FA-92656_96799_CA_O_20230320

MINERAL SPRINGS ENVIRONMENTAL, P.C.
4600 MINERAL SPRINGS LANE
RALEIGH, NORTH CAROLINA, 27616
919.261.8186

INITIAL ABATEMENT
REPORT

SHECKELS PROPERTY SITE
6916 GLYNN MILL FARM DRIVE
FAYETTEVILLE, CUMBERLAND COUNTY,
NORTH CAROLINA
MARCH 20, 2023
MSE JOB NO. 1195

Prepared For:
EHC ENVIRONMENTAL
POST OFFICE BOX 902
RED SPRINGS, NORTH CAROLINA, 28377
TABLE OF CONTENTS
1 INTRODUCTION 2
2 SITE REMEDIATION 2
3 POST-REMEDIATION SAMPLING 2
4 CONCLUSIONS AND PETITION FOR NO-FURTHER ACTION 2
5 LIMITATIONS 3

TABLE OF CONTENTS

DRAWINGS

Drawing 1 Topographic Site Map
Drawing 2 Site Map

TABLES

Table 1 Summary of Soil Analytical Results

APPENDICE

Appendix A Photographs
Appendix B Non-Hazardous Waste Disposal Summary and Manifest
Appendix C Laboratory Analytical Reports and Chain-of-Custody Records

INITIAL ABATEMENT REPORT
SHECKELS PROPERTY SITE
6916 Glynn Mill Farm Drive
Fayetteville, North Carolina
March 20, 2023

1 INTRODUCTION

The subject site is located south of 6916 Glynn Mill Farms Drive and south of Fayetteville, North
Carolina (see Drawing 1). The latitude and longitude of the site are 340 50’ 56.34” north and 780
51’ 47.82” west, respectively. On August 20, 2022 a vehicle owned by an unknown drive was
involved in an incident that resulted in a release of petroleum to the subject property. The
incident occurred between 20 and 30 feet north of County Line Road and approximately 165
feet east of Glynn Mill Farms Drive (see Drawing 2).

2 SITE REMEDIATION

On February 28, 2023 EHC Environmental (EHC) under the technical oversight of Mineral
Springs Environmental PC (MSE) mobilized to the site and excavated 3.03 tons of impacted soil
at the site. The excavation dimensions averaged approximately five feet wide by nine feet long
and between 12 inches and 30 inches deep and are shown on Drawing 2. Photographs of the
remediation activities are provided in Appendix A. The soil was disposed of at the Republic
Services Inc. facility located in Bishopville, South Carolina. RSI’s Certificate of Destruction is
contained in Appendix B. The excavation was backfilled with imported soil.

3 POST-REMEDIATION SAMPLING

In order to determine the effectiveness of the soil remediation activities one soil sample (SS-B1)
was collected from the bottom of the excavated area to document the effectiveness of the
excavation activities. The soil sample location is shown on Drawing 2. The sample was analyzed
for volatile organic compounds (VOCs) and semi VOCs (SVOCs) according to SW-846 Methods
8260 and 8270. The soil sample was also analyzed for volatile and extractable petroleum
hydrocarbons (VPH/EPH). The analytical results for soil sample SS-B1 indicated no VOCs, SVOCs
or VPH/EPH compounds in excess of the soil-to-groundwater maximum soil contaminant
concentration (MSCC).

4 CONCLUSIONS

A release of petroleum product occurred during an incident at the above referenced site. In mid
August 2022 steps were taken to excavate impacted soil on the subject site. Based on the
analytical results, the remediation activity was successful in removing the petroleum release to
below the State’s enforced cleanup standards in the area of impact. As such no further
excavation will be required.

A copy of this report should be submitted to the NC UST Section’s Fayetteville Regional Office.

DRAWINGS
DRAWING NO. 1

TOPOGRAPHIC SITE MAP
SHECKELS PROPERTY SITE
6916 GLYNN MILL FARM DRIVE
FAYETTEVILLE, NORTH CAROLINA
Date: March 2023
Job No.: MSE 1195
File: 1195/Drawing 1
By: KP
SITE
TABLES
Sample NumberSS-B1Bis (2-ethylhexyl) phthalate 0.250J 6.6 47C9-C10 Aromatics 1.0 31 469C9-C18 Aliphatics 2.4J 540 1560C19-C36 Aliphatics 9.7J immobile 31,200C11-C22 Aromatics 7.8J 31 469Notes: mg/Kg - Milligrams per kilogramMSCC - Maximum Soil Contaminant ConcentrationValues shown in bold type exceed their respective soil-to-groundwater MSCCBQL - Below Quantitation LimitNA - Not AnalyzedNE - None establishedExtractable Petroleum HydrocarbonsSoil to Groundwater MSCC (mg/Kg)Volatile Petroleum HydrocarbonsSemi-Volatile Organic CompoundsTABLE 1SOIL SAMPLE LABORATORY ANALYTICAL RESULTSConstituent (mg/Kg)SHECKELS PROPERTYFAYETTEVILLE, NORTH CAROLINAMSE JOB 1195Residential MSCC (mg/Kg)
APPENDICES

APPENDIX A

PICTURES

APPENDIX B

CERTIFICATE OF DESTRUCTION

APPENDIX C

LABORATORY ANALYTICAL RESULTS

October 14, 2022

Kirk Pollard
Mineral Springs Environmental PC
4600 Mineral Spring Lane
Raleigh, North Carolina 27616

Re: PFAS Soil Sample
Work Order: 594902

Dear Kirk Pollard:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on September 29, 2022. This original data report has been prepared and reviewed in
accordance with GEL’s standard operating procedures.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL’s accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 1614.

Sincerely,

PM_SIGN_HERE
Delaney Stone
Project Manager

Enclosures
Page 1 of 17 SDG: 594902
Reviewed by USER_SIGN_HERE
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
MSEP001 Mineral Springs Environmental PC
Client SDG: 594902 GEL Work Order: 594902
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the ’U’ qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Delaney Stone.
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J See case narrative for an explanation
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
for
Page 2 of 17 SDG: 594902
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 14, 2022
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDL PF
LCMSMS PFCs
23285051242ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
10/13/22MB20.483
0.513
0.478
1.03
1.03
0.456
1.03
0.513
0.513
0.466
0.513
0.513
0.513
0.513
0.513
0.513
0.513
0.513
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Kirk PollardContact:
Mineral Springs Environmental PCCompany :
4600 Mineral Spring Lane
Raleigh, North Carolina 27616
Address :
PFAS Soil SampleProject:
594902001
Soil
28-SEP-22 09:00
29-SEP-22
SS-1 MSEP00121Project:
MSEP001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
Moisture:5.75%
0.169
0.169
0.169
0.282
0.338
0.169
0.379
0.169
0.169
0.169
0.205
0.169
0.205
0.205
0.205
0.169
0.169
0.169
1U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-X)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanoic acid (PFNA)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid (PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
EPA 537Mod PFCs by LC-MS/MS "Dry Weight Corrected"
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.234
ND
ND
ND
ND
ND
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
4.83
The following Prep Methods were performed:
EPA 537.1 Modified PFCs Extraction in Solid 10/13/22 23285040545TC2
Method Description Analyst Date Time Prep Batch
Page 3 of 17 SDG: 594902
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Report Date: October 14, 2022
Parameter Result UnitsQualifier Analyst Date TimeDF Batch MethodRLDL PF
Kirk PollardContact:
Mineral Springs Environmental PCCompany :
4600 Mineral Spring Lane
Raleigh, North Carolina 27616
Address :
PFAS Soil SampleProject:
594902001
SS-1 MSEP00121Project:
MSEP001Client ID:Sample ID:
Client Sample ID:
The following Analytical Methods were performed:
1
Method Description
EPA 537.1 Modified
Analyst Comments
Notes:

Lc/LC: Critical Level
PF: Prep Factor
RL: Reporting Limit
SQL: Sample Quantitation Limit
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration
Page 4 of 17 SDG: 594902
Certificate of Analysis
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Gravimetric Solids
Parameter Result UnitsQualifier Analyst Date Time
"As Received"
RL DF
Kirk PollardContact:
Mineral Springs Environmental PCCompany :
4600 Mineral Spring Lane
Raleigh, North Carolina 27616 October 14, 2022Report Date:
Address :
PFAS Soil SampleProject:
594902001
Soil
28-SEP-22
29-SEP-22
SS-1 MSEP00121Project:
MSEP001Client ID:
Client
Sample ID:
Receive Date:
Client Sample ID:
Matrix:
Collect Date:
Collector:
Moisture:
Batch
5.75%
Mtd.
The following Analytical Methods were performed
Method Description
1 ASTM D 2216 (Modified)
Notes:
The MDC is a sample specific MDC.
Acceptable LimitsTestRecovery%Batch IDSurrogate/Tracer Recovery
MDC TPUUncertainty
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
PF
Column headers are defined as follows:
DF: Dilution Factor
DL: Detection Limit
Lc/LC: Critical Level
MDA: Minimum Detectable Activity
MDC: Minimum Detectable Concentration

Mtd.: Method
PF: Prep Factor
RL: Reporting Limit
TPU: Total Propagated Uncertainty
Page 5 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2328505Batch
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-X)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanoic acid (PFNA)
Perfluorooctane sulfonic acid
(PFOS)
Parmname
Kirk PollardContact:
Mineral Springs Environmental PC
4600 Mineral Spring Lane
Raleigh, North Carolina
October 14, 2022Report Date:
Units
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
Anlst Date Time
MB2 10/13/22 09:59
QC
5.59
5.84
5.90
5.48
5.90
5.85
5.51
5.72
5.89
5.09
5.40
5.37
6.39
5.79
NOM Sample Range
(69%-143%)
(70%-135%)
(66%-140%)
(72%-137%)
(66%-141%)
(68%-141%)
(71%-136%)
(66%-139%)
(70%-139%)
(72%-132%)
(68%-139%)
(70%-135%)
(70%-136%)
(73%-135%)
Qual
QC1205215918
REC%
120
118
128
111
120
119
126
116
120
103
120
109
130
117
4.64
4.93
4.59
4.93
4.93
4.93
4.36
4.93
4.93
4.93
4.49
4.93
4.93
4.93
LCS
594902Workorder:
RPD/D%
Page 1 of 6
Page 6 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2328505Batch
Perfluorooctanoic acid (PFOA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-X)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexane sulfonic acid
(PFHxS)
Parmname Units
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
Anlst Date Time
MB2 10/13/22 09:59
10/13/22 09:50
QC
4.36
6.09
6.48
6.15
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NOM Sample Range
(72%-135%)
(72%-139%)
(60%-149%)
(70%-135%)
Qual
U
U
U
U
U
U
U
U
U
U
U
QC1205215917
REC%
88
124
132
125
4.93
4.93
4.93
4.93
MB
594902Workorder:
RPD/D%
Page 2 of 6
Page 7 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2328505Batch
Perfluorohexanoic acid (PFHxA)
Perfluorononanoic acid (PFNA)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-X)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorodecanoic acid (PFDA)
Parmname Units
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
Anlst Date Time
MB2 10/13/22 09:50
10/13/22 10:16
QC
ND
ND
ND
ND
ND
ND
ND
4.90
5.25
5.21
5.67
5.16
5.46
4.83
5.83
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
Range
(43%-141%)
(63%-143%)
(62%-146%)
(61%-150%)
(65%-152%)
(59%-152%)
(67%-146%)
(59%-153%)
Qual
U
U
U
U
U
U
U
QC1205215919 595631001
REC%
114
115
122
124
113
119
119
125
4.31
4.58
4.27
4.58
4.58
4.58
4.05
4.58
MS
594902Workorder:
U
U
U
U
U
U
U
U
RPD/D%
Page 3 of 6
Page 8 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2328505Batch
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanoic acid (PFNA)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
11-Chloroeicosafluoro-3-
oxaundecane-1-sulfonic acid (11-
Cl-PF3OUdS)
4,8-Dioxa-3H-perfluorononanoic
acid (DONA)
9-Chlorohexadecafluoro-3-
oxanonane-1-sulfonic acid (9-Cl-
PF3ONS)
Hexafluoropropyleneoxide dimer
acid (HFPO-DA)(Gen-X)
N-Ethylperfluorooctane
sulfonamido acetic acid
(NEtFOSAA)
Parmname Units
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
Anlst Date Time
MB2 10/13/22 10:16
10/13/22 10:24
QC
6.15
5.97
4.85
5.67
6.71
6.38
3.99
6.02
6.36
6.23
5.95
6.69
6.41
6.48
5.99
NOM Sample
ND
ND
ND
ND
ND
1.25
ND
ND
ND
ND
ND
ND
ND
ND
ND
Range
(59%-147%)
(61%-149%)
(64%-150%)
(61%-151%)
(58%-152%)
(53%-157%)
(53%-155%)
(60%-157%)
(35%-157%)
(58%-154%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
Qual
QC1205215920 595631001
19
24
21
13
15
REC%
134
130
116
124
147
112
87
132
139
136
122
130
133
126
116
4.58
4.58
4.17
4.58
4.58
4.58
4.58
4.58
4.58
4.58
4.86
5.16
4.81
5.16
5.16
MSD
594902Workorder:
U
U
U
U
U
U
U
U
U
U
U
U
U
U
RPD/D%
Page 4 of 6
Page 9 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Perfluorinated Compounds
2328505Batch
N-Methylperfluorooctane
sulfonamido acetic acid
(NMeFOSAA)
Perfluorobutane sulfonic acid
(PFBS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic acid (PFDOA)
Perfluoroheptanoic acid (PFHpA)
Perfluorohexane sulfonic acid
(PFHxS)
Perfluorohexanoic acid (PFHxA)
Perfluorononanoic acid (PFNA)
Perfluorooctane sulfonic acid
(PFOS)
Perfluorooctanoic acid (PFOA)
Perfluorotetradecanoic acid
(PFTDA)
Perfluorotridecanoic acid
(PFTrDA)
Perfluoroundecanoic acid
(PFUnDA)
Parmname Units
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
ng/g
Anlst Date Time
MB2 10/13/22 10:24
QC
6.98
5.54
6.47
7.02
6.49
5.53
5.86
6.01
7.82
4.87
6.53
6.47
6.75
NOM Sample
ND
ND
ND
ND
ND
ND
ND
ND
1.25
ND
ND
ND
ND
Range
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
(0%-30%)
Qual
The Qualifiers in this report are defined as follows:
25
14
10
13
8
13
3
11
20
20
8
2
8
REC%
135
121
123
136
126
118
114
116
127
94
126
125
131
5.16
4.57
5.16
5.16
5.16
4.71
5.16
5.16
5.16
5.16
5.16
5.16
5.16
594902Workorder:
**
<
>
Analyte is a surrogate compound
Result is less than value reported
Result is greater than value reported
U
U
U
U
U
U
U
U
U
U
U
U
RPD/D%
Notes:
Page 5 of 6
Page 10 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Parmname
Page 6 of 6
Units Anlst Date TimeQCNOMSampleRangeQualREC%
594902Workorder:
A
B
C
D
E
H
J
J
JNX
N
N
N/A
N1
ND
NJ
P
Q
R
U
UJ
X
Y
^
h
The TIC is a suspected aldol-condensation product
The target analyte was detected in the associated blank.
Analyte has been confirmed by GC/MS analysis
Results are reported from a diluted aliquot of the sample
Concentration of the target analyte exceeds the instrument calibration range
Analytical holding time was exceeded
See case narrative for an explanation
Value is estimated
Non Calibrated Compound
Organics--Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based
on nearest internal standard response factor
Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest
internal standard response factor
RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Organics--The concentrations between the primary and confirmation columns/detectors is >40% different. For HPLC, the difference is >70%.
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Compound cannot be extracted
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
QC Samples were not spiked with this compound
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +/- the RL is used to
evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
RPD/D%
Page 11 of 17 SDG: 594902
QC Summary
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Parmname
Kirk PollardContact:
Mineral Springs Environmental PCClient :
4600 Mineral Spring Lane
Raleigh, North Carolina
October 14, 2022
Page 1 of 1
Report Date:
Units Anlst Date TimeQCNOMSampleRangeQual
The Qualifiers in this report are defined as follows:
REC%
594902Workorder:
**
<
>
BD
FA
H
J
J
K
L
M
M
N/A
N1
ND
NJ
Q
R
U
UI
UJ
UL
X
Y
^
h
Analyte is a Tracer compound
Result is less than value reported
Result is greater than value reported
Results are either below the MDC or tracer recovery is low
Failed analysis.
Analytical holding time was exceeded
See case narrative for an explanation
Value is estimated
Analyte present. Reported value may be biased high. Actual value is expected to be lower.
Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M if above MDC and less than LLD
REMP Result > MDC/CL and < RDL
RPD or %Recovery limits do not apply.
See case narrative
Analyte concentration is not detected above the detection limit
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Gamma Spectroscopy--Uncertain identification
Gamma Spectroscopy--Uncertain identification
Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Other specific qualifiers were required to properly define the results. Consult case narrative.
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
** Indicates analyte is a surrogate/tracer compound.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC
standard unless qualified on the QC Summary.
RPD%
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Notes:
Page 12 of 17 SDG: 594902
Page 13 of 17 SDG: 594902
Page 14 of 17 SDG: 594902
State Certification
Alabama
Alaska
Alaska Drinking Water
Arkansas
CLIA
California
Colorado
Connecticut
DoD ELAP/ ISO17025 A2LA
Florida NELAP
Foreign Soils Permit
Georgia
Georgia SDWA
Hawaii
Idaho
Illinois NELAP
Indiana
Kansas NELAP
Kentucky SDWA
Kentucky Wastewater
Louisiana Drinking Water
Louisiana NELAP
Maine
Maryland
Massachusetts
Massachusetts PFAS Approv
Michigan
Mississippi
Nebraska
Nevada
New Hampshire NELAP
New Jersey NELAP
New Mexico
New York NELAP
North Carolina
North Carolina SDWA
North Dakota
Oklahoma
Pennsylvania NELAP
Puerto Rico
S. Carolina Radiochem
Sanitation Districts of L
South Carolina Chemistry
Tennessee
Texas NELAP
Utah NELAP
Vermont
Virginia NELAP
Washington
42200
17-018
SC00012
88-0651
42D0904046
2940
SC00012
PH-0169
2567.01
E87156
P330-15-00283, P330-15-00253
SC00012
967
SC00012
SC00012
200029
C-SC-01
E-10332
90129
90129
LA024
03046 (AI33904)
2019020
270
M-SC012
Letter
9976
SC00012
NE-OS-26-13
SC000122023-3
2054
SC002
SC00012
11501
233
45709
R-158
2022-137
68-00485
SC00012
10120002
9255651
10120001
TN 02934
T104704235-22-20
SC000122021-36
VT87156
460202
C780
List of current GEL Certifications as of 14 October 2022
Page 15 of 17 SDG: 594902

Technical Case Narrative
Mineral Springs Environmental PC
SDG #: 594902

LCMSMS-Misc

Product: The Extraction and Analysis of Per and Polyfluroalkyl Substances Using LCMSMS
Analytical Method: EPA 537.1 Modified
Analytical Procedure: GL-OA-E-076 REV# 12
Analytical Batches: 2328505 and 2328504
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
594902001 SS-1
1205215917 Method Blank (MB)
1205215918 Laboratory Control Sample (LCS)
1205215919 595631001(NonSDG) Matrix Spike (MS)
1205215920 595631001(NonSDG) Matrix Spike Duplicate (MSD)

The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this
report met the acceptance criteria specified in the analytical methods and procedures for initial calibration,
continuing calibration, instrument controls and process controls where applicable.

Radiochemistry

Product: Dry Weight
Preparation Method: ASTM D 2216 (Modified)
Preparation Procedure: GL-OA-E-020 REV# 13
Preparation Batch: 2324476
The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification
594902001 SS-1
1205207266 594902001(SS-1) Sample Duplicate (DUP)

The samples in this SDG were analyzed on an "as received" basis.
Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this
report met the acceptance criteria specified in the analytical methods and procedures for initial calibration,
continuing calibration, instrument controls and process controls where applicable.

