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HomeMy WebLinkAboutFA-96056_96998_CA_IAR_20230523MINERAL SPRINGS ENVIRONMENTAL, P.C. 4600 MINERAL SPRINGS LANE RALEIGH, NORTH CAROLINA, 27616 919.261.8186 INITIAL ABATEMENT REPORT CAMPBELL SOUP SITE 2120 NC HIGHWAY 71 N MAXTON, ROBESON COUNTY, NORTH CAROLINA MAY 18, 2023 MSE JOB NO. 1210 Prepared For: EHC ENVIRONMENTAL POST OFFICE BOX 902 RED SPRINGS, NORTH CAROLINA, 28377 TABLE OF CONTENTS 1 INTRODUCTION 2 2 SITE REMEDIATION 2 3 POST-REMEDIATION SAMPLING 2 4 CONCLUSIONS AND PETITION FOR NO-FURTHER ACTION 2 5 LIMITATIONS 3 TABLE OF CONTENTS DRAWINGS Drawing 1 Topographic Site Map Drawing 2 Site Map TABLES Table 1 Summary of Soil Analytical Results APPENDICE Appendix A Photographs Appendix B Non-Hazardous Waste Disposal Summary and Manifest Appendix C Laboratory Analytical Reports and Chain-of-Custody Records INITIAL ABATEMENT REPORT CAMPBELL SOUP SITE 2120 NC Highway 71 N Maxton, North Carolina May 18, 2023 1 INTRODUCTION The subject site is located at 2120 NC Highway 71 N Maxton, North Carolina (see Drawing 1). The latitude and longitude of the site are 340 46’ 20.70” north and 790 19’ 39.94” west, respectively. On April 2, 2023 a vehicle owned by Swift Transport was involved in an incident that resulted in a release of petroleum to the subject property. On April 2, 2023, EHC Environmental (EHC) responded to the spill and recovered free product and cleaned the road. 2 SITE REMEDIATION On April 27, 2023 EHC under the technical oversight of Mineral Springs Environmental PC (MSE) mobilized to the site and excavated 16.5 tons of impacted soil at the site. The excavation dimensions averaged approximately 12 feet wide by 16 feet long and between one and two feet deep and are shown on Drawing 2. Photographs of the remediation activities are provided in Appendix A. The soil was disposed of at the GTA Farms facility located in Lumber Bridge, North Carolina The soil manifest and weigh tickets are contained in Appendix B. The excavation was backfilled with imported soil. 3 POST-REMEDIATION SAMPLING In order to determine the effectiveness of the soil remediation activities seven soil sample (SS-1 thru SS-3) were collected from the bottom of the excavated area to document the effectiveness of the excavation activities. The soil sample location is shown on Drawing 2. The samples were analyzed for the presence of total petroleum hydrocarbons (TPH) as diesel (DRO) and TPH as gasoline (GRO) according to EPA Method 3550 and 5035 by Environmental Conservation Laboratories (ENCO) located in Cary, North Carolina. Soil samples (SS-1 thru SS-3) did not reveal the presence of TPH DRO or GRO at concentrations above the NC UST Section’s cleanup levels. The analytical results are contained in Appendix C and summarized on Table 1. 4 CONCLUSIONS A release of petroleum product occurred during an incident at the above referenced site. On April 27, 2023 steps were taken to excavate impacted soil on the subject site. Based on the analytical results, the remediation activity was successful in removing the petroleum release to below the State’s enforced cleanup standards in the area of impact. As such no further excavation will be required. DRAWINGS DRAWING NO. 1 TOPOGRAPHIC SITE MAP CAMPBELL SOUP SITE 2120 HWY 71 N MAXTON, NORTH CAROLINA Date: May 2023 Job No.: MSE 1210 File: 1210/Drawing 1 By: KP SITE TABLES SS-1SS-2SS-3Gasoline Range Organics17B6.2JB14B50Diesel Range Organics5.1JB3.9JB3.7JB100Notes: mg/Kg - Milligrams per kilogramJ - Estimated ValueMSCC - Maximum Soil Contaminant ConcentrationValues shown in bold type exceed their respective soil-to-groundwater MSCCBQL - Below Quantitation LimitB - Compound Identified in Lab BlankNA - Not AnalyzedNE - None establishedTABLE 1SOIL SAMPLE LABORATORY ANALYTICAL RESULTSCAMPBELL SOUP SITEMAXTON, NORTH CAROLINATotal Petroleum HydrocarbonsMSE JOB 1210Constituent (mg/Kg) Sample NumberSoil to Groundwater APPENDICES APPENDIX A PICTURES APPENDIX B CERTIFICATE OF DISPOSAL AND MANIFEST APPENDIX C LABORATORY ANALYTICAL RESULTS ANALYTICAL REPORT PREPARED FOR Attn: Kirk Pollard Mineral Springs Environmental 4600 Mineral Springs Lane Raleigh, North Carolina 27616 Generated 5/9/2023 8:47:54 AM JOB DESCRIPTION Campbell Soup JOB NUMBER 752-6188-1 See page two for job notes and contact information. Cary NC 27511 102-A Woodwinds Industrial Court Eurofins Raleigh Page 1 of 19 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Raleigh Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 5/9/2023 8:47:54 AM Authorized for release by Bill Scott, Project Manager Bill.Scott@et.eurofinsus.com (919)677-1669 Page 2 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Mineral Springs Environmental Project/Site: Campbell Soup Laboratory Job ID: 752-6188-1 Page 3 of 19 Eurofins Raleigh5/9/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Qualifiers GC VOA Qualifier Description B Compound was found in the blank and sample. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. GC Semi VOA Qualifier Description B Compound was found in the blank and sample. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary These commonly used abbreviations may or may not be present in this report. ¤ Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Raleigh Page 4 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Mineral Springs Environmental Job ID: 752-6188-1 Project/Site: Campbell Soup Job ID: 752-6188-1 Laboratory: Eurofins Raleigh Narrative Job Narrative 752-6188-1 Receipt The samples were received on 5/1/2023 2:47 PM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.4°C Gasoline Range Organics Method 8015D_GRO: The method blank for analytical batch 680-776749 contained Gasoline Range Organics (GRO) above the method detection limit (MDL). Associated samples were not re-analyzed because results were less than one half the reporting limit (RL). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Diesel Range Organics Method 8015D_DRO: The method blank for preparation batch 680-777448 and analytical batch 680-777535 contained Diesel Range Organics (DRO) above the method detection limit (MDL). Associated samples were not re-analyzed because results were less than one half the reporting limit (RL). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins RaleighPage 5 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Client Sample ID: SS-1 Lab Sample ID: 752-6188-1 ☼Gasoline Range Organics (GRO) RL 12 mg/Kg MDL 3.1 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA100B178015D ☼Diesel Range Organics (DRO)8.7 mg/Kg2.8 Total/NA15.1 J B 8015D Client Sample ID: SS-2 Lab Sample ID: 752-6188-2 ☼Gasoline Range Organics (GRO) RL 9.0 mg/Kg MDL 2.3 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA100J B6.2 8015D ☼Diesel Range Organics (DRO)8.9 mg/Kg2.9 Total/NA13.9 J B 8015D Client Sample ID: SS-3 Lab Sample ID: 752-6188-3 ☼Gasoline Range Organics (GRO) RL 12 mg/Kg MDL 2.9 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA100B148015D ☼Diesel Range Organics (DRO)9.2 mg/Kg3.0 Total/NA13.7 J B 8015D Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 6 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Lab Sample ID: 752-6188-1Client Sample ID: SS-1 Matrix: SolidDate Collected: 05/01/23 13:30 Percent Solids: 91.8Date Received: 05/01/23 14:47 Method: SW846 8015D - Gasoline Range Organics (GRO) (GC) RL MDL 17 B 12 3.1 mg/Kg ☼05/03/23 15:52 05/03/23 21:56 100 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Gasoline Range Organics (GRO) a,a,a-Trifluorotoluene 86 70-131 05/03/23 15:52 05/03/23 21:56 100 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: SW846 8015D - Diesel Range Organics (DRO) (GC) RL MDL 5.1 J B 8.7 2.8 mg/Kg ☼05/08/23 12:05 05/08/23 20:46 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Diesel Range Organics (DRO) o-Terphenyl 68 15-139 05/08/23 12:05 05/08/23 20:46 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Lab Sample ID: 752-6188-2Client Sample ID: SS-2 Matrix: SolidDate Collected: 05/01/23 13:45 Percent Solids: 88.3Date Received: 05/01/23 14:47 Method: SW846 8015D - Gasoline Range Organics (GRO) (GC) RL MDL 6.2 J B 9.0 2.3 mg/Kg ☼05/03/23 15:52 05/03/23 22:17 100 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Gasoline Range Organics (GRO) a,a,a-Trifluorotoluene 88 70-131 05/03/23 15:52 05/03/23 22:17 100 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: SW846 8015D - Diesel Range Organics (DRO) (GC) RL MDL 3.9 J B 8.9 2.9 mg/Kg ☼05/08/23 12:05 05/08/23 21:01 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Diesel Range Organics (DRO) o-Terphenyl 72 15-139 05/08/23 12:05 05/08/23 21:01 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Lab Sample ID: 752-6188-3Client Sample ID: SS-3 Matrix: SolidDate Collected: 05/01/23 14:00 Percent Solids: 86.3Date Received: 05/01/23 14:47 Method: SW846 8015D - Gasoline Range Organics (GRO) (GC) RL MDL 