Terrace City Water N/A East Oran!le. NJ 07018
4966-63-3978 Napoleon Grant PO Box 951 City Water N/A Jackson. NC '7845
4966-63-4935 Charles Benthall PO Box !54 City Water N/A Conwav. NC 27820
4966-63-5901 Eddie & Novella Mason PO Box 233 City Water N/A Jackson, NC 27845
4966-63-6915 Dorothy Jones PO Box 494 City Water N/A Jackson, NC 27845
4966-63-6808 Eddie & Novella Mason PO Box 233 City Water N/A Jackson, NC 27845
4966-63-6802 Pearl Grant 1913 Callaway Street City Water N/A Temole Hills. MD 20748
4966-63-783 I Mary Rispee 1519 W Street SE City Water N/A Washin2ton. DC 20020
4966-63-6721 Eleanor Harris PO Box 334 City Water N/A Jackson, NC 27845
4966-63-5754 Carlily Joyner Heirs P0Box413 City Water N/A Jackson. NC ?7845
4966-63-4842 Robert & Mary Davis PO Box 472 City Water N/A Jackson, NC 27845
4966-63-3669 Hattie Boone Heirs 1736 NC Hv.'Y 45 S City Water N/A Cofield, NC 27922
--------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-63-1484 Pontiac Plywood. Inc. 5829 Countryside Road City Water N/A Wilson. NC 27896
4966-63-4611 Ellis & Lottie Joyner 1008 Edgewood Road City Water N/A Philadelphia. PA 19151
4966-63-5506 Mason Hendrick Heirs 80 I Cambridge CouJ1 City Water N/A Roanoke Rapids. NC 27870
4966-62-6719 Harold Thrasher 710 Sign Pine Road City Water N/A Chesapeake. Va. 23322
4966-34-8836 Rctty Leigh Lee 1747 Powder Horn Terrace City Water N/A Woodbridge, Va. 22191
4966-34-9835 Peggy Bullock Bright PO Box 402 City Water N/A Jackson. NC 27845
4966-34-9878 Elmo Cordle PO Box 339 City Water N/A Seaboard. NC 27876
4966-44-0806 Leslie & Lois Bullock PO Box 402 City Water N/A Jackson. NC 27845
4966-34-9631 Ronald & Jerilyn Boone PO Box 607 City Water N/A Jackson. NC 27845
4966-34-6585 Strickland Associates. Inc. PO Box 373 City Water N/A Roanoke Rapids, NC 27870
4966-34-8229 New Dixie Oil Co. PO Box 779 City Water N/A Roanoke Rapids. NC 27870
4966-34-5298 Jean Boone PO Box 7 City Water N/A Jackson, NC 27845
4966-34-7093 Newsome Oil Company 1503 W I om Street City Water N/A Roanoke Rapids, NC 27870
4966-34-9023 Newsome Oil Company 1503 W I 01 Street City Water N/A Roanoke Rapids. NC 27870
4966-44-1838 John & Derother Thomas PO Box 182 City Water N/A Jackson. NC 27845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-44-2899 John & Derother Thomas PO Box 182 City Water N/A Jackson. NC 27845
4966-44-3895 Luther & Virginia Staples PO Box 424 City Water N/A Jackson. NC 27845
4%6-44-4859 Trustees Protestant Episcopal Church P0Box613 City Water N/A Jackson, NC 27845
4966-44-4899 Trustees Protestant Episcopal Church POBox613 City Water N/A Jackson. NC 27845
4966-44-5859 Trustees Protestant Episcopal Church P0Box613 City Water N/A Jackson, NC 27845
4966-44-6896 Carl E. Witt PO Box 1023 City Water N/A Jackson, NC 27845
4966-44-9819 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte. NC 28270
4966-44-9800 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte, NC 28270
4966-44-9785 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte, NC 28270
4966-44-7793 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte. NC 28270
4966-44-6697 Ruby Storey 408 Bryantown Road City Water N/A Rich Square. NC 27869
4966-44-6660 James Odom POBox312 City Water N/A Jackson. NC 27845
4966-44-6564 James and Doris Odom P0Box3l2 City Water N/A Jackson. NC 27845
4966-44-7589 Double S. Inc. 408 Bryantown Road City Water N/A Rich Square. NC 27869
4966-44-7698 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte, NC 28270
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-44-7793 Barbara Bowers 6929 Folger Drive City Water N/A Charlotte. NC 28270
4966-44-9608 Mal)' Outland P0Box410 City Water N/A Rich S(luare, NC 27869
4966-44-8576 Doylt: Taylor PO Box 1203 City Water N/A Newoort NC 28570
4966-44-9506 Futrell Phannacy, Inc. PO Box 768 City Water NIA Jackson, NC 27845
4966-44-9526 Harold Lee Massey PO Box 206 City Water N/A Jackson. NC 27845
4966-44-9546 George & Jcneane Drewctte 3727 Mt. Cannel Road City Water N/A Jackson, NC 27845
4966-44-9586 Northampton Co. Farm Bureau PO Box 645 City Water N/A Jackson. NC 27845
4966-44-2030 Selma Jameson PO Box 236 City Water N/A Jackson. NC 27845
4966-34-7093 Newsome Oil Co. 1503 W 1Oth Street City Water N/A Roanoke Raoids, NC 27870
4966-34-9023 Newsome Oil Co. 1503 W I it" Street City Water N/A Roanoke Raoids. NC 27870
4966-44-3223 RJ & Lillian Riggs PO Box 462 City Water N/A Jackson, NC 27845
4966-44-4295 Northampton Co. PO Box 637 City Water NIA Jackson. NC 27845
4966-44-5377 Northampton Co. Museum, Inc. PO Box 664 City Water N/A Jackson. NC 27845
4966-44-6465 John Odom 45 River Drive City Water NIA Passaic, NC 07055
4966-44-6480 James & Alice Wesley 9668 NC Hwy 305 City Water N/A Jackson. NC ?7845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-44-7400 Joe & Shirley Joyner PO Box 443 City Water N/A Jackson. NC 27845
4966-44-7339 Mary Bowers 5213 Chandler Street City Water N/A Bethesda. MD 20814
4966-44-7360 Mary Bowers 5213 Chandler Street City Water N/A Bethesda. MD 20814
4966-44-8309 Jean Boone PO Box 7 City Water N/A Jackson, NC 27845
4966-44-8329 Edith Lorra Ramsley 934 Occoneechee Neck South Road City Water N/A Jackson. NC 27845
4966-44-8359 Harold & Shirley Wray PO Box P City Water N/A Gaston, NC 27832
4966-44-9318 Harold & Shirley Wray PO Box P City Water NIA Gaston, NC 27832
4966-44-9359 Harold & Shirley Wray PO Box P City Water N/A Gaston, NC 27832
4966-44-9226 Harold & Shirley Wray PO Box P City Water N/A Gaston, NC 27832
4966-44-8276 Harold & Shirley Wray PO Box P City Water N/A Gaston, NC 2783'
4966-44-8236 Fanners Gin Co. Inc. PO Box 703 City Water NIA Jackson. NC 27845
4966-44-8206 Farron & Sons LTD PO Box 807 City Water N/A Jackson. NC 27845
4966~44-7237 Town of Jackson PO Box 614 City Water N/A
Jackson. NC 27845
4966-44-6267 Farmers Gin Co., Inc. PO Box 703 City Water N/A
Jackson. NC 27845
4966-44-6065 VEPCO (NC Po\ver) Roanoke Rapids, NC 27870 City Water N/A
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-44-9182 Eastern Fuels. Inc. POBox 1386 City Water N/A
Ahoskie. NC 27910
4966-44-0090 Newsome Oil Co .. Inc. 1503 W I 01 Street City Water N/A
Roanoke Ranids. NC 27870
4966-43-4962 Farmers Gin Co., Inc. PO Box 703 City Water N/A
Jackson. NC 27845
4966-43-3615 Stuart F. Bowers PO Box 308 City Water N/A
Jackson, NC 27845
4966-43-3588 Stuart F. Bowers PO Box308 City Water N/A
Jackson. NC 27845
4966-43-6452 L.F. & Marian Pearce 11419 Soward Drive City Water N/A
Kensington, MD 20895
4966-44-2030 Selma Jameson PO Box 236 City Water N/A
Jackson, NC 27845
4966-43-7216 Lottie Brdl Joyner PO Box 803 City Water N/A
Jackson, NC 27845
4966-43-6125 Rosanna Joyner PO Box 396 City Water N/A
Jackson. NC 27845
4966-43-9404 Willie & Luther West 888 So~th \9w Street City Water N/A
Newark. NJ 07108
4966-43-9511 Midway Land Developers. Inc. 888 South 191h Street City Water N/A
Newark. NJ 07108
4966-43-9539 Midway Land Developers. Inc. 888 So~th I §Ill Street City Water N/A
Newark. NJ 07108
4966-43-8546 Midway Land Developers, Inc. 888 South \9 Street City Water N/A
Newark. NJ 07108
4966-43-8527 Novello Branch PO Box 426 City Water N/A
Jackson. NC '7845
4966-43-7588 Midway Land Developers. Inc. 888 South 19 Street City Water N/A
Newark. NJ 07108
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-43-7631 Alpha & Omega Holy Temple 2084 State 1-lwy 27 City Water NIA
New Brunswick, NJ 8902
4966-43-8668 Maizie Boone 888 South \9 Street City Water NIA
Newark. NJ 07108
4966-43-8775 Midway Land Developers. Inc. 888 South 19m Street City Water NJ,o..
Newark. NJ 07108
4966-43-8872 Midway Land Developers. Inc. 888 South 19 Street City Water N/A
Newark. NJ 07108
4966-43-9874 Janie Harris PO Box 574 City Water NIA
Jackson. NC 27845
4966-43-7944 Farmers Gin Co .. Inc. PO Box 703 City Water NIA
Jackson. NC 27845
4966-42-8948 Gary Bridgers 3500 School House Lane City Water NIA
Charlotte. NC 28226
4966-55-5915 Jackson Lions Club PO Box 453 City Water NIA
Jackson. NC 27845
4966-55-5710 Timothy & Cheryl Boone PO Box 508 City Water N/A
Jackson. NC 27845
4966-55-5515 Jerry and Judy Beasley PO Box 672 City Water NIA
Jackson. NC 27845
4966-55-5413 Henry Harris Jr. 331 Carlton Drive City Water NIA
Chapel Hill. NC 27516
4966-55-5229 William & Margaret Martin PO Box 5 City Water NIA
Jackson. NC 27845
4966-55-3016 Gary & Pamela McCullough 3424 Chardmore Drive City Water NIA
Matthews, NC 28105
4966-55-2025 Paul & Dixie Harrell PO Box 266 City Water NIA
Jackson. NC 27845
4966-55-2296 Paul & Dixie Harrell PO Box 266 City Water N/A
Jackson. NC 27845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-55-1240 Garland & Traci Storey POBox216 City Water N/A
Jackson, NC 27845
4966-55-0320 Jackson Methodist Church PO Box 121 City Water N/A
Jackson, NC 27845
4966-55-0422 Jackson Methodist Church PO Box 121 City Water N/A
Jackson. NC 27845
4966-55-0427 Jackson Methodist Church POBox\21 Cit~y Water N/A
Jackson, NC 27845
4966-55-4047 Paul Barrett Jr. PO Box 623 City Water N/A
Jackson. NC 27845
4966-55-5008 Duncan Jones PO Box 338 City Water N/A
Jackson. NC 27845
4966-55-5068 Willie Barnes 6!3 Drexel Drive City Water N/A
Rockv Mount. NC 27803
4966-55-6018 Branch Banking & Trust Co. PO Box 1847 City Water N/A
Wilson. NC 27894
4966-55-6088 Jean C. Boone PO Box 7 City Water N/A
Jackson. NC 27845
4966-55-7078 James & Bonnie Boone PO Box 535 City Water N/A
Jackson. NC 27845
4966-55-8!68 Mary Burgwyn PO Box 72 City Water NIA
Jackson. NC 27845
4966-55-8457 Mary Burgwyn PO Box 72 City Water N/A
Jackson. NC 27845
4966-66-5149 E.W. Lewis PO Box 768 City Water NIA
Jackson. NC 27845
4966-45-4808 J.A. & Alexis Boone PO Box 29 City Water N/A
Hatteras. NC 27943
4966-45-4737 Ruth Dean PO Box 223 City Water N/A
Jackson, NC 27845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-45-2724 Barbara & Travis Pickerell PO Box 66 City Water N/A
Jackson, NC '7845
4966-45-0673 Larry & Sally Bullock PO Box 172 City Water N/A
Jackson, NC 27845
4966-45-0574 Helen Stephenson POBox liS City Water N/A
Jackson, NC 27845
4966-45-0476 William Fleenvood PO Box 385 City Water N/A
Jackson, NC 27845
4966-45-0399 Elizabeth King POBoxll2 City Water N/A
Jackson. NC 27845
4966-45-131 0 Harold & Marry Miller 567 Miller Trail City Water N/A
Jackson. NC 27845
4966-45-1232 Harry & Paula Marriner PO Box 373 City Water N/A
Jackson, NC 27845
4966-45-1156 Sharon Johnson PO Box 786 City Water N/A
Jackson, NC 27845
4966-45-1066 Alvin & Connie Wells 300 W Calhoun Street City Water N/A
Jackson, NC 27845
4966-35-7007 Ronald & Jerilyn Boone PO Box 607 City Water N/A
Jackson, NC 27845
4966-35-7077 Ronald & Jerilyn Boone PO Box 607 City Water N/A
Jackson. NC 27845
4966-35-8047 Jack & Shirley Britt PO Box 174 City Water N/A
Jackson, NC 27845
4966-35-9047 Joseph & Debra Beasley PO Box 826 City Water N/A
Jackson, NC 27845
4966-45-7646 Trustees of Jackson Baptist Church General Delivel)' City Water N/A
Jackson, NC 27845
4966-45-6427 Trustees of Jackson Baptist Church General Dclivel)' City Water N/A
Jackson. NC 27845
-------------------
Distance
GIS Pin Water from Site
Number Property Owner Name Mailing Address Source to
Domestic
Well
4966-45-7331 Tn1stees of Jackson Baptist Church General Delivery City Water N/A
Jackson. NC 27845
4966-45-8395 Jackson Methodist Church PO Box 121 City Water N/A
Jackson. NC '7845
4966-45-7107 Heather Liesey P0Boxl71 City Water N/A
Jackson, NC 27845
4966-45-7102 Douglas & Krista Miller 414 North Church Street City Water N/A
Jackson. NC 27845
4966-45-6094 William Beale III PO Box 245 City Water N/A
Jackson, NC 27845
4966-45-7087 William Beale III PO Box 245 City Water NIA
Jackson, NC 27845
4966-45-8068 William & Sallie Futrell PO Box 768 City Water N/A
Jackson, NC 27845
4966-45-9099 William & Judy Gossip PO Box 712 City Water N/A
Jackson, NC 27845
4966-45-3506 Jackson Baptist Church PO Box 445 City Water NIA
Jackson, NC 27845
4966-45-3453 Debra Johnson Gay PO Box 2 City Water N!A
Jackson, NC 27845
4966-45-3397 Mary Eli7llbeth Bacher 412 Cheadle Loop Road City Water N/A
Seaford, VA 23696
4966-45-3228 R.G. & Ella Bowers PO Box 404 City Water N!A
Jackson. NC 27845
4966-45-321 J Barbara Bowers 6929 Folger Drive City Water N/A
Charloue, NC 27270
4966-45-3126 Eleanor Pruden PO Box 583 City Water N/A
Jackson. NC 27845
4966-45-2075 Protestant Episcopal Church Trustees POBox6\3 City Water NIA
Jackson. NC 27845
-------------------
GIS Pin
Number Property Owner Name Mailing Address
.
4966-45-4055 Jackson Episcopal Church P0Box613
Jackson, NC 2.7845
4966-45-5115 Jerry & Sharon Docrrson PO Box 776
Clarksdale. AZ 863'4
4966-45-5206 Joseph O'Brian Cole Jr. PO Box 262
Jackson. NC 27845
4966-46-9146 Carroll Bracy Robertson Jr. 1215 Crescent Drive
Elizabeth Citv. NC 27909
4966-20-3941 Camilla B. Turner PO Box 191
Jackson, NC 27845
Note: * Denotes well in use for non-drinking purposes.
**Denotes well casing intact but no pump or electricity.
++Denotes UST fill ports on-site (unsure of USTs)
Distance
Water from Site
Source to
Domestic
Well
City Water N/A
City Water N/A
City Water NIA
City Water N/A
City Water N/A
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Soil Total Depth
Location (ft)
GP-1 8-10'
GP-2 8-10'
GP-3 8-10'
GP-4 8-10'
GP-5 8-10'
GP-6 8-10'
GP-7 8-10'
GP-8 8-10'
Soil
Sample Dateffime Intenal
(ft)
09/07104 8' 945am
09/07/04 8' 1015am
8' 09107/04
1030am
8' 09/07/04
IIOOam
8' 09/07/04
1130am
8' 09/07/04
1200pm
8' 09/07/04
1230pm
8' 09/07/04
IOOpm
TABLE 4
Field Notes
Red Apple Market #5
NC Highway 158
Jackson. Northampton County. NC
OVA Reading Lithology
0-1' concrete
60ppm 1-5' tan/brown fine silty sand
5-10' oran2e brown silty clay
0-1' concrete
180 ppm 1-5' tan/brown fine silty sand
5-10' orange brown silty clay with riverine pebbles
0-1' concrete
20 ppm 1-4' brown fine silty sand
4-6' grey medium silty sand
6-10' orane:e brown silcy sand
0-1' concrete
480 ppm 1-4' brown fine silty sand
4-6' grey medium silty sand
6-10' oran~e brown silty sand with riverine pebbles
0-1' concrete
1-3' brown fine silty sand
2080 ppm 3-5' grey medium silty sand
5-8' orange brown silty sand with riverine pebbles
8-10' Red orange coarse silty sand with riverine
~ebbles
0-1' concrete
270 ppm 1-4' backfill, yellow medium coarse sand
4-6' dark green silty clay
6-10' Orane:e red silty sand with riverine pebbles
0-1' concrete
18500 ppm 1-4' backfill, yellow medium coarse sand
4-6' dark green silty clay
6-10' Orange red silty sand with riverine pebbles
0-1' concrete
45ppm 1-4' brown fine silty sand
4-6' grey medium silty sand
6-10' orange brown silty sand
Notes
Slight petroleum
odor
Slight petroleum
odor
No noticeable
petroleum odor
Fairly strong
petroleum odor
Fairly strong
petroleum odor
Slight petroleum
odor
Fairly strong
petroleum odor
Slight petroleum
odor
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Soil
Location
GP-9
GP-10
GP-11
GP-12
Soil
Total Depth Sample
(ft) Interval
(ft)
8-10' 8'
8-10' 8'
8-10' 8'
8-10' 8'
Date!fime OVA Reading Lithology Notes
0-1' concrete
09/07/04 5 ppm 1-4' brown fine silty sand No noticeable
130pm 4-6' grey medium silty sand petroleum odor
6-10' orange brown silty sand
0-1' concrete
09/07/04 16ppm 1-4' brown fine silty sand No noticeable
145pm 4-6' grey medium silty sand petroleum odor
6-10' orane:e brown silty sand
0-1' concrete
09/07/04 15 ppm 1-4' brown fine silty sand No noticeable
300pm 4-6' grey medium silty sand petroleum odor
6-10' orane:e brown sil-tv sand
09/07/04 0-4' brown fine silty sand No noticeable
345pm 4ppm 4-6' grey medium silty sand petroleum odor 6-1 0' oranee brown silty sand
-------------------
COASTAL ENVIRONMENTAL
PROJECT LOCATION MAP SERVICES, INC. ,,
Figure: 1
Site: RAM #5
Date: 9-23-92
Scale: 1 "~2,000'
Drawn B : U.S.G.S.
-
I PROPERTY OF TOWN OF JACKSON
I
JACKSON
LAW ENFORCEl\·IENT w FIRE -BUILDING AND JAIL DEPARTMENT oc I a ---
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TELEPHONE & I MARKET# 5 1~.000 GASOI.tNE I
GP-10 I TELEGRAPH COMPANY I ~ 1~.000 GA~O~NE I 01
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II
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RAM#5 PHONE: [phone] W W.\TERSTORAGE1AKK
2_0 I NO:
JACKSON, NC I FAX: [phone]
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FIGURE 3 I s GROt;:<OWA"ITR '!O:<TTORL..;G II 'EU. LOCATIOS DATE: 07/26/2004 NO. DATE CES ENGINEERING, PC ~ Hl'!; Ill DEEP W"EL!. Gl'-1 GWPROBF.I.OCATJOS CHECKED BY: Benzene Soil Concentration Map I 857 W. MAIN STREET 0 SOII.!;.~MPLfLOCAIIO~
SCALE: AS SHOWN 09/09/2004 I MURFREESBORO, NC 27855 --PROPIORn" Ll'>"E
~ FX(" A\' A Tl0" BOI:SO~RY
RAM#5 I PHONE: [phone] W WATI:R STORAGF.TA~I' DRAWING NO:
JACKSON, NC FAX: [phone] k 10 20
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(EQ BY: Ethylbenzene Soil Concentration Map
I 857 W. MAIN STREET 0 ~OIL SA\!PLE LOCATIO>; /~<CAlF: AS SHOWN 09/09/2004 MURFREESBORO, NC 27855 ---l'ROPHTY LISt
~ E.\CA\'AliC>" B<a;:-;[l,~RY
RAM#5 PHONE: [phone] W WATFR~TORAGF.T.\;>;t,; IDR I G-Ni'}
I FAX: [phone]
9. ~ '!" JACKSON, NC
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~A --~,:.:;,~...=.. ..
NCDENR
North Carolina Department of Environment and Natural Resources
Michael F. Easley, Governor
Mr. Frank Williams
Eastern Fuels, Inc.
DIVISION OF WASTE MANAGEMENT
UNDERGROUND STORAGE TANK S~:CTION
August 4, 2004
326 Highway 42 West
Ahoskie, North Carolina 27910
Rc: Notice of Regulatory Requirements
15A NCAC 2L .0115(d)
William G. Ross Jr., Secretary
Risk·based Assessment and Corrective Action for Petroleum Underground Storage Tanks
Red Apple Market #5
Highway 158 E, Jackson
Northampton County, North Carolina
Incident# 9329
Intermediate Risk Classification
~--------D--ea_r_M __ r._w __ ii_h_·a_m~s-:--~-----------------~-~----~~------------~------------------­
Infonnation received by this office on August 2, 2004 confirms a release or discharge fro".!...._~----------· ..
I. ·······-····--·-petroleum undergrou-nd storage tank (UST) system at the above-referenced location. Records
indicate that you are the owner and/or operator of this UST system. This letter. is a standard
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notice explaining the actions you must take as a result of the release or discharge in accordance
with North Carolina statutes and mles. The UST Section of the Division of Waste Management
administers the State's rules for USTs and the required response for petroleum releases. Those
rules arc located in Title 15A, Subchapter 2L and Title 15A, Subchapter 2N of the North
Carolina Administrative Code (NCAC).
The risk-based rule for petroleum USTs, 15A NCAC 2L .0115(d), states that the Department
shall classify the risk of each known discharge or release from the UST system. A review of
information you have provided to this office indicates that:
(I) In the Coastal Plain physiographic region as designated on a map entitled "Geology of
North Carolina" published by the Department in 1985, the source of a confirmed
discharge or release is located in an area in which there is recharge to an unconfined or
semi-confined deeper aquifer that the Department detennines is being used or may by
used as a source of drinking water;
1628 Mail Service Center, Raleigh, North Carolina 27699-1628
Phone: [phone] \Fax: [phone] \Internet: www.enr.state.nc.us/ENR
An Equt~l Opportunity/Affirmative Action EmployN-50% Recycled\10% Post Consumer Paper
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(2)
(3)
The levels of groundwater contamination for any contaminant except ethylene dibromidc,
benzene and aliphatic and aromatic carbon fraction classes exceeds 50 percent of the
solubility of the contaminant at 25 degrees Celsius or 1,000 times the groundwater
standard or interim standard established in 15A NCAC 2L .0202, whichever is lower; and
The levels of groundwater contamination for ethylene dibromide and benzene exceeds
I ,000 times the federal drinking water standard set out in 40 CFR 141.
Based on the conditions above, the discharge or release at the subject site has been classified as
11 intermediate risk.11 In addition, the land use at the site has been classified as residential.
Please note that 15A NCAC 2L .0 II5(e) requires you to notify the Department of any changes
that might affect the risk or land usc classifications that have been assigned.
Session Law 2003-352 requires the Department to consider the availability of funds in the
Commercial Fund and the order in which the discharge or release was reported in setting the
schedule for further assessment or cleanup.
As a result, at this time, you are directed to proceed only with assessment, removal, and
cleanup of contaminated soil and assessment, removal, and cleanup of free product with a
thickness of 1.4" or greater. At this time, you are not directed to proceed with any
assessment or cleanup of contaminated groundwater. However, you are not relieved of the
requirements for further groundwater assessment and cleanup whenever the Department
deems them to be necessary and directs you to proceed or when Section 10 of Session Law
2003-352 expires (1 October 2005).
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Note: You are not prohibited from conducting any groundwater assessment or cleanup activities if you
I choose to do so. However, any claims against the Commercial Fund for costs of activities that have not
----oeen specijicatly71irecied by the Department will be paid after all claims for costs of activities directed by
·---theDeparfmentfor·this-and·otherUST-ndnmts:-Becau:nroftlrr!"imbalance between the revenue commg
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into the Commercial Fund and the potential claims for assessment and cleanup, there will be a
considerable delay in reimbursement for activities not directed to proceed by the Department.
Based 90 the detennination that the risk posed by the discharge or release at the subject site is
intennediate, you must comply with assessment requirements pursuant to 15A NCAC 2L
.0115(g). To achieve compliance with this ~tie, please submit a Comprehensive Site Assessment
(CSA) Report in accordance with !SA NCAC 2L .01 OG(c). !SA NCAC 2L .0 I OG(g). ISA NCAC
2N .0706 and the most recent version of the UST Section guidelines for assessment and
corrective action. The guidelines are available on the Internet at http://ust.ehnr.state.nc.us or
may be purchased from the UST Section for a fcc of $8.50. To purchase a copy of the
guidelines, please send a check made payable to DENR to:
DENRIDWM/UST Section
1637 Mail Service Center
Raleigh, NC 27699-1637
As part of the Comprehensive Site Assessment, you shall also evaluate, based on site-specific
conditions, whether the discharge or release poses a significant risk to human health or the
environment. The CSA Report must he received by this office within 90 days of the date of
receipt of this notice. fn addition, you must submit a summary of the CSA Report to the local
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Health Director and the local Chief Administrative Officer in accordance with l5A NCAC 2L
.0114. The summary should be submitted to these persons no later than five working days after
submittal of the CSA Report to this office.
Your prompt attention to the items described herein is required. Failure to comply with the
State's rules in the manner and time specified, may result in the assessment of civil penalties and
/or the use of other enforcement mechanisms available to the State. Each day that a violation
continues may be considered a separate violation.
Please note that performing assessment and cleanup work that is not required under 15A NCAC
2L. 0115 is not reimbursable from the Commercial or Noncommercial Leaking Petroleum
Underground StOrage Tank Cleanup Funds.
If you have any questions regarding the actions that must be taken or the rules mentioned in this
letter, please contact Mickey Roberts of the Raleigh Regional Office at the letterhead address
and at [phone]. If you have any questions regarding trust fund eligibility or
reimbursement, please contact the UST Section Trust Fund Branch at [phone].