Page 16 of 17 SDG: 594902

Certification Statement

Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 17 of 17 SDG: 594902
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-222306-1
Client Project/Site: CF14729
For:
Environmental Conservation Laboratories
102 Woodwinds Industrial Ct, Suite A
Cary, North Carolina 27511
Attn: Mr. Bill Scott
Authorized for release by:
10/19/2022 2:35:41 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Sample Summary
Client: Environmental Conservation Laboratories Job ID: 680-222306-1
Project/Site: CF14729
Lab Sample ID Client Sample ID Matrix Collected Received
680-222306-1 SS-1 Soil 09/28/22 09:00 10/04/22 08:00
Eurofins SavannahPage 2 of 43 10/19/2022
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Method Summary
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method Method Description LaboratoryProtocol
SW8468260D Volatile Organic Compounds by GC/MS EET SAV
SW8468270E Semivolatile Organic Compounds (GC/MS)EET SAV
SW8466010D Metals (ICP)EET SAV
SW8467470A Mercury (CVAA)EET SAV
EPAMoisture Percent Moisture EET SAV
SW8461311 TCLP Extraction EET SAV
SW8463010A Preparation, Total Metals EET SAV
SW8463546 Microwave Extraction EET SAV
SW8465035A Closed System Purge & Trap EET SAV
SW8467470A Preparation, Mercury EET SAV
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 3 of 43 10/19/2022
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Definitions/Glossary
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Qualifiers
GC/MS VOA
Qualifier Description
*+ LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Case Narrative
Client: Environmental Conservation Laboratories Job ID: 680-222306-1
Project/Site: CF14729
Job ID: 680-222306-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-222306-1
Receipt
The sample was received on 10/4/2022 8:00 AM. Unless otherwise noted below, the sample arrived in good condition, and, where
required, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 3.1°C, 5.5°C, 6.0°C and 6.4°C
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins SavannahPage 5 of 43 10/19/2022
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Detection Summary
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Client Sample ID: SS-1 Lab Sample ID: 680-222306-1
☼n-Butylbenzene
RL
200 ug/Kg
MDL
77
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA408808260D
☼sec-Butylbenzene 200 ug/Kg81 Total/NA40190 J 8260D
☼Ethylbenzene 200 ug/Kg85 Total/NA403208260D
☼Isopropylbenzene 200 ug/Kg89 Total/NA40130 J 8260D
☼4-Isopropyltoluene 200 ug/Kg110 Total/NA406708260D
☼Ethylbenzene 200 ug/Kg85 Total/NA403208260D
☼Naphthalene 200 ug/Kg130 Total/NA4023008260D
☼N-Propylbenzene 200 ug/Kg89 Total/NA40150 J 8260D
☼Isopropylbenzene 200 ug/Kg89 Total/NA40130 J 8260D
☼Toluene 200 ug/Kg110 Total/NA4032008260D
☼4-Isopropyltoluene 200 ug/Kg110 Total/NA406708260D
☼Methyl acetate 1000 ug/Kg330 Total/NA40420 J 8260D
☼Methylcyclohexane 200 ug/Kg81 Total/NA4092 J 8260D
☼1,3,5-Trimethylbenzene 200 ug/Kg98 Total/NA4041008260D
☼m-Xylene & p-Xylene 200 ug/Kg89 Total/NA4078008260D
☼Naphthalene 200 ug/Kg130 Total/NA4023008260D
☼n-Butylbenzene 200 ug/Kg77 Total/NA408808260D
☼o-Xylene 200 ug/Kg94 Total/NA4069008260D
☼m-Xylene & p-Xylene 200 ug/Kg89 Total/NA4078008260D
☼N-Propylbenzene 200 ug/Kg89 Total/NA40150 J 8260D
☼o-Xylene 200 ug/Kg94 Total/NA4069008260D
☼Xylenes, Total 410 ug/Kg150 Total/NA40150008260D
☼sec-Butylbenzene 200 ug/Kg81 Total/NA40190 J 8260D
☼Toluene 200 ug/Kg110 Total/NA4032008260D
☼1,3,5-Trimethylbenzene 200 ug/Kg98 Total/NA4041008260D
☼Xylenes, Total 410 ug/Kg150 Total/NA40150008260D
☼1,2,4-Trimethylbenzene - DL 1000 ug/Kg510 Total/NA200210008260D
☼1,2,4-Trimethylbenzene - DL 1000 ug/Kg510 Total/NA200210008260D
☼1-Methylnaphthalene 350 ug/Kg33 Total/NA129008270E
☼2-Methylnaphthalene 350 ug/Kg40 Total/NA19708270E
☼Anthracene 350 ug/Kg27 Total/NA138 J 8270E
☼Fluorene 350 ug/Kg38 Total/NA154 J 8270E
☼Naphthalene 350 ug/Kg32 Total/NA1320 J 8270E
☼Phenanthrene 350 ug/Kg29 Total/NA1130 J 8270E
Eurofins Savannah
This Detection Summary does not include radiochemical test results.
Page 6 of 43 10/19/2022
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
<450 2000 450 ug/Kg ☼10/07/22 13:44 10/10/22 19:31 40
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Acetone
2000 450 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<450Acetone
2000 1700 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1700Acetonitrile
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Benzene
4100 3000 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<3000Acrolein
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<69Bromobenzene
4100 1200 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1200Acrylonitrile
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Bromochloromethane
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Benzene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Bromodichloromethane
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<69Bromobenzene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Bromoform
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Bromochloromethane
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Bromomethane
1000 370 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<3702-Butanone (MEK)
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Bromoform
200 77 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼880n-Butylbenzene
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Bromomethane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼190 Jsec-Butylbenzene
1000 370 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<3702-Butanone (MEK)
200 100 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<100tert-Butylbenzene
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Carbon disulfide
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Carbon disulfide
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Carbon tetrachloride
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Carbon tetrachloride
200 57 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<57Chlorobenzene
200 57 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<57Chlorobenzene
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Chlorodibromomethane
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Chloroethane
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Chloroethane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Chloroform
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Chloroform
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Chloromethane
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<942-Chlorotoluene
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98Chloromethane
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<854-Chlorotoluene
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Chloroprene
200 140 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1403-Chloropropene
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<85Dibromochloromethane
410 65 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<651,2-Dibromo-3-Chloropropane
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<942-Chlorotoluene
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<691,2-Dibromoethane
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<854-Chlorotoluene
200 120 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<120cis-1,2-Dichloroethene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Dibromomethane
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<691,2-Dichlorobenzene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89cis-1,3-Dichloropropene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,3-Dichlorobenzene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<94Cyclohexane
Eurofins Savannah
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
<65 410 65 ug/Kg ☼10/07/22 13:44 10/10/22 19:31 40
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,2-Dibromo-3-Chloropropane
200 73 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<731,4-Dichlorobenzene
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<691,2-Dibromoethane
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<130 *+Dichlorodifluoromethane
200 120 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1201,1-Dichloroethane
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<941,2-Dichloroethane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Dibromomethane
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<691,2-Dichlorobenzene
200 120 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<120cis-1,2-Dichloroethene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,3-Dichlorobenzene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<94trans-1,2-Dichloroethene
200 150 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1501,1-Dichloroethene
200 73 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<731,4-Dichlorobenzene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1101,2-Dichloropropane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<81Dichlorobromomethane
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<891,3-Dichloropropane
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<130 *+Dichlorodifluoromethane
200 120 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1201,1-Dichloroethane
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<892,2-Dichloropropane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,1-Dichloropropene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<941,2-Dichloroethane
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89cis-1,3-Dichloropropene
200 150 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1501,1-Dichloroethene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110trans-1,3-Dichloropropene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1101,2-Dichloropropane
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼320Ethylbenzene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<891,3-Dichloropropane
200 170 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<170Hexachlorobutadiene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<892,2-Dichloropropane
1000 770 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<7702-Hexanone
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,1-Dichloropropene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼130 JIsopropylbenzene
4100 1900 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<19001,4-Dioxane
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼6704-Isopropyltoluene
10000 10000 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<10000Ethanol
410 330 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<330Methylene Chloride
1000 730 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<7304-Methyl-2-pentanone (MIBK)
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼320Ethylbenzene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110Ethyl methacrylate
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Methyl tert-butyl ether
200 120 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<120Freon 113
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼2300Naphthalene
200 170 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<170Hexachlorobutadiene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼150 JN-Propylbenzene
1000 770 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<7702-Hexanone
200 77 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<77Styrene
200 53 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<531,1,1,2-Tetrachloroethane
200 69 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<69Iodomethane
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<851,1,2,2-Tetrachloroethane
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
<3800 10000 3800 ug/Kg ☼10/07/22 13:44 10/10/22 19:31 40
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Isobutyl alcohol
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼130 JIsopropylbenzene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110Tetrachloroethene
410 61 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<61Isopropyl ether
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼3200Toluene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,2,3-Trichlorobenzene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼6704-Isopropyltoluene
200 100 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1001,2,4-Trichlorobenzene
2000 940 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<940Methacrylonitrile
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1101,1,1-Trichloroethane
1000 330 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼420 JMethyl acetate
200 61 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<611,1,2-Trichloroethane
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼92 JMethylcyclohexane
410 330 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<330Methylene Chloride
200 73 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<73Trichloroethene
410 180 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<180Methyl methacrylate
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<130Trichlorofluoromethane
200 73 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<731,2,3-Trichloropropane
1000 730 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<7304-Methyl-2-pentanone (MIBK)
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<89Methyl tert-butyl ether
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼41001,3,5-Trimethylbenzene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼7800m-Xylene & p-Xylene
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼2300Naphthalene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110Vinyl chloride
200 77 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼880n-Butylbenzene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼6900o-Xylene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼7800m-Xylene & p-Xylene
200 89 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼150 JN-Propylbenzene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼6900o-Xylene
410 150 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼15000Xylenes, Total
410 260 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<260Pentachloroethane
2000 1100 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1100Propionitrile
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼190 Jsec-Butylbenzene
200 77 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<77Styrene
200 100 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<100tert-Butylbenzene
200 53 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<531,1,1,2-Tetrachloroethane
200 85 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<851,1,2,2-Tetrachloroethane
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110Tetrachloroethene
410 250 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<250Tetrahydrofuran
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼3200Toluene
410 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<98trans-1,4-Dichloro-2-butene
200 94 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<94trans-1,2-Dichloroethene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110trans-1,3-Dichloropropene
200 81 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<811,2,3-Trichlorobenzene
200 100 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1001,2,4-Trichlorobenzene
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<1101,1,1-Trichloroethane
200 61 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<611,1,2-Trichloroethane
200 73 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<73Trichloroethene
200 130 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<130Trichlorofluoromethane
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
<73 200 73 ug/Kg ☼10/07/22 13:44 10/10/22 19:31 40
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,2,3-Trichloropropane
200 98 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼41001,3,5-Trimethylbenzene
410 220 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<220Vinyl acetate
200 110 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼<110Vinyl chloride
410 150 ug/Kg 10/07/22 13:44 10/10/22 19:31 40☼15000Xylenes, Total
4-Bromofluorobenzene (Surr)93 65-130 10/07/22 13:44 10/10/22 19:31 40
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr) 107 10/07/22 13:44 10/10/22 19:31 4065-130
1,2-Dichloroethane-d4 (Surr) 106 10/07/22 13:44 10/10/22 19:31 4065-130
Toluene-d8 (Surr)93 10/07/22 13:44 10/10/22 19:31 4065-130
1,2-Dichloroethane-d4 (Surr) 106 10/07/22 13:44 10/10/22 19:31 4065-130
Dibromofluoromethane (Surr) 107 10/07/22 13:44 10/10/22 19:31 4065-130
4-Bromofluorobenzene (Surr) 93 10/07/22 13:44 10/10/22 19:31 4065-130
Toluene-d8 (Surr)93 10/07/22 13:44 10/10/22 19:31 4065-130
Method: SW846 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
21000 1000 510 ug/Kg ☼10/07/22 13:44 10/11/22 14:43 200
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,2,4-Trimethylbenzene
1000 510 ug/Kg 10/07/22 13:44 10/11/22 14:43 200☼210001,2,4-Trimethylbenzene
4-Bromofluorobenzene (Surr)100 65-130 10/07/22 13:44 10/11/22 14:43 200
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr) 108 10/07/22 13:44 10/11/22 14:43 20065-130
1,2-Dichloroethane-d4 (Surr) 112 10/07/22 13:44 10/11/22 14:43 20065-130
Toluene-d8 (Surr)99 10/07/22 13:44 10/11/22 14:43 20065-130
1,2-Dichloroethane-d4 (Surr) 112 10/07/22 13:44 10/11/22 14:43 20065-130
Dibromofluoromethane (Surr) 108 10/07/22 13:44 10/11/22 14:43 20065-130
4-Bromofluorobenzene (Surr) 100 10/07/22 13:44 10/11/22 14:43 20065-130
Toluene-d8 (Surr)99 10/07/22 13:44 10/11/22 14:43 20065-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
<33 350 33 ug/Kg ☼10/11/22 19:45 10/13/22 02:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,2,4-Trichlorobenzene
350 39 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<391,2-Dichlorobenzene
350 36 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<361,3-Dichlorobenzene
350 37 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<371,4-Dichlorobenzene
350 33 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼29001-Methylnaphthalene
350 37 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<372,4,5-Trichlorophenol
350 31 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<312,4,6-Trichlorophenol
350 37 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<372,4-Dichlorophenol
350 47 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<472,4-Dimethylphenol
