FA-29687_48813_CA_LSA_20230426

Resolve Environmental Services PLLC
500 Devonport Drive • Matthews, North Carolina 28104
Phone [phone]
April 26, 2023

Mr. Ken Currie
North Carolina Department of Environmental Quality
Fayetteville Regional Office
225 Green Street, Suite 714
Fayetteville, North Carolina 28301

Re: Limited Site Assessment Report
Express Lane Petro
8931 US Highway 52 North
Ansonville, Anson County, North Carolina
Incident Number: 48813

Dear Mr. Currie:

Please find the attached LSA report for the above-referenced site located in Ansonville, Anson County,
North Carolina.

Should you have any questions or comments, please do not hesitate to contact me at [phone] or
by email to [e-mail].
Sincerely,
Resolve Environmental Services, PLLC

Laura Minor
Project Manager

enclosure

500 Devonport Drive, Matthews NC 28104
Email: [e-mail]
Phone: [phone]
Limited Site Assessment Report
Express Lane Petro
8931 US Highway 52 North
Ansonville, Anson County
North Carolina 28007
Facility ID Number: 0-00-0000026041
Incident Number: 48813

Prepared for:

Gook Yun Knapp
11502 Destin Lane
Charlotte, North Carolina 28277-1208

April 26, 2023

Laura Minor
Project Manager
Terry Kennedy, P.G.

___________________________________________________________________________________________
Prepared by: Resolve Environmental Services Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
i
EXECUTIVE SUMMARY
Express Lane Petro operates as a fuel station and convenience store. The site is located at 8931 US
Highway 52 North in Ansonville, Anson County, North Carolina. The adjoining properties are commercial
and residential. Municipal water is available to the site. The site contains one (1) UST basin and three (3)
fuel dispensers. One (1) 8,000-gallon and two (2) 4,000-gallon gasoline USTs are currently located on site.

Based on information provided by the NCDEQ incident manager, an LSA was required at the site based on
site check results conducted in 2022 by a previous consultant.

A previous release (Incident Number 11109; “Sweetie’s Express Lane”) was reported at the site in 1993
during UST system upgrading. Six (6) former USTs (3 registered, 3 orphaned) and associated piping and
dispensers were reportedly removed in 1999. Assessment activities conducted at the site were
subsequently conducted. No receptors were identified during previous LSA activities. Only the
concentration of lead in ground water exceeded the MACs. Based on a subsequent resampling of the on-
site monitoring well, the lead concentration was non-detect. The incident was granted a NFA in February
2002.

A Type II Monitoring well (MW-1A) was installed adjacent to the previously damaged (and subsequently
replaced) spill buckets at the site on March 6, 2023. Soil samples were collected at appropriate intervals
for analyses by SW-846 Method 8260 and MADEP VPH. Concentrations of benzene, toluene, xylenes,
naphthalene, isopropylbenzene, methylene chloride, C5-C8 aliphatics and C9-C10 aromatics that
exceeded the soil-to-water MSCCs were reported in the soil sample MW-1A-5’. The concentration of C5-
C8 aliphatics exceeded the residential MSCC.

A ground water quality sample was collected from the monitoring well (MW-1A) on March 8, 2023 and
submitted for laboratory analyses for EPA Method 6200B plus oxygenates, EDB by EPA Method 504.1,
lead and MADEP VPH. Concentrations of benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics and
C9-C10 aromatics exceeded the ground water quality standards specified in 15A NCAC 2L .0202. None of
the reported concentrations exceeded the gross contamination levels, if published.

Resolve personnel conducted a receptor survey of all properties within 1,500 feet of the site in March
2023 to verify the 2001 receptor survey information. No receptors, including water supply wells were
identified within 1,500 feet of the site. A pond is located approximately 650 feet west of the site.

Based on the ground water quality data and the receptor survey, the incident meets the NCDEQ criteria
for a low-risk classification. The incident should be closed following deed recordation of a Notice of
Residual Petroleum and associated public notice.

___________________________________________________________________________________________
Prepared by: Resolve Environmental Services Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
ii
SITE INFORMATION
1. Site Identification
 Express Lane Petro (Facility ID 0-00-0000026041)
 Incident Number 48813 – Low Risk
 Location of Source Area: 8931 US Highway 52 North
Ansonville, NC 28007
Anson County (Figures 1 and 2A)
36. 34.981265°N, 80.549706°W (Google Earth)
2. Information about Contacts Associated with the Leaking UST System
UST/AST Owner
Gook Yun Knapp
11502 Destin Lane
Charlotte, NC 28277-1208

UST/AST Operator
Express Lane Petro
8931 US Highway 52 North
Ansonville, NC 28007

Property Owner
Gook Yun Knapp
11502 Destin Lane
Charlotte, NC 28277-1208

Property Occupant
Express Lane Petro
8931 US Highway 52 North
Ansonville, NC 28007

Consultant/Contractor
Resolve Environmental Services,
PLLC
500 Devonport Drive
Matthews, NC 28104
704.289.5881

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217

3. Information about Release
Release was reported on December 30, 2022
An unknown volume of gasoline was released from a leaking spill bucket

CERTIFICATION
I, Terry Kennedy, a Licensed Geologist for Resolve Environmental Services, PLLC, do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Resolve Environmental Services is licensed to practice geology in North Carolina. The certification number of
the corporation is C-416.

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
iv
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iv
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................7
6. LIMITATIONS ........................................................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Land Use Map
Figure 3: Site Map
Figure 4: Soil Quality Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Anson County Parcel Information
Appendix B: Well Construction Record and Subsurface Log
Appendix C: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A
If YES, describe.

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Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
2
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility in the near future.
7. What is the zoning status of the property?

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Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
3
According to the Town of Ansonville Zoning Map, the site is zoned G-B General Business.
8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store in the near future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is located approximately 450 feet northwest of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

The Ansonville Methodist Church is located approximately 270 feet southwest of the source area
at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Ansonville Zoning Map, the surrounding areas are zoned G-B General Business
and R-1 and R-A (Residential, Residential-Agricultural).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, public/institutional and residential.
Land use information has been included as Table 3. A zoning map has been included as Figure
2B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on March 8, 2023. No potable or non-potable wells were
identified within the appropriate search radii of 1,500, 1,000 and 250 feet of the source area. A
Site Location Map is provided as Figure 1 and a Site Vicinity Map showing property boundaries for
the site and surrounding properties has been included as Figure 2A. Water supply well
information has been provided in Table 4. Distributed water use questionnaires have yet to be
returned.

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
4

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by Anson County.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
One pond is located approximately 650 feet west of the site.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On April 10, 2023, Resolve personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along US 52 and several underground utility lines were
observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners
are attached as Appendix A.

3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Carolina Slate Belt. The
bedrock is generally described as meta-mudstone and meta-argillite. The soil samples collected during
well installation activities was gray to black silt. PWR was encountered at a depth of approximately 8-9
feet. Competent argillite was encountered at an approximate depth of 9 feet and was dry. A water bearing
fracture was encountered at approximately 37 feet in depth. The potentiometric surface, measured in
MW-1A on March 8, 2023, was 22.07 feet. A copy of the well construction record and subsurface log have

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
5
been included as Appendix B. A Site Map is included as Figure 3. Well construction and gauging
information is presented in Table 6.
4. SITE INVESTIGATION

Based on information provided by the NCDEQ incident manager, an LSA was required at the site based on
site check results conducted in 2022 by a previous consultant. In summary, further investigation of a
release was required based on soil site check samples collected at two (2) damaged (and subsequently
replaced) spill buckets. A copy of the Site Check Report was not provided to Resolve.

A Type II Monitoring well (MW-1A) was installed adjacent to the affected spill buckets on March 6, 2023.
A soil sample was collected at the appropriate interval for analyses by SW-846 Method 8260 and MADEP
VPH. Concentrations of benzene, toluene, xylenes, naphthalene, isopropylbenzene, methylene chloride,
C5-C8 aliphatics and C9-C10 aromatics that exceeded the soil-to-water MSCCs were reported in the soil
sample MW-1A-5’. The concentration of C5-C8 aliphatics exceeded the residential MSCC.

A ground water quality sample was collected from the monitoring well on March 8, 2023 and submitted
for laboratory analyses for EPA Method 6200B plus oxygenates, EDB by EPA Method 504.1, lead and
MADEP VPH. Concentrations of benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics and C9-C10
aromatics exceeded the ground water quality standards specified in 15A NCAC 2L .0202. None of the
reported concentrations exceeded the gross contamination levels, if published.

Gauging data from the March 2023 gauging event has been included in Table 6. A summary of the current
gauging data is shown below:

Well ID
Screened
Interval
(ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1A 19-39 39 100.00 22.07 77.93

1. Soil Sampling:

Soil sample MW-1A-5’ was collected (above rock) on March 6, 2023 during borehole advancement of
MW-1A. The sample was submitted for laboratory analyses by SW-846 Method 8260 and MADEP VPH.

Concentrations of benzene, toluene, xylenes, naphthalene, isopropylbenzene, methylene chloride,
C5-C8 aliphatics and C9-C10 aromatics that exceeded the soil-to-water MSCCs were reported in the
soil sample MW-1A-5’. The concentration of C5-C8 aliphatics exceeded the residential MSCC. A Soil
Quality Map has been included as Figure 4. A summary of the soil sample analytical results is
presented in Table 7. A copy of the laboratory analytical report from the March 2023 soil sampling
event has been included in Appendix C. A copy of the current soil sampling data collected during the
LSA activities is shown below:

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
6

2. Ground Water Sampling:
A ground water sample was collected from MW-1A on March 8, 2023. The collected sample was
submitted for analyses by EPA Method 6200B, MADEP VPH, EPA Method 504.1 and lead. Detectable
concentrations of contaminants of concern that exceeded the maximum allowable concentrations
specified in 15A NCAC 2L.0202 were reported in the ground water sample and summarized below. A
Ground Water Quality Map has been included as Figure 5. A summary of the ground water analytical
data has been included in Table 8. A copy of the laboratory analytical report has been included in
Appendix C. A summary of the current ground water sampling data is shown below:

3. Quality Control:
The collected soil and ground water samples were immediately placed in laboratory-supplied
containers after collection, which were then placed in iced coolers. New disposable bailers were used
to sample the monitoring well and new nitrile gloves were worn during soil and ground water
sampling. Samples were logged using proper chain-of-custody procedures. The samples were
transported to a North Carolina certified laboratory for analysis. A laboratory supplied trip blank was
included in the sample cooler. No detectable concentrations of requested method constituents were
reported in the trip blank.

Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
0.0072 5.4 8 6 0.085 0.2 1.3 0.023 1.4 68 31
12 1,250 60.3 3,120 156 5.5 1,560 93.8 1,560 625 469
MW-1A 03/06/23 LSA well 5 7.31 0.939 J 13.6 10.2 <0.175 2.60 J 1.38 J 0.627 J 3.03 727 36.9
Residential Soil Cleanup Levels (mg/kg)XylenesSoil to Water MSCC (mg/kg)
Contaminant of Concern BenzeneEthylbenzene Toluene MTBENaphthaleneIsopropylbenzeneMethylene chloriden-PropylbenzeneC5-C8 AliphaticsC9-C10 AromaticsWell ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 15 400 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 15,000 NE NE
MW-1A 03/08/23 6.39 <5.00 28.4 25.4 434 88.4 428 4,790 <0.0018 707 225
Trip Blank 03/08/23 <0.500 <0.500 <0.500 <0.500 <1.00 <1.00 <10.0 <10.0 NR NR NRLeadC9-C10 Aromaticstert-Amyl alcohol(TAA)tert-Butyl alcohol(TBA)Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneC5-C8 Aliphatics2L Standard (µg/l)
GCL (µg/l)

___________________________________________________________________________________________
Prepared by: Resolve Environmental Limited Site Assessment Report
Prepared on: April 26, 2023 Express Lane Petro
Project Manager: Laura Minor
7
5. CONCLUSIONS AND RECOMMENDATIONS
 The Express Lane Petro site is located in Ansonville, Anson County, North Carolina. The site is an
operating petroleum retail facility and convenience store.
 Two 4,000-gallon gasoline USTs and one 8,000-gallon gasoline UST are currently in operation at the
site.
 Based on 2022 site check results conducted by a previous consultant, a LSA was required including a
monitoring well installed near the spill buckets (source area).
 MW-1A was installed adjacent to the spill buckets on March 6, 2023.
 Detectable concentrations of VOCs, C5-C8 aliphatics and C9-C10 aromatics above the soil-to- water
MSCCs were reported in the soil sample MW-1A-5’. The concentration of C5-C8 aliphatics exceeded
the residential MSCC.
 Concentrations of benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics and C9-C10 aromatics
exceeded the MACs. None of the concentrations exceeded the GCLs.
 The site is zoned General Business.
 The site and adjacent properties are connected to municipal water.
 A pond is located approximately 650 west of the site. No surface water bodies were identified within
500 feet of the site.
 No potable or non-potable wells were identified with 1,500 feet of the site.
 Based on the data collected during the LSA, the incident meets the criteria for a low-risk classification.
 Resolve recommends no further action following deed recordation of a Notice of Residual Petroleum
and associated public notice.

6. LIMITATIONS
This report has been prepared for the exclusive use of Gook Yun Knapp for specific application to the
referenced site in Anson County, North Carolina. The assessment was conducted based on the scope of
work and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Express Lane Petro
8931 US Highway 52 North
Ansonville, North Carolina
Anson County
Incident No. 48813
Resolve Project No.6398
500 M
2000 FT
Date: 04/25/2023 Location: 35.102981° N -80.108234° W
D
a
d
SITE
646916840685
646916848261
646916847487
646916842092 646916845610646916841215
646916843220 64691684530064 6916842181
646916845086
646916843286
Canal BranchPressley CreekUS HWY 52 PLANK RD
LEE STT H O M A S V I L L E R D
W H E L E S S B LV DMAYNARD AVETHREADGILL STCOLLEGE ST
WADDELL ST
SMITH ST
ANSONVILLE POLKTON RD BURNS STNORTH ST
COLSON AVEBOOKER STLITTLE STNOBLE CIR BASEBALL STLITTLE STFIGURE 2A: SITE VICINITY MAPEXPRESS LANE PETRO8931 US HIGHWAY 52 NORTHANSONVILLE, ANSON COUNTYNORTH CAROLINAINCIDENT NO. 48813/11109
PREPARED BY:RESOLVE ENVIRONMENTAL SERVICES, PLLCMARCH 3, 2023
³
0 300150
Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
1
LEGEND
roads
riversandstreams
waterbodies
Adjacent Properties
nc_anson_parcels_poly_2017_10_27
Receptor ID (See Table 4)1
SITE
Canal BranchPressley CreekUS HWY 52 PLANK RD
LEE STT H O M A S V I L L E R D
W H E L E S S B LV DMAYNARD AVETHREADGILL STCOLLEGE ST
WADDELL ST
SMITH ST
ANSONVILLE POLKTON RD BURNS STNORTH ST
COLSON AVEBOOKER STLITTLE STNOBLE CIR BASEBALL STLITTLE STFIGURE 2B: LAND USE MAPEXPRESS LANE PETRO8931 US HIGHWAY 52 NORTHANSONVILLE, ANSON COUNTYNORTH CAROLINAINCIDENT NO. 48813/11109
PREPARED BY:RESOLVE ENVIRONMENTAL SERVICES, PLLCMARCH 3, 2023
³
0 300150
Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
roads
riversandstreams
waterbodies
ZONING - R-2
ZONING - R-A
ZONING - G-B
ZONING - R-1
nc_anson_parcels_poly_2017_10_27
Land Use Code (See Table 3)1
1
2
3
4
5
6
RESOLVE
ENVIRONMENTAL
SERVICES, PLLC
EXPRESS LANE PETRO
8931 US Highway 52 North
Ansonville, North Carolina
Anson County
Incident No. 48813
Resolve Project No. 6383
500 Devonport Drive
Matthews, North Carolina 28104
Phone: [phone]
LEGEND
FIGURE 3
SITE MAPNNOTE:
1.THIS SITE MAP IS BASED ON DATA FROM ANSON
COUNTY, NC GIS OFFICE.
BUILDING FOOTPRINT
PLANK R
O
A
D
HIGHWAY 52 NORTH
FUEL DISPENSER
TYPE II MONITORING WELL
RESOLVE
ENVIRONMENTAL
SERVICES, PLLC
EXPRESS LANE PETRO
8931 US Highway 52 North
Ansonville, North Carolina
Anson County
Incident No. 48813
Resolve Project No. 6383
500 Devonport Drive
Matthews, North Carolina 28104
Phone: [phone]
LEGEND
FIGURE 4
SOIL QUALITY MAP (03/06/2023)NBUILDING FOOTPRINT
PLANK R
O
A
D
HIGHWAY 52 NORTH
FUEL DISPENSER
TYPE II MONITORING WELL
RESOLVE
ENVIRONMENTAL
SERVICES, PLLC
EXPRESS LANE PETRO
8931 US Highway 52 North
Ansonville, North Carolina
Anson County
Incident No. 48813
Resolve Project No. 6383
500 Devonport Drive
Matthews, North Carolina 28104
Phone: [phone]
LEGEND
FIGURE 5
GROUND WATER QUALITY MAP (03/08/2023)NBUILDING FOOTPRINT
PLANK R
O
A
D
HIGHWAY 52 NORTH
FUEL DISPENSER
TYPE II MONITORING WELL