Sincerely,
-2-ktJ?ats:--
Mickey Roberts
Incident Manager
1------------------------------------
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.... ---·---·cc:· Lelgn-s-umner, CES'Engineenng, Pc;·s-sTw:·Ma-in-srreet~-MliiTreesb-oro; NC-27855-· ---·
Northampton County Health Department
RRO Incident File
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Limited Site Assessment-Receptor Information
A. SITE INI<'ORMATION
DATE OF REPORT: 07/26//04
Facility J.D.: 0-026626 UST Incident Numher (!(known): 9329
Site Name: Red Apple Markel #5
Sire Location: NC 1/wy Jj8 West
Nearest City/Town: .!ackl·on County: Northamplon County
UST Owner: Eastern Fuels. Inc.
Address: HWY 42 W, P.O. Box 772. Ahoskie. NC 27910 Phone: [phone]
UST Operator: Eastern Fuels, Inc.
Address: HWY 42 W, P.O. Box 772, Ahoskie, NC 27910 Phone: [phone]
Property Owner: Eastern Fuels, Inc.
Address: HWY 42 W, P.O. Box 772, Ahoskie. NC 27910 Phone: [phone]
Property Occupant: None-For Sale
Address: Phone:
Consultant/Contractor: CES Engineering, I'.C.
Address: 857 W. Main Street, Murfreesboro. NC 27855 Phone: [phone]
Release Information
Date Discovered: 1992
Latitude: 36• 23' 22" Longitude: 77" 25' 22"
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (e.g., Piping!UST): UST
Sizes and contents of UST system(s) from which the release occurred:
One (I) 1000 -Gallon UST -Gasoline
Three (3) 4,000-Gallon UST-Gasoline
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B. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part]-Groundwatcr/SurliiCc Water/Vapor Impacts
High Risk
I. !las the release cmtlaminaled any water supply well including wty wei/usn/for IIO!Hirinking
2.
3.
4.
5.
fJ1111H!.\'C.\'? YES~
Is a wafer supp(l' wellusedfiw drinking waler localed wirhin l.OfHJ feet of the so wee area of the
release? YES~
Is a waler supply well 110/Usedfor drinking water (e.g., irrigalion, washing cars, industrial
cooling water, }//ling swimming pools) localed within 250 feet of the source area of the release'!
YES~
Does groundwaler within 500 feet rif !he source area of the release have the pot en/ ialfiJrfuture
11.\'e (there is no olher source ofwaler supply oilier !han the groum/11•ater)'! YES~
Do mpor.\'frum the release pose a lhrea/ of explosion because of accumulal ion lif !he mpors in a
confined space or po.1·e any other serious Ihreat Io puhlic health puh!ic .wrfety or the
environment!
If yes. describe.
6. Are there any uiher faciurs Ilwi Jnmld cause I he release /o pose WI imminent danger to public
heal I h. public safely, or !he environment? YES~
lfyes, describe.
lntennediate Risk
7. Is a swfixe water hody focaied within 500 feet t?fthe source area t1Ihe re!ew;e?
YES~
If YES, does I he nuL<imum groundwa/er conlaminani concentral irm exceed the surface water
quality stamlard.\ and criteriafmmd in 15A NCAC 2B .0200 by afaclor lif 10? YES/NO
8. Is the source area t!f the release located within till approved or planned wellhead proleciion area m
defined in -12 USC 300h-7(e)? YES~
lfyes, describe.
9. /.\'the relea.1·e localed in the Coa.\·fal l'lain physiographic region as designated on a map entitled
"Geology (1 North Carolina" pub/i.,·hed by the Department in 1985? ~0
If YES. is the source area t1the release located in an area in which there is recharge to an
uncm1fined or semi-confined deeper aquifer that is being 11.1wl or may be used rJs a source (!f
drinking wafer? YES~
If YES, describe.
I 0. /Jo the levels (1 groundwa/er contamination ji1r any contaminant exceed !he gross contamination
levels (.1·ee Table 9) established by the Department? ~0
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Part II -Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
I. Does the property cm11ain one or more primm:r or secondm:v residences (permunenl or
temporw:1)'! YESX@
/Jescrihe.
The property contains the RAM #5 building. pump island and canopy. There are no residents
on the property.
2. Does the property contain a school, daycare cemer, ho.~pilal, play~rmmd, park, recreation area,
church. nursing home, or other place ofpuhlic assemh/y? YESA@
Descrihe.
The property contains the RAM #5 building. pump island and canopy. There are no places of
public assembly on the property.
3. Does the properly cm1tain a commercial (e.g., retail, warehouse, oifice!husilless space, etc.) or
industrial (e.g, mmuifcu:turing, utilities. industrial research and de1•elopment,
chemical/petroleum hulk storage. etc.) enterprise, an inactive commercial or industrial
enlerpri.\·e. or is the land undn•eloped? ~NO
Describe.
The property contains the RAM #5 building, pump island and canopy.
4. Do children visit/he property? YES@
Expfuin.
No, the site is currently inactive and children do not visit the property.
Is ucces,\·to the property reliah~v restricted consistent with its use (e.g, hyfences, .\·ecuritv
personnel or hothj'! \rEs4@
Etp!ain.
The building and pumps arc locked.
5. Does pavement, buildings, or other Jtructure,\· cap the con/aminated soil? IYE.\j!NO
Describe.
There is a building and pavement partially capping the soil.
lfyes, what meclumisms are in place or can he put into place to enwre !hat the conraminated soil
wifl remain capped in thefiweseeablefuture?
The physical property is not likely to change within the forsecn future.
6. What is the zoning status (!f/he property? Commercial
7. Is the 11.\·e (if/he property likely 10 change in the next 20 years?
10;p/ain.
The property is for sale.
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Property Surroundine Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):
I. What is the dislancefromlhe source area of the release to I he nearest primary or secondar.v
residence (permanent or tempormJ)? The nearest primal)' residence is approximately \50 feet from
the source area.
2. Whal is !he distance from the source area r!fthe release to the neare ... t school, daycare CC'/1/er,
lw.\pilal, playground park. recreation urea, church. nursing home or other place ofpuhlic assemhly?
Across the street from the RAM #5 site is the Northampton County Courthouse.
3. What is the =o11ing s/atus of properties in the swTmmdinK area? Commcrical
.J. Urie.fly characleri=l! !he use wul uclivilie.\· rlihe lund in the surrowuliiiK areu.
• Land surrounding the area is commercial and residential. There arc numerous commercial
businesses along this area of US HWY 158. The surrounding area is very active with people
and traffic due to the Northampton County Courthouse being located across the street from
the RAM #5 building. There are numerous law offices also.
• There are primary or secondary residences (permanent or temporary) surrounding the urea.
• Public water is available to the surrounding area. The Town of Jackson receives its water
from water supply wells. both located outside the 1500 foot radius. There is a water storage
tank located within the 1500 t!.mt radius-according to the Northampton Public Works, this
tower is for storage only, and there is no water wc11 associated with the tower.
• The site no longer operates as Red Apple Market #5 and is currently for sale.
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12065 Lebanon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Me Juliec, TN 3?l22
[phone]
1-S00-767-5859
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-1 10 FT
09/07/04 09:45
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibrornotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobcnzene
Bromodichloromethane
Bromoform
Brom::Jmethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Hesult.s listed are dry weight basis.
8DL -Below Detection Limit
81.9
BDL
BDL
BDL
BDL
94.0
94. 0
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.0039
0. 0014
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Rill,
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
'·' '·' '·' '·'
0.030
0.061
0.012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0. 0012
0.0012
0.0012
0.061
0.0061
0.0012
0.0012
0.0012
0.0024
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
Fax [phone]
Tax I .D. 62-0814289
Est 1970
September 17,2004
ESC Sample • L169027-01
Site ID
Project • 01-105
Units Method Date
• 2540G 09/16/04
IT"8/kg MADEPV 09/14/04
IT"8/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
' Rec. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
mg/kg 82608 09/14/04
119/kg 82608 09/14/04
119/kg 82608 09/14/04
mg/kg 8260!3 09/14/04
J11Cj/kg 82601l 09/14/04
mg/kg 82608 09/14/04
119/kg 62608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/H/04
mg/kg 82608 09/14/04
119/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrrg/kg 8260!3 09/14/04
mg/kg 82608 09/14/04
rrrg/kg 82608 09/14/04
rrrg/kg 82608
mg/kg 82608
09/14/04
09/14/04
rrg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrrg/kg 82608 09/14/04
rrrg/kg 62608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
119/kg 82608 09/14/04
rrg/kg 82608 09/14/04
Laboratory Certification Numbers:
AIHA-100789, A~ -40660, CA-1-2327, CT-PH-0197, FL-E87487, GA
KY -90010, KYUST-0016, NC-ENV37S,DW21704, NO-R-140, SC -84004, TN-
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA-00109, WV
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical t"esults relate only to the sample submitted
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12055 Lebanon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Mt. Juliet, TN 37122
(615) 758-SB~B
1-B00-767-5859
REPORT OF ANALYSIS
Mr. Mark Hafenmaicr
Coastal Environmental, :nc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-l 10 FT
09/07/04 09:45
Parameter Dry Result
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethylbenzene
Hexachlorobut~diene
Isopropylbenzene
p-Isopropyltoluene
2-8utanone (MEK)
Methylene Chloride
4-Methyl-2-pentcmone •:MI8K)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.0049
BDL
BDL
BDL
BDL
BDL
BDL
0.0081
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
RDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantit<J.tion Limit (EQL)
Det. Limit
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.012
0.0061
0.012
0.0012
0.0061
0.0012
0.0012
0 '0012
0.0012
0.0012
0.0061
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0037
Units
lll3/kg
rrg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
lll3/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
lll3/kg
lll3 /kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1"013/kg
mg/kg
1"013/kg
rrg/kg
mg/kg
l!lCj/kg
mg/kg
1"013/kg
llf:]/kg
1"013/kg
llf:]/kg
mg/kg
mg/kg
mg/kg
mg/kg
1"013/kg
fTI3/kg
Laboratory Certification Numbers:
Fax (615) 75B-5SS9
Tax I.D. 62-0Bl4289
Est. 1970
September 17,2004
ESC Sample # ' L169027-01
Site ID
Project # ' 01-105
Method D<J.te
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
8260EJ 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
8260R 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
AIHA-100789, li.L-40660, CA-I-2327, Cl-PH-0197, FL-E87487, GA
KY -90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC -84004, TN-
MN-047-999-395, NY-11742
-923, IN -C-TN-01
2006, VA,-00109, WV
Note:
This report shall not be reproduced, except in full, without the W!"itten approval from ESC.
The reported <mulytical result$ relate onLy to the s<J.mple submitted
Page 2 of 56
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• ENVIRONMENTAL
SCIENCE CORP.
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-1 10 FT
09/07/04 09:45
REPORT OF ANALYSIS
1206~ Lebilnon Rd.
Mt Juliet, TN 37122
(615) 758-~858
1-800 -76'1-5859
Fax (615) 758-~859
Tax I .D 62-0814289
Est. 1970
September 17,2004
ESC Sample # Ll69027-Ql
Site ID
Project # 01-105
Parameter Dry Result Det. Limit Units Method Date Dil.
Surrogate Recovery
Toluene-dB
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
99. no
120
Det. Limit -Estimated Quantitation Limit(EQL)
' Rec.
' Rec.
' Rec.
Laboratory Cr~rti fication Numbero:
B260B
82608
82608
09/14/04 1
09/14/04 1
09/14/04 1
ESC Representative
AII!A-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TII-01
KY -90010, KYUST-0016, NC -ENV375,DW21704, ND-R-140, SC -84004, Til-2006, VA-00109, WV-233
MN -047-999-395, NY -11"142
Note:
This report shall not br~ r-eproduced, except in full, without the writ;ten approval from ESC.
The reported ~nalytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 3 of 56
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• ENVIRONMENTAL
SciENCE CoRP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758·5658
l-SOo-?67-5859
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-2 10 FI'
09/07/04 10:15
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
CS-CB Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromocth~ne
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
8DL -Below Detection Limit
84.2
BDL
BDL
BDL
BDL
105,
106.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0. 014
0.0026
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDI,
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantitation Limit (EQL)
Det. Limit
7 .7
7 .7
7 .7
7 .7
0.030
0.059
0.012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.059
0. 0059
0.0012
0. 0012
0.0012
0. 0024
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
Fax [phone]
Tax 1.0. 62-0814269
Est. 1970
September 1'1, 2004
ESC Sample ' Ll69027-02
Site ID
Project ' 01-105
Units Method Date
' 2540G 09/16/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV
mg/kg MADEPV
09/14/04
09/14/04
' Rcc. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
mg/kg 82608
mg/kg 82608
09/14/01!
09/14/04
09/14/04
mg/kg 82608
mg/kg 82608
mg/kg 82608
09/14/04
09/14/04
09/14/04
mg/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
rrg/kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
rrg/kg 82608
09/14/04
09/14/04
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA
KY -90010, KYUST-0016, NC -ENV375,DW21704, ND -R-140, SC-84004, TN-
MN-047-999-395, NY-11742
Note:
-923, IN -C-TN-01
2006, VA -00109, WV
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 4 of 56
Di 1.
1
65
65
65
65
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
I
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•
D
0
0
D
12065 Lebnnon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Me. Juliet, TN 37122
[phone]
REPORT OF ANALYSIS
Mr. Mark Hnfenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-2 10 FT
09/07/04 10:15
Parameter Dry Result
1,1-Dichloroeth~ne
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloroprop~ne
l,1-Dich1oropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthillene
n-Propy1benzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethenc
Trichlorofluororncth~nc
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Results listed are dry ;.;eight basis.
BDL -Below Detection Limit
EDL
EDL
EDL
EDL
EDL
EDL
EDL
EDL
BDL
EDL
EDL
EDL
EDL
BDL
0. 011
0. 0054
BDL
EDL
EDL
EDL
BDL
0.023
EDL
EDL
EDL
BDL
EDL
BDL
BDL
BDL
BDL
8Dl,
BDL
EDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Ouantitation Limit(EQL)
Det. Limit
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
o. 0012
0.0012
0.0012
0.0012
0. 012
0. 0059
0.012
0.0012
0.0059
0. 0012
0.0012
0. 0012
0. 0012
0.0012
0.0059
0.0012
0.0012
0. 0012
0. 0012
0.0012
O.OOP
0.0012
0.0012
0.0012
0.0012
0.0036
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ID3/kg
rrg/kg
mg/k9
Laboratory Certification Numbers:
1-800-767-5859
F"x [phone]
Tax 1.0 62-0914289
Est. 1970
September 17,2004
ESC Sample #
Site ID
Project H :
Method
82608
82608
82608
82608
82608
8260IJ
82603
82603
82608
82608
82608
82603
82603
82608
82608
82608
82608
82608
82608
82603
82603
82608
82608
82608
82603
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
L169027-02
01-105
Date
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/l4/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
09/14/04
AIHA-100789, Jl.L-40660, CA-I-2327, CT-PH-0197, FL-EB7487, GA-923, IN -C-TN-01
KY -90010, KYUST 0016, NC -ENV37S,DW21704, ND-R-140, SC -84004, TN-2006, VA-00109, WV
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC
The reported analytical results relate only to the s~mple submitted
Page 5 of 56
Oil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
M~ Juliet, TN JH22
((,15) 758-5858
l-800-?6?-5859
Fax [phone]
I
I
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I
I
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I
I
I
I
I
I
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Mr. Mark Hafenmaier
Constal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-2 10 FT
09/07/04 10:15
REPORT OF ANALYSIS
Tax 1 .!l 62-0814289
Est. 1970
September 17,2004
ESC Sample ~ L169027-02
Site ID
Project II : 01-105
Parameter Dry Result Det. Limit Units Method D<Jte Oil.
Surrogate Recovery
Toluene-dB
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
81. "· 160
Det. Limit -Estimated Quantitation Limit(EQL)
' ' '
Ji
Rec.
Rec.
Rec.
82608
82608
82608
09/14/04 1
09/14/04 1
09/14/04 1
y Hunt, ESC ReprcsentatLve
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-EB7487, GA-923, IN-C-TN-01
KY -90010, KYUST-0016, ~C -ENV375,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
R•~ported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 6 of 56
I
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12065 Lebanon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Mt. Juliet, TN J"/122
(615) 758·5858
1-800-767-5859
REPORT OF ANALYSIS
Mr. Mark H~fenmaier
Coastal Environmental, lnc.
857 '.-<est Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
Gfl-3 10 FT
09/07/04 10:30
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-ClO Aroma~ics
Surrogate Recovery
2,5-Dibromotoluene(FID.I
2,5-DibroiTDtoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
8romomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
CarOOn tetrachloride
Chlorobenzene
Cblorodibromomethome
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
83.4
BDL
BOL
BDL
BDL
117.
115.
BDL
BDL
BOL
BDL
BDL
BDL
BDL
SOL
BDL
BDL
BDL
BDL
BOL
BOL
BDL
DOL
BDL
BDL
BDL
BDL
SOL
BDL
SOL
BDL
SOL
BDL
BDL
Det. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
3.5
3.5
3. 5
3. 5
0. 030
0.060
0. 012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0. 0012
0.060
0.0060
0.0012
0.0012
0.0012
0.0024
0 0012
0.0012
0. 0012
0.0012
0.0012
0.0012
Fax [phone]
Tax l.D 62-0814289
Est. 1970
September 17,2004
ESC Sample ' ' L169027-03
Site ID
Project • 01-105
Units Method Date
• 2540G 09/16/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
• Rec . MADEPV 09/H/04. • Rec. MADEPV 09/14/04
mg/kg 62608 09/14/04
rrg/kg 82608 09/14/04
rrg/kg 8260B 09/14/04.
rrg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrg/kg 8260B 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 62608 09/14/04
rrg/kg 82608 09/14/04
mg/kg 82608 09/ l'l/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrg/kg 8260B 09/14/04
mg/kg 82608 09/14/01
mg/kg 82608 09/14/04
mg/kg 62608 09/14/04
11¥3/kg 82608 09/H/04
mg/kg 82608 09/14/04
rrg/kg 82608 09/14/04
lf"9/kg 82608 09/14/04
!T"9/kg 82608 09/14/04.
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-Pll-0197, FL-E87487, GA
KY -90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN -
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA -00109, WJ
This report.: shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 7 of 56
Oil.
1
29
29
29
"
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
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B
I
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12065 Lebanon Rd. • ENVIRONMENTAL
SCIENCE CORP.
Mt Juliet, TN 37122
[phone]
1-800-767-5659
REPORT OF ANALYSIS
Mr. M<n·k Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
Sept.ember 09, 2004
RAM 5
GP-3-10 FT
09/07/04 10:30
Pnrameter Dry Result
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trano-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uo.Lotnethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDI,
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Oet. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
0.0012
0. 0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.012
0.0060
0.012
0. 0012
0.0060
0.0012
0.0012
0.0012
0. 0012
0.0012
0. 0060
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0036
Units
mg/kg
rrg/kg
rrg/kg
rrg/kg
mg/kg
rrrg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
rrrg /kg
mg/kg
rrg/kg
rrg/kg
ID9/kg
rrg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
ID9/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
m:J/kg
mg/kg
mg/kg
mg/kg
mg/kg
IT'8/kg
Laboratory Certification Numbers:
Fax (615) 75B-5859
Tax I.D. 62·0814289
Est. 1970
Sept:ember 17,2004
ESC Sample ' L169027-03
Site IO
Project II 01-105
Method Date
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
A2608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
AIHA-100789, AL-1\0660, CA-l-2327, CT-PH-0197, FL-1>87487, GA
KY-90010, KYUST -0016, NC -ENV37S,OW21704, NO-R-140, SC-84004, TN-
MN-047-999-395, NY -11742
-923, IN -C-TN-01
2006, VA -00109, WV
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical ~esults relate only to the sample submitted
Page 8 of 56
Oil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
I
I
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u
0
D
I
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I
I
I
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I
• ENVIRONMENTAL
SCIENCE CORP.
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Dnte
Parameter
GP-3 10 FT
09/07/04 10:30
Surrogate Recovery
Toluene-dB
Dibromofluoromcthane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Reoult Det. Limit
100
100
100
Det. Limit -Estimated Quantitation Limit(EQL)
12065 Lebanon Rd.
Mt Juliet, TN 37122
(615) 7~8-5858
1-800-767-5859
Fax (615) 7SB-58S9
Tax I.D. 62-0614289
Est. 1970
September 17,2004
ESC Sample II : L169027-03
Site ID
Project II 01-105
Units Method Date Dil.
' Rec.
' Rec.
' Rec.
Ji :my Hunt,
82608
826GB
82608
09/14/04 1
09/14/04 1
09/14/04 1
E~C Repreoentative
Laboratory Certification Numb rs:
AIHA -100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY -90010, KYUST 0016, NC-ENV375,DW21704, ND-R-140, SC -84004, TN -2006, VA-00109, IN-233
MN-047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approv<J.l from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 9 of 56
I. I ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd
Mt:. Juliet. TN 3712/.
[phone]
1-B00-767-5859
Fa:< (615) "158-5859
I
I
D
I
I
I
I
I
I
I
I
I
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REPORT OF ANALYSIS
Mr. Mark llafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-4 10 FT
09/07/04 11:00
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
C5-C8 AliphaLics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,5-DibromotolueneiFID)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-8utylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1, 2 -Dibromo-3 -Chloroprop1me
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Oichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
80.5
12.
8.6
11.
'-'
125.
129.
BDL
BDL
BDL
EDL
EDL
EDL
EDL
EDL
EDL
0.15
BDL
BDL
EDL
EDL
BDL
EDL
BDL
EDL
BDL
EDL
EDL
Bm,
EDL
EDL
EDL
EDL
EDL
Det. Limit -Estimated Qua~titation Limit(EQL)
Det. Limit
'. 6 4. 6
4.6
4. 6
3. 0
6.0
1. 2
0 .12
0.12
0 .12
0.12
0 .12
0.12
0. 12
0.12
0.12
0.12
0.12
0.12
6.0
0.60
0.12
0.12
0.12
0.24
0.12
0.12
0.12
0.12
0.12
0 .12
Tax I .D. 62-0814289
Est. 19"10
September 17,2004
ESC Sample II L169027-04
Site ID
Project II 01-105
Units Method Date
% 2540G 09/16/04
rrg/kg MADEPV 09/14/04
rrg/kg MADEPV 09/14/04
mg/kg MADI::PV
mg/kg MADEPV
09/14/04
09/14/04
% Rec. MADBPV 09/14/04
% Rec. MADEPV 09/14/04
1!9/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrg/kg 82608 09/14/04
1!9/kg 82608
1!9 /kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
1!9/kg 82608
1!9/kg 82608
rng/kg 82608
mg/kg 82608
09/14/04
09/14/04
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608
mg/kg 8?.608
09/14/04
09/14/04
rrg/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608 09/14/04
rrg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrr,:~/kg 82608
mg/kg 82608
09/14/04
09/14/04
mg/kg 82608
rrg/kg 82608
09/14/04
09/14/04
lll3/kg 82608 09/14/04
mg/kg 82608 09/14/04
!1J3/kg 82608 09/14/04
!1J3/kg 82608 09/14/04
Laboratory Certification Numbers:
AIHA-100789, AL-40660. CA-1-2327, cr-PH-0197, FL-E87487, GA
KY-90010, KYUST-0016, NC-ENV37S,DW21704, ND-R-140, SC -84004, TN-
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA -00109. WV
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 10 of 56
Oil.
1
37
37
37
37
1
1
97
97
97
97
97
97
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97
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97
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97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
-233
I. I ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
l-800-757-5859
Fax (615) "158-5859
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Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreenboro, NC 27855
Date Received September 09, 2004
Description RAM 5
Sample ID GP-4 "
Collected By
Collection Date 09/07/04
Parameter
1,1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
tr~ns-1,2-Dichloroethene
1,2-Dichloropropane
l, 1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4 -Methyl-2-pentanone (MTBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromcth~ne
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
FT
11:00
Results listed are dry wei'3ht b<tsis.
BDL -Below Detection Limis
Dry
REPORT OF ANALYSIS
Result
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0. 3 8
BDL
0.36
0.20
BDL
BDL
BDL
BDL
BDL
0.72
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1 '' 0.91
BDL
BDL
Det. Limit
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0 .12
0.12
0.12
0.12
0.12
0. 12
0.12
0.12
0.12
"' 0.60
l .2
0.12
0.60
0.12
0.12
0.12
0.12
0.12
0.60
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.36
Det. Limit -Estimated Quantitation Limit(EQL)
Units
rrg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
m::J/kg
mg/k_g
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
11"13/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
JTg/kg
JTg/kg
JTg/kg
mg/kg
Laboratory Certification Numbers:
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample • L169027-04
Site ID
Project • 01-105
Method Date
826GB 09/14./04
826GB 09/14/04
82608 09/ltl/04
82608 09/14/04
826GB 09/14/04
82608 09/14/04
82608 O'.l/14/04
82608 09/14/04
82608 09/14/04
B260B 09/14/04
826GB 09/14/04
82608 09/14/04
82608 09/14/04
826GB 09/14/04
826GB 09/14/04
82608 09/14/04
82608 09/14/04
826GB 09/14/04
82608 09/14/04
8260B 09/14/04
826GB 09/14/04
826GB 09/14/04
62608 09/14/04
826GB 09/14/04
826GB 09/14/04
82608 09/14/04
826GB 09/14/04
826GB 09/14/04
826GB 09/14/04
826GB 09/14/04
826GB 09/14/04
826GB 09/14/04
8260B 09/14/04
6260B 09/14/04
826GB 09/14/04
826GB 09/14/04
626GB 09/14/04
826GB 09/14/04
AIIiA-1G0789, AL 40660, CA-I-2327, CT-PH-019'1, FL-EB7487, GA
KY-90010, KYUST-0016, NC -ENV375,D'Ii21704, ND -R-140, SC-84004, TN-
MN -047-999-395, NY -11742
-923, IN -C-TN-01
2006, VA-00109, WV
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical re~lults relate only to the sample submitted
Page 11 of 56
Oil.
" 97
97
" " " 97
" " 97
97
97
" 97
97
" " 97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
97
-233
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I
ENVIRONMENTJ\L
SCIENCE CORP.
Mr. Mark Hafenmaier
Coastal Environmental, rnc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-4 10 F'I'
09/07/04. 11:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt Juliet, 1'N 37122
[phone]
l-Bo0-767-5859
Fax [phone]
Ta>< I.D. 62-0814289
Est. 1970
September l7,2004
ESC Sample II : Ll69027-04
Site Io
Project II 01-105
Parameter Dry Result Det. Limit Units Method Date Oil.
Surrogate Recovery
Toluene-dB
Dibromofluoromethane
4.-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
100
80
130
Det. Limit -Estimated Quantitation Limit(EQL)
• ' '
Rec.
Rec.
Rec.
..
Hunt,
82608
82608
82608
09/14/04 97
09/14/04 97
09/14./04 97
ESC Re resentat~ve
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, Cf-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, W-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 12 of 56
I I. ENVIRONMENTAL
SciENCE CoRP.
12065 I,ebanon Rct.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
I
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I
I
a
0
I
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I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-5 10 F"T
09/07/04 11:30
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
C5-C8 Aliphatics
C9-C12 Aliphatice
C9-Cl0 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FIDI
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
8romobenzene
8romodichloromethane
Bromoform
Bromomethanc
n-8utylbenzene
sec-8utylbenzene
tert-8utylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-DibromoeLhanc
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
83.0
SOL
SOL
BOL
SOL
10'1.
104.
