RA-996_6559_CA_RPTS_20180123

GROUNDWATER MONITORING
REPORT

MURPHY OIL USA, INC.
FORMER SPUR NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA

INCIDENT NO. 6559
FACILITY I.D. NO. 0-006861
LOW RISK

PPM PROJECT NO. 250608-GWM

JANUARY 23, 2018

TABLE OF CONTENTS PAGE

1.0 INTRODUCTION .......................................................................................... 1
2.0 BACKGROUND ........................................................................................... 1
2.1 Site Description ................................................................................. 1 2.2 Site History ........................................................................................ 2
2.3 Risk Classification ............................................................................. 6
3.0 FIELD ACTIVITIES ...................................................................................... 9
3.1 Sensitive Receptor Survey ................................................................ 9 3.2 Groundwater Sampling .....................................................................10
4.0 FINDINGS ...................................................................................................11
4.1 Groundwater Elevation .....................................................................11
4.2 Analytical Results .............................................................................11
5.0 CONCLUSIONS ..........................................................................................12
6.0 RECOMMENDATIONS ...............................................................................13

FIGURES (APPENDIX A)

Figure 1 Site Map Figure 2 Area Map Figure 3 Groundwater Elevation Contour Map (December 7, 2017)
Figure 4 Petroleum Concentrations in Groundwater (December 7, 2017)
Figure 5 Benzene Concentrations in Groundwater (December 7, 2017)
Figure 6 Aliphatics C5-C8 Concentrations in Groundwater (December 7, 2017) Figure 7 Aromatics C9-C10 Concentrations in Groundwater
(December 7, 2017)

TABLES (APPENDIX B)
Table 1 Summary of Groundwater Elevation Survey Data
Table 2 Summary of Groundwater Analytical Data
APPENDICES
Appendix A Figures
Appendix B Tables
Appendix C Groundwater Analytical Report
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1.0 INTRODUCTION
PPM Consultants, Inc. (PPM) has completed Groundwater Monitoring (GWM) activities at
the former Spur Station No. 1211 located at 708 South Goldsboro Street in Wilson, Wilson
County, North Carolina. The purpose of the field activities was to obtain current
groundwater quality data through the collection and analysis of groundwater samples.
PPM was retained by Murphy Oil USA (Murphy) to conduct the GWM, which was
conducted in accordance with North Carolina Department of Environment and Natural
Resources (NCDENR) Monitoring Guidelines. This report provides a summary of
previous investigations conducted at the site and presents analytical results, findings, and
conclusions from the recent GWM activities.

2.0 BACKGROUND

2.1 SITE DESCRIPTION

The Former Spur No. 1211 is located at 708 South Goldsboro Street in Wilson, Wilson
County, North Carolina. The city of Wilson, North Carolina is located within the Neuse
River Watershed Area. All area creeks, rivers, and streams are tributaries of the Neuse
River. Geographically, the site is located at 35o 43’ 10” N and 77o 55’ 08” W. The site is
located west of the intersection of South Goldsboro Street and Bank Street Southwest. The
site is relatively flat and gently slopes to the east.

The site is improved with an approximately 875 square foot building that is located on the
west end of the property and operates as a snow cone stand/restaurant. A paved parking
area extends from the store front to South Goldsboro Street. The area to the east of the
paved parking area is the former underground storage tank (UST) pit and is a mostly grass
and gravel covered area.

The former USTs consisted of one 15,000-gallon UST and three 6,000-gallon USTs, all of
which were closed by removal in 1991, with the exception of a 6,000 gallon UST that was
closed in 1986. NCDENR has classified the site as Residential and ranked the facility as a
low risk site.

There are currently five active onsite groundwater monitoring wells, MW-3 through
MW-6, and MW-8 (MW-1 and MW-2 have been abandoned). There are currently three
offsite monitoring wells, MW-9, MW-10, and MW-11, located along the right-of-way of
Banks Street (MW-9 and MW-10) and the right-of-way of South Goldsboro Street
(MW-11). These features are shown in Figure 1, Site Map, in Appendix A.
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Vacant commercial land adjoins the property to the north and northwest. Commercial
properties (Kingsmill Construction Company is located northeast of the site, while
Petroleum Equipment Services is located east of the site across the intersection of South
Goldsboro Street and Banks Street. Garris Evans Lumber Company is located south of the
site and a self-serve carwash adjoins the site on the west. An intermittent stream extends
from the northeast (under Banks Street) to the southwest, where it enters a tributary of
Hominy Swamp, approximately 250 feet southwest of the site. To the west and northwest
of the intermittent stream are vacant properties. These features are shown in Figure 2,
Area Map, Appendix A.

2.2 SITE HISTORY
On February 20, 1986 Murphy Oil registered one 15,000 gallon and two 6,000 gallon
USTs in service and one 6,000 gallon UST permanently out of service. The UST pit was
located on the northeast portion of the property. Operation of the station ceased on
September 30, 1990, when the Lease & Franchise Agreement and Sales Agreement with
the station owner was cancelled.

Preliminary Site Assessment

In January 1991, UTTS Environmental of Ayden, North Carolina, completed a soil
assessment at the site, due to a suspected motor fuel release. Five soil samples were
submitted for laboratory analysis of Total Petroleum Hydrocarbons (TPH) as kerosene.
Two of the soil samples collected [BH-3 (8’-9’) and BH-4 (9’-10’)] exceeded the Risk
Based Screening Level (RBSL) for TPH as kerosene. Bore hole BH-3 was located south
of the UST pit and BH-4 was located in the center of the UST pit.

UST Closure

In June 1991, Sunbelt Environmental permanently closed by removal all four of the
gasoline USTs, as well as, one 1,000 gallon kerosene tank and the dispensers. A total of
thirteen soil samples were collected for laboratory analysis during the UST Closure and
analyzed for Total TPH and Total benzene, toluene, ethylbenzene, and xylenes (BTEX).
The highest total TPH was from soil sample 11 [534.0 milligrams per kilogram (mg/kg)],
which was located in the center of the UST pit.

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Comprehensive Site Assessment (CSA)

In December 1991, Hazclean Corporation advanced seven soil borings at the site. A total
of 17 soil samples were collected from the seven borings for laboratory analysis. The
highest TPH concentration was reported as 5,700 mg/kg of kerosene from the soil boring
for MW-2. Six of these borings were converted to groundwater monitoring wells (MW-1
through MW-6), all installed to a depth of approximately 14.0 feet below ground surface
(BGS). According to the Hazclean report, a deep well was attempted at a location for
MW-7 in front of the store, but auger refusal and probable bedrock was encountered at a
depth of about 18.0 feet BGS and this well was not installed.

A total of six groundwater samples were collected from monitoring wells MW-1 through
MW-2. Concentrations of benzene in groundwater exceeded the North Carolina
Groundwater Quality Standard (GWQS) in the samples collected from MW-1 through
MW-5. The sample collected from MW-2 also exceeded the North Carolina GWQS for
concentrations of ethylbenzene in groundwater.

Phase II Comprehensive Site Assessment

In June 1992, Hazclean conducted a Phase II CSA at the site, based on the need for
additional assessment. Four additional monitoring wells (MW-8 through MW-11) were
installed at this time. A total of six soil samples, one creek water sample and five
groundwater samples (MW-2 and MW-8 through MW-11) were collected for laboratory
analysis. None of the soil samples collected exceeded the regulatory limits for TPH in soil.

Groundwater samples were analyzed for BTEX, methyl tertiary butyl ether (MTBE),
naphthalene, and total lead. Benzene concentrations in groundwater exceeded the GWQS
in the samples collected from MW-2, MW-8, and MW-10. Concentrations of MTBE in
groundwater exceeded the GWQS in the samples collected from MW-2, MW-8, and
MW-11. Naphthalene concentrations in groundwater exceeded the GWQS in the sample
collected from MW-8. Concentration of lead in groundwater exceeded the GWQS in the
samples collected from MW-2, MW-8, MW-9, and MW-11.

Groundwater Monitoring Event

In July 1993, RUST Environmental & Infrastructure (RUST E&I) conducted a
groundwater monitoring event and collected a composite soil sample from the UST pit.
The TPH (gasoline) concentration in the composite soil sample was 31 mg/kg.
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Groundwater concentrations of benzene exceeded the GWQS in the samples collected
from MW-1 through MW-8, MW-10, and MW-11. Concentrations of ethylbenzene in
groundwater exceeded the GWQS in the samples collected from MW-2 through MW-5,
MW-8, MW-10, and MW-11. Concentrations of MTBE in groundwater exceeded the
GWQS in the samples collected from MW-1, MW-2, MW-8, and MW-10.

Corrective Action Plan (CAP)

In August 1993, RUST E&I conducted a Corrective Action Plan (CAP) that included an
Air Sparge Pilot Test at the site. The test consisted of the installation of one air injection
well, one vapor extraction well, and two pressure piezometers installed within the area of
monitoring well MW-8. Monitoring well MW-8 was used to determine the efficiency of
the air sparge test. The test was conducted in four phases: using a vacuum pump to extract
vapors from the extraction well; injecting compressed air into the injection well and
measuring the pressure at the piezometers; injecting air into the injection well and actively
recovering vapors with a blower; and modifying a piezometer as the extraction well while
injecting compressed air into the injection well.

The results of the air sparge test were evaluated by collecting a groundwater sample from
MW-8 and comparing the results to the results of the July 1993 Groundwater Monitoring
Event. The groundwater results showed a 39 percent reduction of benzene concentrations,
58 percent reduction in toluene concentrations, 67 percent reduction of ethylbenzene
concentrations, 68 percent reduction of xylene concentrations, and 7 percent reduction of
MTBE concentrations. RUST E&I recommended Air Sparging as the remediation method
for this site.

Monitoring Well Abandonment (MWA)and Soil Removal

In September 1993, RUST E&I performed a well abandonment of monitoring wells MW-1
and MW-2. The wells were abandoned to accommodate petroleum contaminated soil
removal.

Approximately 1,200 cubic yards of soil were removed from the site. A total of 10 soil
samples were collected for laboratory analysis of TPH. Soil sample SS-7 (45 mg/kg)
exceeded the state action level of 10 mg/kg for TPH gasoline. Soil sample SS-7 was
located along the center south wall of the UST pit. Soil samples SS-1 (40 mg/kg), SS-3
(110 mg/kg), SS-5 (100 mg/kg), SS-6 (85 mg/kg), and SS-9 (230 mg/kg) all exceeded the
state action level of 40 mg/kg for TPH kerosene. These soil samples are located on all
surrounding walls of the UST pit.
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Groundwater Monitoring Event

On January 29, 1996, RUST E&I completed a quarterly monitoring event. Groundwater
samples were collected from MW4, MW-6, MW- 8, and MW-9 and analyzed for BTEX
and MTBE. Benzene concentrations exceeded the regulatory limits set by the NCDENR in
MW-4, MW-6, and MW-8. Ethylbenzene concentrations exceeded regulatory limits in
MW-4 and MW-8. MTBE concentrations exceeded the regulatory limit in MW-8.

NCDENR Site Ranking

In 1996 the NCDENR ranked the site as 55E (Low Risk) and requested that all assessment
activities cease.

Limited Site Assessment (LSA)

In June 2001 Murphy Oil retained PPM to resample the soil and groundwater at the site
and determine if the site was eligible to be granted a No Further Action status.

On July 24, 2001, PPM performed the LSA. Soil borings B-1 through B-5 were advanced
on site. Free product was not encountered during the site investigation. Benzene, toluene,
and total xylene concentrations were below quantification limits (BQL) in all soil samples
collected. Alphatics C5-C8 and n-propylbenzene exceeded the MSCC of 72.0 parts per
million (ppm) and 2.00 ppm in soil sample B-3 (140 ppm and 2.70 ppm, respectively).

