FA-29655_48901_CA_20-Day_20230329

Groundwater & Environmental Services, Inc.
104 Corporate Boulevard, Suite 411
West Columbia, SC 29169
T. 866.765.4851

GESonline.com
March 29, 2023
Liz Price
Hydrogeologist
NCDEQ – DWM – UST Section – WiRO
127 Cardinal Drive Extension
Wilmington, North Carolina 28405

Re: Murphy USA #8549
4993 NC Highway 42 West
Garner, Johnston County
Incident Number: 48901
Dear Ms. Price:
Groundwater & Environmental Services, Inc., on behalf of Murphy Oil USA, Inc., is providing the
enclosed 20-Day Report for the referenced site for your review and approval. Should you have
any questions, please do not hesitate to contact the undersigned by phone at [phone]
x4524 or by email at [e-mail].
Sincerely,
Groundwater & Environmental Services, Inc.

Aaron R. Williamson, P.G. Daniel Dabkowski
Staff Geologist Senior Project Manager

Cc: Ryan Pederson, Murphy Oil USA, Inc. (electronic)
Enclosure: 20-Day Report

Murphy Oil USA, Inc.

20-Day Report
Murphy USA # 8549
4993 NC Highway 42 West
Garner, Johnston County, North Carolina 27529
NCDEQ Incident #48901

March 29, 2023

Version 1

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page i

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, North Carolina 27529
Prepared for:
Murphy Oil USA, Inc.
200 Peach Street, PO Box 7300
El Dorado, Arkansas 71731
Prepared by:
Groundwater & Environmental Services, Inc.
104 Corporate Boulevard – Suite 411
West Columbia, South Carolina 29169
TEL: [phone]
www.gesonline.com
GES Project:
2701997
Date:
March 29, 2023

Aaron R Williamson, PG
Staff Geologist

Daniel Dabkowski
Senior Project Manager

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page ii

Table of Contents
1 Introduction ......................................................................................................................... 1
2 Site History and Characterization ........................................................................................ 1
2.1 Owner/Operator Information ........................................................................................... 1
2.2 UST System Information ................................................................................................ 1
2.3 Past Releases ................................................................................................................ 1
2.4 Current Release ............................................................................................................. 1
2.5 Site Characteristics......................................................................................................... 2
3 Initial Response and Abatement Activities ........................................................................... 3
3.1 Tightness Testing – December 19, 2022 & January 10, 2023 ......................................... 3
3.2 Site Check – February 20-24, 2023 ................................................................................ 3
3.3 Laboratory Analytical Results – March 7, 2023 ............................................................... 4
3.4 Release Reporting – March 8, 2023 ............................................................................... 4
4 Source Investigation & Further Action ................................................................................. 5
5 References ......................................................................................................................... 5

Figures
Figure 1 – Site Location Map
Figure 2 – Site Map
Figure 3 – Sample Location Map
Tables
Table 1 – Site History – UST Owner/Operator & Other Responsible Party Information
Table 2 – UST System & Other Release Information
Appendices
Appendix A – Relevant Correspondence
Appendix B – Tank Tightness Testing Results
Appendix C – Laboratory Analytical Report
Appendix D – 24-hr Release Reporting Form

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page iii

Acronyms
AST Aboveground Storage Tank
BGS Below Ground Surface
EPA U.S. Environmental Protection Agency
EPH Extractable Petroleum Hydrocarbons
GES Groundwater & Environmental Services, Inc.
MADEP Massachusetts Department of Environmental Protection
NCDEQ North Carolina Department of Environmental Quality
NORR Notice of Regulatory Requirements
PVC Polyvinyl Chloride
STP Submersible Turbine Pump
SWAP Source Water Assessment Program
TPH-GRO Total Petroleum Hydrocarbons – Gasoline Range Organics
TPH-DRO Total Petroleum Hydrocarbons – Diesel Range Organics
UST Underground Storage Tank
VOC Volatile Organic Compound
VPH Volatile Petroleum Hydrocarbons

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page iv

SITE INFORMATION
Date of Report: March 29, 2023
SITE IDENTIFICATION
Facility ID: 00-0-0000037042
UST Incident No: 48901
Site Risk: Not Determined
Agency Contact: Liz Price, NCDEQ, Wilmington Regional Office
Site Name: Murphy Express #8549
Site Street Address: 4993 NC Highway 42 West
Garner, North Carolina 27529
County: Johnston
Latitude / Longitude: 35.611320° / -78.553754° (UST Database)

SITE CONTACT INFORMATION
UST Owner/Operator: Murphy USA, Inc.
Address: 200 Peach Street / PO Box 7300
El Dorado, AR 71731
Telephone: [phone]
Contact: Ryan Pederson, Rem. & Env. Risk Manager

Property Owner: Murphy Oil USA, Inc.
Address: PO Box 7300
El Dorado, AR 71731
Telephone [phone]
Contact Ryan Pederson

Consultant: Groundwater & Environmental Services, Inc.
Address: 104 Corporate Boulevard, Suite 411
West Columbia, SC 29169
Telephone: [phone]
NC License No: C-353 (Geology) & C-2236 (Engineering)

Analytical Laboratory: SGS North America, Inc.
Address: 4405 Vineland Road, Suite C-15, Orlando, FL 32811
Telephone: [phone]
State Certification No: 573

INFORMATION ABOUT THE RELEASE
Date Discovered: March 8, 2023
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: UST System
UST(s) Size & Contents: See Table 2

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page v

CERTIFICATION
I, Aaron R. Williamson, a Licensed Geologist employed by Groundwater & Environmental
Services, Inc. do certify that the information contained in this report is correct and accurate to the
best of my knowledge.

Aaron R. Williamson, P.G.
P.G. License No. 2712

Groundwater & Environmental Services, Inc. is licensed to practice geology in North Carolina.
The certification number of the company or corporation to practice geology is C-353.

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page vi

EXECUTIVE SUMMARY
As required, the following executive summary provides the most pertinent information discussed
in this report. For additional information please refer to subsequent sections of this report.
 A release of petroleum product from the tank system was suspected due to groundwater
contamination discovered on an adjacent property.
 No prior release incidents were identified.
 Tank tightness testing indicated passing conditions.
 Results of a site check indicated soil contamination was present near the tank system.
 Based on initial soil analytical data, a release of petroleum product from the tank system was
reported to the regulatory agency on March 8, 2023.
 No sensitive environmental receptors have been identified to date.
 Based on depth of the soil contamination and proximity to the active tank system, soil
excavation is deemed infeasible.
 An Initial Abatement Action Report is being prepared with complete results of the site check.

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page 1

1 Introduction
Groundwater & Environmental Services, Inc. (GES) was retained by Murphy Oil USA, Inc.
(Murphy) to provide assessment and required regulatory reporting associated with a suspected
release of petroleum product at the Murphy USA #8549 facility located at 4993 NC Highway 42
West in Garner, Johnston County, North Carolina (site). The site location is illustrated on Figure
1. The purpose of this “20-Day Report” is to provide a progress update of initial response and
abatement actions performed within the first 20-days following discovery of the release.
2 Site History and Characterization
The site is located at the southeast corner of the intersection of NC Highway 42 West and Bratton
Drive. The site currently operates as a Murphy Express gas station and convenience store with
an active underground storage tank (UST) system. No aboveground storage tank (AST) systems
are present at the site.
2.1 Owner/Operator Information
The UST system at the site is currently owned and operated by Murphy. Murphy has owned and
operated the UST system since it was installed in 2009. UST owner/operator information is
summarized in Table 1.
2.2 UST System Information
UST system information is summarized in Table 2 and illustrated on Figure 2. The system
consists of 3 USTs within a common tank pit generally oriented northeast to southwest located
within the northeastern quarter of the site the property, approximately 50 feet from the site
property boundaries. The USTs utilize separate sumps for the fill ports and submersible turbine
pumps (STPs).
Eight (8) dispenser islands are located beneath a dispenser canopy trending northeast to
southwest. Double-sided gasoline dispensers are present at each dispenser island. Double-sided
diesel dispensers are coupled with the gasoline dispensers at the southwestern most and
southeastern most dispenser islands.
2.3 Past Releases
GES reviewed the North Carolina Department of Environmental Quality (NCDEQ) UST Incident
Management Database pertaining to past releases at the site. No past releases at the site were
found to be on file with the NCDEQ.
2.4 Current Release
The NCDEQ issued a Notice of Regulatory Requirements (NORR) on December 16, 2022
directing tank tightness testing and a site check due to petroleum compounds detected in
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page 2

groundwater at The Car Wash Lodge on the adjacent property to the east of the site. A copy of
this correspondence is included in Appendix A. The site check was performed in February of
2023 and confirmed contamination near the site UST system, however the exact date and nature
of the release are unknown.
2.5 Site Characteristics
The site currently operates as Murphy USA #8549, an active convenience store and fueling
station with unbranded petroleum fuel. The convenience store is constructed with a slab on grade
foundation. The site is utilized for commercial purposes with adjoining properties to the east,
south, and west also utilized as commercial purposes. Adjoining property to the north, across NC
Highway 42 West, is undeveloped. The nearest residential structures are located approximately
925 to 950-ft north and west of the USTs.
Municipal water appears to be supplied to the site and nearby properties by the Johnston County
West Public Water System (PWS ID NC0351070). The source of municipal water for this system
is reported to be surface water intake from the Neuse River near Wilsons Mills approximately 13-
miles east of the site.
A cursory windshield receptor survey identified no suspect water supply wells on or adjacent to
the site, however a complete receptor survey has not been completed as of the time of this report.
The NCDEQ Source Water Assessment Program (SWAP) Info 2.0 database indicates no water
wells or wellhead protection areas are present within 1,500-ft of the site.
Site topography is relatively flat resting at an elevation of approximately 220 to 230-feet above
sea level, but land surface in the vicinity of the site slopes towards the east. Regional surface
drainage appears to trend towards the east. Surface cover at the site consists primarily of concrete
with landscaped areas along the perimeter. Surface runoff from paved areas of the site flows
towards two (2) storm drain inlets near the central east and west sides of the site, and is then
routed to an off-site storm sewer system near the southeastern corner of the site which appears
to discharge to a stormwater detention basin south of the site. Final disposition of the storm water
is beyond the scope of this assessment.
The nearest natural surface water body appears to be Swift Creek located approximately 1,400-
ft east of the USTs. No other surface water bodies were identified within 1,500-ft of the site.
Underground utility lines on and near the site include the UST system, municipal water, irrigation,
sanitary sewer, storm sewer, communications, and electric as illustrated on Figure 2.
Groundwater is encountered at approximately 32-ft below ground surface (BGS). The site is
located in the Piedmont physiographic province of NC and thickness of the surficial aquifer is
unknown. Depth to bedrock beneath the site is unknown but is reported to be intrusive rock of the
Raleigh Belt described as foliated to massive granitic rock of the Rolesville suite. Regional
groundwater flow is expected to follow surficial topography towards the east.
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page 3

3 Initial Response and Abatement Activities
In conducting initial response and abatement activities at the site, the most recent revision of the
NCDEQ “Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases” (STIRA Guidelines) was referenced.
3.1 Tightness Testing – December 19, 2022 & January 10, 2023
In response to the NORR dated December 16, 2022, Murphy performed tightness testing on the
UST system on December 19, 2022 and January 10, 2023. Results of the testing indicated
passing conditions. The testing documentation is included in Appendix B.
3.2 Site Check – February 20-24, 2023
GES mobilized to the site with a private utility locator and NC licensed driller on February 20, 2023
for advancement of soil borings adjacent to the UST system per STIRA Guidelines. Between
February 20 and February 23, 2023, a total of 40 soil borings were advanced at the site as follows:
 Adjacent to each dispenser (10);
 Approximately every 10-ft along the perimeter of the USTs (16);
 Approximately every 10-ft along product piping runs (14).
Boring locations are illustrated on Figure 3 and were adjusted where needed for the presence of
underground utilities. Borings were advanced to at least two (2) ft below the depth of the UST
system component being assessed. Soils were continuously classified and logged, and field
screening samples were collected at approximately two (2) ft intervals from each soil boring. One
(1) soil sample was retained from each boring for laboratory analysis from the depth interval
exhibiting the highest field screening reading above the water table. All soil borings were
abandoned following sample collection activities.
Pea gravel backfill material was encountered in nearly all soil borings, ranged in thickness from
approximately 0.5 to 8-ft, and was encountered at a maximum depth of 16-ft BGS in soil borings
SB-6, SB-7, and SB-9. Soil samples were collected below the base of pea gravel where
encountered. Soil boring SB-15 was advanced to approximately 30-ft BGS and groundwater was
encountered between approximately 25 and 30-ft BGS. The primary soil type encountered during
soil boring activities was silty and clayey sands with rock fragments.
Due to the presence of pea gravel backfill materials around the UST system components, a
permanent monitoring well was installed in the assumed downgradient location of the soil boring
exhibiting the highest field screening result. The monitoring well was constructed to a total depth
of approximately 35-ft BGS using 15-ft of 2-inch diameter polyvinyl chloride (PVC) screen and 20-
ft of 2-inch diameter PVC riser. The well was completed flush with ground surface using an 8-inch
steel vault set in a concrete pad and developed on February 23, 2023. The well was gauged,
purged, and sampled on February 24, 2023; depth to water at this time was reported to be
approximately 31.5-ft BGS.
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page 4

