RA-0749_5393_CA_RPTS_19910611_CSA

COMPREHENSIVE SITE ASSESSMENT REPORT
MURPHY MANUFACTURING COMPANY
2000 AIRPORT DRIVE
WILSON, NORTH CAROLINA
PREPARED BY
APPLIED ENVIRONMENTAL SERVICES, INC
RALEIGH, NORTH CAROLINA
AES, INC. JOB NO. A100372
JUNE 11, 1991
TABLE OF CONTENTS
Page
1.0 Introduction 1
2.0 Summary of Previous Activities
2.1 Initial Environmental Audit 1
2.2 Soil Excavation 3
2.3 Soil Disposal 4
3.0 Groundwater Assessment 5
3.1 Geologic Setting 6
3.2 Groundwater Monitoring/Well Installation 6
3.3 Hydrogeology 7
3.4 Groundwater Quality 8
4.0 Conclusions 1®
Figures
1. Site Location Map
2. Site Map
3. Initial Soil Sampling Locations
4. Secondary Soil Sampling Locations
5. Soil Excavation Map
6. Groundwater Monitory Well Locations
7. Groundwater Flow Map
8. Hydrogeologic Cross-Section
9. Contaminant Delineation Map
Appendices
A - Soil Sample Laboratory Reports
B - Groundwater Sample Laboratory Reports
C - Well Construction Records
1.0 INTRODUCTION
In January of 1990, Murphy Manufacturing Company of Wilson, North
Carolina became aware of soil pollution in three areas around the
exterior of the facility building. The pollution, which included
contamination of soils with several regulated chemicals, was discovered
during the course of a standard Phase I environmental audit performed
by Applied Environmental Services, Inc.
During the subsequent months. Murphy proceeded to determine the
extent of the soil contamination, excavate and properly dispose of
affected soils, and investigate the impact of the pollution on
groundwater in one suspect area. The following report serves to
summarize these activities and to present the most recent data from the
groundwater investigation.
Data generated indicates that soils in the three areas originally
identified as being contaminated, have been adequately removed and
properly disposed of. Groundwater irt the vicinity of the largest of the
affected areas has been investigated and shown to have been only
slightly affected.
2.0 SUMMARY OF PREVIOUS ACTIVITIES
2.1 INITIAL ENVIRONMENTAL AUDIT
The initial discovery of contaminated soils came in the course of
an environmental audit which was undertaken by Murphy Manufacturing to
satisfy requirements of a financial institution as part of a business
arrangement. AES, Inc. concluded in the audit report dated February 13,
1990, that soils in several areas contained regulated chemicals. Five
soil samples were procured and analyzed for organic compounds based on
-1-
knowledge of which chemicals were routinely used in processes at the
refrigerated truck body manufacturing facility. Figure 3 illustrates
the original sample locations and Table 1 below includes chemicals
identified and their concentrations.
Samples 1 and 2 were taken from an area from which three small (500
gallons or less capacity) underground storage tanks had been removed.
The tanks had been used to store lacquer thinner, enamel reducer, and
paint/solvent waste. Samples 3 and 4 were taken in an unpaved area
where visible surface stains were present. Sample 5 was taken from an
area where empty drums were being stored. Samples 2 through 5 were
taken at ground surface while sample 1 was taken at a depth of 3.5'.
TABLE 1
Laboratory Analytical Data
Initial Sampling Concentrations in^
Chemical Compound 1 2' 3
g)
4 5
Acetone 7.7 210.0 3.0 0.074
Toluene 7.0 33.0 0.027
Xylene 4.1 0. 110
Methylene Chloride 1. 1
Styrene 46.0 0.054 34.0
Dimethyl Phthaiate 4.7 3.5
Ethyl benzene 0.027
Naphthalene 0. 870
Fluorene 0. 960
Phenanthrene 2 . 3
Di-n-butylphthalate 0. 890
-2-
A second set of soil samples were taken and analyzed in mid
February, 1990. These samples were part of a soil boring program aimed
at more clearly defining the extent of soil contamination initially
identified. Figure 4 illustrates the locations of samples numbered 7,
10, 14, 17 and 18. Sample #7 was taken at a depth of "" 3.5' in the
former location of a methylene chloride underground tank. Sample #10
was taken at a depth ~ 3.5' from the empty drum storage area where
sample #5 has been taken at ground surface. Samples 14, 17 and 18 were
taken from hand auger borings surrounding the former tank bed area from
which initial samples 1 and 2 were taken.
Analytical results from the second set of samples were below the
detection limits for those compounds previously identified. Having
accomplished some definition of the extent of contaminated soil present,
the next step was to remediate the affected soils.
2.2 SOIL EXCAVATION
A written work plan was submitted to and approved by the Hazardous
Waste Branch of the North Carolina Department of Environment, Health and
Natural Resources regarding the excavation and disposal of the
contaminated soil. The scope of work outlined in the plan called for
soils from the three separate source areas to be excavated and staged
on site in approved roll-off containers. The containers were to be
sampled and soils characterized for appropriate disposal.
On September 17, 1990, excavation of contaminated soil was
initiated in the former underground storage tank bed area.
Approximately sixty cubic yards of soil was excavated from an area 12'
X 18' X 8' deep. The soil was placed in two thirty cubic yard roll
-3-
off boxes and covered with plastic. Samples were procured from the
bottom of the excavation and submitted to a qualified laboratory to
verify the effectiveness of the clean-up. Sample A-1 from the
excavation showed no remaining contamination.
On September 18, 1990, the remaining two source areas were
excavated. Eighteen cubic yards of soil was removed from an area
measuring 10' x 20' x 2.5' deep at the former empty drum storage area.
The soil was staged in a roll-off container for characterization.
Sample C-1 from within the excavation was analyzed and indicated 0.48
parts per million of Bis-2-Ethylhexyl phthalate remains in place in this
area.
Soils in the surfaced stained area were also excavated on September
18th. Ten cubic yards of soil was removed to a depth of approximately
1 foot. Sample B-1 from the excavation yielded results indicating 2.1
ppm of Bis-2-Ethylhexyl phthalate and 0.32 ppm of Dimethyl phthalate
remain in place.
2.3 SOIL DISPOSAL
To insure proper disposal of the excavated soils, the staged
material from each source area was sampled separately. Each sample was
analyzed separately using the TCLP methods for determining whether a
waste is considered hazardous. Tests to determine if the soil could be
considered hazardous waste based on the characteristics of ignitability,
corrosivity, and reactivity were also conducted.
Sample STB, from the containerized soil excavated from the former
tank bed area, yielded laboratory analysis that classify the sixty cubic
yards as non-regulated waste. Since the material requires no off-site
-4-
disposal and to be conservative in handling the soil. Murphy built a
plastic lined containment structure for the soil. The structure enabled
the soil to be spread to approximately 1 foot thick. The soil is
covered with plastic.
Sample SA2 was taken from the former empty drum storage area
stockpile. Analysis indicated that this soil also was classified as
non-regulated waste. It was spread in like manner to that described
above.
Sample SAl indicated that the ten cubic yards of soil excavated
form the ground surface in the stained areas was classified as a
hazardous waste. Levels of acetone and 111 trichloroethane exceeded
federal land - ban limits thus it was determined that the best available
treatment technology was incineration. After receiving proper
authorization from the State of South Carolina, the single truckload of
soil was transported by a licensed hauler to Thermal Kem, Inc. in Rock
Hill, South Carolina for incineration and final disposal.
3.0 GRQUNDWATER ASSESSMENT
The groundwater section of the North Carolina Department of
Environment, Health and Natural Resources, Division of Environmental
Management requested that Murphy perform a groundwater assessment in the
vicinity of the former underground storage tank bed. Initially, one
groundwater monitoring well was installed adjacent to the excavated
former tank bed. Subsequently, four additional shallow wells and one
deeper well were installed. The remainder of this document addresses
the findings of the groundwater investigation.
-5-
3.1 GEOLOGIC SETTING
The twenty-four acre site is located near the western edge of the
Coastal Plain Physiographic Province near Wilson, North Carolina.
Topography in the area is generally flat.
The subsurface at the site is composed of silty clays to a depth
of ~ 10'. Fine sandy silt extends to a depth of ~ 20' where a dense
grey clay was encountered. The thickness of the clay unit is 3 to 4
feet in MW2. Underlying the clay is an eight feet thick medium to
coarse sand. The entire upper sequence is typical of the Tertiary aged
Yorktowne Formation.
Underlying the Tertiany Yorktowne sediments at the site is a light
green meta-mudstone which was encountered at a depth of ~ 35 feet.
Figure 8 is a cross-sectional drawing of the subsurface at the site.
3.2 GROUNDWATER MONITORING/WELL INSTALLATION
Five shallow groundwater monitoring wells were installed in the
vicinity of the former underground UST area in an effort to first
determine whether groundwater had been impacted and secondly to
determine the horizontal extent of any contamination identified.
The first well, MW-1, was installed adjacent to the area where soil
had been excavated. The well was installed using a four inch diameter
hand auger. Ten feet of two inch diameter PVC well screen was placed
in the 17' deep boring with 2" PVC riser extending to land surface.
Torpedo sand was used as gravel pack around the screen. The sand pack
and screen were sealed off using bentonite pellets. The remainder of
the annulus was filed with cement grout to land surface. The well head
is protected by a locking cap and an eight inch diameter manhole cover.
-6-
Subsequent shallow wells, MW-3, MW-4, MW-5 and MW6 were installed
in like manner with similar construction specifications.
One doubled encased (or telescoping) well was installed to obtain
a groundwater sample at a greater depth. MW-2 was constructed by
installing 25' of six inch diameter initial or outer casing using a
hollow stem auger drilling rig. The casing was sealed at the bottom and
grouted into place with cement grout. After allowing the initial casing
to set up, a boring was advanced through the casing to a final depth of
"35'. Five feet of two inch diameter PVC screen was set to the bottom
of the boring. Torpedo sand makes up the gravel pack and a bentonite
seal separates the sand pack from the cement grout which fills the
annulus to the surface. Well construction records are provided as an
appendix.
The top of the casing of each well has been surveyed to provide
relative casing elevations and for location of the wells for mapping.
Figure 6 shows the well locations, ^ater levels have been measured to
determine the relative pressure head exhibited in each well.
Prior to being sampled, each well was first developed by removing
a minimum of three well volumes of water using a single use disposable
bailer. Wells were then sampled using a single use disposable bailer
and samples transported on ice to a qualified laboratory for analysis.
3.3 HYDROGEOLOGY
The uppermost water bearing zone at the site is the tan-gray fine
sandy silt found at the depth of approximately ten feet across the area.
This unit is overlain by silty clays and underlain by a dense confining
clay unit. The water levels demonstrated by the five shallow wells
-7-
which are screened penetrating the sandy silty unit are consistently
higher than the levels at which saturation was encountered, A table of
water level data is provided below.
TABLE 2
TABLE OF WATER LEVEL DATA
MWl MW2 MW3 MW4 MW5 MW6
Casing Elevation 97. 13 97. 30 97. 56 96.26 97.00 97.44
4/08/91
Water Level 2.85 3.23 2. 31 3.20 3.21
Water Elevation 94.28 94. 33 93. 95 93. 80 94 . 23
4/10/91
Water Level 3. 17 3. 96 3 34 2.48 3. 27 3.25
Water Elevation 93. 96 93.34 94. 22 93.78 93.73 94. 19
4/15/91
Water Level 3.31 3.97 3. 33 2.27 3. 36 3.3
Water Elevation 93. 82 93. 33 94. 23 93. 99 93.64 94. 1
*A11 elevations in feet
Using the most recent water level data, a potentiometric map was
generated to illustrate the general direction of groundwater flow
through the area. Figure 7 shows that groundwater flows from northwest
to southeast across the site.
3.4 GROUNDWATER QUALITY
Groundwater samples from all wells installed were analyzed
targeting volatile organic compounds using EPA-SW846 method 8240. Well
MW-1 was sampled in November 1990 and results indicated presence of
trichlorofluoromethane, methylene chloride, benzene, ethylbenzene, and
xylenes. In December 1990 the well (MW-1) was resampled and extra
-8-
quality control measures were taken to eliminate sampling or laboratory
errors. The same compounds were present at slightly lower levels.
Four additional shallow wells were placed surrounding MW-1 to
determine the horizontal extent of compounds found. One deep well (MW2)
was placed adjacent to MW-1 to determine the vertical extent of those
compounds present in MW-1. The following table includes all groundwater
sample data accumulated to date.
TABLE 3
TABLE OF LABORATORY DATA
Values Given In Micrograms Per Liter (ppb)
Date Sampled
Compound/Well
Trichlorofluoro-
methane
Methylene Chloride
Benzene
Bthylbenzene
Xylenes
Styrene
Toluene
Chloroform
Standard
5
1
29
400
1,000
n/a
11/90
MWl
420
7.2
120 '
90
195
12/90
MWl
280^
8.3-^
100/
61^
158
4/91
MW2
8.2
MW3
50
MW4
190
54
25
MW5 HW6
NOTES: No value indicates results below laboratory detection limits
* - Standards calculated from NCAC Title 15:02L.0200d(1) using
reference dose values provided in "Drinking Water Regulations
and Health Advisories by the Office of Water - USEPA, April 1991.
** - Attributed to lab error - see trip blank and equipment blank
12/90 sample.
-9-
4.0 CONCLUSIONS
Murphy Manufacturing Company has successfully Identified,
determined the magnitude of, and remediated soil contamination at three
specific source areas described previously. At two of the three (former
empty drum storage area and surface stained area) contamination did not
extend deep enough to pose a threat to groundwater. In the former UST
area, groundwater assessment was requested by the NC-DEM.
J In the initial well MW-1, placed closest to the former source area,
(y compounds were demonstrated as present at levels exceeding NC
Groundwater Quality Standards as set forth in NCAC Title 15:02L.002.
The three compounds and their respective standards are methylene
chloride (5 ppb), benzene (1 ppb), and ethlybenzene (29 ppb). In most
recent data for MW-1 shows methylene chloride at 8.3 ppb (3.3 ppb above
standard), benzene at 100 ppb (99 ppb above standard), and ethylbenzene
at 61 ppb (32 ppb above standard).
Subsequent Installation of wells MW-3, MW-4, MW-5, and MW-6 has
successfully defined the horizontal extent of the above standard
compounds. Well MW-2 was placed adjacent to MW-1 and analysis of the
groundwater from a depth of approximately 32 feet demonstrates the
vertical extent of groundwater impact in the area.
Groundwater in the vicinity of the former tank bed area has been
sufficiently investigated. There is no current use of groundwater in
the area for municipal or industrial purposes. Municipal water is used
by all facilities in the area.
The primary (USTS) and secondary (contaminated soils) sources for
any further groundwater impact have been appropriately eliminated. NC
-10-
Groundwater Standards have been exceeded in a small area well within
the boundaries of the 34 acre site. Applied Environmental Services,
Inc. recommends that no further assessment work is warranted and that
a semi-annual sampling program be initiated in leu of active (i.e.:
pump and treat) groundwater recovery and treatment of the site.
APPLIED ENVIRONMENTAL SERVICES, INC.
oseph M. Mattheis
Director of Environmental Sciences
Brent Chambers, P.O., REP
President
-11-
FIGURES
'
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r
Wiison Az
.C
>
s< ¨ w» •y
WILSON AIRPORT
Nx«S6
St Maithe>«
ch';
Jerusalem .
x/67
SN. 1^3^
57'30"2.5 TO GA. ^2 ^
W.'LSON CCURTHOUSE ^''1
NOTE: TAKEN FROM U.S.G.S. WINSTEAD CROSSROADS 7.5' SERIES TOPO QUAD
SITE LOCATION MAP
MURPHY MANUFACTURING
WILSON COUNTY
APPLIED ENVIRONMENTAL
SERVICES. INC.
SCALE: 1"= 2000'
PROJECT NO.: A100372
DRAWING NO.: 1
GRASS GRASS
ASPHALT
PAVED
PARKING
GRASS
AREA
GRASS
MURPHY MAHUFACIURING
PLANT
GRASS GRASS
ASPHALT
GRAVEL PARKING
AREA
FENCE
SR 1321
AIRPORT ROAD
DITCH LINES
GRAVEL PARKING
AREA
I
GENERALIZED SITE MAP
MURPHY MANUFACTURING
WILSON COUNTY RALEIGH . N.C.
SCALE: 1"= <00'
DWG. NO.: 2
PROJECT NO.: aiod372
GRASSGRASS
ASPHALT
PAVED
PARKING
GRAVEL PARKING
AREAMURPHY MANUFACTURING
PLANT
GRASS
AREA
GRASS
GRASS
ASPHALT
FENCE
SR 1521
AIRPORT ROAD GRAVEL PARKING
AREA
DITCH LINES
SCALE: 1"= 100'
DWG. NO.: 5
PROJECT NO.: A100372
INITIAL SOIL SAMPLE LOCATIONS
MURPHY MANUFACTURING
WILSON COUNTY RALEIGH , N.C.
GRASSGRASS
ASPHALT
PAVED
PARKING
GRAVEL PARKING
AREAMURPHY MANUFACTURING
PLANT
GRASS
AREA
GRASS
ASPHALT
FENCE
SR 1321
AIRPORT ROAD GRAVEL PARKING
AREA
DITCH UNES
SCALE: r'= loo'
DWG. NO.: 4
PROJECT NO.: A100372
SECOND SET SOIL SAMPt£ LOCATIONS
MURPHY MANUFACTURING
WILSON COUNTY RALEIGH . N.C.
ASPHALT
PAVED
PARKING
GRASS
AREA
GRASSGRASS
GRASS
— SR 1S21
AIRPORT ROAD
MURPHY MANUFACTURING
PLANT
GRASS
ASPHALT
DITCH LINES
GRAVEL PARKING
AREA
NOTE: EXCAVATED AREA DENOTED
BY HATCHED PATTERNS
GRAVEL PARKING
AREA
I
FENCE
SOIL EXCAVATION LOCALS
MURPHY MANUFACTURING
WILSON COUNTY
iPfi |[ SEIIS, i,
RALEIGH . NX.
SCALE: 1"= 100'
DWG. NO.: 5
PROJECT NO.: Aiao372
c
PARKING MURPHY MANUFACTURING
FENCE
— SR 1321
AIRPORT ROAD GRAVEL PARKING
DITCH LINES
6R0UNDWATER MONITOR WELL LOCALS
MURPHY MANUFACTURING
WILSON COUNH
iPH SittS, I.