1800 880 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<8802,4-Dinitrophenol
350 52 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<522,4-Dinitrotoluene
350 45 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<452,6-Dinitrotoluene
350 37 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<372-Chloronaphthalene
350 42 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<422-Chlorophenol
350 40 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼9702-Methylnaphthalene
350 29 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<292-Methylphenol
1800 48 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<482-Nitroaniline
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
<44 350 44 ug/Kg ☼10/11/22 19:45 10/13/22 02:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2-Nitrophenol
350 46 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<463 & 4 Methylphenol
700 30 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<303,3'-Dichlorobenzidine
1800 49 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<493-Nitroaniline
1800 180 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<1804,6-Dinitro-2-methylphenol
350 38 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<384-Bromophenyl phenyl ether
350 37 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<374-Chloro-3-methylphenol
700 55 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<554-Chloroaniline
350 47 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<474-Chlorophenyl phenyl ether
1800 52 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<524-Nitroaniline
1800 350 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<3504-Nitrophenol
350 44 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<44Acenaphthene
350 38 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<38Acenaphthylene
350 27 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼38 JAnthracene
2900 880 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<880Benzidine
350 29 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<29Benzo[a]anthracene
350 55 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<55Benzo[a]pyrene
350 40 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<40Benzo[b]fluoranthene
350 23 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<23Benzo[g,h,i]perylene
350 69 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<69Benzo[k]fluoranthene
1800 880 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<880Benzoic acid
350 35 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<35Benzyl alcohol
350 32 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<32bis (2-chloroisopropyl) ether
350 41 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<41Bis(2-chloroethoxy)methane
350 48 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<48Bis(2-chloroethyl)ether
350 31 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<31Bis(2-ethylhexyl) phthalate
350 28 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<28Butyl benzyl phthalate
350 22 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<22Chrysene
350 41 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<41Dibenz(a,h)anthracene
350 35 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<35Dibenzofuran
350 39 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<39Diethyl phthalate
350 36 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<36Dimethyl phthalate
350 32 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<32Di-n-butyl phthalate
350 31 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<31Di-n-octyl phthalate
350 34 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<34Fluoranthene
350 38 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼54 JFluorene
350 41 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<41Hexachlorobenzene
350 38 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<38Hexachlorobutadiene
350 44 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<44Hexachlorocyclopentadiene
350 30 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<30Hexachloroethane
350 30 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<30Indeno[1,2,3-cd]pyrene
350 35 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<35Isophorone
350 32 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼320 JNaphthalene
350 28 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<28Nitrobenzene
350 130 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<130N-Nitrosodimethylamine
350 34 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<34N-Nitrosodi-n-propylamine
350 35 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<35N-Nitrosodiphenylamine
1800 350 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<350Pentachlorophenol
350 29 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼130 JPhenanthrene
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Client Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Lab Sample ID: 680-222306-1Client Sample ID: SS-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
<36 350 36 ug/Kg ☼10/11/22 19:45 10/13/22 02:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Phenol
350 29 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<29Pyrene
700 350 ug/Kg 10/11/22 19:45 10/13/22 02:52 1☼<350Pyridine
2,4,6-Tribromophenol (Surr)65 21-132 10/11/22 19:45 10/13/22 02:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl (Surr) 54 10/11/22 19:45 10/13/22 02:52 125-130
2-Fluorophenol (Surr) 58 10/11/22 19:45 10/13/22 02:52 118-130
Nitrobenzene-d5 (Surr) 53 10/11/22 19:45 10/13/22 02:52 119-130
Phenol-d5 (Surr)54 10/11/22 19:45 10/13/22 02:52 121-130
Terphenyl-d14 (Surr)60 10/11/22 19:45 10/13/22 02:52 131-133
Method: SW846 6010D - Metals (ICP) - TCLP
RL MDL
<0.20 0.20 0.20 mg/L 10/17/22 05:34 10/17/22 21:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Arsenic
1.0 1.0 mg/L 10/17/22 05:34 10/17/22 21:30 1<1.0Barium
0.10 0.10 mg/L 10/17/22 05:34 10/17/22 21:30 1<0.10Cadmium
0.20 0.20 mg/L 10/17/22 05:34 10/17/22 21:30 1<0.20Chromium
0.20 0.20 mg/L 10/17/22 05:34 10/17/22 21:30 1<0.20Lead
0.50 0.50 mg/L 10/17/22 05:34 10/17/22 21:30 1<0.50Selenium
0.10 0.10 mg/L 10/17/22 05:34 10/17/22 21:30 1<0.10Silver
Method: SW846 7470A - Mercury (CVAA) - TCLP
RL MDL
<0.020 0.020 0.020 mg/L 10/17/22 08:57 10/17/22 15:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Mercury
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-744365/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
RL MDL
Acetone <11 50 11 ug/Kg 10/10/22 12:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<41 4150 ug/Kg 10/10/22 12:44 1Acetonitrile
<74 74100 ug/Kg 10/10/22 12:44 1Acrolein
<30 30100 ug/Kg 10/10/22 12:44 1Acrylonitrile
<2.4 2.45.0 ug/Kg 10/10/22 12:44 1Benzene
<1.7 1.75.0 ug/Kg 10/10/22 12:44 1Bromobenzene
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Bromochloromethane
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1Bromoform
<2.4 2.45.0 ug/Kg 10/10/22 12:44 1Bromomethane
<9.2 9.225 ug/Kg 10/10/22 12:44 12-Butanone (MEK)
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Carbon disulfide
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Carbon tetrachloride
<1.4 1.45.0 ug/Kg 10/10/22 12:44 1Chlorobenzene
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1Chloroethane
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Chloroform
<2.4 2.45.0 ug/Kg 10/10/22 12:44 1Chloromethane
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Chloroprene
<3.5 3.55.0 ug/Kg 10/10/22 12:44 13-Chloropropene
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Chlorodibromomethane
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Dibromochloromethane
<2.3 2.35.0 ug/Kg 10/10/22 12:44 12-Chlorotoluene
<2.1 2.15.0 ug/Kg 10/10/22 12:44 14-Chlorotoluene
<2.3 2.35.0 ug/Kg 10/10/22 12:44 1Cyclohexane
<1.6 1.610 ug/Kg 10/10/22 12:44 11,2-Dibromo-3-Chloropropane
<1.7 1.75.0 ug/Kg 10/10/22 12:44 11,2-Dibromoethane
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Dibromomethane
<1.7 1.75.0 ug/Kg 10/10/22 12:44 11,2-Dichlorobenzene
<2.9 2.95.0 ug/Kg 10/10/22 12:44 1cis-1,2-Dichloroethene
<2.0 2.05.0 ug/Kg 10/10/22 12:44 11,3-Dichlorobenzene
<1.8 1.85.0 ug/Kg 10/10/22 12:44 11,4-Dichlorobenzene
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Bromodichloromethane
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Dichlorobromomethane
<3.2 3.25.0 ug/Kg 10/10/22 12:44 1Dichlorodifluoromethane
<2.9 2.95.0 ug/Kg 10/10/22 12:44 11,1-Dichloroethane
<2.3 2.35.0 ug/Kg 10/10/22 12:44 11,2-Dichloroethane
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1cis-1,3-Dichloropropene
<3.6 3.65.0 ug/Kg 10/10/22 12:44 11,1-Dichloroethene
<2.6 2.65.0 ug/Kg 10/10/22 12:44 11,2-Dichloropropane
<2.2 2.25.0 ug/Kg 10/10/22 12:44 11,3-Dichloropropane
<2.2 2.25.0 ug/Kg 10/10/22 12:44 12,2-Dichloropropane
<2.0 2.05.0 ug/Kg 10/10/22 12:44 11,1-Dichloropropene
<46 46100 ug/Kg 10/10/22 12:44 11,4-Dioxane
<250 250250 ug/Kg 10/10/22 12:44 1Ethanol
<2.1 2.15.0 ug/Kg 10/10/22 12:44 1Ethylbenzene
<2.8 2.85.0 ug/Kg 10/10/22 12:44 1Ethyl methacrylate
<2.9 2.95.0 ug/Kg 10/10/22 12:44 1Freon 113
<4.1 4.15.0 ug/Kg 10/10/22 12:44 1Hexachlorobutadiene
<19 1925 ug/Kg 10/10/22 12:44 12-Hexanone
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-744365/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
RL MDL
Iodomethane <1.7 5.0 1.7 ug/Kg 10/10/22 12:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<93 93250 ug/Kg 10/10/22 12:44 1Isobutyl alcohol
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1Isopropylbenzene
<1.5 1.510 ug/Kg 10/10/22 12:44 1Isopropyl ether
<2.6 2.65.0 ug/Kg 10/10/22 12:44 14-Isopropyltoluene
<23 2350 ug/Kg 10/10/22 12:44 1Methacrylonitrile
<8.1 8.125 ug/Kg 10/10/22 12:44 1Methyl acetate
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1Methylcyclohexane
<8.0 8.010 ug/Kg 10/10/22 12:44 1Methylene Chloride
<4.5 4.510 ug/Kg 10/10/22 12:44 1Methyl methacrylate
<18 1825 ug/Kg 10/10/22 12:44 14-Methyl-2-pentanone (MIBK)
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1Methyl tert-butyl ether
<3.1 3.15.0 ug/Kg 10/10/22 12:44 1Naphthalene
<1.9 1.95.0 ug/Kg 10/10/22 12:44 1n-Butylbenzene
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1m-Xylene & p-Xylene
<2.2 2.25.0 ug/Kg 10/10/22 12:44 1N-Propylbenzene
<2.3 2.35.0 ug/Kg 10/10/22 12:44 1o-Xylene
<6.3 6.310 ug/Kg 10/10/22 12:44 1Pentachloroethane
<26 2650 ug/Kg 10/10/22 12:44 1Propionitrile
<2.0 2.05.0 ug/Kg 10/10/22 12:44 1sec-Butylbenzene
<1.9 1.95.0 ug/Kg 10/10/22 12:44 1Styrene
<2.5 2.55.0 ug/Kg 10/10/22 12:44 1tert-Butylbenzene
<1.3 1.35.0 ug/Kg 10/10/22 12:44 11,1,1,2-Tetrachloroethane
<2.1 2.15.0 ug/Kg 10/10/22 12:44 11,1,2,2-Tetrachloroethane
<2.6 2.65.0 ug/Kg 10/10/22 12:44 1Tetrachloroethene
<6.2 6.210 ug/Kg 10/10/22 12:44 1Tetrahydrofuran
<2.6 2.65.0 ug/Kg 10/10/22 12:44 1Toluene
<2.4 2.410 ug/Kg 10/10/22 12:44 1trans-1,4-Dichloro-2-butene
<2.3 2.35.0 ug/Kg 10/10/22 12:44 1trans-1,2-Dichloroethene
<2.6 2.65.0 ug/Kg 10/10/22 12:44 1trans-1,3-Dichloropropene
<2.0 2.05.0 ug/Kg 10/10/22 12:44 11,2,3-Trichlorobenzene
<2.5 2.55.0 ug/Kg 10/10/22 12:44 11,2,4-Trichlorobenzene
<2.6 2.65.0 ug/Kg 10/10/22 12:44 11,1,1-Trichloroethane
<1.5 1.55.0 ug/Kg 10/10/22 12:44 11,1,2-Trichloroethane
<1.8 1.85.0 ug/Kg 10/10/22 12:44 1Trichloroethene
<3.1 3.15.0 ug/Kg 10/10/22 12:44 1Trichlorofluoromethane
<1.8 1.85.0 ug/Kg 10/10/22 12:44 11,2,3-Trichloropropane
<2.5 2.55.0 ug/Kg 10/10/22 12:44 11,2,4-Trimethylbenzene
<2.4 2.45.0 ug/Kg 10/10/22 12:44 11,3,5-Trimethylbenzene
<5.5 5.510 ug/Kg 10/10/22 12:44 1Vinyl acetate
<2.8 2.85.0 ug/Kg 10/10/22 12:44 1Vinyl chloride
<3.6 3.610 ug/Kg 10/10/22 12:44 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)113 65 -130 10/10/22 12:44 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
109 10/10/22 12:44 1Dibromofluoromethane (Surr)65 -130
95 10/10/22 12:44 14-Bromofluorobenzene (Surr)65 -130
91 10/10/22 12:44 1Toluene-d8 (Surr)65 -130
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744365/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
Acetone 250 255 ug/Kg 102 10 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acrolein 1000 950 ug/Kg 95 27 -150
Acrylonitrile 500 524 ug/Kg 105 50 -150
Benzene 50.0 50.4 ug/Kg 101 70 -130
Bromobenzene 50.0 50.5 ug/Kg 101 70 -130
Bromochloromethane 50.0 53.9 ug/Kg 108 66 -130
Bromoform 50.0 51.1 ug/Kg 102 68 -130
Bromomethane 50.0 56.1 ug/Kg 112 70 -130
2-Butanone (MEK)250 277 ug/Kg 111 40 -150
Carbon disulfide 50.0 52.4 ug/Kg 105 70 -130
Carbon tetrachloride 50.0 52.6 ug/Kg 105 70 -130
Chlorobenzene 50.0 51.8 ug/Kg 104 70 -130
Chloroethane 50.0 57.7 ug/Kg 115 70 -130
Chloroform 50.0 51.1 ug/Kg 102 70 -130
Chloromethane 50.0 59.9 ug/Kg 120 70 -130
3-Chloropropene 50.0 52.8 ug/Kg 106 66 -134
Chlorodibromomethane 50.0 53.4 ug/Kg 107 64 -133
Dibromochloromethane 50.0 53.4 ug/Kg 107 64 -133
2-Chlorotoluene 50.0 50.2 ug/Kg 100 70 -130
4-Chlorotoluene 50.0 48.9 ug/Kg 98 70 -130
Cyclohexane 50.0 49.5 ug/Kg 99 70 -130
1,2-Dibromo-3-Chloropropane 50.0 51.4 ug/Kg 103 42 -145
1,2-Dibromoethane 50.0 52.7 ug/Kg 105 48 -150
Dibromomethane 50.0 53.9 ug/Kg 108 59 -142
1,2-Dichlorobenzene 50.0 52.1 ug/Kg 104 70 -130
cis-1,2-Dichloroethene 50.0 51.9 ug/Kg 104 70 -130
1,3-Dichlorobenzene 50.0 51.8 ug/Kg 104 70 -130
1,4-Dichlorobenzene 50.0 51.1 ug/Kg 102 70 -130
Bromodichloromethane 50.0 50.9 ug/Kg 102 70 -130
Dichlorobromomethane 50.0 50.9 ug/Kg 102 70 -130
Dichlorodifluoromethane 50.0 66.8 *+ ug/Kg 134 43 -131
1,1-Dichloroethane 50.0 51.9 ug/Kg 104 70 -130
1,2-Dichloroethane 50.0 55.0 ug/Kg 110 68 -139
cis-1,3-Dichloropropene 50.0 50.8 ug/Kg 102 70 -130
1,1-Dichloroethene 50.0 52.4 ug/Kg 105 69-130
1,2-Dichloropropane 50.0 50.9 ug/Kg 102 70-130
1,3-Dichloropropane 50.0 51.8 ug/Kg 104 54-150
2,2-Dichloropropane 50.0 51.2 ug/Kg 102 70-130
1,1-Dichloropropene 50.0 50.5 ug/Kg 101 70-130
1,4-Dioxane 1000 1000 ug/Kg 100 35-150
Ethylbenzene 50.0 51.3 ug/Kg 103 70-130
Ethyl methacrylate 50.0 48.9 ug/Kg 98 40-150
Freon 113 50.0 53.5 ug/Kg 107 70-130
Hexachlorobutadiene 50.0 49.8 ug/Kg 100 70-130
2-Hexanone 250 262 ug/Kg 105 30-150
Iodomethane 50.0 58.6 ug/Kg 117 65-138
Isobutyl alcohol 1250 1190 ug/Kg 95 14-150
Isopropylbenzene 50.0 50.8 ug/Kg 102 70-130
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744365/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
4-Isopropyltoluene 50.0 51.3 ug/Kg 103 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Methyl acetate 100 120 ug/Kg 120 22 -150
Methylcyclohexane 50.0 48.5 ug/Kg 97 69 -110
Methylene Chloride 50.0 52.5 ug/Kg 105 54 -149
4-Methyl-2-pentanone (MIBK)250 267 ug/Kg 107 34 -150
Methyl tert-butyl ether 50.0 54.0 ug/Kg 108 70 -130
Naphthalene 50.0 49.4 ug/Kg 99 46 -150
n-Butylbenzene 50.0 52.5 ug/Kg 105 70 -130
m-Xylene & p-Xylene 50.0 50.5 ug/Kg 101 70 -130
N-Propylbenzene 50.0 51.3 ug/Kg 103 70 -130
o-Xylene 50.0 50.4 ug/Kg 101 70 -130
sec-Butylbenzene 50.0 50.7 ug/Kg 101 69 -142
Styrene 50.0 50.5 ug/Kg 101 70 -130
tert-Butylbenzene 50.0 50.0 ug/Kg 100 67 -145
1,1,1,2-Tetrachloroethane 50.0 51.9 ug/Kg 104 70 -130
1,1,2,2-Tetrachloroethane 50.0 50.7 ug/Kg 101 64 -130
Tetrachloroethene 50.0 50.3 ug/Kg 101 70 -130
Tetrahydrofuran 100 103 ug/Kg 103 15 -150
Toluene 50.0 50.4 ug/Kg 101 70 -130
trans-1,4-Dichloro-2-butene 50.0 54.6 ug/Kg 109 54 -150
trans-1,2-Dichloroethene 50.0 51.8 ug/Kg 104 67 -130
trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 54 -150
1,2,3-Trichlorobenzene 50.0 50.6 ug/Kg 101 70 -130
1,2,4-Trichlorobenzene 50.0 49.9 ug/Kg 100 70 -130
1,1,1-Trichloroethane 50.0 50.7 ug/Kg 101 70 -130
1,1,2-Trichloroethane 50.0 49.0 ug/Kg 98 56 -146
Trichloroethene 50.0 49.8 ug/Kg 100 70 -130
Trichlorofluoromethane 50.0 58.3 ug/Kg 117 70 -130
1,2,3-Trichloropropane 50.0 50.7 ug/Kg 101 64 -130
1,2,4-Trimethylbenzene 50.0 49.7 ug/Kg 99 70 -130
1,3,5-Trimethylbenzene 50.0 49.7 ug/Kg 99 70 -130
Vinyl acetate 100 117 ug/Kg 117 53 -150
Vinyl chloride 50.0 50.6 ug/Kg 101 70 -130
Xylenes, Total 100 101 ug/Kg 101 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
108
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)65 -130
1024-Bromofluorobenzene (Surr)65 -130
104Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744365/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
Acetone 250 276 ug/Kg 110 10 -150 8 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Acrolein 1000 1020 ug/Kg 102 27 -150 7 30
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Page 16 of 43 10/19/2022
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744365/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
Acrylonitrile 500 550 ug/Kg 110 50 -150 5 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 50.1 ug/Kg 100 70 -130 1 30
Bromobenzene 50.0 49.9 ug/Kg 100 70 -130 1 30
Bromochloromethane 50.0 54.1 ug/Kg 108 66 -130 0 30
Bromoform 50.0 50.1 ug/Kg 100 68 -130 2 30
Bromomethane 50.0 57.8 ug/Kg 116 70 -130 3 30
2-Butanone (MEK)250 286 ug/Kg 114 40 -150 3 30
Carbon disulfide 50.0 52.5 ug/Kg 105 70 -130 0 30
Carbon tetrachloride 50.0 51.7 ug/Kg 103 70 -130 2 30
Chlorobenzene 50.0 51.0 ug/Kg 102 70 -130 2 30
Chloroethane 50.0 57.4 ug/Kg 115 70 -130 0 30
Chloroform 50.0 50.4 ug/Kg 101 70 -130 1 30
Chloromethane 50.0 61.1 ug/Kg 122 70 -130 2 30
3-Chloropropene 50.0 53.0 ug/Kg 106 66 -134 1 30
Chlorodibromomethane 50.0 53.2 ug/Kg 106 64 -133 0 30
Dibromochloromethane 50.0 53.2 ug/Kg 106 64 -133 0 30
2-Chlorotoluene 50.0 49.1 ug/Kg 98 70 -130 2 30
4-Chlorotoluene 50.0 47.8 ug/Kg 96 70 -130 2 30
Cyclohexane 50.0 49.1 ug/Kg 98 70 -130 1 30
1,2-Dibromo-3-Chloropropane 50.0 50.0 ug/Kg 100 42 -145 3 30
1,2-Dibromoethane 50.0 52.9 ug/Kg 106 48 -150 0 30
Dibromomethane 50.0 53.7 ug/Kg 107 59 -142 0 30
1,2-Dichlorobenzene 50.0 50.7 ug/Kg 101 70 -130 3 30
cis-1,2-Dichloroethene 50.0 51.8 ug/Kg 104 70 -130 0 30
1,3-Dichlorobenzene 50.0 50.8 ug/Kg 102 70 -130 2 30
1,4-Dichlorobenzene 50.0 50.6 ug/Kg 101 70 -130 1 30
Bromodichloromethane 50.0 50.6 ug/Kg 101 70 -130 1 30
Dichlorobromomethane 50.0 50.6 ug/Kg 101 70-130 1 30
Dichlorodifluoromethane 50.0 67.9 *+ ug/Kg 136 43-131 2 30
1,1-Dichloroethane 50.0 50.8 ug/Kg 102 70-130 2 30
1,2-Dichloroethane 50.0 55.8 ug/Kg 112 68-139 2 30
cis-1,3-Dichloropropene 50.0 50.7 ug/Kg 101 70-130 0 30
1,1-Dichloroethene 50.0 51.2 ug/Kg 102 69-130 2 50
1,2-Dichloropropane 50.0 50.4 ug/Kg 101 70-130 1 30
1,3-Dichloropropane 50.0 51.7 ug/Kg 103 54-150 0 30
2,2-Dichloropropane 50.0 50.1 ug/Kg 100 70-130 2 30
1,1-Dichloropropene 50.0 50.7 ug/Kg 101 70-130 0 30
1,4-Dioxane 1000 1020 ug/Kg 102 35-150 1 30
Ethylbenzene 50.0 50.9 ug/Kg 102 70-130 1 30
Ethyl methacrylate 50.0 52.4 ug/Kg 105 40-150 7 30