To reduce the potential of cross contamination, dedicated nitrile gloves were worn during all
phases of sample handling. Non-disposable sampling equipment was decontaminated using a
non-phosphate detergent and potable water. Each laboratory sample was placed into pre-cleaned
laboratory provided containers pre-filled with appropriate preservatives, labeled with indelible ink,
entered into chain-of-custody, immediately placed on wet ice in a cooler maintained at
approximately four (4) degrees Celsius (°C), and transported to the contract laboratory under
standard chain-of-custody protocol for analysis. The samples were submitted to SGS North
America, Inc. (SGS) of Orlando, FL, a NCDEQ accredited laboratory (#573), for analyses as
follows:
 Soils
o Total Petroleum Hydrocarbons – Gasoline Range Organics (TPH-GRO) and Total
Petroleum Hydrocarbons – Diesel Range Organics (TPH-DRO) by U.S.
Environmental Protection Agency (EPA) Method 8015;
o Volatile organic compounds (VOCs) by EPA Method 8260.
 Groundwater
o VOCs by Standard Methods 6200;
o Ethylene dibromide by EPA Method 504.1;
o Bases, neutrals, and acids by EPA Method 625;
o Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons
(EPH) by Massachusetts Department of Environmental Protection (MADEP)
Methods;
o Lead by EPA Method 6010.
Investigative derived soil and groundwater waste was disposed of on-site as a deemed permitted
waste per NCDEQ UST guidelines.
3.3 Laboratory Analytical Results – March 7, 2023
The initial laboratory analytical report for soil samples collected on February 20, 2023 was
received from SGS on March 7, 2023; this laboratory report was later revised and reissued by
SGS on March 21, 2023 to correct an analyte reporting error and is included in Appendix C. The
analytical data was compared to the NCDEQ action levels and maximum soil contaminant
concentrations. Regulatory exceedances for TPH-GRO and various VOCs were reported in soil
samples SB-1, SB-6, and SB-7 which are all located near the northeast corner of the UST pit and
were collected at depths ranging from approximately 18 to 20-ft BGS.
3.4 Release Reporting – March 8, 2023
Due to regulatory exceedances observed by GES during review of the initial laboratory results
received on March 7, 2023, a release was reported via email to Ms. Liz Price of the NCDEQ on
March 8, 2023. The 24-hr Release Reporting Form and transmittal are included in Appendix D.
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Page 5

4 Source Investigation & Further Action
The exact source, cause, volume, and date of the release from the UST system is not determined
but currently known soil impacts including TPH-GRO suggest a previously unreported leak or spill
of gasoline within or near the UST pit. Complete results of the site check performed at the site will
be presented in the Initial Abatement Action Report and will include laboratory reports for all
samples, tabulated data, boring logs, groundwater sampling logs, additional figures, and
documentation of the known extent of contamination. Due to the depth of the impacted soils and
proximity to the active UST system, soil excavation is deemed infeasible.
5 References
 NCDEQ UST Databases & Reports website, accessed March 28, 2023:
https://deq.nc.gov/about/divisions/waste-management/underground-storage-tanks-
section/underground-storage-tank-databases-and-reports
 Johnston County website, accessed March 28, 2023: https://johnstonnc.com/
 NCDEQ Public Water Supply - Source Water Assessment Report website for Johnston
Co-West, accessed March 28, 2023: https://www.ncwater.org/?page=600
 NCDEQ SWAPInfo 2.0 website accessed March 28, 2023:
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=26f4e2b3140f4e5882
5e48781ccebf5e
 North Carolina Geological Survey, 1985, Geologic Map of North Carolina: Raleigh, North
Carolina Department of Natural Resources and Community Development, Geological
Survey Section, scale 1:500,000, in color.

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Figures

Murphy USA #8549
4993 NC Highway 42 West
Garner, North Carolina 27529
Site Location Map
Quadrangle Location
SITE
Source:
USGS 7.5 Minute Series
Topographic Quadrangle,
Edmondson, North Carolina
Contour Interval =
1999
10'
North Carolina
Designed
Approved
Scale In Feet
0 2000
W.G.S.
Drawn
N
Figure
2/20/23
Date
Groundwater & Environmental Services, Inc.M:\Graphics\2700-Columbia\MISC\Murphy Oil USA\8549 Garner\8549 Garner SLM.dwg, SLM, WSheaA.W.
D.D.
1
Murphy USA #8549
4993 NC Highway 42 West Garner, North Carolina 27529
Site Map
Designed
Approved
Scale In Feet
0 40
W.G.S.
Drawn
N
Figure
2/27/23
Date
Groundwater & Environmental Services, Inc.M:\Graphics\2700-Columbia\MISC\Murphy Oil USA\8549 Garner\8549 Garner SM.dwg, B40sm, WShea#2
#1
#3A
#3B The Ca
r
Wash
Lodge
2A.W.
D.D.
Sample Location Map
Murphy USA
Station #8549
4993 NC-42 W
Garner, North Carolina
Designed
Approved
Scale In Feet
0 20
W.G.S.
Drawn
N
Figure
3/6/23
Date
Groundwater & Environmental Services, Inc.M:\Graphics\2700-Columbia\MISC\Murphy Oil USA\8549 Garner\8549 Garner SM.dwg, B20soil, WSheaA.W.
D.D.
3
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Tables

20-Day Report
Murphy USA #8549
4993 NC Highway 42 West, Garner, NC, 27529
UST ID Number 1, 2, 3A, 3B Facility ID Number 00-0-0000037042
City State Zip Telephone Number
El Dorado AR 71730 [phone]
City State Zip Telephone Number
El Dorado AR 71730 [phone]
Incident Number None Date Incident Occurred N/A
Date Incident Report N/A
Date Incident Closed N/A
City State Zip Telephone Number
N/A N/A N/A N/A
*Tank owner/operator records indicate tank installation date of 09/27/2009; NCDEQ records indicating the earlier date are reported here.
TABLE 1
SITE HISTORY - UST OWNER / OPERATOR & OTHER RESPONSIBLE PARTY INFORMATION
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)*
Murphy Oil USA, Inc.08/26/2009 to Present
Street Address
200 Peach Street / PO Box 7300
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)*
Murphy Oil USA, Inc.08/26/2009 to Present
N/A
Street Address
200 Peach Street / PO Box 7300
Other Incidents Onsite or Commingled/In Close Proximity
Name of Other Responsible Party
N/A
Street Address
Privileged and Confidential Page 1 of 1
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West, Garner, NC, 27529
UST ID
Number*
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
(feet)
Description of
Associated Piping
and Pumps
Date Tank
Installed**
Status of
UST
Was Release
Associated with
the UST System?
1 Gasoline (Regular)N/A 20,000 DW FRP Unknown FRP/Pressure 8/26/09 Active Unknown
2 Gasoline (Regular)N/A 20,000 DW FRP Unknown FRP/Pressure 8/26/09 Active Unknown
3A Diesel N/A 12,000 DW FRP Unknown FRP/Pressure 8/26/09 Active Unknown
3B Gasoline (Premium)N/A 8,000 DW FRP Unknown FRP/Pressure 8/26/09 Active Unknown
AST ID Number
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated Piping
and Pumps
Date Tank
Installed
Status of
AST
Was Release
Associated with
the AST System?
Incident
Number Material Released Date of Release
None N/A N/A
Notes:
FRP = Fiberglass Reinforced Plastic
DW = Double Wall
*Keyed to Figure 2.
**Tank owner/operator records indicate tank installation date of 09/27/2009; NCDEQ records indicating the earlier date are reported here.
TABLE 2
UST SYSTEM AND OTHER RELEASE INFORMATION
None
Descrtiption of Release
N/A
Privileged and Confidential Page 1 of 1
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Appendix A – Relevant Correspondence

North Carolina Department of Environmental Quality | Division of Waste Management
Wilmington Regional Office | 127 Cardinal Drive Extension | Wilmington, NC 28405 | [phone]
December 16, 2022

CERTIFIED MAIL 7021 2720 0002 3808 2925
RETURN RECEIPT REQUESTED
Christopher A. Click, Executive Director
Murphy Oil USA, Inc.
200 Peach Street
El Dorado, AR 71730-5836
Re: Notice of Regulatory Requirements
15A NCAC 02N .0602 and .0603
Investigation and Confirmation of a Suspected
Release from an Underground Storage Tank

Murphy Express #8549
4993 NC 42 HWY West, Garner
Johnston County
Facility ID#: 00-0-0000037042
Incident Number: Pending
Risk Classification: Pending
Ranking: Pending

Dear Click:
Information received by the Wilmington Regional Office of the UST Section, Division of Waste
Management, on December 9, 2022 indicates the potential for a suspected release, from the subject facility,
due to the discovery of offsite impacts, including the detection of petroleum compounds on offsite property
monitoring wells.
Records indicate that you are the owner or operator of a UST system suspected of being the source for this
release. Therefore, you must immediately investigate to confirm the suspected release pursuant to Title 15A
NCAC 02N .0603. To achieve compliance with this rule, you must:
1. conduct tank tightness tests for each UST in accordance with federal regulation 40 CFR
280.43(c) (as incorporated by Title 15A NCAC 02N .0504),

2. conduct line tightness tests for each piping system associated with a UST in accordance
with 40 CFR 280.44(b) (as incorporated by Title 15A NCAC 02N .0505), and
3. conduct a site check in accordance with 40 CFR 280.52(b) (as incorporated by Title 15A
NCAC 02N .0603) as described in the most recent version of the Guidelines for Site
Checks, Tank Closure, and Initial Response and Abatement Action, as available at
https://deq.nc.gov/about/divisions/waste-management/underground-storage-tanks-
section/ust-guidance-documents .
The results of the tank tightness test(s) and line tightness test(s) must be received by this office within 7
days of receipt of this notice. The results of the site check must be received by this office within 30 days of
receipt of this notice. If a release or discharge is confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department of Environmental Quality in accordance with Title 15A NCAC 02L .0103(e) and 02L .0111(e).
Failure to comply in the manner and time specified may result in the assessment of civil penalties
and/or the use of other enforcement mechanisms.
Please note that, as the aforementioned site investigation efforts described above are being required by the
Department based upon a determination that this UST system represents a suspected source of an off-site
impact, and, in this case, are not routine leak detection procedures associated with an onsite detection of a
suspected release, some or all of the investigative costs may be eligible for reimbursement from the
Commercial Leaking Petroleum Underground Storage Tank Cleanup Fund (Trust Fund) reimbursement
under North Carolina General Statute (G.S.) 143-205.94B(b)(8). If you have any questions regarding Trust
Fund eligibility or reimbursement, please contact the UST Section Trust Fund Branch at [phone].
If you have any questions regarding the actions that must be taken or the rules mentioned in this letter,
please contact me at [phone] or the address listed below.
Sincerely,
Liz Price
Hydrogeologist
Wilmington Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Johnston County Health Department
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Appendix B – Tank Tightness Testing Results