RALEIGH , H.C.
SCALE: 1"= 100'
DWG. NO.: 6
PROJECT NO.: AIO0372
MURPHY
BUILDING
94.10
94.00
4.23MW3 O
93.90
93.80
94.20
93.70
O 93.64
MW4 I O 93,99
NOTE : ALL ELEVATIONS RECORDED IN FEET
SURVEY BENCHMARK = 100
DITCH
GROUNDWATER FLOW NET
MURPHY MANUFACTURING
WILSON COUNTY
APPLIED ENVIRONMENTAL
SERVICES. INC.
SCALE: 1"= 40'
PROJECT NO.; A100372
DRAWING NO.: 7
CItPL iVfftVfT 'r T*' MlfMlkl teiiUM
too -1 MW2
90 —
80 —
70 —
60 —
MW3
MW1
MW6
ORANGE-GREY SILTY CLAY
TAN-GREY FINE SANDY SILTY GUY
TAN-GREY FINE SANDY SILT
GREY CLAY.
GREY-i*EO^C!OARSE-:SANO-
GREEN META-MUDSTONE (€)
55
MDRPHY MANUFACTURING
NOTE: ALL ELEVATIONS RECORDED IN FEET
DENOTES STATIC HEAD
MW3-MW2-MW1-MW6 CROSS SECTIONAL VEIW
MURPHY MANUFACTURING
WILSON COUNTY
if C
. J \\vt
RALEIGH . NX.
SCALE: VERT-i"= 10' hor-1"=20'
DWG. NO.: 8
PROJECT NO.: A100372
■jiHr
PARKING MURPHY MANUFACTURING
MOTE: HATCHED PATTERN DENOTES COMPOUNDS
EXCEEDING NCAC TITLE 15 SUBCHAPTER 2L
GROUNDWATER STANDARDS
FENCE
— SR 1321
AIRPORT ROAD
MWS^
DTCH LINES
GRAVEL PARKING
GROUNDWATER CONTAMINATION MAP
MURPHY MANUFACTURING
WILSON COUNTY
ill iiil HE, II
RALEIGH , N.C.
SCALE: 1"= 100*
DWG. NO.: 9
PROJECT NO.: aiod372
APPENDIX A
Soil Sample Laboratory Reports
01/29/1990 17:41 MID-PACIFIC Enw. Lab.415 961 7113 P.04
Table 1. Volatile Organic Results
AES, Inc. Sample ID
AES, Inc.
9001078
Page 3 of 12
MM-1 MM-2 MM-3 MM-4 MM-5
8240 Compounds ug/kg ug/kg ug/kg ug/kg ug/kg
Chloromethane <1300 <2600 <1300 <50 <2600
vinyl chloride <1300 <2600 <1300 <50 <2600
Bromotuethane <1300 <2600 <1300 <50 <2600
Chloroethane <1300 <2600 <1300 <50 <2600
1,1-Dichloroethene <630 <1300 <630 <25 <1300
Carbon Disulfide <630 <1300 <630 <25 <1300
Acetone 7700 210000*3000 74 <2600
Methylene chloride <630 <1300 1100 <20 <i30'o
1,1-Dichloroethane <630 <1300 <630 <25 <1300
1,2-Dichloroethane <630 <1300 <630 <25 <1300
Vinyl acetate <1300 <2600 <1300 <50 <2600
2-Butanone <1300 <2600 <1300 <50 <2600
Chloroform <630 <1300 <630 <25 <1300
1,1.l-Trichloroethane <630 <1300 <630 <25 <1300
Carbon tetrachloride <630 <1300 <630 <25 <1300
Benzene <630 <1300 <630 <25 <1300
1,2-Dichloroethene <630 <1300 <630 <25 <1300
Trichloroethene <630 <■1300 <630 <25 <1300
1,2-Dichloropropane <630 ■'<1300 <530 <25 <1300
Bromodichloromethane <630 <1300 <630 <25 <1300
cis-l,3-DichloroprGpene <630 <1300 <630 <25 <1300
4-Methyl-2-pentanone <1300 <2600 <1300 <50 <2600
Toluene 7000 33000 <630 27 <1300
trans-1,3-Dichloropropene <630 <1300 <630 <25 <1300
1,1,2-Trichloroethane <630 <1300 <630 <25 <1300
Tetrachloroethene <630 <1300 <630 <25 <1300
2-Hexanone <1300 <2600 <1300 <50 <2600
Dibromochloromethane <630 <1300 <630 <25 <1300
Chlorobenzene <630 <1300 <630 <25 <1300
Ethylbenzene <630 <1300 <630 27 <1300
Total xylenes 4100 <1300 <630 110 <1300
Styrehe <630 <1300 46000*54 34000
Bromoform <630 <1300 <630 <25 <1300
1,1,2,2-Tetrachloroethane <630 <1300 <630 <25 <1300
Date Analyzed 1/23/90 1/23/90 1/22/90 1/19/90 1/22/90
* - Based on a 1:20 dilution analyzed 1/23/90.
01/29/1990 17:43 MID-PACIFIC Enu. Lab.415 961 7113 P.10
AES, Inc.
9001078
Page 9 of l?.
Table 2, Semivolatilc Organic Results
AES, Inc. Sample ID
MM-1 MM-2 MM-3 MM-4 MM-5
8270 Compounds ug/kg ug/kg ug/kg ug/kg ug/kg
Phenol <660 <660 <660 <660 <660
Bis(2-chloroethyl)ether <660 <660 <660 <660 <660
2-Chlorophenol <660 <660 <660 <660 <660
1,3-Dichioroben2ene <660 <660 <660 <660 <660
X, 4-'Dichloroben2ene <660 <660 <660 <660 <660
1,2-Dichlorobcn2ene <660 <660 <660 <660 <660
Bis(2-chloroisopropyl)ether <660 <660 <660 <660 <660
N-Nitroso-di-n-propylamine <660 <660 <660 <660 <660
Hoxachloroethane <660 <660 <660 <660 <660
Nitrobenzene <660 <660 <650 <660 <660
Isophorone <660 <660 <660 <660 <660
2-NitrophenoT <660 <660 <660 <660 <660
214-Dintethylphenol <660 <660 <660 <660 <660
Bis(2-chloroethoxy)methane <660 <660 <660 <660 <660
2,4-Dichlorophenol <660 <660 <660 <660 <660
1,2,4~Trichlorobenzene <660 <660 <660 <660 <660
Naphthalene <660 <660 <660 370 <660
Hexachlorobutadiene <660 <660 <660 <660 <660
4--Chloro-3-inethylphenol <660 <66a <660 <660 <660
Hexachlorocyclopentadiene <660 <660 <660 <660 <660
2,4,6-Trichlorophenol <660 <660 <660 <660 <660
2-Chloronaphthalene <660 <660 <660 <660 <660
Dimethyl phthalate <660 <660 4700 <660 3500
Acenaphthyiene <660 <660 <660 <660 <660
Acenaphthene <660 <660 <660 <660 <660
2,4-Dinitrophenol <3200 <3200 <3200 <3200 <3200
4-NitrophGnol <3200 <3200 <3200 <3200 <3200
2,4-Dinitrotolueno <660 <660 <660 <660 <660
2,6-Dinitrotoluene <660 <660 <660 <660 <660
Diethyl phthalate <660 <660 <660 <660 <660
4-Chlorophenyl phenylether <660 <660 <660 <660 <660
Fluorene <660 <660 <660 960 <660
4,6-Dinxtro-2-methylphenol <3200 <3200 <3200 <3200 <3200
N-Nitrosodiphenylamine <660 <660 <660 <660 <660
4-Bromophenyl phenylether <660 <660 <660 <660 <660
01/29/1990 17:44 MID-PACIFIC Enw. Lab.415 961 7113 P.11
AES, Inc.
9001078
Page 10 of 12
Table 2. Semivolatile Organic Results (Continued)
AES, Inc. Sample ID
MM-l MM-2 MM-3 MM-4 MM-5
8270 Compounds ug/kg ug/kg ug/kg ug/kg ug/kg
—————————
Hexachlorobenzene <660 <660 <560 <660 <660
Pentachiorophenol <3200 <3200 <3200 <3200 <3200
Phenanthrene <660 <660 <660 2300 <660
Anthracene <660 <660 <660 <660 <660
Di-n-Butyl phthalate <660 <660 <660 <660 890
Fluoranthene <660 <660 <660 <660 <660
Pyrene <660 <660 <660 <660 <660
Date Analyzed
Date Extracted
1/23/90 1/23/90 1/23/90 1/23/90 1/23/90
1/18/90 1/18/90 1/18/90 1/18/90 1/18/90
Surrogates Percent Recovery (%)
2-PluQrophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Trifaroinophenol
p-Terphenyl-dl4
54
52
49
51
56
51
58
67
55
62
56
54
66
64
53
67
48
39
62
58
54
64
55
44
59
60
56
65
42
46
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Environmenlaf Systems Division
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aitwn.NC 27713
(919) 544'4S35
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Chain of Custody Record
PROJECT SRE
ANALYSES
-^es, % t isrrEP^i^x-Of-oi DATE REPORT DUE
w / / /COaECTEOSY rs^fiaft/re;
VERBALT^AXyHARDCOPY
FIELD
SAMPLE ID
RUSH
FACTOR
V/«e7SAMPLE
MATRIX
DATE/
TIME LAB ID NO
(lor lab use onMREMARKS
" / I M*mJ
MM-£~
RB^ARKS RELINQUI D8Y:
DATE TIME
^dimm
RBJNQUtSHEDBY:RECEfVEDBY:RaiNCXJISHEDBY:
LAB USE ONLY
OPENEOBY:,:
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a:.HX ;®lp coNorrm
j'lHK ID ' ID-XH '•- tnu.i i
0!Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ENGINEERING AND LABORATORY SERVICES
JOHN M. OGLH
PRESIDENT
MR. JOE MATTKEIS
APPLIED environmental SERVICES
PO BOX 1145
GARY, NC 27512
P. O. BOX 12290
RESEARCH TRIANGLE PARK. N. C 27709
Phone [phone]O
Fax [phone]
MARCH 12, 1990
RE: MURPHY MFG.
CLIENT ID
7
10
14
17
18
SAMPLE HISTORY
GET SAMPLE DATS RECEIVED
34779
34780
34731
347S2
34783
2-12-90
2-12-90
2-12-90
2-12-90
2-12-90
DATS ANALYZED
2-27-50 TO 2-2S
2-28-90
2-28-90
3-07-90
3-07-90
■90
JEB/bws
CH^ICAL & environmental TECHNOLOGY, INC
Hn E. BAUR
GANIC CHEMIST
MfiR 15 '90 16:14 CHtf'i tfsurs I
PURGEABLB HALOCARBONS
METHOD 8240
DATE ANALYZED: 2-28-90
CLIENT ID; 7
GET SAMPLE: 34779
DETECTION
PARAMETER LIMIT
(ug/kg)
BENZENE 5.0
BROHODICHLOROMETHANE 5.0
BROMOFORM 5.0
BROHOMETHANE 5.0
CARBON TETRACHLORIDE 5.0
CHLOROBENZENE 5.0
GHLOROETHANE 10.0
2-CHLOROETHYLVINYL ETHER 10 . 0
CHLOROFORM 5 .0
DIBROHOCHLOROMETHANE 5 . 0
1,2-DICHLOROBENZENE 5.0
1,3-DICHLOROBENSENE 5.0
i , 4-DICHLOROBENZENE 5.0
1,1-DICHLOROETHANB 5 . 0
L, 2-DICHLOROETHANE 5.0
1,1-DICHLOROBTHENE 5.0
TRANS-1,2-DICHLOROETHENE 5.0
1,2-DICHLOROPROPANE 5.0
CIS-1,3-DlCHLOROPROPBNB 5.0
TRANS-1,3-DICHL0R0PR0PENE 5.0
ETHYL BENZENE 5.0
METHYLENE CHLORIDE 5.0
1,1,2,2-TETRACHLOROBTHANE 5 , 0
TETRACHLOROETHENE 5 . 0
TOLUENE 5 - 0
1,1,1-TRICHLOROETHANE 5.0
1,1,2-TRICHLOROETHANE 5.0
TRICHLOROETHENE 5 .0
TRICHLOROFLUORCMETHANE 5.0
VINYL CHLORIDE 10 . 0
XYLENBS 5 ,0
RESULTS
(ug/kg)
BDL
BDL
BDL
SDL
BDL
BDL
BDL
SDL
BDL
BDL
SDL
BDL
BDL
BDL
BDL
BDL
SOL
BDL
BDL
BDL
BDL
BDL
EDL
BDL
BDL
BDL
EDL
BDL
BDL
BDL
BDL
BDL - BELOM DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-846, VOLUME 3,
SEPTEMBER, 1986
J - Indioatss an estimated value. This flag is used when the mass
spectral data indicated the presence of a compound that meets the
indentification criteria but the result is less than the specifie
detection limit.
mR 15 '90 16:15 CHhfl tNMN ItCH rK)"-*
PURGEABLB HALOCARBONS
METHOD S240
DATE ANALYZED! 2-28-90
CLIENT IDi 10
GET SAMPLE! 34780
DETECTION
PARAMETER LIMIT RESULTS
(ug/kg)(ug/kg )-
BENZENE 5.0 BDL
BROMODICHLOROMETHANE 5,0 BDL
BROMOFORM 5.0 BDL
BROMOMETHANE 5.0 BDL
CARBON TETRACHLORIDE 5.0 BDL
CHLOROBENZENE 5. 0 BDL
CHLOROETHANE 10.0 BDL
2-CHLOROETHYLVINYL ETHER 10.0 BDL
CHLOROFORM 5 . 0 BDL
DIBROMOCHLOROMETHANE 5 . 0 BDL
1,2-DICHL0R0BEN2ENB 5.0 BDL
1, 3-DICHLOROBENZENE 5 . 0 BDL
1, 4-DXCHLOROBENZENE 5.0 BDL
1, l-DICHLOROETHANE 5.0 BDL
X,2-DICHLOROETHANE 5.0 SDL
1,1-DICHLOROETHENE 5,0 BDL
TRANS-1,2-DICHLOROETHENE 5 . 0 BDL
1, 2-DICHLOROPROPAKE 5.0 BDL
CIS-1,3-DICHLOROPROPENE 5.0 BDL
TRANS-1,3-DICHLOROPROPENE 5.0 BDL
ETHYL BENZENE 5.0 BDL
METHYLENE CHLORIDE 5.0 BDL
1,1,2, 2-TETRACHLOROETHANE 5.0 BDL
TETRACHLOROETHENE 5.0 BDL
TOLUENE 5.0 BDL
1,1, 1-TRICHLOROETHANE 5 . 0 BDL
1,1,2-TRICHLOROETHANB S . 0 DDL
TRICHLOROETHENE 5.0 BDL
TRICHLOROFLUOROMETHANE 5.0 BDL
VINYL CHLORIDE 10.0 BDL
XYLENES 5 .0 BDL
HDL - BELOW DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-846,VOLUME 3,
SEPTEMBER, 1986
J - Indicates an estimated value. This fla^ is used when the mass
spectral data indicated the presence of a compound that meets the
indentificatlon criteria but the result is less than the specified
detection limit.
MAR 15 '90 16:15 L.Mtri blNVN I bl-N
PURGEABLB HALOCARBONS
METHOD 3240
DATE ANALYZED: 2-28-90
CLIENT iDi 14
GET SAMPLE: 34781
detection
PARAMETER LIMIT
(ug/kg)
BENZENE 5 . 0
BROMODICHLOROMETHANE 5.0
BROMOFORM 5 . 0
BROMOMETHANE 5 . 0
CARBON TETRACHLORIDE 5.0
CHLOROBENZENE 5.0
CHLOROETHANE 10 . 0
2-CKLORQETHYLVINYL ETHER 10 . 0
CHLOROFORM 5.0
DIBROMOCHLOROMBTHANE 5.0
1,2-DICHLOROBENZENE 5 . 0
1,3-DICHL0R0BEN2ENE 5.0
1,4-DICHLOROBBNZENE 5.0
1,1-DICHLOROETHANE 5 . 0
1,2-DICHLOROETHANE 5.0
1,1-DICHLOROETHENE 5.0
TRANS-1,2-DICHLOROETHENE 5 . 0
1,2-DICHLOROPROPANE 5.0
CIS-1,3-DICHLOROPROPENE 5 . 0
TRANS-1,3-DICHLOROPROPENE 5.0
ETHYL BENZENE 5 . 0
METHYLENE CHLORIDE 5.0
1,1,2,2-TETRACHLOROETHANE 5.0
TBTRACHLOROSTHENE 5.0
TOLUENE 5.0
1,1,1-TRICHLOROETHANE 5 i 0
1,1,2-TRICHLOROETHANE 5 .0
TRICHLOROETHENE 5.0
trichlorofluoromethane 5 . 0
VINYL CHLORIDE 10 . 0
XYLBNES 5 .0
RESULTS
(ug/kg)
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL - BELOW DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-846, VOLUME 3,
SEPTEMBER, 1986
J - Indicates an estimated value. This flag is used when the mass
spectral data indicated the presence of a compound that meets theindentification criteria but the result is less than the specifie
detection limit.
riHK 'yu lb:ib i^nc.1'1 ciNviH 1 fwH
PURGEABLE HALOCARBONS
METHOD 8240
DATE ANALYZED! 3-07-90
CLIENT IDi 17
CET SAMPLE; 34782
DETECTION
PARAMETER LIMIT RESULTS
(ug/kg)(ug/kg)
BENZENE 5 . 0 BDL
BROMODICHLOROHETHANE 5.0 BDL
BROHOFORM 5.0 BDL
BROMOMETHANS 5.0 BDL
CARBON TETRACHLORIDE 5.0 BDL
CHLOROBBNZBNE 5. 0 BDL
CHLOROETHANE 10.0 BDL
2-CHLOROETHYLVINYL ETHER 10 . 0 BDL
CHLOROFORM 5 . 0 BDL
DIBROMOCHLOROMETHANE 5 . 0 BDL
1,2-DICHLOROBENZENE 5.0 BDL
1, 3-DICHLOROBENZENE 5.0 BDL
1, 4-DICHL0R0BEN2ENE 5.0 BDL
1,1-DICHLOROETHANE 5.0 BDL
1,2-DICHLORCETHANE 5.0 BDL
1,1-DICHLOROETHBNE 5 . 0 BDL
TRANS-1,2-DICHLOROETHENE 5 . 0 BDL
1, 2-DICHLOROPROPANB 5.0 BDL
CIS-1,3-DICHLORQPROPENE 5.0 BDL
TRANS-1,3-DICHLOROPROPENE 5 . 0 BDL
ETHYL BENZENE 5.0 BDL
METHYLENE CHLORIDE 5.0 BDL
1,1,2, 2-TETRACHLOROETHANB 5.0 BDL
TETRACHLOROETHBNE 5.0 BDL
TOLUENE 5.0 BDL
1,1, 1-TRICHLOROSTHANE 5.0 BDL
1,1, 2-TRICHLORQETHANE 5.0 BDL
TRICHLOROETHENE 5.0 BDL
TRICHLOROFLUOROMETHANE 5.0 BDL
VINYL CHLORIDE 10.0 BDL
XYLENES 5.0 BDL
BDL - BELOW DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-845, VOLUME 3,
SEPTEMBER, 1986
J - Indicates an estimated value. This flag is used when the mass
spectral data indicated the presence of a compound that meets the
indentification criteria but the result is less than the specified
detection limit.