Freon 113 50.0 52.0 ug/Kg 104 70-130 3 40
Hexachlorobutadiene 50.0 48.0 ug/Kg 96 70-130 4 30
2-Hexanone 250 278 ug/Kg 111 30-150 6 30
Iodomethane 50.0 56.2 ug/Kg 112 65-138 4 30
Isobutyl alcohol 1250 1280 ug/Kg 103 14-150 8 30
Isopropylbenzene 50.0 50.1 ug/Kg 100 70-130 2 30
4-Isopropyltoluene 50.0 50.1 ug/Kg 100 70-130 2 30
Methyl acetate 100 131 ug/Kg 131 22-150 9 30
Methylcyclohexane 50.0 48.5 ug/Kg 97 69-110 0 30
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744365/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744365
Methylene Chloride 50.0 53.1 ug/Kg 106 54 -149 1 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Methyl-2-pentanone (MIBK)250 282 ug/Kg 113 34 -150 5 30
Methyl tert-butyl ether 50.0 57.2 ug/Kg 114 70 -130 6 30
Naphthalene 50.0 48.7 ug/Kg 97 46 -150 1 30
n-Butylbenzene 50.0 50.1 ug/Kg 100 70 -130 5 30
m-Xylene & p-Xylene 50.0 49.9 ug/Kg 100 70 -130 1 30
N-Propylbenzene 50.0 50.7 ug/Kg 101 70 -130 1 30
o-Xylene 50.0 50.3 ug/Kg 101 70 -130 0 30
sec-Butylbenzene 50.0 49.4 ug/Kg 99 69 -142 3 30
Styrene 50.0 49.5 ug/Kg 99 70 -130 2 30
tert-Butylbenzene 50.0 49.0 ug/Kg 98 67 -145 2 30
1,1,1,2-Tetrachloroethane 50.0 50.7 ug/Kg 101 70 -130 2 30
1,1,2,2-Tetrachloroethane 50.0 50.2 ug/Kg 100 64 -130 1 30
Tetrachloroethene 50.0 50.2 ug/Kg 100 70 -130 0 30
Tetrahydrofuran 100 109 ug/Kg 109 15 -150 5 30
Toluene 50.0 50.8 ug/Kg 102 70 -130 1 30
trans-1,4-Dichloro-2-butene 50.0 54.4 ug/Kg 109 54 -150 0 30
trans-1,2-Dichloroethene 50.0 50.9 ug/Kg 102 67 -130 2 30
trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 54 -150 0 30
1,2,3-Trichlorobenzene 50.0 49.6 ug/Kg 99 70 -130 2 30
1,2,4-Trichlorobenzene 50.0 49.1 ug/Kg 98 70 -130 2 30
1,1,1-Trichloroethane 50.0 50.2 ug/Kg 100 70 -130 1 30
1,1,2-Trichloroethane 50.0 49.5 ug/Kg 99 56 -146 1 30
Trichloroethene 50.0 49.3 ug/Kg 99 70 -130 1 30
Trichlorofluoromethane 50.0 58.4 ug/Kg 117 70 -130 0 30
1,2,3-Trichloropropane 50.0 49.1 ug/Kg 98 64 -130 3 30
1,2,4-Trimethylbenzene 50.0 48.8 ug/Kg 98 70 -130 2 30
1,3,5-Trimethylbenzene 50.0 48.8 ug/Kg 98 70 -130 2 30
Vinyl acetate 100 124 ug/Kg 124 53-150 6 30
Vinyl chloride 50.0 51.4 ug/Kg 103 70-130 2 30
Xylenes, Total 100 100 ug/Kg 100 70-130 1 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
109
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)65 -130
1004-Bromofluorobenzene (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-744553/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
RL MDL
Acetone <11 50 11 ug/Kg 10/11/22 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<41 4150 ug/Kg 10/11/22 13:08 1Acetonitrile
<74 74100 ug/Kg 10/11/22 13:08 1Acrolein
<30 30100 ug/Kg 10/11/22 13:08 1Acrylonitrile
<2.4 2.45.0 ug/Kg 10/11/22 13:08 1Benzene
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-744553/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
RL MDL
Bromobenzene <1.7 5.0 1.7 ug/Kg 10/11/22 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Bromochloromethane
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1Bromoform
<2.4 2.45.0 ug/Kg 10/11/22 13:08 1Bromomethane
<9.2 9.225 ug/Kg 10/11/22 13:08 12-Butanone (MEK)
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Carbon disulfide
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Carbon tetrachloride
<1.4 1.45.0 ug/Kg 10/11/22 13:08 1Chlorobenzene
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1Chloroethane
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Chloroform
<2.4 2.45.0 ug/Kg 10/11/22 13:08 1Chloromethane
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Chloroprene
<3.5 3.55.0 ug/Kg 10/11/22 13:08 13-Chloropropene
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Chlorodibromomethane
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Dibromochloromethane
<2.3 2.35.0 ug/Kg 10/11/22 13:08 12-Chlorotoluene
<2.1 2.15.0 ug/Kg 10/11/22 13:08 14-Chlorotoluene
<2.3 2.35.0 ug/Kg 10/11/22 13:08 1Cyclohexane
<1.6 1.610 ug/Kg 10/11/22 13:08 11,2-Dibromo-3-Chloropropane
<1.7 1.75.0 ug/Kg 10/11/22 13:08 11,2-Dibromoethane
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Dibromomethane
<1.7 1.75.0 ug/Kg 10/11/22 13:08 11,2-Dichlorobenzene
<2.9 2.95.0 ug/Kg 10/11/22 13:08 1cis-1,2-Dichloroethene
<2.0 2.05.0 ug/Kg 10/11/22 13:08 11,3-Dichlorobenzene
<1.8 1.85.0 ug/Kg 10/11/22 13:08 11,4-Dichlorobenzene
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Bromodichloromethane
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Dichlorobromomethane
<3.2 3.25.0 ug/Kg 10/11/22 13:08 1Dichlorodifluoromethane
<2.9 2.95.0 ug/Kg 10/11/22 13:08 11,1-Dichloroethane
<2.3 2.35.0 ug/Kg 10/11/22 13:08 11,2-Dichloroethane
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1cis-1,3-Dichloropropene
<3.6 3.65.0 ug/Kg 10/11/22 13:08 11,1-Dichloroethene
<2.6 2.65.0 ug/Kg 10/11/22 13:08 11,2-Dichloropropane
<2.2 2.25.0 ug/Kg 10/11/22 13:08 11,3-Dichloropropane
<2.2 2.25.0 ug/Kg 10/11/22 13:08 12,2-Dichloropropane
<2.0 2.05.0 ug/Kg 10/11/22 13:08 11,1-Dichloropropene
<46 46100 ug/Kg 10/11/22 13:08 11,4-Dioxane
<250 250250 ug/Kg 10/11/22 13:08 1Ethanol
<2.1 2.15.0 ug/Kg 10/11/22 13:08 1Ethylbenzene
<2.8 2.85.0 ug/Kg 10/11/22 13:08 1Ethyl methacrylate
<2.9 2.95.0 ug/Kg 10/11/22 13:08 1Freon 113
<4.1 4.15.0 ug/Kg 10/11/22 13:08 1Hexachlorobutadiene
<19 1925 ug/Kg 10/11/22 13:08 12-Hexanone
<1.7 1.75.0 ug/Kg 10/11/22 13:08 1Iodomethane
<93 93250 ug/Kg 10/11/22 13:08 1Isobutyl alcohol
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1Isopropylbenzene
<1.5 1.510 ug/Kg 10/11/22 13:08 1Isopropyl ether
<2.6 2.65.0 ug/Kg 10/11/22 13:08 14-Isopropyltoluene
<23 2350 ug/Kg 10/11/22 13:08 1Methacrylonitrile
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-744553/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
RL MDL
Methyl acetate <8.1 25 8.1 ug/Kg 10/11/22 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1Methylcyclohexane
<8.0 8.010 ug/Kg 10/11/22 13:08 1Methylene Chloride
<4.5 4.510 ug/Kg 10/11/22 13:08 1Methyl methacrylate
<18 1825 ug/Kg 10/11/22 13:08 14-Methyl-2-pentanone (MIBK)
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1Methyl tert-butyl ether
<3.1 3.15.0 ug/Kg 10/11/22 13:08 1Naphthalene
<1.9 1.95.0 ug/Kg 10/11/22 13:08 1n-Butylbenzene
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1m-Xylene & p-Xylene
<2.2 2.25.0 ug/Kg 10/11/22 13:08 1N-Propylbenzene
<2.3 2.35.0 ug/Kg 10/11/22 13:08 1o-Xylene
<6.3 6.310 ug/Kg 10/11/22 13:08 1Pentachloroethane
<26 2650 ug/Kg 10/11/22 13:08 1Propionitrile
<2.0 2.05.0 ug/Kg 10/11/22 13:08 1sec-Butylbenzene
<1.9 1.95.0 ug/Kg 10/11/22 13:08 1Styrene
<2.5 2.55.0 ug/Kg 10/11/22 13:08 1tert-Butylbenzene
<1.3 1.35.0 ug/Kg 10/11/22 13:08 11,1,1,2-Tetrachloroethane
<2.1 2.15.0 ug/Kg 10/11/22 13:08 11,1,2,2-Tetrachloroethane
<2.6 2.65.0 ug/Kg 10/11/22 13:08 1Tetrachloroethene
<6.2 6.210 ug/Kg 10/11/22 13:08 1Tetrahydrofuran
<2.6 2.65.0 ug/Kg 10/11/22 13:08 1Toluene
<2.4 2.410 ug/Kg 10/11/22 13:08 1trans-1,4-Dichloro-2-butene
<2.3 2.35.0 ug/Kg 10/11/22 13:08 1trans-1,2-Dichloroethene
<2.6 2.65.0 ug/Kg 10/11/22 13:08 1trans-1,3-Dichloropropene
<2.0 2.05.0 ug/Kg 10/11/22 13:08 11,2,3-Trichlorobenzene
<2.5 2.55.0 ug/Kg 10/11/22 13:08 11,2,4-Trichlorobenzene
<2.6 2.65.0 ug/Kg 10/11/22 13:08 11,1,1-Trichloroethane
<1.5 1.55.0 ug/Kg 10/11/22 13:08 11,1,2-Trichloroethane
<1.8 1.85.0 ug/Kg 10/11/22 13:08 1Trichloroethene
<3.1 3.15.0 ug/Kg 10/11/22 13:08 1Trichlorofluoromethane
<1.8 1.85.0 ug/Kg 10/11/22 13:08 11,2,3-Trichloropropane
<2.5 2.55.0 ug/Kg 10/11/22 13:08 11,2,4-Trimethylbenzene
<2.4 2.45.0 ug/Kg 10/11/22 13:08 11,3,5-Trimethylbenzene
<5.5 5.510 ug/Kg 10/11/22 13:08 1Vinyl acetate
<2.8 2.85.0 ug/Kg 10/11/22 13:08 1Vinyl chloride
<3.6 3.610 ug/Kg 10/11/22 13:08 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)113 65 -130 10/11/22 13:08 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
108 10/11/22 13:08 1Dibromofluoromethane (Surr)65 -130
95 10/11/22 13:08 14-Bromofluorobenzene (Surr)65 -130
98 10/11/22 13:08 1Toluene-d8 (Surr)65 -130
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744553/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
Acetone 250 281 ug/Kg 113 10 -150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Acrolein 1000 1100 ug/Kg 110 27 -150
Acrylonitrile 500 558 ug/Kg 112 50 -150
Benzene 50.0 50.1 ug/Kg 100 70 -130
Bromobenzene 50.0 50.6 ug/Kg 101 70 -130
Bromochloromethane 50.0 55.2 ug/Kg 110 66 -130
Bromoform 50.0 51.6 ug/Kg 103 68 -130
Bromomethane 50.0 53.6 ug/Kg 107 70 -130
2-Butanone (MEK)250 280 ug/Kg 112 40 -150
Carbon disulfide 50.0 51.5 ug/Kg 103 70 -130
Carbon tetrachloride 50.0 52.4 ug/Kg 105 70 -130
Chlorobenzene 50.0 51.1 ug/Kg 102 70 -130
Chloroethane 50.0 55.4 ug/Kg 111 70 -130
Chloroform 50.0 50.4 ug/Kg 101 70 -130
Chloromethane 50.0 59.4 ug/Kg 119 70 -130
3-Chloropropene 50.0 52.3 ug/Kg 105 66 -134
Chlorodibromomethane 50.0 54.1 ug/Kg 108 64 -133
Dibromochloromethane 50.0 54.1 ug/Kg 108 64 -133
2-Chlorotoluene 50.0 49.6 ug/Kg 99 70 -130
4-Chlorotoluene 50.0 53.9 ug/Kg 108 70 -130
Cyclohexane 50.0 48.4 ug/Kg 97 70 -130
1,2-Dibromo-3-Chloropropane 50.0 50.6 ug/Kg 101 42 -145
1,2-Dibromoethane 50.0 53.5 ug/Kg 107 48 -150
Dibromomethane 50.0 54.3 ug/Kg 109 59 -142
1,2-Dichlorobenzene 50.0 50.8 ug/Kg 102 70 -130
cis-1,2-Dichloroethene 50.0 52.6 ug/Kg 105 70 -130
1,3-Dichlorobenzene 50.0 50.9 ug/Kg 102 70 -130
1,4-Dichlorobenzene 50.0 50.4 ug/Kg 101 70 -130
Bromodichloromethane 50.0 51.7 ug/Kg 103 70 -130
Dichlorobromomethane 50.0 51.7 ug/Kg 103 70 -130
Dichlorodifluoromethane 50.0 67.2 *+ ug/Kg 134 43 -131
1,1-Dichloroethane 50.0 51.9 ug/Kg 104 70 -130
1,2-Dichloroethane 50.0 56.0 ug/Kg 112 68 -139
cis-1,3-Dichloropropene 50.0 53.1 ug/Kg 106 70 -130
1,1-Dichloroethene 50.0 50.3 ug/Kg 101 69-130
1,2-Dichloropropane 50.0 50.1 ug/Kg 100 70-130
1,3-Dichloropropane 50.0 52.3 ug/Kg 105 54-150
2,2-Dichloropropane 50.0 51.7 ug/Kg 103 70-130
1,1-Dichloropropene 50.0 51.0 ug/Kg 102 70-130
1,4-Dioxane 1000 969 ug/Kg 97 35-150
Ethylbenzene 50.0 51.5 ug/Kg 103 70-130
Ethyl methacrylate 50.0 53.3 ug/Kg 107 40-150
Freon 113 50.0 52.0 ug/Kg 104 70-130
Hexachlorobutadiene 50.0 47.5 ug/Kg 95 70-130
2-Hexanone 250 273 ug/Kg 109 30-150
Iodomethane 50.0 55.6 ug/Kg 111 65-138
Isobutyl alcohol 1250 1250 ug/Kg 100 14-150
Isopropylbenzene 50.0 49.8 ug/Kg 100 70-130
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744553/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
4-Isopropyltoluene 50.0 50.3 ug/Kg 101 70 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Methyl acetate 100 129 ug/Kg 129 22 -150
Methylcyclohexane 50.0 49.1 ug/Kg 98 69 -110
Methylene Chloride 50.0 53.2 ug/Kg 106 54 -149
4-Methyl-2-pentanone (MIBK)250 271 ug/Kg 109 34 -150
Methyl tert-butyl ether 50.0 57.4 ug/Kg 115 70 -130
Naphthalene 50.0 49.4 ug/Kg 99 46 -150
n-Butylbenzene 50.0 50.6 ug/Kg 101 70 -130
m-Xylene & p-Xylene 50.0 51.1 ug/Kg 102 70 -130
N-Propylbenzene 50.0 50.9 ug/Kg 102 70 -130
o-Xylene 50.0 51.0 ug/Kg 102 70 -130
sec-Butylbenzene 50.0 49.5 ug/Kg 99 69 -142
Styrene 50.0 50.2 ug/Kg 100 70 -130
tert-Butylbenzene 50.0 49.2 ug/Kg 98 67 -145
1,1,1,2-Tetrachloroethane 50.0 50.6 ug/Kg 101 70 -130
1,1,2,2-Tetrachloroethane 50.0 48.8 ug/Kg 98 64 -130
Tetrachloroethene 50.0 50.6 ug/Kg 101 70 -130
Tetrahydrofuran 100 109 ug/Kg 109 15 -150
Toluene 50.0 51.6 ug/Kg 103 70 -130
trans-1,4-Dichloro-2-butene 50.0 52.6 ug/Kg 105 54 -150
trans-1,2-Dichloroethene 50.0 52.9 ug/Kg 106 67 -130
trans-1,3-Dichloropropene 50.0 50.4 ug/Kg 101 54 -150
1,2,3-Trichlorobenzene 50.0 50.2 ug/Kg 100 70 -130
1,2,4-Trichlorobenzene 50.0 48.9 ug/Kg 98 70 -130
1,1,1-Trichloroethane 50.0 50.1 ug/Kg 100 70 -130
1,1,2-Trichloroethane 50.0 49.5 ug/Kg 99 56 -146
Trichloroethene 50.0 49.8 ug/Kg 100 70 -130
Trichlorofluoromethane 50.0 56.4 ug/Kg 113 70 -130
1,2,3-Trichloropropane 50.0 49.2 ug/Kg 98 64 -130
1,2,4-Trimethylbenzene 50.0 49.3 ug/Kg 99 70 -130
1,3,5-Trimethylbenzene 50.0 49.1 ug/Kg 98 70 -130
Vinyl acetate 100 126 ug/Kg 126 53 -150
Vinyl chloride 50.0 50.3 ug/Kg 101 70 -130
Xylenes, Total 100 102 ug/Kg 102 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
111
LCS LCS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)65 -130
994-Bromofluorobenzene (Surr)65 -130
101Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744553/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
Acetone 250 256 ug/Kg 103 10 -150 9 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Acrolein 1000 1020 ug/Kg 102 27 -150 8 30
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744553/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
Acrylonitrile 500 518 ug/Kg 104 50 -150 7 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Benzene 50.0 49.7 ug/Kg 99 70 -130 1 30
Bromobenzene 50.0 50.0 ug/Kg 100 70 -130 1 30
Bromochloromethane 50.0 53.5 ug/Kg 107 66 -130 3 30
Bromoform 50.0 50.6 ug/Kg 101 68 -130 2 30
Bromomethane 50.0 54.0 ug/Kg 108 70 -130 1 30
2-Butanone (MEK)250 265 ug/Kg 106 40 -150 5 30
Carbon disulfide 50.0 50.6 ug/Kg 101 70 -130 2 30
Carbon tetrachloride 50.0 52.5 ug/Kg 105 70 -130 0 30
Chlorobenzene 50.0 50.9 ug/Kg 102 70 -130 1 30
Chloroethane 50.0 53.9 ug/Kg 108 70 -130 3 30
Chloroform 50.0 51.3 ug/Kg 103 70 -130 2 30
Chloromethane 50.0 57.5 ug/Kg 115 70 -130 3 30
3-Chloropropene 50.0 51.5 ug/Kg 103 66 -134 2 30
Chlorodibromomethane 50.0 53.6 ug/Kg 107 64 -133 1 30
Dibromochloromethane 50.0 53.6 ug/Kg 107 64 -133 1 30
2-Chlorotoluene 50.0 49.3 ug/Kg 99 70 -130 1 30
4-Chlorotoluene 50.0 53.3 ug/Kg 107 70 -130 1 30
Cyclohexane 50.0 48.6 ug/Kg 97 70 -130 0 30
1,2-Dibromo-3-Chloropropane 50.0 50.6 ug/Kg 101 42 -145 0 30
1,2-Dibromoethane 50.0 52.1 ug/Kg 104 48 -150 3 30
Dibromomethane 50.0 53.8 ug/Kg 108 59 -142 1 30
1,2-Dichlorobenzene 50.0 49.4 ug/Kg 99 70 -130 3 30
cis-1,2-Dichloroethene 50.0 51.7 ug/Kg 103 70 -130 2 30
1,3-Dichlorobenzene 50.0 50.2 ug/Kg 100 70 -130 1 30
1,4-Dichlorobenzene 50.0 49.8 ug/Kg 100 70 -130 1 30
Bromodichloromethane 50.0 51.4 ug/Kg 103 70 -130 1 30
Dichlorobromomethane 50.0 51.4 ug/Kg 103 70-130 1 30
Dichlorodifluoromethane 50.0 64.3 ug/Kg 129 43-131 4 30
1,1-Dichloroethane 50.0 52.5 ug/Kg 105 70-130 1 30
1,2-Dichloroethane 50.0 56.1 ug/Kg 112 68-139 0 30
cis-1,3-Dichloropropene 50.0 52.4 ug/Kg 105 70-130 1 30
1,1-Dichloroethene 50.0 49.5 ug/Kg 99 69-130 2 50
1,2-Dichloropropane 50.0 50.1 ug/Kg 100 70-130 0 30
1,3-Dichloropropane 50.0 51.1 ug/Kg 102 54-150 2 30
2,2-Dichloropropane 50.0 52.1 ug/Kg 104 70-130 1 30
1,1-Dichloropropene 50.0 51.1 ug/Kg 102 70-130 0 30
1,4-Dioxane 1000 975 ug/Kg 98 35-150 1 30
Ethylbenzene 50.0 51.6 ug/Kg 103 70-130 0 30
Ethyl methacrylate 50.0 49.9 ug/Kg 100 40-150 6 30
Freon 113 50.0 52.5 ug/Kg 105 70-130 1 40
Hexachlorobutadiene 50.0 46.4 ug/Kg 93 70-130 2 30
2-Hexanone 250 257 ug/Kg 103 30-150 6 30
Iodomethane 50.0 56.5 ug/Kg 113 65-138 2 30
Isobutyl alcohol 1250 1190 ug/Kg 95 14-150 5 30
Isopropylbenzene 50.0 50.2 ug/Kg 100 70-130 1 30
4-Isopropyltoluene 50.0 49.4 ug/Kg 99 70-130 2 30
Methyl acetate 100 118 ug/Kg 118 22-150 8 30
Methylcyclohexane 50.0 48.7 ug/Kg 97 69-110 1 30
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-744553/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744553
Methylene Chloride 50.0 51.8 ug/Kg 104 54 -149 3 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Methyl-2-pentanone (MIBK)250 256 ug/Kg 102 34 -150 6 30
Methyl tert-butyl ether 50.0 55.3 ug/Kg 111 70 -130 4 30
Naphthalene 50.0 47.9 ug/Kg 96 46 -150 3 30
n-Butylbenzene 50.0 50.2 ug/Kg 100 70 -130 1 30
m-Xylene & p-Xylene 50.0 50.1 ug/Kg 100 70 -130 2 30
N-Propylbenzene 50.0 50.7 ug/Kg 101 70 -130 0 30
o-Xylene 50.0 51.0 ug/Kg 102 70 -130 0 30
sec-Butylbenzene 50.0 49.2 ug/Kg 98 69 -142 1 30
Styrene 50.0 49.8 ug/Kg 100 70 -130 1 30
tert-Butylbenzene 50.0 49.3 ug/Kg 99 67 -145 0 30
1,1,1,2-Tetrachloroethane 50.0 51.0 ug/Kg 102 70 -130 1 30
1,1,2,2-Tetrachloroethane 50.0 47.6 ug/Kg 95 64 -130 2 30
Tetrachloroethene 50.0 50.3 ug/Kg 101 70 -130 1 30
Tetrahydrofuran 100 103 ug/Kg 103 15 -150 5 30
Toluene 50.0 50.8 ug/Kg 102 70 -130 2 30
trans-1,4-Dichloro-2-butene 50.0 51.3 ug/Kg 103 54 -150 2 30
trans-1,2-Dichloroethene 50.0 51.9 ug/Kg 104 67 -130 2 30
trans-1,3-Dichloropropene 50.0 49.9 ug/Kg 100 54 -150 1 30
1,2,3-Trichlorobenzene 50.0 49.4 ug/Kg 99 70 -130 2 30
1,2,4-Trichlorobenzene 50.0 48.3 ug/Kg 97 70 -130 1 30
1,1,1-Trichloroethane 50.0 50.7 ug/Kg 101 70 -130 1 30
1,1,2-Trichloroethane 50.0 48.5 ug/Kg 97 56 -146 2 30
Trichloroethene 50.0 50.3 ug/Kg 101 70 -130 1 30
Trichlorofluoromethane 50.0 55.9 ug/Kg 112 70 -130 1 30
1,2,3-Trichloropropane 50.0 48.5 ug/Kg 97 64 -130 1 30
1,2,4-Trimethylbenzene 50.0 48.9 ug/Kg 98 70 -130 1 30
1,3,5-Trimethylbenzene 50.0 49.2 ug/Kg 98 70 -130 0 30
Vinyl acetate 100 123 ug/Kg 123 53-150 2 30
Vinyl chloride 50.0 48.0 ug/Kg 96 70 -130 5 30
Xylenes, Total 100 101 ug/Kg 101 70-130 1 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
110
LCSD LCSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)65 -130
994-Bromofluorobenzene (Surr)65 -130
101Toluene-d8 (Surr)65 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-744701/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
RL MDL
1,2,4-Trichlorobenzene <30 320 30 ug/Kg 10/11/22 19:45 10/12/22 18:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<36 36320 ug/Kg 10/11/22 19:45 10/12/22 18:12 11,2-Dichlorobenzene
<33 33320 ug/Kg 10/11/22 19:45 10/12/22 18:12 11,3-Dichlorobenzene
<34 34320 ug/Kg 10/11/22 19:45 10/12/22 18:12 11,4-Dichlorobenzene
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-744701/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
RL MDL
1-Methylnaphthalene <30 320 30 ug/Kg 10/11/22 19:45 10/12/22 18:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<34 34320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4,5-Trichlorophenol
<28 28320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4,6-Trichlorophenol
<34 34320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4-Dichlorophenol
<43 43320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4-Dimethylphenol
<810 8101700 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4-Dinitrophenol
<48 48320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,4-Dinitrotoluene
<41 41320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12,6-Dinitrotoluene
<34 34320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Chloronaphthalene
<39 39320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Chlorophenol
<37 37320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Methylnaphthalene
<26 26320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Methylphenol
<44 441700 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Nitroaniline