14 B 12 2.9 mg/Kg ☼05/03/23 15:52 05/03/23 22:39 100 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Gasoline Range Organics (GRO) a,a,a-Trifluorotoluene 87 70-131 05/03/23 15:52 05/03/23 22:39 100 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: SW846 8015D - Diesel Range Organics (DRO) (GC) RL MDL 3.7 J B 9.2 3.0 mg/Kg ☼05/08/23 12:05 05/08/23 21:16 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Diesel Range Organics (DRO) o-Terphenyl 70 15-139 05/08/23 12:05 05/08/23 21:16 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Eurofins Raleigh Page 7 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Method: 8015D - Gasoline Range Organics (GRO) (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (70-131) TFT1 86752-6188-1 Percent Surrogate Recovery (Acceptance Limits) SS-1 88752-6188-2 SS-2 87752-6188-3 SS-3 119LCS 680-776749/6 Lab Control Sample 122LCSD 680-776749/7 Lab Control Sample Dup 91MB 680-776749/8 Method Blank Surrogate Legend TFT = a,a,a-Trifluorotoluene Method: 8015D - Diesel Range Organics (DRO) (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (15-139) OTPH 68752-6188-1 Percent Surrogate Recovery (Acceptance Limits) SS-1 72752-6188-2 SS-2 70752-6188-3 SS-3 112LCS 680-777448/20-A Lab Control Sample 96MB 680-777448/19-A Method Blank Surrogate Legend OTPH = o-Terphenyl Eurofins Raleigh Page 8 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Method: 8015D - Gasoline Range Organics (GRO) (GC) Client Sample ID: Method BlankLab Sample ID: MB 680-776749/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 776749 RL MDL Gasoline Range Organics (GRO) 3.63 J 10 2.5 mg/Kg 05/03/23 16:04 100 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier a,a,a-Trifluorotoluene 91 70-131 05/03/23 16:04 100 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-776749/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 776749 Gasoline Range Organics (GRO)50.0 54.3 mg/Kg 109 64 -133 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec Limits a,a,a-Trifluorotoluene 70 -131 Surrogate 119 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-776749/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 776749 Gasoline Range Organics (GRO)50.0 55.1 mg/Kg 110 64 -133 2 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec Limits LimitRPD RPD a,a,a-Trifluorotoluene 70 -131 Surrogate 122 LCSD LCSD Qualifier Limits%Recovery Method: 8015D - Diesel Range Organics (DRO) (GC) Client Sample ID: Method BlankLab Sample ID: MB 680-777448/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 777535 Prep Batch: 777448 RL MDL Diesel Range Organics (DRO) 2.71 J 7.9 2.6 mg/Kg 05/08/23 12:05 05/08/23 18:41 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier o-Terphenyl 96 15-139 05/08/23 18:41 1 MB MB Surrogate 05/08/23 12:05 Dil FacPrepared AnalyzedQualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-777448/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 777535 Prep Batch: 777448 Diesel Range Organics (DRO)33.1 25.1 mg/Kg 76 26 -133 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec Limits o-Terphenyl 15 -139 Surrogate 112 LCS LCS Qualifier Limits%Recovery Eurofins Raleigh Page 9 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup GC VOA Analysis Batch: 776749 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015D 776804752-6188-1 SS-1 Total/NA Solid 8015D 776804752-6188-2 SS-2 Total/NA Solid 8015D 776804752-6188-3 SS-3 Total/NA Solid 8015DMB 680-776749/8 Method Blank Total/NA Solid 8015DLCS 680-776749/6 Lab Control Sample Total/NA Solid 8015DLCSD 680-776749/7 Lab Control Sample Dup Total/NA Prep Batch: 776804 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035A752-6188-1 SS-1 Total/NA Solid 5035A752-6188-2 SS-2 Total/NA Solid 5035A752-6188-3 SS-3 Total/NA GC Semi VOA Prep Batch: 777448 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546752-6188-1 SS-1 Total/NA Solid 3546752-6188-2 SS-2 Total/NA Solid 3546752-6188-3 SS-3 Total/NA Solid 3546MB 680-777448/19-A Method Blank Total/NA Solid 3546LCS 680-777448/20-A Lab Control Sample Total/NA Analysis Batch: 777535 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015D 777448752-6188-1 SS-1 Total/NA Solid 8015D 777448752-6188-2 SS-2 Total/NA Solid 8015D 777448752-6188-3 SS-3 Total/NA Solid 8015D 777448MB 680-777448/19-A Method Blank Total/NA Solid 8015D 777448LCS 680-777448/20-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 776871 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture752-6188-1 