MAR 15 '90 16:16 CHEM EMUN TECH ru r
PURGEABLE HALOCARBONS
METHOD 8240
DATE ANALYZED: 3-07-90
CLIENT ID: 13
GET SAMPLBi 34783
DETECTION
PARAMETER LIMIT
(ug/kg)
BENZENE 5.0
BROMODICHLOROMETHANE 5.0
BROHOFORM 5 .0
BROHOMETHANE 5.0
CARBON TBTRACHLORIDE 5.0
CHLOROBENZENE 5 .0
CHLOROETHANE 10.0
2-CHLOROETHYLVINYL ETHER 10,0
CHLOROFORM 5.0
DISROMOCHLOROMETHANE 5.0
1,2-DICHLOROBENZENE 5.0
1, 3-DICHL0R0BEN2ENE 5 . 0
1,4-DlCHLOROBENZENE 5 . 0
1, 1-DICHLOROETHANE 5.0
1,2-DICHLOROETHANS 5 . 0
1,I-DICHLOROETHENE 5.0
TRANS-1,2-DICHLOROETHnNE 5.0
1,2-DICHLOROPROPANE 5.0
CIS-1,3-DICHLOROPROPENE 5.0
TRANS-l,3-DlCHLOROPROPENB 5.0
ETHYL BENZENE 5,0
HBTHYLENE CHLORIDE 5.0
1,1,2,2-TETRACHLOROBTHANB 5.0
TETRACHLOROETHENE 5.0
TOLUENE 5.0
1,1,1-TRICHLOROETHANE 5.0
1,1,2-TRICHLOROETHANE 5.0
TRICHLOROETHENE 5.0
TRICHLOROFLUOROMETHANB 5.0
VINYL CHLORIDE 10.0
XYLENES 5.0
RESULTS
(ug/kg)
SDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
EDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL - BELOW DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-846, VOLUME 3,
SEPTEMBER, 1986
J - Indicates an estimated value. This flag is used when the mass
spectral data indicated the presence of a compound that
indentification criteria but the result is less than the specific
detection limit.
MPlR 15 'ykJ lb:iY L-ntn cnvi^ le-.-n
BASE NEUTRAL/ACIDS
METHOD 8270
DATE ANALYZEDi 2-27-90
CLIENT IDi 7
CET SAMPLEi 34779
BASE NEUTRAL
DETECTION
limit results
ug/kg) (ug/kg)
200 BDL
PARAMETER
ACENAPHTHENB
ACENAPHTHYLENE 200 BDL
ANTRACBNB
BENZO(A)ANTHRACENE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BBNZ0(GHI)PSRYLENE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROETHOXY)METHANE
BIS{2-ETHYLHEXYL)FHTHALATE
BIS(2-CHLOROISOPROPYL)ETHER
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 BDL
200 SDL
200 BDL
200 BDL
200 BDL
200 BDL
4-bromophenyl phsnyl ether 200
BUTYL BENZYL FHTHALATE
2-CHLORONAPHTKALENE
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE ,
DIBENZ0(A,H)ANTHRACENE 200
DI-N-BUTYLPHTHALATE
1, 2-DICHLOROBENZBNE
1, 3-DICHLOROBENZENB
1,4-DICHLOROBBNZBNE 200 ^
3,3'-DICH1.0R0BENZIDINE
DIETHYL FHTHALATE 200
DIMETHYL FHTHALATE 2002.4-DINITROTOLUENE -®®
2.5-DINITROTOLUENE 2®® g^L
DI-N-OCTYLPHTHALATEFLUORANTHENE ^00
200
HBXACHLOROBUTADIENE 200
200
HEXACHLOROBENZENB 200
VMMFLUORENE _ _ ppL
HEXACHLOROETHANE 200
IDENO(1,2,3-CD)PYRBNB -
ISOPHORONE ; BDL
2-METHYLNAPHTHALENE
NAPHTHALENE BDL
nitrobenzene bdlN-NITROSODI-N-PROPYLAMINE 2
PHENANTHRSNE bdl
PYRENE bdl
1,2,4-TRICHLOROBENZENE 200
nf=iR lb 'yw lb:iY UMtn tnvrs i ciL-fi oui riiT
PAGE #2
BASE NEUTRAL/ACIDS
METHOD 8270
CLIENT IDi 7
CET SAMPLE. 34779
ACIDS
PARAMETER
4-CHLORO-3-METHYLPHENOL
2-CHLOROPHBNOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHSNOL
2,4-DINITROPHSNOL
2-METHYL-4,6-DINITROPHENOL
2-NlTROPHENOL
4-NITROPKENOL
PENTACHLOROPHENOL
PHENOL
2,4,6-TRICHLOROPHBNOL
DETECTION
LIMIT
iMg/kg)
200
200
200
200
1000
1000
200
1000
1000
200
200
RESULTS
(ug/kg)
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL - BELOW DETECTION LIMIT
"TEST METHODS FOR EVALUATING SOLID WASTES", SW-a46, VOLUME 3,
SEPTEMBER, 1986
J - Indicates an estimated value. This
spectral data indicated the presence of
indentification criteria but the result
detection limit.
flag is used when the mass
a compound that meets the
is less than the specified
m
Chctracal & EnvironmenUl Technology, Inc.
102-A Woodwinds Industrial Cl.
Gary. NC 27511 CHAIN OF CUSTODY RfCORO
PROJ. NO.PROJECT N^£
a4 .NO.
or
CON-
TAINCRS
"EWARKS
ST A. MO.OATl Tiwe i 5
5 STATION LOCATION
Z'CC /
}/i /
/f cx-' I /\
/?f!/
H /.
Relinquished by: (S-i^munj
Reiinquiihed by;
R«Ur
Dctt / Time
Date / Time
necelwd by: SfeMcwv;nttfoquirfved byt fSifrmur*)
Rtctlvtd by; (Sffnfmw}Hailnqulched by
IXtlrfeution: OrlfiAal Aocom(S«nl«» Shipmant; Copy to
/Tiim
iiii
Oett /Time
Otte/rima
Received by: AiewmraJ
Recetvd by:
Remtfks
/ ^<^*i
w I AW
GeoChem, Incorporated
Environmental Laboratories
October 15, 1990
Mr. Joe Mattheis
Applied Environmental Services, Inc.
1805 Running Oak Drive
Raleigh, NC 27612
Reference: Hurphey
A100372
GCI# 9009-055
Dear Mr. Joe Mattheis:
• "1^'" s"^"s"foranalysis. The tests that you requested have been subcontracted to
lEA. The results, on lEA's letterhead are enclosed.
analytical needs.
a rely,
Dean GoKel
President
2S00 Gate Way Centre Blvd.. Suite 300 • MorrisviHe, NO 27560Telephone: [phone] • FAX: [phone]
gc/ms purgsables
SW'846 METHOD 8240
I£A Sample Kumberz 916-045-1
saxnpla Identification! 1310
Date Analysed: 10/01/90 By: Harris
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bromoforzn
5 Bromomethane
6 2-ButaAone
7 Carbon disulfide
6 Carbon tetrachloride
9 Chlorobehzene
10 Dibromochloromethane
11 Chloroethane
12 2-Chloroethylvinyl ether
13 Chloroform
14 Chloromethane
15 l#l-Dichloroethane
16 1/2-Dichloroethane
17 1,1-Dichloroethene
18 1,2-Oichloroethene (total)
19 1/2-Dichloropropane
20 cis-l,3-Dichloropropene
21 trans-1,3-Dichloropropene
22 Bthylbenzene
23 2-Hexanone
24 Methylene chloride
2 5 4-Methy1-2-pentanone
26 Styrene
27 1,1,2/2-Tetcachloroethane
28 Tetrachloroethene
29 Toluene
30 l/lfl-Trichloroethane
31 l/lr2-Trichloroethane
32 Trichloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenee (total)
Quantitation Heaulta
Limit Concentration
(ug/kg)(ug/kg)
100 BQL
5 BQL
S BQL
5 BQL
10 BQL
100 BQL
5 BQL
5 BQL
5 BQL
5 BQL
10 BQL
10 BQL
5 BQL
10 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
50 BQL
5 BQL
50 BQL
5 BQL
5 BQL
5 BQL
S BQL
5 BQL
5 BQL
5 BQL
50 BQL
10 BQL
5 BQL
Conunents:
SQL n Below Quantitation Limit
GC/KS PURGEABLES
5W-846 METHOD S240
ISA Sample Number; 916-045-2
Sample Identifications 1311
Date Analyzed: 10/01/90
By: Harris
Number Compound Quantitation
Limit
(ug/kg)
1 Acetone 100
52Benzene
3 Bromodichloromethane 5
4 Bromoforro 5
5 Bromomethane 10
6 2-Butanone 100
7 Carbon diaulfide 5
8 Carbon tetrachloride s
9 Chlorobenzene 5
10 Dibromochloromethane 5
11 Chloroethsne 10
12 2-Chloroethylvinyl ether 10
13 Chloroform 5
14 Chloromethane 10
15 1;l-Dichloroethane 5
16 1,2-Dichloraethane 5
17 1tl-Dichloroethene 5
18 1,2-Dichloroethena (total)5
19 1t2-Dichloropropane 5
20 cia-1,3-Dichloropropene 5
21 trans-1,3-Dichloropropene 5
22 Ethylbenzene 5
23 2-Hexanone 50
24 Methylene chloride 5
25 4-Methy1-2-pentanone 50
26 Styrene 5
27 1,1,2/2-TetrachloroethaAe 5
23 Tetrachloroethene 5
29 Toluene 5
30 1,1/1-Trichloroethane 5
31 1/1,2-Trichloroethane 5
32 Trichlorcethene 5
33 Vinyl acetate 50
34 Vinyl chloride 10
35 Xylenes (total)5
Results
Concentration
(ug/kg)
BQL
BOX.
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL -
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Comments;
BQL s Below Quantitation Limit
GC/MS PURGEABLBS
SW-846 METHOD 8240
XBA Sample Number: 916-045«-3
Sample Identification: 1312
^ate Analyzed: 10/01/90 By: Harris
Number Compound Quantitation Results
Limit Concentration
(ug/kg) (ug/kg)
1 Acetone 100 BQL
2 Benzene 5 BQL
3 Bromodichlorotnethane S BQL
4 Bromoform S BQL
5 Bromomethane 10 BQL
6 2-Butanone 100 BQL
7 Carbon disulfide s BQL
8 Carbon tetrachloride 5 BQL
9 Chlorobenzene 5 BQL
10 Dibromochloromethane S BQL
11 Chloroethane 10 BQL
12 2-Chloroethylvinyl ether 10 EQL
13 Chloroform 5 BQL
14 chloromethane 10 bql
15 1,1-Dichloroethane 5 BQL
16 1,2-Dichioroethana 5 BQL
17 1,1-Dichloroethene 5 SQL
18 1,2-Dichloroethene (total) 5 BQL
19 1,2-Dichloropropane 5 BQL
20 ciS-i,3-Dichloroptopene , 5 BQL
21 trans-l^S-Oichloropropene S BQL
22 Ethylbenzene 5 BQL
23 2-Hexanone 50 BQL
24 Methylena chloride 5 BQL
25 4-MethyI-2-pentanone 50 BQL
26 Styrene S BQL
27 1,1,2,2-Tetrachloroethane 5 BQL
28 Tetrachloroethene 5 BQL
29 Toluene 5 BQL
30 1,1,1-Trichloroethane S BQL
31 1,1,2-Trichloroethane 5 BQL
32 Trichloroethene 5 BQL
33 Vinyl acetate 50
34 Vinyl chloride 10 BQL
35 Xylenes (total) 5 BQL
Comments:
BQL ^ Below Quantitation Limit
base/neutral/acid extractables
SW-a46 METHOD 8270
ISA Sample Numberi 916-045-2
Sample Identification: 1311
Date Extracted: 10/02/90
Date Analyzed; 10/06/90 By: Mace
Cuantitation Re
Limit Conce:
Number Compound (ug/kg)(u-
1 Acenaphthene 200 BQL
2 Acenaphthylene 200 BQL
3 Anthracene 200 BQL
4 Benzoic acid 1000 BQL
5 Benzo < a}anthracene 200 BQL
6 Benzo<b}fluoranthene 200 BQL
7 Benzo(k)flucranthene 200 BQL
S Benzo(g,h,i)perylene 200 BQL
9 Benzo(a)pyrene 200 BQL
10 Benzyl alcohol 400 BQL
11 bis(2-Chloroethoxy)methane 200 BQL
12 bis(2-chloroethy1)ether 200 BQL
13 bis < 2-Chloroiaopropyl)ether 200 BQL
14 bis(2-Ethylhsxyl)phthalate 200
15 4-Broinophenyl phenyl ether 200 BQL
16 Benzyl butyl phthalate 200 BQL
17 4-'Chloroanlline 400 BQL
18 2-Chloronaphthalene 200 BQL
19 4-Chloro-3-methylphenol 400 BQL
20 2-Chlorophenol 200 BQL
21 4-Chlorophenyl phenyl ether 200 BQL
22 Chrysene 200 BQL
23 Dibenzb(a,h)anthracene 200 BQL
24 D ibenzofuran 200 BQL
25 Di-n-butylphthalate 200 BQL
26 1,3-Dichlorobenzene 200 BQL
27 1,4-Dichlorobenzene 200 BQL
28 1,2-Dichloroben2ene 200 BQL
29 3,3'-Dichlorobenzidine 400 BQL
30 2,4'-DichlorophenoI 200 BQL
31 Diethyl phthalate 200 BQL
32 2,4-Diii^thylphenol 200 BQL
33 Dimethyl phthalate 200
34 4,S-Dinitro-2-raethylphenol 1000 BQL
35 2,4-Dinitrophenol lOOO BQL
36 2,4-Dinitrotoluene 200 BQL
37 2,6-Dinitrotoluene 200 BQL
38 Di-n-octylphthalate 200 BQL
39 Fluoranthene 200 BQL
2,100
320
FORM 8270 (1)ReVt 050589
basb/neutral/acid extsactables
SW-846 METHOD 8270
lEA Sample Number: 916-045-2
Sample Identifications 1311
Date Extracted: 10/02/90
Date Analyzed: 10/06/90 By: Hace
^antitation R
Limit Conci
Number Compound (ug/kg)(■
40 Fluorene 200 BQL
41 Kexachlorobenzene 200 BQL
42 Hexachlorobutadiene 200 BQL
43 Hexachlorocyclopentadiene 200 SQL
44 Hexachloroethane 200 BQL
45 Indeno(1,2/3-cd)pyrene 200 BQL
46 Zsophorone 20O BQL
47 2-Methylnaphthalene 200 BQL
48 2-Methylplienol (o-creaol)200 BQL
49 4-Metliylphenol (p-cresol)200 BQL
50 Naphthalene 200 BQL
51 2-Nitroaniline 1000 BQL
52 3-Nitroaniline 1000 BQL
53 4-Nitroaniline lOOO BQL
54 Nitrobenzene 200 BQL
55 2-NitrophenoI 200 BQL
56 4-Nitropheno1 1000 BQL
57 N-Nitrpso-di-n-propylamine 200 BQL
58 N-Nitroaodiphenylamine 200 BQL
59 Pentachlorophenol 1000 BQL
60 Phenanthrene 200 BQL
61 Phenol 200 BQL
62 Pyrene 200 BQL
63 1,2,4-Trichlorobenzene 200 BQL
64 2,4,S-Trichlorophenol 200 BQL
65 2,4,6-Trlchlorophenol 200 BQL
ug/kg)
Comments:
SQL B Below Quantitaticn Limit
FORM 8270 (2)Rev. 050589
1
BASE/NEUTRAL/ACID EXTRACTABLES
SW-34S METHOD 8270
ISA Sample Number: 916-045-3
Sample Identification! 1312
Date Extracted! 10/02/90
Date Analyzed: 10/06/90 By: Mace
Number Compound
1 Acenaphthene
2 Acenaphthylene
3 Anthracene
4 Benzole acid
5 Benzo(a}anthracene
6 6enzo(b)fluoranthene
7 8enzo(k)fluoranthene
8 Benzo(9,h,i)perylene
9 6enzo(a)pyrene
10 Benzyl alcohol
11 bis(2-Chloroethoxy}methane
12 bis(2-Chloroethyl)ether
13 bis(2-Chloroisopropyl)ether
14 bisC2-Ethylhexyl)phthalate
15 4-Bromophenyl phenyl ether
16 Benzyl butyl phthalate
17 4-Chloroaniline
18 2-Chloronaphthalene
19 4-Chloro-3-methylphenol
20 2-Chlorophenol
21 4-chlorophenyl phenyl ether
22 Chryeene
23 Dibenzo(a/h}anthracene
24 Dibenzofuran
25 Di-n-butylphthalate
26 1,3-Dic hlorobenz ene
27 If4-Dichlorobenzene
28 1|2-Dichlorobenzene
29 3,3'-Dichlorobenzidine
30 2f 4-Dichlorophenol
31 Diethyl phthalate
32 2f4-Dimethylphenol
33 Dimethyl phthalate
34 4f6-Dinitro-2-metbylphenol
35 2,4-Dinitrophenol
36 2f4-DlnitrotoXuene
37 2f 6'Dinitrotoluene
38 Di-n-octylphthalate
39 Pluoranthene
Quantitation
Limit
(ug/kg)
200
200
200
1000
200
200
200
200
200
400
200
200
200
200
200
200
400
200
400
200
200
200
200
200
200
200
200
200
400
200
200
200
200
1000
1000
200
200
200
200
Results
Concentration
(ug/kg)
BQL
BQL
BQL
8QL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
480
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
FORM 8270 (1)Rev. 050589
base/neuthal/acid extractables
SW-a46 KETHOD 8270
lEA Sample Kumber: 916-045-3
Sample Identification; 1312
Date Extracted: 10/02/90
Date Analyzed: 10/06/90 By: Hace
Number Compound
Quantitation
Limit
(ug/Jcg)
Results
Concentration
(ug/kg)
40 Fluorene 200 BQL
41 Hexachlorobensene 200 BQL
42 Hexachlorobutadiene 200 BQL
43 Hexachlorocyclopentadiene 200 BQL
44 Hexachloroethane 200 BQL
45 Indeno(1<2,3-cd)pyrene 200 BQL
46 Isophorone 200 BQL
47 2-Methylnaphthalene 200 BQL
48 2-MethylphenoI (o-cresol)200 BQL
49 4-Methylphenol (p-cresol)200 SQL
50 Naphthalene 200 BQL
51 2-Nitroaniline 1000 BQL
52 3-Nitroaniline 1000 BQL
53 4-Nitroaniline 1000 BQL
54 Nitrobenzene 200 BQL
55 2-Nitrophenol 200 BQL
56 4-Nitrophenol 1000 BQL
57 N-Nitroso-di-n-propylamine 200 BQL
58 N-Nitrosodiphenylamine 200 SQL
59 Fentachlorophenol 1000 BQL
60 Fhenanthrene 200 BQL
61 Phenol 200 BQL
62 Pyrene 200 BQL
63 1,2,4-Trichlorobenzene 200 BQL
64 2,4,5-Trichlorophenol 200 BQL
65 2,4,6-Trichlorophenol 200 BQL
Comments:
BQL s Below Quantitation Limit
FORK d270 (2)Hev* 050569
APPLIED
ENVIRONMENTAL
SERVICES,
INC.