TABLES
UST ID Number 1 through 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 through 3 Facility ID Number
Owner or Operator?
Operator
UST ID Number 1 through 3 Facility ID Number
Owner or Operator?
Owner
00-0-0000028611
TABLE 1
UST OWNER/OPERATOR INFORMATION
EXPRESS LANE PETRO
00-0-0000026041
11502 Destin Lane, Charlotte, NC 28277-1208 704-314-5499
Name of Owner or Operator Dates of Ownership / Operation
Gook Yun Knapp 06/10/2016 - current
Address Telephone Number
Name of Owner or Operator Dates of Ownership / Operation
Scott Gordon 1/1/1999 - 6/10/2016
Address Telephone Number
PO Box 769, Marshville, NC 28103 704-233-2600
00-0-0000028611
Name of Owner or Operator Dates of Ownership / Operation
Jeffrey C. Deese 1/1/1999 - 6/10/2016
Address Telephone Number
Unknown Unknown
Page 1 of 1
Date: 4/8/2023
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 4,000 01/28/99 Single Wall
Steel/FPR 64" x 24'Single Wall FRP Active Yes
2 Gasoline Gasoline 4,000 01/28/99 Single Wall
Steel/FPR 64" x 24'Single Wall FRP Active Yes
3 Gasoline Gasoline 8,000 01/28/99 Single Wall
Steel/FPR 96″ x 21′4″Single Wall FRP Active Yes
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
Facility ID #: 0-00-0000026041
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
EXPRESS LANE PETRO
Page 1 of 1
Date: 4/22/23 Facility ID # : 00-0-0000026041
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Ansonville United Methodist
Church R1 Church 27 Plank Road
Ansonville, NC 28007 ~200
2 Sonny Beachum Classic Car
Museum (temporarily closed)GB Museum 8832 Main Street
Wadesboro, NC 28170 ~300
3 All Souls Episcopal Church GB Church 8812 Main Street
Wadesboro, NC 28170 ~550
4 Ansonville Town Hall GB Municipal 8778 Main Street
Ansonville, NC 28007 ~775
5 Ansonville Elementary School R1 Institutional 9104 US Hwy 52
Wadesboro, NC 28170 ~1,250
6 Ansonville Fire & Rescue
Department R1 Municipal 9145 US Hwy 52
Wadesboro, NC 28170 ~1,250
n/a GB General Business n/a n/a
n/a R1 Residential/Educational/
Church n/a n/a
n/a R2 Multiple Family
Residential n/a n/a
n/a R3 Multiple Family
Residential n/a n/a
n/a RA Residential/Agricultural n/a n/a
Note:
• Properties are keyed to Figure 2B.
TABLE 3
LAND USE INFORMATION
EXPRESS LANE PETRO
INCIDENT NUMBER 48813
Page 1 of 1
Facility ID #: 0-00-0000026041
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
Receptor ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
1 35.103353,
-80.110518 n/a 650
Notes:
• Receptors are shown on Figure 2A.
• n/a: not applicable.
Pond Parcel 646916840685 (109 Plank Road)Unknown Surface Water
TABLE 4
RECEPTOR INFORMATION
INCIDENT NUMBER 48813
Date: 4/8/23
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
EXPRESS LANE PETRO
No Potable Wells within 1,500 Feet
No Non-Potable Wells within 250 Feet
Description Location Contact/Phone Number Usage
Page 1 of 1
Date: 4/8/23 Facility ID #: 0-00-0000026041
PIN Number Property Owner Name Property Owner Address
646916845300 (site)KNAPP GOOK YUN 11502 Destin Lane
Charlotte, North Carolina 28277
646916845610 LEE GREG etal PO Box 67
Ansonville, North Carolina 28007
646916847487 SP FDS LLC 4004 Barrett Drive, Suite 106
Raleigh, North Carolina 27609
646916848261 &
646916845086 B&M LEE OIL CO INC PO Box 67
Ansonville, North Carolina 28007
646916842092 &
646916842181 ANSONVILLE METHODIST CHURCH 9655 US Highway 52 North
Ansonville, North Carolina 28007
646916843220 ROSS LL SR HEIRS 200 Breslin Street
Wadesboro, North Carolina 28170
646916841215 &
646916843286 VARGAS MARCO GARCIA & OSBELLA PO Box 953
Norwood, North Carolina 28128
646916840685 DAVIS DONNA LYNN PO Box 231
Ansonville, North Carolina 28007
Note:
• Properties are keyed to Figure 2.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
INCIDENT NUMBER 48813
EXPRESS LANE PETRO
Page 1 of 1
Date: 4/8/23 Facility ID #: 0-00-0000026041
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
MW-1A 03/06/23 03/08/23 39 19-39 39 100.00 22.07 ---77.93
Notes:
• ft BGS : feet below ground surface.
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
EXPRESS LANE PETRO
INCIDENT NUMBER 48813
Page 1 of 1
Date: 4/8/2023 Facility ID #: 0-00-0000026041
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
0.0072 5.4 8 6 0.085 0.2 1.3 0.023 1.4 68 31
12 1,250 60.3 3,120 156 5.5 1,560 93.8 1,560 625 469
MW-1A 03/06/23 LSA well 5 7.31 0.939 J 13.6 10.2 <0.175 2.60 J 1.38 J 0.627 J 3.03 727 36.9
• Concentrations in bold face type indicate the concentration exceeds the MSCC.
Notes:
• Results reported in mg/kg;
• ft-BGS: feet below ground surface.
EXPRESS LANE PETRO
TABLE 7
Analytical Method
Soil to Water MSCC (mg/kg)
Contaminant of Concern
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS BenzeneEthylbenzene Toluene MTBENaphthaleneIsopropylbenzeneResidential Soil Cleanup Levels (mg/kg)XylenesSW-846 8260 MADEP VPH
INCIDENT NUMBER 48813
Methylene chloriden-PropylbenzeneC5-C8 AliphaticsC9-C10 AromaticsPage 1 of 1
Date: 04/08/23
SW-6010D
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 15 400 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 15,000 NE NE
MW-1A 03/08/23 6.39 <5.00 28.4 25.4 434 88.4 428 4,790 <0.0018 707 225
Trip Blank 03/08/23 <0.500 <0.500 <0.500 <0.500 <1.00 <1.00 <10.0 <10.0 NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established.
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
VPH
C5-C8 Aliphatics• NR: Analysis not requested.
2L Standard (µg/l)
GCL (µg/l)
SM-6200
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
EXPRESS LANE PETRO
INCIDENT NUMBER 48813
LeadC9-C10 Aromaticstert-Amyl alcohol(TAA)Analytical Method tert-Butyl alcohol(TBA)Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthalenePage 1 of 1

APPENDICES

APPENDIX A
Anson County Property Cards
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:121/0289
Address:11502 DESTIN LANE
Owner Name:KNAPP GOOD YUN
PIN:646916845300
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
CHARLOTTE,NC 28277-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:167/0374
Address:PO BOX 67
Owner Name:LEE GREG ETAL
PIN:646916845610
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:282/0334
Address:4004 BARRETT DRIVE SUITE 106
Owner Name:SP FDS LLC
PIN:646916847487
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
RALEIGH,NC 27609-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:397/0342
Address:PO BOX 67
Owner Name:B & M OIL CO INC
PIN:646916848261
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:213/0362
Address:PO BOX 67
Owner Name:B & M LEE OIL CO INC
PIN:646916845086
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:181/0708
Address:9655 US HWY 52 N
Owner Name:ANSONVILLE METHODIST CHURCH
PIN:646916842092
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:181/0708
Address:9655 US HWY 52 N
Owner Name:ANSONVILLE METHODIST CHURCH
PIN:646916842181
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:181/0045
Address:200 BRESLIN ST
Owner Name:ROSS L L SR HEIRS
PIN:646916843220
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
WADESBORO,NC 28170-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:284/0276
Address:PO BOX 953
Owner Name:VARGAS MARCO GARCIA & OSBELLA
PIN:646916843286
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
NORWOOD,NC 28128-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:284/0276
Address:PO BOX 953
Owner Name:VARGAS MARCO GARCIA & OSBELLA
PIN:646916841215
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
NORWOOD,NC 28128-0000
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan,Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand),
April 22, 2023

Deed Reference:901/0335
Address:PO BOX 231
Owner Name:DAVIS DONNA LYNN
PIN:646916840685
1:1,812
0 0.03 0.060.015 mi
0 0.045 0.090.0225 km
ANSONVILLE,NC 28007-0000

APPENDIX B
Well Construction Record and Subsurface
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Express Lane
Address 8931 US 52 N, Ansonville, NC
Boring Number MW-1A Date Drilled
Sample Method Macrocore Drilling Method SSA
Completion Details Set 25' 0.01 slot PVC screen
Driller Steele Log By Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0.-0.5'Asphalt
0.5'-8'Black sandy SILT; petroleum odor
5 MW-1A-5'4.5-5.0
8'-9'PWR
10
9'-39'Argillite; dry
15
20
25

30
35 water bearing fracture encountered at 37 feet
TD 39'
40

45
50
55

60
65
70

75
80
85

90
95

100
03/06/23
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX C
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/22/2023
Resolve Environmental Scott Ball
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Revised Lab Report Number: 23-069-9024 (Original Report 23-069-0024) Client Project Description: Express Lane Petro
Dear Scott Ball:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/10/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Danyale Love Project Manager
Page 1 of 43
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-069-9024
Page 2 of 43
Report Number:
Sample Summary Table
Client Project Description:
23-069-9024
Express Lane Petro
Lab No Client Sample ID Matrix Date Collected Date Received
03/06/2023 09:45Solids 90896 MW-1A-5'03/10/2023 13:50
03/08/2023 13:38Aqueous 90897 MW-1A 03/10/2023 13:50
03/08/2023Aqueous 90936 Trip Blank 03/10/2023 13:50
Page 3 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-069-9024
Report Limit
Project:Express Lane Petro
V 90896MW-1A-5'
8.39 03/15/2023 11:362540G-2011 Moisture %0
7.31 03/13/2023 20:208260DBenzenemg/Kg - dry 0.164
J1.15 03/13/2023 20:208260Dn-Butylbenzene mg/Kg - dry 0.138
J0.596 03/13/2023 20:208260Dsec-Butyl benzene mg/Kg - dry 0.159
13.6 03/13/2023 20:208260DEthylbenzenemg/Kg - dry 0.164
29.5 03/13/2023 20:208260Dn-Hexane mg/Kg - dry 0.186
J1.38 03/13/2023 20:208260DIsopropylbenzenemg/Kg - dry 0.130
J0.627 03/13/2023 20:208260DMethylene Chloride mg/Kg - dry 0.416
J2.60 03/13/2023 20:208260DNaphthalenemg/Kg - dry 0.279
3.03 03/13/2023 20:208260Dn-Propylbenzene mg/Kg - dry 0.152
J0.939 03/13/2023 20:208260DToluenemg/Kg - dry 0.187
6.00 03/13/2023 20:208260D1,2,4-Trimethylbenzene mg/Kg - dry 0.138
1.84 03/13/2023 20:208260D1,3,5-Trimethylbenzene mg/Kg - dry 0.152
2.08 03/13/2023 20:208260Do-Xylene mg/Kg - dry 0.141
8.14 03/13/2023 20:208260Dm,p-Xylene mg/Kg - dry 0.355
10.2 03/13/2023 20:208260DXylene (Total)mg/Kg - dry 0.141
727 03/13/2023 18:25CALCULATIONAliphatic C5-C8 (Adjusted)mg/Kg - dry 9.41
132 03/13/2023 18:25CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 9.41
36.9 03/13/2023 18:25CALCULATIONAromatic C9-C10 (Adjusted)mg/Kg - dry 9.41
736 03/13/2023 18:25MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 9.41
193 03/13/2023 18:25MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 9.41
36.9 03/13/2023 18:25MADEP-VPH Aromatic C9-C10 mg/Kg - dry 9.41
V 90897MW-1A
6.39 03/16/2023 21:376200BBenzeneµg/L 5.00
362 03/16/2023 21:376200BDi-Isopropyl Ether (DIPE)µg/L 5.00
28.4 03/16/2023 21:376200BEthylbenzeneµg/L 5.00
6.31 03/16/2023 21:376200BIsopropylbenzeneµg/L 5.00
434 03/16/2023 21:376200BMethyl tert-butyl ether (MTBE)µg/L 10.0
88.4 03/16/2023 21:376200BNaphthaleneµg/L 10.0
9.83 03/16/2023 21:376200Bn-Propylbenzene µg/L 5.00
4790 03/18/2023 00:126200Btert-Butyl Alcohol (TBA)µg/L 1000
428 03/16/2023 21:376200Btert-Amyl Alcohol (TAA)µg/L 100
55.3 03/16/2023 21:376200B1,2,4-Trimethylbenzene µg/L 5.00
5.95 03/16/2023 21:376200B1,3,5-Trimethylbenzene µg/L 5.00
25.4 03/16/2023 21:376200Bm,p-Xylene µg/L 10.0
25.4 03/16/2023 21:376200BXylene (Total)µg/L 5.00
Page 4 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-069-9024
Report Limit
Project:Express Lane Petro
V 90897MW-1A
707 03/14/2023 13:20CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 50.0
161 03/14/2023 13:20CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 50.0
225 03/14/2023 13:20CALCULATIONAromatic C9-C10 (Adjusted)µg/L 50.0
713 03/14/2023 13:20MADEP-VPH Aliphatic C5-C8 µg/L 50.0
440 03/14/2023 13:20MADEP-VPH Aliphatic C9-C12 µg/L 50.0
225 03/14/2023 13:20MADEP-VPH Aromatic C9-C10 µg/L 50.0
Page 5 of 43