TEST RESULTS
Cover Sheet
This is to certify that the tests identified above were conducted at Murphy 8549 on 12/19/2022 .
I hereby certify that I am responsible for the services described in this document and for the preparation of this document. The services
described in this document have been provided in a manner consistent with the current standards of the profession and to the best of
my knowledge comply with all applicable federal, state and local statutes, regulations and ordinances.
SIGNATURE:
451 APOLLO BEACH BLVD.
APOLLO BEACH, FL 33572
TEL: [phone]
FAX: [phone]
COMPANY TESTED:
Site / Station:Murphy 8549
Test Date:12/19/2022
Work Ord #:199878
Address:4993 NC-42
County:Wake
City, State:Garner, NC
COMMENTS
TESTS PERFORMED:
Petrotite Lines
Leak Detector
UST Monitor Inspection
Impact Valve
E-Stop
Pressure Decay
PV Valve
Murphy Facility Inspection
TEST REASON:
Compliance
PERFORMING TECHNICIAN:
Technician Name:David Moore
Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:30 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:05 Pretest 60
10:35 Start Line Test 60 0.0490
10:50 Line Test Cont.60 60 .049 0.0490 0.0000
11:05 Line Test Cont.60 60 0.0490 0.0490 0.0390
11:06 Bleedback 60 0 0.0490 0.3510 0.3020
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Regular
Line #:1
Material:UPP
Length (feet):90
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.455 gal
Measured:0.3020 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:31 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:06 Pretest 60
10:36 Start Line Test 60 0.0300
10:51 Line Test Cont.60 60 0.0300 0.0300 0.0000
11:06 Line Test Cont.60 60 0.0300 0.0300 0.0000
11:07 Bleedback 60 0 0.0300 0.4030 0.3730
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Regular
Line #:2
Material:UPP
Length (feet):90
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.455 gal
Measured:0.3730 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:32 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:07 Pretest 60
10:37 Start Line Test 60 0.0150
10:52 Line Test Cont.60 60 0.0150 0.0150 0.0000
11:07 Line Test Cont.60 60 0.0150 0.0150 0.0000
11:08 Bleedback 60 0 0.0150 0.4630 0.4480
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Regular
Line #:3
Material:UPP
Length (feet):120
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.590 gal
Measured:0.4480 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:33 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:08 Pretest 60
10:38 Start Line Test 60 0.0390
10:53 Line Test Cont.60 60 0.0390 0.0390 0.0000
11:08 Line Test Cont.60 60 0.0390 0.0390 0.0000
11:09 Bleedback 60 0 0.0390 0.5810 0.5420
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Regular
Line #:4
Material:UPP
Length (feet):120
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.590 gal
Measured:0.5420 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:34 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:09 Pretest 60
10:39 Start Line Test 60 0.0200
10:54 Line Test Cont.60 60 0.0200 0.0200 0.0000
11:09 Line Test Cont.60 60 0.0200 0.0200 0.0000
11:10 Bleedback 60 0 0.0200 0.2140 0.1940
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Diesel
Line #:7
Material:UPP
Length (feet):40
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.230 gal
Measured:0.1940 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:35 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:10 Pretest 60
10:40 Start Line Test 60 0.0330
10:55 Line Test Cont.60 60 0.0330 0.0330 0.0000
11:10 Line Test Cont.60 60 0.0330 0.0330 0.0000
11:11 Bleedback 60 0 0.0330 0.6950 0.6750
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Diesel
Line #:8
Material:UPP
Length (feet):140
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.680 gal
Measured:0.6750 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:36 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:11 Pretest 60
10:41 Start Line Test 60 0.0400
10:56 Line Test Cont.60 60 0.0400 0.0400 0.0000
11:11 Line Test Cont.60 60 0.0400 0.0400 0.0000
11:12 Bleedback 60 0 0.0400 0.5240 0.4840
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Premium
Line #:5
Material:UPP
Length (feet):120
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:0.590 gal
Measured:0.4840 gal
Petro Tite Lines
STP Mauf.:Fe-PetroRed Jacket
Type of System:Pressure
Line test conducted at:09:37 | Impact Valve | Screwed Down Check Valve
Time (Military)Log of Test Procedures Pbefore Pafter Vbefore Vafter Net
Change
Comments
10:12 Pretest 60
10:42 Start Line Test 60 0.0530
10:57 Line Test Cont.60 60 0.0530 0.0530 0.0000
11:12 Line Test Cont.60 60 0.0530 0.0530 0.0000
11:13 Bleedback 60 0 0.0530 0.7510 0.6980
PETROTITE LINES TEST
Station:Murphy #8549
Address:4993 NC-42
City, State:Garner, NC
Test Date:12/19/2022
Petro Tite Cert #:Petro-Tite Line & Leak Detector Tester
ee27c2e9
Result:Pass
Grade:Premium
Line #:6
Material:UPP
Length (feet):220
Diameter:2
Number of Flex Connectors:0
Test Pressure:60 psi
Bleedback:
Allowable:1.040 gal
Measured:0.6980 gal
LEAK DETECTOR TEST
TEST DATE
12/19/2022
Test Location Information
Name Murphy #8549
Address 4993 NC-42
City Garner, NC 27529
Phone
Contact
Testing Company Information
Name Valley Tank Testing
Address 451 Apollo Beach Blvd.
City Apollo Beach
Phone [phone]
Technician Information
Name David Moore
Cert #Petro-Tite Line & Leak Detector
Tester ee27c2e9
TYPE OF LEAK DETECTOR
PUMP #MAKE MODEL SERIAL #
1 Fe-Petro STP-MLD 09031075
2 Fe-Petro STP-MLD 09030996
4 Fe-Petro STP-MLD-D 09050303
3 Fe-Petro STP-MLD Unknown
PUMP #PRODUCT DISPENSER METERING PRESSURE
FUNCTIONAL
ELEMENT
HOLDING PSI
(GALLONS)
RESILIENCY
TEST LEAK
RATE
ML/MIN
(SEC)
OPENING TIME PASS/FAIL
1 Regular 1/2 25 17 .149 189ml 3 Pass
2 Regular 15/16 32 16 .123 189ml 3 Pass
4 Diesel 3/4 25 18 .094 189ml 4 Pass
3 Premium 1/2 25 17 .161 189ml 2 Pass
Monitor Model (Type):Veeder Root TLS 350-R  Serial #:
Annular Type:Wet  Certification Result:Pass
Sensor Type Quantity Result Visual Inspection?
Tank Annular:3 Pass Yes
Electronic Leak Detector (Pressure): 
Turbine Sump:4 Pass Yes
Fill Sump:
Transition/Piping Sump:
Spill Bucket Sensor:4 Pass No
Dispenser Pan:10 Pass Yes
Alarms Audible Visual Battery Backup
Yes Yes Yes
Tank Gauge Only?Yes
Automatic Tank Gauge Monthly Test?No
CSLD (Continuous Statistical Leak Detection)?No
Was probe visually inspected?Yes
Tested for accuracy of water and product levels?Yes
Comments:
I certify that the equipment identified in this document was inspected/serviced in accordance with the manufacturer's guidelines, is calibrated per
the manufacturer's specifications, and operation upon my departure unless otherwise noted.
Inspected By:
Print Name:David Moore
Date:12/19/2022
UST MONITOR INSPECTION TEST
Client:
Test Date:12/19/2022
Work #:199878
Store:Murphy #8549
Address:4993 NC-42
Garner, NC 27529
Dispenser Impact Valve Operation/Installation Inspection
Product Number of
Shear Valves
Comments
Regular 8
Diesel 2
Premium 8
IMPACT VALVE TEST
Station:Murphy #8549
Address:4993 NC-42
 Garner, NC 27529
Valley Tank Testing
Test Date:12/19/2022
Work Ord #:199878
DoALL shear valves operate? Yes
AreALL shear valves installed and mounted properly? Yes
Certification of Operational Testing of Emergency Electronic Shutoff Switches
Valley Tank Testing
451 Apollo Beach Blvd.
Apollo Beach, FL 33572
813-671-9065
Name #:Murphy #8549
Address:4993 NC-42
City:Garner
State:NC
Operational
I certify that I personally tested the emergency electricalshutoff switches at the above referenced facility. I turned the emergency switches off,
individually testing each such switch, and all electrical power to all pumps, dispensers and dispenser lighting disconnected all at one time.
Number of Switches: 3
Name of Tester: David Moore
Signature:
Date of Test: 12/19/2022
Test Conducted by:Test Company:Date of Test:
David Moore Valley Tank Testing 12/19/2022
PRESSURE DECAY TEST
SOURCE INFORMATION FACILITY PARAMETERS
Site Name and address Site Representative and Title PHASE II SYSTEM TYPE
Murphy #8549
Garner, NC
Unknown
Garner, NC 27529 Site Phone No.MANIFOLDED
Stage I NESHAP Yes
Applicable Regulations VN Recommended
Source Test Results and Comments
Tank #:01 02 03
Product Grade Regular Regular Premium
Actual Tank Capacity, gallons 19703 19703 7815
Gasoline Volume 9036 9564 5700
Ullage, gallons (#2#3)10667 10139 2115
Number of Nozzles   
Initial Pressure, inches H2O 2.00   
Pressure After 1 Minute, inches H2O 2.00   
Pressure After 2 Minute, inches H2O 1.99   
Pressure After 3 Minute, inches H2O 1.98   
Pressure After 4 Minute, inches H2O 1.98   
Pressure After 5 Minute, inches H2O 1.97   
Allowable Final Pressure 1.90   
PASS/FAIL (P/F)PASS   
Pressure/Vaccuum (P/V) Vent Valve Data Sheet
Facility Name:Murphy #8549 Test Date:Mon Dec 19 2022 01:00:00 GMT-0500 (Eastern Standard Time)
Address:4993 NC-42 Test Company:
City:Garner Tester Name:David Moore
P/V Valve Manufacturer:PV Valve Threaded 3" OPW Model Number:OPW-523LP-3203 Pass
Tank Grade:Manifolded
Measured Positive Leak Rate (CFH):.03 Measured Negative Leak Rate (CFH):-.17
Positive Cracking Pressure (in H2O):4.10 Negative Cracking Pressure (in H2O):-7.00
PV VALVE TEST
TP-201.1E, Page 7California Air Resources Board October 8, 2003
Murphy Oil USA Site Checklist 2011
Murphy #: 8549
City, State:Garner, NC
Work Order: 199878
Tank Monitor
Compare the water and fuel stick readings with the EMC probe readings.
Tank 1:Stick 55  Water 0
EM 54.66  Water 0

Tank 2:Stick 58  Water 0
EM 57.07  Water 0

Tank 3:Stick 69  Water 0
EM 68.98  Water 0

Tank 4:Stick 81  Water 0
EM 80.70  Water 0

Please Record All Sensor Alarms, Investigate, and Identify the Cause.
Alarm:
Cause: (Is there any fee product?)

Alarm:
Cause: (Is there any fee product?)

Alarm:
Cause: (Is there any fee product?)

Alarm:
Cause: (Is there any fee product?)

Alarm:
Cause: (Is there any fee product?)

Alarm:
Cause: (Is there any fee product?)