<40 40320 ug/Kg 10/11/22 19:45 10/12/22 18:12 12-Nitrophenol
<42 42320 ug/Kg 10/11/22 19:45 10/12/22 18:12 13 & 4 Methylphenol
<27 27650 ug/Kg 10/11/22 19:45 10/12/22 18:12 13,3'-Dichlorobenzidine
<45 451700 ug/Kg 10/11/22 19:45 10/12/22 18:12 13-Nitroaniline
<170 1701700 ug/Kg 10/11/22 19:45 10/12/22 18:12 14,6-Dinitro-2-methylphenol
<35 35320 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Bromophenyl phenyl ether
<34 34320 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Chloro-3-methylphenol
<51 51650 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Chloroaniline
<43 43320 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Chlorophenyl phenyl ether
<48 481700 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Nitroaniline
<320 3201700 ug/Kg 10/11/22 19:45 10/12/22 18:12 14-Nitrophenol
<40 40320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Acenaphthene
<35 35320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Acenaphthylene
<24 24320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Anthracene
<810 8102600 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzidine
<26 26320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzo[a]anthracene
<51 51320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzo[a]pyrene
<37 37320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzo[b]fluoranthene
<22 22320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzo[g,h,i]perylene
<64 64320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzo[k]fluoranthene
<810 8101700 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzoic acid
<32 32320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Benzyl alcohol
<29 29320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1bis (2-chloroisopropyl) ether
<38 38320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Bis(2-chloroethoxy)methane
<44 44320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Bis(2-chloroethyl)ether
<28 28320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Bis(2-ethylhexyl) phthalate
<25 25320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Butyl benzyl phthalate
<21 21320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Chrysene
<38 38320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Dibenz(a,h)anthracene
<32 32320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Dibenzofuran
<36 36320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Diethyl phthalate
<33 33320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Dimethyl phthalate
<29 29320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Di-n-butyl phthalate
<28 28320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Di-n-octyl phthalate
<31 31320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Fluoranthene
<35 35320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Fluorene
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-744701/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
RL MDL
Hexachlorobenzene <38 320 38 ug/Kg 10/11/22 19:45 10/12/22 18:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<35 35320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Hexachlorobutadiene
<40 40320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Hexachlorocyclopentadiene
<27 27320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Hexachloroethane
<27 27320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Indeno[1,2,3-cd]pyrene
<32 32320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Isophorone
<29 29320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Naphthalene
<25 25320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Nitrobenzene
<120 120320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1N-Nitrosodimethylamine
<31 31320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1N-Nitrosodi-n-propylamine
<32 32320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1N-Nitrosodiphenylamine
<320 3201700 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Pentachlorophenol
<26 26320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Phenanthrene
<33 33320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Phenol
<26 26320 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Pyrene
<320 320650 ug/Kg 10/11/22 19:45 10/12/22 18:12 1Pyridine
2,4,6-Tribromophenol (Surr)42 21-132 10/12/22 18:12 1
MB MB
Surrogate
10/11/22 19:45
Dil FacPrepared AnalyzedQualifier Limits%Recovery
48 10/11/22 19:45 10/12/22 18:12 12-Fluorobiphenyl (Surr)25-130
40 10/11/22 19:45 10/12/22 18:12 12-Fluorophenol (Surr)18-130
46 10/11/22 19:45 10/12/22 18:12 1Nitrobenzene-d5 (Surr)19-130
39 10/11/22 19:45 10/12/22 18:12 1Phenol-d5 (Surr)21-130
53 10/11/22 19:45 10/12/22 18:12 1Terphenyl-d14 (Surr)31-133
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744701/20-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
1,2,4-Trichlorobenzene 6330 3350 ug/Kg 53 20 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichlorobenzene 6330 3090 ug/Kg 49 20 -130
1,3-Dichlorobenzene 6330 3040 ug/Kg 48 18 -130
1,4-Dichlorobenzene 6330 3070 ug/Kg 49 19 -130
1-Methylnaphthalene 6330 3540 ug/Kg 56 28 -130
2,4,5-Trichlorophenol 6330 4080 ug/Kg 64 33 -130
2,4,6-Trichlorophenol 6330 4130 ug/Kg 65 31 -130
2,4-Dichlorophenol 6330 3950 ug/Kg 62 30 -130
2,4-Dimethylphenol 6330 4030 ug/Kg 64 34 -130
2,4-Dinitrophenol 12700 8560 ug/Kg 68 10 -130
2,4-Dinitrotoluene 6330 4270 ug/Kg 68 34 -130
2,6-Dinitrotoluene 6330 3990 ug/Kg 63 33 -130
2-Chloronaphthalene 6330 3830 ug/Kg 61 30 -130
2-Chlorophenol 6330 3590 ug/Kg 57 28 -130
2-Methylnaphthalene 6330 3380 ug/Kg 53 28 -130
2-Methylphenol 6330 3550 ug/Kg 56 30 -130
2-Nitroaniline 6330 3810 ug/Kg 60 26 -130
2-Nitrophenol 6330 3460 ug/Kg 55 24 -130
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744701/20-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
3 & 4 Methylphenol 6330 3760 ug/Kg 59 31 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
3,3'-Dichlorobenzidine 6330 3850 ug/Kg 61 10 -130
3-Nitroaniline 6330 3880 ug/Kg 61 10 -130
4,6-Dinitro-2-methylphenol 12700 10500 ug/Kg 83 22 -130
4-Bromophenyl phenyl ether 6330 4300 ug/Kg 68 32 -130
4-Chloro-3-methylphenol 6330 3770 ug/Kg 60 31 -130
4-Chloroaniline 6330 3530 ug/Kg 56 10 -130
4-Chlorophenyl phenyl ether 6330 3930 ug/Kg 62 32 -130
4-Nitroaniline 6330 4010 ug/Kg 63 25 -130
4-Nitrophenol 12700 8460 ug/Kg 67 25 -130
Acenaphthene 6330 4170 ug/Kg 66 33 -130
Acenaphthylene 6330 4030 ug/Kg 64 34 -130
Anthracene 6330 4700 ug/Kg 74 39 -130
Benzidine 6330 3230 ug/Kg 51 10 -130
Benzo[a]anthracene 6330 4610 ug/Kg 73 40 -130
Benzo[a]pyrene 6330 4630 ug/Kg 73 37 -131
Benzo[b]fluoranthene 6330 4580 ug/Kg 72 35 -130
Benzo[g,h,i]perylene 6330 5380 ug/Kg 85 39 -130
Benzo[k]fluoranthene 6330 4330 ug/Kg 68 35 -130
Benzoic acid 6330 2110 ug/Kg 33 10 -139
Benzyl alcohol 6330 3830 ug/Kg 60 19 -130
bis (2-chloroisopropyl) ether 6330 2800 ug/Kg 44 12 -130
Bis(2-chloroethoxy)methane 6330 3390 ug/Kg 54 29 -130
Bis(2-chloroethyl)ether 6330 2640 ug/Kg 42 18 -130
Bis(2-ethylhexyl) phthalate 6330 4400 ug/Kg 70 39 -130
Butyl benzyl phthalate 6330 4220 ug/Kg 67 38 -130
Chrysene 6330 4270 ug/Kg 67 40 -130
Dibenz(a,h)anthracene 6330 5400 ug/Kg 85 37 -130
Dibenzofuran 6330 4030 ug/Kg 64 34 -130
Diethyl phthalate 6330 4530 ug/Kg 72 36 -130
Dimethyl phthalate 6330 3940 ug/Kg 62 36 -130
Di-n-butyl phthalate 6330 4730 ug/Kg 75 39 -130
Di-n-octyl phthalate 6330 4440 ug/Kg 70 38 -131
Fluoranthene 6330 4760 ug/Kg 75 38 -130
Fluorene 6330 4040 ug/Kg 64 34 -130
Hexachlorobenzene 6330 4300 ug/Kg 68 28 -130
Hexachlorobutadiene 6330 3300 ug/Kg 52 22 -130
Hexachlorocyclopentadiene 6330 3880 ug/Kg 61 11 -130
Hexachloroethane 6330 3150 ug/Kg 50 21 -130
Indeno[1,2,3-cd]pyrene 6330 5740 ug/Kg 91 40 -130
Isophorone 6330 3300 ug/Kg 52 26 -130
Naphthalene 6330 3480 ug/Kg 55 25 -130
Nitrobenzene 6330 3290 ug/Kg 52 25 -130
N-Nitrosodimethylamine 6330 3320 ug/Kg 53 20 -130
N-Nitrosodi-n-propylamine 6330 3050 ug/Kg 48 24 -130
N-Nitrosodiphenylamine 6330 4490 ug/Kg 71 37 -130
Pentachlorophenol 12700 8920 ug/Kg 71 16 -135
Phenanthrene 6330 4690 ug/Kg 74 38 -130
Phenol 6330 3580 ug/Kg 57 27 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-744701/20-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 744859 Prep Batch: 744701
Pyrene 6330 4340 ug/Kg 69 40 -130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Pyridine 12700 5340 ug/Kg 42 10 -130
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
63
LCS LCS
Qualifier Limits%Recovery
592-Fluorobiphenyl (Surr)25 -130
552-Fluorophenol (Surr)18 -130
54Nitrobenzene-d5 (Surr)19 -130
55Phenol-d5 (Surr)21 -130
65Terphenyl-d14 (Surr)31 -133
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 680-745401/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 745559 Prep Batch: 745401
RL MDL
Arsenic <0.020 0.020 0.020 mg/L 10/17/22 05:34 10/17/22 21:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.10 0.100.10 mg/L 10/17/22 05:34 10/17/22 21:00 1Barium
<0.010 0.0100.010 mg/L 10/17/22 05:34 10/17/22 21:00 1Cadmium
<0.020 0.0200.020 mg/L 10/17/22 05:34 10/17/22 21:00 1Chromium
<0.020 0.0200.020 mg/L 10/17/22 05:34 10/17/22 21:00 1Lead
<0.050 0.0500.050 mg/L 10/17/22 05:34 10/17/22 21:00 1Selenium
<0.010 0.0100.010 mg/L 10/17/22 05:34 10/17/22 21:00 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-745401/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 745559 Prep Batch: 745401
Arsenic 2.00 1.95 mg/L 98 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Barium 2.00 2.01 mg/L 100 80 -120
Cadmium 1.00 1.02 mg/L 102 80 -120
Chromium 2.00 2.05 mg/L 103 80 -120
Lead 10.1 9.80 mg/L 97 80 -120
Selenium 2.00 1.88 mg/L 94 80 -120
Silver 1.00 0.977 mg/L 98 80 -120
Client Sample ID: Method BlankLab Sample ID: LB 680-745032/1-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 745559 Prep Batch: 745401
RL MDL
Arsenic <0.20 0.20 0.20 mg/L 10/17/22 05:34 10/17/22 21:06 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 1.01.0 mg/L 10/17/22 05:34 10/17/22 21:06 1Barium
<0.10 0.100.10 mg/L 10/17/22 05:34 10/17/22 21:06 1Cadmium
<0.20 0.200.20 mg/L 10/17/22 05:34 10/17/22 21:06 1Chromium
<0.20 0.200.20 mg/L 10/17/22 05:34 10/17/22 21:06 1Lead
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QC Sample Results
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 680-745032/1-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 745559 Prep Batch: 745401
RL MDL
Selenium <0.50 0.50 0.50 mg/L 10/17/22 05:34 10/17/22 21:06 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.10 0.100.10 mg/L 10/17/22 05:34 10/17/22 21:06 1Silver
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-745433/12-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 745522 Prep Batch: 745433
RL MDL
Mercury <0.00020 0.00020 0.00020 mg/L 10/17/22 08:57 10/17/22 14:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-745433/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 745522 Prep Batch: 745433
Mercury 0.250 0.264 mg/L 106 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Method BlankLab Sample ID: LB 680-745032/1-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 745522 Prep Batch: 745433
RL MDL
Mercury <0.020 0.020 0.020 mg/L 10/17/22 08:57 10/17/22 14:59 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Eurofins Savannah
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QC Association Summary
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
GC/MS VOA
Prep Batch: 744123
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-222306-1 - DL SS-1 Total/NA
Soil 5035A680-222306-1 SS-1 Total/NA
Analysis Batch: 744365
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 744123680-222306-1 SS-1 Total/NA
Solid 8260DMB 680-744365/9 Method Blank Total/NA
Solid 8260DLCS 680-744365/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-744365/6 Lab Control Sample Dup Total/NA
Analysis Batch: 744553
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 744123680-222306-1 - DL SS-1 Total/NA
Solid 8260DMB 680-744553/9 Method Blank Total/NA
Solid 8260DLCS 680-744553/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-744553/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 744701
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3546680-222306-1 SS-1 Total/NA
Solid 3546MB 680-744701/19-A Method Blank Total/NA
Solid 3546LCS 680-744701/20-A Lab Control Sample Total/NA
Analysis Batch: 744859
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270E 744701680-222306-1 SS-1 Total/NA
Solid 8270E 744701MB 680-744701/19-A Method Blank Total/NA
Solid 8270E 744701LCS 680-744701/20-A Lab Control Sample Total/NA
Metals
Leach Batch: 745032
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 1311680-222306-1 SS-1 TCLP
Solid 1311LB 680-745032/1-C Method Blank TCLP
Solid 1311LB 680-745032/1-D Method Blank TCLP
Prep Batch: 745401
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3010A 745032680-222306-1 SS-1 TCLP
Solid 3010A 745032LB 680-745032/1-C Method Blank TCLP
Solid 3010AMB 680-745401/1-A Method Blank Total/NA
Solid 3010ALCS 680-745401/2-A Lab Control Sample Total/NA
Prep Batch: 745433
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7470A 745032680-222306-1 SS-1 TCLP
Solid 7470A 745032LB 680-745032/1-D Method Blank TCLP
Solid 7470AMB 680-745433/12-A Method Blank Total/NA
Solid 7470ALCS 680-745433/13-A Lab Control Sample Total/NA
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QC Association Summary
Job ID: 680-222306-1Client: Environmental Conservation Laboratories
Project/Site: CF14729
Metals
Analysis Batch: 745522
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7470A 745433680-222306-1 SS-1 TCLP
Solid 7470A 745433LB 680-745032/1-D Method Blank TCLP
Solid 7470A 745433MB 680-745433/12-A Method Blank Total/NA
Solid 7470A 745433LCS 680-745433/13-A Lab Control Sample Total/NA
Analysis Batch: 745559
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 745401680-222306-1 SS-1 TCLP
Solid 6010D 745401LB 680-745032/1-C Method Blank TCLP
Solid 6010D 745401MB 680-745401/1-A Method Blank Total/NA
Solid 6010D 745401LCS 680-745401/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 744832
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture680-222306-1 SS-1 Total/NA
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Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-222306-1
Project/Site: CF14729
Client Sample ID: SS-1 Lab Sample ID: 680-222306-1
Matrix: SoilDate Collected: 09/28/22 09:00
Date Received: 10/04/22 08:00
Leach 1311 WRB10/13/22 21:40 EET SAV745032
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
TCLP 100.00 g 2000 mL
Prep 3010A 745401 10/17/22 05:34 RR EET SAVTCLP5 mL 50 mL
Analysis 6010D 1 745559 10/17/22 21:30 BJB EET SAVTCLP
ICPHInstrument ID:
Leach 1311 745032 10/13/22 21:40 WRB EET SAVTCLP100.00 g 2000 mL
Prep 7470A 745433 10/17/22 08:57 JKL EET SAVTCLP0.50 mL 50 mL
Analysis 7470A 1 745522 10/17/22 15:25 JKL EET SAVTCLP
QuickTrace2Instrument ID:
Analysis Moisture 1 744832 10/12/22 14:36 WRB EET SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: SS-1 Lab Sample ID: 680-222306-1
Matrix: SoilDate Collected: 09/28/22 09:00
Percent Solids: 92.2Date Received: 10/04/22 08:00
Prep 5035A FES10/07/22 13:44 EET SAV744123
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.335 g 5 mL
Analysis 8260D 40 744365 10/10/22 19:31 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 744123 10/07/22 13:44 FES EET SAVTotal/NA 5.335 g 5 mL
Analysis 8260D DL 200 744553 10/11/22 14:43 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 744701 10/11/22 19:45 MJ EET SAVTotal/NA 15.31 g 1 mL
Analysis 8270E 1 744859 10/13/22 02:52 T1C EET SAVTotal/NA 1 mL 1 mL
CMSGInstrument ID:
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Environmental Conservation Laboratories Job Number: 680-222306-1
Login Number: 222306
Question Answer Comment
Creator: Flanagan, Naomi V
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
FalseIs the Field Sampler's name present on COC?Not requested on COC.
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-222306-1
Project/Site: CF14729
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22
Virginia NELAP 460161 06-14-23
Eurofins Savannah
Page 43 of 43 10/19/2022
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ANALYTICAL REPORT
PREPARED FOR
Attn: Kirk Pollard
Mineral Springs Environmental
4600 Mineral Springs Lane
Raleigh, North Carolina 27616
Generated 3/14/2023 5:02:51 PM
JOB DESCRIPTION
Country Line Rd
JOB NUMBER
752-3710-1
See page two for job notes and contact information.
Cary NC 27511
102-A Woodwinds Industrial Court
Eurofins Raleigh
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Eurofins Raleigh
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
3/14/2023 5:02:51 PM
Authorized for release by
Bill Scott, Project Manager
[e-mail]
[phone]
Page 2 of 38 3/14/2023
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Table of Contents
Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Laboratory Job ID: 752-3710-1
Page 3 of 38 Eurofins Raleigh3/14/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
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Definitions/Glossary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Qualifiers
GC/MS VOA
Qualifier Description
*- LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
*+LCS and/or LCSD is outside acceptance limits, high biased.
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Raleigh
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Case Narrative
Client: Mineral Springs Environmental Job ID: 752-3710-1
Project/Site: Country Line Rd
Job ID: 752-3710-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-3710-1
Receipt
The sample was received on 3/1/2023 3:25 PM. Unless otherwise noted below, the sample arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.6°C
GC/MS VOA
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 680-765873 and analytical batch 680-765882.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E: The matrix spike duplicate (MSD) recoveries for preparation batch 680-765985 and analytical batch 680-766626 were
outside control limits. Non-homogeneity is suspected because the associated laboratory control sample (LCS) recovery was within
acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: The following sample was diluted because the base dilution for VPH soil analysis is 1:50: SS-B1 (752-3710-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins RaleighPage 5 of 38 3/14/2023
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Detection Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Client Sample ID: SS-B1 Lab Sample ID: 752-3710-1