Benzene concentrations exceeded the GWQS of 1.00 parts per billion (ppb) in monitoring
wells MW-3 (28.0 ppb), MW-5 (20.0 ppb), MW-6 (4.00 ppb), and MW-8 (3.00 ppb).
Ethylbenzene concentrations exceeded the GWQS of 29.0 ppb in monitoring wells MW-5
(59.0 ppb), MW-8 (51.0 ppb), and MW-10 (55.0 ppb). Lead concentrations exceeded the
GWQS of 15.0 ppb in monitoring wells MW-5 (19.0 ppb), MW-6 (226 ppb), MW-10 (54.6
ppb), and MW-11 (20.7 ppb). Aliphatics C5-C8 exceeded the GWQS of 400 ppb in
monitoring wells MW-3 (2,500 ppb), MW-5 (3,100 ppb), MW-6 (1,400 ppb), MW-8
(2,600 ppb), and MW-10 (880 ppb). Aromatics C9-C10 exceeded the GWQS of 200 ppb
in monitoring wells MW-3 (440 ppb), MW-5 (470 ppb), MW-6 (300 ppb), and MW-8
(600 ppb). Groundwater flow was toward the northwest at the time of the groundwater
sampling.

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On September 22, 2003, the NCDENR issued a letter requesting that a Soil Assessment
Report (SAR) be submitted. The NCDENR classified the site as Residential with a risk
classification of Low.

Soil Assessment Report (SAR)

In November 2003, PPM conducted a SAR Investigation at the site. The investigation
consisted of: the advancement of 10 soil borings to a total depth of 20 feet BGS, the
collection of 10 soil samples for laboratory analysis; and the collection of one creek water
sample for laboratory analysis.

Soil sample results show the highest BTEX concentrations in boring B-6 (1.07 mg/kg)
from 10’ to 15’ BGS. None of the soil samples collected exceeded any of the Maximum
Soil Contamination Concentration (MSCC). The water sample from the intermittent creek
was below detection limits (BDL) for all Chemicals of Concern (COC).

2.3 RISK CLASSIFICATION Part I – Groundwater/Surface Water/Vapor Impacts

High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the
source area of the release? NO
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars,
industrial cooling water, filling swimming pools) located within 250 feet of the
source area of the release? NO
4. Does groundwater within 500 feet of the source area of the release have the potential
for future use (there is no other source of water supply other than the groundwater)? NO

5. Do vapors from the release pose a threat of explosion because of accumulation of
the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? NO
If yes, describe.
___________________________________________________________________
___________________________________________________________________
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6. Are there any other factors that would cause the release to pose an imminent danger
to public health, public safety, or the environment? NO If yes, describe.
___________________________________________________________________
___________________________________________________________________

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
YES
If YES, does the maximum groundwater contaminant concentration exceed the
surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? NO

8. Is the source area of the release located within an approved or planned wellhead
protection area as defined in 42 USC 300h-7(e)? NO
If yes, describe. ___________________________________________________________________
___________________________________________________________________

9. Is the release located in the Coastal Plain physiographic region as designated on a
map entitled “Geology of North Carolina” published by the Department in 1985? NO
If YES, is the source area of the release located in an area in which there is
recharge to an unconfined or semi-confined deeper aquifer that is being used or
may be used as a source of drinking water? NO
If YES, describe. ___________________________________________________________________
___________________________________________________________________

10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established by the Department? NO

Part II - Land Use

Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent
or temporary)? NO
2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly? NO

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3. Does the property contain a commercial (e.g., retail, warehouse, office/business
space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive
commercial or industrial enterprise, or is the land undeveloped? YES
Describe.
The former store building on the site is currently a snow cone stand/restaurant.
4. Do children visit the property? YES
Explain.
It is very likely that children visit the snow cone stand/restaurant.

Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? NO
Explain.
There is no restricted access to the site.

5. Do pavement, buildings, or other structures cap the contaminated soil? NO Describe.
The former UST pit area is filled in with soil.

If yes, what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future? The former UST pit area can be covered with pavement.

6. What is the zoning status of the property?
The Wilson, North Carolina Zoning Map (revised January 3, 2018), depicts the site
as Light Industrial.
7. Is the use of the property likely to change in the next 20 years? NO
Explain.
The site is surrounded by commercial and industrial properties.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release
(excludes property containing source area of the release):
1. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?
The nearest primary residence is approximately 340 feet east-southeast of the
source area (former UST pit).
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2. What is the distance from the source area of the release to the nearest school,
daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly?
The nearest place of public assembly is St. Rose Church of Christ, located
approximately 450 feet southeast of the source area.
3. What is the zoning status of properties in the surrounding area?
The Wilson, North Carolina Zoning Map (revised January 3, 2018), depicts the
north adjacent property as Open Space; the northeast, east, and southeast adjacent
properties as Industrial Mixed Use; and the south, southwest, and west adjacent properties as Light Industrial.
4. Briefly characterize the use and activities of the land in the surrounding area. The adjacent properties to the north, northeast, and south are industrial properties. The adjacent properties to the east, southeast, and west are commercial properties.
Within a 500-foot radius of the site, there is one residence and one church both
located east-southeast of the site. Residential subdivisions are located
approximately 620 feet southeast, 1,200 feet south, and 960 feet southwest of the site.

3.0 FIELD ACTIVITIES

3.1 SENSITIVE RECEPTOR SURVEY
PPM personnel performed a visual reconnaissance of the properties within an approximate
1,500-foot radius of the site to identify receptors potentially sensitive to a release of
petroleum hydrocarbons. Receptors considered potentially sensitive included:
• Migration pathways such as utilities, conduits, and backfilled trenches
• Biological receptors such as fish, animals, and humans
• Natural receptors such as streams, lakes, or other surface bodies of water
• Man-made receptors such as water wells, basements, crawl spaces, and underground
confined space areas.

Underground utilities at the site include water and sewer lines, which extend from the
northeast to the southwest within the right-of-way of South Goldsboro Street and from the
northwest to the southeast within the right-of-way of Banks Street. Water and sewer
connect to the former Spur No. 1211 building from the right-of-way of South Goldsboro
Street to the center south portion of the store building. PPM did not identify any biological
receptors that appear to be potentially exposed to the release. No areas of stressed
vegetation were identified at the site.
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The site is located within the Neuse River Watershed Area. Although the Neuse River is
located approximately 25 miles south of the site, all of the area creeks, rivers, and streams
are tributaries to the Neuse River, which feeds into the Pamlico Sound. A storm drain is
located approximately 400 feet northwest of the subject property and drains into an
intermittent creek, which extends from the northeast parallel to the northwest property
boundary (approximately 70 feet from the site) to Black Creek, which is located
approximately 250 feet southwest of the site. A Railroad system is located approximately
20 feet north of the site. All of the features identified on the subject property and adjoining
properties are shown in Figure 2, Site Map, Appendix A.

No public supply wells or private wells were identified within a one-mile radius of the site.
A water tower, used only for elevated storage of the public water supply, is located
approximately 1,960 feet northeast of the site.

3.2 GROUNDWATER SAMPLING

Groundwater sampling activities were conducted on December 7, 2017. Prior to sample
collection, the depth to free product (if encountered) and groundwater was measured with
an oil/water interface probe. Monitoring wells MW-4, MW-9, and MW-11 could not be
located, therefore; groundwater samples were not collected from the wells during this
event. Free product was not detected in any of the monitoring wells during the December
2017 sampling event. The depths to groundwater along with the top of casing elevations
were used to calculate the groundwater elevation at the site and determine groundwater
flow direction.

Each monitoring well was sampled utilizing a peristaltic pump and new polyethylene
tubing. During purging, water quality parameters were recorded. Purging was considered
complete when either the water quality parameters stabilized or a maximum of one well
volume of water was purged and samples were collected.

After purging, groundwater samples were collected from monitoring wells MW-3, MW-5,
MW-6, MW-8, and MW-10. Each sample was placed in clean, laboratory supplied bottle
ware, preserved on ice, and delivered under proper chain-of-custody documentation to
Pace Analytical Services, Inc. (Pace) of Huntersville, North Carolina for analysis of
volatile organic compounds (VOC) and 1,2-Dibromoethane (EDB) per Environmental
Protection Agency (EPA) Method 6200B.

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4.0 FINDINGS

4.1 GROUNDWATER ELEVATION
A summary of the current and historical groundwater elevation data is provided in Table 1,
Summary of Groundwater Elevation Survey Data, Appendix B. Groundwater
elevations and flow direction are shown in Figure 3, Groundwater Elevation Contour
Map (December 7, 2017), Appendix A. Based on the groundwater elevation data
collected during the December 7, 2017 sampling event, groundwater is flowing to the
northwest with a hydraulic gradient of 0.065 between MW-5 and MW-8.

4.2 ANALYTICAL RESULTS
None of the groundwater samples collected on December 7, 2017 had reported COC
concentrations that exceeded their respective Gross Contamination Levels (GCL). The
Petroleum Concentrations in Groundwater (December 7, 2017) are shown in Figure 4,
Appendix A.

Benzene in groundwater exceeded the GWQS of 1.00 micrograms per liter (µg/L) in the
samples collected from monitoring wells MW-6 (1.70 µg/L) and MW-8 (1.90 µg/L). The
benzene concentrations from this event are provided in Figure 5, Benzene
Concentrations in Groundwater (December 7, 2017), Appendix A.

Lead in groundwater exceeded the GWQS of 15 ppb in the samples collected from MW-3
(71 ppb), MW-5 (103 ppb), MW-6 (664 ppb), MW-8 (84.8 ppb), and MW-10 (485 ppb).

Aliphatics C5-C8 concentrations in groundwater exceeded the GWQS of 400 ppb in the
samples collected from MW-3 (759 ppb), MW-5 (575 ppb), MW-6 (545 ppb), and MW-8
(1,020 ppb). These results are provided in Figure 6, Aliphatics C5-C8 Concentrations in
Groundwater (December 7, 2017), Appendix A.

Aromatics C9-C10 concentrations in groundwater exceeded the GWQS of 200 ppb in the
samples collected from MW-6 (228 ppb) and MW-8 (317 ppb). These results are provided
in Figure 7, Aromatics C9-C10 Concentrations in Groundwater (December 7, 2017),
Appendix A.

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Groundwater analytical results from this and previous groundwater monitoring events are
summarized in Table 2, Summary of Groundwater Analytical Data, Appendix B.
Laboratory reports for the groundwater sampling event are included in Appendix C,
Groundwater Analytical Report.

5.0 CONCLUSIONS

Based upon the findings of this GWM event, the following conclusions are presented:
• Based on the updated zoning and Risk Characterization of the site, the site is
located in a mixed/light Industrial area.
• Free product was not observed during the December 2017 groundwater monitoring
event. The groundwater flow direction was to the northwest based on the
groundwater elevation data collected on December 7, 2017.
• On-site monitoring well MW-4 and off-site monitoring wells MW-9 and MW-11
could not be located during this event.
• Concentrations of benzene in groundwater exceeded the GWQS in MW-6 and
MW-8.
• Concentrations of lead in the groundwater exceeded the GWQS in MW-3, MW-5,
MW-6, MW-8, and MW-10.
• Concentrations of aliphatics C5-C8 in groundwater exceeded the GWQS in MW-3,
MW-5, MW-6, and MW-8.
• Aromatics C9-C10 concentrations in groundwater exceeded the GWQS in MW-6
and MW-8.
• The areas of highest impact appear to be in the areas of MW-6 and MW-8, based
on the December 2017 analytical data. Monitoring well MW-6 is located in the
south corner of the site and MW-8 is located along the center west property
boundary.
• Off-site monitoring well MW-10 only exceeded for concentrations of lead in
groundwater, which could be due to high turbidity in the sample.

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6.0 RECOMMENDATIONS

PPM recommends that the site be re-classified as a Commercial property, based on the
current risk classification survey and the fact the site is used solely for commercial
purposes and all adjoining properties are either used for commercial or are vacant
properties.