Client: Resolve Environmental CASE NARRATIVE
Project: Express Lane Petro Lab Report Number: 23-069-9024
Date: 4/22/2023
Report Comments This report has been revised to correct the sample date on MW-1A-5' to match the COC. Total Metals Method EPA-200.7 Sample 90899
Analyte: Lead QC Batch No: V30859/V30768
ICV failed high. Sample concentration BRL. Results not affected. EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Sample 90542
QC Batch No: V30816/V30754 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference. Volatile Organic Compounds - GC/MS Method 6200B Analyte: tert-Amyl Methyl Ether
QC Batch No: V30957/V30955 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 6 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.39 %0 0.010Moisture 1 03/15/23 11:36 2540G-2011AMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30834 03/13/23 08:00
<0.680 mg/Kg - dry 0.680 5.67Acetone 500 03/13/23 20:20 V30835TBL
<0.342 mg/Kg - dry 0.342 5.67Acrolein 500 03/13/23 20:20 V30835TBL
<0.212 mg/Kg - dry 0.212 5.67Acrylonitrile 500 03/13/23 20:20 V30835TBL
7.31 mg/Kg - dry 0.164 1.42Benzene 500 03/13/23 20:20 V30835TBL
<0.141 mg/Kg - dry 0.141 1.42Bromobenzene 500 03/13/23 20:20 V30835TBL
<0.227 mg/Kg - dry 0.227 1.42Bromochloromethane 500 03/13/23 20:20 V30835TBL
<0.337 mg/Kg - dry 0.337 1.42Bromodichloromethane 500 03/13/23 20:20 V30835TBL
<0.287 mg/Kg - dry 0.287 1.42Bromoform 500 03/13/23 20:20 V30835TBL
<0.514 mg/Kg - dry 0.514 2.83Bromomethane 500 03/13/23 20:20 V30835TBL
1.15 J mg/Kg - dry 0.138 1.42n-Butylbenzene 500 03/13/23 20:20 V30835TBL
0.596 J mg/Kg - dry 0.159 1.42sec-Butyl benzene 500 03/13/23 20:20 V30835TBL
<0.141 mg/Kg - dry 0.141 1.42tert-Butyl benzene 500 03/13/23 20:20 V30835TBL
<0.181 mg/Kg - dry 0.181 1.42Carbon Disulfide 500 03/13/23 20:20 V30835TBL
<0.448 mg/Kg - dry 0.448 1.42Carbon Tetrachloride 500 03/13/23 20:20 V30835TBL
<0.189 mg/Kg - dry 0.189 1.42Chlorobenzene 500 03/13/23 20:20 V30835TBL
<0.252 mg/Kg - dry 0.252 1.42Chlorodibromomethane 500 03/13/23 20:20 V30835TBL
<0.252 mg/Kg - dry 0.252 2.83Chloroethane 500 03/13/23 20:20 V30835TBL
<0.298 mg/Kg - dry 0.298 1.42Chloroform 500 03/13/23 20:20 V30835TBL
<0.177 mg/Kg - dry 0.177 2.83Chloromethane 500 03/13/23 20:20 V30835TBL
<0.145 mg/Kg - dry 0.145 1.422-Chlorotoluene 500 03/13/23 20:20 V30835TBL
<0.110 mg/Kg - dry 0.110 1.424-Chlorotoluene 500 03/13/23 20:20 V30835TBL
<0.207 mg/Kg - dry 0.207 1.42Di-Isopropyl Ether (DIPE)500 03/13/23 20:20 V30835TBL
<0.124 mg/Kg - dry 0.124 2.831,2-Dibromo-3-Chloropropane 500 03/13/23 20:20 V30835TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30834 03/13/23 08:00
<0.167 mg/Kg - dry 0.167 1.421,2-Dibromoethane 500 03/13/23 20:20 V30835TBL
<0.280 mg/Kg - dry 0.280 1.42Dibromomethane 500 03/13/23 20:20 V30835TBL
<0.087 mg/Kg - dry 0.087 1.421,2-Dichlorobenzene 500 03/13/23 20:20 V30835TBL
<0.107 mg/Kg - dry 0.107 1.421,3-Dichlorobenzene 500 03/13/23 20:20 V30835TBL
<0.170 mg/Kg - dry 0.170 1.421,4-Dichlorobenzene 500 03/13/23 20:20 V30835TBL
<0.373 mg/Kg - dry 0.373 2.83Dichlorodifluoromethane 500 03/13/23 20:20 V30835TBL
<0.232 mg/Kg - dry 0.232 1.421,1-Dichloroethane 500 03/13/23 20:20 V30835TBL
<0.391 mg/Kg - dry 0.391 1.421,2-Dichloroethane 500 03/13/23 20:20 V30835TBL
<0.207 mg/Kg - dry 0.207 1.421,1-Dichloroethene 500 03/13/23 20:20 V30835TBL
<0.223 mg/Kg - dry 0.223 1.42cis-1,2-Dichloroethene 500 03/13/23 20:20 V30835TBL
<0.298 mg/Kg - dry 0.298 1.42trans-1,2-Dichloroethene 500 03/13/23 20:20 V30835TBL
<0.124 mg/Kg - dry 0.124 1.421,2-Dichloropropane 500 03/13/23 20:20 V30835TBL
<0.156 mg/Kg - dry 0.156 1.421,3-Dichloropropane 500 03/13/23 20:20 V30835TBL
<0.360 mg/Kg - dry 0.360 1.422,2-Dichloropropane 500 03/13/23 20:20 V30835TBL
<0.216 mg/Kg - dry 0.216 1.421,1-Dichloropropene 500 03/13/23 20:20 V30835TBL
<0.152 mg/Kg - dry 0.152 1.42cis-1,3-Dichloropropene 500 03/13/23 20:20 V30835TBL
<0.227 mg/Kg - dry 0.227 1.42trans-1,3-Dichloropropene 500 03/13/23 20:20 V30835TBL
13.6 mg/Kg - dry 0.164 1.42Ethylbenzene 500 03/13/23 20:20 V30835TBL
<0.234 mg/Kg - dry 0.234 28.3Ethyl Tertiary Butyl Ether (ETBE)500 03/13/23 20:20 V30835TBL
<0.223 mg/Kg - dry 0.223 2.83Hexachlorobutadiene 500 03/13/23 20:20 V30835TBL
29.5 mg/Kg - dry 0.186 2.83n-Hexane 500 03/13/23 20:20 V30835TBL
<0.175 mg/Kg - dry 0.175 5.672-Hexanone 500 03/13/23 20:20 V30835TBL
1.38 J mg/Kg - dry 0.130 1.42Isopropylbenzene 500 03/13/23 20:20 V30835TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30834 03/13/23 08:00
<0.368 mg/Kg - dry 0.368 1.424-Isopropyl toluene 500 03/13/23 20:20 V30835TBL
<0.184 mg/Kg - dry 0.184 5.67Methyl Ethyl Ketone (MEK)500 03/13/23 20:20 V30835TBL
<0.175 mg/Kg - dry 0.175 1.42Methyl tert-butyl ether (MTBE)500 03/13/23 20:20 V30835TBL
<4.25 mg/Kg - dry 4.25 5.674-Methyl-2-Pentanone 500 03/13/23 20:20 V30835TBL
0.627 J mg/Kg - dry 0.416 1.42Methylene Chloride 500 03/13/23 20:20 V30835TBL
2.60 J mg/Kg - dry 0.279 2.83Naphthalene 500 03/13/23 20:20 V30835TBL
3.03 mg/Kg - dry 0.152 1.42n-Propylbenzene 500 03/13/23 20:20 V30835TBL
<0.402 mg/Kg - dry 0.402 1.42Styrene 500 03/13/23 20:20 V30835TBL
<0.298 mg/Kg - dry 0.298 1.421,1,1,2-Tetrachloroethane 500 03/13/23 20:20 V30835TBL
<0.090 mg/Kg - dry 0.090 1.421,1,2,2-Tetrachloroethane 500 03/13/23 20:20 V30835TBL
<0.255 mg/Kg - dry 0.255 1.42Tetrachloroethene 500 03/13/23 20:20 V30835TBL
0.939 J mg/Kg - dry 0.187 1.42Toluene 500 03/13/23 20:20 V30835TBL
<0.152 mg/Kg - dry 0.152 2.831,2,3-Trichlorobenzene 500 03/13/23 20:20 V30835TBL
<0.181 mg/Kg - dry 0.181 2.831,2,4-Trichlorobenzene 500 03/13/23 20:20 V30835TBL
<0.408 mg/Kg - dry 0.408 1.421,1,1-Trichloroethane 500 03/13/23 20:20 V30835TBL
<0.133 mg/Kg - dry 0.133 1.421,1,2-Trichloroethane 500 03/13/23 20:20 V30835TBL
<0.260 mg/Kg - dry 0.260 1.42Trichloroethene 500 03/13/23 20:20 V30835TBL
<0.590 mg/Kg - dry 0.590 2.83Trichlorofluoromethane 500 03/13/23 20:20 V30835TBL
<0.204 mg/Kg - dry 0.204 1.421,2,3-Trichloropropane 500 03/13/23 20:20 V30835TBL
6.00 mg/Kg - dry 0.138 1.421,2,4-Trimethylbenzene 500 03/13/23 20:20 V30835TBL
1.84 mg/Kg - dry 0.152 1.421,3,5-Trimethylbenzene 500 03/13/23 20:20 V30835TBL
<0.129 mg/Kg - dry 0.129 2.83Vinyl Acetate 500 03/13/23 20:20 V30835TBL
<0.135 mg/Kg - dry 0.135 2.83Vinyl Chloride 500 03/13/23 20:20 V30835TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30834 03/13/23 08:00
2.08 mg/Kg - dry 0.141 1.42o-Xylene 500 03/13/23 20:20 V30835TBL
8.14 mg/Kg - dry 0.355 2.83m,p-Xylene 500 03/13/23 20:20 V30835TBL
10.2 mg/Kg - dry 0.141 1.42Xylene (Total)500 03/13/23 20:20 V30835
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/13/23 20:20500 TBL V30835
Surrogate: Dibromofluoromethane 98.7 Limits: 70-130%03/13/23 20:20500 TBL V30835
Surrogate: Toluene-d8 99.4 Limits: 76-129%03/13/23 20:20500 TBL V30835
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A-5'
90896 Matrix:
3/6/2023 9:45
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
727 mg/Kg - dry 9.41Aliphatic C5-C8 (Adjusted)100 03/13/23 18:25
132 mg/Kg - dry 9.41Aliphatics C9-C12 (Adjusted)100 03/13/23 18:25
36.9 mg/Kg - dry 9.41Aromatic C9-C10 (Adjusted)100 03/13/23 18:25
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30783 03/14/23 08:00
736 mg/Kg - dry 9.41Aliphatic C5-C8 100 03/13/23 18:25 V30784TBL
193 mg/Kg - dry 9.41Aliphatic C9-C12 100 03/13/23 18:25 V30784TBL
36.9 mg/Kg - dry 9.41Aromatic C9-C10 100 03/13/23 18:25 V30784TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)84.3 Limits: 70-130%03/13/23 18:25100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)80.0 Limits: 70-130%03/13/23 18:25100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 1003,3-Dimethyl-1-butanol 10 03/16/23 21:37 6200BENM
<0.0018 mg/L 0.0018 0.0060Lead 1 03/27/23 13:21 EPA-200.7MMR
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00 V30983 03/17/23 09:00
<100 µg/L 100Acetone 10 03/16/23 21:37 V30957ENM
6.39 µg/L 5.00Benzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Bromobenzene 10 03/16/23 21:37 V30957ENM
<10.0 µg/L 10.0Bromochloromethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Bromodichloromethane 10 03/16/23 21:37 V30957ENM
<50.0 µg/L 50.0Bromoform 10 03/16/23 21:37 V30957ENM
<10.0 µg/L 10.0Bromomethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00n-Butylbenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00sec-Butyl benzene 10 03/16/23 21:37 V30957ENM
<20.0 µg/L 20.0tert-Butyl benzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Carbon Tetrachloride 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Chlorobenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Chlorodibromomethane 10 03/16/23 21:37 V30957ENM