1.5
8DL
8DL
8DL
BDL
SOL
SOL
BDL
8DL
8DL
BDL
BOL
BDL
8DL
SOL
8DL
BDL
BOL
BDL
SOL
SOL
BDL
SOL
BOL
BDL
BDL
BDL
Det. Limit -Estimated Cuantitation Limit(EQL)
Det. Limit
7.6
7.6
7.6
"'
L5
3.0
0.60
0.060
0.060
0.060
0.060
0.060
0.060
0.060
0.060
0.060
0.060
0.060
0.060
3. 0
0. 30
0.060
0.060
0.060
0.12
O.O*'i"l
0.060
0.060
0.060
0.060
0.060
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample # ' L169027-05
Site ID
Project # 01-105
Units Method Date
' 2S40G 09/16/04
rog/kg MADEPV 09/14/04
rog/kg MADEPV 09/14/04
rog/kg MADEPV 09/14/04
rog/kg MADEPV 09/1<1/04
' Rec. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
rog/kg 82608 09/15/04
mg/kg 8260B 09/15/04
mg/kg 82608 09/15/0<1
rrg/kg 82608 09/15/04
mg/kg 82608 09/15/04
rrg/kg 82608 09/15/04
!1"9/kg 82608 09/15/04
mg/kg 826013 09/15/04
!1"9/kg 82608 09/15/04
mg/kg 62608 09/15/04
rrg/kg 62608 09/15/04
!1"9/kg 82608 09/15/04
mg/kg 82608 09/15/04
m:::~/kg 82608 09/15/04
!1"9/kg 82608 09/15/04
rrg/kg 62608 09/15/04
mg/kg 82608 09/15/04
rrg/kg 82608 09/15/04
mg/kg 82608 09/lS/04
!1"9/kg 82608 09/15/04
mg/kg 82608 09/15/04
mg/kg H260B 09/15/04
mg/kg 82608 09/15/04
mg/kg 82608 09/15/04
ng/kg 82608 09/15/04
mg/kg 82608 09/15/04
mg/kg 826013 09/15/04
Laboratory Certification Numbers:
AlHA-100789, AL -40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, LN-C-TN-01
Dil.
1
65
65
65
65
1
1
50
50
50
50 so
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
ICY -90010, KYUST 0016, NC -ENV37S,DW21704, ND-R-140, SC -84004, TN-2006, VA-00109, WV-233
MN-047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 13 of 56
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• ENVIRONMENTl\L
SCIENCE CORP.
Mr. Mark Hafenmaier
Coastal Environmentnl, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
GP-5 10 FT Sample ID
Collected By
Collection Date 09/07/04 11:30
Parameter
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
tra:-ts -1, 2 -Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropylbenzcne
p-Isopropyltoluene
2-8utanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MI8K)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzenc
Styrene
1,1,1,2-Tetrachloroeth~ne
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lora( luot·omethane
1,2,3-Trich1oropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, l'otal
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Result Det. Limit
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0. 060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
0. 084 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.60
BDL 0.30
BDL 0.60
BDL 0.060
0.30 0. 30
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.060
BDL 0.30
BDL 0.060
BDL 0.060
BDL 0 .060
BDL 0. 060
BDL 0.060
BDL 0.060
BDL 0.060
0. 26 0.060
0.10 0.060
BDL 0.060
0.37 0.18
Det. Limit -Estimated ~antitation Limit(EQL)
Units
mg/kg
!D3/kg
mg/kg
11"9/kg
mg/kg
rrg/kg
1!¥3/kg
mg/kg
mg/kg
rng/kg
11"8/kg
mg/kg
11"8/kg
rng/kg
mg/kg
mg/kg
rng/kg
rrg/kg
mg/kg
mg/kg
rng/kg
mg/kg
11"8/kg
mg/kg
mg/kg
rng/kg
mg/kg
rng/kg
mg/kg
rng/kg
11"8/kg
rng/kg
mg/kg
mg/kg
rng/kg
mg/kg
rng/kg
mg/kg
Laboratory Certification Numbers:
12065 Lebanon Rd.
Mt. J\lli!!t, TN 37122
[phone]
1-800-767-5859
Fax (615) ?58-5859
Tax I.D. 62-0814.289
Est. 1970
September 17,2004
ESC Sample II L169027-05
Site lD
Project # 01-105
Method Date Dil.
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
8260B 09/15/04 50
826GB 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
82608 09/15/04 50
AIHA-100789, AL-40660, CA-I-2327, cr-PH-0197, FL-E87487, GA -923, IN-C-TN-01
KY-90010, KYUST 0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN -2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report Ghall not be reproduced, except in full, without the writtell upproval from ESC.
The reported analytical results relate only to the sample submitted
Page 14 of 56
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. JUllet, TN 37122
(615) 758-SBS8
1-800-767-5659
Fax [phone]
I
I
D
0
I
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I
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I
I
I
I
Mr. Mark Hafenmaier
Coastal Environmental, I~c.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Date
Parameter
surrognte Recovery
Toluene-dB
GP-5 10 FT
09/07/04 11:30
Dibromofluoromethane
4-Bromofluorobenzene
Dry
REPORT 01-' ANALYSIS
Result Det. Limit
100
110
100
Tax I .D 62-0814289
Est.. 1970
September 17,2004
ESC Sample II-Ll69027-05
Site ID
Project # 01-105
Units Method Date Dil.
' Rec.
% Rec.
' Rec.
82608
82608
82608
09/15/04 50
09/15/04 50
09/15/04 50
--------JCi~of-'H~u~n~,'.~'E{.~,Representatlve
Results listed are dry weight basis.
BDL -Below Detection Limit
Det. Limit -Estimated Quantitation Limit(EQL)
Laboratory Certification Number~:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-£87487, GA-923, IN-C-TII-01
KY-90010, KYUST-0016, tiC-ENV375,DW21"104, ND -R-140, SC-84004, TN-2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 15 of 56
I •• ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet. TN 37122
[phone]
l-800-767-5859
Fax [phone]
I
I
I
I
I
I
g
g
0
0
0
0
0
0
REPORT OF ANALYSIS
Mr. Mark Hafenrnaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM S
Sample ID
Collected By
Collection Date
Parameter
Total Solids
GP-6 10 FT
09/07/04 12:00
Volatile Petroleum Hydrocarbons
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dich1orodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
Det. Limit -F.stimated Quantitation
Dry Result
81.3
BDL
BDL
BDL
BDL
125.
122.
BDL
BDL
BDL
0.13
BDL
BDI,
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Limit (EQL)
Det. Limit
8. 0
8.0
8.0
8.0
1.S
3.1
0.62
0.062
0.062
0. 062
0.062
0. 062
0. 062
0.062
0.062
0.062
0.062
0.062
0.062
3.1
0.31
0.062
0. 062
0.062
0.12
0 (lfi?.
0.062
0.062
0.062
0.062
0.062
Tax I.D. 62-0814289
E!lt. 1970
September 17,2004
ESC Sample ' L169027-06
Site ID
Project ' 01-105
Units Method Date
' 2540G 09/16/04
mg/kg MADEPV
mg/kg MADEPV
09/14/04
09/14/04
mg/kg MADEPV
mg/kg MADEPV
09/14/04
09/14/04
' Rec. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
ll¥]/kg 82608 09/15/04
ll¥]/kg 82608 09/15/04
mg/kg 82608
mg/kg 82608
09/15/04
09/15/04
ll¥]/kg 82608 09/15/04
mg/kg 82608 09/15/04
mg/kg 826013
mg/kg 82608
09/15/04
09/15/04
ll¥]/kg 8260B 09/15/04
mg/kg 8260B
mg/kg 82608
09/15/04
09/15/04
mg/kg 82608
mg/kg 82608
09/15/04
09/15/04
ll¥]/kg 8260B 09/15/04
mg/kg 8260B
ll¥]/kg 82608
09/15/04
09/15/04
ll¥]/kg 82608 09/15/04
mg/kg 82608
mg/kg 8260R
mg/kg 82608
09/15/04
09/15/04
09/15/04
mg/kg 8260B 09/15/04
mg/kg 82608 09/15/04
mg/kg 82608
mg/kg 82608
09/15/04
09/15/04
mg/kg 82608 09/15/04
!T13/kg 82608 09/15/04
rrg/kg 82608 09/15/04
I,<>boratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
Dil.
1
6S
6S
6S
6S
1
1
so so so so so so so so so so so so so so so so so so
50
50 so so so so so so so
KY-90010, KYUST-0016, NC -ENV375,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV-233
M..\1 -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 16 of 56
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Julie~. TN 37122
[phone]
l-800-767-5659
Fax [phone]
I
I
g
0
I
I
I
I
I
I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-6 10 FT
09/07/04 12:00
Parameter Dry Result
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dich1oroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dich1oropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethy1benzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butnnone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trich1orobenzene
1,2,4-Trich1orobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
T 1·i c h1oro fluor orne t home
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.065
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.13
BDL
BDL
0. 27
Det. Limit -Estimated Quantit:ation Limit(EQL)
Det. Limit
0-062
0.062
0-062
0.062
0.062
0-062
0.062
0. 062
0.062
0-062
0.062
0.062
0-062
0.062
0.062
0.062
0.62
0.31
0.62
0. 062
0.31
0.062
0.062
0.062
0.062
0.062
0. 31
0.062
0.062
0. 062
0.062
0.062
0.062
0.062
0.062
0.062
0.062
0.18
Units
rrg/kg
rrg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rn;:J/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rn;:J/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rn;:J/kg
mg/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
11"03/kg
mg/kg
11"03/kg
mg/kg
m<J/kg
Laboratory Certification Numbers:
Tax !.D. 62-0814289
Es~. 1970
September 17,2004
ESC Sample I~ L169027-06
Site ID
Project II 01-105
Method
82608
82608
82608
82608
82608
826013
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
Dnte
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/01
09/15/04
09/15/04
09/15/04
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL -£87487, GA-923, IN -C-TN-01
Oil.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
KY -90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV-233
MN-047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relnte only to the sample submitted
Page 17 of 56
I
I
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D
I
I
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I
12065 L<lbanon Rd.
ENVIRONMENT!I.L
SCIENCE CORP.
Mt. Juliet, TN 37122
(51~) 758-5858
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Date
Parameter
Surrogate Recovery
Toluene-dB
GP-6 10 FT
09/07/04 12:00
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Result Det. Limit
100
100
110
Det. Limit -Estimated Quantitation Limit(EQL)
1-aoo-767-sa 59
Fax [phone]
Til.X !.D. 62-0814289
Est 1970
September 17,2004
ESC Sample If L169027-06
Site ID
Project # : 01-105
Units Method Date
' Rec. 82608 09/15/04
' Rec. 82608 09/15/04
' Rec. 82608 09/15/04
Ji
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL -E87487, GA-923, IN-C-TN-01
Oil.
50
50
50
KY-90010, KYUST-0016, NC-ENV375,DW21704, ND -R-140, SC -84004, TN-2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:32
Page 18 of 56
I I. ENVIRONMENTAL
SCIENCE CORP.
12055 Lebanon Rd.
Mt Juliet, TN J7l22
{615) 758-5658
l-800-767-5859
ra" {6151 758-5859
I
0
u
I
I
I
I
I
I
I
I
I
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-7 10 FT
09/07/04 12:30
REPORT OF ANALYSIS
Parameter Dry Result Det. Limit
Total Solids
Volatile Petroleum Hydrocarbons
C5-C8 Aliphatics
C9-Cl2 Aliphatics
C9-ClO Aromatics
81.1
110
79.
58.
25.
'·' 9.'
9.' '·'
Units
•
rrg/kg
mg/kg
mg/kg
mg/kg
TdX l D. G7.-0814289
Est. 1970
September 17,2004
ESC Sample ' • L169027-07
Site ID
Project • 01-105
Method Date
2540G 09/16/04
MADEPV 09/14/04
MADEPV 09/14/04
MADEPV 09/14/04
MADEPV 09/14/04
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
162.
162. • Rec. MADEPV 09/14/04
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-DibLomoethane
Dibrornomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
0.13
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
3. c
6. 2
1 2
0.12
0.12
0.12
0.12
0.12
0 .12
0.12
0.12
0.12
0.12
0.12
0.12
6. 2
0.62
0-12
0.12
0.12
0-25
0.12
0.12
0.12
0.12
0. 12
0 .12
• Rec.
mg/kg
tn3/kg
tn3/kg
tn3/kg mg/kg
rrg/kg
mg/kg
lfl3/kg
mg/kg
rrg/kg
mg/kg
tn3/kg mg/kg
rrg/kg
mg/kg
mg/k~j
lfl3/kg
tn3/kg
mg/kg
ID3/kg
mg/kg
mg./kg
mg/kg
mg/kg
mg/kg
ll'g/kg
ID3/kg
Det. Limit -Estimated Quantitation Limit (EQL)
Laboratory Certification Numbers:
MADEPV 09/14/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
826013 09/15/04
8260B 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
82608 09/15/04
8260!l 09/15/04
82608 09/15/04
82608 09/15/04
AIIIA -100789, AL -40660, CA -I-2327, CT-PH-0197, FL -E87487, GA -923, IN -C-TN-01
KY-90010, KYUST 0016, NC -ENV375,DW21704, NO-R-140, SC-8400tl, TN-2006, VA-00109, WV
M..'J-047-999-395, NY-11742
Note:
This report shall not be reproduced, except in full, without the written approv<:~1 from ESC.
The reported analytical results relate only to the sample submitted
Ll69027-07 (VPH) -Previous run also had high IS/SURR recovery. Matrix effect.
Page 19 of 56
Oil.
c
" " " "
1
1
100
cOO
100
>00
100
100
100
cOO
cOO
>00
>00
100
100
100
100
>00
100
100
100
100
cOO
>00
100
100
100
100
>00
-233
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 J,ebanon Rd.
Mt. Juliet, TN 37122
(615) 758-51158
1-B00-767-5859
FilX [phone]
I
a
u
D
D
I
I
I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received September 09, 2004
Description RAM s
Sample m GP-7 10
Collected By
Collection Date 09/07/04
Parameter
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1, 2-Dichloroethene
1,2-Dichloropropane
1,1-Dich1oropropene
1,3-Dichloropropane
cis-1, 3-Dichloropropen,~
trans-1, 3 -Dichloroprop,~w~
2,2-Dichloropropane
Di-isopropyl ether
Ethylbenzene
He»wchl orobu tad i ene
Isopropylbenzene
p-Isopropyltoluene
2-8utanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (IH8K)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
styrene
1,1,1,2-Tetrach1oroethane
l,1,2,2-Tetrach1oroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
1'r i ch 1 oro f 1 uorometb .. utt:
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Tot<:~l
IT
12:30
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry Result
EDL
EDL
EDL
EDL
EDL
EDL
EOL
EOL
EOL
BOL
EOL
BOL
0.51
EOL
0.13
BOL
BOL
BOL
EOL
EOL
BOL
0.24
BDL
EOL
BOL
EOL
0.82
EDL
EOL
BOL
BOL
BDL
BOL
BOL
1.6
0.62
BOL
'-<
Det. Limit -Estimated Quantitation Limit (EQL)
Det. Limit
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
1.2
0.62
1.2
0.12
0.62
0. 12
0.12
0.12
0.12
0.12
0.62
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0. 37
Units
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rng/kg
lll3/kg
rng/kg
mg/kg
rrg/kg
mg/kg
rng/kg
mg/kg
mg/kg
rrg/kg
mg/kg
rng/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
IDJ/kg
TIT:3/kg
rng/kg
mg/kg
mg/kg
mg/kg
Laboratory Certification Numbers:
Tax !.D. 62-0814289
EBt. 1970
September 17,2004
ESC Sample # L169027-07
Site ID
Project II 01-105
Method
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
8260B
8260B
8260B
82608
82608
8260B
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
826GB
82608
R2608
82608
82608
8260B
82608
82608
Date
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
09/15/04
AIHA-100789, AL-40660, CA-1-2327, CT-PH-0197, FL-E87487, GA-923, IN -C-TN-01
KY-90010, KYUST-0016, NC -ENV375,DW2l704, ND-R-140, SC -84004, TN-2006, VA-00109, WV
MN-047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical ~esults relate only to the sample submitted
Ll69027-07 (VPH) -Previous run also hild high IS/SUP.R recovery. Matrix effect.
Page 20 of 56
Oil.
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
-233
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
ML. Juliet, TN 3?122
[phone]
1~800-767-5859
Fax [phone]
I
I
D
0
0
I
I
I
I
I
I
I
I
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-7 10 FT
09/07/04 12:30
REPORT OF ANALYSIS
Tax I.D. 6/.-0814~09
Eat. 1970
September 17,2004
ESC Sample # Ll69027-07
Site IO
Project 11-01-105
Parameter Dry Result Det. Limit Units Method Date oil.
Surrogate Recovery
Toluene-dB 100 ' Dibrornofluoromethane 100 • 4-Bromofluorobenzene 100 •
Rec.
Rec.
Rec.
82608
82608
82608
09/15/04 100
09/15/04 100
09/15/04 100
RerHllts listed are dry weight: basis.
BDL -Below Detection Limit
J1mm• Hunt,
Det. Limit -Estimated Quantitation Limit(EQL)
Laboratory Certification Number
AIHA-100789, Al.-40660, CA-I-2327, CT-PH-0197, FL-EB7487, GA
KY -90010, KYUST 0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN-
MN-047-999-395, NY -11742
Note:
ltt
ESC Representative
-923, IN -C-TN-01
2006, VA -00109, WV
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:33
L169027-07 (VPI!) -PreviQus run also hild high IS/SURR recovery. Matrix effect.
Page 21 of 56
-233
I •• ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt.. Juliet, TN 3?l22
(615) "158-5858
1-800-767-5859
Fax (615) 75S-5B59
I
H
B
I
I
I
I
I
I
I
I
I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmai~r
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM :,
GP-8 10 FT
09/07/04 13:00
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-C12 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FIO)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Brom::lrnethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
8DL -Below Detection Limit
82.4
BDL
BDL
BDL
BDL
108.
106.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
6.7
6. 7
6.7
6.7
0.030
0.061
0.012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.061
0.0061
0.0012
0. 0012
0.0012
0. 0024
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample ' L169027-08
Site ID
Project ' 01-105
Units Method Date
• 2540G 09/16/04
rrg/kg MADEPV 09/14/04
m:;J/kg MADEPV 09/14/04
rng/kg MADEPV 09/14/04
rng/kg MADEPV 09/14/04
• Rec. MADEPV 09/14/04 • Rec. MADEPV 09/14/04
rrg/kg 8260B 09/14/04
rng/kg 82608 09/14/04
rng/kg 82608
rrg/kg 82608
09/14/04
09/14/04
rng/kg 8260B 09/14/04
rng/kg 82608 09/14/04
rrg/kg 82608 09/14/04
rngfkg 82608 09/14/04
mg/kg 82608 09/14/04
rng/kg 82608 09/14/04
mg/kg 82608 09/14/04
rngfkg 82608 09/14/04
mg/kg 826013 09/14/04
rng/kg 82608 09/14/04
rrg/kg 82608 09/14/04
rng/kg 82608 09/14/04
mg/kg 82608 09/14/04
rrg/kg 82608 09/14/04
mg/kg 82608 09/14/04
mg/kg 82608 09/14/04
rng/kg 82608
m<J/kg 82f'iOB
09/14/04
09/14/04
mg/kg 82608 09/14/04
mg/kg 826013 09/14/04
mg/kg 82608 09/14/04
rrg /kg 82608 09/14/04
mg/kg 8260B 09/14/04
Laboratory Certification Numbers:
AIHA-100789, AL -40660, CA-I-2327, CT-PH-0197, FL-E87487, GA
KY -90010, KYUST-0016, NC -ENV375,DW21704, NO-R-140, SC-84004, TN-
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA -00109, WV
This 1:eport shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample sub~tted
Page 22 of 56
Oil.
'
55
55
55
55
' '
' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' '
-233
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt Juliet, TN ~7122
(615) 'ISB-5858
1-B00-767-5859
fax (615) ?SB-5859
I
I
0
0
D
I
I
I
I
I
I
I
I
I
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-8 10 FT
09/0"'/01 13:00
Parameter Dry
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropyl benzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (KIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzenc
Styrene
1,1,1,2-Tctrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trich1oroeth~ne
Trichloroethene
TrichlorofluOIOilotothane
1,2,3-Trichloropropane
l,2,4-Trimethy1benzene
1,3,5-Trimethylbenzene
Vinyl chloride
xylenes, Total
Results listed are dry weight basis.
BDL -Below Detection Limit
0
REPORT OF ANAI.YSIS
Result Det. Limit
BDL 0. 0012
BDL O.G012
BOL G.0012
BDL 0.0012
BDL O.GG12
BDL 0.0012
BOL 0.0012
BDL o. 0012
BDL 0 .0012
BDL 0 .0012
BOL 0 . 0012
BDL 0 .0012
BOL 0.0012
BDL 0.0012
BOL G.0012
BDL 0.0012
BDL O.G12
BDL 0.0061
DOL 0.012
.0020 G.G012
BDL 0.0061
BDL 0.0012
BDL 0. OG12
BOL 0.0012
BOL 0.0012
BDL 0.0012
BDL O.GG61
BOL 0.0012
BDL 0.0012
BDL 0. G012
BOL 0.0012
BDL 0.0012
BDL 0. 0012
BDL 0 .0012
BDL 0 .OG12
BDL 0 .0012
BDL 0.0012
BDL 0.0036
Det. Limit -Estimated Quantitation Limit(EQL)
Units
ng/kg
ng/kg
mg/kg
ng/kg
ng/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ng/kg
mg/kg
rrg/kg
mg/kg
ng/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
ll¥]/kg
ll¥]/kg
mg/kg
mg/kg
mg/kg
mg/kg
ll¥]/kg
ID]/kg
mg/kg
mg/kg
mg/kg
mg/kg
ll¥]/kg
Laboratory Certification Numbers:
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample # L169027-08
Site ID
Project # ' 01-105
Method Date
8260B G9/14/04
826GB 09/14/04
8260B 09/14/04
8260B 09/14/G4
826GB 09/14/04
B260B 09/14/04
B260B G9/14/04
8260B 09/14/04
B260B 09/14/04
B260B 09/14/04
8260B 09/14/04
B260B 09/14/04
8260B 09/14/04
8260B G9/14/04
8260B 09/14/04
8260B 09/14/04
8260B 09/14/04
8260B 09/14/04
8260B 09/14/04
6260B 09/14/04
6260B G9/14/04
8260B 09/14/04
8260B 09/14/04
8260B 09/14/04
82608 09/14/04
6260B G9/14/04
9260B 09/14/04
8260B 09/14/04
8260B 09/14/04
6260B 09/14/04
8260B 09/14/04
8260B 09/14/04
A?.60B 09/14/04
8260B 09/14/04
8260B 09/14/G4
6260B 09/14/04
8260B 09/14/04
8260B 09/14/04
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL -E87487, GA-923, IN-C-TN-01
nil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
KY-90010, KYUST-0016, N"C -E~375,DW21704, NO-R-140, SC-84004, TN-2006, VA-OG109, WV-233
MN-047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 23 of 56
I
I • ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN J7l/.2
[phone]
1-800-767-5859
Fill< [phone]
I
I
I
0
B
B
B
I
0
D
0
H
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-8 10 FT
09/07/04 13:00
REPORT OF A.~ALYSIS
TilX I.D. 62-0811289
Eat. 1970
September 17,2004
ESC S<!rrple II Ll69027-08
Site ID
Project II 01-105
Parameter Dry ReGult Det. Limit Units Method Dilte Dil.
Surrogate Recovery
Toluene-dB
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
>00
100
100
Det. Limit -Estimated Quantitation Limit(EQL)
' Rec.
' Rec.
' Rec.
Ji y Hunt,
Laboratory Certification Numbers:
82608
82608
82608
09/14/04 1
09/14/04 1
09/14/04 1
AIHA-100769, AL-40660, CA-1-2327, CT-PH-0197, FL-EB7487, GA-923, IN-C-TN-01
KY -90010, KYUST -0016, NC -ENV375,DW21704, ND -R-140, SC -84004, TN-2006, VA-00109, WV-233
MN-047-999-395, NY -ll742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:33
Page 24 of 56
I I. ENVIRONMENTAL
SciENCE CORP.
12065 Lebanon Rd.
Mt. Juliet. TN 37122
((,15) 756-5856
1-800-767-5859
Fa>< [phone]
I
u
0
0
I
I
I
I
I
I
I
I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coils tal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM S
GP-9 10 FT
09/0'1/04 13:30
Parameter Dry Result
Total Solids
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-C12 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Brornobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chloroto1uene
4-Chlorotoluene
1,2-Dibromo-3-Ch1oropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dich1orobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDI. -!3elow Detection Limit
81.3
BDL
BDL
BDL
BDL
125.
122.
0.043
SOL
BDL
BilL
SOL
SOL
BDL
SOL
BDL
BDL
SOL
BDL
BDL
BDL
BDL
BDL
SOL
SOL
BDL
BDL
BDL
BDL
SOL
SOL
BDL
BDL
SOL
Det. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
8. 8
8.8
8.8
8. 8
0.031
0. 062
0.012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.062
0.0062
0.0012
0.0012
0.0012
0.0025
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
Tax I.D. 62-0814269
Est. 1970
September 17, 2004
ESC Sample ' L169027-09
Site ID
Project.: ' 01-105
Units Method Date
' 2540G 09/16/04
mg/kg MADEPV 09/14/04
m.:J/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
' Rec. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
mg/kg 82608 09/17/04
mg/kg 82 608
m:~/kg 82608
mg/kg 82608
119/kg 82608
rrg/kg 82608
mg/kg 82608
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
mg/kg 82608
mg/kg 82608
mg/kg 82608
09/17/04
09/17/04
09/17/04
rna/kg 82608
rng/kg 82608
mg/kg 82608
09/17/04
09/17/04
09/17/04
mg/kg 82608
mg/kg 82608
09/17/04
09/17/04
fll3/kg 82608 09/17/04
mg/kg 82608 09/17/04
rrg/kg 82608
mg/kg 82608
09/17/04
09/17/04
mg/kg 82608 09/17/04
mg/kg 82608
rrg/k'] R;1!';QB
09/17/04
09/17/04
rrg/kg 82608 09/17/04
rrg/kg 82608 09/17/04
mg/kg 82608 09/17/04
mg/kg 82608 09/17/04
n-g/kg 82608 09/17/04
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-EB7487, GA
KY-90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN-
MN-047-999-395, NY -11742
Note:
-923, IN -C-'I'N-01
2006, VA -00109, W
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported an<llytical results relate only to the sample Sllbmitt:ed
Page 25 of 56
Oil.
l
72
72
72
72
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
l
-233
I •• ENVIRONMENTAL
SciENCE CoRP.
12065 Lebanon Rd.
Mt. Ju1let, TN 37122
(615) 758-~8~8
1-600-767·5859
Fax [phone]
I
I
I
I
I
I
I
n
0
0
I
I
I
I
I
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Satrple ID
collected By
Collection Date
September 09, 2004
RAM 5
GP-9 10 FT
09/07/04 13:30
Parameter Dry Result
l, 1-Dichloroethane
1, 2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
tr<,ns-1, 2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethylbem:ene
Hexachlorobutadiene
Isopropyl benzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1, 1, 2-1'richloroethane
Trichloroethene
Trichlorofluoromechane
1,2, 3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Totill
Results listed are dry weight basis.
8DI. -Below Detection Limit
eDL
BDL
BDL
BDL
eDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0. 017
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
eDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit-Estimated Quantitation Limit(EQI,)
Det. Limit
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.012
0.0062
0. 012
0.0012
0. 0062
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0062
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0037
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg /kg
rrg/kg
ITW3/kg
mg/kg
rrg/kg
ITW3/kg
TT'g/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
TT'g/kg
mg/kg
rrg/kg
Laboratory Certification Numbers:
Ta>< !.D. 6~-0814289
Est. 1970
September 17, 2004
ESC Sample # Ll69027-09
Site ID
ProJ"ect ' ' 01-105
Method Date
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
8260B 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
8:<60R 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
AIHA-100789, AI..-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA
KY-90010, KYUST-0016, NC-ENV37S,DW21704, ND-R-140, SC-84004, TN-
MN-047-999-395, NY-11742
-923, IN -C-TN-01
2006, VA-00109, WV
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 26 of 56
Dil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-23)
I I. ENVIRONMENTAL
SciENCE CoRP.