Laboratory Name:
1805 Running Oak Drive, Rateigh, NC 27612
Post Office Box T145. Gary. NC 27512
919-787-8209 n FAX [phone]
Chain of Custody Record
Report To:
Page of.
PROJECT tty. CLIENT
/W37Z
NO. FOCOSRENIATN REPOITACOLN
ANALYSES
kH !
nn / /
j LABORATORY PROJECT » QCT*—
PROJECT NAME /y j j DATE REPORT DUE
COLLECTED ! j VERBALFAX/HARDCOPY
FIEIX
SAMPLE ID
TURNAROUND
IN DAYS
SAMPLE
MATRIX
DATE
COLLECTED
/ LAB ID NO.
/ REMARKS (for tab use only)
/r 9-/7 /\6iO
/r ^r/f-/S y \3 11
ay /r"9-/6 2 ISI'Z—
- ^ —
REiyiARKS ELINQUiSHED BY:-DATE TIME
bsSL
CEIVEDBY/
ii.
DATE TIIVIE
/^:^Q
RE^^MQUlSHED BY:DATE TIME RECEIVED BY:DAT5^TIME RELINQUISHED BY:DATE TIME
RECEIVED BY:DATE TIME/RELINQUISHED BY;DATE TIME RECEIVED BY:DATE TIME REUNQUISHED BY:DATE TIME
WhiteyLaboratoryCopy, Yellow/Aocoyntlng Copy, Plnk.'Fite Copy
UOT-lb-aU flUN Ibibti tihUUHhn INU. hHA NU. didqouuiDf r. ui
GeoChem, incorporated
Environmental Laboratories
October 15, 1990
Mr* Joe Mattheis
Applied Environmental Services, Inc.
1805 Running Oak Drive
Raleigh, NC 27612
Reference! Rurphey
A100372
GCl# 9009-055
Dear Mr. Joe Mattheis:
This is the analytical report for the above referenced
project. On September 21, 1990 we received three soil samples foranalysis. The tests that you requested have oeen subcontracted to
lEA. The results, on lEA's letterhead are enclosed.
If there are any technical voi^
me at 919-460-8093. Thank you for allowing GboChbm to serve your
analytical needs.
Dean Gokel
President
2500 Gate Way Centre Blvd., Suite 300 • Morrisville, NC 27560
Telephone: 919-460^093 • FAX: [phone]
ukyi"io-3u nun lo-aa UCUOHLll lit'-'.rnA nui oioHuuuiui
1
gc/ms purgsables
SW-846 METHOD 8240
r. ud
ISA Sample Numberi
sample Identification:
Date Analysed:
916-045-1
1310
10/01/90
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bromoform
5 Bromomethane
6 2-Butanone
7 Carbon disulfide
8 Carbon tetrachloride
9 Chlorobenzene
10 Dibromochloromethane
11 Chloroethane
12 2-Chloroethylvinyl ether
13 Chloroform
14 Chloromethane
15 1/l~Dichloroethane
16 1t2-Dichloroethane
17 1,l-Dichloroethene
18 1r 2-Oiehloroethene (total}
19 1/2-Dichloropropane
20 cis-lf 3-oichloropropene
21 trans-1,3-Oichloropropene
22 Ethylbenzene
23 2-Hexanone
24 Methylene chloride
25 4-Met hy1-2-pentanone
26 Styrene
27 1/1/2,2-TetrachloroethaDe
28 Tetrachloroethene
29 Toluene
30 1f1/1-TrichXoroethane
31 1#1r 2-Trichloroethane
32 Trichloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenes (total)
By: Harris
Quantitation Results
Limit Concentration
(tig/kg)(ug/kg)
100 BQL
5 BQL
5 BQL
5 BQL
10 BQL
100 BQL
5 BQL
5 BQL
5 BQL
5 BQL
10 BQL
10 BQL
5 BQL
10 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
S BQL
5 BQL
5 BQL
50 BQL
5 BQL
50 BQL
5 BQL
5 BQL
S BQL
5 BQL
5 BQL
5 BQL
5 BQL
50 BQL
10 BQL
5 BQL
Comments;
BQL n Below Quantitation Limit
GC/MS PURGEABLES
5W-a46 METHOD 8240
lEA Sample Number:
Sample Identification:
Date Analyzed:
916-045-2
1311
10/01/90 By: Harris
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bronoform
5 Bromoroethane
6 2-Butazione
7 Carbon diaulfide
8 Carbon tetrachloride
9 Cblorobenzene
10 Dibromochloromethane
11 Chloroethane
12 2-Chloroethylvinyl ether
13 Chloroform
14 Chloromethane
IS 1/1-Dichloroethane
16 1t2-Dichloroethans
17 1^l-Dichloroethene
18 1,2-Dichloroethene (total)
19 1t2-Dichloropropane
20 cis-1,3-Dichlorcpropene
21 trane-1,3-Dichloroprcpene
22 Bthylbenzene
23 2-Hexancne
24 Methylens chloride
25 4-Methyl-2-pentanone
26 Styrene
27 1,1,2#S-Tetrachloroethane
23 Tetrachloroethene
29 Toluene
30 1,1,l-Trichloroethane
31 1,1,2-Triehloroethane
32 Trichloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenes {total}
Quantitation
Limit
(ug/kg)
100
5
5
5
10
100
5
5
5
5
10
10
5
10
5
5
S
5
5
5
5
5
50
5
50
S
5
5
5
5
5
5
50
10
5
Results
Concentration
(ug/kg)
BQL
SQL
bql
BQL
BQL
BQL
bql
BQL
BQL
bql
BQL
BQL
BQL
BQL
bql
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
bql
BQL
BQL
BQL
Comments:
BQL - Below Quantitation Limit
uoi-iu~t5u nun 1 f - uu ucuuncii inu.rn/\ nu. oiohuuuiu(r, U4
GC/HS PtJRGEABLES
SW-646 METHOD 8240
X£A Sample Number: 916-045-3
Sample Identificatiojij 1312
Date Analyzed: 10/01/90
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bromoform
5 Bromomethane
6 2-Butanone
7 Carbon disuXfide
8 Carbon tetrachloride
9 Chlorobenzene
10 D ibromoch lor ometh ane
11 Chloroethane
12 2-Chloroethylvlnyl ether
13 Chloroform
14 chloromethane
15 1-Dichloroethane
16 1,2-D ichloroethane
17 1,1-Dichloroethene
18 1,2<-Dichloroethene (total)
19 1,^-Dichloropropane
20 cis-l,3-'Dichloropropene
21 trans-1,3-Dichloropropen©
22 Ethylbenzene
23 2-Hexanone
24 Methylene chloride
25 4-Methyl-2-pentanone
26 Styrene
27 1,1,2,2-Tetrachloroethane
28 Tetrachloroethene
29 Toluene
30 1r1,1-Trichloroethane
31 1/If2-Trichloroethane
32 Trlchloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenes (total)
Byx Harris
intitation Results
Limit Concentration
(ug/kg)(ug/kg)
100 BQL
5 BQL
S BQL
5 BQL
10 BQL
100 BQL
5 BQL
5 BQL
5 BQL
5 BQL
10 BQL
10 BQL
5 BQL
10 BQL
s BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
50 BQL
5 BQL
SO BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
5 BQL
50 BQL
10 BQL
5 BQL
Comments;
BQL » Below Quantitation Limit
base/neutral/acio extractablss
SW-846 METHOD 8270
ISA Sample Numberx 916^045-2
Sample Identification} 1311
Date Extracted: 10/02/90
Date Analysed; 10/06/90 By: Mace
Ouantitation Rei
Limit Conce:
Number Compound <ug/kg)(u.
1 Acenaphthene 200 BQL
2 Acenaphthylene 200 BQL
3 Anthracene 200 BQIv
4 Benzole acid 1000 BQL
5 Benso{a}anthracene 200 BQL
6 Benzo{b}fluoranthene 200 BQL
7 Benso(k)fluoranthene 200 BQL
8 Benso(g,h,i)perylene 200 BQL
9 Benzo(a)pyrene 200 BQL
10 Benzyl alcohol 400 BQL
11 bis(2-chloroethoxy)methane 200 BQL
12 bis(2-chloroethyl)ether 200 BQL
13 bis(2-Chloroisopropyl)ether 200 BQL
14 bis(2-Ethy1hexy1)phtha1ate 200
15 4-Bromophenyl phenyl ether 200 BQL
16 Benzyl butyl phthalate 200 BQL
17 4-Chioroaniline 400 BQL
IS 2-Chloronaphthalene 200 BQL
19 4-Chloro-3-methylphenol 400 BQL
20 2-Chlorophenol 200 BQL
21 4-Chlorophenyl phenyl ether 200 BQL
22 Chrysene 200 BQL
23 D iben so(a,h)anthracene 200 BQL
24 Dibenzofuran 200 BQL
25 Di-n-butylphthalate 200 BQL
26 1,3-Dichlorobenzene 200 BQL
27 1,4-Dichlorobensene 200 BQL
28 1,2-D ichlorobensene 200 BQL
29 3,3'-Dichlorobensidine 400 BQL
30 2,4-Dichlorophenol 200 BQL
31 Diethyl phthalate 200 BQL
32 2,4~Dimethylphenol 200 BQL
33 Dimethyl phthalate 200
34 4,6-Dinitro-2-niethylphenol 1000 BQL
35 2,4-Dinitrophenol 1000 BQL
36 2,4-Dinitrotoluene 200 BQL
37 2,6-Dinitrotoluene 200 BQL
38 Di-n-octylphthalate 200 BQL
39 Fluoranthene 200 BQL
2,100
320
FORM 8270 (1)Rev. 050589
uui-iD-yu riUN utuuntn iiHu.rnA nu. oianouuioj
basb/neutral/acid extractables
SW-846 METHOD 8270
r. ui
ISA Sample Number: 916-045-2
Sample Identification: 1311
Date Extracted: 10/02/90
Date Analyzed: 10/06/90 By: Mace
Number Compound
40 Fluorene
41 Hexachlorobenzene
42 Hexachlorobutadlene
43 Hexachlorocyclopentadiene
44 Hexachloroethane
45 tndeno(1/2,3-cd)pyrene
46 leophorone
47 2-Methylnaphthalene
48 2-Methylphenol (o-cresol)
49 4-Methylphenol (p-cresol)
50 Naphthalene
51 2-Nitroaniline
52 3-Kitroaniline
53 4-Nitroaniline
54 Nitrobenzene
55 2-Nitrophenol
56 4-Nitrophenol
57 N-Nitrpso-di-n-propylamine
53 N-Kitroaodiphenylamine
59 Fentachlcrophenol
60 Phenanthrene
61 Phenol
62 Pyrene
63 1,2,4-Trlchlorobenzene
64 2,4,5-Trichlorophenol
65 2,4,e-Trlchlorophenol
Qudntitation
Limit
(ug/kg)
200
200
200
200
200
200
200
200
200
200
200
1000
1000
1000
200
200
1000
200
200
1000
200
200
200
200
200
200
Results
Concentration
(ug/kg)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Comments:
BQL B Below Quantitation Limit
FORM 8270 (2)Rev. 050589
base/neutral/acid EXTKACTABLES
SW-846 METHOD 8270
lEA Sarople Number: 918-045-3
Sample Identification: 1312
Date Extracted: 10/02/90
Date Analyzed; 10/06/90 By: Mace
Number Compound
Quantitation
Limit
(ug/kg)
1 Acenaphthene 200
2 Acenaphthylene 200
3 Anthracene 200
4 Benzoic acid 1000
5 Benzo(a)anthracene 200
6 Benzo(b}fluoranthene 200
7 Ben2o(k}fluoranthene 200
a Benzo(g,h,i)perylene 200
9 Benzo(a)pyrene 200
10 Benzyl alcohol 400
11 b is(2-Chloroethoxy)methane 200
12 bis(2-Chloroethy1)ether 200
13 bi e(2-Chlor0 isopropyl)ether 200
14 bis(2-Ethylhexyl)phthalate 200
15 4-Bromophenyl phenyl ether 200
16 Benzyl butyl phthalate 200
17 4-chloroaniline 400
18 Z-Chloronaphthalene 200
19 4-Chloro-3-rnethylphenol 400
20 2-Oh1oropheno1 200
21 4-Chlorophenyl phenyl ether 200
22 Chryeene 200
23 Dibenzo(a^ h)anthracene 200
24 Dibenzofuran 200
25 Di-n-butylphthalate 200
26 1,3-Dichlorobenzene 200
27 1t4'Dichlorobenzene 200
28 li 2'Dichlorobenzene 200
29 3,3'-Dichlorobenzidlne 400
30 2t4-Dichlorophenol 200
31 Diethyl phthalate 200
32 2,4'Dimethylphenol 200
33 Dimethyl phthalate 200
34 4,6-Dinitro-2-methylphenol 1000
35 2,4-Dinitrophenol lOOO
36 2,4-Oinitrotoluene 200
37 2,6-Dinitrotoluene 200
3a Di-n-octylphthalate 200
39 Fluoranthene 200
Results
Concentration
(ug/kg)
SQL
BQL
BQL
BQL
BQL
BQL
SQL
BQL
BQL
BQL
BQL
BQL
EQL
480
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
FORM 8270 (1)Rev, 050589
uui-io-yu nuN u:ud UhUUHtri iNU.i'm (HU. yid^DUUidf
base/neutral/acid exxractables
SW-a46 METHOD 8270
Ud
IGA Sample Number: 916-045-3
Sample Identification,' 1312
Date Extracted: 10/02/90
Date Analyzed: 10/06/90 By: Hace
Number Compound
Comments:
BQL s Below Quantitation Limit
Quant it at ion
Limit
(ug/kg)
Results
Concentration
(ug/kg)
40 Fluorene 200 BQL
41 Kexachlorobenzene 200 BQL
42 Hexachlorobutadiene 200 BQL
43 Kexachlorocyclopentadiene 200 BQL
44 Hexachloroethane 20l BQL
45 Indeno(1,2,3-ed)pyrene 200 BQL
46 iBOphorone 200 BQL
47 2-Methylnaphthalene 2C BQL
48 2-MethylphenoI (o-cresol)20 BQL
49 4''MethylphenoI (p-cresol)200 BQL
50 Naphthalene 200 BQL
51 2-Nitroaniline 1000 BQL
52 3-Nitroaniiine 1000 BQL
53 4-Nitroaniline 1000 SQL
54 Nitrobenzene 200 BQL
55 2<-Nitrophenol 200 BQL
56 4-Nitrophenol 1000 BQL
57 N-Nitroso-di-n-propylamine 200 BQL
58 N-Nitrosodiphenylamine 200 BQL
59 Pentachlorophenol 1000 BQL
60 Phenanthrene 200 BQL
61 Phenol 200 SQL
62 Pyren©200 BQL
63 1,2,4-TrichlorQbenzene 200 BQL
64 2,4,5-Trichlorophenol 200 BQL
65 2,4,6-Trichlorophenol 200 BQL
TOUH 8270 (2)Rev. 0S0589
APPLIED
ENVIRONMENTAL
SERVICES,
INC.
Laboratory Name;
1805 Running Oak Drive. Rateigh. NC 27612
Post Office Box 1145, Cary. NC 27512
919-787-8209 n FAX [phone]
Chain of Custody Record
Report To:
Page of.
PROJECT#^ CLIENT#^
ON .OFCOSRENIATN PEROITACOLN
ANALYSES
kH !
/w////
/ LABORATORY PROJECT tt 0^"—
PROJECT NAME // ^/ / DATE REPORT DUE
t j VERBALFAX;HARDCOPY
Ffm
SAMPLE JD
TURNAROUND
IN DAYS
SAMPLE
MATRIX
DATE
COLLECTED
/ LAB ID NO.