☼Bis(2-ethylhexyl) phthalate
RL
370 ug/Kg
MDL
33
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J2508270E
☼C9-C10 Aromatics 0.75 mg/Kg0.75 Total/NA501.0 MAVPH
☼C11-C22 Aromatics 19 mg/Kg3.5 Total/NA17.8 J MAEPH2.1
☼C19-C36 Aliphatics 19 mg/Kg3.5 Total/NA19.7 J MAEPH2.1
☼C9-C18 Aliphatics 19 mg/Kg1.5 Total/NA12.4 J B MAEPH2.1
Eurofins Raleigh
This Detection Summary does not include radiochemical test results.
Page 6 of 38 3/14/2023
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Client Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Lab Sample ID: 752-3710-1Client Sample ID: SS-B1
Matrix: SolidDate Collected: 02/28/23 13:00
Percent Solids: 87.6Date Received: 03/01/23 15:25
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 4.3 1.1 ug/Kg ☼03/03/23 08:52 03/03/23 18:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1,2-Tetrachloroethane
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1,1-Trichloroethane
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1,2,2-Tetrachloroethane
4.3 1.3 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1,2-Trichloroethane
4.3 2.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1-Dichloroethane
4.3 3.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1-Dichloroethene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,1-Dichloropropene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2,3-Trichlorobenzene
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2,3-Trichloropropane
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2,4-Trichlorobenzene
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2,4-Trimethylbenzene
8.6 1.4 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2-Dibromo-3-Chloropropane
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2-Dichlorobenzene
4.3 2.0 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2-Dichloroethane
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,2-Dichloropropane
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,3,5-Trimethylbenzene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,3-Dichlorobenzene
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,3-Dichloropropane
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND1,4-Dichlorobenzene
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND2,2-Dichloropropane
21 7.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND2-Butanone (MEK)
4.3 2.0 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND2-Chlorotoluene
21 16 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND2-Hexanone
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND4-Chlorotoluene
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND4-Isopropyltoluene
21 15 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND4-Methyl-2-pentanone (MIBK)
43 9.4 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDAcetone
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDBenzene
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDBromobenzene
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDBromoform
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDBromomethane
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND *+Carbon disulfide
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDCarbon tetrachloride
4.3 1.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDChlorobenzene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDChlorobromomethane
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDChlorodibromomethane
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDChloroethane
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDChloroform
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼ND *-Chloromethane
4.3 2.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDcis-1,2-Dichloroethene
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDcis-1,3-Dichloropropene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDDibromomethane
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDDichlorobromomethane
4.3 2.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDDichlorodifluoromethane
4.3 1.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDEthylbenzene
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDEthylene Dibromide
4.3 3.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDHexachlorobutadiene
8.6 1.3 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDIsopropyl ether
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDIsopropylbenzene
Eurofins Raleigh
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Client Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Lab Sample ID: 752-3710-1Client Sample ID: SS-B1
Matrix: SolidDate Collected: 02/28/23 13:00
Percent Solids: 87.6Date Received: 03/01/23 15:25
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 4.3 1.9 ug/Kg ☼03/03/23 08:52 03/03/23 18:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Methyl tert-butyl ether
8.6 6.8 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDMethylene Chloride
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDm-Xylene & p-Xylene
4.3 2.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDNaphthalene
4.3 1.6 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDn-Butylbenzene
4.3 1.9 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDN-Propylbenzene
4.3 2.0 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDo-Xylene
4.3 1.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDsec-Butylbenzene
4.3 1.6 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDStyrene
4.3 2.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDtert-Butylbenzene
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDTetrachloroethene
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDToluene
4.3 2.0 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDtrans-1,2-Dichloroethene
4.3 2.2 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDtrans-1,3-Dichloropropene
4.3 1.5 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDTrichloroethene
4.3 2.7 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDTrichlorofluoromethane
4.3 2.4 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDVinyl chloride
8.6 3.1 ug/Kg 03/03/23 08:52 03/03/23 18:50 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)98 65-130 03/03/23 08:52 03/03/23 18:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 97 03/03/23 08:52 03/03/23 18:50 165-130
Dibromofluoromethane (Surr) 108 03/03/23 08:52 03/03/23 18:50 165-130
Toluene-d8 (Surr) 103 03/03/23 08:52 03/03/23 18:50 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 370 35 ug/Kg ☼03/03/23 16:20 03/08/23 23:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,2,4-Trichlorobenzene
370 41 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND1,2-Dichlorobenzene
370 38 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND1,3-Dichlorobenzene
370 39 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND1,4-Dichlorobenzene
370 35 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND1-Methylnaphthalene
370 39 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,4,5-Trichlorophenol
370 33 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,4,6-Trichlorophenol
370 39 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,4-Dichlorophenol
370 49 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,4-Dimethylphenol
1900 930 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND F12,4-Dinitrophenol
370 55 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,4-Dinitrotoluene
370 47 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2,6-Dinitrotoluene
370 39 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Chloronaphthalene
370 45 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Chlorophenol
370 43 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Methylnaphthalene
370 30 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Methylphenol
1900 50 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Nitroaniline
370 46 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND2-Nitrophenol
370 48 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND3 & 4 Methylphenol
740 31 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND3,3'-Dichlorobenzidine
1900 52 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND3-Nitroaniline
1900 190 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4,6-Dinitro-2-methylphenol
370 40 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4-Bromophenyl phenyl ether
Eurofins Raleigh
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Client Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Lab Sample ID: 752-3710-1Client Sample ID: SS-B1
Matrix: SolidDate Collected: 02/28/23 13:00
Percent Solids: 87.6Date Received: 03/01/23 15:25
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 370 39 ug/Kg ☼03/03/23 16:20 03/08/23 23:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Chloro-3-methylphenol
740 58 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4-Chloroaniline
370 49 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4-Chlorophenyl phenyl ether
1900 55 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4-Nitroaniline
1900 370 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND4-Nitrophenol
370 46 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDAcenaphthene
370 40 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDAcenaphthylene
370 28 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDAnthracene
3000 930 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼ND F1Benzidine
370 30 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzo[a]anthracene
370 58 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzo[a]pyrene
370 43 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzo[b]fluoranthene
370 25 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzo[g,h,i]perylene
370 73 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzo[k]fluoranthene
1900 930 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzoic acid
370 37 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBenzyl alcohol
370 34 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDbis (2-chloroisopropyl) ether
370 44 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBis(2-chloroethoxy)methane
370 50 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDBis(2-chloroethyl)ether
370 33 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼250 JBis(2-ethylhexyl) phthalate
370 29 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDButyl benzyl phthalate
370 24 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDChrysene
370 44 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDibenz(a,h)anthracene
370 37 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDibenzofuran
370 41 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDiethyl phthalate
370 38 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDimethyl phthalate
370 34 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDi-n-butyl phthalate
370 33 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDi-n-octyl phthalate
370 46 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDDiphenylamine
370 36 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDFluoranthene
370 40 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDFluorene
370 44 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDHexachlorobenzene
370 40 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDHexachlorobutadiene
370 46 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDHexachlorocyclopentadiene
370 31 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDHexachloroethane
370 31 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDIndeno[1,2,3-cd]pyrene
370 37 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDIsophorone
370 34 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDNaphthalene
370 29 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDNitrobenzene
370 130 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDN-Nitrosodimethylamine
370 36 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDN-Nitrosodi-n-propylamine
370 37 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDN-Nitrosodiphenylamine
1900 370 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDPentachlorophenol
370 30 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDPhenanthrene
370 38 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDPhenol
370 30 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDPyrene
740 370 ug/Kg 03/03/23 16:20 03/08/23 23:22 1☼NDPyridine
2,4,6-Tribromophenol (Surr)77 21-132 03/03/23 16:20 03/08/23 23:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Eurofins Raleigh
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Client Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Lab Sample ID: 752-3710-1Client Sample ID: SS-B1
Matrix: SolidDate Collected: 02/28/23 13:00
Percent Solids: 87.6Date Received: 03/01/23 15:25
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
2-Fluorobiphenyl (Surr)68 25-130 03/03/23 16:20 03/08/23 23:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 67 03/03/23 16:20 03/08/23 23:22 118-130
Nitrobenzene-d5 (Surr) 62 03/03/23 16:20 03/08/23 23:22 119-130
Phenol-d5 (Surr) 69 03/03/23 16:20 03/08/23 23:22 121-130
Terphenyl-d14 (Surr) 91 03/03/23 16:20 03/08/23 23:22 131-133
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 2.7 2.7 mg/Kg ☼03/03/23 09:30 03/09/23 01:40 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
C5-C8 Aliphatics
1.4 1.4 mg/Kg 03/03/23 09:30 03/09/23 01:40 50☼NDC9-C12 Aliphatics
0.75 0.75 mg/Kg 03/03/23 09:30 03/09/23 01:40 50☼1.0C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)94 70-130 03/03/23 09:30 03/09/23 01:40 50
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
a,a,a-Trifluorotoluene (pid) 96 03/03/23 09:30 03/09/23 01:40 5070-130
Method: MA DEP MA EPH SUM - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 100 mg/Kg 03/08/23 11:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Total EPH
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
7.8 J 19 3.5 mg/Kg ☼03/02/23 23:20 03/03/23 13:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
C11-C22 Aromatics
19 3.5 mg/Kg 03/02/23 23:20 03/03/23 13:01 1☼9.7 JC19-C36 Aliphatics
19 1.5 mg/Kg 03/02/23 23:20 03/03/23 13:01 1☼2.4 J BC9-C18 Aliphatics
o- terphenyl (Surr)100 40-140 03/02/23 23:20 03/03/23 13:01 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1-Chlorooctadecane 102 03/02/23 23:20 03/03/23 13:01 140-140
Eurofins Raleigh
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Surrogate Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (65-130) (65-130) (65-130) (65-130)
DCA BFB DBFM TOL
98 97 108 103752-3710-1
Percent Surrogate Recovery (Acceptance Limits)
SS-B1
96 97 106 102LCS 680-765882/5 Lab Control Sample
100 97 109 104LCSD 680-765882/6 Lab Control Sample Dup
94 96 106 104MB 680-765882/8 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-132) (25-130) (18-130) (19-130) (21-130) (31-133)
TBP FBP 2FP NBZ PHL TPHL
77 68 67 62 69 91752-3710-1
Percent Surrogate Recovery (Acceptance Limits)
SS-B1
85 64 65 6761 91752-3710-1 MS SS-B1
85 66 64 6960 91752-3710-1 MSD SS-B1
88 70 65 6962 92LCS 680-765985/5-A Lab Control Sample
77 72 70 6961 102MB 680-765985/4-A Method Blank
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130) (70-130)
TFT-F1 TFT-P1
94 96752-3710-1
Percent Surrogate Recovery (Acceptance Limits)
SS-B1
90 91LCS 400-614798/2-A Lab Control Sample
92 90LCSD 400-614798/3-A Lab Control Sample Dup
85 85MB 400-614798/1-A Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Eurofins Raleigh
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Surrogate Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (40-140) (40-140)
OTP1 1COD1
100 102752-3710-1
Percent Surrogate Recovery (Acceptance Limits)
SS-B1
98 107LCS 752-1588/2-A Lab Control Sample
96 98MB 752-1588/1-A Method Blank
Surrogate Legend
OTP = o- terphenyl (Surr)
1COD = 1-Chlorooctadecane
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-765882/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/Kg 03/03/23 12:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 2.65.0 ug/Kg 03/03/23 12:53 11,1,1-Trichloroethane
ND 2.15.0 ug/Kg 03/03/23 12:53 11,1,2,2-Tetrachloroethane
ND 1.55.0 ug/Kg 03/03/23 12:53 11,1,2-Trichloroethane
ND 2.95.0 ug/Kg 03/03/23 12:53 11,1-Dichloroethane
ND 3.65.0 ug/Kg 03/03/23 12:53 11,1-Dichloroethene
ND 2.05.0 ug/Kg 03/03/23 12:53 11,1-Dichloropropene
ND 2.05.0 ug/Kg 03/03/23 12:53 11,2,3-Trichlorobenzene
ND 1.85.0 ug/Kg 03/03/23 12:53 11,2,3-Trichloropropane
ND 2.55.0 ug/Kg 03/03/23 12:53 11,2,4-Trichlorobenzene
ND 2.55.0 ug/Kg 03/03/23 12:53 11,2,4-Trimethylbenzene
ND 1.610 ug/Kg 03/03/23 12:53 11,2-Dibromo-3-Chloropropane
ND 1.75.0 ug/Kg 03/03/23 12:53 11,2-Dichlorobenzene
ND 2.35.0 ug/Kg 03/03/23 12:53 11,2-Dichloroethane
ND 2.65.0 ug/Kg 03/03/23 12:53 11,2-Dichloropropane
ND 2.45.0 ug/Kg 03/03/23 12:53 11,3,5-Trimethylbenzene
ND 2.05.0 ug/Kg 03/03/23 12:53 11,3-Dichlorobenzene
ND 2.25.0 ug/Kg 03/03/23 12:53 11,3-Dichloropropane
ND 1.85.0 ug/Kg 03/03/23 12:53 11,4-Dichlorobenzene
ND 2.25.0 ug/Kg 03/03/23 12:53 12,2-Dichloropropane
ND 9.225 ug/Kg 03/03/23 12:53 12-Butanone (MEK)
ND 2.35.0 ug/Kg 03/03/23 12:53 12-Chlorotoluene
ND 1925 ug/Kg 03/03/23 12:53 12-Hexanone
ND 2.15.0 ug/Kg 03/03/23 12:53 14-Chlorotoluene
ND 2.65.0 ug/Kg 03/03/23 12:53 14-Isopropyltoluene
ND 1825 ug/Kg 03/03/23 12:53 14-Methyl-2-pentanone (MIBK)
ND 1150 ug/Kg 03/03/23 12:53 1Acetone
ND 2.45.0 ug/Kg 03/03/23 12:53 1Benzene
ND 1.75.0 ug/Kg 03/03/23 12:53 1Bromobenzene
ND 2.25.0 ug/Kg 03/03/23 12:53 1Bromoform
ND 2.45.0 ug/Kg 03/03/23 12:53 1Bromomethane
ND 2.15.0 ug/Kg 03/03/23 12:53 1Carbon disulfide
ND 2.15.0 ug/Kg 03/03/23 12:53 1Carbon tetrachloride
ND 1.45.0 ug/Kg 03/03/23 12:53 1Chlorobenzene
ND 2.05.0 ug/Kg 03/03/23 12:53 1Chlorobromomethane
ND 2.15.0 ug/Kg 03/03/23 12:53 1Chlorodibromomethane
ND 2.25.0 ug/Kg 03/03/23 12:53 1Chloroethane
ND 2.05.0 ug/Kg 03/03/23 12:53 1Chloroform
ND 2.45.0 ug/Kg 03/03/23 12:53 1Chloromethane
ND 2.95.0 ug/Kg 03/03/23 12:53 1cis-1,2-Dichloroethene
ND 2.25.0 ug/Kg 03/03/23 12:53 1cis-1,3-Dichloropropene
ND 2.05.0 ug/Kg 03/03/23 12:53 1Dibromomethane
ND 2.05.0 ug/Kg 03/03/23 12:53 1Dichlorobromomethane
ND 3.25.0 ug/Kg 03/03/23 12:53 1Dichlorodifluoromethane
ND 2.15.0 ug/Kg 03/03/23 12:53 1Ethylbenzene
ND 1.75.0 ug/Kg 03/03/23 12:53 1Ethylene Dibromide
ND 4.15.0 ug/Kg 03/03/23 12:53 1Hexachlorobutadiene
ND 1.510 ug/Kg 03/03/23 12:53 1Isopropyl ether
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-765882/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
RL MDL