Please Record All Tank Farm Issues.
Riser Caps - (Tight)
Tight
Spill Buckets - (Bad gaskets, drains, bucket liners, lids)
Good
Vapor Recovery Buckets - (Bad lids, gaskets, popetes, bucket liners)
Good
Manhole Covers
Good
STP Sump - (lids, gaskets, pipe penetration boots)
Good
Dispenser Sumps - (pipe penetration boots, filter, unions)
Good
Dispenser Hanging Hardware - (hoses, swivels, break-away, nozzles)
Good
Overfill Protection
Good
Stage I Vapor Recovery - (swivel dry breaks, tight fit, dual point VR)
Good
Stage II Vapor Recovery - (Vapor Saver, ?)
Cathodic Protection - (Sacrificial Anodes or Impressed Current?)
Hand-held release detection equipment: Are devices such as tank gauge sticks or groundwater bailers operable and serviceable?
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 1 (Interstitial Sensors)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill,
Overfill, Leak Detection, and Secondary Containment Equipment at UST Facilities”. If the manufacturer's instructions do not require a condition to be implemented that
triggers an alarm, then you must also trigger an alarm condition. Print the alarm reports triggered during the operability check and attach to this form.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501 and/or 15A NCAC 2N .0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Sensor Location:
Enter Location #/Description: #:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
Tank Volume (gallons):
Product:
Sensor Manufacturer/Model:
Type of Sensor
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Is Sensor Position sensitive? (N/A if
No and Pos. Sens. not required)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Liquid Water
Product
Water
Product
Water
Product
Water
Product
Water
Product
Is the ATG console clear of any
active or recurring warnings or
alarms regarding the leak sensor? If
the sensor is in alarm and
functioning, indicate why.
Yes No Yes No Yes No Yes No Yes No
Is the sensor alarm circuit
operational?Yes No Yes No Yes No Yes No Yes No
Has sensor been inspected and in
good operating condition?Yes No Yes No Yes No Yes No Yes No
If Position Sensitive, does sensor
alarm when raised off bottom?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
When placed in the test liquid, does
the sensor trigger an alarm?
(If sensor cannot be removed, e.g.,
Emco Spill bucket sensor then N/R)
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
When an alarm is triggered, is the
sensor properly identified on the
ATG console?
Yes No Yes No Yes No Yes No Yes No
Sensor mounted at the lowest point
of interstice (e.g., within 2 inches of
containment sump bottom) (Liquid
detecting float sensors only)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Alarm report attached?Yes No Yes No Yes No Yes No Yes No
Any "No" answer indicates the sensor fails the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/202212/19/2022
✔✔✔✔✔
1/2 3/4 5/6 7/8 9/10
Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 208
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 1 (Interstitial Sensors)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill,
Overfill, Leak Detection, and Secondary Containment Equipment at UST Facilities”. If the manufacturer's instructions do not require a condition to be implemented that
triggers an alarm, then you must also trigger an alarm condition. Print the alarm reports triggered during the operability check and attach to this form.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501 and/or 15A NCAC 2N .0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Sensor Location:
Enter Location #/Description: #:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
Tank Volume (gallons):
Product:
Sensor Manufacturer/Model:
Type of Sensor
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Is Sensor Position sensitive? (N/A if
No and Pos. Sens. not required)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Liquid Water
Product
Water
Product
Water
Product
Water
Product
Water
Product
Is the ATG console clear of any
active or recurring warnings or
alarms regarding the leak sensor? If
the sensor is in alarm and
functioning, indicate why.
Yes No Yes No Yes No Yes No Yes No
Is the sensor alarm circuit
operational?Yes No Yes No Yes No Yes No Yes No
Has sensor been inspected and in
good operating condition?Yes No Yes No Yes No Yes No Yes No
If Position Sensitive, does sensor
alarm when raised off bottom?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
When placed in the test liquid, does
the sensor trigger an alarm?
(If sensor cannot be removed, e.g.,
Emco Spill bucket sensor then N/R)
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
When an alarm is triggered, is the
sensor properly identified on the
ATG console?
Yes No Yes No Yes No Yes No Yes No
Sensor mounted at the lowest point
of interstice (e.g., within 2 inches of
containment sump bottom) (Liquid
detecting float sensors only)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Alarm report attached?Yes No Yes No Yes No Yes No Yes No
Any "No" answer indicates the sensor fails the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
✔✔✔✔✔
11/12 13/14 15/16 17/18 19/20
Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 208
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 1 (Interstitial Sensors)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill,
Overfill, Leak Detection, and Secondary Containment Equipment at UST Facilities”. If the manufacturer's instructions do not require a condition to be implemented that
triggers an alarm, then you must also trigger an alarm condition. Print the alarm reports triggered during the operability check and attach to this form.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501 and/or 15A NCAC 2N .0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Sensor Location:
Enter Location #/Description: #:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
Tank Volume (gallons):
Product:
Sensor Manufacturer/Model:
Type of Sensor
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Is Sensor Position sensitive? (N/A if
No and Pos. Sens. not required)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Liquid Water
Product
Water
Product
Water
Product
Water
Product
Water
Product
Is the ATG console clear of any
active or recurring warnings or
alarms regarding the leak sensor? If
the sensor is in alarm and
functioning, indicate why.
Yes No Yes No Yes No Yes No Yes No
Is the sensor alarm circuit
operational?Yes No Yes No Yes No Yes No Yes No
Has sensor been inspected and in
good operating condition?Yes No Yes No Yes No Yes No Yes No
If Position Sensitive, does sensor
alarm when raised off bottom?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
When placed in the test liquid, does
the sensor trigger an alarm?
(If sensor cannot be removed, e.g.,
Emco Spill bucket sensor then N/R)
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
When an alarm is triggered, is the
sensor properly identified on the
ATG console?
Yes No Yes No Yes No Yes No Yes No
Sensor mounted at the lowest point
of interstice (e.g., within 2 inches of
containment sump bottom) (Liquid
detecting float sensors only)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Alarm report attached?Yes No Yes No Yes No Yes No Yes No
Any "No" answer indicates the sensor fails the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
✔
✔✔✔✔
T1 T2 T3 T4 T1
19703 19703 11849 7815 19703
Regular Regular Diesel Premium Regular
Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 208 Veeder Root 303
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 1 (Interstitial Sensors)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill,
Overfill, Leak Detection, and Secondary Containment Equipment at UST Facilities”. If the manufacturer's instructions do not require a condition to be implemented that
triggers an alarm, then you must also trigger an alarm condition. Print the alarm reports triggered during the operability check and attach to this form.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501 and/or 15A NCAC 2N .0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Sensor Location:
Enter Location #/Description: #:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
Tank Volume (gallons):
Product:
Sensor Manufacturer/Model:
Type of Sensor
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Is Sensor Position sensitive? (N/A if
No and Pos. Sens. not required)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Liquid Water
Product
Water
Product
Water
Product
Water
Product
Water
Product
Is the ATG console clear of any
active or recurring warnings or
alarms regarding the leak sensor? If
the sensor is in alarm and
functioning, indicate why.
Yes No Yes No Yes No Yes No Yes No
Is the sensor alarm circuit
operational?Yes No Yes No Yes No Yes No Yes No
Has sensor been inspected and in
good operating condition?Yes No Yes No Yes No Yes No Yes No
If Position Sensitive, does sensor
alarm when raised off bottom?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
When placed in the test liquid, does
the sensor trigger an alarm?
(If sensor cannot be removed, e.g.,
Emco Spill bucket sensor then N/R)
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
When an alarm is triggered, is the
sensor properly identified on the
ATG console?
Yes No Yes No Yes No Yes No Yes No
Sensor mounted at the lowest point
of interstice (e.g., within 2 inches of
containment sump bottom) (Liquid
detecting float sensors only)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Alarm report attached?Yes No Yes No Yes No Yes No Yes No
Any "No" answer indicates the sensor fails the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
✔✔✔
✔✔
T2 T3/T4 T1 T2 T3
19703 7815/11849 19703 19703 11849
Regular Premium/Diesel Regular Regular Diesel
Veeder Root 303 Veeder Root 303 VR Series 7943 VR Series 7943 VR Series 7943
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
✔✔✔✔✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 1 (Interstitial Sensors)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill,
Overfill, Leak Detection, and Secondary Containment Equipment at UST Facilities”. If the manufacturer's instructions do not require a condition to be implemented that
triggers an alarm, then you must also trigger an alarm condition. Print the alarm reports triggered during the operability check and attach to this form.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501 and/or 15A NCAC 2N .0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Sensor Location:
Enter Location #/Description: #:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
#:
Dispenser
Spill Bucket
Tank Interstice
Tank Top and
Other Sumps
Tank Volume (gallons):
Product:
Sensor Manufacturer/Model:
Type of Sensor
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Discriminating
Non-
Discriminating
Is Sensor Position sensitive? (N/A if
No and Pos. Sens. not required)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Liquid Water
Product
Water
Product
Water
Product
Water
Product
Water
Product
Is the ATG console clear of any
active or recurring warnings or
alarms regarding the leak sensor? If
the sensor is in alarm and
functioning, indicate why.
Yes No Yes No Yes No Yes No Yes No
Is the sensor alarm circuit
operational?Yes No Yes No Yes No Yes No Yes No
Has sensor been inspected and in
good operating condition?Yes No Yes No Yes No Yes No Yes No
If Position Sensitive, does sensor
alarm when raised off bottom?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
When placed in the test liquid, does
the sensor trigger an alarm?
(If sensor cannot be removed, e.g.,
Emco Spill bucket sensor then N/R)
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
Yes No
N/R
When an alarm is triggered, is the
sensor properly identified on the
ATG console?
Yes No Yes No Yes No Yes No Yes No
Sensor mounted at the lowest point
of interstice (e.g., within 2 inches of
containment sump bottom) (Liquid
detecting float sensors only)
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Alarm report attached?Yes No Yes No Yes No Yes No Yes No
Any "No" answer indicates the sensor fails the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
✔
T4
7815
Premium
VR Series 7943
✔
✔
✔
✔
✔
✔
✔
✔
✔
✔
✔
✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 2 (Automatic Tank Gauge / Spill Bucket Visual Gauge)
Inspect the leak detection equipment in accordance with manufacturer guidelines and PEI RP 1200, “Recommended Practices for the Testing and Verification of Spill, Overfill, Leak Detection, and
Secondary Containment Equipment at UST Facilities”.
If the equipment manufacturer (e.g., Veeder Root) requires a training certification to conduct operability checks of there equipment then you must be certified.
Results must be maintained for at least one year at the UST site or the tank owner or operator's place of business and be readily available for inspection.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Tank Volume (gallons):
Tank Diameter (inches):
Product:
Automatic Tank Gauge (ATG)N/A Note: If the facility is using the ATG to obtain data for SIR then the ATG
operability check must be completed.
ATG Brand and Model
1. Using tank stick measure fuel level. Stick value agrees with
Fuel float level displayed on console?Yes No Yes No Yes No Yes No
2. Using tank stick measure water level. Stick value agrees
with Water float level displayed on console?Yes No Yes No Yes No Yes No
3. After removing the ATG probe from the tank, has it been
inspected, and any damaged or missing parts replaced?Yes No Yes No Yes No Yes No
Magnetostrictive Probes
5. Float moves freely on the stem without binding?Yes No Yes No Yes No Yes No
6. Inch level (to nearest 1/8 inch) from bottom of stem when
90% alarm is triggered.
7. Inch level at which the overfill alarm activates corresponds
with value programmed in the gauge?Yes No Yes No Yes No Yes No
8. Inch level (to nearest 1/8 inch) from bottom when the water
float first triggers an alarm or warning.
9. Inch level at which the water float alarm activates
corresponds with value programmed in gauge?Yes No Yes No Yes No Yes No
10. Alarm reports attached?NoYes NoYes NoYes NoYes
If any answers in Lines 1, 2, 3 (all ATGs) or 4 (INCON); 5, 7, 9 or 10 (for Mag Probes); 11 or 12 (for Cap Probes) are “No”, the system has failed the test.
Test Results Pass Fail Pass Fail Pass Fail Pass Fail
Capacitance Probes
11. Initiated diagnostic check of probes from console?Yes No Yes No Yes No Yes No
12. Diagnostic check does not show any open or shorted
segments in measurement section of probe? (Attach
diagnostic report to form)
NoYes NoYes NoYes NoYes
4. Franklin Fueling INCON ATGs: Volume Qualifier is 14% or
greater? (Attach printout) (Skip question for other ATGs)Yes NoYesNoYesNoYesNo
Spill Bucket Interstice Visual Gauge N/A
Gauge manufacturer
Gauge removed and visually inspected, and no damage noted?Yes No Yes No Yes No Yes No
O-ring/seals on entry fitting of gauge are present and not
damaged?Yes No Yes No Yes No Yes No
Float mechanism moves freely up and down?Yes No Yes No Yes No Yes No
Indicator arrow rotates when float moved up and down (Franklin
Fueling, Fairfield Ind and OPW) or Indicator shows red, “TEST”,
when float in up position and green, “Ok” when float in down
position (Emco Wheaton)?
Yes No Yes No Yes No Yes No
Test Results (Any “No” answer indicates the equipment fails.)Pass Fail Pass Fail Pass Fail Pass Fail
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
19703 19703 11849 7815
118 118 118 118
Regular Regular Diesel Premium
✔
VR TLS 350
✔✔✔✔
✔✔✔✔
✔✔✔✔
✔✔✔✔
✔✔✔✔✔✔✔✔
105 106 105 105
✔✔✔✔
111 1
✔✔✔✔
✔✔✔✔
✔✔✔✔
✔
UST-22B Annual Leak Detection Equipment Operability Check
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/11/2022
Page 3 (Mechanical and Electronic Line Leak Detectors)
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .407/.0501.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Tank #:
Tank Volume:
Product:
Leak Detector Manufacturer:
Leak Detector Model:
Type of Leak Detector:MLLD
ELLD
MLLD
ELLD
MLLD
ELLD
MLLD
ELLD
MLLD
ELLD
MLLD (ALL PRESSURE MEASUREMENT ARE MADE IN PSIG)
STP Full Operating Pressure
Check Valve Holding Pressure
Line Resiliency (ml) (line bleed back volume
as measured from check valve holding
pressure to 0 psig)
Step Through Time in Seconds (time the
MLLD hesitates at metering pressure before
going to full operating pressure as measured
from 0 psig with no leak induced on the line)
Metering Pressure (STP pressure when
simulated leak rate, 3 gph at 10 psig)
Opening Time in Seconds (the time the
MLLD opens to allow full pressure after
simulated leak is stopped)
Does the STP pressure remain at or below
the metering pressure for at least 60 seconds
when the simulated leak is induced?
Yes No Yes No Yes No Yes No Yes No
Does the leak detector reset (trip) when the
line pressure is bled off to zero psig?Yes No Yes No Yes No Yes No Yes No
Does the STP properly cycle on/off under
normal fuel system operation conditions?Yes No Yes No Yes No Yes No Yes No
A “No” answer to any of the above questions indicates the MLLD failed the test.
ELLD (ALL PRESSURE MEASUREMENTS ARE MADE IN PSIG)
STP Full Operating Pressure
How many test cycles are observed before
alarm/shutdown occurs?
Does the simulated leak cause an alarm? (If
“No” then leak detector fails) Yes No Yes No Yes No Yes No Yes No
Does the simulated leak cause an STP
shutdown?
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Yes No
N/A
Test Results Pass Fail Pass Fail Pass Fail Pass Fail Pass Fail
ELLD alarm reports attached?
(If “No” then leak detector fails)Yes No Yes No Yes No Yes No Yes No
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
1123
19703 19703 11849 7815
Regular Regular Diesel Premium
Fe Petro Fe Petro Fe Petro Fe Petro
STP-MLD STP-MLD STP-MLD-D STP-MLD
✔✔✔✔
25 32 25 25
17 16 18 17
564 466 356 609
6 6 7 5
16 16 17 15
3 3 4 2
✔✔✔✔
✔✔✔✔
✔✔✔✔
✔✔✔✔
UST-22C Annual Sump Visual Inspections
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/12/2022
(Dispenser Sumps)
Underground Storage Tank (UST) system owners and operators are required to conduct a STP, dispenser, or other sump visual check at least annually
for any UST system regardless of installation date. Results must be maintained for at least one year at the UST site or the tank owner or operator's
place of business and be readily available for inspection.
• Visually inspect STP, dispenser and other sump areas (whether containment present or not) for liquids (water or regulated substances), sump
damage, penetration boot damage, faulty equipment, and equipment leaks. If none of the above items are observed during the inspection,
select Pass in the appropriate column dropdown, otherwise select Fail. If Fail, indicate what action was taken to repair the containment sump
or faulty equipment in the comment portion of this form or attach documentation of any repairs. If a check is not applicable, then select N/A in
the dropdown. If you are completing form by hand then write P, F, or N/A in each box
• If the sump contains a regulated substance or there are other indications of a release of a regulated substance, it must be reported as a
suspected release using the UST-17A form, UST Suspected Release 24 Hour Notice.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .0407/.0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Dispenser Sump Disp #Disp #Disp #Disp #Disp #
ALL
WITHOUT
CONTAINMENT
WITH
CONTAINMENT
No leaks, weeps, or drips observed
Piping is free of defects
Sump does not contain trash, debris and used
filters
Flexible connectors not frayed, twisted,
kinked, or bent beyond manufacturer
specifications
Shear valves operate freely, close completely
and anchored correctly per NCFPC 2206.7.4
Flex connector(s) and other metallic product
piping and piping components are not in
contact with soil or water or are cathodically
protected
Sump is dry and does not contain product
and/or water. (If Fail, enter liquid type in
comment)
Sump walls/bottom are not damaged (i.e.,
cracks, bulges, holes, etc.) (If conducting
sump/interstitial monitoring then any failing
item must be repaired. Repair is optional if not
conducting sump/interstitial monitoring)
Penetration fittings intact and in good
condition (If conducting sump/interstitial
monitoring then any failing item must be
repaired. Repair is optional if not conducting
sump/interstitial monitoring)
Sump Sensor is < 2” from lowest point (N/A if
not conducting interstitial monitoring)
Piping interstitial space is open to the sump
(Open DW piping systems only; interstice
jumpers must be disconnected, N/A if closed
system or not conducting interstitial
monitoring)
Comments and explanation of failing results and other problems noted during inspection:
Piping is manifolded above the shear valve
and does not meet the NCFPC 2206.7.4 *
* Choices: Yes,
No, N/A
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
1/2 3/4 5/6 7/8 9/10
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
N/A N/A N/A N/A N/A
Pass Pass Pass Pass Pass
No No No No No
N/A N/A N/A N/A N/A
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Open Open Open Open Open
UST-22C Annual Sump Visual Inspections
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/12/2022
(Dispenser Sumps)
Underground Storage Tank (UST) system owners and operators are required to conduct a STP, dispenser, or other sump visual check at least annually
for any UST system regardless of installation date. Results must be maintained for at least one year at the UST site or the tank owner or operator's
place of business and be readily available for inspection.
• Visually inspect STP, dispenser and other sump areas (whether containment present or not) for liquids (water or regulated substances), sump
damage, penetration boot damage, faulty equipment, and equipment leaks. If none of the above items are observed during the inspection,
select Pass in the appropriate column dropdown, otherwise select Fail. If Fail, indicate what action was taken to repair the containment sump
or faulty equipment in the comment portion of this form or attach documentation of any repairs. If a check is not applicable, then select N/A in
the dropdown. If you are completing form by hand then write P, F, or N/A in each box
• If the sump contains a regulated substance or there are other indications of a release of a regulated substance, it must be reported as a
suspected release using the UST-17A form, UST Suspected Release 24 Hour Notice.
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .0407/.0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
Dispenser Sump Disp #Disp #Disp #Disp #Disp #
ALL
WITHOUT
CONTAINMENT
WITH
CONTAINMENT
No leaks, weeps, or drips observed
Piping is free of defects
Sump does not contain trash, debris and used
filters
Flexible connectors not frayed, twisted,
kinked, or bent beyond manufacturer
specifications
Shear valves operate freely, close completely
and anchored correctly per NCFPC 2206.7.4
Flex connector(s) and other metallic product
piping and piping components are not in
contact with soil or water or are cathodically
protected
Sump is dry and does not contain product
and/or water. (If Fail, enter liquid type in
comment)
Sump walls/bottom are not damaged (i.e.,
cracks, bulges, holes, etc.) (If conducting
sump/interstitial monitoring then any failing
item must be repaired. Repair is optional if not
conducting sump/interstitial monitoring)
Penetration fittings intact and in good
condition (If conducting sump/interstitial
monitoring then any failing item must be
repaired. Repair is optional if not conducting
sump/interstitial monitoring)
Sump Sensor is < 2” from lowest point (N/A if
not conducting interstitial monitoring)
Piping interstitial space is open to the sump
(Open DW piping systems only; interstice
jumpers must be disconnected, N/A if closed
system or not conducting interstitial
monitoring)
Comments and explanation of failing results and other problems noted during inspection:
Piping is manifolded above the shear valve
and does not meet the NCFPC 2206.7.4 *
* Choices: Yes,
No, N/A
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
11/12 13/14 15/16 17/18 19/20
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
N/A N/A N/A N/A N/A
Pass Pass Pass Pass Pass
No No No No No
N/A N/A N/A N/A N/A
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Pass Pass Pass Pass Pass
Open Open Open Open Open
UST-22C Annual Sump Visual Inspections
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/12/2022
Page 2 (STP, Transition, Other Sump)
Tank Size/Location:
Product:
STP/Transition/ Other Sump
UST FACILITY
Owner / Operator Name Facility IDFacility Name
Facility Street Address Facility City County
CONTRACTOR/PERSON CONDUCTING INSPECTIONS
Company Name Phone Email address
I certify, under penalty of law, that the testing data provided on this form documents the UST system equipment was checked in accordance with the
manufacturer's guidelines and the applicable national industry standards listed in 15A NCAC 2N .0407/.0900.
Print Name of person conducting inspection Signature of person conducting inspection Inspection Date
ALL
WITHOUT
CONTAINMENT
WITH
CONTAINMENT
No leaks at submersible pump, ALLD, or
other pipe components
Piping is free of defects
Sump does not contain trash and debris
Flexible connectors not frayed, twisted,
kinked or bent beyond manufacturer
specifications
Mechanical line leak detector properly vented,
vent tube not kinked or twisted, vent tube
fittings intact and tightened
Submersible pump head, flex connector(s)
and other metallic product piping and piping
components are not in contact with soil or
water or are cathodically protected
Sump is dry and does not contain product
and/or water. (If Fail, enter liquid type in
comment)
Sump walls/bottom are not damaged (i.e.,
cracks, bulges, holes, etc.) (If conducting
sump/interstitial monitoring then any failing
item must be repaired. Repair is optional if not
conducting sump/interstitial monitoring)
Penetration fittings intact and in good
condition (If conducting sump/interstitial
monitoring then any failing item must be
repaired. Repair is optional if not conducting
sump/interstitial monitoring)
Sump Sensor is < 2” from lowest point (N/A if
not conducting interstitial monitoring)
Piping interstitial space is open to the sump
(Open DW piping systems only; interstice
jumpers must be disconnected, N/A if closed
system or not conducting interstitial
monitoring)
Sump lid, gasket and seals present and in
good condition
Comments and explanation of failing results and other problems noted during inspection:
Valley Tank Testing 813-671-9065 [e-mail]
Murphy 8549 Murphy Oil USA 37042
4993 NC-42 Garner Wake
David Moore 12/19/2022
STP / 19703 T1 STP / 19703 T2 STP / 11849 T3 STP / 7815 T4
Regular Regular Diesel Premium
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
N/A N/A N/A N/A
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
Pass Pass Pass Pass
TEST RESULTS
Cover Sheet
This is to certify that the tests identified above were conducted at Murphy 8549 on 01/10/2023 .
I hereby certify that I am responsible for the services described in this document and for the preparation of this document. The services
described in this document have been provided in a manner consistent with the current standards of the profession and to the best of
my knowledge comply with all applicable federal, state and local statutes, regulations and ordinances.
SIGNATURE:
451 APOLLO BEACH BLVD.
APOLLO BEACH, FL 33572
TEL: [phone]
FAX: [phone]
COMPANY TESTED:
Site / Station:Murphy 8549
Test Date:01/10/2023
Work Ord #:200765
Address:4993 NC-42
County:Wake
City, State:Garner, NC
COMMENTS
TESTS PERFORMED:
Tank
TEST REASON:
Investigation
PERFORMING TECHNICIAN:
Technician Name:Sub Contractor
Cert #:
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
Comments and Problems Overview : 2023
Test Performed Product Tech Notes Anode
Bag
Installed
Pictures
Taken
PS&C
Will Make
Repairs
Tanks Unleaded (T1)The primary of The tank passes tank tightness test. There is no water in the tank. Technician physically stuck
secondary of tank and found that there is only 1” of brine in the reservoir. Nothing was pulled into the tank
during testing as well as the brine level in the reservoir remained the same. Technician believes the secondary
of the tank should be further investigated.
q q q
Technician Signature : 2023
Tester's Name Richard David Murrell
Test Date 01/10/2023
Tester's Signature
I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in
accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
X
: 2023
Unleaded (T1)20000 T1 73.5
Fiberglass
Double-Wall 1 N/A
IM UST
73.5 0.026 1.911
0 0.036 0.000
1.911
1 0.036 0.036
1.875
2.375
2.375
52.5 117.750
170.25
73.5
0
55
1
12:10pm
12:15pm
12:32pm
12:56pm
12:56pm
01:40pm
0
0
2.375
2.643
2.643
2.643
I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in
accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
Unleaded (T1)20000 T1 73.5
Fiberglass
Double-Wall 1 N/A
IM
120 110 110
113.333
113.333 0.030 0.600
0:35
Double-Wall 1:05 pm
Brine Tank 1:40 pm
Pass
Pass
Pass
No Water Intrusion
Technician Signature : 2023
Tester's Name Richard David Murrell
Test Date 01/10/2023
Tester's Signature
I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in
accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
Parts Replacement Inspection : 2023
No Parts Replaced
Technician Signature : 2023
Tester's Name Richard David Murrell
Test Date 01/10/2023
Tester's Signature
I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in
accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
Additional Labor : 2023
Pad Locks
Did you have to remove any pad locks for testing?
No
Technician Signature : 2023
Tester's Name Richard David Murrell
Test Date 01/10/2023
Tester's Signature
I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in
accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3
PETROLEUM SERVICE CALIBRATION, INC. &
www.testmytanks.com
Customer/Facility Information Company Information
Customer Name D&H United Fueling Solutions, Inc. (DBA Valley Tank Testing )Company Name Petroleum Service & Calibration, Inc.
Location Name Murphy / 8549 Company Phone Number 877-479-8152
Site Address 4993 NC 42 Highway West Company Address P.O. Box 851
City/State/Zip Garner, NC 27529 City Denver State NC
County Johnston Site Phone Number [phone] Job Number 156332 PSCIN 100754-114
Facility ID#0-037042
Emission PO#66791763
TECHNICIAN LICENSING - Richard David Murrell : 2023
OSHA
Certification Expires Additional Information
SDS NA OSHA Standard: 1910.1200 App D
Aerial Lifts NA OSHA Standard: 1926.453
Confined Space Entry 07/22/2023 OSHA Standard: 1910.146
Fall Protection NA OSHA Standard: 1926.503 Subpart M
Fire Extinguisher 06/23/2023 OSHA Standard: 1910.157
First Aid / CPR Training 01/29/2023 OSHA Standard: 1910.151
Ladders NA OSHA Standard: 1910.23
LockOut / TagOut 07/22/2023 OSHA Standard: 1910.147
Estabrooks
Certification Expires Additional Information
Leak Detector 05/30/2024 License Number: ****70
Line 05/30/2024 License Number: ****70
Tank 05/30/2024 License Number: **-6970
Cathodic Protection
Certification Expires Additional Information
Steel Tank Institute NA License Number: Working Knowledge
ASSISTANT TECHNICIAN LICENSING - Carson Grey Hannah : 2023
OSHA
Certification Expires Additional Information
SDS NA OSHA Standard: 1910.1200 App D
Confined Space Entry 07/22/2023 OSHA Standard: 1910.146
Fire Extinguisher 07/07/2024 OSHA Standard: 1910.157
First Aid / CPR Training 07/07/2024 OSHA Standard: 1910.151
LockOut / TagOut 07/22/2023 OSHA Standard: 1910.147
Powered by TCPDF (www.tcpdf.org)
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Appendix C – Laboratory Analytical Report