12065 Lebanon Rd.
Ml. Juli(!C, TN 37122
[phone]
1-800-767-5859
I
g
0
0
0
I
I
I
I
I
I
I
I
I
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sept•~mber 09, 2004
RAM 5
Sample ID
Collected By
Collect:ion D<~.te
Parameter
Surrogute Recovery
Toluene-dB
GP-9 10 FT
09/07/04 13:30
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight baais.
BDL -Below Detection Lirnit
Dry
REPORT OF ANALYSIS
Result net. Limit
;DO
100
n.
Det. Limit -Estimated Quantitation Limit(EQL)
FilX (6g) 758-5859
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
ESC Sample II : Ll69027-09
Site ID
Project II 01-105
Units Method Date
• Rec. 82608 09/17/04 • Rec. 8260B 09/17/04
' Rec. 8260B 09/17/04
J y Hun , ESC Representative
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL -E87487, GA -923, IN-C-TN-01
Oil.
1
1
1
KY-90010, KYUST-0016, NC -ENV375,DW21704, NO-R-140, SC-84004, TN -2006, VA-00109, WV-233
MN-047-999-395, NY -11742
Note:
This report shnll not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:03 Printed: 09/17/04 16:33
Page 27 of 56
I I. ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliec, TN 37122
1615) 758-5858
l-B00-767-5859
Fux [phone]
g
D
0
R
I
I
I
I
I
I
I
I
I
I
Tax I.D. 62-0814289
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
DeGcription
Sample ID
Collected By
Collection Date
Parameter
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
September 09, 2004
RAM 5
TRIP BLANK
09/07/04 00:00
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethilne
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4.-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dich1orobenzene
1,4-Dich1orobenzene
Dichlorodif1uoromethane
1,1-Dichloroethnne
1,2-Dichloroethane
1,1-Dich1oroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dich1oropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
8DL -Below Detection Limit
REPORT OF ANALYSIS
Result
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.0010
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
net. Limit
0.025 o.oso
0.010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0 .0010 o. 0010
0.0010
0.0010
0.0010
0.0010
0.050
0.0050
0.0010
0.0010
0.0010
0. 0020
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0 .0010
0 .0010
0 .0010
0 .0010 o. 0010 o. 0010 o. 0010
0 .0010
0 .0010
0 .0010
Det. Limit -Estimated Quantitation Limit(EQL)
Units
mg/1
mg/1
mg/1
mg/1
mg/L
mg/1
mg/1
mg/1
,.,; 1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
mg/1
"'3/1
mg/1
mg/1
mg/1
mg/1
,.,; 1
mg/1
"'31 1
mg/1
"'31 1
,.,; 1
mg/1
mg/1
mg/1
mg/1
"91 1
mg/1
"911 "91 1
mg/1
mg/1
Laboratory Certification Numbers:
!J<ot . 19"1 0
September 17, 2004
ESC Sample • ' L169027-10
Site ID
Project • ' 01-105
Method Date
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/01
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
8260F 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
82608 09/14/04
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, Gil. -923, IN -C-TN-01
2006, VA -00109, WV KY -90010, KYUST-0016, NC-ENV375,DW21704, NO-R-140, SC-84004, TN -
MN -047-999-395, NY -11742
Page 2B of 56
Oil.
1
L
L
L
L
L
L
L
L
L
L
L
L
1
L
L
L
1
1
L
L
1
L
L
L
L
L
L
L
L
L
1
1
1
L
L
L
-233
I
I
I
I
I
I
I
g
0
I
I
I
I
I
I
I
I
• ENVIRONMENTAL
SciENCE CoRP.
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main St~eet
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
September 09, 2004
RAM 5
TRIP BLANK
09/07/04 00:00
2,2-Dichloropropane
Di-isopropyl ether
Et.hy1benzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethanc
1, 1, 2-Trichloro-1, 2, 2 -tri fluoro
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzenc
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,2,3-Trimethylbenzene
1,3,5-Trimet.hylbenzene
Vinyl chloride
Xylenes, Total
Surrogate Recovery
Toluene-dB
Dibromofluu~uno.::thane
4-Bromotluorobenzene
BDL -Below Detection Limit
REPORT OF ANALYSIS
Result
BDL
BDL
BOL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
99.
100
95.
net. Limit
0. 0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.010
0.0050
0.010
0 .0010
0 .0050
0 .0010
0 .0010
0 .0010
0 . 0010
0 .0010
0.0010
0.0050
0.0010
0 . 0010
0 .0010
0 .0010
0.0010
0.0010
0 . 0010
0 . 0010
0 .0010
0 .0010
0.0010
0.0030
Det. Limit -Estimated Quantitation Limit(EQL)
Units
mg/1
mg/l
mg/1
mg/1
mg/1
mg/1
mg/l
mg/1
mg/1
mg/1
mg/1
mg/1
"'J/1
mg/1
"'J/1
"'J/1
mg/l
mg/1
mg/1
"'J/1
mg/1
mg/1
mg/l
mg/1
mg/1
"'J/1
mg/1
"'31 1
mg/1
mg/1
' Rec.
' Rec.
' Rec.
Laboratory Certification Numbers:
12065 Lehanan Rd.
Mt Juliet, TN )?122
[phone]
l-800-767-5859
Fax [phone]
Tax I.D 62-0814289
Est. 1970
September 17, 2004
ESC Sample # Ll69027-10
Site ID
Project II 01-105
Method Date Dil.
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/H/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
62608 09/14/04 1
62608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
8260B 09/14/04 1
82608 09/14/04 1
82608 09/14/04 1
8260R 09/14/04 1
82608 09/14/04 1
( ~eeen'"'ive Ji y Hunt
AIHA-100769, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY-90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN -2006, VA-00109, '1-N-233
MN-047-999-395, NY-11742
Note:
The reported analytical reoultn relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approv<l1 from ESC.
Reported: 09/17/04 15:03 Print:ed: 09/17/04 16:33
Page 29 of 56
I
I Sample II
I Ll69027-0l
I Ll69027-02
I Ll69027-03
Ll69027-04
m
L169027-05
I L169027-06
L169027-07
a 1.169027-08
n Ll69027-09
u Ll69027-10
u
u
D
D
0
H
0
H
R
Attachment A
List of Analytes with QC Qualifiers
Analyte
Volatile Petroleum Hydrocarbons
CS-C8 Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
Volatile Petroleum Hydrocarbons
C5-C8 Aliphatics
C9-Cl2 AlLphntics
C9-C10 Aromatics
4-Bromofluorobenzene
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
4-Bromofluorobenzene
Volatile Petroleum Hydrocarbons
cs-cs Aliphatics
C9-C12 Aliphatics
C9-Cl0 Aromatics
Volatile Petroleum Hydrocarbons
cs-cs Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
Volatile Petroleum Hydrocarbons
CS-CB Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
Volatile Petroleum Hydrocarbons
cs-cs Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
1,2,4-Trimethylbenzene
Acrolein
2-ChloL·oethyl vinyl ethet·
Dichlorodifluoromethane
trans-1,3-Dichloropropene
2-Butanone (MEK)
Methyl tert-butyl ether
Vinyl chloride
Qualifier
0
0
0
0
0
0
0
0
Jl
0
0
0
0
Jl
0
0
0
0
0
0
0
0
Jl
Jl
0
0
0
0
0
0
0
0
J<
J<
JJ
J<
J<
JJ
J3
J4
Page 30 of 56
I
I
I
I
a
D
D
I
I
I
I
I
I
I
I
I
Qualifier
J3
J4
0
Meaning
Attachment B
Explanation of QC Qualifier Codes
Surrogate recovery lirnit:s have been exceeded; values are outside upper
control limits
The associated batch QC was outside t:he established quality control range
for precision.
The associated batch QC was outside the established quality control range
for accuracy.
(ESC) Sample diluted due to matrix interferences that impaired the ~bility
to make an accurate analytical determination. The detection limit ~s
elevated in order to reflect the neceGsary dilution.
Qualifier Report Information
ESC Utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifyin~J bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices inco:r:porated by most EPA methods, it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected).
Definitions
Accuracy -The relationship of the observed value of a known sample to the
Precision
Surrogate -
true value of a kno~~ sample. Represented by percent recovery and
n~levant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
The agreement bet"•een a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Organic compounds that are similar in chemical composition, extraction,
and chromatography to v.nalytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
Control Limits
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
31-119
12-134
51-141
Nitrobenzene-d5 43-118 Dibromfluoromethane
2-Fluorobiphenyl 45-128 Toluene-dB
Terphenyl-d14 43-137 4-Bromofluorobenzene
(AQ)
79-126
81-114
65-129
TIC Tentatively Identified Compound, Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogntes.
(SS)
83-ll9
82-116
72-126
Page 31 of' 56
I
12065 Lebrmon Rd.
I • ENVIRONMENTAL
SCIENCE CoRP.
Mt Juliet, TN 37122
1615) 758-5858
1-B00-767-~859
Fax [phone]
llcoastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
lna1 te
Inc.
Quality Assurance Report
Level II
Ll69027
__ L8bi:i:r_ab)'I'y ~lank __
Result -Uriits Date Anal zed
Tax 1.0. 62-0814289
Est. 1970
September 17, 2004
Batch
1'Jl·-; 1, 2 ~_Tetrachloroethane _,:\$,,))o __ f.Jtt .. ·-::::· "'h. o o 1 c3'4tt:.,: ,_,_,_;.,t rng I 1 ::::,c,':4:f'{o 9/13 I 0 4 : : 21' : _4 9 .&F-WG 17 o 6 o 1---~;> ".oo1 mg/1 ____ --09/13/04 21:49 ···wGl'io-601 1,1,1-Trichloroethane
,1,2,2-Tetrach1oroethane
'}1"';-2-T:i:"ichl0£0-1, 2 ;--2-;_ti:"if1iior0ethiiii.e
< .001 fl\g/1 09/13/04 21:49 WG170601
""-:-"';<::;-:'ool'%$ mgfl:.s:<--;~_-;:o9/-1,3/04f.21, 4 9 ~-· __ \'IG1706ol
< ... 001 ---mg/1 09/13/04 21:49 WG170601 1, ·1·, 2 -Tridlloroethane ------....
1,1-Dichloroethane 11··:-,i~gf~~i~~~~~~~~~:::_ .r<
UI,2,3-Trich1orobenzene
1', 2 i3.'~Tri:chlO:roprop<'lne --~-,~.:::-
•
,2,3-Trimethylbenzene ,2,4-Trich1orobenzene
';-~ ::·6I;;;~;~=~:~~~~~;~~o~:~-~!''::-_
1,2-Dibromoethane
•
, 2.-Di'Chloroberiien'i::'t
, 2 -o'iC:tiloroethaOe ....
,2-Dich1oropropane
, J·;·'s:~Trimethylbenzene
1,3-Dich1orobenzene
ft,;':~~gt~~i·:~:~6b~~i:-~:-:
IJ.,2-Dich1oropropane
2-Butanone (MEK)
2 ~-Ch 16:i:"oe thy 1;:\vi ny 1\:. ether"''''"''
< .001 mg/1 09/13/04 21:49 WG170601
~=' ---=-''<;y-;oOl)\~ =---~=-\{?ll\Mmg/lWf&J,: -=-o9/13/04]21-:-49,q.---==:==·wG17060l'( ·11<-
< .001 mg/1 09113104 21:49 WG170601
< .001 mgl1 09113104 21:49 WG170601
_,:-< ,._.:;: 001 :·· 0.,.;:. ·::(_.mg/lf_ti%;)'09/.13/04'':':21-:_,49£±{-_ WG1 70601-_,:od.
< .oo1 mgl1 o9/13/04 21:49 WG17o.Goi-
" .001 mgl1 09113/04 21:49 WG170601
<:''t': o 01 :H~.mg I 1 0 9 I -13/ Oil 21'.: 4 9\::t::;:)( WG1 70_6 01 ·-.::::::::::=···
< .002 mg/1 09113104 21:49 WG170601
< .001 mg/1 09/13/04 21:49 WG170601 · · 4td%-t:r<n·::oo1--··· _f/fngiVt£1( o9/13/04·,:::·21-_:-:4 __ 9))tJ:}wG1'7.o6ort~:'.~-,.
< .001 mg/1 09/13104 21:49 WG170601
< .001 mg/1 09/13104 21:49 WG170601
o ·::::::~~~mg / L~>:::::: _:· _ _o 9 /-1-3/ o 4 ':} 21'': 4 9 ):~:::: WG 1' 7. 0 6 o 1 \:::::::·:·::· ·
< .001 mgl1 09/13104 21:49 WG170601
< .001 mgl1 09113/04 21:49 WG170601 <"=''i_OOlj)J(:· --:::t0'i~l 09/13/04;n1 :'4 9~:::·: WG1 70601:·<·-·,· ---" " .001 ___ , __ ,__, __ ilig/1 09/13lo·4--21,-49. WG170601
< .01 mgl1 09113104 21:49 WG170601 1dt%: o 0 1 . ·· .%$ ::::,;:::,,Jfu mg /1 'ttThK'A 9/13/ 04 ·;p1 : _4 9 _.i.//;,'o WG 17 0 6 o 1 Wf,,_,_,_,
< .001 mg/1 .. 09/13/04 21:49 WG17.0{0l
< .001 mg/1 09113104 21:49 WG170601 I -Chloroto1uene -Chlorotolucne
:~/1_e_t!jyl'~2:::-pentallo_i-le ·, (MIBK) BM-.. Acetone -
'%?0(\ 5,. 01 :-~_n'tg/1/tf\{09/_-1,3/04\21: 49:·:_-:;, __ , WG170601f_
< .-025 mg/1 09/13/04 21:49 WG170601
Acrolein
lllC:i:"yi6ni tri-le .:
enzene romobenzene BiOiiiO'di'ch 10I-6methane -· •-~~:~~~~~~e.. .. ..
arbonltetrachlor ide_
hlorobenzene
Chlorodibromomethane
I Chl op')e t hii.ne ·;:(::::::-::~:t· ···· -:\>:· h1oroform
hloromethane ds:~:-1, 2.::oic':h1oroethene
cis-1,3-Dichloropropene
lg.t~~~~~~-~~~i~~!!:{~~~-~e
Ethy1benzene
H8xach16'r'Obutadi'ene·c .._-;;
< .05 mgll 09113/04 21:49 _ WG170601
< 0.01· ;,::::: .. ,_,,_,_,_ --t~mg/1'-:':<; 09/13/04%21--:'49)%:~-,,,,,,:-wG17060Ll'&t':·
< .001 mgl1 09/13104 21:49. WG170601
< .001 mg/1 09/13/04 21:49 WG170601
. _,_... ... -<<~iiK<t}-_-_-_,_·;w: g g}-·_-THffi 'm_Ifd~~; f?i!Wr· g ~ g ~ ; g!;; i':;:{ ~ ilitH'.,~g i ~-g -~ g i'tL·::::
< .001 mg/1 09113104 21:49 WG170601 4\N%\ ;:,,,,: 0 01 -----::::0\1:.-.-::(\mg/1-tf>ffiftO 9/.13 I 0.4 ~:~' 21 : 4 9 :".f. WG1'70_60 1.:_ .... ,..:::: .. -···
< .001 mgl1 09/13104 21:49 WG170601
< .001 .. fTl911 09113/04 21:49 . __ WG170601
·.:):~::::·:-:-::.< ::·:;:· 0 0 L --·-:;:::, mg /:1 9 /.1-3 / 0 1} 21: .' 4 _9 .':)'~::':':':'~':: WG 1.7. 0 6 0 1 ':''¥.:f': :·:·
< .005-. mg/1 9113104 21:49 WG170601
< .001 mgll 09/13/04 21:49 WG170601
.. ·::··:tt<g; 001'.': ttt#M/mg/ltit:rtt:~ 09/1'-3/04 2 L49.':t'fi\\WG1 7060L
< .001 mg/1 .09113/04 21:49 WG170601
< .001 mg/1 09113104 21:49 WG170601
<:,~::':·00 :';\ing/1 __ 09/l3/0.4':_:21":4 WG170601 ··'%·::·:···
< .001 mgll --09/13104-21:49 WG17o'601
< .001 mg/1 09/13/04 21:49 WG170601 ···::i_J)):'__ ·::\':" ·· < '':·ooL: _jffigll ,_,_,,-y..-, 0.9/1'3/ 04 __ , 2F_49_tffl&WG170601-~-·)_::>:··
< .001 mg/1 09113/04 21:49 WG170601
.{
< .001 mgl1 09/13104 21:49 WG170601
~,~k:,oos B#'PlrTB/:l::::::I--tf@o9/13/04 _21":0.A9,:~.&\ZI'<_G17060l···
< .001 mgll '09/13/04 -21:49 ---WG170601 l~i~~~1:~~-i~-~~~~r~e-~:g?4ij-;-, ___ ,_ :D_>'d:
n-Butylbenzene
n-Propy1benzene ~~~i~~~~~~~~~i'~:~-,--,,:{%',.-:_
sec-Buty1benzene
s_tyren:e.ec·---_.;;J:St-f.··
l tert-Butylbenzene
Tetrachloroethene
I
< .001 mg/1 09113/04 21:49 WG170601
.:ili$f(t ::::::<w. oos&tt:'-.-,~,'.:/mg/li-+ __ .';ili:09I13/04'::::2E.4 9 ·. -----;ilWG170601 .. -:,::<,
< .001 mgl1 09/13104 21:49 WG170601
< .001 mgll 09/13104 21:49 WG170601 A':--"' <_.}:'o o 110... _,_,'':S!f"-iilg I w--~:::.::::09/13/ 04't 21'X,4_9_f q;;:q,wGl 10 60lf-~" '"'\\ c.
< .001 mg/1 "o9I13/04--21:49 WGl70.60l.
< .001 mg/1 09113104 21:49 WG170601
Page 32 of 56
I 12065 L"bauon !<d.
I • ENVIRONMENTAL
SCIENCE CORP.
Mt Juliet, TN 37122
(615) 758·511511
1-800-767-51159
Fax (615) 758·5859
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
61Ueriei:W·:.·:· ..
nal te
Inc.
1-~:~·::i,_; ~€gf~~~~~~~~~~~~e ·'?tt
richloroethene TiiC hloiO f luc:iromethB.ne ··
Viri)rl'' clilOdde
•
ylenes, Total
);'ill\{:... ._: :.'tfhW>----'~--:',.:,,,,;,: .. -:--b:,,.,)::
,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
~~~1\. 212-~.Teti·ii"ChlOrcieth~me: --iliL. a ,-~, -2 -TiiChl.O'ioeth.i:ii.'e
,1-Dichloroethane -~:: ~~~ D i'c h 1'6' i6 e t hen8 \):~:: >·
1,1-Dichloropropene
d; ~ ;,:~i~-~J:~Qi~~~g:~~~:g~, ;~'1{%~-----
, 2, 4 -Trichlorobenzti!'ie
,2,4-Trimethylbenzene
·1, 2 ~o~bi'Oiii0H3 -Cti.l'ciL-6proparie /.'
Q ,2-D~bromoethane
,2-Dichlorobenzene
:-;~g-~~g}gt6·~-f~~~~~O\ --
1,3,5-Trimethylbenzene ar;}:gf;~r~-~~~~~~=~~-*<~-11, 4-Dichlorobenzene
272;_o~_t:hlbr:oprop:ane--,-;_ ,; •L,,/-
2-Butanone (MEK)
I.~Chlg_r_()O::.t:hY~ .. ..v_inyl ether "..><.o:-.. ·;::._Chlorotoluene 'A'"T' · ---->«
-Chlorotoluene
4 -Methyl-2-pentanone IBK}
~~~~Igi:~,n;;,:gr.
Bromobenzene . __ ,,
~~~~~i~~!:::~;::::::
ctil'OiObe-ii.£€rie~---"'
l hlorodibromomethane
hloroethane
hloX:C:i.~9inliHWW::::.::·.:: ,,. ,_,.
Chloromethane
cis-1,2-Dichloroethene
I~ t ~{ !'~~~~~~ ~1 ~-~~~~O'p·e-ne
)ibromomethane
DiChlOrOdi'flUOromet:hane EthY1be·nz.-ene· -------------· ... ---
l~~~i:IS.0}_()r().b.~.tad_ieJ~_em s_opropylbenzene -,::: .. ::,/?:-:·
4ethyl tert-buty1 ether
Methylene Ch1or~de
~~~~~-;~t~~~~t:I~:: .
I
Quality Assurance Report
Level li
L169027
Result
''Labc>ra.t6ry·· Blan~'k")
Units Date Analyzed
Tax I .D. 62-0814289
Esl. 1970
September 17, 2004
Batch
:-:-oo 11 ___ ,, 't~ %$!1Jmg/1,,,,,,:!ttr: :::o 9/-1'3/ o4 21":'4 9}~~ ._}\WGl 1.o6 o 1 '®h'
" .001 mg/1 09/13/04 21:.49 ... WG170601
< .001 mg/1 09/13/04 21:49 WG170601
-: -:·-ggfK \N£tL ~'~~f&i¥ Ig~g~~g: 'i~iT!~~:'-" ·-""~gi·~g~g£·-:-':\
< . 003 mg/1,.,........ 09/13/04 :49 WG170601 .:. --':SWift-::'ttl®I_J}i k'hfW_-::-_ --,-
mg/kg 09/13/04 2 : WG170.6i8
mg/kg 09/13/04 22:10 WG170628
:,:::--.:::'!':'001<" .}:::o:,;;tknt:!"!19/kgU'ftf09/13/04 :~'22: Iot.tzj }11G17.0628 --.. .-,--' "-.001~ mg/kg 09/13/04 22:10 WG170628
<: .001 mg/kg 09/13/04 22:10 WG170628
"·:::<'001-}''. _mg/kg$%f_09/1'3/04--:~ 22 ·:-loft·· -_,_,_WGl 7.0628
< .001 mg/kg 09/13/04 22:10 WG170628
" .001 mg/kg 09/13/04 22:10 WG170628
'f< v; oo 1 '-~-,:--_ m9 /kg·,---_-·a 9/13/ o 4 _,,_2 2·: 1 o wG17062 a :n":?:Z->:-:-o: -~< :oo1 -mg/kg· 09/13/04 22~10 WG170628
" .001 mg/kg 09/13/04 22:10 WG170628
··. c:)t-:.-·ool ,_.;'\':"F©JK<-': ffig/kg_ /\-\ ___ 09/-13/04 22:·.-·1-'o -~-_, __ wGf7062a, -~---s,tJ/2;,
" .001 mg/kg 09/13/04 22:10' WG17062B
<: .001 mg/kg 09/13/04 22:10 WG170628
-;, , :· 0 0 1'::-;\:. --"':?::0:@.:~ :--iiig/kg£:jf{'09/13/ 04 :~: 22'; l ---',WG1 7.062 8
" . 001 mg/kg 09/13/04 ---22_0_1 WG170.628
" . 001 .... !Jl9/kg ........ 09/13/04 22:10 WG170628 -~oo ':"JJ.tng/kg·;::-:A:L_o9/13/0.4:;,22: 1 _WG17062B}t, :--'--'T\lli,<I.(
" .001 rrg/kg 09/13/04 22:10 WG170628
< . 001 mg/kg 09/13/04 22:10 WG170628 Iti£& •. 3 . oar·--.:<Tng/kg1t:::iill.D9/1'3 to4-p2:;:1o_:::: CN&WG17062
" . 001 mg/kg 09/13/04 22:10 WG170628
" .001 mg/kg 09/13/04 22:10 WG170628
"_, ~'; 00 _,_,, __ -,-c,o:.;-,£'iitg/kg 9/13/0.4\ 22: 10··· ... ·WG17062B/f,;o
" . 001 mg/kg 09/13/04 22:10 •-WG17·0-628--'~-
" .001 mg/kg 09/13/04 22:10 WG170628
. 0 0 1':):::~::: <~~~tmg/kg{(:@fo 9/13/ 04":.:;22 ·; 1 Of{#i:WGl 7,06 2 8 .. :. " .001 'ffig/kgy ___ ·o9/13/0.4 ... 22--;-1o _ _,. wG17062a·· ·
" .001 mg/kg 09/13/04 22:10 WG170628
...... ' -<';";'00 (Jfirig/kg .-,,~_>o9f_-13'/0.4\-22':-l'O WG1-70628 t:,v .. ,:O -30'· {
" . 001 mg/kg 09/13/04 22:10 WG1'10628
< .001 mg/kg 09/13/04 22:10 WGl70628 i&Wf'!.' < ·-::-·:·o 0 1' t:·· ___ ,,._Mhfuf:_itig/kgf:@@tto 9/13/04 2 2.: to: \tT WG17 0 6 28
< ···.-:oo1-mg/kg 09/13/04 22:10 WG1.7062B
< .001 mg/kg 09/13/04 22:10 WG170628 ---· '-:-! _,<,&-----oo1 ./."'" }-, ,.iiitg/kg_-,,,,,,,,i@'_o9/13/04]22::1o'''"' :.:t\WG1-7062o,,,,,,,, , < .. ·:oo1 mg/kg 09/13/0-4 22;10 WG17062
" .001 mg/kg 09/13/04 22:10 WG170628
''"1 /·.·_ .• ,,,,,,"",<. ~ ~i "":¥%&: :t:>~~~~,-_:''<~~~i~-;~: .. ·-~r: i'~ ____ _J· -~gi ~-~~s~:,,._ •.. Ji),,,,_,x
" . 001 mg/kg _____ 09/13/04 22:10 WG170628
--"':-wool l·: -iiig/kg(<tr'-''09/.-13/04-)22:-1o:: :':~:::'/_WG17.062S ----_,,_-_\P0.W:'\: ...
" .·o·ol mg/kg 09/13/04 22:10 .. ---WG170628
" . 001 mg/kg 09/13/04 22:10 WG170628 m,_;u;z..,,;, " · '::·'o o 1,,"....: ::,::-o"dFf&-__ rug/kg,-,,~d' , ___ o9 /1'3/ o_4 2 2 ·:·ro_ ... ,. WG1 10 62 a:· ___ ..... ,,,,~--; "
< .001 mg/kg 09/13/04 22:10 WG170·6.i8 __ _
xxx·,;x-h1:gg i....... ---. ._,~ '·''-~.--.r~~~~wws:~ ~A~-~~!\~;+ ~-~nrsr: ~gi,~~~ ~~-\./, z,w, " . oo1 ........... mg/kg '09/13/o'4 .--2i: 1o·-~---WG17·o·62B
" .001 mg/kg 09/13/04 7.2 10 WG170628
Cijfio••••····-~d'::"OOLo--, __ filg/~g --. __ :09/1'3/04~--22 10 ·;,wG1;7_0628'''/o--·~, "·---_-o-o_f___ mg/kg 09/13/01! 22 10 WG170628
< . 0
" . 0 01
Page 33 of 56
' '~
I I. ENVIRONMENTAL
SCIENCE CORP.
~~coastal Environmental,
Mr. Mark Hafenmaier
01ss7 West Main Street
IIMurfreesboro, NC 27855
Inc.
'
Quality Assurance Report
Level II
L169027
.001 m /k 09/13/04 22: 10
rfiLiibora,_tor·[ Bl~nkAf qaphthalene
nal te Result Units Date Anal zed
I
-_-.;;~~:vloor
" . 001
< . 001 .c=n· £.< . o o 1
< . 001
< . 001 AS:t . AAi< • oo i'K
< . 001
< • 001
-'':(£ ''''0'00
< .-oo 1
< . 003
< :' .. bar
..•••••• ,..,." .001 " .. ,:<''''':'·oar_--
< . 001
:'{, __
< • 001
···-~-,~-:~:~:''::'(<': -_-. 0 0 1 .:;;.