<10.0 µg/L 10.0Chloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Chloroform 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Chloromethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.002-Chlorotoluene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.004-Chlorotoluene 10 03/16/23 21:37 V30957ENM
362 µg/L 5.00Di-Isopropyl Ether (DIPE)10 03/16/23 21:37 V30957ENM
<20.0 µg/L 20.01,2-Dibromo-3-Chloropropane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Dibromomethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2-Dichlorobenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,3-Dichlorobenzene 10 03/16/23 21:37 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00 V30983 03/17/23 09:00
<5.00 µg/L 5.001,4-Dichlorobenzene 10 03/16/23 21:37 V30957ENM
<50.0 µg/L 50.0Dichlorodifluoromethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1-Dichloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2-Dichloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1-Dichloroethene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00cis-1,2-Dichloroethene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00trans-1,2-Dichloroethene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2-Dichloropropane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,3-Dichloropropane 10 03/16/23 21:37 V30957ENM
<20.0 µg/L 20.02,2-Dichloropropane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1-Dichloropropene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00cis-1,3-Dichloropropene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00trans-1,3-Dichloropropene 10 03/16/23 21:37 V30957ENM
<2000 µg/L 2000Ethanol 10 03/16/23 21:37 V30957ENM
28.4 µg/L 5.00Ethylbenzene 10 03/16/23 21:37 V30957ENM
<30.0 µg/L 30.0Hexachlorobutadiene 10 03/16/23 21:37 V30957ENM
<10.0 µg/L 10.02-Hexanone 10 03/16/23 21:37 V30957ENM
6.31 µg/L 5.00Isopropylbenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.004-Isopropyl toluene 10 03/16/23 21:37 V30957ENM
<50.0 µg/L 50.0Methyl Ethyl Ketone (MEK)10 03/16/23 21:37 V30957ENM
434 µg/L 10.0Methyl tert-butyl ether (MTBE)10 03/16/23 21:37 V30957ENM
<10.0 µg/L 10.04-Methyl-2-Pentanone 10 03/16/23 21:37 V30957ENM
<20.0 µg/L 20.0Methylene Chloride 10 03/16/23 21:37 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00 V30983 03/17/23 09:00
88.4 µg/L 10.0Naphthalene 10 03/16/23 21:37 V30957ENM
9.83 µg/L 5.00n-Propylbenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Styrene 10 03/16/23 21:37 V30957ENM
4790 µg/L 1000tert-Butyl Alcohol (TBA)100 03/18/23 00:12 V30984MSA
<100 µg/L 100tert-Butyl formate (TBF)10 03/16/23 21:37 V30957ENM
428 µg/L 100tert-Amyl Alcohol (TAA)10 03/16/23 21:37 V30957ENM
<100 µg/L 100tert-Amyl Methyl Ether (TAME)10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1,1,2-Tetrachloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1,2,2-Tetrachloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Tetrachloroethene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Toluene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2,3-Trichlorobenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2,4-Trichlorobenzene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1,1-Trichloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,1,2-Trichloroethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Trichloroethene 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Trichlorofluoromethane 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.001,2,3-Trichloropropane 10 03/16/23 21:37 V30957ENM
55.3 µg/L 5.001,2,4-Trimethylbenzene 10 03/16/23 21:37 V30957ENM
5.95 µg/L 5.001,3,5-Trimethylbenzene 10 03/16/23 21:37 V30957ENM
<50.0 µg/L 50.0Vinyl Acetate 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00Vinyl Chloride 10 03/16/23 21:37 V30957ENM
<5.00 µg/L 5.00o-Xylene 10 03/16/23 21:37 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00 V30983 03/17/23 09:00
25.4 µg/L 10.0m,p-Xylene 10 03/16/23 21:37 V30957ENM
25.4 µg/L 5.00Xylene (Total)10 03/16/23 21:37 V30957
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%03/16/23 21:3710 ENM V30957
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%03/16/23 21:3710 ENM V30957
Surrogate: 1,2-Dichloroethane - d4 86.8 Limits: 70-130%03/16/23 21:3710 ENM V30957
Surrogate: Toluene-d8 89.2 Limits: 70-130%03/16/23 21:3710 ENM V30957
Surrogate: 4-Bromofluorobenzene 97.0 Limits: 70-130%03/18/23 00:12100 MSA V30984
Surrogate: Dibromofluoromethane 86.4 Limits: 70-130%03/18/23 00:12100 MSA V30984
Surrogate: 1,2-Dichloroethane - d4 89.4 Limits: 70-130%03/18/23 00:12100 MSA V30984
Surrogate: Toluene-d8 97.6 Limits: 70-130%03/18/23 00:12100 MSA V30984
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V30754 03/14/23 10:22
<0.0237 µg/L 0.02371,2-Dibromoethane 1 03/14/23 16:41 V30816AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:MW-1A
90897 Matrix:
3/8/2023 13:38
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
707 µg/L 50.0Aliphatic C5-C8 (Adjusted)1 03/14/23 13:20
161 µg/L 50.0Aliphatics C9-C12 (Adjusted)1 03/14/23 13:20
225 µg/L 50.0Aromatic C9-C10 (Adjusted)1 03/14/23 13:20
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30792 03/14/23 08:00
713 µg/L 50.0Aliphatic C5-C8 1 03/14/23 13:20 V30794TBL
440 µg/L 50.0Aliphatic C9-C12 1 03/14/23 13:20 V30794TBL
225 µg/L 50.0Aromatic C9-C10 1 03/14/23 13:20 V30794TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)92.2 Limits: 70-130%03/14/23 13:201 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)86.0 Limits: 70-130%03/14/23 13:201 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90936 Matrix:
3/8/2023 0:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.03,3-Dimethyl-1-butanol 1 03/16/23 14:01 6200BENM
Surrogate: 4-Bromofluorobenzene 89.8 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: Dibromofluoromethane 92.8 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: 1,2-Dichloroethane - d4 79.4 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: Toluene-d8 92.4 Limits: 70-130%03/16/23 14:011 ENM V30957
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90936 Matrix:
3/8/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00
<10.0 µg/L 10.0Acetone 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Benzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Bromobenzene 1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.00Bromochloromethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Bromodichloromethane 1 03/16/23 14:01 V30957ENM
<5.00 µg/L 5.00Bromoform 1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.00Bromomethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500n-Butylbenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500sec-Butyl benzene 1 03/16/23 14:01 V30957ENM
<2.00 µg/L 2.00tert-Butyl benzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Carbon Tetrachloride 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Chlorobenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Chlorodibromomethane 1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.00Chloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Chloroform 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Chloromethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5002-Chlorotoluene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5004-Chlorotoluene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 03/16/23 14:01 V30957ENM
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Dibromomethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 03/16/23 14:01 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90936 Matrix:
3/8/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 03/16/23 14:01 V30957ENM
<5.00 µg/L 5.00Dichlorodifluoromethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1-Dichloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2-Dichloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1-Dichloroethene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2-Dichloropropane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,3-Dichloropropane 1 03/16/23 14:01 V30957ENM
<2.00 µg/L 2.002,2-Dichloropropane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1-Dichloropropene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 03/16/23 14:01 V30957ENM
<200 µg/L 200Ethanol 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Ethylbenzene 1 03/16/23 14:01 V30957ENM
<3.00 µg/L 3.00Hexachlorobutadiene 1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.002-Hexanone 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Isopropylbenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5004-Isopropyl toluene 1 03/16/23 14:01 V30957ENM