PPM also recommends that the monitoring wells be abandoned and the site given an
unconditional No Further Action (NFA), based on the current groundwater analytical
results.

APPENDICES

APPENDIX A FIGURES
DRAWN BY:
FIGURE
NUMBER
PROJECT NUMBER:
DRAWN DATE:
BILLING GROUP:
MLR
250608
01/22/18
2017GWM
SITE MAP
MURPHY OIL USA, INC.
FORMER SPUR STATION NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA 1
P P M C O N S U L T A N T S , I N C . PPM www.ppmco.com
R
A
I
L
R
O
A
D
MW-10
MW-8
MW-3
MW-5
MW-6
SIDEWALKSIDEWALK
GRASS
VACANT
PETROLEUM
EQUIPMENT
SERVICES
KINGSMILL
CONSTRUCTION
COMPANY
CULVERT
STORM DRAIN
CREEK CREEKGRASSY
SL
O
P
E
SL
O
P
E
WOODED
AREA
VACANT
PROPERTY
SELFCARWASH
ABANDONED
INDUSTRIAL
PROPERTY
MONITORING WELL LOCATION
NOTES:
1) AREA WITHIN DASHED LINE HAS BEEN
EXCAVATED.
2) ALL USTs WERE REMOVED FROM SITE ON JUNE
16, 2001.FORMER
SPUR
STATIONNO. 1211
GRASSY
CONCRETE
WATER LINE
CONCRETE
CONCRETE
MW-9
MW-1
ABANDONED
MW-4
MW-2
ABANDONED
MW-11
0
N
(Approximate)
25
SCALE: 1"=50'
50
AREA MAP2NUMBERFIGUREDRAWN BY:PROJECT NUMBER:DRAWN DATE:BILLING GROUP:MLR25060801/22/182017GWMMURPHY OIL USA, INC.FORMER SPUR STATION NO. 1211708 SOUTH GOLDSBORO STREETWILSON, NORTH CAROLINAP P M C O N S U L T A N T S , I N C . PPMwww.ppmco.com5
0
0

F
O
O
T

R
A
D
I
U
S
5
0
0

F
O
O
T

R
A
D
I
U
S
1SELF CAR WASH2345678I.D.DESCRIPTION1VACANT PROPERTYALLIANCE ONEKINGSMILL CONSTRUCTION COMPANYPETROLEUM EQUIPMENTGARRIS EVANS LUMBER COMPANYEXCLUSIVE CLEANERS AND LAUNDRYRICHIE'S CAR LOTBLACK CREEKBLACK CREEKSTREAMSTREAM2345678
DRAWN BY:
FIGURE
NUMBER
PROJECT NUMBER:
DRAWN DATE:
BILLING GROUP:
MLR
250608
01/22/18
2017GWM
GROUNDWATER
ELEVATION CONTOUR
MAP
(DECEMBER 7, 2017)
MURPHY OIL USA, INC.
FORMER SPUR STATION NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA 3
P P M C O N S U L T A N T S , I N C . PPM www.ppmco.com
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MW-8
SIDEWALKSIDEWALK
GRASS
VACANT
PETROLEUM
EQUIPMENT
SERVICES
KINGSMILL
CONSTRUCTION
COMPANY
CULVERT
STORM DRAIN
CREEK CREEKGRASSY
VACANT
PROPERTY
SELFCARWASH
ABANDONED
INDUSTRIAL
PROPERTY
MONITORING WELL LOCATION
GRASSY
CONCRETE
CONCRETE
CNL
GROUNDWATER ELEVATION (ft.)
GROUNDWATER ELEVATION CONTOUR (ft.)
GROUNDWATER FLOW DIRECTION
92.42
COULD NOT LOCATECNL
86.45
87.00NO. 121187.0088.0089.0090.0091.0092.0091.90
MW-6
MW-5
92.85
92.42
MW-3
MW-11
CNL
CNL
MW-4
ABANDONED
MW-1SL
O
P
E
MW-2
ABANDONED
SL
O
P
E
WOODED
AREA
CONCRETEFORMERSPUR
STATION
MW-9
0
N
(Approximate)
25
SCALE: 1"=50'
50
MW-10
91.94
DRAWN BY:PROJECT NUMBER:DRAWN DATE:BILLING GROUP:MLR25060801/22/182017GWMPETROLEUMCONCENTRATIONS IN GROUNDWATER(DECEMBER 7, 2017)MURPHY OIL USA, INC.FORMER SPUR STATION NO. 1211708 SOUTH GOLDSBORO STREETWILSON, NORTH CAROLINAP P M C O N S U L T A N T S , I N C . PPMwww.ppmco.comRAILROADSI
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VACANTPETROLEUMEQUIPMENTSERVICESKINGSMILLCONSTRUCTIONCOMPANYCULVERTSTORM DRAINCREEK
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MONITORING WELL LOCATIONF
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1
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1
GRASSYCONCRETECONCRETECONCRETECNLRED NUMBER INDICATES GWQS71EXCEEDANCEMW-312/07/17BDL3.502.01.101.102.100.92BDLBENZENE (μg/L)SEC-BUTYLBENZENE (μg/L)TERT-BUTYLBENZENE (μg/L)CIS-DICHLOROETHENE (μg/L)ISOPPROPYLBENZENE (μg/L)N-PROPYLBENZENE (μg/L)DI-ISOPROPYL ETHER (μg/L)1,2,4-TRIMETHYLBENZENE (μg/L)COULD NOT LOCATECNL71LEAD (μg/L)759ALIPHATICS (μg/L)199AROMATICS (μg/L)FIGURENUMBER40N(Approximate)25SCALE: 1"=50'50BDLTOLUENE (μg/L)BDLETHYLBENZENE (μg/L)BDLXYLENES (μg/L)BDLMTBE (μg/L)MW-512/07/17BDL1.801.701.40BDLBDLBDLBDLBENZENE (μg/L)SEC-BUTYLBENZENE (μg/L)TERT-BUTYLBENZENE (μg/L)CIS-DICHLOROETHENE (μg/L)ISOPPROPYLBENZENE (μg/L)N-PROPYLBENZENE (μg/L)DI-ISOPROPYL ETHER (μg/L)1,2,4-TRIMETHYLBENZENE (μg/L)103LEAD (μg/L)575ALIPHATICS (μg/L)113AROMATICS (μg/L)BDLTOLUENE (μg/L)BDLETHYLBENZENE (μg/L)BDLXYLENES (μg/L)BDLMTBE (μg/L)MW-612/07/171.704.502.01.406.202.10BDLBDLBENZENE (μg/L)SEC-BUTYLBENZENE (μg/L)TERT-BUTYLBENZENE (μg/L)CIS-DICHLOROETHENE (μg/L)ISOPPROPYLBENZENE (μg/L)N-PROPYLBENZENE (μg/L)DI-ISOPROPYL ETHER (μg/L)1,2,4-TRIMETHYLBENZENE (μg/L)664LEAD (μg/L)545ALIPHATICS (μg/L)228AROMATICS (μg/L)0.55TOLUENE (μg/L)0.53ETHYLBENZENE (μg/L)1.20XYLENES (μg/L)BDLMTBE (μg/L)MW-812/07/171.906.703.300.738.9015.202.401.30BENZENE (μg/L)SEC-BUTYLBENZENE (μg/L)TERT-BUTYLBENZENE (μg/L)CIS-DICHLOROETHENE (μg/L)ISOPPROPYLBENZENE (μg/L)N-PROPYLBENZENE (μg/L)DI-ISOPROPYL ETHER (μg/L)1,2,4-TRIMETHYLBENZENE (μg/L)84.80LEAD (μg/L)1,020ALIPHATICS (μg/L)317AROMATICS (μg/L)BDLTOLUENE (μg/L)BDLETHYLBENZENE (μg/L)BDLXYLENES (μg/L)5.20MTBE (μg/L)MW-1012/07/17BDLBDLBDLBDLBDLBDL12.40BDLBENZENE (μg/L)SEC-BUTYLBENZENE (μg/L)TERT-BUTYLBENZENE (μg/L)CIS-DICHLOROETHENE (μg/L)ISOPPROPYLBENZENE (μg/L)N-PROPYLBENZENE (μg/L)DI-ISOPROPYL ETHER (μg/L)1,2,4-TRIMETHYLBENZENE (μg/L)485LEAD (μg/L)88.50ALIPHATICS (μg/L)BDLAROMATICS (μg/L)BDLTOLUENE (μg/L)BDLETHYLBENZENE (μg/L)BDLXYLENES (μg/L)BDLMTBE (μg/L)MW-9ABANDONEDMW-1MW-2ABANDONEDCNLMW-4CNLMW-11SI
D
EW
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DRAWN BY:
FIGURE
NUMBER
PROJECT NUMBER:
DRAWN DATE:
BILLING GROUP:
MLR
250608
01/22/18
2017GWM
BENZENE
CONCENTRATIONS IN
GROUNDWATER
(DECEMBER 7, 2017)
MURPHY OIL USA, INC.
FORMER SPUR STATION NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA 5
P P M C O N S U L T A N T S , I N C . PPM www.ppmco.com
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MW-10
MW-8
SIDEWALKSIDEWALK
GRASS
VACANT
PETROLEUM
EQUIPMENT
SERVICES
KINGSMILL
CONSTRUCTION
COMPANY
CULVERT
STORM DRAIN
CREEK CREEKGRASSY
SL
O
P
E
WOODED
AREA
VACANT
PROPERTY
SELFCARWASH
ABANDONED
INDUSTRIAL
PROPERTY
MONITORING WELL LOCATIONFORMERSPUR
STATION
GRASSY
CONCRETE
CONCRETE
CONCRETE
NS
BENZENE CONCENTRATION (ug/L)
BELOW DETECTION LIMIT
1.70
NOT SAMPLEDNS
BDL
BENZENE CONCENTRATION CONTOUR
(ug/L)
1.0
BDL
1.90
SL
O
P
E
MW-2
ABANDONED
MW-4
NS
MW-11
NS
ABANDONED
MW-1
MW-5
MW-6
1.70NO. 1211
BDL
MW-9
MW-3
BDL1.00
N
(Approximate)
25
SCALE: 1"=50'
50
DRAWN BY:
FIGURE
NUMBER
PROJECT NUMBER:
DRAWN DATE:
BILLING GROUP:
MLR
250608
01/22/18
2017GWM
ALIPHATICS C5-C8
CONCENTRATIONS
IN GROUNDWATER
(DECEMBER 7, 2017)
MURPHY OIL USA, INC.
FORMER SPUR STATION NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA 6
P P M C O N S U L T A N T S , I N C . PPM www.ppmco.com
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MW-8
MW-5
SIDEWALKGRASS
VACANT
PETROLEUM
EQUIPMENT
SERVICES
KINGSMILL
CONSTRUCTION
COMPANY
CULVERT
STORM DRAIN
CREEK CREEKGRASSY
SL
O
P
E
SL
O
P
E
VACANT
PROPERTY
SELFCARWASH
ABANDONED
INDUSTRIAL
PROPERTY
MONITORING WELL LOCATIONFORMERSPUR
STATIONNO. 1211
CONCRETE
CONCRETE
NS
ALIPHATICS C5-C8 CONCENTRATION (ug/L)759
NOT SAMPLEDNS
ALIPHATICS C5-C8 CONCENTRATION)
CONTOUR (ug/L)
400
575
1,020
MW-9
88.50
MW-10
MW-2
ABANDONED
MW-3
759
CONCRETE
GRASSY
WOODED
AREA
MW-1
ABANDONED
MW-4
NS
MW-11
NSSIDEWALK
545
MW-6
400
8
0
0
0
N
(Approximate)
25
SCALE: 1"=50'
50
DRAWN BY:
FIGURE
NUMBER
PROJECT NUMBER:
DRAWN DATE:
BILLING GROUP:
MLR
250608
01/22/18
2017GWM
AROMATICS C9-C10
CONCENTRATIONS
IN GROUNDWATER
(DECEMBER 7, 2017)
MURPHY OIL USA, INC.
FORMER SPUR STATION NO. 1211
708 SOUTH GOLDSBORO STREET
WILSON, NORTH CAROLINA 7
P P M C O N S U L T A N T S , I N C . PPM www.ppmco.com
R
A
I
L
R
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MW-10
MW-8
SIDEWALKSIDEWALK
GRASS
VACANT
PETROLEUM
EQUIPMENT
SERVICES
KINGSMILL
CONSTRUCTION
COMPANY
CULVERT
STORM DRAIN
CREEK CREEKGRASSY
SL
O
P
E
SL
O
P
E
AREA
VACANT
PROPERTY
SELFCARWASH
ABANDONED
INDUSTRIAL
PROPERTY
MONITORING WELL LOCATIONFORMERSPUR
STATIONNO. 1211
GRASSY
CONCRETE
CONCRETE
NS
AROMATIC C9-C10 CONCENTRATION (ug/L)199
NOT SAMPLEDNS
CONTOUR (ug/L)
AROMATIC C9-C10 CONCENTRATION
BELOW DETECTION LIMITBDL
200
113
317
CONCRETE
MW-5
MW-6
228
NS
MW-11
NS
MW-4MW-3
199
ABANDONED
MW-2
WOODED
ABANDONED
MW-1
BDL
MW-9
0
N
(Approximate)
25
SCALE: 1"=50'
50
200