03/21/23
Technical Report for
Murphy Oil USA
GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
2701997
SGS Job Number: FC2879
Sampling Dates: 02/20/23 - 02/21/23
Report to:
Groundwater & Environmental Services
104 Corporate Blvd Suite 411
West Columbia, SC 29169
[e-mail]
ATTN: Aaron Williamson
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Rosa Junkin 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 03/21/23
e-Hardcopy 2.0
Automated Report
125
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 125
FC2879
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FC2879-1: SB-1 ............................................................................................................8
3.2: FC2879-2: SB-2 ............................................................................................................13
3.3: FC2879-3: SB-3 ............................................................................................................18
3.4: FC2879-4: SB-4 ............................................................................................................23
3.5: FC2879-5: SB-5 ............................................................................................................28
3.6: FC2879-6: SB-6 ............................................................................................................33
3.7: FC2879-7: SB-7 ............................................................................................................38
3.8: FC2879-8: SB-8 ............................................................................................................43
3.9: FC2879-9: SB-9 ............................................................................................................48
3.10: FC2879-10: SB-10 ......................................................................................................53
3.11: FC2879-11: SB-11 ......................................................................................................58
3.12: FC2879-12: SB-17 ......................................................................................................63
Section 4: Misc. Forms ............................................................................................................68
4.1: Chain of Custody ...........................................................................................................69
Section 5: MS Volatiles - QC Data Summaries .....................................................................72
5.1: Method Blank Summary ................................................................................................73
5.2: Blank Spike Summary ...................................................................................................87
5.3: Matrix Spike Summary ..................................................................................................101
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................102
Section 6: GC Volatiles - QC Data Summaries .....................................................................112
6.1: Method Blank Summary ................................................................................................113
6.2: Blank Spike Summary ...................................................................................................116
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................119
Section 7: GC/LC Semi-volatiles - QC Data Summaries .....................................................122
7.1: Method Blank Summary ................................................................................................123
7.2: Blank Spike Summary ...................................................................................................124
7.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................125 12345672 of 125
FC2879
SGS North America Inc.
Sample Summary
Murphy Oil USA
Job No:FC2879
GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Project No: 2701997
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC2879-1 02/20/23 15:45 AW 02/22/23 SO Soil SB-1
FC2879-2 02/20/23 16:00 AW 02/22/23 SO Soil SB-2
FC2879-3 02/20/23 16:30 AW 02/22/23 SO Soil SB-3
FC2879-4 02/20/23 16:45 AW 02/22/23 SO Soil SB-4
FC2879-5 02/20/23 17:00 AW 02/22/23 SO Soil SB-5
FC2879-6 02/20/23 12:31 AW 02/22/23 SO Soil SB-6
FC2879-7 02/20/23 14:18 AW 02/22/23 SO Soil SB-7
FC2879-8 02/20/23 15:05 AW 02/22/23 SO Soil SB-8
FC2879-9 02/20/23 15:20 AW 02/22/23 SO Soil SB-9
FC2879-10 02/21/23 09:57 AW 02/22/23 SO Soil SB-10
FC2879-11 02/21/23 11:15 AW 02/22/23 SO Soil SB-11
FC2879-12 02/21/23 10:20 AW 02/22/23 SO Soil SB-17
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 125
FC28791
Summary of Hits Page 1 of 3
Job Number:FC2879
Account:Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Collected:02/20/23 thru 02/21/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC2879-1 SB-1
n-Butylbenzene 690 520 100 ug/kg SW846 8260D
Ethylbenzene 9310 520 100 ug/kg SW846 8260D
Isopropylbenzene 1350 520 100 ug/kg SW846 8260D
p-Isopropyltoluene 1090 520 100 ug/kg SW846 8260D
Naphthalene 2470 520 210 ug/kg SW846 8260D
n-Propylbenzene 4260 520 100 ug/kg SW846 8260D
Toluene 5500 2100 1000 ug/kg SW846 8260D
1,2,4-Trimethylbenzene 60200 2900 590 ug/kg SW846 8260D
1,3,5-Trimethylbenzene 6870 520 100 ug/kg SW846 8260D
m,p-Xylene 34000 1000 110 ug/kg SW846 8260D
o-Xylene 15100 520 100 ug/kg SW846 8260D
Xylene (total)49100 1600 220 ug/kg SW846 8260D
TPH-GRO (C6-C10)300 100 41 mg/kg SW846 8015C
TPH (C10-C28)32.3 5.8 2.9 mg/kg SW846 8015C
FC2879-2 SB-2
No hits reported in this sample.
FC2879-3 SB-3
Benzene 1.2 J 3.1 0.75 ug/kg SW846 8260D
2-Butanone (MEK)9.2 J 15 4.5 ug/kg SW846 8260D
Methyl Bromide 1.8 J 3.1 1.2 ug/kg SW846 8260D
TPH (C10-C28)3.86 J 5.8 2.9 mg/kg SW846 8015C
FC2879-4 SB-4
No hits reported in this sample.
FC2879-5 SB-5
TPH (C10-C28)3.78 J 5.7 2.9 mg/kg SW846 8015C
FC2879-6 SB-6
n-Butylbenzene 1890 J 2300 460 ug/kg SW846 8260D
Ethylbenzene 34300 2300 460 ug/kg SW846 8260D
Isopropylbenzene 3680 2300 460 ug/kg SW846 8260D
p-Isopropyltoluene 574 J 2300 460 ug/kg SW846 8260D
Naphthalene 5810 2300 920 ug/kg SW846 8260D
n-Propylbenzene 11600 2300 460 ug/kg SW846 8260D
Toluene 38300 9200 4600 ug/kg SW846 8260D
4 of 125
FC28792
Summary of Hits Page 2 of 3
Job Number:FC2879
Account:Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Collected:02/20/23 thru 02/21/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,2,4-Trimethylbenzene 70400 2300 460 ug/kg SW846 8260D
1,3,5-Trimethylbenzene 19300 2300 460 ug/kg SW846 8260D
m,p-Xylene 144000 4600 510 ug/kg SW846 8260D
o-Xylene 61300 2300 460 ug/kg SW846 8260D
Xylene (total)206000 6900 970 ug/kg SW846 8260D
TPH-GRO (C6-C10)1750 480 190 mg/kg SW846 8015C
TPH (C10-C28)22.1 5.8 2.9 mg/kg SW846 8015C
FC2879-7 SB-7
Benzene 145 4.3 1.0 ug/kg SW846 8260D
2-Butanone (MEK) a 73.1 21 6.2 ug/kg SW846 8260D
n-Butylbenzene 16.6 4.3 0.85 ug/kg SW846 8260D
Ethylbenzene 1980 250 49 ug/kg SW846 8260D
Isopropylbenzene 54.3 4.3 0.85 ug/kg SW846 8260D
p-Isopropyltoluene 32.0 4.3 0.85 ug/kg SW846 8260D
4-Methyl-2-pentanone (MIBK) b 19.4 J 21 6.4 ug/kg SW846 8260D
Naphthalene 87.7 4.3 1.7 ug/kg SW846 8260D
n-Propylbenzene 130 4.3 0.85 ug/kg SW846 8260D
Toluene 8200 2000 980 ug/kg SW846 8260D
1,2,4-Trimethylbenzene 4380 250 49 ug/kg SW846 8260D
1,3,5-Trimethylbenzene 1040 250 49 ug/kg SW846 8260D
m,p-Xylene 9520 490 54 ug/kg SW846 8260D
o-Xylene 4060 250 49 ug/kg SW846 8260D
Xylene (total)13600 740 100 ug/kg SW846 8260D
TPH-GRO (C6-C10)14.8 5.6 2.2 mg/kg SW846 8015C
TPH (C10-C28)5.36 J 6.3 3.1 mg/kg SW846 8015C
FC2879-8 SB-8
TPH (C10-C28)4.32 J 5.7 2.8 mg/kg SW846 8015C
FC2879-9 SB-9
2-Butanone (MEK)5.9 J 17 5.1 ug/kg SW846 8260D
n-Butylbenzene 1.0 J 3.5 0.70 ug/kg SW846 8260D
sec-Butylbenzene 1.0 J 3.5 0.70 ug/kg SW846 8260D
Ethylbenzene 5.4 3.5 0.70 ug/kg SW846 8260D
Isopropylbenzene 2.2 J 3.5 0.70 ug/kg SW846 8260D
Naphthalene 2.1 J 3.5 1.4 ug/kg SW846 8260D
n-Propylbenzene 6.0 3.5 0.70 ug/kg SW846 8260D
1,2,4-Trimethylbenzene 25.2 3.5 0.70 ug/kg SW846 8260D
1,3,5-Trimethylbenzene 8.1 3.5 0.70 ug/kg SW846 8260D
TPH-GRO (C6-C10)2.19 J 4.5 1.8 mg/kg SW846 8015C
TPH (C10-C28)4.44 J 5.9 2.9 mg/kg SW846 8015C
5 of 125
FC28792
Summary of Hits Page 3 of 3
Job Number:FC2879
Account:Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Collected:02/20/23 thru 02/21/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC2879-10 SB-10
TPH (C10-C28)5.27 J 5.7 2.8 mg/kg SW846 8015C
FC2879-11 SB-11
TPH (C10-C28)4.10 J 5.8 2.9 mg/kg SW846 8015C
FC2879-12 SB-17
Acetone 261 180 92 ug/kg SW846 8260D
Benzene 1.6 J 4.6 1.1 ug/kg SW846 8260D
2-Butanone (MEK)52.0 23 6.7 ug/kg SW846 8260D
Ethyl Alcohol 189 J 370 69 ug/kg SW846 8260D
(a) Associated CCV outside control limits high. Compound was below calibration range in higher dilution.
(b) Associated CCV outside control limits high. ND at higher dilution.
6 of 125
FC28792
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 125
FC28793
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-1
Lab Sample ID:FC2879-1 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185465.D 1 02/24/23 19:14 AL n/a n/a V3C939
Run #2 3C185573.D 1 03/02/23 16:57 AL n/a n/a V3C943
Run #3 a 3C185523.D 1 02/28/23 23:40 DB n/a n/a V3C941
Initial Weight Final Volume Methanol Aliquot
Run #1 6.65 g 5.0 ml 50.0 ul
Run #2 5.76 g 5.0 ml 10.0 ul
Run #3 5.76 g 5.0 ml 25.0 ul
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone b ND 21000 10000 ug/kg
71-43-2 Benzene ND 520 130 ug/kg
108-86-1 Bromobenzene ND 520 100 ug/kg
74-97-5 Bromochloromethane ND 520 150 ug/kg
75-27-4 Bromodichloromethane ND 520 100 ug/kg
75-25-2 Bromoform ND 520 100 ug/kg
78-93-3 2-Butanone (MEK)ND 2600 750 ug/kg
104-51-8 n-Butylbenzene 690 520 100 ug/kg
135-98-8 sec-Butylbenzene ND 520 100 ug/kg
98-06-6 tert-Butylbenzene ND 520 100 ug/kg
56-23-5 Carbon Tetrachloride ND 520 110 ug/kg
108-90-7 Chlorobenzene ND 520 100 ug/kg
75-00-3 Chloroethane c ND 520 210 ug/kg
67-66-3 Chloroform ND 520 140 ug/kg
95-49-8 o-Chlorotoluene ND 520 100 ug/kg
106-43-4 p-Chlorotoluene ND 520 100 ug/kg
124-48-1 Dibromochloromethane ND 520 100 ug/kg
106-93-4 1,2-Dibromoethane ND 520 100 ug/kg
75-71-8 Dichlorodifluoromethane d ND 520 210 ug/kg
95-50-1 1,2-Dichlorobenzene ND 520 100 ug/kg
541-73-1 1,3-Dichlorobenzene ND 520 100 ug/kg
106-46-7 1,4-Dichlorobenzene ND 520 120 ug/kg
75-34-3 1,1-Dichloroethane ND 520 180 ug/kg
107-06-2 1,2-Dichloroethane ND 520 100 ug/kg
75-35-4 1,1-Dichloroethylene ND 520 100 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 520 140 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 520 100 ug/kg
78-87-5 1,2-Dichloropropane ND 520 100 ug/kg
142-28-9 1,3-Dichloropropane ND 520 100 ug/kg
594-20-7 2,2-Dichloropropane ND 520 100 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 125
FC287933.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-1
Lab Sample ID:FC2879-1 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 520 110 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 520 100 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 520 100 ug/kg
108-20-3 Di-Isopropyl Ether ND 520 240 ug/kg
64-17-5 Ethyl Alcohol d ND 41000 7800 ug/kg
100-41-4 Ethylbenzene 9310 520 100 ug/kg
591-78-6 2-Hexanone ND 2600 780 ug/kg
98-82-8 Isopropylbenzene 1350 520 100 ug/kg
99-87-6 p-Isopropyltoluene 1090 520 100 ug/kg
74-83-9 Methyl Bromide ND 520 210 ug/kg
74-87-3 Methyl Chloride d ND 520 210 ug/kg
75-09-2 Methylene Chloride ND 2100 1100 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2600 780 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 520 100 ug/kg
91-20-3 Naphthalene 2470 520 210 ug/kg
103-65-1 n-Propylbenzene 4260 520 100 ug/kg
100-42-5 Styrene ND 520 100 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 520 110 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 520 100 ug/kg
127-18-4 Tetrachloroethylene ND 520 130 ug/kg
108-88-3 Toluene 5500 2100 1000 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 520 150 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 520 100 ug/kg
71-55-6 1,1,1-Trichloroethane ND 520 100 ug/kg
79-00-5 1,1,2-Trichloroethane ND 520 100 ug/kg
79-01-6 Trichloroethylene ND 520 100 ug/kg
75-69-4 Trichlorofluoromethane ND 520 210 ug/kg
96-18-4 1,2,3-Trichloropropane ND 520 130 ug/kg
95-63-6 1,2,4-Trimethylbenzene 60200 e 2900 590 ug/kg
108-67-8 1,3,5-Trimethylbenzene 6870 520 100 ug/kg
108-05-4 Vinyl Acetate f ND 2600 1700 ug/kg
75-01-4 Vinyl Chloride ND 520 100 ug/kg
m,p-Xylene 34000 1000 110 ug/kg
95-47-6 o-Xylene 15100 520 100 ug/kg
1330-20-7 Xylene (total)49100 1600 220 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
1868-53-7 Dibromofluoromethane 91%98%93%75-124%
17060-07-0 1,2-Dichloroethane-D4 101%108%107%72-135%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 125
FC287933.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-1
Lab Sample ID:FC2879-1 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
2037-26-5 Toluene-D8 106%102%106%75-126%
460-00-4 4-Bromofluorobenzene 94%96%95%71-133%
(a) xNot used, further dilution required
(b) Associated CCV outside control limits high, sample is ND.
(c) Associated CCV and BS outside control limits low.
(d) Associated CCV outside control limits low.
(e) Result is from Run# 2
(f) Associated ICV outside control limits high, however sample ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 125
FC287933.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-1
Lab Sample ID:FC2879-1 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14161.D 1 02/27/23 20:50 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.65 g 5.0 ml 5.0 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)300 100 41 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 113%56-149%
98-08-8 aaa-Trifluorotoluene 100%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 125
FC287933.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-1
Lab Sample ID:FC2879-1 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37926.D 1 02/24/23 16:52 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)32.3 5.8 2.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 69%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 125
FC287933.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-2
Lab Sample ID:FC2879-2 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185463.D 1 02/24/23 18:24 AL n/a n/a V3C939
Run #2
Initial Weight Final Volume
Run #1 7.80 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 150 75 ug/kg
71-43-2 Benzene ND 3.7 0.91 ug/kg
108-86-1 Bromobenzene ND 3.7 0.75 ug/kg
74-97-5 Bromochloromethane ND 3.7 1.1 ug/kg
75-27-4 Bromodichloromethane ND 3.7 0.75 ug/kg
75-25-2 Bromoform ND 3.7 0.75 ug/kg
78-93-3 2-Butanone (MEK)ND 19 5.4 ug/kg
104-51-8 n-Butylbenzene ND 3.7 0.75 ug/kg
135-98-8 sec-Butylbenzene ND 3.7 0.75 ug/kg
98-06-6 tert-Butylbenzene ND 3.7 0.75 ug/kg
56-23-5 Carbon Tetrachloride ND 3.7 0.76 ug/kg
108-90-7 Chlorobenzene ND 3.7 0.75 ug/kg
75-00-3 Chloroethane b ND 3.7 1.5 ug/kg
67-66-3 Chloroform ND 3.7 0.99 ug/kg
95-49-8 o-Chlorotoluene ND 3.7 0.75 ug/kg
106-43-4 p-Chlorotoluene ND 3.7 0.75 ug/kg
124-48-1 Dibromochloromethane ND 3.7 0.75 ug/kg
106-93-4 1,2-Dibromoethane ND 3.7 0.75 ug/kg
75-71-8 Dichlorodifluoromethane c ND 3.7 1.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.7 0.75 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.7 0.75 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.7 0.86 ug/kg