/ REMARKS fab use onfy^
^'/7 /!3,iO
/r f-/S ,'3 / (
/r"2
f 1
■>flELINQUJSHEDBY: ^-DATE TIME
5 ^CEiv^eyj DATE
9-z/~9o
TIME
\r.-oo
RE^^UISHED BY:DATE TIME RECEIVED BY:DAT^'TIME RELINQUISHED BY:DATE TIME
->
RECEIVED BY:DATE TIME RELINQUISHED BY:DATE TIME RECEIVED BY:DATE TIME RELINQUISHED BY:DATE TIME
White/Laboratory C{H>y, Yellow/Accounting Copy, Pink.'Fite Copy
GeoChem, Incorporated
Environmental Laboratories
nj J V i { ' I
j I November 23, 1990
Mr. Joe Mattheis ' " '
Applied Environmental Services
1805 Running Oak Drive
Raleigh, NC 27612
Reference: Murphy
A100372
GCI# 9010-083
Dear Mr, Joe Mattheis:
This is the analytical report for the above referenced
project. on October 30, 1990 we received three soil samples for
analysis. The TCLP work was subcontracted to lEA and data will
appear on lEA's letterhead.
If there are any technical questions please feel free to call
me at 919-460-8093. Thank you for allowing GkoChem to serve your
analytical needs.
S-incej-ely
"Dean Gokel
President
2500 Gate Way Centre Blvd., Suite 300 • Morrlsville. NC 27560
Telephone: [phone] • FAX: [phone]
lEA LABORATORY RESULTS
lEA Project #;
Client Name:
916-062
GeoChem, Inc.
Sample # Client ID Parameter Results
Date
Analyzed
1 SAl-1753 Arsenic <0.50 mg/L 11/09/90
2 SA2-1754 Arsenic <0.50 mg/L 11/09/90
3 STB-1755 Arsenic <0.50 mg/L 11/09/90
1 SAl-1753 Barium <10 mg/L 11/15/90
2 SA2-1754 Barium <10 mg/L 11/15/90
3 STB-1755 Barium <10 mg/L 11/15/90
1 SAl-1753 Cadmium <0.10 rag/L 11/15/90
2 SA2-1754 Cadmium <0.10 mg/L 11/15/90
3 STB-1755 Cadmium <0.10 mg/L 11/15/90
1 SAl-1753 Chromium <0.50 mg/L 11/15/90
2 SA2-1754 Chromium <0.50 mg/L 11/15/90
3 STB-1755 Chromium <0.50 rag/L 11/15/90
1 SA1-17S3 Mercury <0.0005 rog/L 11/12/90
2 SA2-1754 Mercury <0.0005 mg/L 11/12/90
3 STB-1755 Mercury <0.0005 mg/L 11/12/90
1 SAl-1753 Lead <0.50 mg/L 11/09/90
2 SA2-1754 Lead <0.50 mg/L 11/08/90
3 STB-1755 Lead /<0.50 mg/L 11/08/90
1 SAl-1753 Selenium <0.10 rag/L 11/10/90
2 SA2-1754 Selenium <0.10 rag/L 11/10/90
3 STB-1755 Selenium <o'; 10 rag/L 11/10/90
1 SAl-1753 Silver <0.50 mg/L 11/15/90
2 SA2-1754 Silver <0.50 mg/L 11/15/90
3 STB-175S Silver <0.50 mg/L 11/15/90
1 SAl-1753 Sulfur 1.0 mg/L*11/16/90
2 SA2-1754 Sulfur 1.1 mg/L*11/16/90
3 STB-17SS Sulfur 0.69 mg/L*11/16/90
1 SAl-1753 Chloride 6.3 mg/L*11/14/90
2 SA2-1754 Chloride 3.1 mg/L*11/14/90
3 STB-1755 Chloride 3.9 mg/L*11/14/90
1 SAl-1753 Corrosivity <6.35 mmpy 11/02/90
2 SA2-1754 Corrosivity <6.35 mmpy 11/02/90
3 STB-1755 Corrosivity <6.35 mmpy 11/02/90
1 SAl-1753 Ignitahility >200 F 11/14/90
2 SA2-1754 Ignitability >200 F 11/14/90
3 STB-1755 Ignitability >200 F 11/14/90
1 SAl-1753 Ammonia-N <0.1 mg/L*11/12/90
3 STB-1755 Ammonia-N <0.1 mg/L*11/12/90
2 SA2-1754 Ammonia-N <0.1 mg/L*11/12/90
lEA LABORATORY RESULTS
lEA Project #;
Client Name:
Sample # Client ID
916-062
GecChem, Inc.
Parameter Results
Date
Analyzed
SAl-1753
SA2-1754
STB-1755
Total Kjeldahl Nitrogen
Total Kjeldahl Nitrogen
Total Kjeldahl Nitrogen
0.68 mg/L*
<0.10 mg/L*
<0.10 mg/L*
11/09/90
11/09/90
11/09/90
Comments:
* Analysis performed on TCLP leachate.
TCLP/ZHEGC/MS PURGEABLESSW-846 METHOD 8240lEA Sample Number: 916-062-1Sample Identification: SA1-17S3TCLP/ZHE Extraction Date: 11/01/90Date Analyzed: 11/13/90By: HarrisNtimber Compound1 Acetone2 Benzene3 Bromodichloromethane4 Bromoform5 Bromomethane6 2-Butanone7 Carbon disulfide8 Carbon tetrachloride9 chlorobenzene10 Dibromochloromethane11 Chloroethane12 2-Chloroethylvinyl ether13 Chloroform14 chlororaethane15 1,1-Dichloroethane16 1,2-D ichloroethane17 1,1-Dichloroethene18 1,2-Dichloroethene (total)19 1/2-Dichloropropane20 c is-1,3-D ichloropropene21 trans-1,3-Dichloropropene22 Ethylbenzene23 2-Hexanone24 Methylene chloride2 5 4-Methy1-2-pentanone26 Styrene27 1,1,2,2-Tetrachloroethane28 Tetrachloroethene29 Toluene30 1,1,1-Trichloroethane31 1,1,2-Trichloroethane32 Trichloroethene33 Vinyl acetate34 Vinyl chloride35 Xylenes (total)QuantitationLimit(ug/L)200101010202001010101020201020101010101010101010010100101010101010101002010ResultsConcentrat ion(ug/L)850BQLSQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL243055059Comments:BQL = Below Quantitation LimitQuantitation limit elevated due to sample dilution prior to analysis.Sample diluted due to high concentration of target compounds presentFORM 8240-ZHE Rev. 082790
TCLP/ZHE
GC/MS PURGEABLES
SW-846 METHOD 8240
lEA Sample Niimber: 916-062-2
Sample Identification: SA2-1754
TCLP/ZHE Extraction Date: 11/01/90
Date Analyzed:
By: Harris
11/13/90
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bromoform
5 Bromomethane
6 2-Butanone
7 Carbon disulfide
a Carbon tetrachloride
9 Chlorobenzene
10 Dibromochloromethane
11 Chloroethane
12 2-Chloroethylvinyl ether
13 Chloroform
14 Chloromethane
15 1,1-Dichloroethane
16 1,2-Dichloroethane
17 1,1-Dichloroethene
18 1,2-Dichloroethene (total)
19 1,2-Dichloropropane
20 cis-l,3-Dichloropropene
21 trans-1,3-D ichloropropene
22 Ethylbenzene
23 2-Hexanone
24 Methylene chloride
25 4-Methyl-2-pentanone
26 Styrene
27 1,1,2,2-Tetrachloroethane
28 Tetrachloroethene
29 Toluene
30 1,1,1-Trichloroethane
31 1,1,2-Trichloroethane
32 Trichloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenes (total)
Qu ant it at ion
Limit
(ug/L)
100
5
5
5
10
100
5
5
5
5
10
10
5
10
5
5
5
5
5
5
5
5
50
5
50
5
5
5
5
5
5
5
50
10
5
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
24
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
25
Comments:
BQL = Below Quantitation Limit
FORM 8240-ZHE Rev. 082790
TCLP/ZHE
GC/MS PURGEABLES
SW-846 METHOD 8240
lEA Sample Number: 916-062-3
Sample Identification: STB-1755
TCLP/ZHE Extraction Date: 11/01/90
Date Analyzed: 11/13/90
By: Casto
Number Compound Quantitation
Limit
(ug/L)
Results
Concentration
<ug/L)
1 Acetone 100 BQL
2 Benzene 5 BQL
3 Bromodichloromethane 5 BQL
4 Bromoform 5 BQL
5 Bromomethane 10 BQL
6 2-Butanone 100 BQL
7 Carbon disulfide 5 BQL
a Carbon tetrachloride 5 BQL
9 Chlorobenzene 5 BQL
10 D ibromochloromethane 5 BQL
11 Chloroethane 10 BQL
12 2-Chloroethylvinyl ether 10 BQL
13 Chloroform 5 BQL
14 Chloromethane 10 BQL
15 1,1-D ichloroethane 5 BQL
16 1,2-Dichloroethane 5 BQL
17 1,1-Dichloroethene 5 BQL
18 1,2-Dichloroethene (total)5 BQL
19 1,2-Dichloropropane 5 BQL
20 cis-1,3-Dichloropropene 5 BQL
21 trans-l,3-Dichloropropene 5 BQL
22 Ethylbenzene 5 BQL
23 2-Hexanone SO - BQL
24 Methylene chloride 5
25 4-Methyl-2-pentanone 50 BQL
26 Styrene 5 BQL
27 1,1,2,2 -Tetrachloroethane 5 BQL
28 Tetrachloroethene 5 BQL
29 Toluene 5 BQL
30 1,1,1-Trichloroethane 5 BQL
31 1,1,2-Trichloroethane 5 BQL
32 Trichloroethene 5 BQL
33 Vinyl acetate 50 BQL
34 Vinyl chloride 10 BQL
35 Xylenes (total)5 BQL
Comments:
17
BQL « Below Quantitation Limit
FORM 8240-ZHE Rev. 082790
TCLP/ZHE
GC/MS PURGEABLES
SW-846 METHOD 8240
lEA Sample Number: 916-062
Sample Identification: ZHE Blk 60
TCLP/ZHE Extraction Date: 11/01/90
Date Analyzed: 11/13/90
By: Harris
Number Compound
1 Acetone
2 Benzene
3 Bromodichloromethane
4 Bromoform
5 Bromomethane
6 2-Butanone
7 Carbon disulfide
a Carbon tetrachloride
9 chlorobenzene
10 Dibromochloromethane
11 Chloroethane
12 2-Chloroethylvinyl ether
13 Chloroform
14 Chloromethane
15 1,1-Dichloroethane
16 1,2-Dichloroethane
17 1,1-Dichloroethene
18 1/2-Dichloroethene (total)
19 1,2-Dichloropropane
20 cis-l,3-Dichloropropene
21 trans-l,3-Dichloropropene
22 Ethylbenzene
23 2-Hexanone
24 Methylene chloride
25 4-Methyl-2-pentanone
26 Styrene
27 1,1,2,2-Tetrachloroethane
28 Tetrachloroethene
29 Toluene
30 1,1,1-Trichloroethane
31 1,1,2-Trichloroethane
32 Trichloroethene
33 Vinyl acetate
34 Vinyl chloride
35 Xylenes (total)
Qu ant it at ion
Limit
(ug/L)
100
5
5
5
10
100
5
5
5
5
10
10
5
10
5
5
5
5
5
5
5
5
SO
5
50
5
5
5
5
5
5
5
50
10
5
Results
Concentration
(ug/L)
140
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
26
10
38
Comments:
BQL s Below Quantitation Limit
FORM a240-ZHE Rev. 082790
lEA Sample Number:
Sample Identification:
TCLP Extraction Date:
TCLP
base/neutral/acid EXTRACTABLES
SW-846 METHOD 8270
916-062-1
SAl-1753
11/01/90
Date Extracted:
Date Analyzed:
By: Mace
11/08/90
11/14/90
Quantitation
Limit
Number Compound (ug/L)
1 Acenaphthene 25
2 Acenaphthylene 25
3 Anthracene 25
4 Benzoic acid 120
5 Benzo(a)anthracene 25
6 Benzo(b> fluoranthene 25
7 Benzo(k)fluoranthene 25
a Benzo(g,h,i)perylene 25
9 Benzo(a)pyrene 25
10 Benzyl alcohol 50
11 bis(2-Chloroethoxy)methane 25
12 bis(2-Chloroethy1)ether 25
13 bis(2-Chloroisopropyl)ether 25
14 bis(2-Ethylhexyl)phthalate 25
15 4-Bromophenyl phenyl ether 25
16 Benzyl butyl phthalate -25
17 4-Chloroaniline 50
IS 2-Chloronaphthalene 25
19 4-Chloro-3-methylphenol 50
20 2-Chlorophenol 25
21 4-Chlorophenyl phenyl ether 25
22 Chrysene 25
23 Dibenzo(a,h)anthracene 25
24 Dibenzofuran 25
25 Di-n-butylphthalate 25
26 1,3-Dichlorobenzene 25
27 1,4-Dichlorobenzene 25
28 1,2-D ichlorobenzene 25
29 3,3'-Dichlorobenzidine 50
30 2,4-Dichlorophenol 25
31 Diethyl phthalate 25
32 2,4-Dimethylphenol 25
33 Dimethyl phthalate 25
34 4,6-Dinitro-2-methylphenol 120
35 2,4-Dinitrophenol 120
36 2,4-Dinitrotoluene 25
37 2,6-Dinitrotoluene 25
38 Di-n-octylphthalate 25
39 Fluoranthene 25
FORM TCLP-8270 (1) Rev. 082790
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
lEA Sample Number:
S ample Ident if ication:
TCLP Extraction Date:
TCLP
base/neutral/acid extractables
SW-846 METHOD 8270
916-062-1
SA1-17S3
11/01/90
Date Extracted;
Date Analyzed:
By: Mace
11/08/90
11/14/90
Nimiber Compound
40 Fluorene
41 Hexachlorobenzene
42 Hexachlorobutadiene
43 Hexachlorocyclopentadiene
44 Hexachloroethane
45 Indeno(l,2,3-cd)pyrene
46 Isophorone
47 2-Methylnaphthalene
48 Total Cresol
49 Naphthalene
50 2-Nitroaniline
51 3-Nitroaniline
52 4-Nitroemiline
53 Nitrobenzene
54 2-Nitrophenol
55 4-Nitrophenol
56 N-Nitroso-di-n-propylamine
57 N-Nitroaodiphenylamine
58 Pentachlorophenol
59 Phenanthrene
60 Phenol
61 Pyrene
62 1,2,4-Trichlorobenzene
63 2,4,5-Trichlorophenol
64 2,4,6-Trichlorophenol
65 Pyridine
Azobenzene
Quantitation
Limit
(ug/L)
25
25
25
25
25
25
25
25
25
25
120
120
120
25
25
120
25
25
120
25
25
25
25
25
25
10
10
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Comments:
BQL = Below Quantitation Limit
FORM TCLP-8270 (2)Rev. 082790
lEA Sample Number;
Sample Identification;
TCLP Extraction Date;
TCLP
base/neutral/acid EXTRACTABLES
SW-846 METHOD 8270
916-062-2
SA2-1754
11/01/90
Date Extracted:
Date Analyzed:
By: Mace
11/08/90
11/15/90
Number Compound
1 Acenaphthene
2 Acenaphthylene
3 Anthracene
4 Benzole acid
5 Benzo(a)anthracene
6 Benzo(b)fluoranthene
7 Benzo(k)fluoranthene
8 Benzo(g,h,i)perylene
9 Benzo(a)pyrene
10 Benzyl alcohol
11 bis(2-Chloroethoxy)methane
12 bis (2-Chloroethyl)ether
13 bis(2-Chloroisopropyl)ether
14 bis (2-Ethylhexyl)phthalate
15 4-Bromophenyl phenyl ether
16 Benzyl butyl phthalate /
17 4-Chloroaniline
18 2-Chloronaphthalene
19 4-Chloro-3-methylphenol
20 2-Chlorophenol
21 4-Chlorophenyl phenyl ether
22 Chrysene
23 Dibenzo(a,h)anthracene
24 Dibenzofuran
25 Di-n-butylphthalate
26 1,3-Dichlorobenzene
27 1,4-Dichlorobenzene
28 1,2-Dichlorobenzene
29 3,3'-Dichlorobenzidine
30 2,4-Dichlorophenol
31 Diethyl phthalate
32 2,4-Dimethylphenol
33 Dimethyl phthalate
34 4,6-Dinitro-2-methylphenol
35 2,4-Dinitrophenol
36 2,4-Dinitrotoluene
37 2,6-Dinitrotoluene
38 Di-n_octylphthalate
39 Fluoranthene
antitation Results
Limit Concentration
(ug/L)(ug/L)
25 BQL
25 BQL
25 BQL
120 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
50 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
50 BQL
25 BQL
SO BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
50 BQL
25 BQL
25 BQL
25 BQL
25 BQL
120 BQL
120 BQL
25 BQL
25 BQL
25 BQL
25 BQL
FORM TCLP-8270 (1)Rev. 082790
TCLP
base/neutral/acid extractables
SW-846 METHOD 8270
XEA Sample Number:
Sample Identification:
TCLP Extraction Date:
916-062-2
SA2-1754
11/01/90
Number Compound
40 Fluorene
41 Hexachlorobenzene
42 Hexachlorobutadiene
43 Hexachlorocyclopentadiene
44 Hexachloroethane
45 Indeno(l,2,3-cd)pyrene
46 Isophorone
47 2-Methylnaphthalene
48 Total Cresol
49 Naphthalene
50 2-Nitroaniline
51 3-Nitroaniline
52 4-Nitroaniline
53 Nitrobenzene
54 2-Nitrophenol
55 4-Kitrophenol
5 6 N-Nitroso-di-n-propy lamine
57 N-Nitrosodiphenylamine
58 Pentachlorophenol
59 Phenanthrene
60 Phenol
61 Pyrene
62 If 2,4-Trichlorobenzene
63 2,4,5-Trichlorophenol
64 2,4,6-Trichlorophenol
65 Pyridine
Azobenzene
Date Extracted: 11/08/90
Date Analyzed:11/15/90
By: Mace
antitation Results
Limit Concentration
(ug/L)(ug/L)
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
120 BQL
120 BQL
120 BQL
25 BQL
25 BQL
120 BQL
25 BQL
25 BQL
120 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
25 BQL
10 BQL
10 BQL
Comments:
BQL « Below Quantitation Limit
FORM TCLP-8270 (2)Rev, 082790
TCLP
base/neutral/acid extractables
SW-a46 METHOD 8270
lEA Sample Number: 916-062-3
Sample Identification: STB-1755
TCLP Extraction Date; 11/01/90
Date Extracted:
Date Analyzed:
By: Mace
11/08/90
11/15/90
Quant itat ion
Limit
Number Compound (ug/L)
1 Acenaphthene 25
2 Acenaphthylene 25
3 Anthracene 25
4 Benzoic acid 120
5 Benzo(a)anthracene 25
6 Benzo(b)fluoranthene 25
7 Benzo(k) fluoranthene 25
8 Benzo(g,h,i)perylene 25
9 Benzo(a)pyrene 25
10 Benzyl alcohol 50
11 bis(2-Chloroethoxy)methane 25
12 bis < 2-Chloroethy1)ether 25
13 bis(2-Chloroiaopropyl)ether 25
14 bis(2-Ethylhexyl)phthalate 25
15 4—Bromophenyl phenyl ether 25
16 Benzyl butyl phthalate ./25
17 4-Chloroaniline 50
18 2-Chloronaphthalene 25
19 4-Chloro-3-methylphenol 50
20 2-Chlorophenol 25
21 4-Chlorophenyl phenyl ether 25
22 Chrysene 25
23 Dibenzo(a,h)anthracene 25
24 Dibenzofuran 25
25 Di-n-butylphthalate 25
26 1,3-Dichlorobenzene 25
27 1,4-Dichlorobenzene 25
28 1,2-Dichlorobenzene 25
29 3,3'-Dichlorobenzidine 50
30 2,4-D ichlorophenol 25
31 Diethyl phthalate 25
32 2,4-Dimethylphenol 25
33 Dimethyl phthalate 25
34 4,6-Dinitro-2-methylphenol 120
35 2,4-Dinitrophenol 120
36 2,4-Dinitrotoluene 25
37 2,6-Dinitrotoluene 25
38 Di-n-octylphthalate 25
39 Fluoranthene 25
FORM TCLP-8270 (1) Rev. 082790
Results
Co nc ent r at ion
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
lEA Sample Number:
Sample Identification:
TCLP Extraction Date;
TCLP
BASE/NEUTRAL/ACID EXTRAGTABLES
SW-846 METHOD 8270
916-062-3
STB-17S5
11/01/90
Date Extracted:
Date Analyzed:
By: Mace
11/08/90
11/15/90
Nvutiber Compound
40 Fluorene
41 Hexachlorobenzene
42 Hexachlorobutadiene
43 Hexachlorocyclopentadiene
44 Hexachloroethane
45 Indeno (1,2,3-cd) pyrene
46 Isophorone
47 2-Methylnaphthalene
48 Total Cresol
49 Naphthalene
50 2-Nitroaniline
51 3-Nitroaniline
52 4-Nitroaniline
53 Nitrobenzene
54 2-Nitrophenol
55 4-Nitrophenol
56 N-Nitroso-di-n-propylamine
57 N-Nitrosodiphenylamine
58 Pentachlorophenol
59 Phenanthrene
60 Phenol
61 Pyrene
62 1,2,4-Trichlorobenzene
63 2,4,5-Trichlorophenol
64 2,4,6-Trichlorophenol
65 Pyridine
Azobenzene
Quantitation
Limit
(ug/L)
25
25
25
25
25
25
25
25
25
25
120
120
120
25
25
120
25
25
120
25
25
25
25
25
25
10
10
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
-.«!