Isopropylbenzene ND 5.0 2.2 ug/Kg 03/03/23 12:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 2.25.0 ug/Kg 03/03/23 12:53 1Methyl tert-butyl ether
ND 8.010 ug/Kg 03/03/23 12:53 1Methylene Chloride
ND 2.25.0 ug/Kg 03/03/23 12:53 1m-Xylene & p-Xylene
ND 3.15.0 ug/Kg 03/03/23 12:53 1Naphthalene
ND 1.95.0 ug/Kg 03/03/23 12:53 1n-Butylbenzene
ND 2.25.0 ug/Kg 03/03/23 12:53 1N-Propylbenzene
ND 2.35.0 ug/Kg 03/03/23 12:53 1o-Xylene
ND 2.05.0 ug/Kg 03/03/23 12:53 1sec-Butylbenzene
ND 1.95.0 ug/Kg 03/03/23 12:53 1Styrene
ND 2.55.0 ug/Kg 03/03/23 12:53 1tert-Butylbenzene
ND 2.65.0 ug/Kg 03/03/23 12:53 1Tetrachloroethene
ND 2.65.0 ug/Kg 03/03/23 12:53 1Toluene
ND 2.35.0 ug/Kg 03/03/23 12:53 1trans-1,2-Dichloroethene
ND 2.65.0 ug/Kg 03/03/23 12:53 1trans-1,3-Dichloropropene
ND 1.85.0 ug/Kg 03/03/23 12:53 1Trichloroethene
ND 3.15.0 ug/Kg 03/03/23 12:53 1Trichlorofluoromethane
ND 2.85.0 ug/Kg 03/03/23 12:53 1Vinyl chloride
ND 3.610 ug/Kg 03/03/23 12:53 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)94 65-130 03/03/23 12:53 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
96 03/03/23 12:53 14-Bromofluorobenzene (Surr)65-130
106 03/03/23 12:53 1Dibromofluoromethane (Surr)65-130
104 03/03/23 12:53 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-765882/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
1,1,1,2-Tetrachloroethane 50.0 50.5 ug/Kg 101 70-130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 50.7 ug/Kg 101 70-130
1,1,2,2-Tetrachloroethane 50.0 42.3 ug/Kg 85 64-130
1,1,2-Trichloroethane 50.0 47.9 ug/Kg 96 56-146
1,1-Dichloroethane 50.0 52.2 ug/Kg 104 70-130
1,1-Dichloroethene 50.0 54.8 ug/Kg 110 69-130
1,1-Dichloropropene 50.0 54.5 ug/Kg 109 70-130
1,2,3-Trichlorobenzene 50.0 43.2 ug/Kg 86 70-130
1,2,3-Trichloropropane 50.0 41.7 ug/Kg 83 64-130
1,2,4-Trichlorobenzene 50.0 46.2 ug/Kg 92 70-130
1,2,4-Trimethylbenzene 50.0 50.8 ug/Kg 102 70-130
1,2-Dibromo-3-Chloropropane 50.0 33.7 ug/Kg 67 42-145
1,2-Dichlorobenzene 50.0 49.9 ug/Kg 100 70-130
1,2-Dichloroethane 50.0 48.5 ug/Kg 97 68-139
1,2-Dichloropropane 50.0 52.6 ug/Kg 105 70-130
1,3,5-Trimethylbenzene 50.0 50.3 ug/Kg 101 70-130
1,3-Dichlorobenzene 50.0 50.9 ug/Kg 102 70-130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-765882/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
1,3-Dichloropropane 50.0 50.0 ug/Kg 100 54-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,4-Dichlorobenzene 50.0 49.7 ug/Kg 99 70-130
2,2-Dichloropropane 50.0 49.6 ug/Kg 99 70-130
2-Butanone (MEK)250 180 ug/Kg 72 40-150
2-Chlorotoluene 50.0 50.2 ug/Kg 100 70-130
2-Hexanone 250 186 ug/Kg 74 30-150
4-Chlorotoluene 50.0 45.5 ug/Kg 91 70-130
4-Isopropyltoluene 50.0 49.9 ug/Kg 100 70-130
4-Methyl-2-pentanone (MIBK)250 199 ug/Kg 80 34-150
Acetone 250 182 ug/Kg 73 10-150
Benzene 50.0 55.0 ug/Kg 110 70-130
Bromobenzene 50.0 51.0 ug/Kg 102 70-130
Bromoform 50.0 42.3 ug/Kg 85 68-130
Bromomethane 50.0 60.2 ug/Kg 120 70-130
Carbon disulfide 50.0 67.8 *+ ug/Kg 136 70-130
Carbon tetrachloride 50.0 51.6 ug/Kg 103 70-130
Chlorobenzene 50.0 52.2 ug/Kg 104 70-130
Chlorobromomethane 50.0 56.4 ug/Kg 113 66-130
Chlorodibromomethane 50.0 49.8 ug/Kg 100 64-133
Chloroethane 50.0 51.5 ug/Kg 103 70-130
Chloroform 50.0 51.1 ug/Kg 102 70-130
Chloromethane 50.0 31.2 *- ug/Kg 62 70-130
cis-1,2-Dichloroethene 50.0 51.6 ug/Kg 103 70-130
cis-1,3-Dichloropropene 50.0 50.2 ug/Kg 100 70-130
Dibromomethane 50.0 51.3 ug/Kg 103 59-142
Dichlorobromomethane 50.0 48.6 ug/Kg 97 70-130
Dichlorodifluoromethane 50.0 34.3 ug/Kg 69 43-131
Ethylbenzene 50.0 50.8 ug/Kg 102 70-130
Ethylene Dibromide 50.0 50.0 ug/Kg 100 48-150
Hexachlorobutadiene 50.0 49.3 ug/Kg 99 70-130
Isopropylbenzene 50.0 52.0 ug/Kg 104 70-130
Methyl tert-butyl ether 50.0 48.3 ug/Kg 97 70-130
Methylene Chloride 50.0 52.4 ug/Kg 105 54-149
m-Xylene & p-Xylene 50.0 50.4 ug/Kg 101 70-130
Naphthalene 50.0 38.1 ug/Kg 76 46-150
n-Butylbenzene 50.0 49.2 ug/Kg 98 70-130
N-Propylbenzene 50.0 51.2 ug/Kg 102 70-130
o-Xylene 50.0 50.2 ug/Kg 100 70-130
sec-Butylbenzene 50.0 51.7 ug/Kg 103 69-142
Styrene 50.0 51.1 ug/Kg 102 70-130
tert-Butylbenzene 50.0 50.7 ug/Kg 101 67-145
Tetrachloroethene 50.0 56.4 ug/Kg 113 70-130
Toluene 50.0 55.2 ug/Kg 110 70-130
trans-1,2-Dichloroethene 50.0 56.2 ug/Kg 112 67-130
trans-1,3-Dichloropropene 50.0 50.4 ug/Kg 101 54-150
Trichloroethene 50.0 55.0 ug/Kg 110 70-130
Trichlorofluoromethane 50.0 50.1 ug/Kg 100 70-130
Vinyl chloride 50.0 40.9 ug/Kg 82 70-130
Xylenes, Total 100 101 ug/Kg 101 70-130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)65 -130
106Dibromofluoromethane (Surr)65 -130
102Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-765882/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
1,1,1,2-Tetrachloroethane 50.0 51.4 ug/Kg 103 70-130 2 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 50.4 ug/Kg 101 70-130 0 30
1,1,2,2-Tetrachloroethane 50.0 44.3 ug/Kg 89 64-130 5 30
1,1,2-Trichloroethane 50.0 49.8 ug/Kg 100 56-146 4 30
1,1-Dichloroethane 50.0 52.9 ug/Kg 106 70-130 1 30
1,1-Dichloroethene 50.0 47.5 ug/Kg 95 69-130 14 50
1,1-Dichloropropene 50.0 53.9 ug/Kg 108 70-130 1 30
1,2,3-Trichlorobenzene 50.0 43.6 ug/Kg 87 70-130 1 30
1,2,3-Trichloropropane 50.0 44.5 ug/Kg 89 64-130 6 30
1,2,4-Trichlorobenzene 50.0 46.0 ug/Kg 92 70-130 0 30
1,2,4-Trimethylbenzene 50.0 51.4 ug/Kg 103 70-130 1 30
1,2-Dibromo-3-Chloropropane 50.0 34.7 ug/Kg 69 42-145 3 30
1,2-Dichlorobenzene 50.0 49.9 ug/Kg 100 70-130 0 30
1,2-Dichloroethane 50.0 50.0 ug/Kg 100 68-139 3 30
1,2-Dichloropropane 50.0 53.5 ug/Kg 107 70-130 2 30
1,3,5-Trimethylbenzene 50.0 51.1 ug/Kg 102 70-130 2 30
1,3-Dichlorobenzene 50.0 50.9 ug/Kg 102 70-130 0 30
1,3-Dichloropropane 50.0 51.6 ug/Kg 103 54-150 3 30
1,4-Dichlorobenzene 50.0 50.9 ug/Kg 102 70-130 2 30
2,2-Dichloropropane 50.0 50.1 ug/Kg 100 70-130 1 30
2-Butanone (MEK)250 188 ug/Kg 75 40-150 4 30
2-Chlorotoluene 50.0 51.1 ug/Kg 102 70-130 2 30
2-Hexanone 250 193 ug/Kg 77 30-150 4 30
4-Chlorotoluene 50.0 46.1 ug/Kg 92 70-130 1 30
4-Isopropyltoluene 50.0 49.0 ug/Kg 98 70-130 2 30
4-Methyl-2-pentanone (MIBK)250 203 ug/Kg 81 34-150 2 30
Acetone 250 161 ug/Kg 64 10-150 12 50
Benzene 50.0 56.4 ug/Kg 113 70-130 2 30
Bromobenzene 50.0 53.1 ug/Kg 106 70-130 4 30
Bromoform 50.0 45.1 ug/Kg 90 68-130 6 30
Bromomethane 50.0 60.6 ug/Kg 121 70-130 1 30
Carbon disulfide 50.0 57.6 ug/Kg 115 70-130 16 30
Carbon tetrachloride 50.0 51.6 ug/Kg 103 70-130 0 30
Chlorobenzene 50.0 53.6 ug/Kg 107 70-130 3 30
Chlorobromomethane 50.0 58.2 ug/Kg 116 66-130 3 30
Chlorodibromomethane 50.0 50.5 ug/Kg 101 64-133 1 30
Chloroethane 50.0 51.8 ug/Kg 104 70-130 1 30
Chloroform 50.0 51.8 ug/Kg 104 70-130 1 30
Chloromethane 50.0 31.8 *- ug/Kg 64 70-130 2 30
cis-1,2-Dichloroethene 50.0 53.3 ug/Kg 107 70-130 3 30
cis-1,3-Dichloropropene 50.0 51.0 ug/Kg 102 70-130 2 30
Eurofins Raleigh
Page 16 of 38 3/14/2023
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-765882/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765882
Dibromomethane 50.0 52.8 ug/Kg 106 59-142 3 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Dichlorobromomethane 50.0 49.8 ug/Kg 100 70-130 3 30
Dichlorodifluoromethane 50.0 34.5 ug/Kg 69 43-131 1 30
Ethylbenzene 50.0 52.2 ug/Kg 104 70-130 3 30
Ethylene Dibromide 50.0 51.5 ug/Kg 103 48-150 3 30
Hexachlorobutadiene 50.0 49.1 ug/Kg 98 70-130 0 30
Isopropylbenzene 50.0 52.4 ug/Kg 105 70-130 1 30
Methyl tert-butyl ether 50.0 50.3 ug/Kg 101 70-130 4 30
Methylene Chloride 50.0 50.7 ug/Kg 101 54-149 3 30
m-Xylene & p-Xylene 50.0 50.9 ug/Kg 102 70-130 1 30
Naphthalene 50.0 38.8 ug/Kg 78 46-150 2 30
n-Butylbenzene 50.0 48.3 ug/Kg 97 70-130 2 30
N-Propylbenzene 50.0 51.5 ug/Kg 103 70-130 1 30
o-Xylene 50.0 51.5 ug/Kg 103 70-130 2 30
sec-Butylbenzene 50.0 52.0 ug/Kg 104 69-142 1 30
Styrene 50.0 53.3 ug/Kg 107 70-130 4 30
tert-Butylbenzene 50.0 51.8 ug/Kg 104 67-145 2 30
Tetrachloroethene 50.0 57.3 ug/Kg 115 70-130 2 30
Toluene 50.0 55.3 ug/Kg 111 70-130 0 30
trans-1,2-Dichloroethene 50.0 57.1 ug/Kg 114 67-130 2 30
trans-1,3-Dichloropropene 50.0 51.3 ug/Kg 103 54-150 2 30
Trichloroethene 50.0 56.3 ug/Kg 113 70-130 2 30
Trichlorofluoromethane 50.0 45.6 ug/Kg 91 70-130 9 30
Vinyl chloride 50.0 43.1 ug/Kg 86 70-130 5 30
Xylenes, Total 100 102 ug/Kg 102 70-130 2 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)65 -130
109Dibromofluoromethane (Surr)65 -130
104Toluene-d8 (Surr)65 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-765985/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
RL MDL
1,2,4-Trichlorobenzene ND 320 30 ug/Kg 03/03/23 16:20 03/08/23 18:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 36320 ug/Kg 03/03/23 16:20 03/08/23 18:45 11,2-Dichlorobenzene
ND 33320 ug/Kg 03/03/23 16:20 03/08/23 18:45 11,3-Dichlorobenzene
ND 34320 ug/Kg 03/03/23 16:20 03/08/23 18:45 11,4-Dichlorobenzene
ND 30320 ug/Kg 03/03/23 16:20 03/08/23 18:45 11-Methylnaphthalene
ND 34320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,4,5-Trichlorophenol
ND 28320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,4,6-Trichlorophenol
ND 34320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,4-Dichlorophenol
ND 43320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,4-Dimethylphenol
ND 8101600 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,4-Dinitrophenol
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-765985/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
RL MDL
2,4-Dinitrotoluene ND 320 48 ug/Kg 03/03/23 16:20 03/08/23 18:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 41320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12,6-Dinitrotoluene
ND 34320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Chloronaphthalene
ND 39320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Chlorophenol
ND 37320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Methylnaphthalene
ND 26320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Methylphenol
ND 441600 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Nitroaniline
ND 40320 ug/Kg 03/03/23 16:20 03/08/23 18:45 12-Nitrophenol
ND 42320 ug/Kg 03/03/23 16:20 03/08/23 18:45 13 & 4 Methylphenol
ND 27640 ug/Kg 03/03/23 16:20 03/08/23 18:45 13,3'-Dichlorobenzidine
ND 451600 ug/Kg 03/03/23 16:20 03/08/23 18:45 13-Nitroaniline
ND 1601600 ug/Kg 03/03/23 16:20 03/08/23 18:45 14,6-Dinitro-2-methylphenol
ND 35320 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Bromophenyl phenyl ether
ND 34320 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Chloro-3-methylphenol
ND 50640 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Chloroaniline
ND 43320 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Chlorophenyl phenyl ether
ND 481600 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Nitroaniline
ND 3201600 ug/Kg 03/03/23 16:20 03/08/23 18:45 14-Nitrophenol
ND 40320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Acenaphthene
ND 35320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Acenaphthylene
ND 24320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Anthracene
ND 8102600 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzidine
ND 26320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzo[a]anthracene
ND 50320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzo[a]pyrene
ND 37320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzo[b]fluoranthene
ND 21320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzo[g,h,i]perylene
ND 63320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzo[k]fluoranthene
ND 8101600 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzoic acid
ND 32320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Benzyl alcohol
ND 29320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1bis (2-chloroisopropyl) ether
ND 38320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Bis(2-chloroethoxy)methane
ND 44320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Bis(2-chloroethyl)ether
ND 28320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Bis(2-ethylhexyl) phthalate
ND 25320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Butyl benzyl phthalate
ND 20320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Chrysene
ND 38320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Dibenz(a,h)anthracene
ND 32320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Dibenzofuran
ND 36320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Diethyl phthalate
ND 33320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Dimethyl phthalate
ND 29320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Di-n-butyl phthalate
ND 28320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Di-n-octyl phthalate
ND 40320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Diphenylamine
ND 31320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Fluoranthene
ND 35320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Fluorene
ND 38320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Hexachlorobenzene
ND 35320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Hexachlorobutadiene
ND 40320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Hexachlorocyclopentadiene
ND 27320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Hexachloroethane
ND 27320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Indeno[1,2,3-cd]pyrene
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-765985/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
RL MDL
Isophorone ND 320 32 ug/Kg 03/03/23 16:20 03/08/23 18:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 29320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Naphthalene
ND 25320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Nitrobenzene
ND 120320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1N-Nitrosodimethylamine
ND 31320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1N-Nitrosodi-n-propylamine
ND 32320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1N-Nitrosodiphenylamine
ND 3201600 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Pentachlorophenol
ND 26320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Phenanthrene
ND 33320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Phenol
ND 26320 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Pyrene
ND 320640 ug/Kg 03/03/23 16:20 03/08/23 18:45 1Pyridine
2,4,6-Tribromophenol (Surr)77 21-132 03/08/23 18:45 1
MB MB
Surrogate
03/03/23 16:20
Dil FacPrepared AnalyzedQualifier Limits%Recovery
72 03/03/23 16:20 03/08/23 18:45 12-Fluorobiphenyl (Surr)25-130
70 03/03/23 16:20 03/08/23 18:45 12-Fluorophenol (Surr)18-130
61 03/03/23 16:20 03/08/23 18:45 1Nitrobenzene-d5 (Surr)19-130
69 03/03/23 16:20 03/08/23 18:45 1Phenol-d5 (Surr)21-130
102 03/03/23 16:20 03/08/23 18:45 1Terphenyl-d14 (Surr)31-133
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-765985/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
1,2,4-Trichlorobenzene 6500 4430 ug/Kg 68 20-130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichlorobenzene 6500 4070 ug/Kg 63 20-130
1,3-Dichlorobenzene 6500 4000 ug/Kg 62 18-130
1,4-Dichlorobenzene 6500 3930 ug/Kg 60 19-130
1-Methylnaphthalene 6500 4570 ug/Kg 70 28-130
2,4,5-Trichlorophenol 6500 5850 ug/Kg 90 33-130
2,4,6-Trichlorophenol 6500 6110 ug/Kg 94 31-130
2,4-Dichlorophenol 6500 5450 ug/Kg 84 30-130
2,4-Dimethylphenol 6500 4640 ug/Kg 71 34-130
2,4-Dinitrophenol 13000 16000 ug/Kg 123 10-130
2,4-Dinitrotoluene 6500 6520 ug/Kg 100 34-130
2,6-Dinitrotoluene 6500 5860 ug/Kg 90 33-130
2-Chloronaphthalene 6500 4790 ug/Kg 74 30-130
2-Chlorophenol 6500 4630 ug/Kg 71 28-130
2-Methylnaphthalene 6500 5050 ug/Kg 78 28-130
2-Methylphenol 6500 4740 ug/Kg 73 30-130
2-Nitroaniline 6500 5830 ug/Kg 90 26-130
2-Nitrophenol 6500 5870 ug/Kg 90 24-130
3 & 4 Methylphenol 6500 5020 ug/Kg 77 31-130
3,3'-Dichlorobenzidine 6500 5250 ug/Kg 81 10-130
3-Nitroaniline 6500 5560 ug/Kg 85 10-130
4,6-Dinitro-2-methylphenol 13000 16200 ug/Kg 125 22-130
4-Bromophenyl phenyl ether 6500 5330 ug/Kg 82 32-130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-765985/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
4-Chloro-3-methylphenol 6500 5610 ug/Kg 86 31-130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
4-Chloroaniline 6500 4430 ug/Kg 68 10-130
4-Chlorophenyl phenyl ether 6500 5240 ug/Kg 81 32-130
4-Nitroaniline 6500 6120 ug/Kg 94 25-130
4-Nitrophenol 13000 13800 ug/Kg 106 25-130
Acenaphthene 6500 5260 ug/Kg 81 33-130
Acenaphthylene 6500 5470 ug/Kg 84 34-130
Anthracene 6500 5480 ug/Kg 84 39-130
Benzidine 6500 3650 ug/Kg 56 10-130
Benzo[a]anthracene 6500 6400 ug/Kg 98 40-130
Benzo[a]pyrene 6500 6090 ug/Kg 94 37-131
Benzo[b]fluoranthene 6500 6770 ug/Kg 104 35-130
Benzo[g,h,i]perylene 6500 5840 ug/Kg 90 39-130
Benzo[k]fluoranthene 6500 5450 ug/Kg 84 35-130
Benzoic acid 6500 6180 ug/Kg 95 10-139
Benzyl alcohol 6500 4590 ug/Kg 71 19-130
bis (2-chloroisopropyl) ether 6500 4190 ug/Kg 64 12-130
Bis(2-chloroethoxy)methane 6500 4680 ug/Kg 72 29-130
Bis(2-chloroethyl)ether 6500 4080 ug/Kg 63 18-130
Bis(2-ethylhexyl) phthalate 6500 6370 ug/Kg 98 39-130
Butyl benzyl phthalate 6500 6870 ug/Kg 106 38-130
Chrysene 6500 5480 ug/Kg 84 40-130
Dibenz(a,h)anthracene 6500 6480 ug/Kg 100 37-130
Dibenzofuran 6500 5070 ug/Kg 78 34-130
Diethyl phthalate 6500 5680 ug/Kg 87 36-130
Dimethyl phthalate 6500 5530 ug/Kg 85 36-130
Di-n-butyl phthalate 6500 6190 ug/Kg 95 39-130
Di-n-octyl phthalate 6500 6350 ug/Kg 98 38-131
Diphenylamine 5560 4530 ug/Kg 82 51-130
Fluoranthene 6500 5990 ug/Kg 92 38-130
Fluorene 6500 5190 ug/Kg 80 34-130
Hexachlorobenzene 6500 5500 ug/Kg 85 28-130
Hexachlorobutadiene 6500 4360 ug/Kg 67 22-130
Hexachlorocyclopentadiene 6500 4540 ug/Kg 70 11-130
Hexachloroethane 6500 3940 ug/Kg 61 21-130
Indeno[1,2,3-cd]pyrene 6500 5920 ug/Kg 91 40-130
Isophorone 6500 4640 ug/Kg 71 26-130
Naphthalene 6500 4450 ug/Kg 68 25-130
Nitrobenzene 6500 4370 ug/Kg 67 25-130
N-Nitrosodimethylamine 6500 3770 ug/Kg 58 20-130
N-Nitrosodi-n-propylamine 6500 4320 ug/Kg 66 24-130
N-Nitrosodiphenylamine 6500 5310 ug/Kg 82 37-130
Pentachlorophenol 13000 13100 ug/Kg 100 16-135
Phenanthrene 6500 5400 ug/Kg 83 38-130
Phenol 6500 4790 ug/Kg 74 27-130
Pyrene 6500 6520 ug/Kg 100 40-130
Pyridine 13000 6930 ug/Kg 53 10-130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-765985/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
702-Fluorobiphenyl (Surr)25 -130
652-Fluorophenol (Surr)18 -130
62Nitrobenzene-d5 (Surr)19 -130
69Phenol-d5 (Surr)21 -130
92Terphenyl-d14 (Surr)31 -133
Client Sample ID: SS-B1Lab Sample ID: 752-3710-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
1,2,4-Trichlorobenzene ND 7430 4930 ug/Kg 66 20-130☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,2-Dichlorobenzene ND 7430 4520 ug/Kg 61 20-130☼