APPENDIX B TABLES
Well ID Event Date
Measured
Top of
Casing
Elevation
(ft)
Depth to
Product
Depth to
Water (ft-
BTOC)
Free Product
Thickness
(ft)
Groundwater
Elevation
(ft)
LSA 7/24/2001 NE 7.95 --91.67
GWM 12/7/2017 NE 7.20 --92.42
LSA 7/24/2001 NA
GWM 12/7/2017 99.87
LSA 7/24/2001 99.99 NE 6.98 --92.01*
GWM 12/7/2017 99.03 NE 6.18 --92.85
LSA 7/24/2001 98.72 NE 7.12 --91.60
GWM 12/7/2017 98.82 NE 6.92 --91.90
LSA 7/24/2001 93.23 NE 3.27 --89.96
GWM 12/7/2017 93.45 NE 7.00 --86.45
LSA 7/24/2001 93.63 NE 5.13 --88.50
GWM 12/7/2017
LSA 7/24/2001 98.77 NE 7.12 --91.65
GWM 12/7/2017 98.99 NE 7.05 --91.94
LSA 7/24/2001 99.36 NE 7.08 --92.28
GWM 12/7/2017 99.52
Notes:
The TOC elevations were re-surveyed during the May 3, 2008 groundwater monitoring event.
Re-surveyed TOC elevations that differed from the original elevation are shown in Bold .
708 SOUTH GOLDSBORO STREET, WILSON, NORTH CAROLINA
BTOC: Below top of casing
All elevations are based on an assigned elevation to land surface of 100 ft.
MW-8
MW-6
MW-9
TABLE 1
SUMMARY OF GROUNDWATER ELEVATION SURVEY DATA
Could Not Locate
FORMER SPUR 1211
MW-11
MW-10
Could Not Locate
Could Not Locate
MW-5
MW-4
99.62MW-3
Could Not Locate
Well &
Sample ID Event Date
Collected
LSA 7/24/2001 28.0 2.0 23.0 10.0 63.0 25.0 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 6.64 2,500 1,200 440
GWM 12/7/2017 BDL BDL BDL BDL --BDL NA BDL 3.50 2.0 1.10 1.10 2.10 0.92 BDL BDL BDL 71 759 171 199
GWM DUP 12/7/2017 BDL BDL BDL BDL --BDL NA BDL 3.10 2.0 1.10 1.0 2.0 0.97 BDL BDL BDL NA 696 164 188
MW-4 GWM 12/7/2017
LSA 7/24/2001 20.0 1.0 59.0 BDL 80.0 19.0 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 19.0 3,100 1,400 470
GWM 12/7/2017 BDL BDL BDL BDL --BDL NA BDL 1.80 1.70 1.40 BDL BDL BDL BDL BDL BDL 103 575 117 113
LSA 7/24/2001 4.0 2.0 2.0 5.0 13.0 12.0 BDL BDL BDL BDL BDL BDL BDL 10.0 BDL BDL BDL 226 1,400 750 300
GWM 12/7/2017 1.70 0.55 0.53 1.20 3.98 BDL NA BDL 4.50 2.0 1.40 6.20 2.10 BDL BDL BDL BDL 664 545 BDL 228
LSA 7/24/2001 3.0 BDL 51.0 42.0 96.0 35.0 BDL BDL BDL BDL BDL BDL BDL 10.0 BDL BDL BDL 11.3 2,600 1,700 600
GWM 12/7/2017 1.90 BDL BDL BDL 1.90 5.20 NA BDL 6.70 3.30 0.73 8.90 15.20 2.40 BDL 1.30 BDL 84.80 1,020 129 317
MW-9 GWM 12/7/2017
MW-10 GWM 12/7/2017 BDL BDL BDL BDL --BDL NA BDL BDL BDL BDL BDL BDL 12.40 BDL BDL BDL 485 88.50 BDL BDL
MW-11 GWM 12/7/2017 1.00 600 600 500 --20 6,000 70 70 70 70 70 70 70 6 400 400 15 400 700 200
5,000 260,000 84,500 85,500 --20,000 6,000,000 6,900 8,500 15,000 70,000 25,000 30,000 70,000 6,000 28,500 25,000 15,000 ------
Notes:
LSA: Limited Site Assessment
GWM: Groundwater Monitoring
GCL - Gross Contamination Levels (NCDEQ Guidance Rev. 4/16/2012)
GWQS - North Carolina Groundwater Quality Standard (NCDEQ Guidance Rev. 4/16/2012)Bold print indicates that the concentration exceed the North Carolina GWQS
Source(s):
All results are in milligrams per liter (µg/L), which is equivalent to parts per billion (ppb)
BDL - Below Detection Limits
708 SOUTH GOLDSBORO STREET, WILSON, NORTH CAROLINA
n-Butylbenzenesec-ButylbenzeneGCL (ug/L)cis-DichloroetheneXylenesAromatics C9-C10TABLE 2
Aliphatics C5-C81,3,5-TrimethylbenzeneContaminant of Concern
Aliphatics C9-C12PPM Project No. 250608-GWM
NA - Not Analyzed
PPM Consultants, Inc.
Only COCs with at least one concentration above detection limits are included
GWQS (ug/L)
VOC by 602/8021/8260 (µg/L)MADEP VPH (µg/L)MTBEAcetoneDi-Isopropyl ethertert-ButylbenzeneNOT SAMPLED (COULD NOT LOCATE)
SUMMARY OF GROUNDWATER ANALYTICAL DATA
Lead 239.2/6010 (ppb)FORMER SPUR 1211
Analytical Method BTEXMW-3 EthylbenzeneBenzeneTolueneNOT SAMPLED (COULD NOT LOCATE)
NOT SAMPLED (COULD NOT LOCATE)
MW-5
MW-6
MW-8 1,2,4-TrimethylbenzeneNaphthaleneIsoppropylbenzenen-Propylbenzene