SS-1 Total/NA Solid Moisture752-6188-2 SS-2 Total/NA Solid Moisture752-6188-3 SS-3 Total/NA Eurofins Raleigh Page 10 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Mineral Springs Environmental Job ID: 752-6188-1 Project/Site: Campbell Soup Client Sample ID: SS-1 Lab Sample ID: 752-6188-1 Matrix: SolidDate Collected: 05/01/23 13:30 Date Received: 05/01/23 14:47 Analysis Moisture KG1 776871 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/04/23 10:04 Client Sample ID: SS-1 Lab Sample ID: 752-6188-1 Matrix: SolidDate Collected: 05/01/23 13:30 Percent Solids: 91.8Date Received: 05/01/23 14:47 Prep 5035A FES776804 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/03/23 15:52 Analysis 8015D 100 776749 DBM EET SAVTotal/NA 05/03/23 21:56 Prep 3546 777448 MEW EET SAVTotal/NA 05/08/23 12:05 Analysis 8015D 1 777535 DBM EET SAVTotal/NA 05/08/23 20:46 Client Sample ID: SS-2 Lab Sample ID: 752-6188-2 Matrix: SolidDate Collected: 05/01/23 13:45 Date Received: 05/01/23 14:47 Analysis Moisture KG1 776871 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/04/23 10:04 Client Sample ID: SS-2 Lab Sample ID: 752-6188-2 Matrix: SolidDate Collected: 05/01/23 13:45 Percent Solids: 88.3Date Received: 05/01/23 14:47 Prep 5035A FES776804 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/03/23 15:52 Analysis 8015D 100 776749 DBM EET SAVTotal/NA 05/03/23 22:17 Prep 3546 777448 MEW EET SAVTotal/NA 05/08/23 12:05 Analysis 8015D 1 777535 DBM EET SAVTotal/NA 05/08/23 21:01 Client Sample ID: SS-3 Lab Sample ID: 752-6188-3 Matrix: SolidDate Collected: 05/01/23 14:00 Date Received: 05/01/23 14:47 Analysis Moisture KG1 776871 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/04/23 10:04 Client Sample ID: SS-3 Lab Sample ID: 752-6188-3 Matrix: SolidDate Collected: 05/01/23 14:00 Percent Solids: 86.3Date Received: 05/01/23 14:47 Prep 5035A FES776804 EET SAV Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 05/03/23 15:52 Analysis 8015D 100 776749 DBM EET SAVTotal/NA 05/03/23 22:39 Prep 3546 777448 MEW EET SAVTotal/NA 05/08/23 12:05 Analysis 8015D 1 777535 DBM EET SAVTotal/NA 05/08/23 21:16 Eurofins Raleigh Page 11 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Mineral Springs Environmental Job ID: 752-6188-1 Project/Site: Campbell Soup Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Raleigh Page 12 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Mineral Springs Environmental Job ID: 752-6188-1 Project/Site: Campbell Soup Laboratory: Eurofins Savannah Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 269 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte 8015D 3546 Solid Diesel Range Organics (DRO) 8015D 5035A Solid Gasoline Range Organics (GRO) Moisture Solid Percent Moisture Moisture Solid Percent Solids Eurofins Raleigh Page 13 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 752-6188-1Client: Mineral Springs Environmental Project/Site: Campbell Soup Method Method Description LaboratoryProtocol SW8468015D Gasoline Range Organics (GRO) (GC)EET SAV SW8468015D Diesel Range Organics (DRO) (GC)EET SAV EPAMoisture Percent Moisture EET SAV SW8463546 Microwave Extraction EET SAV SW8465035A Closed System Purge & Trap/Methanol EET SAV Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Raleigh Page 14 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Mineral Springs Environmental Job ID: 752-6188-1 Project/Site: Campbell Soup Lab Sample ID Client Sample ID Matrix Collected Received 752-6188-1 SS-1 Solid 05/01/23 13:30 05/01/23 14:47 752-6188-2 SS-2 Solid 05/01/23 13:45 05/01/23 14:47 752-6188-3 SS-3 Solid 05/01/23 14:00 05/01/23 14:47 Eurofins RaleighPage 15 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 16 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 17 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Mineral Springs Environmental Job Number: 752-6188-1 Login Number: 6188 Question Answer Comment Creator: Hyatt, Samantha List Source: Eurofins Raleigh List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. Eurofins Raleigh Page 18 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Mineral Springs Environmental Job Number: 752-6188-1 Login Number: 6188 Question Answer Comment Creator: Harley, Tynisha List Source: Eurofins Savannah List Creation: 05/03/23 12:26 PMList Number: 2 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Raleigh Page 19 of 19 5/9/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15