1,3-Dichlorobenzene ND 7430 4390 ug/Kg 59 18-130☼
1,4-Dichlorobenzene ND 7430 4410 ug/Kg 59 19-130☼
1-Methylnaphthalene ND 7430 5090 ug/Kg 68 28-130☼
2,4,5-Trichlorophenol ND 7430 6460 ug/Kg 87 33-130☼
2,4,6-Trichlorophenol ND 7430 6760 ug/Kg 91 31-130☼
2,4-Dichlorophenol ND 7430 6080 ug/Kg 82 30-130☼
2,4-Dimethylphenol ND 7430 5340 ug/Kg 72 34-130☼
2,4-Dinitrophenol ND F1 14900 20300 F1 ug/Kg 136 10-130☼
2,4-Dinitrotoluene ND 7430 7280 ug/Kg 98 34-130☼
2,6-Dinitrotoluene ND 7430 6500 ug/Kg 87 33-130☼
2-Chloronaphthalene ND 7430 5280 ug/Kg 71 30-130☼
2-Chlorophenol ND 7430 5310 ug/Kg 71 28-130☼
2-Methylnaphthalene ND 7430 5590 ug/Kg 75 28-130☼
2-Methylphenol ND 7430 5280 ug/Kg 71 30-130☼
2-Nitroaniline ND 7430 6450 ug/Kg 87 26-130☼
2-Nitrophenol ND 7430 6480 ug/Kg 87 24-130☼
3 & 4 Methylphenol ND 7430 5580 ug/Kg 75 31-130☼
3,3'-Dichlorobenzidine ND 7430 5210 ug/Kg 70 10-130☼
3-Nitroaniline ND 7430 6120 ug/Kg 82 10-130☼
4,6-Dinitro-2-methylphenol ND 14900 19100 ug/Kg 129 22-130☼
4-Bromophenyl phenyl ether ND 7430 5920 ug/Kg 80 32-130☼
4-Chloro-3-methylphenol ND 7430 6380 ug/Kg 86 31-130☼
4-Chloroaniline ND 7430 4730 ug/Kg 64 10-130☼
4-Chlorophenyl phenyl ether ND 7430 5740 ug/Kg 77 32-130☼
4-Nitroaniline ND 7430 6200 ug/Kg 83 25-130☼
4-Nitrophenol ND 14900 15500 ug/Kg 104 25-130☼
Acenaphthene ND 7430 5850 ug/Kg 79 33-130☼
Acenaphthylene ND 7430 5940 ug/Kg 80 34-130☼
Anthracene ND 7430 6110 ug/Kg 82 39-130☼
Benzidine ND F1 7430 ND F1 ug/Kg 0 10-130☼
Benzo[a]anthracene ND 7430 7090 ug/Kg 95 40-130☼
Benzo[a]pyrene ND 7430 6760 ug/Kg 91 37-131☼
Benzo[b]fluoranthene ND 7430 7340 ug/Kg 99 35-130☼
Benzo[g,h,i]perylene ND 7430 6480 ug/Kg 87 39-130☼
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SS-B1Lab Sample ID: 752-3710-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
Benzo[k]fluoranthene ND 7430 6030 ug/Kg 81 35-130☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Benzoic acid ND 7430 9530 ug/Kg 128 10-139☼
Benzyl alcohol ND 7430 5390 ug/Kg 73 19-130☼
bis (2-chloroisopropyl) ether ND 7430 4690 ug/Kg 63 12-130☼
Bis(2-chloroethoxy)methane ND 7430 5050 ug/Kg 68 29-130☼
Bis(2-chloroethyl)ether ND 7430 4580 ug/Kg 62 18-130☼
Bis(2-ethylhexyl) phthalate 250 J 7430 7130 ug/Kg 93 39-130☼
Butyl benzyl phthalate ND 7430 7770 ug/Kg 105 38-130☼
Chrysene ND 7430 6000 ug/Kg 81 40-130☼
Dibenz(a,h)anthracene ND 7430 7010 ug/Kg 94 37-130☼
Dibenzofuran ND 7430 5480 ug/Kg 74 34-130☼
Diethyl phthalate ND 7430 6090 ug/Kg 82 36-130☼
Dimethyl phthalate ND 7430 5920 ug/Kg 80 36-130☼
Di-n-butyl phthalate ND 7430 6830 ug/Kg 92 39-130☼
Di-n-octyl phthalate ND 7430 6930 ug/Kg 93 38-131☼
Diphenylamine ND 6360 5060 ug/Kg 80 51-130☼
Fluoranthene ND 7430 6560 ug/Kg 88 38-130☼
Fluorene ND 7430 5720 ug/Kg 77 34-130☼
Hexachlorobenzene ND 7430 6060 ug/Kg 82 28-130☼
Hexachlorobutadiene ND 7430 4850 ug/Kg 65 22-130☼
Hexachlorocyclopentadiene ND 7430 5080 ug/Kg 68 11-130☼
Hexachloroethane ND 7430 4460 ug/Kg 60 21-130☼
Indeno[1,2,3-cd]pyrene ND 7430 6700 ug/Kg 90 40-130☼
Isophorone ND 7430 5220 ug/Kg 70 26-130☼
Naphthalene ND 7430 4860 ug/Kg 65 25-130☼
Nitrobenzene ND 7430 4870 ug/Kg 65 25-130☼
N-Nitrosodimethylamine ND 7430 4280 ug/Kg 58 20-130☼
N-Nitrosodi-n-propylamine ND 7430 4840 ug/Kg 65 24-130☼
N-Nitrosodiphenylamine ND 7430 5920 ug/Kg 80 37-130☼
Pentachlorophenol ND 14900 14800 ug/Kg 100 16-135☼
Phenanthrene ND 7430 5970 ug/Kg 80 38-130☼
Phenol ND 7430 5400 ug/Kg 73 27-130☼
Pyrene ND 7430 7290 ug/Kg 98 40-130☼
Pyridine ND 14900 1900 ug/Kg 13 10-130☼
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
85
MS MS
Qualifier Limits%Recovery
642-Fluorobiphenyl (Surr)25 -130
652-Fluorophenol (Surr)18 -130
61Nitrobenzene-d5 (Surr)19 -130
67Phenol-d5 (Surr)21 -130
91Terphenyl-d14 (Surr)31 -133
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SS-B1Lab Sample ID: 752-3710-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
1,2,4-Trichlorobenzene ND 7480 4850 ug/Kg 65 20-130 2 50☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,2-Dichlorobenzene ND 7480 4570 ug/Kg 61 20-130 1 50☼
1,3-Dichlorobenzene ND 7480 4370 ug/Kg 58 18-130 0 50☼
1,4-Dichlorobenzene ND 7480 4370 ug/Kg 58 19-130 1 50☼
1-Methylnaphthalene ND 7480 5140 ug/Kg 69 28-130 1 50☼
2,4,5-Trichlorophenol ND 7480 6760 ug/Kg 90 33-130 5 50☼
2,4,6-Trichlorophenol ND 7480 7000 ug/Kg 94 31-130 3 50☼
2,4-Dichlorophenol ND 7480 6270 ug/Kg 84 30-130 3 50☼
2,4-Dimethylphenol ND 7480 5390 ug/Kg 72 34-130 1 50☼
2,4-Dinitrophenol ND F1 15000 20400 F1 ug/Kg 137 10-130 1 50☼
2,4-Dinitrotoluene ND 7480 7370 ug/Kg 99 34-130 1 50☼
2,6-Dinitrotoluene ND 7480 6700 ug/Kg 90 33-130 3 50☼
2-Chloronaphthalene ND 7480 5480 ug/Kg 73 30-130 4 50☼
2-Chlorophenol ND 7480 5360 ug/Kg 72 28-130 1 50☼
2-Methylnaphthalene ND 7480 5680 ug/Kg 76 28-130 2 50☼
2-Methylphenol ND 7480 5310 ug/Kg 71 30-130 1 50☼
2-Nitroaniline ND 7480 6830 ug/Kg 91 26-130 6 50☼
2-Nitrophenol ND 7480 6600 ug/Kg 88 24-130 2 50☼
3 & 4 Methylphenol ND 7480 5860 ug/Kg 78 31-130 5 50☼
3,3'-Dichlorobenzidine ND 7480 5440 ug/Kg 73 10-130 4 50☼
3-Nitroaniline ND 7480 6200 ug/Kg 83 10-130 1 50☼
4,6-Dinitro-2-methylphenol ND 15000 19400 ug/Kg 130 22-130 2 50☼
4-Bromophenyl phenyl ether ND 7480 6070 ug/Kg 81 32-130 2 50☼
4-Chloro-3-methylphenol ND 7480 6510 ug/Kg 87 31-130 2 50☼
4-Chloroaniline ND 7480 4940 ug/Kg 66 10-130 4 50☼
4-Chlorophenyl phenyl ether ND 7480 5910 ug/Kg 79 32-130 3 50☼
4-Nitroaniline ND 7480 6060 ug/Kg 81 25-130 2 50☼
4-Nitrophenol ND 15000 15500 ug/Kg 104 25-130 0 50☼
Acenaphthene ND 7480 6090 ug/Kg 81 33-130 4 50☼
Acenaphthylene ND 7480 6180 ug/Kg 83 34-130 4 50☼
Anthracene ND 7480 6280 ug/Kg 84 39-130 3 50☼
Benzidine ND F1 7480 ND F1 ug/Kg 0 10-130 NC 50☼
Benzo[a]anthracene ND 7480 7240 ug/Kg 97 40-130 2 50☼
Benzo[a]pyrene ND 7480 7010 ug/Kg 94 37-131 4 50☼
Benzo[b]fluoranthene ND 7480 7700 ug/Kg 103 35-130 5 50☼
Benzo[g,h,i]perylene ND 7480 6710 ug/Kg 90 39-130 4 50☼
Benzo[k]fluoranthene ND 7480 6170 ug/Kg 83 35-130 2 50☼
Benzoic acid ND 7480 8720 ug/Kg 117 10-139 9 50☼
Benzyl alcohol ND 7480 5480 ug/Kg 73 19-130 2 50☼
bis (2-chloroisopropyl) ether ND 7480 4680 ug/Kg 63 12-130 0 50☼
Bis(2-chloroethoxy)methane ND 7480 5080 ug/Kg 68 29-130 1 50☼
Bis(2-chloroethyl)ether ND 7480 4470 ug/Kg 60 18-130 2 50☼
Bis(2-ethylhexyl) phthalate 250 J 7480 7310 ug/Kg 94 39-130 2 50☼
Butyl benzyl phthalate ND 7480 7870 ug/Kg 105 38-130 1 50☼
Chrysene ND 7480 6110 ug/Kg 82 40-130 2 50☼
Dibenz(a,h)anthracene ND 7480 7460 ug/Kg 100 37-130 6 50☼
Dibenzofuran ND 7480 5630 ug/Kg 75 34-130 3 50☼
Diethyl phthalate ND 7480 6280 ug/Kg 84 36-130 3 50☼
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SS-B1Lab Sample ID: 752-3710-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766626 Prep Batch: 765985
Dimethyl phthalate ND 7480 6080 ug/Kg 81 36-130 3 50☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Di-n-butyl phthalate ND 7480 7110 ug/Kg 95 39-130 4 50☼
Di-n-octyl phthalate ND 7480 7190 ug/Kg 96 38-131 4 50☼
Diphenylamine ND 6390 5210 ug/Kg 82 51-130 3 50☼
Fluoranthene ND 7480 6760 ug/Kg 90 38-130 3 50☼
Fluorene ND 7480 5860 ug/Kg 78 34-130 2 50☼
Hexachlorobenzene ND 7480 6220 ug/Kg 83 28-130 3 50☼
Hexachlorobutadiene ND 7480 4720 ug/Kg 63 22-130 3 50☼
Hexachlorocyclopentadiene ND 7480 5180 ug/Kg 69 11-130 2 50☼
Hexachloroethane ND 7480 4430 ug/Kg 59 21-130 1 50☼
Indeno[1,2,3-cd]pyrene ND 7480 6820 ug/Kg 91 40-130 2 50☼
Isophorone ND 7480 5310 ug/Kg 71 26-130 2 50☼
Naphthalene ND 7480 4820 ug/Kg 64 25-130 1 50☼
Nitrobenzene ND 7480 4850 ug/Kg 65 25-130 0 50☼
N-Nitrosodimethylamine ND 7480 4390 ug/Kg 59 20-130 2 50☼
N-Nitrosodi-n-propylamine ND 7480 4950 ug/Kg 66 24-130 2 50☼
N-Nitrosodiphenylamine ND 7480 6130 ug/Kg 82 37-130 4 50☼
Pentachlorophenol ND 15000 15500 ug/Kg 104 16-135 5 50☼
Phenanthrene ND 7480 6090 ug/Kg 81 38-130 2 50☼
Phenol ND 7480 5520 ug/Kg 74 27-130 2 50☼
Pyrene ND 7480 7380 ug/Kg 99 40-130 1 50☼
Pyridine ND 15000 2050 ug/Kg 14 10-130 8 50☼
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
85
MSD MSD
Qualifier Limits%Recovery
662-Fluorobiphenyl (Surr)25 -130
642-Fluorophenol (Surr)18 -130
60Nitrobenzene-d5 (Surr)19 -130
69Phenol-d5 (Surr)21 -130
91Terphenyl-d14 (Surr)31 -133
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-614798/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 614759 Prep Batch: 614798
RL MDL
C5-C8 Aliphatics ND 2.7 2.7 mg/Kg 03/03/23 09:30 03/03/23 15:04 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.41.4 mg/Kg 03/03/23 09:30 03/03/23 15:04 50C9-C12 Aliphatics
ND 0.750.75 mg/Kg 03/03/23 09:30 03/03/23 15:04 50C9-C10 Aromatics
a,a,a-Trifluorotoluene (fid)85 70-130 03/03/23 15:04 50
MB MB
Surrogate
03/03/23 09:30
Dil FacPrepared AnalyzedQualifier Limits%Recovery
85 03/03/23 09:30 03/03/23 15:04 50a,a,a-Trifluorotoluene (pid)70-130
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-614798/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 614759 Prep Batch: 614798
C5-C8 Aliphatics 15.0 11.7 mg/Kg 78 70-130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C9-C12 Aliphatics 17.5 14.1 mg/Kg 81 70-130
C9-C10 Aromatics 2.50 1.98 mg/Kg 79 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
91a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-614798/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 614759 Prep Batch: 614798
C5-C8 Aliphatics 15.0 14.1 mg/Kg 94 70-130 19 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C12 Aliphatics 17.5 16.2 mg/Kg 92 70-130 13 25
C9-C10 Aromatics 2.50 2.27 mg/Kg 91 70-130 14 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
90a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 752-1588/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 1599 Prep Batch: 1588
RL MDL
C11-C22 Aromatics ND 17 3.1 mg/Kg 03/02/23 23:20 03/03/23 11:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 3.117 mg/Kg 03/02/23 23:20 03/03/23 11:20 1C19-C36 Aliphatics
1.86 J 1.317 mg/Kg 03/02/23 23:20 03/03/23 11:20 1C9-C18 Aliphatics
o- terphenyl (Surr)96 40-140 03/03/23 11:20 1
MB MB
Surrogate
03/02/23 23:20
Dil FacPrepared AnalyzedQualifier Limits%Recovery
98 03/02/23 23:20 03/03/23 11:20 11-Chlorooctadecane 40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-1588/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 1599 Prep Batch: 1588
C11-C22 Aromatics 22.7 19.0 mg/Kg 84 40-140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
C19-C36 Aliphatics 21.3 23.1 mg/Kg 108 40-140
C9-C18 Aliphatics 16.0 13.6 J mg/Kg 85 40-140
o- terphenyl (Surr)40 -140
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
Eurofins Raleigh
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QC Sample Results
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-1588/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 1600 Prep Batch: 1588
1-Chlorooctadecane 40 -140
Surrogate
107
LCS LCS
Qualifier Limits%Recovery
Eurofins Raleigh
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QC Association Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
GC/MS VOA
Prep Batch: 765873
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035752-3710-1 SS-B1 Total/NA
Analysis Batch: 765882
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 765873752-3710-1 SS-B1 Total/NA
Solid 8260DMB 680-765882/8 Method Blank Total/NA
Solid 8260DLCS 680-765882/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-765882/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 765985
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546752-3710-1 SS-B1 Total/NA
Solid 3546MB 680-765985/4-A Method Blank Total/NA
Solid 3546LCS 680-765985/5-A Lab Control Sample Total/NA
Solid 3546752-3710-1 MS SS-B1 Total/NA
Solid 3546752-3710-1 MSD SS-B1 Total/NA
Analysis Batch: 766626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 765985752-3710-1 SS-B1 Total/NA
Solid 8270E 765985MB 680-765985/4-A Method Blank Total/NA
Solid 8270E 765985LCS 680-765985/5-A Lab Control Sample Total/NA
Solid 8270E 765985752-3710-1 MS SS-B1 Total/NA
Solid 8270E 765985752-3710-1 MSD SS-B1 Total/NA
GC VOA
Analysis Batch: 614759
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 614798MB 400-614798/1-A Method Blank Total/NA
Solid MAVPH 614798LCS 400-614798/2-A Lab Control Sample Total/NA
Solid MAVPH 614798LCSD 400-614798/3-A Lab Control Sample Dup Total/NA
Prep Batch: 614798
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035752-3710-1 SS-B1 Total/NA
Solid 5035MB 400-614798/1-A Method Blank Total/NA
Solid 5035LCS 400-614798/2-A Lab Control Sample Total/NA
Solid 5035LCSD 400-614798/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 615607
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 614798752-3710-1 SS-B1 Total/NA
GC Semi VOA
Prep Batch: 1588
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C752-3710-1 SS-B1 Total/NA
Solid 3550CMB 752-1588/1-A Method Blank Total/NA
Eurofins Raleigh
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QC Association Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
GC Semi VOA (Continued)
Prep Batch: 1588 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550CLCS 752-1588/2-A Lab Control Sample Total/NA
Analysis Batch: 1599
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAEPH2.1 1588752-3710-1 SS-B1 Total/NA
Solid MAEPH2.1 1588MB 752-1588/1-A Method Blank Total/NA
Solid MAEPH2.1 1588LCS 752-1588/2-A Lab Control Sample Total/NA
Analysis Batch: 1600
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAEPH2.1 1588752-3710-1 SS-B1 Total/NA
Solid MAEPH2.1 1588MB 752-1588/1-A Method Blank Total/NA
Solid MAEPH2.1 1588LCS 752-1588/2-A Lab Control Sample Total/NA
Analysis Batch: 1694
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA EPH SUM752-3710-1 SS-B1 Total/NA
General Chemistry
Analysis Batch: 765888
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture752-3710-1 SS-B1 Total/NA
Eurofins Raleigh
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Lab Chronicle
Client: Mineral Springs Environmental Job ID: 752-3710-1
Project/Site: Country Line Rd
Client Sample ID: SS-B1 Lab Sample ID: 752-3710-1
Matrix: SolidDate Collected: 02/28/23 13:00
Date Received: 03/01/23 15:25
Analysis MA EPH SUM RF1 1694 EET ESC
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA 03/08/23 11:14
Analysis Moisture 1 765888 KG EET SAVTotal/NA 03/03/23 10:52
Client Sample ID: SS-B1 Lab Sample ID: 752-3710-1
Matrix: SolidDate Collected: 02/28/23 13:00
Percent Solids: 87.6Date Received: 03/01/23 15:25
Prep 5035 FES765873 EET SAV
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA 03/03/23 08:52
Analysis 8260D 1 765882 Y1S EET SAVTotal/NA 03/03/23 18:50
Prep 3546 765985 MJ EET SAVTotal/NA 03/03/23 16:20
Analysis 8270E 1 766626 T1C EET SAVTotal/NA 03/08/23 23:22
Prep 5035 614798 SAB EET PENTotal/NA 03/03/23 09:30
Analysis MAVPH 50 615607 SAB EET PENTotal/NA 03/09/23 01:40
Prep 3550C 1588 BR EET ESCTotal/NA 03/02/23 23:20
Analysis MAEPH2.1 1 1599 DM EET ESCTotal/NA 03/03/23 13:01
Prep 3550C 1588 BR EET ESCTotal/NA 03/02/23 23:20
Analysis MAEPH2.1 1 1600 DM EET ESCTotal/NA 03/03/23 13:01
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
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Accreditation/Certification Summary
Client: Mineral Springs Environmental Job ID: 752-3710-1
Project/Site: Country Line Rd
Laboratory: Eurofins Raleigh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 591 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
MA EPH SUM Solid Total EPH
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Alabama State 40150 06-30-23
ANAB ISO/IEC 17025 L2471 02-22-26
Arkansas DEQ State 88-0689 09-01-23
California State 2510 06-30-23
Florida NELAP E81010 06-30-23
Georgia State E81010(FL)06-30-23
Illinois NELAP 200041 10-09-23
Kansas NELAP E-10253 10-31-23
Kentucky (UST) State 53 06-30-23
Louisiana (All) NELAP 30976 06-30-23
Louisiana (DW) State LA017 12-31-23
Maryland State 233 09-30-23
Michigan State 9912 06-30-23
North Carolina (WW/SW) State 314 12-31-23
Oklahoma NELAP 9810 08-31-23
Pennsylvania NELAP 68-00467 01-31-24
South Carolina State 96026 06-30-23
Tennessee State TN02907 06-30-23
Texas NELAP T104704286 09-30-23
US Fish & Wildlife US Federal Programs A22340 06-30-23
USDA US Federal Programs FLGNV23001 01-08-26
USDA US Federal Programs P330-21-00056 05-17-24
Virginia NELAP 460166 06-14-23
West Virginia DEP State 136 03-31-24
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
Eurofins Raleigh
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Method Summary
Job ID: 752-3710-1Client: Mineral Springs Environmental
Project/Site: Country Line Rd
Method Method Description LaboratoryProtocol
SW8468260D Volatile Organic Compounds by GC/MS EET SAV
SW8468270E Semivolatile Organic Compounds (GC/MS)EET SAV
MA DEPMAVPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN
MA DEPMA EPH SUM Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET ESC
MA DEPMAEPH2.1 Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET ESC
EPAMoisture Percent Moisture EET SAV
SW8463546 Microwave Extraction EET SAV
SW8463550C Ultrasonic Extraction EET ESC
SW8465035 Closed System Purge and Trap EET PEN
SW8465035 Closed System Purge and Trap EET SAV
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
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Sample Summary
Client: Mineral Springs Environmental Job ID: 752-3710-1
Project/Site: Country Line Rd
Lab Sample ID Client Sample ID Matrix Collected Received
752-3710-1 SS-B1 Solid 02/28/23 13:00 03/01/23 15:25
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Login Sample Receipt Checklist
Client: Mineral Springs Environmental Job Number: 752-3710-1
Login Number: 3710
Question Answer Comment
Creator: Yonish, Rachel
List Source: Eurofins Raleigh
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
Eurofins Raleigh
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Login Sample Receipt Checklist
Client: Mineral Springs Environmental Job Number: 752-3710-1
Login Number: 3710
Question Answer Comment
Creator: Peckinpaugh, Marshall
List Source: Eurofins Pensacola
List Creation: 03/04/23 11:01 AMList Number: 3
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.3.2°C IR11
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Raleigh
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Login Sample Receipt Checklist
Client: Mineral Springs Environmental Job Number: 752-3710-1
Login Number: 3710
Question Answer Comment
Creator: Harley, Tynisha
List Source: Eurofins Savannah
List Creation: 03/02/23 02:20 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Raleigh
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