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 03/16/23 14:01 V30957ENM
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 03/16/23 14:01 V30957ENM
<2.00 µg/L 2.00Methylene Chloride 1 03/16/23 14:01 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90936 Matrix:
3/8/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00
<1.00 µg/L 1.00Naphthalene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500n-Propylbenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Styrene 1 03/16/23 14:01 V30957ENM
<10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 03/16/23 14:01 V30957ENM
<10.0 µg/L 10.0tert-Butyl formate (TBF)1 03/16/23 14:01 V30957ENM
<10.0 µg/L 10.0tert-Amyl Alcohol (TAA)1 03/16/23 14:01 V30957ENM
<10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Tetrachloroethene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Toluene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Trichloroethene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Trichlorofluoromethane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 03/16/23 14:01 V30957ENM
<5.00 µg/L 5.00Vinyl Acetate 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Vinyl Chloride 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500o-Xylene 1 03/16/23 14:01 V30957ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-069-9024
00238
Resolve Environmental
3502 Hayes Road
Scott Ball
Monroe
Received : 03/10/2023
Express Lane Petro
Revised Report Date: 04/22/2023
Original Report Date : 03/27/2023
Sample ID :
Lab No :
Sampled:Trip Blank
90936 Matrix:
3/8/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V30955 03/16/23 09:00
<1.00 µg/L 1.00m,p-Xylene 1 03/16/23 14:01 V30957ENM
<0.500 µg/L 0.500Xylene (Total)1 03/16/23 14:01 V30957
Surrogate: 4-Bromofluorobenzene 89.8 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: Dibromofluoromethane 92.8 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: 1,2-Dichloroethane - d4 79.4 Limits: 70-130%03/16/23 14:011 ENM V30957
Surrogate: Toluene-d8 92.4 Limits: 70-130%03/16/23 14:011 ENM V30957
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
Total, Fixed, and Volatile Solids
2540G-2011
V30827QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91045-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
15.0 03/15/23 11:360.082.982.9%Moisture
Page 1 of 18Date:04/22/2023 12:19 PM
Page 24 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Total Metals
EPA-200.7
V30999,V31367QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-200.7 (PREP)
QC Prep:V30768
Associated Lab Samples: 90897
LRB-V30768 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/20/23 17:410.00600.0018<0.0018mg/LLead
LCS-V30768Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.1010.100mg/LLead 85-115
V 90899-MS-V30768 V 90899-MSD-V30768Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.106 1030.1200.1000.1000.0026mg/LLead 117 70-130 12.3 20.0
Page 2 of 18Date:04/22/2023 12:19 PM
Page 25 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
Associated Lab Samples: 90897, 90936
LRB-V30955 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/16/23 13:3710.0< 10.0µg/LAcetone
03/16/23 13:370.500< 0.500µg/LBenzene
03/16/23 13:370.500< 0.500µg/LBromobenzene
03/16/23 13:371.00< 1.00µg/LBromochloromethane
03/16/23 13:370.500< 0.500µg/LBromodichloromethane
03/16/23 13:375.00< 5.00µg/LBromoform
03/16/23 13:371.00< 1.00µg/LBromomethane
03/16/23 13:370.500< 0.500µg/Ln-Butylbenzene
03/16/23 13:370.500< 0.500µg/Lsec-Butyl benzene
03/16/23 13:372.00< 2.00µg/Ltert-Butyl benzene
03/16/23 13:370.500< 0.500µg/LCarbon Tetrachloride
03/16/23 13:370.500< 0.500µg/LChlorobenzene
03/16/23 13:370.500< 0.500µg/LChlorodibromomethane
03/16/23 13:371.00< 1.00µg/LChloroethane
03/16/23 13:370.500< 0.500µg/LChloroform
03/16/23 13:370.500< 0.500µg/LChloromethane
03/16/23 13:370.500< 0.500µg/L2-Chlorotoluene
03/16/23 13:370.500< 0.500µg/L4-Chlorotoluene
03/16/23 13:370.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
03/16/23 13:372.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
03/16/23 13:370.500< 0.500µg/LDibromomethane
03/16/23 13:370.500< 0.500µg/L1,2-Dichlorobenzene
03/16/23 13:370.500< 0.500µg/L1,3-Dichlorobenzene
03/16/23 13:370.500< 0.500µg/L1,4-Dichlorobenzene
03/16/23 13:375.00< 5.00µg/LDichlorodifluoromethane
03/16/23 13:370.500< 0.500µg/L1,1-Dichloroethane
03/16/23 13:370.500< 0.500µg/L1,2-Dichloroethane
Page 3 of 18Date:04/22/2023 12:19 PM
Page 26 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
Associated Lab Samples: 90897, 90936
LRB-V30955 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/16/23 13:370.500< 0.500µg/L1,1-Dichloroethene
03/16/23 13:370.500< 0.500µg/Lcis-1,2-Dichloroethene
03/16/23 13:370.500< 0.500µg/Ltrans-1,2-Dichloroethene
03/16/23 13:370.500< 0.500µg/L1,2-Dichloropropane
03/16/23 13:370.500< 0.500µg/L1,3-Dichloropropane
03/16/23 13:372.00< 2.00µg/L2,2-Dichloropropane
03/16/23 13:370.500< 0.500µg/L1,1-Dichloropropene
03/16/23 13:370.500< 0.500µg/Lcis-1,3-Dichloropropene
03/16/23 13:370.500< 0.500µg/Ltrans-1,3-Dichloropropene
03/16/23 13:37200< 200µg/LEthanol
03/16/23 13:370.500< 0.500µg/LEthylbenzene
03/16/23 13:373.00< 3.00µg/LHexachlorobutadiene
03/16/23 13:371.00< 1.00µg/L2-Hexanone
03/16/23 13:370.500< 0.500µg/LIsopropylbenzene
03/16/23 13:370.500< 0.500µg/L4-Isopropyl toluene
03/16/23 13:375.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
03/16/23 13:371.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
03/16/23 13:371.00< 1.00µg/L4-Methyl-2-Pentanone
03/16/23 13:372.00< 2.00µg/LMethylene Chloride
03/16/23 13:371.00< 1.00µg/LNaphthalene
03/16/23 13:370.500< 0.500µg/Ln-Propylbenzene
03/16/23 13:370.500< 0.500µg/LStyrene
03/16/23 13:3710.0< 10.0µg/Ltert-Butyl Alcohol (TBA)
03/16/23 13:3710.0< 10.0µg/Ltert-Butyl formate (TBF)
03/16/23 13:3710.0< 10.0µg/Ltert-Amyl Alcohol (TAA)
03/16/23 13:3710.0< 10.0µg/Ltert-Amyl Methyl Ether (TAME)
03/16/23 13:370.500< 0.500µg/L1,1,1,2-Tetrachloroethane
Page 4 of 18Date:04/22/2023 12:19 PM
Page 27 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
Associated Lab Samples: 90897, 90936
LRB-V30955 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/16/23 13:370.500< 0.500µg/L1,1,2,2-Tetrachloroethane
03/16/23 13:370.500< 0.500µg/LTetrachloroethene
03/16/23 13:370.500< 0.500µg/LToluene
03/16/23 13:370.500< 0.500µg/L1,2,3-Trichlorobenzene
03/16/23 13:370.500< 0.500µg/L1,2,4-Trichlorobenzene
03/16/23 13:370.500< 0.500µg/L1,1,1-Trichloroethane
03/16/23 13:370.500< 0.500µg/L1,1,2-Trichloroethane
03/16/23 13:370.500< 0.500µg/LTrichloroethene
03/16/23 13:370.500< 0.500µg/LTrichlorofluoromethane
03/16/23 13:370.500< 0.500µg/L1,2,3-Trichloropropane
03/16/23 13:370.500< 0.500µg/L1,2,4-Trimethylbenzene
03/16/23 13:370.500< 0.500µg/L1,3,5-Trimethylbenzene
03/16/23 13:375.00< 5.00µg/LVinyl Acetate
03/16/23 13:370.500< 0.500µg/LVinyl Chloride
03/16/23 13:370.500< 0.500µg/Lo-Xylene
03/16/23 13:371.00< 1.00µg/Lm,p-Xylene
03/16/23 13:3710.0< 10.0µg/L3,3-Dimethyl-1-butanol
03/16/23 13:374-Bromofluorobenzene (S)89.4 70-130
03/16/23 13:37Dibromofluoromethane (S)93.8 70-130
03/16/23 13:371,2-Dichloroethane - d4 (S)84.0 70-130
03/16/23 13:37Toluene-d8 (S)91.2 70-130
LCS-V30955 LCSD-V30955Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.7 71.771.528.640.0µg/LAcetone 40-160 0.3 20.0
Page 5 of 18Date:04/22/2023 12:19 PM
Page 28 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
LCS-V30955 LCSD-V30955Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10410721.420.0µg/LBenzene 70-130 2.8 20.0
16.5 82.585.017.020.0µg/LBromobenzene 70-130 2.9 20.0
22.4 11211022.020.0µg/LBromochloromethane 70-130 1.8 20.0
19.8 99.099.519.920.0µg/LBromodichloromethane 70-130 0.5 20.0
19.7 98.596.019.220.0µg/LBromoform 70-130 2.5 20.0
24.7 12412825.520.0µg/LBromomethane 60-140 3.1 20.0
17.7 88.595.519.120.0µg/Ln-Butylbenzene 70-130 7.6 20.0
16.9 84.592.018.420.0µg/Lsec-Butyl benzene 70-130 8.4 20.0
16.1 80.588.517.720.0µg/Ltert-Butyl benzene 70-130 9.4 20.0
21.0 10511021.920.0µg/LCarbon Tetrachloride 70-130 4.1 20.0
19.1 95.510120.220.0µg/LChlorobenzene 70-130 5.5 20.0
19.0 95.093.018.620.0µg/LChlorodibromomethane 70-130 2.1 20.0
22.0 11012124.120.0µg/LChloroethane 60-140 9.1 20.0
20.0 10010320.520.0µg/LChloroform 70-130 2.4 20.0
17.2 86.091.018.220.0µg/LChloromethane 60-140 5.6 20.0
15.9 79.584.516.920.0µg/L2-Chlorotoluene 70-130 6.0 20.0
16.1 80.586.017.220.0µg/L4-Chlorotoluene 70-130 6.6 20.0
20.3 10299.519.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.9 20.0
20.7 10486.517.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 17.8 20.0
21.6 10810120.220.0µg/LDibromomethane 70-130 6.6 20.0
17.5 87.591.018.220.0µg/L1,2-Dichlorobenzene 70-130 3.9 20.0