< . 001
Page 34 of 56
12065 Lebanon Rd.
Mt. Juliet, TN 37122
{615) 75B-585B
1-B00-767-5659
Fax [phone]
Tax I .D. 62-0Bl42B9
Est. 1970
September 17. 2004
WG170628
Batch
·y-·o-·----
12065 Lebn.non Rd I I. ENVIRONMENTAL
SCIENCE CORP.
MC. Jull-et, TN 3'1122
(G15) 758-5858
l-800-76?-5859
Fill< (615) "158-5859
~~Coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~~Murfreesboro, NC 27855
llexachlorobutadiene
Analyte
I
Inc.
Quality Assurance Report
Level II
Ll69027
< . 001 mg/kg 09/14/04 14:16
Result
·_Laboratory BlB:nk_ .. Units Date Analyzed
Tax 1 .D. 62-0814289
Est. 1970
September 17, 2004
WG170773
Batch
< ··• 001 ·:·-··.:1tViJ/k§lit:S09/.i"4'/04 ,14:16 l~q, WG170773----
< .001 mg/kg 09/14/04 14:16 WG170773 _____ _
< .001 mg/kg 09/14/04 14:16 WG170773
.OOl"W(" _· __ , mg/kg·-~;':-.09/14/04 1':4:;-16~ _,,WG1707.73
< .001 mg/kg 09/14/04 14:16 WG170773
< .001 mg/kg 09/14/04 14:16 WG170773
< '.oar,. ~'--~ :..;w·mg;kgJW"'::09/14/0_4]-1'4: 16"$/l, WG17.0P3''\lliW"
< .001 mglkg 09114104 14:16 WG170773
< . 001 mglkg 09114104 14:16 WG170773
:.:.d;:3£:;':?' ':>-~?fl.< .... 001 mg/kg__ ;_,09114 104'-.1_4_:1_6<: .~101·7.07_73.
< .001 mg/kg 09114104 14:16 WG170773
:i£~ ..
< .001 mg/kg 09/14104 14:16 WG170773
< . 001\ ;;~mg/kg£:~%09114/0.4{14: 16t;_·_,,/ WG170.773]£if §t;,,_t
< .001 mg/kg 09114104 14:16 WG170773
< .001 mglkg 09114/04 14:16 WG170773 __ ,:.{i/2\:. "{;=~: :':Jt::::<;_. 001 ·r.-·"' ·mg/kg:$'h,_~·09/14I04_?1:{: 16V.s~WG1707_.73
< .001 mg/kg 09114104 14:16 WG170773
< .003 mg/kg 09/14/04 14:16 WG170773 .. ·· w--. -rttW':'::~~" nm.~<-·ir~~?~1r -~0'~ .-.-.JJt*:-::::''::·:::::ratimn ::::r:::::w::...
< .001 mglkg 09/15104 17:59 WG170929
< .001 mg/kg 09115/04 17:59 WG170929
;. 001' · :;.. mg/kg.,£.:::['09I15/04:~P-.':59 ~ ,_,iWG170929
< .001 mg/kg 09/15/04 17:59 WG170929
< .001 mglkg 09/15/04 17:59 WG170929 .·.-.. {#% .... ,2£< . oor:c~w:-:":.-mglkg:0J\<'::.o9/l's/o4;;M7, S9f¥f1.:, WG170929
< . 001 mglkg 09/15/04 17:59 WG170929
< . 001 mg/kg 09115/04 17:59 WG170929
. 001 .:: mg/kg~~09/.1_5I04f17.·: 59 J.-:(WG170929 _._;c·· '""'"''·'·· < .001 mg/kg 09/15104 17:59 WG170929
< .001 mg/kg 09/15/04 17:59 WG170929
. 001 ::::fffiglkg.}t::::=t)09/i5/0'4''\17,:'59 WG170929 ''<'fffu~:··
< . 001 mg/kg 09115/04 17:59 WG170929
< . 001 mg/kg 09/15/04 17:59 WG170929
<: ,::::-.·001 .S:lt®K .. ~;:..-.Jri\glkgW'tW09/l'SI04}1,7.':' 59' !ft::WGl 709
< .001 mg/kg 09/15104 17:59 WG170929
< .001 mg/kg 09115/04 17:59 WG170929 "':::·~·y. 00 ... ·:::.:.nig/kg }{ :::'f{09/1'S/04".::r7,:Sg·:·=:::·::::=·=:;=';WG170929
< . 001 mg/kg 09/15/04 17:59 WG170929
"' .001 mglkg 09/15104 17:59 WG170929
0 :,.J§ffng /.kg J}:::::):,::o 9 /.1' 5 I 0 4 j]::: 1 :7.' i. 5 9 [@t:, WG 1.7 09 2 9 {.,,,: l;Cf\'\
< .001 mg/kg 09115/04 17:59 WG170929
< . 001 mg/kg 09115/04 17:59 WG170929
" "'"' '"""'"'""'"" , '·"'! o o 1., .. , ffig /kg_~'S:/JO 91 is/ 04·.;·==1 1:: s 9 ... · ····.·=:==<wo 1 7o 92 9,:::·: ..
< . 001 mg/kg 09/15/04 17:59 WGl70929
< . 001 mg/kg 09/15/04 17:59 WG170929 '''fVI& ·" :=:::-~·o 0 r··=,nmn::::::r. <O ::: mgl kg ~:)::mm:o 9 I 1'5/. 0 4'''::1.7.: 59' .. n: ::,WG17 0 9 2 9 1>.:::::: .. "' .oo1 ··\iig/kg""'··-· .... ·.······o9/1s/o4 1 .. 7:'59··--"wG170929,·.w--.--
"' .001 mg/kg 09/15/0il 17:59 WG170929
.'.001. ..< .. ,.,:.tiig/kg J \ j09/1'5/04 ... :,1:7_·:·s9 ... :<=:{WG170929.::=·.:
< .001 mg/kg 09/15/04 17:59 WG170929
,,,,;,!WYi ;\::-:=_g g i ·:·::::.:;,;:.'~~ j ~~::::::::::::::::::::::g ~ j_i=~-j g ~-, .g,~ ~ ~ -" ,~ <=:gi ~ ~ ~; 9
"' .oo1 irig/kg ........... o9/1's;o·4 17:59 ·wca7on
: .= :i~ g g i .. =.,:tift .-r:::: :;:::::-~~ j ~~ Ml% g ~ j_ .i ~ j g ~ =:::;:.i ~ _ _.;: ~ ~ ·:::::::::::Jt ~g i ~ g ~ ~ ~ :·.:
< .001 mg/kg 09/15/04 17:59 WG170929
< .001 mg/kg 09/15/04 17:59 WG170929
j ;·o nig/kg 9/15/04:.:: 17.:': 59)·:0.· .. :·:::_~IG1.7092
< .0 mg/kg 9115/0il 17:59 WG170929
Page 35 of 56
I
I • ENVIRONMENTA.L
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
~~is-1,2-Dichloroethene
Anal te
I
Inc.
-··
Quality Assurance Report
Level II
L169027
< • 001 mg/kg 09/15/04 17:59
·::r;~p()ra tory, .. 1311l..f1.k -.'
Result Units Date Anal zed
12065 Leb~non Rd.
Mt. Juliet, TN 37122
(615) ?58-5858
1-800-767-5859
FdX (615) '1~8-58~9
Tax I.D 62-08i4289
Est. 1970
September 17, 2004
WG170929
Biltch
. .<)'/001 ---ifWi;l :Jiiij/K~:i:ffffo9/1S/04 17 :·sg· }}}}.WG170929! < . 001 mg/kg 09/15/04 17-: sg· -----------------WG170929 ·
< .001 mg/kg 09/15/04 17:59 WG170929 ·:><t2:ooL .. :'.~iilg/kg -\).:\.:)_:o9/1S/04' 17·;-sg -: WG170929. Yh
< .001 "nlg/kg ...... 09/lS/0·4--"t?·:·sg· WG170929-
< .001 mg/kg 09/15/04 17:59 WG170929 ,.:: :::< 001 ... .J%1\t" -7(itig/kgjifff'-'09/l'S/04 17.': 59.: tft''.WG170929-< .001 mg/kg 09/15/04 17:59 -----WG17.0929h
.:: .001 mg/kg 09/15/04 17:59 WG170929
;B'Jft-.;'oot '"' ~·mg;kg _o9/1S/04_:_n:s9-' ; ~IG170929'
< .001 mg/kg --69/15/04---17:59---WG170929 ·---" .:: .005 mg/kg 09/15/04 17:59 WG170929
oof· ... :Af:ffig/kg_:·M@I09/.l'S/04 17.':··sg =:-:::::m_wopon9:
.:: .001 mg/kg 09/15/04 17 .. :59 WG170929
< . 001 mg/kg 09/15/04 17:59 WG170929
-'.'<'COOl ::rng/kg---_3;..09/15/04'_' 17·;·sg=-:,--: -WG170929{•pc )Ii
.:: .·ooi mg/kg 09/15/04 17.:'59 WG170929
.:: .005 mg/kg 09/15/04 17:59 WG170929
001 flf@j( !"itig/kg.:tf@:09/iS/04 17_·;··sg :-:::::::::/WG170929).\.'-
< .001 mg/kg---09/15/04 17:59-WG170929
< . 001 mg/kg 09/15/04 17:59 WG170929
. 00 h:-:::::::::·.· ::::)ifing/kg,:)]:):\' 09/15/04: :17.: 59 ·(:]:WG1 70929{('·
< . 001 """ffig/kg" 09/15/04-17.:'59 WG170929
.:: .003 mg/kg 09/15/04 17:59 WG170929 :PP% -'Ad dTIIi Wif" .·.··.·. •·c+ffii• ;'-It; __
0. 00 % 09/16/04 ii: 09 WG171054
_,::-
·-s
Page 36 of 56
I I. ENVIRONMENTAL
SciENCE CoRP.
~~Coastal Environmental,
Mr. Mark Hafenmaier lf57 West Main Street
~~Murfreesboro, NC 27855
ramo form
te
I
Inc.
Quality Assurance Report
Level II
L169027
< .001 m /k 09/16/04 20:08
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-~BSB
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 17. 2004
WG171139
Laboi"atar'j::-sliiii.k Result ---· -·uni'tS _______ Date Analyzed B<~tch
Units
&pup_l_ic_<i_t;e·~tc
Result Du licate RPD Limit
-:WJ
Ref Sam Batch
:,:.: LabO:r:!:it:O_i'Y}_96i1t.~ol ',:'S_#_i'iiplei,(. ..
Units -Known Val Result Limit %-Rec Batch
---O''l''Ol941@:;·:,_ . )\:-::~97·. 2 84:~_128]f;,WG17060l 'tf\ o.·ot82~ .. 90.9 71-122 wG17o6ot --
o.ot90 94.8 78-120 WG17060l Yi'ltll~.··•·~t -.;:raas:::'J:!: _ .. ;3:7Jt27:l%{WG1706ol
.01 -95 .. 5 82-117 WG170601
0.0186 93.0 59-135 WG17060l
. 20.6 103~-:~.:t {\6o·;:,.l66~~J~,,-:-::·wG17o60l
0.0193 96':4· 67-132 WG170601
0.0226 113. 81-122 WG17060l
·:::<g--~-~i-~8 -~~i:':~>-. ~:ii-~3\,L:,,:,~g~ ~-~-~~1
0.0227 45.3 78-132 WG170601
0 ._,;,·.-0 18 9 ,%",\{.::· ···:·,:·.'·':\'(:'9 .. 4.' . -7.: ·,:·,:·,:·::,:·,:·,.:_,:,,· 8 2 .'f.'-1' 1:7 J.i;%WG 1 7 0 6 o 1'.:,·.
0.0177 88.5 58-140 WG170601
0.0204 102. 79-121 WG170601
~h.\ . 0 .'' 0 20 4 -;: 'ti-1fJt't 4 0-: 8 '::::~:~:t~::::::: 8 3 ~ 11' 3 t; ,:::: WG1.' 7 0 6 0 o .0193 96.7 ·················a1:·122" "'wG1.70601
Page 37 of 56
I
I • ENVIRONMENTAL
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
I
Inc.
Quality Assurance Report
Level II
Ll69027
Pnge 38 of 56
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
TCIX I.D. G2-0814289
Eat. 1970
September 17, 2004
94. 5 74-125 WG170601
12065 Lebanon Rd.
I •• ENVIRONMENTAL
SCIENCE CORP.
Mt. Juli"~• TN 37122
{Gl5) 758-5858
l-800-767-5859
Fax [phone]
lloastal Environmental,
Mr. Mark Hafenmaier 1f57 West Main Street
~urfreesboro, NC 27855
11,2,4-Trichlorobenzene
Analyte
Inc.
I·:::·;T~};;~~~~=~:~~i~~~~~;~~ane
,2-Dibromoethane
1:\'2 i D ~ c hl (:i_l:.-oben ze~.E! ),:·::::
1,2-Dlchloroethane
1,2-Dichloropropane
i 3 ;s'::. __ Tr"iinEithylho2ri'ZE!Ii.e
, 3-0ichlorol;enzene
1,3-Dichloropropane
1"':'"4 '.:: DichToi"oberiz'ene
I , '2 ·_ Dichl6i:-opropa:ne
:: 8cuhtl}~.r!~~eh.<Ml,f:;.I.<~ .. ··1· -··eth······r· .' ;:, oroet y -;:y1ny '
2-Chlorotoluene
•
-Chlorotoluene
b~~;g~1 '"'-2-~-pent"i:lr10h~.::· (MIBK)f-
crolein
ACiY:lOOit"i:·ileW
l enzene
romobenzene
:r;_oni0d~¢i:J.loi"om_et_hio__n_e_,._ -~:::._. · ?·
Bromoform
Bromomethane l~t~~~;;~;~~-~hloride
hlorodibromomethane
.Chl~~cJ:et;_Jj_a:_rle_Mf:t-" · ··• '"'•''="" • Chloroform
1-N~~~~~~~-~h~oi:Oethene .. :-
is-1,3-Dichloropropene
Di-isopropyl ether
-~~mmg~~::::::~;ne**·
Isopropylbenzene
1-HC@t~:!!~~~~~l~~~e-r 'tiD··
·······:-,.
Quality Assurance Report
Level II
Ll69027
m /k . 02 0.0215
Labo_ratOi"y 'Contrpkf.Sample
Units Known Val Result
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
108. 65-137 WG170628
% Rec Limit Batch
·:::::·mg;kg ':r·:~\/{02 '':::']Wh··· --o":"ol95:?·W~:;·,:... 97':,··-,. 74~127 'WG170628
mg/kg .02 o·.o11C .. .__.... 8·8·.·a·· 6·0.::133 WG170628
mg/kg .02 0.0202 101. 65-133 WG170628 .1fL·_ -,,"_·:.fig/kg ·'}:·02 o·:''0209 105_:-'j:_'[f 72'~128 __ .-_WG1'70628,.-:······
mg/kg .02 o·.-0219 109. 64:..146 ~IG170628
mg/kg .02 0.0198 99.1 77-128 WG170628 .,:cmg; kg .:··-:w:r. 02 __ 0 J?'i ---:-'\:::::::·o>.o 19 6 ,_ .mf)'/ 9.7 ~''8 :::-:· ---,-~,,. 12 ';:' 12 5 ------WG1 1 o 6 2 8 .ff>~
mg/kg .02 0.0207 103 .. --68:128 WG170628 ··········.:&
··w:-.,: :·,'':\':\':\':'.'~~j~§-..... .,.: g~~-'rm.-. .:.:····· ._.-_,g.:.,g~6~-_.,...... 1~i,_,-:.,.S ~t+:i~6_,-:·. ·:·: ~gi ~g~~~-:-, ... ::.::·
mg/kg .02 ····0 .. 0223. 111. 63-156 .. _.WGl7.o'628.
m%~j~~m?' ::::ri':i:::._ ··"lx---kfffig~g~~ 9 . ~,~_,;-~-,: ''''~NJ.\~~?i!i·,gq~gi ~-g~28
· mg/kg·--··-. 02 ,.._ ·a·. 02.07 104. 6<1-131 WG170628
··--.·~§j~~ · 02
.. ~ .. ;:-~~~}. · ........... !/_i-~i:_,,;._,_._. ~~:.=·i~~<·::·~:,~~gi ~~g 8
mg/kg .1 o .... 0873 87.3 18-:\'<13 WG170628
_____ 1119/kg 1 0.489 48.9 20-137 WG170628 :tif:.t-.. ttmg/kgft :%21{-.; ~· --.%0} ::::ro-~~0734-,73 ';~4]ff.@;6o:l'42'_,,_-__ / WG170628
mg/kg .02 -----·-o·.-o-197 98.4 76-140 WG170628
mg/kg .02 0.0214 107. 73-124 WG170628
mg/kg':/:. . 0 . 0219·:. -~MTO;>. 1:·~.1'36fi{_;_,}WG17062S mg/kg . 0 . 0207 ----·-·103. 73~'124-~, .. --·.wca 70628
____ tn9/kg .02 0.0149 74.5 26-164 WG170628
::&tk.. "':{mg/kgJ::: ::::::::,:;_:-o2w~. :c.;Jt: ~~{o c'o22:7_'_-_, ____ ,;,_.-::::::-n3··c\-tlliUMS2,21S4· ..--~ WGu_o628
mg/kg .02 0.0203 102. 65-131 WG170628
mg/kg .02 0.0207 103. 70-114 WG170628
'':::fLtilg/kg:(:-.02 0.0186.. .·.ott~/· 44·160 >-'-WG170628
mg/kg .02 0.0196 97.9 70-139 WG170628
,,.::D t:WJ:}(\ ~~:~:~:~::.~~~:~ j ~~ TI-)\f~ g 2 ·-4%¥ g -~-g ~ 0 1
·::, ::~ .i g ~'':t ---:: ·::':M ~ ~ ~ i·! i':·~'::::::::: :, ~gi ~ g ~ ~ ~ ---mg/kg .02 0.02 ·106.---.o8·1:150 ....... WG1i0628 __ _
mg/kg .02 0.0171 85.3 74-147 WG170628
.. :&:!!19/kg.~ 02 .. o':'0209 :: ·' --1-os>_-,~~~~:;:::,,,, .·7 . .7.~121)il::@WG170628
mg/kg .02 ··'o .. 0238. 119. 17-134 WG170628
>;; :tt-: · .. ;·: :t::::::::::r;%~ j ~§ WT-: ~--;-g ~ -·:,:-:'_iBfJ g ::::· g i: ~ ~ ~:).; .. ·-:::t~: ~ ~ ,,; j _, --W$ ~ ~ -~ i-~ ~ :::::::::::::--~g i ~ g ~ ~ ~ mg/kg .02 0.0198 ... 9·9-.1 .. 63:120·:·:········· WG170628
mg/kg .02 0.0201 100. 64-142 WG170fi28
--~:w~-'''t'HHi.~/kg, :_.y;•o2::::' ;'f':it> ,,_-~0~0162"'''7 -·y8o _._-B)f::. 70-;:;141\K1tWG170628· ('
mg/kg .02 ·-·o-.0192 95.8 58-161 WG170628
mg/kg .02 0.0193 96.5 73-128 WG170628 n-Propylbenzene
N i'l Ph t ha 1 ene ;::~t~~~~~:~:\:· " •( ''"'' '*''''''''''' mg;k9 T:--::::::::}·::-o .·:.ttwm:n:o::-:o1·B3 1~;',7/f+J~;Ao~~:r32: WG17.o628
1:~-~~-:~i~~;~~;tr~:-. Sti. tert-Butylbenzene
Tetrachloroethene
IO:li.i'i:i'ri'Ei\~:::: ::\)~~tH·... .:·.::::<~~\:·,·
r<JnS-1,2-Dic.:hloroethene
rans-1,3-Dichloropropene
Ti'ichl'O:t<ieth.e_ne·-· ·yi@OO: ~--·A!!?" Trichlorofluoromethane
.., i.t1ly_l,_._c_tJ:lor: icl;e1,_v .··.··.·.·.•,-'""':0.: .. • ~Y enes·;,_::,Tota -, =
1,1,1,2-Tetrachloroethane
1'',:1, l.:Tri'chl'oroet.hane '¥~-·-~l ,'1, i;2 ~Te·tr:ach:ioroethane
mg/kg .02 0.0208 04. 69-130 WG170628
mg/kg .02 0.0200 99.8 64-124 WG170628
.: -~~g/kg· · ''{;'02M :;'"~:Jto"::0201';:;~--':·-:-:-:{\[101 , ___ ,,, ___ ,_, ___ , " :64'i128_t&kWG17062_8
mg/kg .02 0.0203 101. 65-127 WG170628
~~ j~§_:-::-,,_._. i g~ <.:·;_,_:Jill.@ r:~:~:~:g tg i-~ 9°,IK ,,,,,,,,, .. '" 9° ~'Y4 ~~~~~:)~4:~~ ~;.i~ ~-~gi ~ g ~~ ~
mg/kg .02 0.019 % .. 0 ...... -.,9:152 WG17.o'628
mg/kg .02 0.0185 92.7 65-150 WG1'/0628 x:w;, ,,_11!9/kg ;yo2-------·-o":'o2o4/ 1o2:·~·?':: 1s;;x4s_.. WG17.0628 _._
mg/kg . 02 o". 0194--97··.·1--30-130 WG170628
mg/kg .02 0.0172 86.1 39-127 WG170628 .:.tar':_ .· . .)ing/.kg"\ :t%oG __ ,,.., rrtc'"' '" ,u.m,,,..... .98~:''1. -:'-':·_-64'£129-"WG17o628
mg/kg
,.-.:-,_mg/kg:·:
mg/kg'
. 02
:o2y···
.02
Page 39 of 56
0.0214
O'f01'84
0 :·0210
WG170773
WG170,7.,73
WG170773
I
I • ENVIRONMENTAL
SCIENCE CORP.
~~coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~~Murfreesboro, NC 27855
,1,2-Trichloroethane
I
Inc.
Quality Assurance Report
Level II
Ll69027
. 02 0.0207
f_ L_aborcit"¢:fit.Contr'()_HfSa_iiiPle_Jj Unite Known Val Result
Page 40 of 56
1~065 L"bo.non Rd.
Mt. Julie~, TN 3'1122
[phone]
1-800-7G7-5859
Fax (Gl5) 758-5859
Ta>< I.D. 62-0614289
Est. 1970
September 17, 2004
] 03 . 66-127 WG170773
% Rec Limit Batch
I
I ENVIRONMENTAL
SCIENCE CORP.
lllaastal Environmental,
Mr. Mark Hafenmaier
Inc:.
~57 West Main
.urfreesboro,
Street
NC 27855
r. rene·s, '".TOtal
,1,1,2-Tetrachloroethane
1', 1 ;t'~Tr'iChloi-oethane _
-1, 1, 2: 2-Tetrachloroetha-ne
1: i~~~;::;ht--~~;~~h=-~-~~-~-~-
,1-Dichloroethene
1,1-Dichloropropene
1', 2, 3~Trichlorobenzene :~-:­
,2,3-Trtchloropropane
,2,4-Trtchlorobenzene
, 2/{~Trimethylbenzene ·
1,2-Dibromo-3-Chloropropane
~~-~iH~~~i~§~~gi~-~_e_-._:--: ...
.,,2-Dichloropropane
-1, 3 /S':',Ti''imethylb€ri'iene
1,3-Dichlorobenzene
,3-Dichloropropane
'/,4~DichlOrobE;!J,izene
2,2-Dichloropropane
2-Butanone (MEK)
~~g~t~!~~~r~~g·tnYL :etn·er,_}:---~;
·4::o_Mei_tJ1yl''f._~~~pEmt;anone (MIBK)'
Acetone IC::_I:01!2i~ ..... .,_,,,,,,, ,, crylonl-tri-le:' ___ ~ ', ,,,,?CIC'i'''"X,
enzene
Bromobenzene
~~~roin'OdiC:hl'oroin'ethane -~~~-~~i.~~~i~COlOiide CCtwli
Chlorobenzene
1·~~§~~-~ ~-r~~~u_:,:,,~).~,~-,~;/0 lie -crw'/
Chloromethane
:c-rs~'i',-2~DiChl0i"oethene ;\r·:··
l is-1,3-Dichloropropene
tbt·~~-~~~i_h!n:~m-ctiWP/ Dichlorodifluoromethane
Ethylbenzene ~~~~:~~~r!~~~~~~~:n:::,~er -: ... _,,~,, .....
_M.E!tl1Yien.E!::IC!:Llgfid_~ffi%: t:::: :LL. _ t: «
•
-Butylbenzene
-Propylbenzene
~~~;g~;~~1 ~-~tt:~ ;·;·e
sec-Butylben~cnc s t y reile ~,,,,,,,,,, .. -_,-,,_,_-,,,_,i'~t(!Wr l:'ert'-Bu~:y·lbenz ene
I
Quality Assurnnce Report
Level II
L169027
Page 41 of 56
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
97.5 39-127 WG170773
I I. ENVIRONMENTAL
SCIENCE CORP.
ll:aastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~urfreesboro, NC 27855
I
Inc.
Quality Assurance Report
Level II
L169027
Page 42 of 56
'\)\o:·:_ola
0.019
0.0172
-~~~:~<AU: o ·:;'on 2lf·:'_----o.ola4
0.0210
\:'~0-.0528.-.
12065 Lebanon Rd.
M~. Juliet, TN 31122
[phone]
l-800-767-SBS9
Fax (615) '158-5859
Tax l.D. 62-0814289
Est. 1970
September 17, 2004
"<R\92. s
99.4
86.1
sa_:~3~v-·
92.2
105. <tf_,r,-· a a :
.75~'-1'25~~::-
79-152
65-150
,'75'.::.1'45 .. 30-130
39-127 64:~:129.
._.WG170929/i
WG170929
WG170929
·-:-:wol70929.:·
WG170929
WG170929
:·:wG1'7.0929
I I. ENVIRONMENTAL
SCIENCE CORP.
llloastal Environmental,
Mr. Mark Hafenmaier gf57 West Main Street
UIMurfreesboro, NC 27855
lfthylene Chloride
Inc.
Quality Assurance Report
Level II
Ll69027
mg/kg . 02 0.0215
lf_Lab~·r~ tory} COn t roJ _[ Sil.inp re·--
107.
1206~ J,eba!lon Rd.
Mt. Juliet, TN 3'1122
[phone]
1-B00-767-~859
fa>< [phone]
Tux I D. 62-0814289
Est. 1970
September 17, 2004
70-141 WG171139
Analyot"e"----------------------------------U~n"i"t~e ____ "Kn~o"wcnccVoaclc_ ___ R~e"s~u"l't-------"'~R'e~cc_ __ -"L"i'moiote-__ ,B"act"c"hc_ ____ _
Page 43 of 56
I
I I. ENVIRONMENTAL
SCIENCE CORP.
I . Coastal Environmental, Inc.
Mr. Mark Hafenmaier
[
57 West Main Street
urfreesboro, NC 27855
rloroform
Anal te
I
Quality Assurance Report
Level II
L169027
mg/1 0.0180 0.0181 0.720 26
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax !.D. 62-0814289
llgt. 1970
September 17, 2004
90.0 WG170601
-,::)J:...ilb()ra toiYX Con_t_z::ol·)·s<lmpl¢} DLiplTCa t:e$
Units LCSD Res Ref Res . --RPD -Limit %Rec Batch
Page 44 of 56
".."·.
12065 Lebanon Rd. I •• ENVIRONMENTAL
SCIENCE CORP.