APPENDIX C GROUNDWATER ANALYTICAL REPORT
#=CL#
December 22, 2017
LIMS USE: FR - RODNEY KILGORE
LIMS OBJECT ID: 92366283
92366283
Project:
Pace Project No.:
RE:
Rodney Kilgore
PPM Consultants
30704 Sergeant E.I. Thomas Dr
Spanish Fort, AL 36527
FORMER SPUR 1211 WILSON, NC
Dear Rodney Kilgore:
Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
cc:Carol Austin, PPM Consultants
Mr. Brad Weinischke, Murphy USA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92366283001 MW 3 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASER
SM 6200B 63 PASI-CSWB
92366283002 MW 5 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASER
SM 6200B 63 PASI-CSWB
92366283003 MW 6 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASER
SM 6200B 63 PASI-CSWB
92366283004 MW 8 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASER
SM 6200B 63 PASI-CSWB
92366283005 MW 10 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASER
SM 6200B 63 PASI-CCAH
92366283006 DUP MADEP VPH 5 PASI-CWDV
SM 6200B 63 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 3 Lab ID:92366283001 Collected:12/07/17 08:07 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)759 ug/L 12/12/17 20:12 N250.0 1
Aliphatic (C09-C12)171 ug/L 12/12/17 20:12 N250.0 1
Aromatic (C09-C10)199 ug/L 12/12/17 20:12 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)115 %12/12/17 20:12 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)94 %12/12/17 20:12 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead 71.0 ug/L 12/18/17 02:49 7439-92-112/12/17 03:405.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/13/17 14:02 71-43-20.50 1
Bromobenzene ND ug/L 12/13/17 14:02 108-86-10.50 1
Bromochloromethane ND ug/L 12/13/17 14:02 74-97-50.50 1
Bromodichloromethane ND ug/L 12/13/17 14:02 75-27-40.50 1
Bromoform ND ug/L 12/13/17 14:02 75-25-20.50 1
Bromomethane ND ug/L 12/13/17 14:02 74-83-95.0 1
n-Butylbenzene ND ug/L 12/13/17 14:02 104-51-80.50 1
sec-Butylbenzene 3.5 ug/L 12/13/17 14:02 135-98-80.50 1
tert-Butylbenzene 2.0 ug/L 12/13/17 14:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/13/17 14:02 56-23-50.50 1
Chlorobenzene ND ug/L 12/13/17 14:02 108-90-70.50 1
Chloroethane ND ug/L 12/13/17 14:02 75-00-31.0 1
Chloroform ND ug/L 12/13/17 14:02 67-66-30.50 1
Chloromethane ND ug/L 12/13/17 14:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/13/17 14:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/13/17 14:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/13/17 14:02 96-12-81.0 1
Dibromochloromethane ND ug/L 12/13/17 14:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/13/17 14:02 106-93-40.50 1
Dibromomethane ND ug/L 12/13/17 14:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/13/17 14:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/13/17 14:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/13/17 14:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/13/17 14:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/13/17 14:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/13/17 14:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/13/17 14:02 75-35-40.50 1
cis-1,2-Dichloroethene 1.1 ug/L 12/13/17 14:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/13/17 14:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/13/17 14:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/13/17 14:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/13/17 14:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/13/17 14:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/13/17 14:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/13/17 14:02 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 3 Lab ID:92366283001 Collected:12/07/17 08:07 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 0.92 ug/L 12/13/17 14:02 108-20-30.50 1
Ethylbenzene ND ug/L 12/13/17 14:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/13/17 14:02 87-68-32.0 1
Isopropylbenzene (Cumene)1.1 ug/L 12/13/17 14:02 98-82-80.50 1
Methylene Chloride ND ug/L 12/13/17 14:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/13/17 14:02 1634-04-40.50 1
Naphthalene ND ug/L 12/13/17 14:02 91-20-32.0 1
n-Propylbenzene 2.1 ug/L 12/13/17 14:02 103-65-10.50 1
Styrene ND ug/L 12/13/17 14:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/13/17 14:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/13/17 14:02 79-34-50.50 1
Tetrachloroethene ND ug/L 12/13/17 14:02 127-18-40.50 1
Toluene ND ug/L 12/13/17 14:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/13/17 14:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/17 14:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/13/17 14:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/13/17 14:02 79-00-50.50 1
Trichloroethene ND ug/L 12/13/17 14:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/13/17 14:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/13/17 14:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/13/17 14:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/13/17 14:02 108-67-80.50 1
Vinyl chloride ND ug/L 12/13/17 14:02 75-01-41.0 1
m&p-Xylene ND ug/L 12/13/17 14:02 179601-23-11.0 1
o-Xylene ND ug/L 12/13/17 14:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %12/13/17 14:02 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/13/17 14:02 460-00-470-130 1
Toluene-d8 (S)101 %12/13/17 14:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 5 Lab ID:92366283002 Collected:12/07/17 08:22 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)575 ug/L 12/12/17 20:41 N250.0 1
Aliphatic (C09-C12)117 ug/L 12/12/17 20:41 N250.0 1
Aromatic (C09-C10)113 ug/L 12/12/17 20:41 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)114 %12/12/17 20:41 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)96 %12/12/17 20:41 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead 103 ug/L 12/18/17 02:53 7439-92-112/12/17 03:405.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/13/17 14:19 71-43-20.50 1
Bromobenzene ND ug/L 12/13/17 14:19 108-86-10.50 1
Bromochloromethane ND ug/L 12/13/17 14:19 74-97-50.50 1
Bromodichloromethane ND ug/L 12/13/17 14:19 75-27-40.50 1
Bromoform ND ug/L 12/13/17 14:19 75-25-20.50 1
Bromomethane ND ug/L 12/13/17 14:19 74-83-95.0 1
n-Butylbenzene ND ug/L 12/13/17 14:19 104-51-80.50 1
sec-Butylbenzene 1.8 ug/L 12/13/17 14:19 135-98-80.50 1
tert-Butylbenzene 1.7 ug/L 12/13/17 14:19 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/13/17 14:19 56-23-50.50 1
Chlorobenzene ND ug/L 12/13/17 14:19 108-90-70.50 1
Chloroethane ND ug/L 12/13/17 14:19 75-00-31.0 1
Chloroform ND ug/L 12/13/17 14:19 67-66-30.50 1
Chloromethane ND ug/L 12/13/17 14:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/13/17 14:19 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/13/17 14:19 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/13/17 14:19 96-12-81.0 1
Dibromochloromethane ND ug/L 12/13/17 14:19 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/13/17 14:19 106-93-40.50 1
Dibromomethane ND ug/L 12/13/17 14:19 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/13/17 14:19 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/13/17 14:19 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/13/17 14:19 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/13/17 14:19 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/13/17 14:19 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/13/17 14:19 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/13/17 14:19 75-35-40.50 1
cis-1,2-Dichloroethene 1.4 ug/L 12/13/17 14:19 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/13/17 14:19 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/13/17 14:19 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/13/17 14:19 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/13/17 14:19 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/13/17 14:19 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/13/17 14:19 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/13/17 14:19 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 5 Lab ID:92366283002 Collected:12/07/17 08:22 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/13/17 14:19 108-20-30.50 1
Ethylbenzene ND ug/L 12/13/17 14:19 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/13/17 14:19 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/13/17 14:19 98-82-80.50 1
Methylene Chloride ND ug/L 12/13/17 14:19 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/13/17 14:19 1634-04-40.50 1
Naphthalene ND ug/L 12/13/17 14:19 91-20-32.0 1
n-Propylbenzene ND ug/L 12/13/17 14:19 103-65-10.50 1
Styrene ND ug/L 12/13/17 14:19 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/13/17 14:19 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/13/17 14:19 79-34-50.50 1
Tetrachloroethene ND ug/L 12/13/17 14:19 127-18-40.50 1
Toluene ND ug/L 12/13/17 14:19 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/13/17 14:19 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/17 14:19 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/13/17 14:19 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/13/17 14:19 79-00-50.50 1
Trichloroethene ND ug/L 12/13/17 14:19 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/13/17 14:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/13/17 14:19 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/13/17 14:19 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/13/17 14:19 108-67-80.50 1
Vinyl chloride ND ug/L 12/13/17 14:19 75-01-41.0 1
m&p-Xylene ND ug/L 12/13/17 14:19 179601-23-11.0 1
o-Xylene ND ug/L 12/13/17 14:19 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %12/13/17 14:19 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %12/13/17 14:19 460-00-470-130 1
Toluene-d8 (S)103 %12/13/17 14:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 6 Lab ID:92366283003 Collected:12/07/17 08:10 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)545 ug/L 12/12/17 21:10 N250.0 1
Aliphatic (C09-C12)ND ug/L 12/12/17 21:10 N250.0 1
Aromatic (C09-C10)228 ug/L 12/12/17 21:10 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %12/12/17 21:10 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)96 %12/12/17 21:10 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead 664 ug/L 12/18/17 02:57 7439-92-112/12/17 03:405.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 1.7 ug/L 12/13/17 14:36 71-43-20.50 1
Bromobenzene ND ug/L 12/13/17 14:36 108-86-10.50 1
Bromochloromethane ND ug/L 12/13/17 14:36 74-97-50.50 1
Bromodichloromethane ND ug/L 12/13/17 14:36 75-27-40.50 1
Bromoform ND ug/L 12/13/17 14:36 75-25-20.50 1
Bromomethane ND ug/L 12/13/17 14:36 74-83-95.0 1
n-Butylbenzene ND ug/L 12/13/17 14:36 104-51-80.50 1
sec-Butylbenzene 4.5 ug/L 12/13/17 14:36 135-98-80.50 1
tert-Butylbenzene 2.0 ug/L 12/13/17 14:36 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/13/17 14:36 56-23-50.50 1
Chlorobenzene ND ug/L 12/13/17 14:36 108-90-70.50 1
Chloroethane ND ug/L 12/13/17 14:36 75-00-31.0 1
Chloroform ND ug/L 12/13/17 14:36 67-66-30.50 1
Chloromethane ND ug/L 12/13/17 14:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/13/17 14:36 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/13/17 14:36 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/13/17 14:36 96-12-81.0 1
Dibromochloromethane ND ug/L 12/13/17 14:36 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/13/17 14:36 106-93-40.50 1
Dibromomethane ND ug/L 12/13/17 14:36 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/13/17 14:36 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/13/17 14:36 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/13/17 14:36 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/13/17 14:36 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/13/17 14:36 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/13/17 14:36 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/13/17 14:36 75-35-40.50 1
cis-1,2-Dichloroethene 1.4 ug/L 12/13/17 14:36 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/13/17 14:36 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/13/17 14:36 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/13/17 14:36 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/13/17 14:36 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/13/17 14:36 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/13/17 14:36 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/13/17 14:36 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 6 Lab ID:92366283003 Collected:12/07/17 08:10 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/13/17 14:36 108-20-30.50 1