Comments:
BQL — Below Quantitation Limit
FORM TCLP-8270 (2)Rev. 082790
TCLP
base/neutral/acid extractables
SW-846 METHOD 8270
lEA Sample Number:
Sample Identification:
TCLP Extraction Date:
916-062
TCLP Blk 105
11/01/90
Date Extracted:
Date Analyzed:
By: Mace
11/08/90
11/15/90
Qu ant it at ion Results
Limit Concentration
umber Compound (ug/L)(ug/L)
1 Acenaphthene 25 BQL
2 Acenaphthylene 25 BQL
3 Anthracene 25 BQL
4 Benzoic acid 120 BQL
5 Benzo(a)anthracene 25 BQL
6 Benzo(b)flucranthene 25 BQL
7 Benzo(k) fluoranthene 25 BQL
8 Benzo (g, h, i) perylene 25 BQL
9 Benzo(a)pyrene 25 BQL
10 Benzyl alcohol 50 BQL
11 bia (2-Chloroethoxy)methane 25 BQL
12 bis(2-Chloroethyl)ether 25 BQL
13 bis(2-Chloroisopropyl)ether 25 BQL
14 bis(2-Ethylhexyl)phthalate 25 BQL
15 4-3romophenyl phenyl ether 25 BQL
16 Benzyl butyl phthalate 25 BQL
17 4-Chloroaniline 50 BQL
18 2-Chloronaphthalene 25 BQL
19 4-Chloro-3-methylphenol 50 BQL
20 2-Chlorophenol 25 BQL
21 4-Chlorophenyl phenyl ether 25 BQL
22 Chrysene 25 BQL
23 D ibenzo (a, h} anthracene 25 BQL
24 Dibenzofuran 25 BQL
25 Di-n-butylphthalate 25 BQL
26 1,3-Dichlorobenzene 25 BQL
27 1,4-Dichlorobenzene 25 BQL
28 1,2-DichlorQbenzene 25 BQL
29 3,3' -Dichlorobenzidine 50 BQL
30 2,4-Dichlorophenol 25 BQL
31 Diethyl phthalate 25 BQL
32 2,4-Dimethylphenol 25 BQL
33 Dimethyl phthalate 25 BQL
34 4,6-Dinitro-2-raethylphenol 120 BQL
35 2,4-Dinitrophenol 120 BQL
36 2,4-Dinitrotoluene 25 BQL
37 2,6-Dinitrotoluene 25 BQL
38 Di-n-octylphthalate 25 BQL
39 Fluorsmthene 25 BQL
FORM TCLP-8270 (1)Rev. 082790
TCLP
base/neutral/acid extractables
SW-846 METHOD 8270
916-062 Date Extracted; 11/08/90
Sample Identification: TCLP Blk 105 Date Analyzed:11/15/90
TCLP Extraction Date; 11/01/90 By: Mace
Quant it at io n Results
Limit Concentration
Number Compound (ug/L)(ug/L)
40 Fluorene 25 BQL
41 Hexachlorobenzene 25 BQL
42 Hexachlorobutadiene 25 BQL
43 Hexachlorocyclopentadiene 25 BQL
44 Hexachloroethane 25 BQL
45 Indeno(1,2,3-cd)pyrene 25 BQL
46 Isophorone 25 BQL
47 2-Methylnaphthalene 25 BQL
48 Total Cresol 25 BQL
49 Naphthalene 25 BQL
50 2-Nitroaniline 120 BQL
51 3-NitrocUiiline 120 BQL
52 4-Nitroaniline 120 BQL
53 Nitrobenzene 25 BQL
54 2-Nitrophenoi 25 BQL
55 4-Nitrophenol 120 BQL
56 N-Nitroso-di-n-propylamine 25 BQL
57 N-Nitrosodiphenylamine 25 BQL
58 Pentachlorophenol 120 BQL
59 Phenanthrene 25 BQL
60 Phenol 25 BQL
61 Pyrene 25 BQL
62 1,2,4-Trichlorobenzene 25 BQL
63 2,4,5-Trichlorophenol 25 BQL
64 2,4,6-Trichiorophenol 25 BQL
65 Pyridine 25 BQL
Azobenzene 25 BQL
Comments:
BQL » Below Quantitation Limit
FORM TCLP-8270 (2)Rev. 082790
TCLP
PESTICIDES / PCBa
SW-a46 METHOD 8080
lEA Sample Niunber: 916-062-1
Sample Identification: SAl-1753
TCLP Extraction Dates 11/01/90
Date Extracted:
Date Analyzed:
By: Travis
11/07/90
11/08/90
Number Compound
1 alpha-BHC
2 beta-BHC
3 delta-BHC
4 gamma-BHC (Lindane)
5 Heptachlor
6 Aldrin
7 Heptachlor epoxide
8 Endosulfan I
9 Dieldrin
10 4,4'-DDE
11 Endrin
12 Endosulfan II
13 4,4'-DDD
14 Endosulfan sulfate
15 4,4'-DDT
16 Methoxychlor
17 Toxaphene
18 Aroclor 1016
19 Aroclor 1221
20 Aroclor 1232
21 Aroclor 1242
22 Aroclor 1248
23 Aroclor 1254
24 Aroclor 1260
25 Chlordane (technical)
26 Endrin aldehyde
Quantitation
Limit
(ug/L)
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.50
0.50
0.50
0.50
0.50
0.50
2.5
5.0
2.5
2.5
2.5
2.5
2.5
5.0
5.0
2.5
0.50
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Additional Compounds:
27 Endrin ketone
28 alpha-Chlordane
29 gamma-Chlordane
Comments:
BQL =» Below Quantitation Limit
0.50
2.5
2.5
BQL
BQL
BQL
FORM TCLP-8080 Rev. 082790
TCLPPESTICIDES /PCBaSW-846 METHOD8080lEA Sample Number: 916-062-2Date Extracted:11/07/90SampleIdentification: SAl-1754Date Analyzed:11/08/90TCLP Extraction Date: 11/01/90By: TravisQuantitationResultsLimit ConcentrationNumberCompound(ug/L)(ug/L)1alpha-BHC0.25BQL2beta-BHC0.25SQL3delta-BHC0.25BQL4gamma-BHC (Lindane)0.25BQL5Heptachlor0.25BQL6Aldrin0.25BQL7Heptachlor epoxide0.25BQL8Endosulfan I0.25BQL9Dieldrin0.25BQL104,4'-DDE0.50BQL11Endrin0.50BQL12Endosulfan II0.50BQL134,4'-DDDO.SOBQL14Endosulfan sulfate0.50BQL154,4'-DDT0.50BQL16Methoxychlor2.5BQL17Toxaphene5.0BQL18Aroclor 10162.5BQL19Aroclor 12212.5BQL20Aroclor 12322.5BQL21Aroclor 12422.5BQL22Aroclor 12482,5BQL23Aroclor 12545.0BQL24Aroclor 12605.0BQL25Chlordane (technical)2.5BQL26Endrin aldehyde0.50BQLAdditional Compounds:27Endrin ketone0.50BQL28alpha-Chlordane2.5BQL29gamma-Chlordane2.5BQLComments:SQL = Below Quantitatlon LimitFORM TCLP-a080Rev. 082790
TCLP
PESTICIDES / PCBs
SW-a46 METHOD 8080
lEA Sample Number: 916-062-3
Sample Identification: STB-1755
TCLP Extraction Date; 11/01/90
Date Extracted: 11/07/90
Date Analyzed: 11/07/90
By: Travis
Quantitation
Limit
Number Compound (ug/L)
1 alpha-BHC 0.25
2 beta-BHC 0.25
3 delta-BHC 0.25
4 gamma-BHC (Lindane)0.25
5 Heptachlor 0.25
6 Aldrin 0.25
7 Heptachlor epoxide 0.25
8 Endosulfan I 0.25
9 Dieldrin 0.25
10 4,4'-DDE 0.50
11 Endrin 0.50
12 Endosulfan II 0.50
13 4,4'-DDD 0.50
14 Endosulfan sulfate 0.50
15 4,4'-DDT 0.50
16 Methoxychlor 2.5
17 Toxaphene 5.0
18 Aroclor 1016 2.5
19 Aroclor 1221 2.5
20 Aroclor 1232 2.5
21 Aroclor 1242 2.5
22 Aroclor 1248 2.5
23 Aroclor 1254 5.0
24 Aroclor 1260 5.0
25 Chlordane (technical)2.5
26 Endrin aldehyde 0.50
Additional Compounds:
27 Endrin ketone 0.50
28 alpha-Chlordane 2.5
29 gamma-Chlordane 2.5
Comments:
BQL =Below Quantitation Limit
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
FORM TCLP-8080 Rev. 082790
TCLP HERBICIDES
METHOD 8150
lEA Sample Number: 916-062-1
Sample Identification: SAl-1753
TCLP Extraction Date: 11/01/90
Date Extracted: 11/07/90
Date Analyzed: 11/15/90
By: Travis
Number
1
2
Compound
2,4-D
2,4,5-TP
Quantitation
Limit
(mg/L)
0.010
0.0020
Results
Concentration
(mg/L)
SQL
BQL
Comments:
BQL = Below Quantitation Limit
FORM TCLP-HERB Rev. 100290
TCLP HERBICIDES
METHOD 8150
lEA Sample Number: 916-062-2
Sample Identification: SA2-1754
TCLP Extraction Date: 11/01/90
Date Extracted: 11/07/90
Date Analyzed: 11/15/90
By: Travis
Number
1
2
Compound
2,4-D
2,4,5-TP
Quantitation
Limit
(mg/L)
0.010
0.0020
Results
Concentration
(mg/L)
BQL
BQL
Comments:
BQL « Below Quantitation Limit
FORM TCLP-HERB Rev. 100290
TCLP HERBICIDES
METHOD 8150
lEA Sample Number: 916-062-3
Sample Identification: STB-1756
TCLP Extraction Date; 11/01/90
Date Extracted:
Date Analyzed:
By: Travis
11/07/90
11/15/90
Number
1
2
Compound
2,4-D
2,4,5-TP
Quant itat ion
Limit
(mg/L)
0.010
0.0020
Results
Concentration
(mg/L)
BQL
SQL
Comments:
BQL - Below Quantitation Limit
FORM TCLP-HERB Rev. 100290
REACTIVITY
XEA Sample Number: 916-062-1
Sample Identification: SAl-1753
Date Analyzed; 11/06/90 By: Campbell
Niimber Compound
1 pH
2
3
4
Su
Results
5.1
lfide Reactivity <25 mg/kg
Cyanide Reactivity <0.50 mg/kg
Overall Reactivity N/R
Comments:
N/R = Not Reactive
FORM REAC Rev. 111390
REACTIVITY
lEA Sample Number: 916-062-2
Sample Identification: SA2-1754
Date Analyzed: 11/06/90 By: Campbell
Results
Nijmber Compound
1 pH 5.2
2 Sulfide Reactivity <25 rag/kg
3 Cyanide Reactivity <0.50 mg/kg
4 Overall Reactivity N/R
Comments:
N/R « Not Reactive
FORM REAC Rev. 111390
REACTIVITY
lEA Sample Number; 916-062-3
Sample Identification: STB-1755
Date Analyzed; 11/06/90 By: Campbell
Results
Number Compound
1 pH 5,1
2 Sulfide Reactivity <25 mg/kg
3 Cyanide Reactivity <0,50 mg/kg
4 Overall Reactivity N/R
Comments:
N/R = Not Reactive
FORM REAC Rev. 111390
Report To;
GeoChem. incorporated
E nvlronmenial Laboratories
2500 Gate Way Centre Blvd., Suite 300
Morrisville, NO 27560
Chain of Custody Record
BITo:
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DATE ■RMER0^(ARKS
RECEIVED BY:
RECEIVED BY:
DATE
DATE
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RELINQUISHED BY:
RELINQUISHED BY:
DATE
DATE
TIME
TIME
RELINQUISHED^:, .
RECEIVED BY:
ElVED BY:}//')./
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RELINQUISHED BY:
REUNQUISHED BY:
DATE
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This Chain of Custody is oonsiderod a written contract to perform the servicos requested in the ariatyses section of this document.
APPENDIX B
Groundwater Sample Laboratory Reports
NUV~lii"yU nUN u:il lituuntri ino. rnn nu. oio'tuuuiuf r. ui
GeoChem, Incorporated
Environmental Laboratories
November 12, 1990
Mr. Joe Mattheis
Applied Environmental Services
1805 Running Oak Drive
Reference; Murphy
A10037a
GCl# 9011-0X8
Dear Mr. Joe Mattheis:
This is the analytical report for the above referenced
project. On November 6, 1990 we received one water sample for
analysis.
The analytical and quality control results are presented in
separate tables for your convenience. Brief summaries of analytical
methods employed are as follows.
EPA 8240
Method 8240 can be used to quantify most volatile organic
compounds that have boiling points below 200 C. The volatile
compounds are introduced into the gas chromatograph by the purge-
and-trap method or by direct injection (in limited applications).
The components are separated via the gas chromatograph and detected
using a mass spectrometer, which Is used to provide both■qualitative and quantitative information.
If there are any technical questions please feel free to call
me at 919-460-3093. Thank you for allowing GeoChbm to serve your
analytical needs.
Sincerely,
Dean Gokel^<_
President
2500 Gate Way Centre Blvd., Suite 300 • Morrisville, NC 27560
T -1 r\*r\ t c^r\ ortftO . CAV.
NOV-12-90 HON 17:11 UhUUHhn ifiu.TMA IHU. yia^OUUlD r. Udi
GeoChem, Incorporated
Environmental Laboratories
Geochem
Project#90Xl-018
Site Name Murphy
Number A100372
LAB ID.
DATE SAMPLED
FIELD ID.
1847
U/6/90
MWl
MXT»00
ANALYTE ua/1
8240
Dichlorodifluoromethane BOL
Chiotfomethane BDL
Vinyl Chloride BDL
Brcmomethane BDL
Chloroethane BDL
Trichlorof luorcrnethane 420
Acroiein ~
1,l-Dichloroethene
lodoraethane
Acetone
Carbon Didulfide
Ethanol
Methvlene Chloride
trans-1,20icnioroethene BDL
Acrylonitrile BDL
1.1-Dichloroethane BDL
Vinyl Acetate BDL
2-Butanone BDL
Chloroform BDL
1.1.1-Trichloroethane BDL
Carbon Tetrachloride BDL
Benzene
1.2-Dicnioroethane 5DL
Trichloroethene SDL
1,2-Oichloropropane BDL
Dibromotnethane BDL
Bromodichloromethane BDL
2ChloroethylvinyL Ether BDL
tran8l,3Dichloropropene BDL
2-H©xanone bdl
Toluene SDL
cis-l,3-Dichloropropene BDL
1.1.2-Trichloroethane BDL
Tetrachloroethane BDL
Ethyl Methacrylate BDL
Chlorodibromomethane BDL
4--Methyl-'2-Pentanone BDL
Chlorobensene BDL
2500 Gate Way Cenire Blvd.. Suite 300 • Morrisville. NC 27560
KUv-l^-yU nUN ll'Vd Iituontn rriA i'i>ji oionuuuiui
GeoChem, incorporated
Environmental Laboratories
Geochem
Project#90ll'018
site Name Murphy
Number A100372
LAB ID.