Mt. Juliet, 'TN 37122
(615) "158-5858
1-800-767-5859
Fax [phone]
llloastal Environmental,
Mr. Mark Hafenmaier
11ss7 West Main Street
~~Murfreesboro, NC 27855
'
romoform
nal te
Inc.
romometha-ne':<&Jk, .•·ffi'>i!k
•
arbon tetraChlor
hlorobenzene
chlbi'odibfOrriCime thaile ·chlOroetli.ane··-· · · ·
~~~~~~~~~~~gio:!eg·~~~e "·••••••••••••••••••••••
cis-1,3-Dichloropropene
ni~P•.<?P:I:<JPYXr:e_th¢i:'}\L' ~~-l ibromomethane
ichlorodifluoromethane
thylbenz·ene··. ·.:·:~?\~~~~/')}t:': ••• A®i.i.( Hexachlorobutadiene ·-'-''
Quality Assurance Report
Level I I
Ll69027
mg/kg 0.0224 0.0207 7.80
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
17 112. WG170628
))Laboratory Coiit'i:~ql SamP.F~/DupliC:ate
Units LCSD Res Ref Res . RPD Limit %Rec Batch
· ·"tl%.tiiii9/k9·-::;;w:::o 1s 9."/'' o ·;·o 1'4 9ft ·,· 6'}soY·· .. 1 7 ~ :g,79,. 5 "\M\wGno62a ''R%;C: . · · '·mg/kg ........ o·.0220_ ... ,,o .. 0227·~''""i.ss 23 110. WG170626
mg/kg 0.0213 0.0203 4.52 25 106. WG170628
~~; ~~ W.i.'.t .g~.~ ~ ~ ~..iJJ.~.t g :~g t ~~·.).&f.~-:-6 g4 ·i'::~ ~ z zr:s:~ ~-~~ '~'?<:~. , ''':'.:. ~g i ~ g ~ ~ ~ .:· ,, . , 'f
mg/kg 0.0182 0.0196 7.47 22 90.8 WG170628
... ,., ]ffig/kg o·'':'o21'3 o~'~'o20lf;:':::-,:·6:':''i3 ,:·2 101,i' ~~~~<:/t~WG170628 ,.,,"'
"mg/kg o·.o197 0.0211 ...... 9:73 22 98.3 WG170628
mg/kg 0.0213 0.0211 0.989 28 107. WG170628
~·. ~/kgdffO}O 1 71')J@'_O·tO l7l':Xf0''; 293{.j 23: .))1@8S"i'§. .WG1706 28t ~. ":'-"'...";
mg/kg 0.0208 0.0209 ·o·:s27 29 ...... 104. WG170626
mg/kg 0. 0250 0. 0238 4. 55 21 125. WG170628
•i-illfiF/." ··:· Trig/kg·~·.. o·.:··o20-J'·"'·'··· o. 01'95:::3>··· 3 93 .... ,2 0 f'%»\(iWG170.62B'". ···• mg/kg:: 0 :·0189:·:· o :·0189,.~,.,,. o: oo 24 94.3 ,.,,.' .WG170628 ·.·.·
-~~~~~~~!~~~~~~r~~~_t_her ~~-Butylbenzene
mg/kg 0. 0208 0. 0198 4. 78 20 104. WG170628
v•••···•·············:::;~ ~jJJ.IT.\9 1 kg tmt.o :ro 19 9 Jt'tJ.O _.;: o 2 o 1\C.~, o '~ o1 5o.. 2 ·4 . .-.'8"\9.~.·,: 6 ·.·,:·:t~:::{~ wm 1 o 6 2 8 .. '':'%'" ~"
mg/kg .. 0.0162 0.0162 ·o·:·494 11 .. 81.2 WG170628
·n;Propyu.i·enzene c ~'WJJ:~··':···
~~.!] ~-~~~~~!~.~-~~; ~ .. ' "e" ''•••• Styrene
tert-Butylbenzene
et·racliloro-etneriey -> o-··., .. £fill.. l oluene
rans-1,2-Dichloroethene
tz::aJ1·0.:CJ'"i"'}.~Dich~·()_r_()P.r'OPe:iJ:e·~:(::/ Trichloroethene ·
~~?~~'1·~~~~~!~~·\t~.:fhan~ma:r,·
I
mg/kg 0.0197 0.0192 2.58 22 98.3 WG170628 '%#:;} ' ffigfkg}} '' o":' 02 05 i{ff:i.O:":"O 193)§1%5'!98':',':~'"':~2.4{;:::. ·>1 02.'-:jtt:;f~WGl 7062 8@W:\) .. ~
mg/kg 0.0203 0.0183 10.2 26 101. WG170628
mg/kg 0.0217 0.0208 4.15 23 108. WG170628
/)\).f)':~mg/kg/'' ._.,0,'0209}/ o::.·_o200)/· ... 4·_,_'51. 2 104 o.628 ·.r:a;:;:·:::-
mg/kg 0. 0208 0. 0201 3. 28 26 104. WG170628
mg/kg 0.0212 0.0203 4.48 25 106. WG170628 .-.:Jttf,, .mg/kgNf:<o·:~o209Nt:Io'~o2oo..:;:.w4:'~-n't::: i24tillt@104 %iWLWG17.062SI., .. --..:..X.YJJ.f/
mg/kg 0.0205 0.0199 3.17 17 103. WG170628
mg/kg 0. 0181 0. 0192 5. 79 20 90.6 WG170628
_ .. , .. ,_j~fu.iitg /kg .. )\O}.Of8 7 )\o:·~'.0185ft):~:;(o'::··5 9 2 5~( ... :.: 93~'~' 3 ~'?<;:::.::.".WG1·7.062 a..)${<}\}~.
mg/kg o.0206 o.0204 .... 0.828 /.2 103. WG170628 · ··
mg/kg 0. 0184 0. 0194 5. 39 20 92.0 WG170628
"@•••••••••••• , .. ·. '''\(Cffig / kg .:f1W 0:: 0 18 6 'i%.0' 0 :·:' 0 1 72 @@(7-. 8 7&;::kl6 ~-.7.'{ 9 3 ··;· 2 ~·/t':i WG 1.7 0 6 2 8 £;.~·· .. · "¥\
mg/kg 0.0609 0.0589 3.39 20 102. WG170628
Page 45 of 56
I
I ENVIRONMENTAL
SCIENCE CORP.
llcoastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~urfreesboro, NC 27855
-~etone
lllnalyte
I
Inc.
Quality Assurance Report
Level II
Ll69027
m /k 0.115 0.108 6.47 23
12065 Lebanon Rd.
M~. Jullet, TN 37122
[phone]
1-600-767-5859
Fax [phone]
Tax I .D. 62-0914289
EBt, 1970
September 17, 2004
115. WG170773
::t:J,il_bora t:OiY.ICOnt:;.':!?l.::Soiliip_le ..:.PiJPH'ca te ·
Units LCSD·Res Ref Res RPD Limit \Rec Batch
Page 46 of 56
I
I ENVIRONMENTAL
SciENCE CoRP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
11,2-Dichloropropane
Analyte
Inc.
Quality Assurance Report
Level II
Ll69027
mg/kg 0.0201 0.0206 2.66 17
::, _,_I.Ilh§i-a tci'iY.f Ccint;:ol J.S?-'mp_l_~ .&pup 1 i' ca_t e 0
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-?67-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 17, 2004
100. WG170929
Units LCSD Res Ref Res RPD Limit %Rec Batch
Page 47 of 56
I •• ENVIRONMENTAL
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
!1,2-Dichloroethane
Analyte
Inc.
Quality Assurance Report
Level II
Ll69027
mq/kg 0.0200 0.0206 3.05 23
.\l\_I._ilb(itat_ory Cont.'J:"_ol Samp~-~\Pi,lpl'i''cfltep:
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
TilX I .D. 62-0814269
Est. 19?0
September 17, 2004
100. WG171139
Units LCSD Res Ref Res RPD Llmlt %Rec Batch
illJM~-~-~~~"i-?P_ikeJ.i Anal te Units MS Res Ref Res TV % Rec Limit Ref Samp Batch
Page 48 of 56
I
I
I ENVIRONMENT l\L
SCIENCE CORP.
ll:oastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~urfreesboro, NC 27855
,1-Dichloroethane
I
Inc.
Quality Assurance Report
Level II
L169027
m/l 0.0220 0.0021 .02
Units
_o:::::::, Matr:_ix · .. Sp"~kep MS ____ Res Ref Res TV
Page 49 of 56
12055 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fux [phone]
Tax !.D. 62-0814289
EBt. 1970
September 17, 2004
99.4 47-138 Ll68999-07 WG170601
\: Rec Limit Ref Samp Batch
I
I ENVIRONMENTAL
SCIENCE CORP.
llcoastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street
~~Murfreesboro, NC 27855
~inyl chloride
nalyte
I
Inc.
Quality Assurance Report
Level II
L169027
mg/1 0.0192 0.00 . 02
Units
mfM_<ttrix_ SjjikeE
MS Res -Ref Res
Page SO of 56
TV
12065 Lebanon Rd.
ML. Jl!lil~t, TN 37122
[phone]
1-800-767-5859
Fi!X (61~) 758-5859
Tax I .D. 62-0814289
Eat. 1970
September 17, 2004
95.8 26-110 L168999-07 WG170601
% Rec Limit Ref Samp Bntch
L168999i07f.WG170601--
I
I ENVIRONMENTAL
SCIENCE CORP.
~~Coastal Environmental,
Mr. M<:~rk Hafenmaier
857 West Main Street ~~Murfreesboro, NC 27855
etrachloroethene
nalyte
Inc.
Quality Assurance Report
Level II
Ll69027
m /k 0.0827 0.0009 .02
Units
:::::::tMati'iX _$p-~ke]/
MS .. Re-:3" Ref Res TV
12065 Lebanon Rd.
Me. Juliet, TN 37122
1615) 75S-5SS8
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 19?0
September 17, 2004
81.8 55-117 Ll68968-0l WG170628
% Rec Limit Ref Samp Batch
.,@j]ilift::;, ,; m9J kg :,,,:,,,J 0 ~-08 53 ;tt;::·· 0 ';-00 Z::::W:' 0 2 :~'JbJ> 8 5 -~c 3 ]"6 0 ::o 12 6 ::~ L 16 B 96 a:~-0 1 :'_WGl ,7 06 2 8:
mg/kg 0.0859 0.00 .02 85.9 36-146 L168968-0l WG170628
mgjkg 0.0796 0.00 .02 79.6 57-144 Ll68968-0l WG170628 -~-':Jrfig /kg :.0\08_4 7-0}_ 00 _o_~£1 02Jf.h<J;: 84'':'· l<ss-~-14 3':i1L168 96B"'Ol"-':'WG1706 2 8
mg/kg o. 0645 o. oo . 02 64.5 '25-:::-tn'·''"'L.l6B96B~·:of"wG170628
""'""""\1//)L .,·<Yf~~;~g;: :: __ _,:::~::;:~~5 ~: ~0
. ~2 8 ~:~'~;.,~~= i~~,,::::::::-ti~~~-~~f:~_i' ~gg~~~~
Page 51 of 56
I
I • ENVIRONMENTJI.L
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street
l(:urfreesboro, NC 27855
~~-Propylbenzene
Analyte
l aPhtha1ene .t~~~:~:~:y·:~::··· -Isopropyltoluene
ec-Butylbenzene s_t;;YI:!"!ne_::tt'.:;.t:::mthl@f '-_,_,_:_·_ ·
tert-Butylbenzene
Inc.
16i~~ri~-~~{J:Y:~n:e ~-
rans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Tii"chlaroethene . ·: . m·\''.r< l ifCtiloiofl uorometh.ane - -
~ny_~ _ch~m:i.cJ.e~ .... _ .... ylenes·;--:·.Totalo/--.... :::. ___ ,,, ..
I
Quality Assurance Report
Level II
1169027
mg/kg 0.0136 0.00 . 02
Units 'ill M1'l,_l;.r_i_;( --: §p-~ K¢}} MS Res Ref Res TV
12065 Lebanon Rd.
MC. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I .D. 62-0814289
Est. 1970
september 17, 2004
68.2 40-142 1,168812-01 WG170773
%-Rec Limit Ref Samp Batch
rii9/k9<H o~ooea-:::r· o:'oo:m ::::::::::'-02 . s 32~ IA-7.~ ~):L168Sli.~ ol}wG170773~
mg/kg o.·o-uf--o.oo .o2 65.3 -43-129 Ll68812-0l wG170773
mg/kg 0.0132 0.00 .02 66.2 -45-123 Ll68812-01 WG170773
)_i_)_¥j_l_l_l9/kg .::Wo_\0142 .o. oo -:-o2;''';(j;"j_j-7F 1 .46;~1'31ffit.Ll68812~ol--WG1·70},73j
mg/kg 0.0153 0.00 .0 76.3 45-133 L168812-01 WG170773
mg/kg 0.0226 0.00 .02 113. 55-117 L168812-0l WG170773
};·-(fui'itg/kg 7illiO~'O 14 7ffi{30'''''0o·:o:;:;>mF-o2::::::::::o:o-·-73~5 6Q?-126:"\}Ll"68 812::::-o l{WG170,773'-·>"• mg/kg ·o-:0173 -=-'o-:oo''d-:o2,_,_______ a6 .. 3 -36:1-46 ---Ll68812:-ol ____ WG(ionJ-
mg/kg 0.0127 0.00 .02 63.6 57-14-4 Ll68812-01 WG170773
Jn.'rng/kg ··:.':')0!0174J%·}0~'~00_ -~i_;~_!/f!02\· 8.7fT-.• ss:7:143· Ll68812i-oL-WG17.0.7,:73
mg/kg 0.0119 0.00 .02 59.5 25-111 L168812-01 WG170773
mg/kg 0.0141 0.00 .02 70.5 37-109 L168812-0l WG170773
-----::::::::i. ,.,,,,,, ffig/ kg *' ::::a '~'-04 sa~:~:t:::::::::o ·. o o -·:/'foG<: ; __ 75:·:·:·-4 '55'::.1'25'-' ·:'' L16 aa12 ·~·o1 wa1 1011 J
Page 52 of 56
I
I ENVIRONMENTAL
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street ~~Murfreesboro, NC 27855
·· rs·~-I, 2-oi"Chl'circiecne·ne
Inc.
Quality Assurance Report
Level I I
L169027
12065 Lebanon Rd
Mt. Juliet, TN 37122
(615} ?56-5956
1-B00-767-5859
Fe>X (615) ?SB-5859
Tax I.D. 62-0814269
Est. 1970
September 17, 2004
"' '/1"· 0'~'0199. '.(_,;o··: 0189Mms ·;OS'~-PiS-· _@gg-~ 4 %Ll68999~0:7~'WG170601
\_Ma t r ~_X{Sp i k1~d: Diipli C:a):-e"'o:--
Units MSD Res Ref Res RPD Limit %-Rec Ref Samp Batch
Page 53 of 56
I
I • ENVIRONMENT11L
SCIENCE CORP.
~~Coastal Environmental,
Mr. Mark Hafenmaier
1857 West Main Street
Murfreesboro, NC 27855
arbon tetrachloride
I
Inc.
Quality Assurance Report
Level II
Ll69027
m /k 0.0884 0.0766 14.3
: _:jMa t:r_ix.f~pi ke:~~~Di.ipliC;i_te .. -..
Units MSD Res Ref Res RPD
Page 54 of 56
12065 Lebanon Rd.
Mt Juliet, TN 31122
(GlS) 758-5858
l-800-767-5859
FilX (615) 75B-5859
TilX 1 .D. 62-0814289
Ellt. 1970
September 17, 2004
88.4 Ll68968-01 WG170628
Li"mit %Rec Ref Samp Batch
I
I • ENVIRONMENTAL
SCIENCE CORP.
llcoastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street
JIMurfreesboro, NC 27855
Iller lonitri1e
llnal te
l e·nz-eneffuttfJ{:::o:o,o,;,_ :$%'
romobenzene
romodichloromethane
Br_cj_ino f orl'!l\ft'S:~i_}_( _
Bromomethane
l ar]')o_!) __ t:et_z.:achlo_z.:~?~­
hl'orobenzene ·''}\Wt'·· ..
hlorodibromomethane
Chloroethane
Chloi'OfOiiii'::;' ':>'·' --.::-
11 r~--~-r~;;~ r.~¢~_()_Z.:()~_t:.h.e~.~ .l s~ 1··; 3.:::Dlchloropropene
Di-isopropyl ether
Dibromomethane
Inc.
~~~~~i·g~-~:~.!~!uoromet~ane ~exachlorobutadiene
-rSOPiO"i:>")rlbenz"en"ei" . ."f{t't 5i4!iiil'i\{.
dethyl tert-butyl ether
ethylene Chlor1de
2B.UtJ'.lbeii~:e·itewc.·· .. ·····
-Propylbenzene
J':l~Pl1.~.11ii lene .......... .
d ;;.Isopropyl toluene·,_
ec-Butylbenzene
tyrene
t ~ r .t: ~ Bi.i ty_g~~i1 z·~n·ci. ~:~:~:~:~:~~~~:%., ., .. Tetrachloroethene
D'·f~ ri~~~-;-: 2 ·~ Di Ch16icie thene rans-1,3-Dichloropropene
Trichloroethene
Tri"ChlO!"Cifll.iOi'Omethan·e·F:rr ';{"l®it:1Kf { ~~~~;e~?1*~-~~f. . .
Quality Assurance Report
Level II
Ll69027
mg/kg 0.0899 0. 0918 2.03
Mat r i Xf.sppce:::: Di.i P.~ :i ca: te
Units MSD Res Ref Res RPD
Batch number /Run number I SampLe number cross reference I WG170633: R207597: L169027-0l 02 03 05 06 08 09
WG170601: R207646: Ll69027-10
WG170628: R207658: Ll69027-0l 02 03
I WG170773: R207709: Ll69027-04 08
WG170929: R207957: Ll69027-05 06 07
WG171054: R208029: L169027-0l 02 03 04 05 06 07 08 09
WG170676: R208041: L169027-04 07
WG171139: R208098: Ll69027-09 •
I
12065 Lebanon Rd.
Mt. Juliet, TN 3?122
[phone]
1-800-767-5859
Fax [phone]
Tax I .D. 62-08142119
Eat. 1970
September 17, 2004
19 89.9 Ll68812-0l WGl70773
Limit %Rec Ref Samp Batch
• denotes out of limit range result. See Attachment B of standard report for list of qualifiers.
I • • Calculations are performed prior to rounding of ·reported values
Page 55 of 56
I
I I. ENVIRONMENTP,L
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-BOO-"16'1-5859
Fax [phone]
1'ax t.D. 62-0814289
lcoastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street
Inc.
Quality Assurance Report
Level II
Eat. 1970
IIMurfreesboro, NC 27855
L169027
September 17, 2004
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ESC Level 2 Data Package
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The qual1ty control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limit:J, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank -an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample -is a sample of known concentration
that ia carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate -is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has stcttistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference. (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 56 of 56
~~~~---------------
VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: Coastal Environmental. Inc. Laboratory Name: Environmental Science Corporation
Project Name: RAM 5 NC Certification# (LAB) 375
Site Location: _N_C ______________ _
Sample Identification L 169027-01 L 169027-02 L 169027-03 L 169027-05 \
GP-1 10FT GP~2 10FT GP-3 10FT GP-5 10FT
Sample Matrix SOIL SOIL SOIL SOIL
Collection Option (for soil)* TerraCore TerraCore TerraCore TerraCore
Date Collected 9/7/04 9/7/04 9/7/04 9/7/04
Date Received I 9/9/04 9/9/04 9/9/04 9/9/04
Date Extracted 9/7/04 9/7/04 9/7/04 917/04
Date Analyzed 9/14/04 9/14/04 9/14/04 9/14/04
Dry Weight% 81.9% 84.2% 83.4% 83%
Dilution Factor
C5-C8 Aliphatics* in mg/kg <8.7 711 <7.7 1 65 <3.5 291 <7.8 651
C9-C12 Aliphatics* in mg/kg <8.7 71 <7.7 65 <3.5 29 <7.8
C9-C1 0 Aromatics* in mg/kg <8.7 71 <7.7 65 <3.5 29 <7.8
Surrogate % Recovery-FID 94% 105% 117% 107%
Surrogate % Recovery-PID I 94% 106% 115% 104%
• Opt1on 1-Establlshed fill line on v1al Opt1on 2-Sampllng Oev1ce (md1cate brand, e.g. EnCore) Opt1on 3-Field we1ght of so1l.
H Range results should exclude any surrogates, internal standards, or Target PAH analytes.
~,cs:c8~: ~ dl:C.12~~~:~cg:.C1 a;•~ '~ A -'-.... ....t. fA~i~~3!i~}~~~~pliti2 Alijlh~citic . · •• -c-.;:,-
Percent Recovery-Fortified Blank (Spike)-PID I 85.6%
Relative Percent Difference-PID Duplicate I 2
Percent Recovery-Fortified Blank (Spike)-FlO 120.5% 99.3% I
Relative Percent Difference -FlO Duplicate 1 8 1.8 I
65
65
L169027~06
GP-6 10FT
SOIL
TerraCore
9/7/04
9/9/04
917/04
9/14/04
81.3%
<8 1 65
<8 65
<8 65
125%
122%
~~-~~--------------
VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: Coastal Environmental, Inc. Laboratory Name: Environmental Science Corporation
Project Name: RAMS NC Certification# {LAB) 375
Site Location: NC ---------------------
-~-1f"]E~~.i'f~~~'t74:~4-;~-!:-;~-~~?"~l~f :*.~~$~¢~~~~inP.!e lrifOf'!'~~ii?fE~!l.i:LA_n~JY!i~a~ '~es-ujt_~:~~~r.-.<~~:----~;::;_-----~ ,-, ~ ~~--;::: ~:!-:_f.:: .-~-~ ~-~~ <
Sample Identification L 169027-08 I L 169027-09 I
Sample Description GP-8 10 FT GP-9 10 FT I
Sample Matrix SOIL SOIL I
Collection Option {for soil)* TerraCore TerraCore I
Date Collected 9/7/04 9/7/04
Date Received 9/9/04 9/9/04
Date Extracted 9/7/04 9/7/04
Date Analyzed 9/14/04 9/14/04
Dry Weight% 82.4% 81.3%
·-,-~---• ...._~ •••• -! -'='" -· " ~~~~~~Vii~~ rl'oi-l·j~ :~'7REfsult·::~ ~oi1@ ~?.{Re'Sulf~ i•; Dilution Factor -?--:Result~:'..:; ~f_!l.il!;' J><!= ... -·~-·.f-~ S<._-., --~~: ~r -~ . . --,or I -~,..-.. . . '• . ., -·~-"-· '
C5-C8 Aliphatics* in mg/kg <6.7 55 <8.8 72
C9-C12 Aliphatics* in mg/kg <6.7 55 <8.8 72
C9-C10 Aromatics* in mg/kg I <6.7 55 <8.8 72 I
Surrogate % Recovery-FID 108% 125% I
Surrogate % Recovery -PlD 106% 122%
• Option 1 ~Established ftl! line on vtal Optton 2=Sampling Oevtce {tndtcate brand, e.g. EnCore) Opl!on 3-Fteld wetght of sot I.
··Range results should exclude any surrogates, internal standards, or Target PAH analytes.
t:Cs.,ca~: ~-~·c-·· .. ,,. c9~c·1·iv~ ... _cs~c12il: ..... ·, ~"•' ;;~ -~"1"' •• T '• o' ~ .,~~ _,_ • .l:f-;;
AliPhatic • Alif!.h_at!c 1 ~~r~~~ti~., "#-~ ·"-""'' ~ --~····-Percent Recovery-Fortified Blank {Spike)-PID 85.6%
Relative Percent Difference-PID Duplicate 2
Percent Recovery-Fortified Blank {Spike)-FlO 120.5% 99.3%
Relative Percent Difference-FlO Duplicate 1.8 1.8
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~--:-·oi-l!'>i"
:,_.. • .. «
~0~-· ,,. ·--w:{ilf" .-... :~"',R~.su\t, }; :::Ll'.!l;·fi
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Attachment 2
VPH Laboratory Reporting Form
... , ...... -...... 1"~ ·~-...... ,~ 7:1'''\:""ll:-'\~~----'r· ....... ---~--·-· ·--~,---.... _,., ..• ,.. _______ ,_1.-----..,.--.., .......... ~~-_,,..?,!"' "''1"'"1''~ ... --~ -.... ..,., ···cr~-............ ,.-'~ r:~ ~-... ~--.t'·"<*· -~,!,,., •· •.. l. 4·-·:. ·. · .·, v•-'" :•·:~; ., · ··. Calibratioh: and. QAJQC .lriformati6n. :-;.../j~ · :-·.1: •. '1!~. -1/ .'<• .. >'\ ·' -,}''. • -·~:···1~, ...... ,,,:, fo,....;;... .;,,;:.__:::;r..l;e'.;.-. ,.. ___ ;...,_ .... :-< -~~ • • • ;.. ::;,.~ · .• -•. --· -~--___ .:.._ _..: .... ..: ••• • •• #•' ....:-~ --· _._~,_ ... !. ": . .,. ) .• , .,.;..,, -·· ,.,.._.~,
Initial Calibration Date 9/12/2004
Calibration Ranges and limits
'. ,,~111'. Rahg~_·_:, ·. " " ' ,, Ml ·. ,. " '• MDL . ' .... •· .. : . ' . .
C5-C8 Aliphatics 1.0062 mg/L 1.02 mg/L
C9-C12 Aliphatics 1.0032 mgll 1.01 mg/L
C9-C1 0 Aromatics 1.0011 mg/L 1.003 mg/L
NOTE: Please Include un1ts as appropnate
Method of Quantitation (Circle one)
Calibration Concentration levels
Average Response Factor
'F~:~~-R~~~~-~9::/'~~,, ·. ··:. ; r .. ~.· ·cev"els •,. : ·: ~\ .. • --. :,1. r,%RSD or.ccc. ' N.'< ~ ,. ,, • ._r, ,.,.,. . ' .. . . ~ . .
1.075 mg/L
C5-C8 1.375 mg/L Coef of Del (r"2)
Aliphatics 1.750 mgll 14.68
17.5 mg/L RSD
111.25 mg/L
1.055 mg/L
C9·C12 1.275 mgfl Coef of Del {r"2)
1.550 mg/L 10.50
Aliphatics
15.50 mg/L RSO
18.25 mg/L
1.010 mg/L
C9-C10 1.050 mg/L Coef of Del (r"2)
Aromatics 1.100 mgll 1.000
11.00 mg/L Linear Fit
11.50 mg/L
NOTE: Please md1cate un1ts as appropnate.
Calibration Check Date 9112/2004
'<..' I. . ; :.~"~ • • .. ..
1.1 mg/L
1.1 mg/L
1.1 mg/L
I Calibration
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' ~ ,•. . . . .. ,. _.. .-;_ ·t-·.:;.t ~a_nge:./ ~-: :,~ . · '·· ·,., • · ··, .• ·:;" · -, ... ·a ·f·_,,., . ,. :: •. ~ev~_l,(l.!), Mg/t) .· .. : -:~·, ,• . .R~[! (m.Y?) .. ··"·,A ACtUa·I-ValUe· (in Mg!LS
C5-C8 Aliphatics .75
C9-C12 Aliphatics .55
C9-C1 0 Aromatics .1 0
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
Coastal Environmental, Inc.
RAMS
NC
L 169027-01
·-... ' . . . . .
8.4 .816
5.8 .583
5.1 .095
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
------=====--------
VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: Coastal Environmental, Inc. Laboratory Name: Environmental Science Corporation
Project Name: RAMS NC Certification# {LAB) 375
Site Location: NC ---------------------
Sample Identification L 169027-04 L 169027-07
Sample Description GP-4 10FT GP-7 10FT
Sample Matrix SOIL I SOIL
Collection Option (for soil)* TerraCore I TerraCore
Date Collected 9/7/04 I 9/7/04
Date Received 9/9/04 9/9/04
Date Extracted 9/7/04 I 9/7/04
Date Analyzed 9/14/04 9/14/04
Dry Weight% 80.5% 81.1%
Dilution Factor
CS-CB Aliphatics* in mg/kg 1 s.B 37 79 79 1 1
C9-C12 Aliphatics* in mg/kg 11 I 37 58 79
C9-C1 0 Aromatics* in mg/kg 7.2 37 25 791
Surrogate% Recovery -FID 125% 162%
Surrogate % Recovery-PID I 129% 162%
* Opt1on 1-Estab!ished f1llllne on v1al Opt1on 2-Samplmg Dev1ce (1nd1cate brand, e.g. EnCore) Opt1on 3-Fie\d we1ght of so1\.