Ethylbenzene 0.53 ug/L 12/13/17 14:36 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/13/17 14:36 87-68-32.0 1
Isopropylbenzene (Cumene)6.2 ug/L 12/13/17 14:36 98-82-80.50 1
Methylene Chloride ND ug/L 12/13/17 14:36 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/13/17 14:36 1634-04-40.50 1
Naphthalene ND ug/L 12/13/17 14:36 91-20-32.0 1
n-Propylbenzene 2.1 ug/L 12/13/17 14:36 103-65-10.50 1
Styrene ND ug/L 12/13/17 14:36 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/13/17 14:36 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/13/17 14:36 79-34-50.50 1
Tetrachloroethene ND ug/L 12/13/17 14:36 127-18-40.50 1
Toluene 0.55 ug/L 12/13/17 14:36 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/13/17 14:36 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/17 14:36 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/13/17 14:36 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/13/17 14:36 79-00-50.50 1
Trichloroethene ND ug/L 12/13/17 14:36 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/13/17 14:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/13/17 14:36 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/13/17 14:36 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/13/17 14:36 108-67-80.50 1
Vinyl chloride ND ug/L 12/13/17 14:36 75-01-41.0 1
m&p-Xylene 1.2 ug/L 12/13/17 14:36 179601-23-11.0 1
o-Xylene ND ug/L 12/13/17 14:36 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %12/13/17 14:36 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/13/17 14:36 460-00-470-130 1
Toluene-d8 (S)102 %12/13/17 14:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 8 Lab ID:92366283004 Collected:12/07/17 07:49 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)1020 ug/L 12/12/17 21:38 N250.0 1
Aliphatic (C09-C12)129 ug/L 12/12/17 21:38 N250.0 1
Aromatic (C09-C10)317 ug/L 12/12/17 21:38 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)118 %12/12/17 21:38 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)98 %12/12/17 21:38 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead 84.8 ug/L 12/18/17 03:01 7439-92-112/12/17 03:405.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 1.9 ug/L 12/13/17 14:54 71-43-20.50 1
Bromobenzene ND ug/L 12/13/17 14:54 108-86-10.50 1
Bromochloromethane ND ug/L 12/13/17 14:54 74-97-50.50 1
Bromodichloromethane ND ug/L 12/13/17 14:54 75-27-40.50 1
Bromoform ND ug/L 12/13/17 14:54 75-25-20.50 1
Bromomethane ND ug/L 12/13/17 14:54 74-83-95.0 1
n-Butylbenzene ND ug/L 12/13/17 14:54 104-51-80.50 1
sec-Butylbenzene 6.7 ug/L 12/13/17 14:54 135-98-80.50 1
tert-Butylbenzene 3.3 ug/L 12/13/17 14:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/13/17 14:54 56-23-50.50 1
Chlorobenzene ND ug/L 12/13/17 14:54 108-90-70.50 1
Chloroethane ND ug/L 12/13/17 14:54 75-00-31.0 1
Chloroform ND ug/L 12/13/17 14:54 67-66-30.50 1
Chloromethane ND ug/L 12/13/17 14:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/13/17 14:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/13/17 14:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/13/17 14:54 96-12-81.0 1
Dibromochloromethane ND ug/L 12/13/17 14:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/13/17 14:54 106-93-40.50 1
Dibromomethane ND ug/L 12/13/17 14:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/13/17 14:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/13/17 14:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/13/17 14:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/13/17 14:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/13/17 14:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/13/17 14:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/13/17 14:54 75-35-40.50 1
cis-1,2-Dichloroethene 0.73 ug/L 12/13/17 14:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/13/17 14:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/13/17 14:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/13/17 14:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/13/17 14:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/13/17 14:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/13/17 14:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/13/17 14:54 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 8 Lab ID:92366283004 Collected:12/07/17 07:49 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 2.4 ug/L 12/13/17 14:54 108-20-30.50 1
Ethylbenzene ND ug/L 12/13/17 14:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/13/17 14:54 87-68-32.0 1
Isopropylbenzene (Cumene)8.9 ug/L 12/13/17 14:54 98-82-80.50 1
Methylene Chloride ND ug/L 12/13/17 14:54 75-09-22.0 1
Methyl-tert-butyl ether 5.2 ug/L 12/13/17 14:54 1634-04-40.50 1
Naphthalene ND ug/L 12/13/17 14:54 91-20-32.0 1
n-Propylbenzene 15.2 ug/L 12/13/17 14:54 103-65-10.50 1
Styrene ND ug/L 12/13/17 14:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/13/17 14:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/13/17 14:54 79-34-50.50 1
Tetrachloroethene ND ug/L 12/13/17 14:54 127-18-40.50 1
Toluene ND ug/L 12/13/17 14:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/13/17 14:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/17 14:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/13/17 14:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/13/17 14:54 79-00-50.50 1
Trichloroethene ND ug/L 12/13/17 14:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/13/17 14:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/13/17 14:54 96-18-40.50 1
1,2,4-Trimethylbenzene 1.3 ug/L 12/13/17 14:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/13/17 14:54 108-67-80.50 1
Vinyl chloride ND ug/L 12/13/17 14:54 75-01-41.0 1
m&p-Xylene ND ug/L 12/13/17 14:54 179601-23-11.0 1
o-Xylene ND ug/L 12/13/17 14:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %12/13/17 14:54 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/13/17 14:54 460-00-470-130 1
Toluene-d8 (S)103 %12/13/17 14:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 10 Lab ID:92366283005 Collected:12/07/17 07:40 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)88.5 ug/L 12/12/17 19:44 N250.0 1
Aliphatic (C09-C12)ND ug/L 12/12/17 19:44 N250.0 1
Aromatic (C09-C10)ND ug/L 12/12/17 19:44 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)108 %12/12/17 19:44 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)99 %12/12/17 19:44 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead 485 ug/L 12/18/17 03:06 7439-92-112/12/17 03:405.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/10/17 06:54 71-43-20.50 1
Bromobenzene ND ug/L 12/10/17 06:54 108-86-10.50 1
Bromochloromethane ND ug/L 12/10/17 06:54 74-97-50.50 1
Bromodichloromethane ND ug/L 12/10/17 06:54 75-27-40.50 1
Bromoform ND ug/L 12/10/17 06:54 75-25-20.50 1
Bromomethane ND ug/L 12/10/17 06:54 74-83-95.0 1
n-Butylbenzene ND ug/L 12/10/17 06:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/10/17 06:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/10/17 06:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/10/17 06:54 56-23-50.50 1
Chlorobenzene ND ug/L 12/10/17 06:54 108-90-70.50 1
Chloroethane ND ug/L 12/10/17 06:54 75-00-31.0 1
Chloroform ND ug/L 12/10/17 06:54 67-66-30.50 1
Chloromethane ND ug/L 12/10/17 06:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/10/17 06:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/10/17 06:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/10/17 06:54 96-12-81.0 1
Dibromochloromethane ND ug/L 12/10/17 06:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/10/17 06:54 106-93-40.50 1
Dibromomethane ND ug/L 12/10/17 06:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/10/17 06:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/10/17 06:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/10/17 06:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/10/17 06:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/10/17 06:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/10/17 06:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/10/17 06:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/10/17 06:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/10/17 06:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/10/17 06:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/10/17 06:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/10/17 06:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/10/17 06:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/10/17 06:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/10/17 06:54 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
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Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:MW 10 Lab ID:92366283005 Collected:12/07/17 07:40 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 12.4 ug/L 12/10/17 06:54 108-20-30.50 1
Ethylbenzene ND ug/L 12/10/17 06:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/10/17 06:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/10/17 06:54 98-82-80.50 1
Methylene Chloride ND ug/L 12/10/17 06:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/10/17 06:54 1634-04-40.50 1
Naphthalene ND ug/L 12/10/17 06:54 91-20-32.0 1
n-Propylbenzene ND ug/L 12/10/17 06:54 103-65-10.50 1
Styrene ND ug/L 12/10/17 06:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/10/17 06:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/10/17 06:54 79-34-50.50 1
Tetrachloroethene ND ug/L 12/10/17 06:54 127-18-40.50 1
Toluene ND ug/L 12/10/17 06:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/10/17 06:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/10/17 06:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/10/17 06:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/10/17 06:54 79-00-50.50 1
Trichloroethene ND ug/L 12/10/17 06:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/10/17 06:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/10/17 06:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/10/17 06:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/10/17 06:54 108-67-80.50 1
Vinyl chloride ND ug/L 12/10/17 06:54 75-01-41.0 1
m&p-Xylene ND ug/L 12/10/17 06:54 179601-23-11.0 1
o-Xylene ND ug/L 12/10/17 06:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %12/10/17 06:54 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/10/17 06:54 460-00-470-130 1
Toluene-d8 (S)99 %12/10/17 06:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:DUP Lab ID:92366283006 Collected:12/07/17 00:00 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)696 ug/L 12/12/17 22:07 N250.0 1
Aliphatic (C09-C12)164 ug/L 12/12/17 22:07 N250.0 1
Aromatic (C09-C10)188 ug/L 12/12/17 22:07 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)119 %12/12/17 22:07 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)99 %12/12/17 22:07 460-00-470-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/13/17 15:11 71-43-20.50 1
Bromobenzene ND ug/L 12/13/17 15:11 108-86-10.50 1
Bromochloromethane ND ug/L 12/13/17 15:11 74-97-50.50 1
Bromodichloromethane ND ug/L 12/13/17 15:11 75-27-40.50 1
Bromoform ND ug/L 12/13/17 15:11 75-25-20.50 1
Bromomethane ND ug/L 12/13/17 15:11 74-83-95.0 1
n-Butylbenzene ND ug/L 12/13/17 15:11 104-51-80.50 1
sec-Butylbenzene 3.1 ug/L 12/13/17 15:11 135-98-80.50 1
tert-Butylbenzene 2.0 ug/L 12/13/17 15:11 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/13/17 15:11 56-23-50.50 1
Chlorobenzene ND ug/L 12/13/17 15:11 108-90-70.50 1
Chloroethane ND ug/L 12/13/17 15:11 75-00-31.0 1
Chloroform ND ug/L 12/13/17 15:11 67-66-30.50 1
Chloromethane ND ug/L 12/13/17 15:11 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/13/17 15:11 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/13/17 15:11 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/13/17 15:11 96-12-81.0 1
Dibromochloromethane ND ug/L 12/13/17 15:11 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/13/17 15:11 106-93-40.50 1