17.4 87.093.018.620.0µg/L1,3-Dichlorobenzene 70-130 6.6 20.0
17.0 85.090.518.120.0µg/L1,4-Dichlorobenzene 70-130 6.2 20.0
16.4 82.085.017.020.0µg/LDichlorodifluoromethane 60-140 3.5 20.0
19.8 99.092.518.520.0µg/L1,1-Dichloroethane 70-130 6.7 20.0
19.6 98.092.518.520.0µg/L1,2-Dichloroethane 70-130 5.7 20.0
Page 6 of 18Date:04/22/2023 12:19 PM
Page 29 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
LCS-V30955 LCSD-V30955Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.2 10611322.620.0µg/L1,1-Dichloroethene 70-130 6.3 20.0
19.8 99.010120.220.0µg/Lcis-1,2-Dichloroethene 70-130 2.0 20.0
19.3 96.599.519.920.0µg/Ltrans-1,2-Dichloroethene 70-130 3.0 20.0
20.8 10410521.020.0µg/L1,2-Dichloropropane 70-130 0.9 20.0
19.0 95.094.018.820.0µg/L1,3-Dichloropropane 70-130 1.0 20.0
21.3 10711322.520.0µg/L2,2-Dichloropropane 70-130 5.4 20.0
21.4 10711222.320.0µg/L1,1-Dichloropropene 70-130 4.1 20.0
21.4 10710621.120.0µg/Lcis-1,3-Dichloropropene 70-130 1.4 20.0
22.5 11310721.320.0µg/Ltrans-1,3-Dichloropropene 70-130 5.4 20.0
646 129118591500µg/LEthanol 60-140 8.8 20.0
17.8 89.093.518.720.0µg/LEthylbenzene 70-130 4.9 20.0
16.8 84.093.518.720.0µg/LHexachlorobutadiene 70-130 10.7 20.0
17.8 89.075.015.020.0µg/L2-Hexanone 60-140 17.0 20.0
16.6 83.091.018.220.0µg/LIsopropylbenzene 70-130 9.1 20.0
17.5 87.594.018.820.0µg/L4-Isopropyl toluene 70-130 7.1 20.0
17.4 87.077.015.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 12.1 20.0
21.1 10697.019.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 8.3 20.0
22.5 11397.019.420.0µg/L4-Methyl-2-Pentanone 60-140 14.7 20.0
19.1 95.597.519.520.0µg/LMethylene Chloride 70-130 2.0 20.0
21.0 10591.018.220.0µg/LNaphthalene 70-130 14.2 20.0
16.2 81.089.517.920.0µg/Ln-Propylbenzene 70-130 9.9 20.0
19.1 95.510120.120.0µg/LStyrene 70-130 5.1 20.0
46.9 11798.739.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 17.1 20.0
47.9 12011345.140.0µg/Ltert-Butyl formate (TBF)40-140 6.0 20.0
18.9 94.511222.420.0µg/Ltert-Amyl Alcohol (TAA)40-140 16.9 20.0
47.5 11996.238.540.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 20.9*20.0
Page 7 of 18* QC Fail Date:04/22/2023 12:19 PM
Page 30 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30957QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30955
LCS-V30955 LCSD-V30955Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.6 93.095.519.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.6 20.0
19.8 99.093.018.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 6.2 20.0
19.4 97.010521.020.0µg/LTetrachloroethene 70-130 7.9 20.0
21.0 10510821.520.0µg/LToluene 70-130 2.3 20.0
20.2 10194.018.820.0µg/L1,2,3-Trichlorobenzene 70-130 7.1 20.0
19.4 97.097.019.420.0µg/L1,2,4-Trichlorobenzene 70-130 0.0 20.0
19.5 97.510220.420.0µg/L1,1,1-Trichloroethane 70-130 4.5 20.0
22.7 11410520.920.0µg/L1,1,2-Trichloroethane 70-130 8.2 20.0
20.8 10410621.220.0µg/LTrichloroethene 70-130 1.9 20.0
23.1 11612224.320.0µg/LTrichlorofluoromethane 60-140 5.0 20.0
19.0 95.085.017.020.0µg/L1,2,3-Trichloropropane 70-130 11.1 20.0
16.6 83.089.017.820.0µg/L1,2,4-Trimethylbenzene 70-130 6.9 20.0
16.5 82.591.018.220.0µg/L1,3,5-Trimethylbenzene 70-130 9.7 20.0
16.6 83.089.517.920.0µg/LVinyl Acetate 60-140 7.5 20.0
20.2 10110420.720.0µg/LVinyl Chloride 60-140 2.4 20.0
17.9 89.595.519.120.0µg/Lo-Xylene 70-130 6.4 20.0
37.6 94.010040.140.0µg/Lm,p-Xylene 70-130 6.4 20.0
19.1 95.591.018.220.0µg/L3,3-Dimethyl-1-butanol 70-130 4.8 20.0
90.890.44-Bromofluorobenzene (S)70-130
95.494.6Dibromofluoromethane (S)70-130
92.082.01,2-Dichloroethane - d4 (S)70-130
90.893.8Toluene-d8 (S)70-130
Page 8 of 18Date:04/22/2023 12:19 PM
Page 31 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V30984QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V30983
Associated Lab Samples: 90897
LRB-V30983 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/17/23 15:3510.0< 10.0µg/Ltert-Butyl Alcohol (TBA)
03/17/23 15:354-Bromofluorobenzene (S)96.0 70-130
03/17/23 15:35Dibromofluoromethane (S)87.4 70-130
03/17/23 15:351,2-Dichloroethane - d4 (S)89.6 70-130
03/17/23 15:35Toluene-d8 (S)98.0 70-130
LCS-V30983 LCSD-V30983Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.6 81.581.232.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.3 20.0
98.298.24-Bromofluorobenzene (S)70-130
87.487.0Dibromofluoromethane (S)70-130
90.490.01,2-Dichloroethane - d4 (S)70-130
97.697.8Toluene-d8 (S)70-130
Page 9 of 18Date:04/22/2023 12:19 PM
Page 32 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
Associated Lab Samples: 90896
LRB-V30834 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 15:480.0200.002<0.002mg/KgAcetone
03/13/23 15:480.0200.001<0.001mg/KgAcrolein
03/13/23 15:480.0200.0008<0.0008mg/KgAcrylonitrile
03/13/23 15:480.0050.0006<0.0006mg/KgBenzene
03/13/23 15:480.0050.0005<0.0005mg/KgBromobenzene
03/13/23 15:480.0050.0008<0.0008mg/KgBromochloromethane
03/13/23 15:480.0050.001<0.001mg/KgBromodichloromethane
03/13/23 15:480.0050.001<0.001mg/KgBromoform
03/13/23 15:480.0100.001<0.001mg/KgBromomethane
03/13/23 15:480.0050.0005<0.0005mg/Kgn-Butylbenzene
03/13/23 15:480.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/13/23 15:480.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/13/23 15:480.0050.0006<0.0006mg/KgCarbon Disulfide
03/13/23 15:480.0050.001<0.001mg/KgCarbon Tetrachloride
03/13/23 15:480.0050.0007<0.0007mg/KgChlorobenzene
03/13/23 15:480.0050.0009<0.0009mg/KgChlorodibromomethane
03/13/23 15:480.0100.0009<0.0009mg/KgChloroethane
03/13/23 15:480.0050.001<0.001mg/KgChloroform
03/13/23 15:480.0100.0006<0.0006mg/KgChloromethane
03/13/23 15:480.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/13/23 15:480.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/13/23 15:480.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/13/23 15:480.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/13/23 15:480.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/13/23 15:480.0050.0010<0.0010mg/KgDibromomethane
03/13/23 15:480.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/13/23 15:480.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 18Date:04/22/2023 12:19 PM
Page 33 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
Associated Lab Samples: 90896
LRB-V30834 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 15:480.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/13/23 15:480.0100.001<0.001mg/KgDichlorodifluoromethane
03/13/23 15:480.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/13/23 15:480.0050.001<0.001mg/Kg1,2-Dichloroethane
03/13/23 15:480.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/13/23 15:480.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/13/23 15:480.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/13/23 15:480.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/13/23 15:480.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/13/23 15:480.0050.001<0.001mg/Kg2,2-Dichloropropane
03/13/23 15:480.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/13/23 15:480.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/13/23 15:480.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/13/23 15:480.0050.0006<0.0006mg/KgEthylbenzene
03/13/23 15:480.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/13/23 15:480.0100.0008<0.0008mg/KgHexachlorobutadiene
03/13/23 15:480.0100.0007<0.0007mg/Kgn-Hexane
03/13/23 15:480.0200.0006<0.0006mg/Kg2-Hexanone
03/13/23 15:480.0050.0005<0.0005mg/KgIsopropylbenzene
03/13/23 15:480.0050.001<0.001mg/Kg4-Isopropyl toluene
03/13/23 15:480.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/13/23 15:480.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/13/23 15:480.0050.001<0.001mg/KgMethylene Chloride
03/13/23 15:480.0100.0010<0.0010mg/KgNaphthalene
03/13/23 15:480.0050.0005<0.0005mg/Kgn-Propylbenzene
03/13/23 15:480.0050.001<0.001mg/KgStyrene
03/13/23 15:480.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 11 of 18Date:04/22/2023 12:19 PM
Page 34 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
Associated Lab Samples: 90896
LRB-V30834 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 15:480.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/13/23 15:480.0050.0009<0.0009mg/KgTetrachloroethene
03/13/23 15:480.0050.0007<0.0007mg/KgToluene
03/13/23 15:480.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/13/23 15:480.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/13/23 15:480.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/13/23 15:480.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/13/23 15:480.0050.0009<0.0009mg/KgTrichloroethene
03/13/23 15:480.0100.002<0.002mg/KgTrichlorofluoromethane