**Range results should exclude any surrogates, internal standards, or Target PAH analytes.
<cs'cs ~I[ cs:Ci2· ·cg-e1o •• ~o:ii~li~tiC: AiiP.hat!c ·Aromatic~ •"'-'"i '-.~·· ..... ~ ...... .t._; •• .,..~ ' .. ~, .. ;_~
Percent Recovery-Fortified Blank (Spike)~ PID 98.9%
Relative Percent Difference~ PID Duplicate 1 .1
Percent Recovery-Fortified Blank (Spike)-FlO 97.9% 95.9%
Relative Percent Difference-FlO Duplicate 0.2 0.3 I
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Attachment 2
VPH Laboratory Reporting Form
·~...-·-1·--·~,.,-'"':!I•~ ,. ·~·~ ,-... ---·----~--~~ .. ----.·-=------.~•""''."'"""'lr.r.:-'r.'l;--,-~-,-.,..,...j, ~~ft:'~~~'!l":-·-ry l,i:tf'i"~-:';~ri}'f(l:r ;~:t'· -rl't":~:•:N(.[JH_-f'·.·li'.<M'!.:~~-:;i;, ;;··/-r;C81ibra_tion;andr0AJ_QC·Inforinat_ionl~ •· J;~\3::-~.J.~;•·:~~~~~t: ,:<.i/.''5"~): :~·'-j·~:~?tt, . :'''rl'·~-· i .:0.-~-~-\..:.o:.:->.. .• ,>l!...i-.... w. .•.. ,,_ "'··""---· ,_,_..,_, . __ ....... _ •. ~..!~.L.._....__,____.).I;. ··-l::it-----1..-___ .._ ___ -.__j_,\_ •• ,.~
Initial Calibration Date 9/14/2004
Calibration Ranges and Limits
~~,. _f:._-~·-J~-~-~9-e ~:--.. :-·. -~-., -' -. .,. "' . Mt,: -· " . '>' ... i'-:R[' ., .,¥ n.>:l '" .. :l.'t: •. ·.JI:I1Dl·, .. ·: ... ,_1 ~-•• -~--1' '· '•· ... '• ·'·. . __ ., ! .,;· •,'\ ..;.:,_ __ .. ,._,' t~ ·""->-·
C5-C8 Aliphatics 1.0062 mg/L 1.02 mg/L 1 . 1 mg/L
C9-C12 Aliphatics 1.0032 mg/L 1.01 mg/L 1 .1 mg/L
C9-C10 Aromatics 1.0011 mg/L 1.003 mg/L 1 .1 mg/L
NOTE: Please include umts as appropnate
Method of Ouantitation (Circle one)
Calibration Concentration Levels
Average Response Factor
i' ,, "'R""' "w.·:o· ,. ..... . .;·• ·; .. " . . .. ' •;··' •, •· ange • . , ~ ~-i· ·, L:.evets'• ·,·:--.... : ~-.
' ,)1-"'"'' ~ .•• .. ...... .. .•.• _...__ . ~ :t . -··
1.075 mg/L
C5-C8 1.375 mg/L
Aliphatics 1.750 mg/L
17.5 mg/L
111.25mg/L
1.055 mg/L
C9-C12 1.275 mg/L
Aliphatics 1.550 mg/L
15.50 mg/L
18.25 mg/L
1.010 mg/L
C9-C10 1.050 mg/L
Aromatics 1.100 mg/L
11.00 mg/L
11.50 mg/L
NOTE: Please 1nd1cate umts as appropnate.
Calibration Check Date
Calibration
8/24/2004
• ,. • ~-, • l'
.. -·%RSD or CCC . ... -
Coef of Del (r~'~2)
17.81
RSD
Coef of Del (r~'~2)
9.64
RSD
Coef of Del (r~'~2)
14.41
RSD
/ ,}'~·:;.: RanQe\ ··~ ,.; ·; ." ·;:,,.'_leVel'(ii"l•MQ!\2)""~:~.-:: ~ ... L~:R.P~D·(frl',o}o)',,;: l.f:"o: AChiiil VaiUfd"in ~·fQ/L)" ........ _,...,._____ ··-· .-. n.. .. , . "''"'·-"-~---~ -~------·' .. ~ ...... :~\ "'""""•'•···----t ... l .....
C5-C8 Aliphatics .75 3 .728
C9-C12 Atiphatics .55 3.5 .531
C9-C10 Aromatics .1 0
MDL= Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
Coastal Environmental, Inc.
RAM 5
NC
L 169027-04
6.2 .094
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
-=~--~~~-"""'":'--:-_"'=~-"""'":''__"'":'~-TA;;:;~';,~;:;:;;;;;;<,;~~'_--"~'!_-11=~A~o~o~i;~/~o~ta~I~OO~I~1P~IO~o~O~N@o~tiv~o===~I!"'!!!_--'!"'!!!'!._~C~ho~1-~-;ifCC~•-~I'"~-~-"!_l'-• Alternate billing information: ".... ~~ .........
.. Coasial Environ.mental, Inc. -·.1 [I I I [ ""-''-
857 West Main Street '
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Murfreesboro,NC 27855 1 Prepared by:
I I • Ei\'VIROi\':\IE~TAL
Report to:
rojec:
escnpt1on:
Email'
:'\lr. :\lark Hafenmaicr
RA.M 5
mhafenm@coastalcnvironmc
;City/State
otlected
J: 'il ~ "' 1-----~-------r.c~,,~oo~I~P~ro~,oc~l~,~, ---'-----+~,~.,"p~,~,,~oc"<"# _____ ----+ 0
hone: [phone] C/0
k~~X~·~(~l~5;2)~3;9~8=4:7~G:8 ____ -h0~1;-1~0~5~~-----~~C~u~-~A~E~,~-\~''~I~'~C~-~O~I!~0~5---+ 0
ollected by (print): ile!Facillly ID#: _ P.O # -'2::
f----------+===;---:-c-==--:c_J,-:--;---c---:---:---c-c--.--+ ~ p,1~ 1"";::, o!: Lob MUST BeN::~) D'" Re;"h' ~eodedoo ;o
J~ _NextDsy.. . .... 100% X (J
, "'"" '"% Email? _No _Yes No. > ~ 1 , l>,;ru=J><.X_.,._ _____ J=::..:_Tw:o~O~e~,~--~-~--~-~--~-~--~-~--~-~--~-='_--t.JF~'~"2-~N~'"--"'"---+ f~ackedon ·:\ · /"o.A ~ YH of • c
Cntrs ~ ~
" 1'2 Sample 10 Depth Date Time
•Matrix: SS-Soil GW-Groundwater WW-WasteWater DW-Drinkmg Water OT-Othe11 ___ _
Remarks:
Rece1ved by: (Sognature)
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12065 Lebanon Road
Mt. Juliet, Th' 37122
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I Phone [phone] -I FAX [phone] -, I :1
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CoCode: COAENYMN(Iab use only)
TemplateJPrelogin T252l9' P121350
GOOd~ 75/2:"1-
Shipped v,a·._,.. f;dEX Ground
Remar1<sJContaminant Sample II {lab only)
pH -------Temp
Flow Other
Condition: (lab use only)
p Checked: _NCF:
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• ENVIRONMENTAL
SciENCE CoRP.
12065 Lebanon Rd.
Mt. Jullet, TN 17122
[phone]
1-800-767-5859
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 Weot Main Street
Murfreesboro, NC 27855
Date Received Sept:ember 09. 2004
Description RAM 5
Sample ID GP-10 10 IT
Collected By
Collection Date 09/07/04 14:15
Parameter
Total Solids
Volatile Petroleum Hydrocarbons
CS-CB Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2,s:oibromotoluene(FID)
2,5-Dibromotoluene(PID)
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-8utylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry Result
81.0
BDL
BDL
BDL
BDL
98.0
98.0
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantitation Limit(EQL}
Det. Limit
9.6
9.6
9. 6
9. 6
0.031
0.062
0. 012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0. 0012
0. 0012
0.0012
0.0012
0. 062
0.0062
0.0012
0. 0012
0. 0012
0.0025
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
Fax [phone]
Tax l.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample • ' Ll69049-01
Site ID
Project • • 01-105
Units Method Date
• 2540G 09/16/04
mg/kg MAD6PV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
mg/kg MADEPV 09/14/04
' Rec. MADEPV 09/14/04
' Rec. MADEPV 09/14/04
mg/kg 82608 09/17/04
mg/kg 82608 09/17/04
lll3/kg 82608 09/17/04
lll3lkg 82608 09/17/04
lll3/kg 82608 09/17/04
lll3/kg 92608 09/17/04
lll3/kg 82608 09/17/04
11'9/kg 82608 09/17/04
mg/kg 92608 09/17/04
mg/kg 82608 09/17/04
mg/kg 82608 09/17/04
lll3/kg 82608 09/17/04
lll3/kg 82608 09/17/04
1f9/kg 82608 09/17/04
1f9/kg 82608 09/17/04
rrg/kg 92608 09/17/04
1J9/kg 82608 09/17/04
mg/kg 82608 09/17/04
mg/kg 92608 09/17/04
mg/kg 82608 09/17/04
1f9/kg 82608 09/17/04
mg/kg 82603 09/17/04
11'9/kg 82608 09/17/04
1f9/kg 82608 09/17/04
lll3/kg 82608 09/17/04
lll3/kg 82608 09/17/04
11'9/kg 82608 09/17/04
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA
KY-90010, KYUST -0016, NC-ENV37S,DW21704, ND -R-140, SC-£14004, TN-
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA -00109, WV
Thio report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 1 of 16
Di 1.
1
" " " "
1
1
1
1
1
1
1
1
1
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1
1
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• ENVIRONMENTAL
SciENCE CoRP.
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, [nc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-10 10 FT
09/07/04 H:lS
Parnmeter Dry Result
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-l,2~Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropyl benzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
N<J.phthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluo:romeLhane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
R<~Sults listed are dry weight basis.
BDL -Below Detection J,imit
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Qunntitation Limit(EQL)
Det. Limit
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 012
0.0062
0.012
0.0012
0.0062
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0062
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0037
Units
rn;:~/kg
rn;:J/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
mg/kg
rrg/kg
mg/kg
rrg/kg
rrg/kg
rn;:~/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rn;:~/kg
rro/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
Laboratory Certification Numbers:
12065 Lebanon Rd.
Mt. Juliet. TN 37122
(615) ?58-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample II
Site ID
Project II :
Method
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
Ll69049-01
01-105
Date Dil.
09/17/04 l
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 l
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 l
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
09/17/04 1
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY-90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV-2)3
MN -047-999-395, f:N -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Page 2 of 16
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ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
{615) 759-5858
1-800-767-5859
Mr. Mark Hafenmaier
Coastal Environmental, rnc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Date
Parameter
Surrogate Recovery
Toluene-dB
GP-10 10 FT
09/07/04 14:15
Dibromofluoromethane
4-Brornofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Result Det. Limit
"' 100 ".
Det. Limit -Estimated Quantitation Limit(EQL)
Fax [phone]
Tax I .D. 62-0814289
Eat. 1970
September 17,2004
ESC Sample # : Ll69049-01
Site ID
Project # 01-105
Units Method Date
' Rec. 8260B 09/17/04
' Rec. 82608 09/17/04
' Rec. 8260B 09/17/04
Ji ny Hunt, ESC Re resentative
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-Pll-0197, FL-E87487, GA
KY-90010, KYUST-0016, NC -ENV375,DW21704, ND-R-140, SC-84004, TN-
MN -047-999-395, NY -11742
Note:
-923, IN -C-TN-01
2006, VA -00109, WV
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:16 Printed: 09/17/04 15:16
Page 3 of 16
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• ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
l-800-767-5859
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-11 10 FT
09/07/04 15:00
REPORT OF ANALYSIS
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 17,2004
ESC Sample # L169049-02
Site ID
Project # : 01-105
Parameter Dry Result Det. Limit Units Method Date Dil.
Total Solids 84.2 ' 2540G 09/16/04 1
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
Surrogate Recovery
2, 5-Dibromotoluene (FID)
2,5-Dibromotoluene(PID}
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
8romodichloromethane
Bromoform
8romomethane
n-Butylbenzene
sec-8utylbenzene
tert-8utylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluenc
4-Chlorotoluenc
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
BDL
BDL
BDL
BDL
144.
142.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
<.4
4.4
4. 4
4.4
0. 030
0.059
0.012
0. 0012
0.0012
0.0012
0.0012
0. 0012
0. 0012
0.0012
0. 0012
0.0012
0. 0012
0. 0012
0.0012
0.059
0.0059
0.0012
0. 0012
0.0012
0.0024
0.0012
0. 0012
0. 0012
0. 0012
0.0012
0.0012
rrg/kg
rrg/kg
rrg/kg
rrg/kg
% Rec.
% Rec.
mg/kg
rrg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
ug/kg
mg/kg
rrg/kg
mg/kg
"'J/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
m.:~/kg
mg/kg
rrg/kg
mg/kg
m.:~/kg
mg/kg
Det. Limit -Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
MADEPV
MADEPV
MADEPV
MADEPV
MADEPV
MADEPV
82608
82608
82608
82608
82608
82608
8260!l
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260!l
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
09/16/04
09/16/04
09/16/04
09/16/04
09/16/04
09/16/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
AIHA-100789, AL-40660, CA-I-2327, cr-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY -90010, KYUST -0016, NC -EW/375, DW21704, ND -R-140, SC -84004, TN -2006, VA -00109, WV
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Ll69049-02 (VPH} -Previous run also had high SURR recovery. Matrix effect.
Page 4 of 16
37.5
37.5
37.5
37.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
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ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
REPORT OF ANALYSIS
Mr. Mark Hafenmaier
Coastal Environmental, J.nc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
SepLember 09, 2004
RAM 5
GP-11 10 FT
09/07/04 15:00
Parameter Dry Result
1,1-Dich1oroethane
1,2-Dichloroethane
1,1-Dichloroethene
cio-1,2-Dichloroethene
trans-1, 2-Dichloroetho~ne
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexach1orobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Results listed are dry weight basis.
BDL -Below Detection t,imit
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Det. Limit -Estimated Quantitation Limit(EQL)
Det. Limit
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.0012
0.012
0. 0059
0.012
0.0012
0.0059
0.0012
0.0012
0.0012
0.0012
0.0012
0.0059
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0. 0012
0.0012
0.0012
0.0012
0.0036
fax {615) 758-5859
Tax l.D. 62-0914289
Est. 1970
September 17,2004
ESC Sample II L169049-02
Site ID
Project II 01-105
Units Method Date
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
rrg/kg
mg/kg
rrg/kg
mg/kg
mg/kg
rrg/kg
mg/kg
rrg/kg
IT13/kg
mg/kg
mg/kg
mg/kg
mg/kg
IT13/kg
rrg/kg
rrg/kg
rrg/kg
fll3/kg
fll3/kg
mg/kg
rn:J/kg
fll3/kg
1!¥3/kg
mg/kg
mg/kg
mg/kg
8260B
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
8260B
8260B
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
O'J/17/04
09/17/04
09/17/04
09/17/04
09/17/04
09/17/04
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY-90010, KYUST-0016, NC-ErN375,DW21704, ND -R-140, SC-84004, TN-2006, VA-00109, WI!
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
L169049-02 (VPH) -Previous run also had high SURR recovery. Matrix effect.
Page 5 of 16
Dil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
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• ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd,
Mt. Juliet, TN 37122
[phone]
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Date
Parameter
Surrogate Recovery
Toluene-dB
GP-11 10 IT
09/07/04 15:00
Dibromofluoromethane
4-Bromofluorobenzene
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Result Det. Limit
"' 110
99.
Det. Limit -Estimated Quantitation Limit{EQL)
l-B00-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est_ 1970
September 17,2004
ESC Sample # Ll69049-02
Site ID
Project II : 01-105
Units Method Date
• Rec . 82608 09/17/04 • Rec. 82608 09/17/04 • Rec . 82608 09/17/04
J y Hunt ESC Representative
Laboratory Certification Numbers:
AIHA-100789, AL-40660, CA-1-2327, cr-PH-0197, FL-E87487, GA-923, IN-C-TN-01
Oil.
1
1
1
KY-90010, KYUST-0016, NC-ENV375,DW21704, ND-R-140, SC-84004, TN -2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:16 Printed: 09/17/04 15:16
L169049-02 (VPH) -Previous run also had high SURR recovery. Matrix effect.
Page 6 of 16
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• ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Mr. Mnrk Hafenmaier
Coaotal Environmental, lnc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
Sample ID
Collected By
Collection Date
September 09, 2004
RAM 5
GP-12 10 FT
09/07/04 15:45
REPORT OF ANALYSIS
Parameter Dry Result Det. Limit
Total Solids
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
81.6
BDL
BDL
BDL
BDL
5.0
5. 0
5. 0
5.0
Units
•
!f9/kg
rrg/kg
rrg/kg
mg/kg
Fax [phone]
Tax 1.0. 62-0814289
Est. 1970
September 17,2004
ESC Sample ' L169049-03
Site ID
Project ' 01-105
Method Date
2540G 09/16/04
MADEPV 09/16/04
MADEPV 09/16/04
MADEPV 09/16/04
MADEPV 09/16/04
Surrogate Recovery
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
144.
14q. • Rec. MADEPV 09/16/04
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
q-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
Results listed are dry weight basis.
BDL -Below Detection Limit
0.036
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.031
0. 061
0.012
0.0012
0.0012
0. 0012
0. 0012
0.0012
0.0012
0.0012
0.0012
0.0012
0. 0012
0.0012
0.0012
0.061
0. 0061
0. 0012
0.0012
0.0012
0. 0024
0. 0012
0. 0012
0.0012
0.0012
0.0012
0.0012
• Rec.
mg/kg
mg/kg
ID3/kg
rrg/kg
mg/kg
mg/kg
11"9/kg
rrg/kg
1!'9/kg
mg/kg
mg/kg
rrg/kg
!f9/kg
rrg/kg
rrg/kg
m:;J/kg
mg/kg
mg/kg
rrg/kg
rrg/kg
rrg/kg
mg/kg
mg/kg
ff9/kg
mg/kg
mg/kg
rrg/kg
Dct. Limit -Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
MADEPV 09/16/04
82608 09/17/04
82608 09/17/04
62608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
62608 09/17/04
62608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82GOB 09/17/04
82608 09/17/04
82608 09/17/04
62608 09/17/04
82608 09/17/04
82608 09/17/04
AIHA-100789, AL-40660, CA-I-2327, cr-PH-0197, FL-E87487, GA-923, IN-C-TN-01
KY-90010, KYUST 0016, NC-ENV375,DW21704, NO-R-140, SC-84004, TN-2006, VA-00109, WV
MN -047-999-395, NY -117q2
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
L169049-03 (VPH) -Previous run also had high SURR recovery. Matrix effect.
Page 7 of 16
Dil.
1
40.5
40.5
40.5
qo.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
-233
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12065 Lebanon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Mt. Juliet, TN 37122
(615) ?56-5858
1-800-?6?-5859
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
GP-12 10 FT Sample ID
Collected By
Collection Dilte 09/07/04 15:45
Parameter
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di-isopropyl ether
Ethyl benzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-8utanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MI8K)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrach1oroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenea, Total
Results listed are dry weight basis.
BDL -Below Detection Limit
Dry
REPORT OF ANALYSIS
Result Det. Limit
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0. 0012
BDL 0. 0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0. 0012
BDL 0.0012
BDL 0. 0012
BDL 0.012
BDL 0.0061
BDL 0.012
0.036 0.0012
BDL 0.0061
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0061
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0012
BDL 0.0037
Det. Limit -Estimated Quantitation Limit(EQL)
Units
mg/kg
rrg/kg
mg/kg
rrg/kg
rrrg/kg
mg/kg
mg/kg
mg/kg
rrg/kg
ID3/kg
11J3/kg
11J3/kg
ID3/kg
11J3/kg
rrg/kg
11J3/kg
rrg/kg
rrg/kg
rrg/kg
rrg/kg
11J3/kg
ID3/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
lf"9/kg
mg/kg
mg/kg
Laboratory Certification Numbers:
Fax [phone]
Tax I .D. 62-0914289
Est 19?0
September 17,2004
ESC Sample # L169049-03
Site ID
Project II : 01-105
Method Date
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04.
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
82608 09/17/04.
82608 09/17/04
82608 09/17/04
AIHA -100789, AL -4.0660, CA -I-2327, Cf-PH-0197, FL -E87487, GA -923, IN -C-TN-01
Oil.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
KY -90010, KYUST 0016, NC -ENV375, DW21704, ND -R-140, SC -84004., TN -2006, VA -00109, WV -233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Ll69049-03 (VPH) -Previous run also had high SURR recovery. Mat.rix effect.
Page B of 16
I
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12065 Lebanon Rd.
ENVIRONMENTAL
SCIENCE CORP.
Mt. Juliet, TN' 37122
[phone]
1-800-767-5859
Mr. Mark Hafenmaier
Coastal Environmental, Inc.
857 West Main Street
Murfreesboro, NC 27855
Date Received
Description
September 09, 2004
RAM 5
Sample ID
Collected By
Collection Date
Parameter
Surrogate Recovery
Toluene-dB
GP-12 10 FT
09/07/04 15:45
Oibromofluoromethane
4-Bromofluorobenzene
Dry
REPORT OF ANALYSIS
Result Det. Limit
100
100
99.
Fax (615) 7SB-S859
Tax I .D. 62 0814289
Est. 1970
September 17,2004
ESC Sample # ' Ll69049-03
Site ID
Project # ' 01-105
Units Method Date
' Rec. 82608 09/17/04
' Rec. 82608 09/17/04
' Rec. 82608 09/17/04
------~Jcicd~y~H~u~n~c~.f-~E~C Re resentative
Results listed are dry weight basis.
BDL -Below Detection Limit
Det. Limit -Estimated Quantitation Limit(EQL)
Labor~tory Certificat1on Numbers:
AIHA-100789, AL-40660, CA-I-2327, CT-PH-0197, FL-E87487, GA-923, IN-C-TN-01
Dil.
1
1
1
KY -90010, KYUST-0016, NC-ENV37S,DW21704, ND-R-140, SC-84004, TN-2006, VA-00109, WV-233
MN -047-999-395, NY -11742
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 09/17/04 15:16 Printed: 09/17/04 15:16
Ll69049-03 {VPH) -Pre·•ious run also had high SURR recovery. Matrix effect.
Page 9 of 16
I
I Sample II
I Ll69049-01
I Ll69049-02
I
L169049-03
I
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Attachment A
List of Analytes with QC Qualifiers
Analyte
Volatile Petroleum Hydrocarbons
cs-ca Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
1,2,4-Trimethylbenzene
Volatile Petroleum Hydrocarbons
CS-CB Aliphatics
C9-Cl2 Aliphatics
C9-C10 Aromatics
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
1,2,4-Trimethylbenzene
Volatile Petroleum Hydrocarbons
CS-CB Aliphatics
C9-Cl2 Aliphatics
C9-Cl0 Aromatics
2,5-Dibromotoluene(FID)
2,5-Dibromotoluene(PID)
1,2,4-Trimethylbenzene
Qualifier
0
0
0
0
J4
0
0
0
0
Jl
Jl
J4
0
0
0
0
Jl
Jl
J4
Page 10 of 16
I
I
g
D
0
0
I
I
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I
I
Qualifier
Jl
J4
0
Attachment B
Explanation of QC Qualifier Codes
Meaning
Surrogate recovery limits have been exceeded; values are outside upper
control limits
The associated batch QC was outside the established quality control range
for accuracy.
(ESC) Sample diluted due to matrix interferences that impaired the ~bility
to make an accurate analytical determination. The detection limit ~s
elevated in order to reflect the necessary dilution.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods, it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected)
Definitions
Accuracy -The relationship of the observed value of a known sample to the
Precision
Surrogate -
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc,
The agreemen~ between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Organic compounds that are similar in chemical composition, extraction,
and chromatography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically relat.~d to the surrogate compound. SurrogateG are added to the
sample and carried through all stages of preparation and analyses.
Control Limits (AQ)
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
31-119
12-134
5l-l41
Nitrobenzene-dS 43-118 Dibromfluoromethane 79-126
2-Fluorobiphenyl 45-128 Toluene-de 81-114
Terphenyl-d14 43-137 4-Bromofluorobenzene 65-129
TIC Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
(SS)
83-119
82-116
72-126
Page 11 of 16
I
ENVIRONMENTl'.L
SciENCE CoRP.
I Coastal Environmental,
Mr. Mark Hafenmaier
11 as7 West Main Street
IIMurfreesboro, NC 27855
lnalyte
I
Inc.
Quality Assurance Report
Level I I
Ll69049
::~:~:~(Labor a t'or·y J B liiflkSi Result .. · · ----Unit's.-------Date Analyzed
12065 Lebanon Rd.
Mt. Juliet, TN 37122
{615) 758-5858
1-800-767-5859
Fax [phone]
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
Batch
'09/16/04 }21'": 09.:.< CWG171054-: ,,,-x----------
Page 12 of 16
I ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN J7122
[phone]
1-800-767-5859
Fax [phone]
~Coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street I Murfreesboro, NC 27855
Inc.