Dibromomethane ND ug/L 12/13/17 15:11 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/13/17 15:11 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/13/17 15:11 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/13/17 15:11 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/13/17 15:11 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/13/17 15:11 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/13/17 15:11 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/13/17 15:11 75-35-40.50 1
cis-1,2-Dichloroethene 1.1 ug/L 12/13/17 15:11 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/13/17 15:11 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/13/17 15:11 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/13/17 15:11 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/13/17 15:11 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/13/17 15:11 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/13/17 15:11 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/13/17 15:11 10061-02-60.50 1
Diisopropyl ether 0.97 ug/L 12/13/17 15:11 108-20-30.50 1
Ethylbenzene ND ug/L 12/13/17 15:11 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/13/17 15:11 87-68-32.0 1
Isopropylbenzene (Cumene)1.0 ug/L 12/13/17 15:11 98-82-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Sample:DUP Lab ID:92366283006 Collected:12/07/17 00:00 Received:12/08/17 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Methylene Chloride ND ug/L 12/13/17 15:11 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/13/17 15:11 1634-04-40.50 1
Naphthalene ND ug/L 12/13/17 15:11 91-20-32.0 1
n-Propylbenzene 2.0 ug/L 12/13/17 15:11 103-65-10.50 1
Styrene ND ug/L 12/13/17 15:11 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/13/17 15:11 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/13/17 15:11 79-34-50.50 1
Tetrachloroethene ND ug/L 12/13/17 15:11 127-18-40.50 1
Toluene ND ug/L 12/13/17 15:11 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/13/17 15:11 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/13/17 15:11 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/13/17 15:11 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/13/17 15:11 79-00-50.50 1
Trichloroethene ND ug/L 12/13/17 15:11 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/13/17 15:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/13/17 15:11 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/13/17 15:11 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/13/17 15:11 108-67-80.50 1
Vinyl chloride ND ug/L 12/13/17 15:11 75-01-41.0 1
m&p-Xylene ND ug/L 12/13/17 15:11 179601-23-11.0 1
o-Xylene ND ug/L 12/13/17 15:11 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)110 %12/13/17 15:11 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/13/17 15:11 460-00-470-130 1
Toluene-d8 (S)103 %12/13/17 15:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
390116
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283005, 92366283006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2164693
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283005, 92366283006
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N212/09/17 11:40
Aliphatic (C09-C12)ug/L ND 50.0 N212/09/17 11:40
Aromatic (C09-C10)ug/L ND 50.0 N212/09/17 11:40
4-Bromofluorobenzene (FID) (S)%85 70-130 12/09/17 11:40
4-Bromofluorobenzene (PID) (S)%80 70-130 12/09/17 11:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2164694LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2164695
Aliphatic (C05-C08)ug/L 231 N23007770-13090270 16 25
Aliphatic (C09-C12)ug/L 271 N23009030-13090269 1 25
Aromatic (C09-C10)ug/L 79.7 N21008070-1309291.8 14 25
4-Bromofluorobenzene (FID) (S)%85 70-13091
4-Bromofluorobenzene (PID) (S)%80 70-13087
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
390341
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2165865
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283005
Matrix:Water
Analyzed
Lead ug/L ND 5.0 12/18/17 01:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2165866LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 460500 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2165867MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92366546001
2165868
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L M6500-1880 75-125-300 2500474000464000472000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
390142
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92366283005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2164756
Associated Lab Samples:92366283005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/10/17 05:45
1,1,1-Trichloroethane ug/L ND 0.50 12/10/17 05:45
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/10/17 05:45
1,1,2-Trichloroethane ug/L ND 0.50 12/10/17 05:45
1,1-Dichloroethane ug/L ND 0.50 12/10/17 05:45
1,1-Dichloroethene ug/L ND 0.50 12/10/17 05:45
1,1-Dichloropropene ug/L ND 0.50 12/10/17 05:45
1,2,3-Trichlorobenzene ug/L ND 2.0 12/10/17 05:45
1,2,3-Trichloropropane ug/L ND 0.50 12/10/17 05:45
1,2,4-Trichlorobenzene ug/L ND 2.0 12/10/17 05:45
1,2,4-Trimethylbenzene ug/L ND 0.50 12/10/17 05:45
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/10/17 05:45
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/10/17 05:45
1,2-Dichlorobenzene ug/L ND 0.50 12/10/17 05:45
1,2-Dichloroethane ug/L ND 0.50 12/10/17 05:45
1,2-Dichloropropane ug/L ND 0.50 12/10/17 05:45
1,3,5-Trimethylbenzene ug/L ND 0.50 12/10/17 05:45
1,3-Dichlorobenzene ug/L ND 0.50 12/10/17 05:45
1,3-Dichloropropane ug/L ND 0.50 12/10/17 05:45
1,4-Dichlorobenzene ug/L ND 0.50 12/10/17 05:45
2,2-Dichloropropane ug/L ND 0.50 12/10/17 05:45
2-Chlorotoluene ug/L ND 0.50 12/10/17 05:45
4-Chlorotoluene ug/L ND 0.50 12/10/17 05:45
Benzene ug/L ND 0.50 12/10/17 05:45
Bromobenzene ug/L ND 0.50 12/10/17 05:45
Bromochloromethane ug/L ND 0.50 12/10/17 05:45
Bromodichloromethane ug/L ND 0.50 12/10/17 05:45
Bromoform ug/L ND 0.50 12/10/17 05:45
Bromomethane ug/L ND 5.0 12/10/17 05:45
Carbon tetrachloride ug/L ND 0.50 12/10/17 05:45
Chlorobenzene ug/L ND 0.50 12/10/17 05:45
Chloroethane ug/L ND 1.0 12/10/17 05:45
Chloroform ug/L ND 0.50 12/10/17 05:45
Chloromethane ug/L ND 1.0 12/10/17 05:45
cis-1,2-Dichloroethene ug/L ND 0.50 12/10/17 05:45
cis-1,3-Dichloropropene ug/L ND 0.50 12/10/17 05:45
Dibromochloromethane ug/L ND 0.50 12/10/17 05:45
Dibromomethane ug/L ND 0.50 12/10/17 05:45
Dichlorodifluoromethane ug/L ND 0.50 12/10/17 05:45
Diisopropyl ether ug/L ND 0.50 12/10/17 05:45
Ethylbenzene ug/L ND 0.50 12/10/17 05:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2164756
Associated Lab Samples:92366283005
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/10/17 05:45
Isopropylbenzene (Cumene)ug/L ND 0.50 12/10/17 05:45
m&p-Xylene ug/L ND 1.0 12/10/17 05:45
Methyl-tert-butyl ether ug/L ND 0.50 12/10/17 05:45
Methylene Chloride ug/L ND 2.0 12/10/17 05:45
n-Butylbenzene ug/L ND 0.50 12/10/17 05:45
n-Propylbenzene ug/L ND 0.50 12/10/17 05:45
Naphthalene ug/L ND 2.0 12/10/17 05:45
o-Xylene ug/L ND 0.50 12/10/17 05:45
sec-Butylbenzene ug/L ND 0.50 12/10/17 05:45
Styrene ug/L ND 0.50 12/10/17 05:45
tert-Butylbenzene ug/L ND 0.50 12/10/17 05:45
Tetrachloroethene ug/L ND 0.50 12/10/17 05:45
Toluene ug/L ND 0.50 12/10/17 05:45
trans-1,2-Dichloroethene ug/L ND 0.50 12/10/17 05:45
trans-1,3-Dichloropropene ug/L ND 0.50 12/10/17 05:45
Trichloroethene ug/L ND 0.50 12/10/17 05:45
Trichlorofluoromethane ug/L ND 1.0 12/10/17 05:45
Vinyl chloride ug/L ND 1.0 12/10/17 05:45
1,2-Dichloroethane-d4 (S)%97 70-130 12/10/17 05:45
4-Bromofluorobenzene (S)%96 70-130 12/10/17 05:45
Toluene-d8 (S)%98 70-130 12/10/17 05:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2164757LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.150 106 60-140
1,1,1-Trichloroethane ug/L 51.450 103 60-140
1,1,2,2-Tetrachloroethane ug/L 51.450 103 60-140
1,1,2-Trichloroethane ug/L 51.450 103 60-140
1,1-Dichloroethane ug/L 49.350 99 60-140
1,1-Dichloroethene ug/L 50.750 101 60-140
1,1-Dichloropropene ug/L 49.150 98 60-140
1,2,3-Trichlorobenzene ug/L 53.450 107 60-140
1,2,3-Trichloropropane ug/L 49.650 99 60-140
1,2,4-Trichlorobenzene ug/L 53.250 106 60-140
1,2,4-Trimethylbenzene ug/L 51.750 103 60-140
1,2-Dibromo-3-chloropropane ug/L 54.150 108 60-140
1,2-Dibromoethane (EDB)ug/L 52.550 105 60-140
1,2-Dichlorobenzene ug/L 51.850 104 60-140
1,2-Dichloroethane ug/L 44.450 89 60-140
1,2-Dichloropropane ug/L 52.350 105 60-140
1,3,5-Trimethylbenzene ug/L 52.950 106 60-140
1,3-Dichlorobenzene ug/L 51.350 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2164757LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.650 105 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 44.450 89 60-140
2-Chlorotoluene ug/L 51.350 103 60-140
4-Chlorotoluene ug/L 51.350 103 60-140
Benzene ug/L 50.450 101 60-140
Bromobenzene ug/L 52.550 105 60-140
Bromochloromethane ug/L 48.850 98 60-140
Bromodichloromethane ug/L 53.150 106 60-140
Bromoform ug/L 41.350 83 60-140
Bromomethane ug/L 35.850 72 60-140
Carbon tetrachloride ug/L 54.650 109 60-140
Chlorobenzene ug/L 50.750 101 60-140
Chloroethane ug/L 53.650 107 60-140
Chloroform ug/L 47.650 95 60-140
Chloromethane ug/L 42.750 85 60-140
cis-1,2-Dichloroethene ug/L 50.950 102 60-140
cis-1,3-Dichloropropene ug/L 52.250 104 60-140
Dibromochloromethane ug/L 54.050 108 60-140
Dibromomethane ug/L 49.650 99 60-140
Dichlorodifluoromethane ug/L 38.450 77 60-140
Diisopropyl ether ug/L 51.250 102 60-140
Ethylbenzene ug/L 51.850 104 60-140
Hexachloro-1,3-butadiene ug/L 56.150 112 60-140
Isopropylbenzene (Cumene)ug/L 53.950 108 60-140
m&p-Xylene ug/L 101100 101 60-140
Methyl-tert-butyl ether ug/L 46.650 93 60-140
Methylene Chloride ug/L 45.850 92 60-140
n-Butylbenzene ug/L 53.350 107 60-140
n-Propylbenzene ug/L 53.950 108 60-140
Naphthalene ug/L 53.450 107 60-140
o-Xylene ug/L 51.450 103 60-140
sec-Butylbenzene ug/L 54.950 110 60-140
Styrene ug/L 51.150 102 60-140
tert-Butylbenzene ug/L 44.750 89 60-140
Tetrachloroethene ug/L 51.350 103 60-140
Toluene ug/L 51.650 103 60-140
trans-1,2-Dichloroethene ug/L 50.350 101 60-140
trans-1,3-Dichloropropene ug/L 51.450 103 60-140
Trichloroethene ug/L 50.750 101 60-140
Trichlorofluoromethane ug/L 47.550 95 60-140
Vinyl chloride ug/L 52.550 105 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2165027MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92366281009
2165028
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 117 60-140115 220ND23.5 23.0
1,1,1-Trichloroethane ug/L 20 120 60-140118 120ND24.0 23.7
1,1,2,2-Tetrachloroethane ug/L 20 110 60-140110 120ND22.0 21.9
1,1,2-Trichloroethane ug/L 20 111 60-140113 220ND22.2 22.7
1,1-Dichloroethane ug/L 20 116 60-140115 120ND23.3 23.0
1,1-Dichloroethene ug/L 20 117 60-140119 120ND23.4 23.8
1,1-Dichloropropene ug/L 20 118 60-140118 020ND23.5 23.6
1,2,3-Trichlorobenzene ug/L 20 115 60-140113 220ND23.0 22.6
1,2,3-Trichloropropane ug/L 20 107 60-140109 220ND21.4 21.8
1,2,4-Trichlorobenzene ug/L 20 115 60-140116 120ND22.9 23.2
1,2,4-Trimethylbenzene ug/L 20 119 60-140114 420ND23.8 22.9
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140104 320ND21.4 20.8
1,2-Dibromoethane (EDB)ug/L 20 115 60-140111 320ND22.9 22.2
1,2-Dichlorobenzene ug/L 20 115 60-140110 520ND23.1 21.9
1,2-Dichloroethane ug/L 20 101 60-140100 120ND20.2 19.9
1,2-Dichloropropane ug/L 20 121 60-140117 420ND24.3 23.4
1,3,5-Trimethylbenzene ug/L 20 119 60-140116 320ND23.9 23.2
1,3-Dichlorobenzene ug/L 20 115 60-140111 420ND23.0 22.2
1,3-Dichloropropane ug/L 20 119 60-140115 320ND23.7 23.0
1,4-Dichlorobenzene ug/L 20 111 60-140107 420ND22.3 21.4
2,2-Dichloropropane ug/L 20 111 60-140113 220ND22.2 22.6
2-Chlorotoluene ug/L 20 119 60-140113 520ND23.8 22.6
4-Chlorotoluene ug/L 20 118 60-140115 220ND23.5 23.0
Benzene ug/L 20 116 60-140113 320ND23.2 22.6
Bromobenzene ug/L 20 118 60-140113 420ND23.6 22.7
Bromochloromethane ug/L 20 110 60-140108 220ND22.0 21.6
Bromodichloromethane ug/L 20 117 60-140114 320ND23.4 22.8
Bromoform ug/L 20 94 60-14091 420ND18.9 18.1
Bromomethane ug/L 20 108 60-140104 320ND21.5 20.9
Carbon tetrachloride ug/L 20 123 60-140122 120ND24.5 24.4
Chlorobenzene ug/L 20 116 60-140112 320ND23.2 22.5
Chloroethane ug/L 20 123 60-140119 320ND24.5 23.7
Chloroform ug/L 20 109 60-140109 020ND21.9 21.8
Chloromethane ug/L 20 111 60-140111 120ND22.3 22.1
cis-1,2-Dichloroethene ug/L 20 120 60-140117 320ND24.1 23.4
cis-1,3-Dichloropropene ug/L 20 120 60-140116 320ND24.0 23.2
Dibromochloromethane ug/L 20 113 60-140112 120ND22.5 22.4