75-34-3 1,1-Dichloroethane ND 3.7 1.3 ug/kg
107-06-2 1,2-Dichloroethane ND 3.7 0.75 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.7 0.75 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.7 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.7 0.75 ug/kg
78-87-5 1,2-Dichloropropane ND 3.7 0.75 ug/kg
142-28-9 1,3-Dichloropropane ND 3.7 0.75 ug/kg
594-20-7 2,2-Dichloropropane ND 3.7 0.75 ug/kg
563-58-6 1,1-Dichloropropene ND 3.7 0.76 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.7 0.75 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 125
FC287933.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-2
Lab Sample ID:FC2879-2 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 3.7 0.75 ug/kg
108-20-3 Di-Isopropyl Ether ND 3.7 1.7 ug/kg
64-17-5 Ethyl Alcohol c ND 300 56 ug/kg
100-41-4 Ethylbenzene ND 3.7 0.75 ug/kg
591-78-6 2-Hexanone ND 19 5.6 ug/kg
98-82-8 Isopropylbenzene ND 3.7 0.75 ug/kg
99-87-6 p-Isopropyltoluene ND 3.7 0.75 ug/kg
74-83-9 Methyl Bromide ND 3.7 1.5 ug/kg
74-87-3 Methyl Chloride c ND 3.7 1.5 ug/kg
75-09-2 Methylene Chloride ND 15 8.2 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 19 5.6 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.7 0.75 ug/kg
91-20-3 Naphthalene ND 3.7 1.5 ug/kg
103-65-1 n-Propylbenzene ND 3.7 0.75 ug/kg
100-42-5 Styrene ND 3.7 0.75 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.7 0.77 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.7 0.75 ug/kg
127-18-4 Tetrachloroethylene ND 3.7 0.95 ug/kg
108-88-3 Toluene ND 15 7.5 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.7 1.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.7 0.75 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.7 0.75 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.7 0.75 ug/kg
79-01-6 Trichloroethylene ND 3.7 0.75 ug/kg
75-69-4 Trichlorofluoromethane ND 3.7 1.5 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.7 0.93 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.7 0.75 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.7 0.75 ug/kg
108-05-4 Vinyl Acetate d ND 19 12 ug/kg
75-01-4 Vinyl Chloride ND 3.7 0.75 ug/kg
m,p-Xylene ND 7.5 0.82 ug/kg
95-47-6 o-Xylene ND 3.7 0.75 ug/kg
1330-20-7 Xylene (total)ND 11 1.6 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%75-124%
17060-07-0 1,2-Dichloroethane-D4 109%72-135%
2037-26-5 Toluene-D8 102%75-126%
460-00-4 4-Bromofluorobenzene 96%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 125
FC287933.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-2
Lab Sample ID:FC2879-2 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated CCV and BS outside control limits low.
(c) Associated CCV outside control limits low.
(d) Associated ICV outside control limits high, however sample ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 125
FC287933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-2
Lab Sample ID:FC2879-2 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14137.D 1 02/27/23 11:06 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.64 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.6 1.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 103%56-149%
98-08-8 aaa-Trifluorotoluene 94%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 125
FC287933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-2
Lab Sample ID:FC2879-2 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:86.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37928.D 1 02/24/23 17:52 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 5.8 2.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 66%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 125
FC287933.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-3
Lab Sample ID:FC2879-3 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185464.D 1 02/24/23 18:49 AL n/a n/a V3C939
Run #2
Initial Weight Final Volume
Run #1 9.49 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 120 62 ug/kg
71-43-2 Benzene 1.2 3.1 0.75 ug/kg J
108-86-1 Bromobenzene ND 3.1 0.62 ug/kg
74-97-5 Bromochloromethane ND 3.1 0.91 ug/kg
75-27-4 Bromodichloromethane ND 3.1 0.62 ug/kg
75-25-2 Bromoform ND 3.1 0.62 ug/kg
78-93-3 2-Butanone (MEK)9.2 15 4.5 ug/kg J
104-51-8 n-Butylbenzene ND 3.1 0.62 ug/kg
135-98-8 sec-Butylbenzene ND 3.1 0.62 ug/kg
98-06-6 tert-Butylbenzene ND 3.1 0.62 ug/kg
56-23-5 Carbon Tetrachloride ND 3.1 0.63 ug/kg
108-90-7 Chlorobenzene ND 3.1 0.62 ug/kg
75-00-3 Chloroethane b ND 3.1 1.2 ug/kg
67-66-3 Chloroform ND 3.1 0.82 ug/kg
95-49-8 o-Chlorotoluene ND 3.1 0.62 ug/kg
106-43-4 p-Chlorotoluene ND 3.1 0.62 ug/kg
124-48-1 Dibromochloromethane ND 3.1 0.62 ug/kg
106-93-4 1,2-Dibromoethane ND 3.1 0.62 ug/kg
75-71-8 Dichlorodifluoromethane c ND 3.1 1.2 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.1 0.62 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.1 0.62 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.1 0.71 ug/kg
75-34-3 1,1-Dichloroethane ND 3.1 1.1 ug/kg
107-06-2 1,2-Dichloroethane ND 3.1 0.62 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.1 0.62 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.1 0.85 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.1 0.62 ug/kg
78-87-5 1,2-Dichloropropane ND 3.1 0.62 ug/kg
142-28-9 1,3-Dichloropropane ND 3.1 0.62 ug/kg
594-20-7 2,2-Dichloropropane ND 3.1 0.62 ug/kg
563-58-6 1,1-Dichloropropene ND 3.1 0.63 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.1 0.62 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 125
FC287933.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-3
Lab Sample ID:FC2879-3 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 3.1 0.62 ug/kg
108-20-3 Di-Isopropyl Ether ND 3.1 1.4 ug/kg
64-17-5 Ethyl Alcohol c ND 250 46 ug/kg
100-41-4 Ethylbenzene ND 3.1 0.62 ug/kg
591-78-6 2-Hexanone ND 15 4.6 ug/kg
98-82-8 Isopropylbenzene ND 3.1 0.62 ug/kg
99-87-6 p-Isopropyltoluene ND 3.1 0.62 ug/kg
74-83-9 Methyl Bromide 1.8 3.1 1.2 ug/kg J
74-87-3 Methyl Chloride c ND 3.1 1.2 ug/kg
75-09-2 Methylene Chloride ND 12 6.8 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 15 4.6 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.1 0.62 ug/kg
91-20-3 Naphthalene ND 3.1 1.2 ug/kg
103-65-1 n-Propylbenzene ND 3.1 0.62 ug/kg
100-42-5 Styrene ND 3.1 0.62 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.1 0.64 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.1 0.62 ug/kg
127-18-4 Tetrachloroethylene ND 3.1 0.79 ug/kg
108-88-3 Toluene ND 12 6.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.1 0.86 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.1 0.62 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.1 0.62 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.1 0.62 ug/kg
79-01-6 Trichloroethylene ND 3.1 0.62 ug/kg
75-69-4 Trichlorofluoromethane ND 3.1 1.2 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.1 0.77 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.1 0.62 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.1 0.62 ug/kg
108-05-4 Vinyl Acetate d ND 15 10 ug/kg
75-01-4 Vinyl Chloride ND 3.1 0.62 ug/kg
m,p-Xylene ND 6.2 0.68 ug/kg
95-47-6 o-Xylene ND 3.1 0.62 ug/kg
1330-20-7 Xylene (total)ND 9.3 1.3 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%75-124%
17060-07-0 1,2-Dichloroethane-D4 111%72-135%
2037-26-5 Toluene-D8 102%75-126%
460-00-4 4-Bromofluorobenzene 94%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 125
FC287933.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-3
Lab Sample ID:FC2879-3 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated CCV and BS outside control limits low.
(c) Associated CCV outside control limits low.
(d) Associated ICV outside control limits high, however sample ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 125
FC287933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-3
Lab Sample ID:FC2879-3 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:85.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14138.D 1 02/27/23 11:30 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.68 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.2 1.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 107%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 125
FC287933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-3
Lab Sample ID:FC2879-3 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:85.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37929.D 1 02/24/23 18:22 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)3.86 5.8 2.9 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 70%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 125
FC287933.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-4
Lab Sample ID:FC2879-4 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.6
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B21556.D 1 03/01/23 15:47 AL n/a n/a V2B907
Run #2
Initial Weight Final Volume
Run #1 5.05 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 230 120 ug/kg
71-43-2 Benzene ND 5.8 1.4 ug/kg
108-86-1 Bromobenzene ND 5.8 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.8 1.7 ug/kg
75-27-4 Bromodichloromethane a ND 5.8 1.2 ug/kg
75-25-2 Bromoform ND 5.8 1.2 ug/kg
78-93-3 2-Butanone (MEK)ND 29 8.4 ug/kg
104-51-8 n-Butylbenzene ND 5.8 1.2 ug/kg
135-98-8 sec-Butylbenzene ND 5.8 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 5.8 1.2 ug/kg
56-23-5 Carbon Tetrachloride a ND 5.8 1.2 ug/kg
108-90-7 Chlorobenzene ND 5.8 1.2 ug/kg
75-00-3 Chloroethane b ND 5.8 2.3 ug/kg
67-66-3 Chloroform ND 5.8 1.5 ug/kg
95-49-8 o-Chlorotoluene ND 5.8 1.2 ug/kg
106-43-4 p-Chlorotoluene ND 5.8 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.8 1.2 ug/kg
106-93-4 1,2-Dibromoethane ND 5.8 1.2 ug/kg
75-71-8 Dichlorodifluoromethane c ND 5.8 2.3 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.8 1.2 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.8 1.2 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.8 1.3 ug/kg
75-34-3 1,1-Dichloroethane ND 5.8 2.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.8 1.2 ug/kg
75-35-4 1,1-Dichloroethylene a ND 5.8 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.8 1.6 ug/kg
156-60-5 trans-1,2-Dichloroethylene a ND 5.8 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.8 1.2 ug/kg
142-28-9 1,3-Dichloropropane ND 5.8 1.2 ug/kg
594-20-7 2,2-Dichloropropane a ND 5.8 1.2 ug/kg
563-58-6 1,1-Dichloropropene a ND 5.8 1.2 ug/kg
10061-01-5 cis-1,3-Dichloropropene a ND 5.8 1.2 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 125
FC287933.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-4
Lab Sample ID:FC2879-4 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.6
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.8 1.2 ug/kg
108-20-3 Di-Isopropyl Ether a ND 5.8 2.7 ug/kg
64-17-5 Ethyl Alcohol ND 460 87 ug/kg
100-41-4 Ethylbenzene ND 5.8 1.2 ug/kg
591-78-6 2-Hexanone ND 29 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.8 1.2 ug/kg
99-87-6 p-Isopropyltoluene ND 5.8 1.2 ug/kg
74-83-9 Methyl Bromide b ND 5.8 2.3 ug/kg
74-87-3 Methyl Chloride c ND 5.8 2.3 ug/kg
75-09-2 Methylene Chloride ND 23 13 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 29 8.7 ug/kg
1634-04-4 Methyl Tert Butyl Ether a ND 5.8 1.2 ug/kg
91-20-3 Naphthalene ND 5.8 2.3 ug/kg
103-65-1 n-Propylbenzene ND 5.8 1.2 ug/kg
100-42-5 Styrene ND 5.8 1.2 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.8 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.8 1.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.8 1.5 ug/kg
108-88-3 Toluene ND 23 12 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.8 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.8 1.2 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 5.8 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.8 1.2 ug/kg
79-01-6 Trichloroethylene ND 5.8 1.2 ug/kg
75-69-4 Trichlorofluoromethane c ND 5.8 2.3 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.8 1.4 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.8 1.2 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.8 1.2 ug/kg
108-05-4 Vinyl Acetate ND 29 19 ug/kg
75-01-4 Vinyl Chloride c ND 5.8 1.2 ug/kg
m,p-Xylene ND 12 1.3 ug/kg
95-47-6 o-Xylene ND 5.8 1.2 ug/kg
1330-20-7 Xylene (total)ND 17 2.4 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%75-124%
17060-07-0 1,2-Dichloroethane-D4 101%72-135%
2037-26-5 Toluene-D8 114%75-126%
460-00-4 4-Bromofluorobenzene 108%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 125
FC287933.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-4
Lab Sample ID:FC2879-4 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.6
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated ICV and CCV outside control limits high, however sample ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 125
FC287933.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-4
Lab Sample ID:FC2879-4 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:85.6
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14141.D 1 02/27/23 12:47 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.48 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.3 1.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 125
FC287933.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-4
Lab Sample ID:FC2879-4 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:85.6
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37930.D 1 02/24/23 18:51 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 5.8 2.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 70%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 125
FC287933.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-5
Lab Sample ID:FC2879-5 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.8
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B21557.D 1 03/01/23 16:12 AL n/a n/a V2B907
Run #2
Initial Weight Final Volume
Run #1 5.91 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 190 97 ug/kg
71-43-2 Benzene ND 4.9 1.2 ug/kg
108-86-1 Bromobenzene ND 4.9 0.97 ug/kg
74-97-5 Bromochloromethane ND 4.9 1.4 ug/kg
75-27-4 Bromodichloromethane a ND 4.9 0.97 ug/kg
75-25-2 Bromoform ND 4.9 0.97 ug/kg
78-93-3 2-Butanone (MEK)ND 24 7.1 ug/kg
104-51-8 n-Butylbenzene ND 4.9 0.97 ug/kg
135-98-8 sec-Butylbenzene ND 4.9 0.97 ug/kg
98-06-6 tert-Butylbenzene ND 4.9 0.97 ug/kg
56-23-5 Carbon Tetrachloride a ND 4.9 0.99 ug/kg
108-90-7 Chlorobenzene ND 4.9 0.97 ug/kg
75-00-3 Chloroethane b ND 4.9 1.9 ug/kg
67-66-3 Chloroform ND 4.9 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 4.9 0.97 ug/kg
106-43-4 p-Chlorotoluene ND 4.9 0.97 ug/kg
124-48-1 Dibromochloromethane ND 4.9 0.97 ug/kg
106-93-4 1,2-Dibromoethane ND 4.9 0.97 ug/kg
75-71-8 Dichlorodifluoromethane c ND 4.9 1.9 ug/kg
95-50-1 1,2-Dichlorobenzene ND 4.9 0.97 ug/kg
541-73-1 1,3-Dichlorobenzene ND 4.9 0.97 ug/kg
106-46-7 1,4-Dichlorobenzene ND 4.9 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 4.9 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 4.9 0.97 ug/kg
75-35-4 1,1-Dichloroethylene a ND 4.9 0.97 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.9 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene a ND 4.9 0.97 ug/kg
78-87-5 1,2-Dichloropropane ND 4.9 0.97 ug/kg
142-28-9 1,3-Dichloropropane ND 4.9 0.97 ug/kg
594-20-7 2,2-Dichloropropane a ND 4.9 0.97 ug/kg
563-58-6 1,1-Dichloropropene a ND 4.9 0.99 ug/kg