~~;·~-~~~::!1~1~~!~~~~~~~~~~::::::-
H
Tr i ChToro f 1 uorome t'ha ile N\W?bei
Vinyl· chl'ci'ride-
lenee, Total
Tax I .D. 62-0814289
Quality Assurance Report
Level II
Est. 1970
September 17, 2004
L169049
:,-}J,;;J._J:;p:ra:1:.o"r;r B1'<3,nk%)
Result Un1ts Date Analyzed Batch
<\:J\W&i.K < , . o o 1
< . 001
H :gnr,'rm:xr:< · o a 1
_ .,: .001
< . 001
< . 003
Units
mg/ k~ii!::L-'o/ o 9/1"6 I o ··f(:2 a··:o at%+\WGl-71.13 9{/} _
mg/kg 09/16/04 20;08 WG171139
mg/kg 09/16/04 20:08 WG171139
: ''.'',~i:":"/~',~·,:·,:·,:',":"/'\. mg /kg It:fit£ o 9/ f 6/ o 4 ·-::· 2 0 :· 0 8,\. :\i\. WG 1 7113 9 _ ....... mg/kg ______ "o9/i6/04 2o:"oe" ··wG171139
m /k 09/16/04 20:08 WG171139
M·oU-pliCate '~h~~:
Result Duplicate RPD Limit Ref Samp Batch
t:,::;E_ a 2J.sp:::-· _ 81J.Otf"fE't;"'=; 1 ~:-_a 6 __ @[ 20Jfldt: :::.:I Ll6 904 9_,:;=;oi"r_:wG1 710 54:
77.6 76.8 0.972 20 L169189-02 WG171054
;;, •.. LabO:i:-atory_lCOnt'rOF s3ii_i.Ple-
Units Known Val Result % Rec Limit Batch
Page 13 of 16
I • ENVIRONMENTAL
SCIENCE CORP.
g Coastal Environmental,
Mr. Mark Hafenmaier
857 West Main Street
IIMurfreesboro, NC 27855
is-1,3-Dichloro ro ene
Inc.
l i"::''fSOPl-OPYl :~-'ether --··'''' ]@"@:':::::.::,· ,,, -,.-, ...... ibromometharie ._,,_, . -~~::::-:-:-·-·
ichlorodifluoromethane
EthY..~be)?-:~-~f!._e;'--~1-WM%:~~,
Hexachlorobutadiene
l~:jop~opy}l:Jer;bz.ene1 ... ethe<'•••••••••<HH"H''''"'"'"'"'""'' ethylt':.tert~ uty '-
1ethylene Chloride n-Butylbenzene
Quality Assurance Report
Level II
L169049
.02 0.0215
Labor at oi'y ·-con t ro1_: SIJ._triP le)?{
Units Known Val Result
12065 Lebanon Rd.
MC. Juliet, TN 37122
[phone]
1-8 00-767-5859
Fax [phone]
Tax I .D. 62-0814289
Est. 1970
September 17, 2004
108. 81-150 WG171139
%-Rec Limit Batch
::{'':f~'i~~-/~ ~~~<~~~~~y:::g~ wr g~g::nt& ~:~~~:~:\:.:, i g~ : ':; -:~t ii {:'~' ···:y~~gi~i i'~
mg/kg .02 0.0193 96.6 17-134 WG171139
_':rng/kgJM:--~_02t% Jijjj_}_j_Jjif0!_0206f~d!_J,03~Wt' A 63:::-133---WG171139ifffi
mg/kg . 02 o. 0181 90.3 53·:::-f48" WG171139
mg/kg~_,,, . 02 0. 0185 92.3 63-120 WG171139 mg/kg;,;-~,. :'·:';'~':o2@? .:,;··o···;:-0219 .·. 09_ 64 -'142, .:.:,::\WG1 71139)$%
mg/kg .02 0.0215 107. 70_:141 ___ WG171139
mg/kg .02 0.0199 .99.6 58-161 WG171139
~~:i.~~~~~!~r:::::ge . ¥tWfiK.;2£ · ___ IIIII?:::_~~~~~-g-~x:----~g~.g~~~Jfu' ifi:i-i-6:':3· ~~=i~~Dm~gi~ig~: 3
Q; ec ~ But y lben z ene wH::~~~~~:~:):
Styrene
, __ -_ : Ai \.:::·_.:,;:;;a~~~~~ .: g ~ .. ::~1\tgt g i-~ ;.®4:': ~~ :.~ ~~,~~~~~~~:+t~!:;g~-~:J~~%i:gi ~i:i ~ ~)/'
mg/kg .02 0.0181 90.·6 64-128 WG171139
umg~;:J:::::::!:thene
tiii Oii ~ l''i'-3 :.;:· oi'Ch 1 Oropropeiie:tiili-::~
mg/kg .02 0.0183 91.4 65-127 WG171139
-"'tttf)( '>'(r:lg/kg,,_,:,,, ______ .:o2~_0'?0189 f!i:, __ ·:·c::;:t)9.4't!5.Wfft5B:i137" "WG171139> --J:~;
mg/kg .02 0.0214 107. 75-125 . WGlill39-·
mg/kg .02 0.0224 112. 79-152 WG171139
mg/kgJ;IiJF"-:~o2tl? .... )··· ·::.o .-0190 ,._.;:::,:::::/::::[@[95·~2l':\t':'"' 65 -:1so .... WGl 71139}:': ':::%
~~richloroethene :r; ic h_l_oro f_ll!-orome thane
J,nyJJc:J:;_lor_lde ___ .. "'"~-0---
ylenes, Total
mgjkg .02 0.0219 109. 75-145 WG171139
mg/kg .02 0.0188 93.9 30-130 WG171139
,, __ ,: ___ ::t{i},Lmg/kg_>xtffi!_02k--o:':''0207,::t.··· <:"':_"#f_1_04:'::--~ 39~1275i.#WG171139f.'"$
mg:/kg .06 0.0628 105. 64-129 WG171139
LabOr at o'i)'){c6'ri t rOF sauip l'Ed niip n cat e :;:-( ·
Units LCSD Res Ref Res RPD Limit %Rec Batch
-~~~~J ~~~:~\:t::-gi~: ::::::::.::_ g-: gi-~-~ilitrr-~~il# ~,~ ~,,,.,, , .. ,,.,,.,,,, ~~---::· ~--~gi ~ i i~ ~ ):_, __ ,:: _;,::-..... t
:~&Wf.Jt<:/~ ~ ~~ ;~ ::tt. g :-: g i·: ~ J%,:;;, _g :0 g i· ~ ~)}}:: ~ :(:: ~ ~ ~~T:_ -i-! I t_\J~ ~.! i ~ JW:® ~g i ,~ i g ;_._,%_:-'A:
mg/kg 0.0207 0.0204 1.32 21 103. WG171139
mg/kg 0. 0223 0. 0235 5. 28 20 112. WG171139
.. _mg/kgij_£~o:::o21 7,:·:: Xo'!'_o222, .· .... , 2 .19)@20': ~FWJ10~_-;'-· __ : IfJ_WG171!~~)N( ,.;,,{(,;,;,;;,;,;,.,;;,;,.,;,;
mg/kg 0.0199 0.0183 8.33 25 99.4 WG17113
mg/kg 0.0177 0.0191 7.60 23 88.6 WG171139 _-,:, ----,:-iilg I kg ::::::::f:ii o '::'" o 1 1 1 ~ ---o . o 1 9 o ;-,J'-.',7 ~ 2 5 -~ -:~., 2 2 n~.m~ a 8 :'· 4 -,,---:-::wm-7113 9 _.:: -:::-:':'I'i'fdf1% --mg/kg ........ ·.····o· •. o13·o o. 0138-... 6 .. 01 .. 22 __ ........ ,64. a WG171139
mg/kg ....... ·.··· 0_~0191 ... 0. 0185 4. 70 24 97.0 WG171139
·iJ!Ig/kg·· ·o:::ots.7,~,~-.::::. o:~.o19o __ 1.7 ~5.. ..wGl-71139
mg/kg 0.0179 0.0177 1.29 22 .7 WG171139
mg/kg 0.0200 0.0206 3.05 23 100. WG171139
-.-rilg/kg{}:-0. 020 0'; 0202·0~_54.4\: 22____ 101 .~_~--.·WG1-71139':'':{Y%tf09
mgjkg 0.0170 0.0183 7.54 20 84.9 WG171139
mg/kg 0. 0186 0. 0204 9.12 22 93.1 WG171139
iiig/kg/'':·:' 'O·~··o2o 0 _;0196:;:,<tiX~'52 100.': :-'-WG171139
mgjkg-o.·o20 0.0205 -----1--:92 2 101. WG171139
mg/kg 0. 0214 0. 0220 2. 67 17 107. WG171139
;:ji:&T;,-:1W£irrg-jkg 0 ":' 112]tNff O'? 10:4 ~'~:-';·70 m:.._::_:2B%t1ill112%#f$ WG17l-l-3 g·:--''P-"-'0
mg/kg 0.0998 0.101 .26 25 99.8 WG171139
mg/kg 0.0188 0.0208 9.98 28 94.2 WG171139
~9 /kg:.:-::··:-·:·:o.~'O 1'70 0 . 018 4':::.. a·. 3l'':~~:t)~:;-D£Mtl8_4":' 8-.. .:~\~,_.WG1 7113 9
mg/kg 0.128 0.108 17.0 29 128. WG171139
mg/kg 0.0978 0.111 12.7 23 97.8 WG171139 . it ""N"! ~&Wfj ";ing/kg --'-o_,:-276't:tt o~Jl'9)if:{14 ·.·3 20/tif@27,16:"t·¥KI-l"G171139]}lUWfWili.f:i
mg/kg 0.100 0.103 2. 07 19 100. WG171139
mg/kg 0. 0205 o. 0196 4. 39 20 102. WG171139
mg /kg ,., .... , 0 >: 0 1'.9 7 (},\ ... 0. ~ 0 21 B} ~. 1 0 .-1 :· :·.:::::~~~~~~~~:~'3 o~~~H/(\\ 9 B.'~).:.,;,· .. -,:,::i} WG 1,7 113 9-, '""'""'"'Lkl\<
mg/kg 0.0208 0.0219 5.20 22 104. WG171139 ....
Page 14 of 16
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ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. chtliet, TN J7122
(615) 758-SBSB
1-800-767-5859
Fax (615} 758-5859
~Coastal Environmental,
Mr. Mark Hafenmaier
Inc.
T<IX I .D. 62-0814289
Est. 1970
II 857 West Main Street Quality Assurance Report
Level I I
(IMurfreesboro, NC 27855
Ll69049
September 17, 2004
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romoform m /k 0.0174 0.0197 12.4 17 87 .1 WG171139
§LabO:ratorYJCcmt.rC)l __ Sample~ Duplicate
Units LCSD Res Ref Res RPO Limit %Rec Batch
_::/t/JJ\iliJFri9/kg -::·, o .. _o usn:., o . o 12 7)@io<·2 -o\ 11 .) ,,.:;:~:~:~~~: s 7:''f.4 · .. ;::;:;.wG1 71-13 93:\ )))@@[
mg/kg 0.0202 0.0218 7.82 23 101. WG171139
mg/kg 0.0186 0.0199 7.12 25 92.8 WG171139
'i•cfti t .td!J't '5%.~~~~ g::.g~}~i 2 :·'g~:ittit{-~~ ;~-:-WJtJ~~?-'~--::::' .. ~gi ~ii~~-·)\'.\V''-Y @Hi
mg/kg 0.0216 0.0212 1.92 22 108. WG171139
.J)T&Wf:: ffig/kg_&0;:'0228:.. o_·: 024 -;·a 20]%\~~l'{;-1-1'4 · .. ·_-"_';:WG171139 mftffft;;·,,:::::::-:::
mg/kg 0.0208 0.0206 1.35 22 104. WG171139
mg/kg 0.0241 0.0215 11.2 28 120. WG171139 mg/kgt@to~'-0206 (.\:' :o.~'0_20_4t/:::'/ o ._e3o: -,:_23~:~::::-.,·. :103. ·':@WG17H39????>•wiN.
mg/kg 0. 0202 0. 0204 0. 640 29 101. WGi71139
mg/kg 0.0180 0.0193 6.80 21 90.2 WG171139
--':-:.;~{::fff'Q;;L. __ ---:-'::fing/kg· o':-0192-0'?'0206:: ~7_. 08[@22:: --96';--L:, .-lWG1 71-1-39l: ":~_: __ _
mg/kg 0.0174 0.0181 4.01 24 86.8 WG171139
mg/kg 0.0170 0.0185 8.42 20 84.8 WG171139
mg I kg y~~ :.'.. o;: o 219 .)~~,~~~:>~ o ;-~·.o 219 tr:F o :;' 1'3 :7: }/ 2 4 X ---.: 11 o -,;'?\( ~:~~~~: wm :71' 13 9 f¥4 ,-_-,-
mg/kg 0.0212 0.0215 1.08 11 --10-6.-··•" WG171139
mg/kg 0.0193 0.0199 3.16 22 96.5 WG171139
.. ·it'tbirig/kgf@t:_O:':'ol72•0:':'oi89_::.--:· 9~04tffi 24·.· §86':'-1~WG171139
mg/kg 0.0217 0.0220 1.69 26 108. WG171139
mg/kg 0. 0164 0. 0182 10.3 23 82.2 WG171139 MmY ~~~~~t-)'·%~j~~ .. ,,_,:):::g .. ;·.g ~~}~\-g : g i ~ i>n~ ~ : ~-9 -::::-_ ~ 6 ~~:::-:~~::·:,.,.·.· .. ' ~gi ~ii~ ~ ""'''"'"''"mm;,,,"""
mg/kg 0.0165 0.0183 10.1 25 82.6 WG171139
mg I kg iJJfr 0 '; 0 1 7 6; A :; 0 ··;' 0 1' 8 9 ;.::::::~ 7; 3 0 _, •. )k_ 2 4'%_?-:,, ___ 8 ?..::·_8_\l-''-i'-s WG 1 711-3 9 )'::· '•'
mg/kg 0.0221 o.0214 3.22 11 110. ·wG171139.
mg/kg 0.0217 0.0224 3.18 20 108. WG171139
)Iing/kg::·':~ -'0 ·; 019 S_:(ffito:'~O 190 2>.44 '$\:~:~:·25~{: ::;-''9 7 . 6 :;~)f@'~ WG1 7113 9!fu-J'_}
mg/kg 0.0203 0.0219 7.78 22 -101. WG171139
mg/kg 0.0181 0.0188 3.41 20 90.7 WG171139
::Jiffi9/kg 0. 0194tihlO';·o207-:· .. ?: 6'%3'llifn6 ?j7 .1 1ili::WG171139
mg/kg 0.0583 0.0628 7.32 20 97.2 WG171139
Batch number /Run number 1 sample number cross reference
WG170633: R207597: Ll69049-01
WG171054: R208029: L169049-01 02 03
WG170851: R208085: Ll69049-02 03
WG171139: R208098: Ll69049-01 02 03
*denotes out of limit range result. See Attachment B of standard report for list of qualifiers.
* * Calculations are performed prior to rounding of reported values
Page 15 of 16
g • ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-757-5859
Fax [phone]
0 . Coastal Env1ronmental, Inc.
Mr. Mark Hafenmaier
Tax I.D. 62-0814289
Est. 1970
0 857 West Main Street
Murfreesboro, NC 27855
Quality Assurance Report
Level II
September 17, 2004
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L169049
ESC Level 2 Data Package
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank -an aliquot of reagent water carried through the
entire analytic process. The method blank results indlC1lte if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytea above the reporting limit in the method blank are
qualified with the "8" qualifier.
Laboratory Control Sample -is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate -is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 16 of 16
VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: Coastal Environmental, Inc. Laboratory Name: Environmental Science Corporation
Project Name: RAM5 NC Certification# (LAB) 375
Site Location: NC ---------------------
F~~j_.::}.· :gg~-;;,-y_.,~,-~.,.::::~ · ¥F.;,Ji¥? ~~~~!r-.~..:. ~i_S3mPie;lnfOrmatiori'arl"diArialytiC-ai;ReSUitS-~ · :y:;e _. ,,_: ~~·'!..<t.=¥ . ..:.::..~x-""'-~-.;,~;_~ -~-.-.... -:"''·"'!'" .. "-~~<::--..,~-""' _ -~-------. : ~ ....... ~--~--'--··. ~._.,,..._ .. _•~·. ":>.~~-".:; ~~~...:--: .... ,,.~; . '.J! ~ :.Jt.f -~:.~: -~ ?-1:-~ ~
Sample Identification L 169049-01 I
Sample Description GP-10 10FT
Sample Matrix SOIL
Collection Option (for soil)* TerraCore
Date Collected 9/7/04
Date Received 9/9/04 I
Date Extracted 9/7/04
Date Analyzed 9/14/04
Dry Weight% 81%
Dilution Factor :1£~-Re~til~;:;~; ·~--.. -...... i:;f;.ReS-tllt~~: ·-:~D-ii.t-'_j; :f~~e~~~ltt_~ ~~[?~~":-~ ~~~ReSUlt .•'·-;; ,_, --. ~-~ -. :k-~-~1~)': . "'-~ .----~--~ •h-•. -._, -. -·~-.
C5-C8 Aliphatics* in mgfkg <9.6 78 I
C9-C12 Aliphatics* in mg/kg <9.6 78
C9-C10 Aromatics* in mgfkg <9.6 78 I
Surrogate% Recovery-FID 98%
Surrogate% Recovery -PID 98%
"Opt1on 1-Establlshed fill hne on v1al Opt1on 2=Sampling Dev1ce (1nd1cate brand, e.g. EnCore) Opt1on 3-Field we1ght of so1l.
··Range results should exclude any surrogates, internal standards, or Target PAH analytes.
;. cSlcB: _, ...... --. ~cg:cio--' '· C9'C12C-Auphiti~ L .. .,.-···. J'';~ tAromati~., ;Aliphatic·~
-, '-- -'."' . '·"'~ __ \-
Percent Recovery-Fortified Blank (Spike)-PID 85.6%
Relative Percent Difference -PID Duplicate 2
Percent Recovery-Fortified Blank (Spike)-FlO 120.5% 99.3%
Relative Percent Difference -FID Duplicate 1.8 1.8
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:t)Dil-~::.7,:~ A~:,-,.:ReSUft'-::<'!
'-' ~ --~--. ... ---. ~~:Di~;r-'~ .........
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Attachment 2
I VPH Laboratory Reporting Form
. "'·•:· "'·'"'~'"·'. ·-···~ "'" .....,.---.. ----...---.......... __............ ,. r --~"""'''~~-··~·--,,.,._.,~r.rr;r."""~ ..... ·~· ,,._ ~:' ~ . -Calibration_and,QAiOC.rlnfQ_rmatiQn :' _, ,:f_ :.. •• -::_ · .. '-':' ~.r .. ,..·· , -~ ~:·; 1: •• ~' ',~·~~'-··, r~ ~~,~ ___ ......_.. -· •. ~ ---_.,. .... --"·--~ ---.... ----:1'-..... ·--• --~ ". -· .. t -·
Initial Calibration Date __ 9"!!_,12"'/-"2~00"4'----
~ Calibration Ranges and Limits
• 'J• ..... -• . " ' \.;,.~: "~-Rang~ ' . . ' \l, ~ ~-• :o~ . ML' .. .. ".. ' ,:: RL}''; ~-o...">'< ··~ t l;~ ,. ' MDL ... L ••. ,, -'<· . ' • !. • ' . ,.,,, -·~-·' '
C5-C8 Aliphatics 1.0062 mg/L 1.02 mg/L 1.1 mg/L
C9-C12 Aliphatics 1.0032 mg/L 1.01 mg/L 1.1 mg/L
C9-C10 Aromatics 1.0011 mg/L 1.003 mg/L 1.1 mg/L
0 NOTE: Please Include units as appropnate
Method of Quantitation (Circle one)
Calibration Concentration Levels
Average Response Factor
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•'"•'·•'fR·"'~--• ·'h :~_ ',' te·vels'·t· =·\:~:· r .,·, _ ~E1ge , . ,4 • '. ,, . . " ..
1.075 mg/L
CS·CB 1.375 mg/L
Aliphatics 1.750 mg/L
17.5 mg/L
111.25mg/L
1.055 mg/L
C9-C12 1.275 mg/L
Aliphatics 1.550 mg/L
15.50 mg/L
18.25 mg/L
1.010 mg/L
C9-C10 1.050 mg/L
Aromatics 1.100mg/L
11.00 mg/L
11.50 mg/L
NOTE: Please 1nd1cate un1ts as appropnate.
Calibration Check Date 9/12/2004 I Calibration
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• '71q.l' .•. ~ ..... ' '• ' .l!eVEif(iil M91L:)~-}· ,,..r;.~ lt;'_·tM Rang~_.: -~'-: " '~-,., . ' ". ' .. ' ' . ··--~
C5-C8 Aliphatics .75
C9-C12 Aliphatics .55
C9-C1 0 Aromatics .10
MDL = Method Detection limit
ML = Minimum limit
RL = Reportable Limit
Coastal Environmental, Inc.
RAM5
NC
L 169049-01
·,.--,•• ...... ... ( %RSD or CCC
Coef of Del {r112)
14.68
RSD
Coef of Del {r112)
10.50
RSD
Coef of Del (r"2)
1.000
Linear Fit
. : ''RPD ('·',q •;,.· ,. •,,,-..•~ •...• · -!!'!. _o •:· .. ,,·,. ActUal Value (fii' MQ/L:) .. . . .. .. ~ -" .
8.4 .816
5.8 .583
5.1 .095
RPD·= Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
-------------ll!!ll!lll:lc:=liilli--
VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: Coastal Environmental, Inc. Laboratory Name: Environmental Science Corporation
Project Name: RAMS NC Certification #(LAB) 375
Site Location: _N_C ______________ ~
Sample Identification L 169049-02 L 169049-03 I
Sample Description GP-11 10FT GP-12 10FT
Sample Matrix I SOIL SOIL
Collection Option (for soil)* TerraCore TerraCore
Date Collected 9/7/04 9/7/04
Date Received 9/9/04 9/9/04
Date Extracted 9/7/04 9!7/04
Date Analyzed 9/16/04 9/16/04
Dry Weight% 84.2% 81.6%
Dilution Factor
C5-C8 Aliphatics"' in mg/kg <4.4 37.5 <5 40.5
C9-C12 Aliphatics* in mg/kg <4.4 37.5 <5 40.5
C9-C10 Aromatics* in mg/kg <4.4 37.5 <5 40.5
Surrogate % Recovery-FlO 144% 144%
Surrogate % Recovery -PID 142% 144%
"'Opt1on 1-Estab!ished f1U hne on v1al Opt1on 2-Samphng Oev1ce (tnd1cate brand, e.g. EnCore) Opt1on 3-Field we1ght of so1l.
.. Range results should exclude any surrogates, internal standards, or Target PAH analytes.
'cs:cs,' 'cs-c.iF .~c9:c1o· .. ,.. .. :',.•' '"' -"";' .. ,j: ~ .. ;;.. -/•"" .. ,_ .. , ..
Aliphatic ""AiiRhatic~ ~Aromatic ..•. ".T.: ':..-.:.;..······'""" ··~ --·'----
Percent Recovery-Fortified Blank (Spike)-PID I 98.9%
Relative Percent Difference-PID Duplicate I 1 . 1
Percent Recovery-Fortified Blank (Spike)-FlO I 97.9% 95.9%
Relative Percent Difference-FlO Duplicate 0.2 0.3
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Attachment 2
VPH Laboratory Reporting Form
1't'~'!:!'t"-~ ., .• ~,, --. ·.-(4
..,... ·; ·:" ..... ;:--:"!'!< ~~·:--:·c~·-l·b·· ---~--_.,..,~.........-d·Q-Al-QC I f ~---~··· -""""'!'' ... ., ...... , .. ";!~"1lffl"' ... --..~~'\'Jt ·r--.... _, :. r,rJ' r-;. i· ·:~•n• ··'""':fl' . -• • ,_,,r,t-,. , ... ,, •.·· .' ~--•• -~--, ,_ a 1 ra 10n ,a_n · .-_ -! n .o~ma 10n. :•1 .. ~. , .. ,. ,·,1,, •-,"~F-•" .:t,:,•1.'1' .~<;><>,, , ~r::. 1 ,, · v:' . • .:.o...,.,,/,.::;.1.61,;..,,_, ,,~j! .r(. ,.,,.,..J ,._ ,t, ..•. _ 1.~ ..._.,~,._ •• , _, --....... ,_,,._,...., l.l.f.o.:.~ ...... -~ .w.. •• ~ f,f .. !.Jf-,,,,,.,, ..... li, , , ..•..... n... .1, ..• ~
Initial Calibration Date 9/"1 4/2004
Calibration Ranges and Limits
l<f.) j_l:: ·~··Ri:trig·e •t' '/h"' ~--' ".·:t.: Mol"FI•.J; · ..• ·-,;~ •. .J, ~ '•ML;,,; ~h ~-.
~ •' .. ..__ . . ' ' . ~--·-:. ,I ••,I,' ,.__ t , , '•' .t ',,
C5-C8 Aliphatics 1.0062 mg/L 1.02 mg/L
C9-C12 Aliphatics 1.0032 mg/L 1 .01 mg/L
C9-C10 Aromatics 1.0011 mg/L 1.003 mgA..
NOTE: Please 1nclude umts as app10pnale
Method of Quanlitalion (Circle one)
Calibration Concentration Levels
Average Response Factor
·k1·~--l'.)'R·ang'e· t·;,·~· '' c '·~·-·--;·~····· ,--·~ ,•. · (.• ~/oRS[l~·,>ccC: ' ' ~ evels ~f<· • •. 1. ;,.-~ . ·'· . ----I • o ~ • . ~· . " . . .
1.075 mg/L
C5-C8 1.375 mg/L Coef of Del (r112)
Aliphatics 1.750 mg/L 17.81
17.5 mg/L RSD
111.25mg/L
1.055 mg/L
C9-C12 1.275 mg/L Coef of Det (r''2)
1 550 mg/L 9.64
Aliphatics RSD 15.50 mg/L
18.25 mg/L
1.010 mg/L
C9-C10 1.050 mg/L Coef of Del (r..,2)
Aromatics 1.100 mg/L 14.41
11.00 mg/L RSD
11.50 mg/L
NOTE: Please 1nd1cate un1ts as app1opnate.
Calibration Check Date 8/24/2004
.:•f'J ·r ~: }_;_ ;._R~,;~·;< . .,.~.
'"':'."':.·
1 .1 mg/L
1.1 mg/L
1.1 mg/L
I Calibration
.~: -,.-~-: ~;~.:~~_ang~:.'\1 ~: _· _:, Mg/L):.' -·,}:'~<-.-Rpo'-(iri-%) J:.~.,~; 'ACtua i' V 81 ue ~ (i 1-i · iviQJL;)
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· ,-Level.(in '; ' ' .. ~-" .
C5-C8 Aliphatics 75
C9-C12 Aliphatics .55 -
C9-C10 Aromatics .1 0
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
Coastal Environmental, Inc.
RAM 5
NC
L 169049-02
. " • ·l· .. .... -. " ' ~-"" . .. .. . ' " --
3 .728
3.5 .531
6.2 .094
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
r-"'""---"""'-----""""--__.!""""---"'""'---"""''--~:;;:;;;;,;o;~:;;;;;;;;~""---"'""'--"i=~A~c§e~'~"~'~'~";J;te;)!'"~e1(o~c~e~"~;v~e~"'~e=:;::::""r"'-----"""'----'~~;;c~:--4-Aitemate billing information: Chain of Custody I I I Pege_of_ Ci•asi ai· Environmental, Inc.
857 West Main Street
,v!urfreesboro,NC 27855
Report to:
:\lr. :\lark Hafenmaier
reject
escMption: RA.:\1 5
Emait· 0: 0 mhafcnm@.coastalcnvironme IU :;; ityiStatc ·I::
oUected (l:l 1 ------------cc~err~.------~~"*~--------+ -0~ r Client Project#. lab Project# hone: [phone] Cl'l
AX: [phone] 01-105 COAE:\'V.:\fi\"C-01105 ~
pone_cted by (print): Site/Fadlity ID#: p 0 #: ~
a " :;;
" "' ~
" "' ~ ; ~ otlecte~d by (signature): Date Results \reeded
0
0 S
~ ~ E
' ,_ , ";..;, 1 Email? _No ~Yes No. > 0 ~
!Rush? I (Lab MUST Be Notified }
_Same Day .200%
_Next Day .. 100%
f'~"""'-"UI~ooC£N __ i!:;lf\)-------t='---'--;-----.,-----J--'FAXe,s,0c..__N~o~-~-o-"y~,,~---+of c) ~ ~
ICntrs ۤ ~I~ Sample 10 Date
_Two Day. . .. 50%
Comp/Grab Matrix' Depth
c " " " u
"' u
0 >
I
~P-/D I ss 1of-t lsiXIXIXIXI I I I
c, P-II ss siXIXIXIXI I I I
lr~p-IL ss v siXIXIXIXI I I I
ss
ss
Prepared by:
• E;\'VIROl\';\IEl\'TAL
SCIE;>;CE CORP.
12065 Lebanon Road
Mt. Juliet, Tl\' 37122
Phone [phone]
FAX [phone]
CoCode: ·cOAENVMNII?b use only}
Template/Prelogin T2521 0' f!21350
Goold 5/tB 7'5/2"'/i
Shipped Via: Fed EX Ground
Remarks/Contaminant Sample II (lab only)
... ,;~
ss ~--------------4-----4-~--+----+----+----+~s~IX~IX~'+I~X~I~X~I-+1~1--~1 -+--------+---~-~ I I -I I I I I I I
I I I I I I I I I
I I I I I I I I I
'Matrix: SS-Soil GW-Groundwater WW-WasteWater OW-Drinking Water OT-Othecc ___ _ pH _____________ Temp
Ro:ITL3.rks:
Relinquished by: {$1gnature}
I
I -,,;;;1~1,:,!:;<;;11;• :if--A r e onqwshed by: (Signatuie) ~~-'-:;
Rehnquoshed '-~§~~~~) -"
Flow ______ _ Other