Dibromomethane ug/L 20 109 60-140105 320ND21.8 21.1
Dichlorodifluoromethane ug/L 20 97 60-14098 020ND19.5 19.5
Diisopropyl ether ug/L 20 118 60-140115 220ND23.6 23.0
Ethylbenzene ug/L 20 120 60-140117 220ND23.9 23.4
Hexachloro-1,3-butadiene ug/L 20 126 60-140130 320ND25.1 25.9
Isopropylbenzene (Cumene)ug/L 20 122 60-140118 320ND24.5 23.6
m&p-Xylene ug/L 40 115 60-140114 140ND46.0 45.4
Methyl-tert-butyl ether ug/L 20 106 60-140102 420ND21.2 20.4
Methylene Chloride ug/L 20 106 60-140106 020ND21.3 21.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2165027MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92366281009
2165028
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 124 60-140120 420ND24.9 24.0
n-Propylbenzene ug/L 20 124 60-140122 220ND24.7 24.4
Naphthalene ug/L 20 112 60-140113 120ND22.3 22.6
o-Xylene ug/L 20 116 60-140114 120ND23.2 22.9
sec-Butylbenzene ug/L 20 127 60-140123 420ND25.4 24.5
Styrene ug/L 20 117 60-140114 220ND23.3 22.8
tert-Butylbenzene ug/L 20 103 60-140101 220ND20.7 20.2
Tetrachloroethene ug/L 20 117 60-140113 420ND23.4 22.6
Toluene ug/L 20 116 60-140115 120ND23.3 23.0
trans-1,2-Dichloroethene ug/L 20 118 60-140116 220ND23.6 23.1
trans-1,3-Dichloropropene ug/L 20 115 60-140112 220ND23.0 22.4
Trichloroethene ug/L 20 114 60-140113 120ND22.8 22.5
Trichlorofluoromethane ug/L 20 113 60-140113 020ND22.5 22.6
Vinyl chloride ug/L 20 128 60-140125 220ND25.6 25.0
1,2-Dichloroethane-d4 (S)%99 70-13099
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%100 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
390630
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2167375
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/13/17 12:36
1,1,1-Trichloroethane ug/L ND 0.50 12/13/17 12:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/13/17 12:36
1,1,2-Trichloroethane ug/L ND 0.50 12/13/17 12:36
1,1-Dichloroethane ug/L ND 0.50 12/13/17 12:36
1,1-Dichloroethene ug/L ND 0.50 12/13/17 12:36
1,1-Dichloropropene ug/L ND 0.50 12/13/17 12:36
1,2,3-Trichlorobenzene ug/L ND 2.0 12/13/17 12:36
1,2,3-Trichloropropane ug/L ND 0.50 12/13/17 12:36
1,2,4-Trichlorobenzene ug/L ND 2.0 12/13/17 12:36
1,2,4-Trimethylbenzene ug/L ND 0.50 12/13/17 12:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/13/17 12:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/13/17 12:36
1,2-Dichlorobenzene ug/L ND 0.50 12/13/17 12:36
1,2-Dichloroethane ug/L ND 0.50 12/13/17 12:36
1,2-Dichloropropane ug/L ND 0.50 12/13/17 12:36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/13/17 12:36
1,3-Dichlorobenzene ug/L ND 0.50 12/13/17 12:36
1,3-Dichloropropane ug/L ND 0.50 12/13/17 12:36
1,4-Dichlorobenzene ug/L ND 0.50 12/13/17 12:36
2,2-Dichloropropane ug/L ND 0.50 12/13/17 12:36
2-Chlorotoluene ug/L ND 0.50 12/13/17 12:36
4-Chlorotoluene ug/L ND 0.50 12/13/17 12:36
Benzene ug/L ND 0.50 12/13/17 12:36
Bromobenzene ug/L ND 0.50 12/13/17 12:36
Bromochloromethane ug/L ND 0.50 12/13/17 12:36
Bromodichloromethane ug/L ND 0.50 12/13/17 12:36
Bromoform ug/L ND 0.50 12/13/17 12:36
Bromomethane ug/L ND 5.0 12/13/17 12:36
Carbon tetrachloride ug/L ND 0.50 12/13/17 12:36
Chlorobenzene ug/L ND 0.50 12/13/17 12:36
Chloroethane ug/L ND 1.0 12/13/17 12:36
Chloroform ug/L ND 0.50 12/13/17 12:36
Chloromethane ug/L ND 1.0 12/13/17 12:36
cis-1,2-Dichloroethene ug/L ND 0.50 12/13/17 12:36
cis-1,3-Dichloropropene ug/L ND 0.50 12/13/17 12:36
Dibromochloromethane ug/L ND 0.50 12/13/17 12:36
Dibromomethane ug/L ND 0.50 12/13/17 12:36
Dichlorodifluoromethane ug/L ND 0.50 12/13/17 12:36
Diisopropyl ether ug/L ND 0.50 12/13/17 12:36
Ethylbenzene ug/L ND 0.50 12/13/17 12:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2167375
Associated Lab Samples:92366283001, 92366283002, 92366283003, 92366283004, 92366283006
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/13/17 12:36
Isopropylbenzene (Cumene)ug/L ND 0.50 12/13/17 12:36
m&p-Xylene ug/L ND 1.0 12/13/17 12:36
Methyl-tert-butyl ether ug/L ND 0.50 12/13/17 12:36
Methylene Chloride ug/L ND 2.0 12/13/17 12:36
n-Butylbenzene ug/L ND 0.50 12/13/17 12:36
n-Propylbenzene ug/L ND 0.50 12/13/17 12:36
Naphthalene ug/L ND 2.0 12/13/17 12:36
o-Xylene ug/L ND 0.50 12/13/17 12:36
sec-Butylbenzene ug/L ND 0.50 12/13/17 12:36
Styrene ug/L ND 0.50 12/13/17 12:36
tert-Butylbenzene ug/L ND 0.50 12/13/17 12:36
Tetrachloroethene ug/L ND 0.50 12/13/17 12:36
Toluene ug/L ND 0.50 12/13/17 12:36
trans-1,2-Dichloroethene ug/L ND 0.50 12/13/17 12:36
trans-1,3-Dichloropropene ug/L ND 0.50 12/13/17 12:36
Trichloroethene ug/L ND 0.50 12/13/17 12:36
Trichlorofluoromethane ug/L ND 1.0 12/13/17 12:36
Vinyl chloride ug/L ND 1.0 12/13/17 12:36
1,2-Dichloroethane-d4 (S)%102 70-130 12/13/17 12:36
4-Bromofluorobenzene (S)%98 70-130 12/13/17 12:36
Toluene-d8 (S)%98 70-130 12/13/17 12:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2167376LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 60-140
1,1,1-Trichloroethane ug/L 54.750 109 60-140
1,1,2,2-Tetrachloroethane ug/L 49.550 99 60-140
1,1,2-Trichloroethane ug/L 51.450 103 60-140
1,1-Dichloroethane ug/L 52.050 104 60-140
1,1-Dichloroethene ug/L 53.150 106 60-140
1,1-Dichloropropene ug/L 52.550 105 60-140
1,2,3-Trichlorobenzene ug/L 51.850 104 60-140
1,2,3-Trichloropropane ug/L 50.050 100 60-140
1,2,4-Trichlorobenzene ug/L 52.650 105 60-140
1,2,4-Trimethylbenzene ug/L 52.350 105 60-140
1,2-Dibromo-3-chloropropane ug/L 51.050 102 60-140
1,2-Dibromoethane (EDB)ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 51.750 103 60-140
1,2-Dichloroethane ug/L 47.850 96 60-140
1,2-Dichloropropane ug/L 53.150 106 60-140
1,3,5-Trimethylbenzene ug/L 53.150 106 60-140
1,3-Dichlorobenzene ug/L 51.450 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2167376LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 53.050 106 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 59.250 118 60-140
2-Chlorotoluene ug/L 51.650 103 60-140
4-Chlorotoluene ug/L 52.150 104 60-140
Benzene ug/L 51.250 102 60-140
Bromobenzene ug/L 51.950 104 60-140
Bromochloromethane ug/L 49.750 99 60-140
Bromodichloromethane ug/L 55.150 110 60-140
Bromoform ug/L 40.050 80 60-140
Bromomethane ug/L 37.550 75 60-140
Carbon tetrachloride ug/L 57.150 114 60-140
Chlorobenzene ug/L 51.050 102 60-140
Chloroethane ug/L 53.350 107 60-140
Chloroform ug/L 50.050 100 60-140
Chloromethane ug/L 50.150 100 60-140
cis-1,2-Dichloroethene ug/L 52.950 106 60-140
cis-1,3-Dichloropropene ug/L 56.150 112 60-140
Dibromochloromethane ug/L 52.850 106 60-140
Dibromomethane ug/L 50.450 101 60-140
Dichlorodifluoromethane ug/L 54.950 110 60-140
Diisopropyl ether ug/L 52.850 106 60-140
Ethylbenzene ug/L 52.150 104 60-140
Hexachloro-1,3-butadiene ug/L 57.750 115 60-140
Isopropylbenzene (Cumene)ug/L 53.550 107 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 46.950 94 60-140
Methylene Chloride ug/L 46.350 93 60-140
n-Butylbenzene ug/L 55.250 110 60-140
n-Propylbenzene ug/L 53.550 107 60-140
Naphthalene ug/L 50.450 101 60-140
o-Xylene ug/L 51.150 102 60-140
sec-Butylbenzene ug/L 54.550 109 60-140
Styrene ug/L 52.150 104 60-140
tert-Butylbenzene ug/L 44.950 90 60-140
Tetrachloroethene ug/L 52.950 106 60-140
Toluene ug/L 51.350 103 60-140
trans-1,2-Dichloroethene ug/L 52.250 104 60-140
trans-1,3-Dichloropropene ug/L 54.550 109 60-140
Trichloroethene ug/L 51.750 103 60-140
Trichlorofluoromethane ug/L 52.650 105 60-140
Vinyl chloride ug/L 58.250 116 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2167377MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92366001003
2167378
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 108 60-140123 132000ND21702460
1,1,1-Trichloroethane ug/L 2000 117 60-140123 52000ND23502460
1,1,2,2-Tetrachloroethane ug/L 2000 99 60-140113 132000ND19802250
1,1,2-Trichloroethane ug/L 2000 107 60-140117 92000ND21502340
1,1-Dichloroethane ug/L 2000 109 60-140112 32000ND21902250
1,1-Dichloroethene ug/L 2000 112 60-140120 72000ND22502400
1,1-Dichloropropene ug/L 2000 111 60-140119 72000ND22202380
1,2,3-Trichlorobenzene ug/L 2000 100 60-140116 152000ND20002320
1,2,3-Trichloropropane ug/L 2000 99 60-140116 152000ND19902320
1,2,4-Trichlorobenzene ug/L 2000 103 60-140114 102000ND20602280
1,2,4-Trimethylbenzene ug/L 2000 107 60-140128 13200079329403350
1,2-Dibromo-3-chloropropane ug/L 2000 98 60-140113 142000ND19602250
1,2-Dibromoethane (EDB)ug/L 2000 103 60-140117 12200090.2 2160 2430
1,2-Dichlorobenzene ug/L 2000 105 60-140118 112000ND21002350
1,2-Dichloroethane ug/L 2000 100 60-140102 22000ND20502080
1,2-Dichloropropane ug/L 2000 112 60-140124 112000ND22302490
1,3,5-Trimethylbenzene ug/L 2000 123 60-140137 112000ND24602750
1,3-Dichlorobenzene ug/L 2000 104 60-140116 112000ND20702320
1,3-Dichloropropane ug/L 2000 109 60-140119 92000ND21702390
1,4-Dichlorobenzene ug/L 2000 101 60-140113 112000ND20202250
2,2-Dichloropropane ug/L 2000 103 60-140110 72000ND20502200
2-Chlorotoluene ug/L 2000 107 60-140115 72000ND21302290
4-Chlorotoluene ug/L 2000 104 60-140122 152000ND20902430
Benzene ug/L 2000 97 60-140118 52000681087609170
Bromobenzene ug/L 2000 106 60-140121 132000ND21202420
Bromochloromethane ug/L 2000 102 60-140109 72000ND20402180
Bromodichloromethane ug/L 2000 112 60-140118 52000ND22402360
Bromoform ug/L 2000 84 60-14089 62000ND16701780
Bromomethane ug/L M120005960-14066 112000ND11901330
Carbon tetrachloride ug/L 2000 123 60-140134 92000ND24602690
Chlorobenzene ug/L 2000 107 60-140117 92000ND21402350
Chloroethane ug/L 2000 128 60-140128 02000ND25602560
Chloroform ug/L 2000 108 60-140110 22000ND21602200
Chloromethane ug/L 2000 104 60-140111 62000ND20902220
cis-1,2-Dichloroethene ug/L 2000 112 60-140117 42000ND22502340
cis-1,3-Dichloropropene ug/L 2000 110 60-140118 72000ND22002370
Dibromochloromethane ug/L 2000 104 60-140115 102000ND20802290
Dibromomethane ug/L 2000 103 60-140109 62000ND20602190
Dichlorodifluoromethane ug/L 2000 119 60-140127 62000ND23802530
Diisopropyl ether ug/L 2000 110 60-140114 32000ND22002270
Ethylbenzene ug/L 2000 107 60-140126 102000153036604060
Hexachloro-1,3-butadiene ug/L 2000 112 60-140128 142000ND22302560
Isopropylbenzene (Cumene)ug/L 2000 113 60-140125 10200072.8 2340 2570
m&p-Xylene ug/L 4000 103 60-140122 104000336074708260
Methyl-tert-butyl ether ug/L 2000 99 60-140103 42000ND19802060
Methylene Chloride ug/L 2000 105 60-140106 12000ND21002120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2167377MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92366001003
2167378
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 2000 110 60-140124 122000ND22002490
n-Propylbenzene ug/L 2000 118 60-140132 112000ND23702650
Naphthalene ug/L 2000 99 60-140118 15200042224002780
o-Xylene ug/L 2000 102 60-140123 102000195040004410
sec-Butylbenzene ug/L 2000 113 60-140127 122000ND22502540
Styrene ug/L 2000 107 60-140118 102000ND21402370
tert-Butylbenzene ug/L 2000 93 60-140106 142000ND18502120
Tetrachloroethene ug/L 2000 109 60-140123 132000ND21702470
Toluene ug/L 2000 88 60-140123 62000102001200012700
trans-1,2-Dichloroethene ug/L 2000 110 60-140116 52000ND22102310
trans-1,3-Dichloropropene ug/L 2000 107 60-140116 82000ND21302310
Trichloroethene ug/L 2000 111 60-140119 72000ND22102380
Trichlorofluoromethane ug/L 2000 116 60-140123 62000ND23202450
Vinyl chloride ug/L 2000 123 60-140132 72000ND24602630
1,2-Dichloroethane-d4 (S)%102 70-13098
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92366283
FORMER SPUR 1211 WILSON, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92366283001 390116MW 3 MADEP VPH
92366283002 390116MW 5 MADEP VPH
92366283003 390116MW 6 MADEP VPH
92366283004 390116MW 8 MADEP VPH
92366283005 390116MW 10 MADEP VPH
92366283006 390116DUPMADEP VPH
92366283001 390341 390499MW 3 EPA 3010A EPA 6010
92366283002 390341 390499MW 5 EPA 3010A EPA 6010
92366283003 390341 390499MW 6 EPA 3010A EPA 6010
92366283004 390341 390499MW 8 EPA 3010A EPA 6010
92366283005 390341 390499MW 10 EPA 3010A EPA 6010
92366283001 390630MW 3 SM 6200B
92366283002 390630MW 5 SM 6200B
92366283003 390630MW 6 SM 6200B
92366283004 390630MW 8 SM 6200B
92366283005 390142MW 10 SM 6200B
92366283006 390630DUPSM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2017 05:18 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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Simplifying the Complex
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