DATE SAMPLED
FIELD ID,
1847
11/6/90
MWl
MEtaOO
ANALYTE
8240 (Continued)
uq/I
90
160
35-
Ethvlbenzene
in,p-Xylene
Q-Xvlene
Styrene BDL
Bromoform BDL
i,2,3-Trichloropropane BDL
1,1,2,2TetrachloroethaneBDL
1,4-Dichloro-2-Butene BDL
.£01
5.0
5.0
5.0
5.0
5,0
5.0
5.0
100
Z'\
HoO
soil water
parts per million ® mg/kg mg/1
parts per billion = ug/^g ^9/1
pql a practia&l quantitation limit due to matrr;: effects
2500 Gate Way Centre Blvd., Suite 300 • Morrisvllie, NC 27560
Q'iQ..<iAn.»ng!^ • PAX: 919-460-0167
NUV-iii-yu nUN a'id Iituunnn ino.rnA tiu. oioHuuuiui r, U4
GeoChem, incorporated
Environmental Laboratories
QUALITY CONTROL RESULTS
METHOD RECOVERY METHOD
DETECTION LIMIT
8240
1,1-Dichloroethene 106 %5.0 ppb
Benzene 104 %
Trichloroethene 95 %
Toluene 94 %
chlorobenzene 97 %
REVIEWED BY
2500 Gate Way Centre Blvd.. Suite 300 • Morrisviile. NO 27560
rt^n. y4cn_QnQO • CAV' Ql A7
GeoChem, incorporated
Environmental Laboratories
QUALITY CONTROL RESULTS
METHOD RECOVERY METHOD
DETECTION LIMIT
8240
1,1-Dichloroethene 106 %5.0 ppb
Benzene 104 %
Trichloroethene 95 %
Toluene 94 %
Chlorobenzene 97 %
2500 Gate Way Centre Blvd., Suite 300 • MorrlsvHIe, NO 27560
Telephone: [phone] • FAX: 919-460U167
t/L^' U ou >J1 I 1 1 1'
GeoChem, Incorporated
Environmental Laboratories
December 9, 1990
Mr. Scott Driscoll
Applied Environmental Services
1805 Running Oak Drive
Raleigh, NC 27612
Reference: Hurphy
A100372
GCI# 9011-050
Dear Mr. Scott Driscoll:
This is the analytical report for the above referenced
project. On November 16, 1990 we received three water samples for
analysis.
The analytical and quality control results are presented in
separate tables for your convenience. Brief summaries of analytical
methods employed are as follows.
Furgeables EPA 8240
This method can be used to quantify most volatile organic
compounds that have boiling points below 200 C. The volatile
compounds are introduced into the gas chromatograph by purge-and-
trap methodology. The components are separated via gas
chromatograph and detected using a mass spectrometer, which is used
to provide both qualitative and quantitative information.
If there are any technical questions please feel free to call
me at 919-460-8093. Thank you for allowing GeoChem to serve your
analytical needs.
Dean Gokel
President
2500 Gate Way Centre ? vd., • Morrisvllle, NC 27560
Telenhone" 919-460-0167
l/uv \J <y"y' k.!! 1 1 1 I n s/'w'
GeoChem, Incorporated
Environmental Laboratories
Geochem
Project#9011-050
LAB ID, •
DATE SAMPLED
FIELD ID.
1963
11/16/90
MWl
Site Name Murphy
Number A100372
1964
11/16/90
MW2
1965
11/16/90
KW3
METHOD
ANALYTE DCl ua/1 ©al uo/1 DCTl
8240
Dichlorodifluoromethane BDL 10 BDL 10 SDL 10
Chloromethane BDL 10 BDL 10 BDL 10
Vinyl Chloride BDL 10 BDL 10 BDL - 10
Brcmomethane BDL 10 BDL 10 BDL 10
Chloroethane BDL 10 BDL 10 BDL 10
Trichlorofluoromethane BDL 10 BDL 10 — lil
Acrolein BDL 10 BDL 10 BDL ,. 10 • '
1,1-Dichloroethene BDL 5.0 BDL 5.0 BDL 5.0
lodomethane BDL 10 BDL 10 01 w 10
Acetone BDL 100 BDL 100 DDL 100
Carbon Disulfide BDL 5,0 BDL 5.0 BDL s.o
Sthanol BDL 10 BDL 10 BDL 10
Methyiene Chloride BDL 5.0 BDL 5.0 8.3 5.0
trans-l,2Dichloroethene BDL 5.0 BDL 5.0 BDL 5.0
Acrylonitrile BDL 100 BDL 100 BDL 100
1,1-Dichloroethane BDL 5.0 BDL 5.0 BDL 5.0
Vinyl Acetate BDL 10 BDL 10 BDL 10
2-Butanone BDL 100 BDL 100 BDL 100
Chloroform 13 5.0 16 5.0 BDL S.O
1,1,1-Trichloroethane BDL 5.0 BDL 3.0 BDL 5.0
Carbon Tetrachloride BDL 5.0 75 Tw ^5.0 BDL 5.0
Benzene BDL 5.0 BDL 5.0 100 5.0.
1,2-'Dichloroethane BDL 5.0 BDL 5.0 BDL 5.0
Trichloroethene BDL 5.0 BDL 5.0 BOL 5.0
1,2~Dichloropropane BDL 5.0 BDL 5.0 BDL 5.0
Dibromomethane BDL 5.0 BDL 5.0 5.0
Brombdichloromethane BDL 5.0 BDL 5.0 BDL 5.0
2Chloroethylvinyl Ether BDL 5.0 BDL 5.0 BDL 5.0
trarial, 3Dichloropropene BDL 5.0 BDL 5.0 BDL 5.0
2-Hexanone BDL 50 BDL 50 BDL 50
Toluene BDL 5.0 BDL 5.0 BDL 5.0
cis-1,3-Dichloropropene BDL 5.0 BDL 5.0 BDL 5.0
2500 O -.te W
Tele;
'trr-, Suite 300
•aou'' - •
rrisvllle, '";C 27560
M60-C- •
uco- o~au oni u•ooucuk^ncii inv.rnA nu. oio4uuuiur. uoGeoChem, IncorporatedEnvironmental LaboratoriesGeochemProject#9011'-050LAB ID.DATE SAMPLEDFIELD ID.196311/16/90«W1Site Name MurphyNumber A100372196411/16/90MW2196511/16/90MW3soil waterparts per million = mg/kg mgpparts per billion « ug/kg ug_pgl = practical quantitation due to matrix effects.MSTHQOANALYTEua/1Dalua/1Dalua/1Dal8240 (continued)1,1,2-TrichloroethaneBDL5.0BDLs.oBDL5.0Tetrachloroethar.eBDL5.0BDL5.0BDL5.0Ethyl MethacrylateBDL5.0BDL5.0BDL5.0 •ChlorodibromomethaneBDL5.0BDL5.0BDL5.04-Methyl-2-Pentan<?neBDL50BDL50BDL50ChlorobenzeneBDL5,0BDL5.0BDL5.0SthylbenzeneBDL5.0BDL5.05.0 .m,p~XyleneBDL5,0BDL5.0^120 -5.0o-XylensBDL5,0BDL5.0i.OStyreneBDL5.0BDL5.0BDL5.0Brorfioformi>DL5.0BDL5.0BDL5.01,2,3-TrichloropropaneBDL5.0BDL5.0BDL5.01,1,2,2TetrachloroetbaneBDLB.OBDL5.0BDL5,01,4-Dichloro-2-ButeneBDL100BDL100BDL1002500 Gate Way Centre Blvd., Suite 300 • NC 27560Telaohop®" -^093 • FAX: 9»9-l60-0l67
o~ou oni ij'ji unji^ncii lu'-'.rnn iiu. oioiuuuiui r. U4
GeoChem, Incorporated
Environmental La bo rat cries
QUALITY CONTROL RESULTS
METHOD
8240
1,1-Dichloroethene
Benzene
Trichloroethene
Toluene
Chlorobenzene
RECOVERY
101 %
99 %
96 %
103 %
97 %
METHOD
DETECTION LIMIT
5 4 0 ppb
REVIEWED BY
2500 Gate Way Centre Blvd., Suite 300 ' Morrisvilid, NO 27560
TAtnnhnnA- Oin.-■"y.flnoq « . aAQ-lfiAJllfiT
GeoChem, Incorporated
Environmental Laboratories
G O ?
November 12, 1990
Mr. Joe Mattheis
Applied Environmental Services f
1805 Running Oak Drive i y
Reference: Murphy
A100372
GCI# 9011-018
Dear Mr. Joe Mattheis:
This is the analytical report for the above referenced
project. On November 6, 1990 we received one water sample for
analysis.
The analytical and quality control results are presented in
separate tables for your convenience. Brief summaries of analytical
methods employed are as follows.
EPA 8240
Method 8240 can be used to quantify most volatile organic
compounds that- have boiling points below 200 C. The volatile
compounds are introduced into the gas chromatograph by the purge
and-trap method or by direct injection (in limited applications).
The components are separated via the gas chromatograph and^ detected
using a mass spectrometer, which is used to provide both
qualitative and quantitative information.
If there are any technical questions please feel free to call
me at 919-460-8093. Thank you for allowing GkoChsm to serve your
analytical needs.
Sincerely,
0
Dean Gokel^^^
President
2500 Gate Way Centre Blvd., Suite 300 • Morrlsville, NO 27560
Telephone: [phone] • FAX: [phone]
GeoChem, Incorporated
Environmental Laboratories
Geochem
Project#9011-018
LAB ID.
DATE SAMPLED
FIELD ID.
1847
11/6/90
MWl
Site Name Murphy
Number A100372
KETHOO
ANALYTE
8240
ua/1 pqi
Dichlorodifluoromethane HDL 10
Chloromethane BDL 10
Vinyl Chloride BDL 10
Bromomethane BDL 10
Chloroethane BDL 10
Trichlorofluoromethane 420 10
Acrolein BDL 10
1,1-Dichloroethene BDL 5.0
lodomethane BDL 10
Acetone BDL 100
Carbon Disulfide BDL 5.0
Ethanol BDL 10
Methylene Chloride 7.2 5.0
trans-1,2Dichloroethene BDL 5.0
Acrylonitrile BDL 100
1,1-Dichloroethane BDL 5.0
Vinyl Acetate BDL 10
2-Butanone BDL 100
Chloroform BDL 5.0
1,1,l~Trichloroethane BDL 5.0
Carbon Tetrachloride BDL 5.0
Benzene 120 5.0
1,2-Dichloroethane BDL 5.0
Trichloroethene BDL 5.0
1,2-D ichloropropane BDL 5.0
D ibromomethane BDL 5.0
Bromodichloromethane BDL 5.0
2Chloroethylvinyl Ether BDL 5.0
transl,3Dichloropropene BDL 5.0
2-Hexanone BDL 50
Toluene BDL 5.0
cis-1,3-Dichloropropene BDL 5.0
1,1,2-Trichloroethane BDL 5.0
Tetrachloroethane BDL 5.0
Ethyl Methacrylate BDL 5.0
Chlorodibromomethane BDL 5.0
4-Methyl-2-Pentanone BDL 50
Chlorobenzene BDL 5.0
2500 Gate Way Centre Blvd., Suite 300 • Morrisville, NC 27560
Telephone: [phone] • FAX: [phone]
GeoChem, incorporated
Environmental Labora t o r 1 e s
Geochem Site Name Murphy
Project#9011-018 2 Number A100372
LAB ID. 1847
DATE SAMPLED 11/6/90
FIELD ID. MWl
KETHOD
ANALYTE uq/I PctI
8240 (Continued)
Ethylbenzene 90 5.0
m,p-Xylene 160 B.O
o-Xylene 35 5.0
Styrene BDL 5.0
Bromoform BDL 5.0
1,2,3-Trichloropropane BDL 5.0
l,l,2,2TetrachloroethaneBDL 5.0
1,4--Dichloro-2-Butene BDL 100
soil water
parts per million = mg/kg tag/l
parts per billion ~ ug/kg ^9/1
pql = practical qxiantltatlon limit due to matrix effects
2500 Gate Way Centre Blvd., Suite 300 • Morrisville, NO 27560
Telephone: [phone] • FAX: [phone]
GeoChem, Incorporated
Environmental Laboratories
April 16, 1991
Mr. Joe Matthies
Applied Environmental Services
1805 Running Oak Drive | ^
Raleigh, NC 27612 \
Reference: Kurphy
A100372
GCI# 9104-020
Dear Mr. Joe Matthies:
This is the analytical report for the above referenced
oroiect On April 9, 1991 we received five water samples for
analysis. The analytical and quality control results
in separate tables for your convenience. Brief summariesanalytical methods employed are as follows.
Purgeables EPA 8240
This method can be used to quantify most volatile organiccompounds that have boiling points below 200 C. The volat^lcompounds are introduced into the gas chromatograph by purge and
t>-aD methodology. The components are separated^ via gaschromatograph and detected using a mass spectrometer, "hi^ i® used
to provide both qualitative and quantitative inj.ormatj.on.
If there are any technical questions please feel free to call
me at 919-460-8093. Thank you for allowing GboChkm to serve your
analytical needs.
Sincerely, ^
Dean Gokel
President
2500 Gate Way Centre Blvd., Suite 300 • Morrisviiie, NC 27560
Telephone; 919-460-8093 • FAX: [phone]
GeoChem, incorporated
Environmental Laboratories
Geochem
Project#9104-020 Site Name Murphy
LAB ID.
DATE SAMPLED
FIELD ID.
1023
4/3/91
MW2
1024
4/8/91
MW3
1025
4/8/91
MW4
uq/1ANALYTE
8240
Dichlorodifluoromethane BDL
Chioromethane SOL
Vinyl Chloride BDL
Bromomethane BOL
Chloroethane BDL
Trichlorof luoromethane BDL
Acrolein BDL
1,l-Dlchloroethene BDL
lodomethane BDL
Acetone BDL
Carbon Disulfide BDL
Ethanol BDL
Methylene Chloride BDL
trans-1,2Dichloroethene BDL
Aerylonitrile
1.1-Dichloroethane
Vinyl Acetate
2-Butanone
Chlorofonn
1.1.1-Trichloroethane
Carbon Tetrachloride
Benzene
1.2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Dibromomethane
Bromcdichloromethane
2Chloroethylvinyl Ether BDL
transli,3Dichloropropene BDL
2-Hexanone BDL
Toluene BDL
cis-l,3-Dichloropropene BDL
1.1.2-Trichloroethane BDL
Tetrachloroethene
Ethyl Methacrylate
Chlorodibromomethane
4-Methyi-2-Pentanone
Chlorobenzene
Ethylbenzene
m,p-Xylene
o-Xylene
Styrene
Bromoform
1.2.3-Trichloropropane
1,1,2,2TetrachloroethaneBDL
1,4-Dichloro-2-Butene BDL
BDL
BDL
BDL
BDL
8.2
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
pqi
10
10
10
10
10
10
10
5.0
10
50
5.0
10
5.0
5.0
100
5.0
10
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
ua/1 oal ua/1 aal
BDL 10 BDL 10
BDL 10 BDL 10
BDL 10 BDL 10
BDL 10 BDL 10
BDL 10 BDL 10
50 10 190 10
BDL 10 BDL 10
BDL 5.0 BDL 5.0
BDL 10 BDL 10
BDL 50 BDL 50
BDL 5.0 BDL 5.0
BDL 10 BDL 10
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 100 BDL 100
BDL 5.0 BDL 5.0
BDL 10 BDL 10
BDL ICO BDL 100
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 50 BDL 50
25 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 50 BDL 50
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
54 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 5.0 BDL 5.0
BDL 100 BDL 100
pql = praczical quantitatlon limit due to matrix effects,
bdl = below method detection limit,
bql = below quantization limit.
2500 Gate Way Centre Blvd., Suite 300 • Morrisville. HC 27560
Telephone: [phone] • FAX: [phone]
GeoChem, incorporated
Environmental Labora t ories
Geochem
Project#9104-020 Site Name Murphy
LAB ID.
DATE SAMPLED
FIELD ID.
1026
4/8/91
MW5
uq/1ANALYTE
8240Dichlorodifluoromethane BDL
Chloromethane BDL
Vinyl Chloride BDL
Bromomethane BDL
Chloroethane BDL
Trichlorofluoromethane BDL
Acrolein BDL
1,i-Dichloroethene BDL
lodomethane BDL
Acetone
Carbon Disulfide BDL
Ethanol BDL
Methylene Chloride BDL
trans-l,2Dichloroethene BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Acrylonitrile
1.1-Dichloroethane
Vinyl Acetate
2-Butanone
Chloroform
1.1.1-Tr ichloroethane
Carbon Tetrachloride
Benzene
1.2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Dibromomethane
Bromodichloromethane
2Chloroethylvinyl Ether BDL
transl,3Dichloropropene BDL
2-Hexanone BDL
Toluene BDL
cis-l,3-Dichloropropene BDL
1.1.2-Trichloroethane BDL
Tetrachloroethene
Ethyl Methacrylate
Chlorodibromomethane
4-Methy1-2-Pent anone
Chlorobenzene
Ethylbenzene
m,p-Xylene
o-Xylene
Styrene
Bromoform
1.2.3-Trichloropropane
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1,1,2,2TetrachloroethaneBDL
l,4-Dichloro-2-Butene BDL
JB3X
10
10
10
10
10
10
10
5.0
10
50
5.0
10
5.0
5.0
100
5.0
10
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
1027
4/8/91
MW6
ua/1 Dal
BDL 10
BDL 10
BDL 10
BDL 10
BDL 10
BDL 10
BDL 10
BDL 5.0
BDL 10
BDL 50
BDL 5.0
BDL 10
BDL 5.0
BDL 5.0
BDL 100
BDL 5.0
BDL 10
BDL 100
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 50
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 50
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 5.0
BDL 100
pql = practical quantitation limrt due
bdl - belov method detection limit,
bql = below quantitation limit.
to matrix effects
2500 Gate Way Centre Blvd., Suite 300 • Morrisviile, NO 27560
Telephone: 919-460^093 • FAX: [phone]
GeoChem, Incorporated
E n V i r o n nn e n t a 1 Laboratories
QUALITY CONTROL RESULTS
METHOD RECOVERY METHOD
DETECTION LIMIT
8240
1,i-Dichloroethene
Benzene
Trichloroethene
Toluene
112 %
100 %
103 %
113 %,
5.0 ppb
Chlorobenzene 101 %
—
REVIEWED BY
/K
2500 Gate Way Centre Blvd., Suite 300 • Morrisvilte, NO 27560
Telephone: 91^460-8093 • FAX: [phone]
Geocnem. incorporatea
Report To £ n V I r onmenial Laboratories
2500 Gato Way Centre Blvd., Suite 300
Morrisville, NO 27560
BITo r(L/.