03/13/23 15:480.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/13/23 15:480.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/13/23 15:480.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/13/23 15:480.0100.0005<0.0005mg/KgVinyl Acetate
03/13/23 15:480.0100.0005<0.0005mg/KgVinyl Chloride
03/13/23 15:480.0050.0005<0.0005mg/Kgo-Xylene
03/13/23 15:480.0100.001<0.001mg/Kgm,p-Xylene
03/13/23 15:484-Bromofluorobenzene (S)101 70-130
03/13/23 15:48Dibromofluoromethane (S)100 70-130
03/13/23 15:48Toluene-d8 (S)100 76-129
LCS-V30834 LCSD-V30834Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031010.1010.100mg/KgAcetone 29-198 1.9 20
0.092 92.390.10.0900.100mg/KgAcrolein 70-130 2.4 20
0.107 1071080.1080.100mg/KgAcrylonitrile 65-134 0.9 20
Page 12 of 18Date:04/22/2023 12:19 PM
Page 35 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
LCS-V30834 LCSD-V30834Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.490.80.0450.050mg/KgBenzene 74-127 1.7 20
0.044 89.090.60.0450.050mg/KgBromobenzene 73-125 1.7 20
0.048 96.895.00.0470.050mg/KgBromochloromethane 72-134 1.8 20
0.046 93.692.00.0460.050mg/KgBromodichloromethane 75-122 1.7 20
0.048 97.093.60.0460.050mg/KgBromoform 66-135 3.5 20
0.045 90.093.00.0460.050mg/KgBromomethane 20-180 3.2 20
0.045 91.895.80.0470.050mg/Kgn-Butylbenzene 65-135 4.2 20
0.043 87.490.80.0450.050mg/Kgsec-Butyl benzene 66-131 3.8 20
0.044 89.490.60.0450.050mg/Kgtert-Butyl benzene 67-132 1.3 20
0.044 89.292.60.0460.050mg/KgCarbon Disulfide 61-129 3.7 20
0.044 89.491.80.0450.050mg/KgCarbon Tetrachloride 64-143 2.6 20
0.046 92.092.40.0460.050mg/KgChlorobenzene 74-118 0.4 20
0.046 93.891.40.0450.050mg/KgChlorodibromomethane 73-122 2.5 20
0.049 98.41000.0500.050mg/KgChloroethane 33-149 1.8 20
0.045 90.691.20.0450.050mg/KgChloroform 73-127 0.6 20
0.047 95.697.00.0480.050mg/KgChloromethane 45-143 1.4 20
0.045 90.291.60.0450.050mg/Kg2-Chlorotoluene 67-124 1.5 20
0.045 90.291.80.0450.050mg/Kg4-Chlorotoluene 71-126 1.7 20
0.046 92.291.40.0450.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.8 20
0.044 88.885.60.0420.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.6 20
0.048 96.695.80.0470.050mg/Kg1,2-Dibromoethane 70-132 0.8 20
0.046 93.692.40.0460.050mg/KgDibromomethane 74-133 1.2 20
0.046 92.293.00.0460.050mg/Kg1,2-Dichlorobenzene 72-123 0.8 20
0.045 91.694.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 3.4 20
0.045 90.490.40.0450.050mg/Kg1,4-Dichlorobenzene 71-123 0.0 20
0.042 84.687.00.0430.050mg/KgDichlorodifluoromethane 26-146 2.7 20
Page 13 of 18Date:04/22/2023 12:19 PM
Page 36 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
LCS-V30834 LCSD-V30834Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.091.80.0450.050mg/Kg1,1-Dichloroethane 74-127 0.8 20
0.046 93.491.40.0450.050mg/Kg1,2-Dichloroethane 68-128 2.1 20
0.045 90.892.60.0460.050mg/Kg1,1-Dichloroethene 67-149 1.9 20
0.046 93.092.40.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 0.6 20
0.046 93.692.80.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 0.8 20
0.046 92.691.80.0450.050mg/Kg1,2-Dichloropropane 73-130 0.8 20
0.047 94.894.40.0470.050mg/Kg1,3-Dichloropropane 75-124 0.4 20
0.045 90.691.20.0450.050mg/Kg2,2-Dichloropropane 50-142 0.6 20
0.045 91.291.80.0450.050mg/Kg1,1-Dichloropropene 71-130 0.6 20
0.047 95.293.60.0460.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.049 99.097.00.0480.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.0 20
0.044 88.291.80.0450.050mg/KgEthylbenzene 74-128 4.0 20
0.092 92.591.30.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.3 20
0.046 93.41010.0500.050mg/KgHexachlorobutadiene 64-125 7.4 20
0.046 92.492.60.0460.050mg/Kgn-Hexane 70-130 0.2 20
0.048 96.095.40.0470.050mg/Kg2-Hexanone 61-157 0.6 20
0.044 88.089.80.0440.050mg/KgIsopropylbenzene 68-126 2.0 20
0.044 89.291.80.0450.050mg/Kg4-Isopropyl toluene 68-129 2.8 20
0.039 79.681.00.0400.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.7 20
0.046 92.889.40.0440.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.7 20
0.044 88.885.80.0420.050mg/KgMethylene Chloride 74-129 3.4 20
0.047 94.895.40.0470.050mg/KgNaphthalene 57-157 0.6 20
0.043 87.091.20.0450.050mg/Kgn-Propylbenzene 67-130 4.7 20
0.046 92.494.60.0470.050mg/KgStyrene 77-121 2.3 20
0.046 92.491.80.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.6 20
0.043 87.485.00.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.7 20
Page 14 of 18Date:04/22/2023 12:19 PM
Page 37 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30835QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30834
LCS-V30834 LCSD-V30834Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.696.20.0480.050mg/KgTetrachloroethene 68-130 4.8 20
0.044 89.689.40.0440.050mg/KgToluene 71-129 0.2 20
0.046 93.496.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.1 20
0.048 97.299.20.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.0 20
0.044 88.888.80.0440.050mg/Kg1,1,1-Trichloroethane 67-131 0.0 20
0.046 92.492.80.0460.050mg/Kg1,1,2-Trichloroethane 70-133 0.4 20
0.045 91.292.80.0460.050mg/KgTrichloroethene 75-133 1.7 20
0.046 92.494.60.0470.050mg/KgTrichlorofluoromethane 44-146 2.3 20
0.045 90.288.40.0440.050mg/Kg1,2,3-Trichloropropane 60-137 2.0 20
0.043 87.690.40.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.1 20
0.043 87.490.00.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.9 20
0.053 1071150.0570.050mg/KgVinyl Acetate 60-140 7.0 20
0.045 91.091.60.0450.050mg/KgVinyl Chloride 48-147 0.6 20
0.045 90.692.00.0460.050mg/Kgo-Xylene 74-126 1.5 20
0.089 89.792.20.0920.100mg/Kgm,p-Xylene 75-124 2.7 20
10097.64-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)70-130
99.0103Toluene-d8 (S)76-129
Page 15 of 18Date:04/22/2023 12:19 PM
Page 38 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V30816QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V30754
Associated Lab Samples: 90897
LRB-V30754 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
03/14/23 12:140.0200< 0.0200µg/L1,2-Dibromoethane
LCS-V30754 LCSD-V30754Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.240 96.01020.2560.250µg/L1,2-Dibromoethane 70-130 6.4 20.0
V 90543-DUP-V30754Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/14/23 14:030.0< 0.00394< 0.0239µg/L1,2-Dibromoethane
V 90542-MS-V30754Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.139 44.8*0.310< 0.0248µg/L1,2-Dibromoethane 70-130
Page 16 of 18Date:04/22/2023 12:19 PM
Page 39 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V30784QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V30783
Associated Lab Samples: 90896
LRB-V30783 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 16:038.00<8.00mg/KgAliphatic C5-C8
03/13/23 16:038.00<8.00mg/KgAliphatic C9-C12
03/13/23 16:038.00<8.00mg/KgAromatic C9-C10
03/13/23 16:032,5-Dibromotoluene (FID) (S)83.1 70-130
03/13/23 16:032,5-Dibromotoluene (PID) (S)81.5 70-130
LCS-V30783 LCSD-V30783Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.8 90.085.927.532.0mg/KgAliphatic C5-C8 70-130 4.6 50
39.6 12412038.332.0mg/KgAliphatic C9-C12 70-130 3.3 50
11.7 10910411.110.7mg/KgAromatic C9-C10 70-130 5.2 50
84.387.52,5-Dibromotoluene (FID) (S)70-130
76.580.72,5-Dibromotoluene (PID) (S)70-130
Page 17 of 18Date:04/22/2023 12:19 PM
Page 40 of 43
Quality Control Data
23-069-9024Report No:
Project Description:
Client ID:Resolve Environmental
Express Lane Petro
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V30794QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V30792
Associated Lab Samples: 90897
LRB-V30792 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/14/23 12:5650.0< 50.0µg/LAliphatic C5-C8
03/14/23 12:5650.0< 50.0µg/LAliphatic C9-C12
03/14/23 12:5650.0< 50.0µg/LAromatic C9-C10
03/14/23 12:562,5-Dibromotoluene (FID) (S)102 70-130
03/14/23 12:562,5-Dibromotoluene (PID) (S)96.0 70-130
LCS-V30792 LCSD-V30792Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
315 105103310300µg/LAliphatic C5-C8 70-130 1.6 50.0
359 120119356300µg/LAliphatic C9-C12 70-130 0.8 50.0
108 108104104100µg/LAromatic C9-C10 70-130 3.7 50.0
84.188.92,5-Dibromotoluene (FID) (S)70-130
79.181.12,5-Dibromotoluene (PID) (S)70-130
Page 18 of 18Date:04/22/2023 12:19 PM
Page 41 of 43
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-069-0024
Resolve Environmental
00238
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.5c
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Trip Blank was included but not listed on the COC. Proceed with analysis per
Scott Ball.
Signature:Danyale Love Date & Time:03/10/2023 15:28:47
Special precautions or instructions included?
Comments:
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