Pa9e_Ld__^
PROJECT STTE PC#
ON. FO SRENIATNOC; REPNOITACOL
ANALYSES /j y't3»<)ChBmPRCYlECT#^.^'^^
STTENAME .
!
j j DATE REPORT DUE f/
COUJECTED BY fSi&n^J j VERBAL/FAXWAROCOPY
RELD
SAMPLE ID
TURNAROUNC
WDAYS
SAMPLE
MATRIX
DATE
coaecTED r
/
i RRutARKS
LAB ID NO.
ffor\abuseor)iv)
ir lU.o Hld^hi 5 1
rv\wi 3 lifcSiSiii-'.
3
3 Y
3 \liBiiisiips
J
n
L_..^
RKEIVED BY:
W,
RECE]vk)BY?
DATE
m;
DATE
TffvIE
/aioSAt
TIME
RELINQUISHED BY:R^INOUia
RaiNOUlSHED'-DATE
™e
TIME
RECEIVED BY:
RECEIVED
t).
)ATE TIME
REUNOUISHED BY: DATE TIME
This Chain o« Custody is consWorwl a wrttten cjonlrad io pertorm the seivicos requested In the analyses section o( this ctocument.
APPENDIX C
Well Construction Records
NORTH CAROLINA OEPARTMENT OF ENVIRONMENT, HEALTH ANO NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT n GROUNOWATER SECTION
P.O. BOX 27687 - RALEIGH. NC 27611-7687
PHONE [phone]
WELL CONSTRUCTION RECORD MW-1
FOR OFFICE USE ONLY
Ouad. Nn. _Serial No.
1 .-It
OW-1 Fnt
n... 6rrno Aoolied Enviroiunencal Services, Inc.RILLING CON FHAC \ UH STATE WELL CONSTRUCTION
XER REGISTRATION NUMBER PERMIT NUMBER:Q7-07.ni -WM-nn6-^
■■■"LL LOCATION; CShow sketcfi of the location below)
Wilsonlarest Town:County:Wilson
Murphy Manufacturing Co.. 2000 Airport Drive
'"'oad. Community, or Subdivision and Lot No.)C.W. LaymanWNER
From To
DRILLING LOG
Formation Deschotion
ADDRESS P.O. Box 2009
CStreet or Route No.)NC
0
Wilson 27894
City or Town
11/6/90
state
USE OF WELL
17.5' CUTTINGS COLLECTED Sves □ No
FT. □ above TOP OF CASING.XS belowFT. ABOVE LAND SURFACE.
DATE DRILLED
DTAL DEPTH.
wOES WELL REPLACE EXISTING WELL? □ Yes Q No
^TATIC WATER i PVFl ■ 3.31
TOP OF CASING IS Q
YIELD Cgpm): METHOD OF TEST
ATER ZONES Cdeotti):
, CHLORINATION: Type
BASING;
Amount
Zio Code
Monitor
8.5 14.5
14.5 17.5
8.5 Orange-gray silty CLAY
Tan-gray fine sandy silty CLAY
Tan-gray fine sandy SILT
If addttionai soace is needed use back of form.
Deotti Diameter or Weignt/Ft. Material
0 To 7.5 Ft 7." SCKin PVC *
Ft -
—Ft -
3R0UT;
Deoth Material Method
3.5 To b.5 Ft.Bentonite
0 To Ft Neat Cement
SCREEN:
Deoth Diameter Slot Size Material
7.5 To 17.5Ft 2 in. 0.01 in PVC 7
To Ft in in.
From_To_Ft In in.
LOCATION SKETCH
GRAVEL PACK;
Size Material
Torpedo Sand
Deotn
From
From
REMARKS
-J^XIfS6
St MatUww .
I DO HERESY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 20. WELL CONSTRUCTIONSTANDARDS. ANO THAT A COPY OF THIS RECCRO HAS^NPRWpE^^jyE^^-^^
iV-1 REVISED 2/90
Sie^lATURE CONTRACTOR OR AGENT OATc
Submit original to Division of Environmental Management ana coby to well owner.
NORTH CAROLINA DEPABTMeNT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
OiVISION OF ENVIRONMENTAL MANAGEMENT • GBOUNOWATER SECTION
P.O. aOX27M7. RALEIGH, NC 27611-7M7 Quad. No.
FOR OFFICE USE ONLY
Serial No.
PHONE [phone] nl
WELL CONSTRUCTION RECORD MW-2 C3W-1 Pnr
XING CONTRACTOR
Fishburne Drilling, Iiic.
XER REGISTRATION NUMBER
oTATE WELL CONSTRUCnON
PERMIT NUMBER: Q7~0201 -T-TM-DDA?
ELL LOCATION: (Show sketch of the location Qelow]
i-.earest Town:
^^llrphy Manufacturing Co., 2000 Aimort Drive
oad. Community, or Subdivision and Lot No.]
C.W. Layman
County;Wilson
From
Deot^(ft.)
To
DRILLING LOG
Formation Descnotion
,wNeR
•OGRESS P.O. Box 2009
7,5 Orange-gray silty CLAY
Wilson
(Street or Route No.J
NC 27894
7.5 13.5 Tan-gray fine sandy silty CLAY
City or Town
-ATE DRILLED
State
USE OF WELL
Zip Code
Monitor
13.5 25 Tan-gray fine sandy SILT
Gray CLAY
FT. Q above TOP OF CASING.
^ below
FT. ABOVE LAND SURFACE.
-iTAi ncoTM 36.5 CUTTINGS COLLECTED Sves □ No
DOES WELL REPLACE EXISTING WELL? □ Yes CX No
3 Q7TATIC WATER LEVEL _XLLX
TOP OF CASING IS Q
. YIELD Cgpm]: METHOD OF TEST
?ATER ZONES Cdeotnl:
Tyoe-HLORINATION:Amount
25 28.5 Gray CLAY
28.5 36.5 Gray medium to coarse grain SANI
:aSING:
Death
Wall ThicknessDiameter or Weignt/Ft. Material
If additional soace is needed use back of form.
From
From
From
GROUT:
From
From
iz. SCREEN:
u
0
To _
31.5
Ft,
2" SCH40 PVC
Death Material Method
0 To 29.5 Ft Neat Cement Iniection
To.,Ft.
LOCATION SKETCH
Deoth
31.5 TO 36.5 Ft
Diameter
2
Slot Size
in 0.01 in.
Material
PVC T
Tn Ft in in.--
From_Tn Ft in in.
GRAVEL PACK:
□eotn Size
30.5 To 36.5 PL Coarse
30.5 29.5 pt Bentonite Pellets
REMARKS
Material
Toroedo Sand
St
. %
1 00 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WEuL CCNSTHUCilONSTANDARDS. AND THAT A COPY OF THIS RECORD HAS
SIGJlAlilRE 6f CONTRACTOR OR AGENT OATE-V-l REVISED 2'QO Suomit original to Division of Environmental Management and cooy to well owner.
NOnTM CAROLINA OSPARTMENT OP ENVlRONMeNT. HEALTH ANO NATURAL RESOURCES
OIVISION OF ENVIRONMENTAL MANAGEMENT • GROUNOWATER SECTION
P.O. BOX 27687 • RALEIGH. NC 27811-7687
PHONE [phone]
WELL CONSTRUCTION RECORD MW-3
FOR OFFICE USE ONLY
Quad. Nn.Serial No.
1 at Long Br
ow-1 Fnt
. ...1^/-r^MTOArrno Aoolied Environmental Services, Inc.RILLING GUN I MAG IUM STATE WELL CONSTRUCTION
1163 PERMIT NUMBER: 97-0201 -1^-0063.LER REGISTRATION NUMBER
■■■"LL LOCATION: (Show sketch of the location below)
:ares. Town:County;Wilson
Murphy Manufacturing Co.. 2000 Airport Drive
'"aad. Community, or Subdivision and Lot No.)
C,W. La3nnanWNER
Daoth(ft. )
ADDRESS P.O. Box 2009
CStreet or Route No.)NCWilson 27894
City or Town
4/5/91
state
USE OF WELL
16 CUTTINGS COLLECTED S Yes □ No
DATE DRILLED
JTAL DEPTH .
wOES WELL REPLACE EXISPNG WELL? □ Yes Q No
"ATIC WATER I FVP! • 3.33
TOP OF CASING 'g Q
YIELD Cspm): METHOD OF TEST
FT. O above TOP
Zip Code
Monitor
From To
0 5
5 12
12 16
DRILLING LOG
Formation Description
OF CASING.3CS belowFT. ABOVE LAND SURFACE.
ATEH ZONES (depth):
CHL0RINATI0r4:
JASING;
Type Amount
Oran^e-grFiv silfv CLAY
Tan-^ray fine sandy silty CLAY
Tan-gray fine sandy SILT
if additional space is needed use back of form.
0
Death
To 6
Diameter or Weigtit/Ft. Material
Ft 2" SCF40 PVC
To Ft..
SHOUT:
3
Depth
To 5 Ft
Material Method
Bentonite
0 To 3 Ft Neat Cement
SCREEN:
6
Depth
To 16 Ft
Diameter Slot Size Material
2 in 0.01 in. PVC
In Ft in in.
Tn Ft in in.
3RAVEL PACK;
From _5
Depth
To 16 Ft.
Size Material
Torpedo Sand
LOCATION SKETCH
From
4. REMARKS:
St Msnhcw
nN. !§\
I 00 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTIONSTANDARDS. AND THAT A COPY OF THIS RECORD HA^^EEN ^ ff j/"HA^EEN PR^Ii
^-1 REVISED 2/90
SKSJ^ATURE 6f CONTRACTOR OR AGENT DATE
Submit original to Division of Environmental Management ana cooy to well owner.
north CAROUNA OEPARTMeNT OF ENVIBONMENT, HEALTH AND NAnjHAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNOWATER SECTION
P.O. BOX 27M7-RALEIGH. NO 27611-7687
PHONE [phone]
WELL CONSTRUCTION RECORD
MW-4
FOR OFFICE USE ONLY
Serial No.
1 nnn Pc
GW-1 Pnf
RILUNG CONTRACTOR Applied Environmental Services, CONSTRUCTION
.LER REGISTRATION NUMBER li63_ PERMIT NUMBER: Q7-0201 WM
WELL LOCATION: (Show sketch of the location below)
,arest Town:
..jrphy Manufacturing Co.. 2000 Alxroort Drive
CHoad. Community, or Subdivision and Lot No.)
C.W. Layman
WNER
County:Wilson
Deoth
From To
DRILLING LOG
Formation Descriotion
ADDRESS P.O. Box 2009 7.3 Orange-gray siltv CLAY
Wilson
(Street or Route No.)
NC 27894
7.5 14
City or Town State _Zio Code
DATE DRILLED ^/5/91 USE OF WELL Monitor
->TAi ncpTu 18.3 CUTTINGS COLLECTED Sves □ No
OES WELL REPLACE EXISTING WELL? □ Yes Q No
STATIC WATER LEVEL:
TOP OF CASING IS Q
rlELD Cgpm): METHOD OF TEST
'VATHR ZONES (deoth);
FT □ above TOP OF CASING.XS- belowFT. ABOVE LAND SURFACE.
14 18.3
. CHLORINATICN:
CASING:
Tvne
Deoth
Amount ■
Wall ThicknessDiameter or Weight/Ft. Material
0 T. 8.5 Ft 7" RCTTAO PVr
Ft
' GROUT:
Deoth Material Method
-^.3 Th 6 Ft Benconite
0 T. 3.5 Ft Neat Cement
SCREEN:
Deoth Diameter Slot Size Material
8.3 18.5 Ft 2 in 0.01 in PVC
Tn Ft in in.
Tn Ft in in.
GRAVEL PACK:
A
Deoth
TnlR.3 Ft
Size Material
Torpedo Sand
Tn Ft
BBMAPlfQ-
Tan-grav fine snadv siltv CLAY
Tan-grav finp sanHv .STT.T
if additional soace is needed use back of form.
LOCATION SKETCH
xffSS
St ^lAOhcw
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANIZE WITH 15 NCA 2C. WELL CONSTRUCTIONSTANDARDS. AND THAT A COPY OF THIS RECORD ^
SiGfiATClRE dF CONTRACTOR OR AGENT DATESubmit original to Division of Environmental Management and copy to well owner.iW-1 REVISED 2/'90
40RTM CAROLINA OEPARTMeNT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNOWATER SECTION
P.O. BOX 2768T • RALEIGH. NC 27an'768T
PHONE [phone]
WELL CONSTRUCTION RECORD MW-5
FOR OFFICE USE ONLY
Serial No.
1 at Long Pr
rtW-l Pnt
billing CONTHACTOR Applied Environmental Services, Inc^^ CONSTRUC710N
J.ER REGISTRATION NUMBER PERMIT NUMBER: ^7-0701 -^^-0061.
WELL LOCATION: CShow sketch of the location below]Il.res. Town:
uurphy Manufacturing Co.. 2000 Airpor
County:Wilson
t Drive
^oad. Community, or Subdivision and Lot No.)
C.W. Layman
VNEB
From
Deoth (ft. )
To
DRILLING LOG
Formation Qeschoiion
address P.O. Box 2009
CSlreet or Route No.i
NC
0
Wilson 27894 14.5
State
USE OF WELL
Zip Code
Monitor
14.5 18.5
City or Town
□ATE DRILLED 4/5/91.
1TAI npoTLi 18.5 CUTTINGS COLLECTED Sves □ No
_ 3ES WELL REPLACE EXISTING WELL? □ Yes Q No
STATIC WATER LEVEL: 3.36
TOP OF CASING IS _Q
YIELD Cgpm]: METHOD OF TEST
'ATER ZONES (depth):
CHLORINATION: Type
:asing;
FT □ above TOP OF CASING,XZi belowFT. ABOVE LAND SURFACE.
Amount
Wall Thickness
Orange-gray silty CLAY
Tan-grav finp .ganrly .gilfy TT.Ay
Tan-gray fine sandy SILT
Deoth c
0 To 8.5 Ft
To Ft
To Ft
GROUT;
3.5
Deoth
To 6 Ft.
0 To 3.5 Ft
SCREEN:
8.5
Depth
To 18.5 Ft.
To Ft.
Tn Ft
GRAVEL PACK:
From_6
Depth
To 18.5 Ft.
2".
or Weight/Ft.
_ 8CK40
If additional space is neeoed use back of form.
pvr
LOCATION SKETCH
Material Method
Diameter
2
Slot Size Material
in. 0.01 in. PVC
in,
, in
in.
. in.
Size Material
TorDedo Sand
<^Wilson
St iiaafleu- . >
/
} Pineii/sa
From.
4. REMARKS:
.To.Ft..
i§\
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTIONSTANDARDS. AND THAT A COPY OF THIS RECORD ^
SIGN^TURE'OF contractor or AGENTSucmit original to Division ol Environmental Management and cooy to well owner.W.I REVISED 2/90
.JRTH CAROLINA DEPARTMENT OF ENVIRONMENT. HEALTH AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNOWATER SECTION
P.O. BOX 27M7. RALEIGH. NC 27611-7687
PHONE [phone]
WELL CONSTRUCTION RECORD MW-6
FOR OFFICE USE ONLY
Oiiad. No.Serial No.
1 at Lon^7 Dr
C5W-1 Pnt
I. /-r^MTo&rTno Aoolied Environmental Services, Inc.' CONTRACTOH STATE WELL CONSTRUCTION
.ER REGISTRATION NUMBER PERMIT NUMBER: 97-07.01 -WM-DD^"^
.L LOCATION: CShow sketch of the location below)
res. Town: Wilson
:ur-phv Manufacturing Co.. 2000 Airport Drive
Id. Community, or Subdivision and Lot No.)
C.W. Layman
NER
County:Wilson
Deoth(ft. )DRILLING LOG
CORESS P.O, Box 2009
Wilson
CStreet o.'- Route No.)
NC 27894
Zip Code
Monitor
City or Town State
lATS DRILLED ^/^/91 USE OF WELL
•AL DEPTH 18 CUTTINGS COLLECTED S Yes □ No
lOES WELL REPLACE EXISTING WELL? □ Yes Q No
~\Tic water 1 pvFi ■ 3.31
TOP OF CASING IS Q
'lELD (gpm): METHOD OF TEST
FT. n above TOP OF CASING,ICC belowFT. ABOVE LAND SURFACE.
From To Formation Desc-'iption
0 7 Orange-arav siltv CLAY
7 14 Tan-erav fine sandv siltv CLAY
14 18 Tan-grav fine sandv SILT
TER ZONES Cdaoth):
IHLCRINATION:
.SING:
From
From
From
^OUT:
Type Amount
From
From
-CREEN;
Depth
_To «
,Tc
To
Depth
6 To. 7
Wall Thickness . . ,Diameter or Weight/Ft. Material
If additional space is needea use back of form.
Ft.__21
.Ft..
-Ft..
LOCATION SKETCH
Maiertaf
pt. Bentonite
Ft. Neat Cement
_Nx#SS
Method
Material
Toirpedo Sand
Depth
From
From
Depth
8 18 Ft
Diameter
2
Slot Size
in 0.01 in.
Material
PVC 7
To Ft in in.
Prnm To Ft in in.
RAVEL PACK:
I DO HERP3Y CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTIONstandards, and THAT A COPY OF THIS RECORD HAS BE^N fRpviD^^T^E ^ .- //
1 REVISED 2/90
SIGN^RE OF CONTRACTOR OR AGENT DATE
Suomit original to Division of Environmental Management and copy to well owner.