10061-01-5 cis-1,3-Dichloropropene a ND 4.9 0.97 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 125
FC287933.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-5
Lab Sample ID:FC2879-5 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.8
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.9 0.97 ug/kg
108-20-3 Di-Isopropyl Ether a ND 4.9 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 390 73 ug/kg
100-41-4 Ethylbenzene ND 4.9 0.97 ug/kg
591-78-6 2-Hexanone ND 24 7.3 ug/kg
98-82-8 Isopropylbenzene ND 4.9 0.97 ug/kg
99-87-6 p-Isopropyltoluene ND 4.9 0.97 ug/kg
74-83-9 Methyl Bromide b ND 4.9 1.9 ug/kg
74-87-3 Methyl Chloride c ND 4.9 1.9 ug/kg
75-09-2 Methylene Chloride ND 19 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 24 7.3 ug/kg
1634-04-4 Methyl Tert Butyl Ether a ND 4.9 0.97 ug/kg
91-20-3 Naphthalene ND 4.9 1.9 ug/kg
103-65-1 n-Propylbenzene ND 4.9 0.97 ug/kg
100-42-5 Styrene ND 4.9 0.97 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.9 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 0.97 ug/kg
127-18-4 Tetrachloroethylene ND 4.9 1.2 ug/kg
108-88-3 Toluene ND 19 9.7 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.9 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.9 0.97 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 4.9 0.97 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.9 0.97 ug/kg
79-01-6 Trichloroethylene ND 4.9 0.97 ug/kg
75-69-4 Trichlorofluoromethane c ND 4.9 1.9 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.9 1.2 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.9 0.97 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.9 0.97 ug/kg
108-05-4 Vinyl Acetate ND 24 16 ug/kg
75-01-4 Vinyl Chloride c ND 4.9 0.97 ug/kg
m,p-Xylene ND 9.7 1.1 ug/kg
95-47-6 o-Xylene ND 4.9 0.97 ug/kg
1330-20-7 Xylene (total)ND 15 2.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%75-124%
17060-07-0 1,2-Dichloroethane-D4 101%72-135%
2037-26-5 Toluene-D8 113%75-126%
460-00-4 4-Bromofluorobenzene 108%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 125
FC287933.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-5
Lab Sample ID:FC2879-5 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:86.8
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated CCV and BS outside control limits high, sample is ND.
(c) Associated ICV and CCV outside control limits high, however sample ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 125
FC287933.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-5
Lab Sample ID:FC2879-5 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:86.8
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14142.D 1 02/27/23 13:11 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.12 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.3 1.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 125
FC287933.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-5
Lab Sample ID:FC2879-5 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:86.8
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37931.D 1 02/24/23 19:21 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)3.78 5.7 2.9 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 68%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 125
FC287933.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-6
Lab Sample ID:FC2879-6 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185574.D 1 03/02/23 17:22 AL n/a n/a V3C943
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.86 g 5.0 ml 10.0 ul
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 92000 46000 ug/kg
71-43-2 Benzene ND 2300 560 ug/kg
108-86-1 Bromobenzene ND 2300 460 ug/kg
74-97-5 Bromochloromethane ND 2300 680 ug/kg
75-27-4 Bromodichloromethane ND 2300 460 ug/kg
75-25-2 Bromoform ND 2300 460 ug/kg
78-93-3 2-Butanone (MEK) a ND 12000 3400 ug/kg
104-51-8 n-Butylbenzene 1890 2300 460 ug/kg J
135-98-8 sec-Butylbenzene ND 2300 460 ug/kg
98-06-6 tert-Butylbenzene ND 2300 460 ug/kg
56-23-5 Carbon Tetrachloride a ND 2300 470 ug/kg
108-90-7 Chlorobenzene ND 2300 460 ug/kg
75-00-3 Chloroethane b ND 2300 920 ug/kg
67-66-3 Chloroform ND 2300 620 ug/kg
95-49-8 o-Chlorotoluene ND 2300 460 ug/kg
106-43-4 p-Chlorotoluene ND 2300 460 ug/kg
124-48-1 Dibromochloromethane a ND 2300 460 ug/kg
106-93-4 1,2-Dibromoethane ND 2300 460 ug/kg
75-71-8 Dichlorodifluoromethane a ND 2300 920 ug/kg
95-50-1 1,2-Dichlorobenzene ND 2300 460 ug/kg
541-73-1 1,3-Dichlorobenzene ND 2300 460 ug/kg
106-46-7 1,4-Dichlorobenzene ND 2300 530 ug/kg
75-34-3 1,1-Dichloroethane ND 2300 820 ug/kg
107-06-2 1,2-Dichloroethane a ND 2300 460 ug/kg
75-35-4 1,1-Dichloroethylene ND 2300 460 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 2300 640 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 2300 460 ug/kg
78-87-5 1,2-Dichloropropane ND 2300 460 ug/kg
142-28-9 1,3-Dichloropropane ND 2300 460 ug/kg
594-20-7 2,2-Dichloropropane ND 2300 460 ug/kg
563-58-6 1,1-Dichloropropene ND 2300 470 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 2300 460 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 125
FC287933.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-6
Lab Sample ID:FC2879-6 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2300 460 ug/kg
108-20-3 Di-Isopropyl Ether ND 2300 1100 ug/kg
64-17-5 Ethyl Alcohol a ND 180000 35000 ug/kg
100-41-4 Ethylbenzene 34300 2300 460 ug/kg
591-78-6 2-Hexanone a ND 12000 3500 ug/kg
98-82-8 Isopropylbenzene 3680 2300 460 ug/kg
99-87-6 p-Isopropyltoluene 574 2300 460 ug/kg J
74-83-9 Methyl Bromide ND 2300 920 ug/kg
74-87-3 Methyl Chloride ND 2300 920 ug/kg
75-09-2 Methylene Chloride a ND 9200 5100 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 12000 3500 ug/kg
1634-04-4 Methyl Tert Butyl Ether a ND 2300 460 ug/kg
91-20-3 Naphthalene 5810 2300 920 ug/kg
103-65-1 n-Propylbenzene 11600 2300 460 ug/kg
100-42-5 Styrene ND 2300 460 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane a ND 2300 480 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 2300 460 ug/kg
127-18-4 Tetrachloroethylene ND 2300 590 ug/kg
108-88-3 Toluene 38300 9200 4600 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 2300 650 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 2300 460 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 2300 460 ug/kg
79-00-5 1,1,2-Trichloroethane ND 2300 460 ug/kg
79-01-6 Trichloroethylene ND 2300 460 ug/kg
75-69-4 Trichlorofluoromethane a ND 2300 920 ug/kg
96-18-4 1,2,3-Trichloropropane ND 2300 580 ug/kg
95-63-6 1,2,4-Trimethylbenzene 70400 2300 460 ug/kg
108-67-8 1,3,5-Trimethylbenzene 19300 2300 460 ug/kg
108-05-4 Vinyl Acetate c ND 12000 7600 ug/kg
75-01-4 Vinyl Chloride ND 2300 460 ug/kg
m,p-Xylene 144000 4600 510 ug/kg
95-47-6 o-Xylene 61300 2300 460 ug/kg
1330-20-7 Xylene (total)206000 6900 970 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 94%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 125
FC287933.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-6
Lab Sample ID:FC2879-6 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated BS recovery outside control limits low.
(c) Associated ICV and CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 125
FC287933.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-6
Lab Sample ID:FC2879-6 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:85.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14216.D 10 03/01/23 16:16 JR n/a n/a G1U619
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.48 g 5.0 ml 10.0 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)1750 480 190 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 132%56-149%
98-08-8 aaa-Trifluorotoluene 89%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 125
FC287933.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-6
Lab Sample ID:FC2879-6 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:85.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37932.D 1 02/24/23 19:51 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)22.1 5.8 2.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 67%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 125
FC287933.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-7
Lab Sample ID:FC2879-7 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:79.7
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185567.D 1 03/02/23 14:28 AL n/a n/a V3C943
Run #2 2B21609.D 1 03/03/23 12:52 AL n/a n/a V2B909
Run #3 3C185617.D 1 03/04/23 11:40 AL n/a n/a V3C945
Initial Weight Final Volume Methanol Aliquot
Run #1 7.38 g 5.0 ml
Run #2 8.64 g 5.0 ml 100 ul
Run #3 8.64 g 5.0 ml 50.0 ul
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 170 85 ug/kg
71-43-2 Benzene 145 4.3 1.0 ug/kg
108-86-1 Bromobenzene ND 4.3 0.85 ug/kg
74-97-5 Bromochloromethane ND 4.3 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.3 0.85 ug/kg
75-25-2 Bromoform ND 4.3 0.85 ug/kg
78-93-3 2-Butanone (MEK) b 73.1 21 6.2 ug/kg
104-51-8 n-Butylbenzene 16.6 4.3 0.85 ug/kg
135-98-8 sec-Butylbenzene ND 4.3 0.85 ug/kg
98-06-6 tert-Butylbenzene ND 4.3 0.85 ug/kg
56-23-5 Carbon Tetrachloride a ND 4.3 0.87 ug/kg
108-90-7 Chlorobenzene ND 4.3 0.85 ug/kg
75-00-3 Chloroethane c ND 4.3 1.7 ug/kg
67-66-3 Chloroform ND 4.3 1.1 ug/kg
95-49-8 o-Chlorotoluene ND 4.3 0.85 ug/kg
106-43-4 p-Chlorotoluene ND 4.3 0.85 ug/kg
124-48-1 Dibromochloromethane a ND 4.3 0.85 ug/kg
106-93-4 1,2-Dibromoethane ND 4.3 0.85 ug/kg
75-71-8 Dichlorodifluoromethane a ND 4.3 1.7 ug/kg
95-50-1 1,2-Dichlorobenzene ND 4.3 0.85 ug/kg
541-73-1 1,3-Dichlorobenzene ND 4.3 0.85 ug/kg
106-46-7 1,4-Dichlorobenzene ND 4.3 0.98 ug/kg
75-34-3 1,1-Dichloroethane ND 4.3 1.5 ug/kg
107-06-2 1,2-Dichloroethane a ND 4.3 0.85 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.3 0.85 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.3 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.3 0.85 ug/kg
78-87-5 1,2-Dichloropropane ND 4.3 0.85 ug/kg
142-28-9 1,3-Dichloropropane ND 4.3 0.85 ug/kg
594-20-7 2,2-Dichloropropane ND 4.3 0.85 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 125
FC287933.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-7
Lab Sample ID:FC2879-7 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:79.7
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
563-58-6 1,1-Dichloropropene ND 4.3 0.87 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.3 0.85 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.3 0.85 ug/kg
108-20-3 Di-Isopropyl Ether ND 4.3 2.0 ug/kg
64-17-5 Ethyl Alcohol a ND 340 64 ug/kg
100-41-4 Ethylbenzene 1980 d 250 49 ug/kg
591-78-6 2-Hexanone a ND 21 6.4 ug/kg
98-82-8 Isopropylbenzene 54.3 4.3 0.85 ug/kg
99-87-6 p-Isopropyltoluene 32.0 4.3 0.85 ug/kg
74-83-9 Methyl Bromide ND 4.3 1.7 ug/kg
74-87-3 Methyl Chloride ND 4.3 1.7 ug/kg
75-09-2 Methylene Chloride a ND 17 9.4 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB e 19.4 21 6.4 ug/kg J
1634-04-4 Methyl Tert Butyl Ether a ND 4.3 0.85 ug/kg
91-20-3 Naphthalene 87.7 4.3 1.7 ug/kg
103-65-1 n-Propylbenzene 130 4.3 0.85 ug/kg
100-42-5 Styrene ND 4.3 0.85 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane a ND 4.3 0.88 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.3 0.85 ug/kg
127-18-4 Tetrachloroethylene ND 4.3 1.1 ug/kg
108-88-3 Toluene 8200 f 2000 980 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.3 1.2 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.3 0.85 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 4.3 0.85 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.3 0.85 ug/kg
79-01-6 Trichloroethylene ND 4.3 0.85 ug/kg
75-69-4 Trichlorofluoromethane a ND 4.3 1.7 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.3 1.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene 4380 d 250 49 ug/kg
108-67-8 1,3,5-Trimethylbenzene 1040 d 250 49 ug/kg
108-05-4 Vinyl Acetate g ND 21 14 ug/kg
75-01-4 Vinyl Chloride ND 4.3 0.85 ug/kg
m,p-Xylene 9520 d 490 54 ug/kg
95-47-6 o-Xylene 4060 d 250 49 ug/kg
1330-20-7 Xylene (total)13600 d 740 100 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
1868-53-7 Dibromofluoromethane 98%92%98%75-124%
17060-07-0 1,2-Dichloroethane-D4 124%101%118%72-135%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 125
FC287933.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-7
Lab Sample ID:FC2879-7 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:79.7
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
2037-26-5 Toluene-D8 105%103%101%75-126%
460-00-4 4-Bromofluorobenzene 103%103%94%71-133%
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated CCV outside control limits high. Compound was below calibration range in higher dilution.
(c) Associated BS recovery outside control limits low.
(d) Result is from Run# 2
(e) Associated CCV outside control limits high. ND at higher dilution.
(f) Result is from Run# 3
(g) Associated ICV and CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 125
FC287933.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-7
Lab Sample ID:FC2879-7 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:79.7
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14215.D 1 03/01/23 15:50 JR n/a n/a G1U619
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.30 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)14.8 5.6 2.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 126%56-149%
98-08-8 aaa-Trifluorotoluene 85%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 125
FC287933.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-7
Lab Sample ID:FC2879-7 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:79.7
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37933.D 1 02/24/23 20:20 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)5.36 6.3 3.1 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 70%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 125
FC287933.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-8
Lab Sample ID:FC2879-8 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B21610.D 1 03/03/23 13:17 AL n/a n/a V2B909
Run #2
Initial Weight Final Volume
Run #1 5.04 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 230 110 ug/kg
71-43-2 Benzene ND 5.6 1.4 ug/kg
108-86-1 Bromobenzene ND 5.6 1.1 ug/kg
74-97-5 Bromochloromethane ND 5.6 1.7 ug/kg
75-27-4 Bromodichloromethane ND 5.6 1.1 ug/kg
75-25-2 Bromoform ND 5.6 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 28 8.2 ug/kg
104-51-8 n-Butylbenzene ND 5.6 1.1 ug/kg
135-98-8 sec-Butylbenzene ND 5.6 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 5.6 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.6 1.1 ug/kg
108-90-7 Chlorobenzene ND 5.6 1.1 ug/kg
75-00-3 Chloroethane a ND 5.6 2.3 ug/kg
67-66-3 Chloroform ND 5.6 1.5 ug/kg
95-49-8 o-Chlorotoluene ND 5.6 1.1 ug/kg
106-43-4 p-Chlorotoluene ND 5.6 1.1 ug/kg
124-48-1 Dibromochloromethane ND 5.6 1.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.6 1.1 ug/kg
75-71-8 Dichlorodifluoromethane b ND 5.6 2.3 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.6 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.6 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.6 1.3 ug/kg
75-34-3 1,1-Dichloroethane ND 5.6 2.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.6 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.6 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.6 1.6 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.6 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.6 1.1 ug/kg
142-28-9 1,3-Dichloropropane ND 5.6 1.1 ug/kg
594-20-7 2,2-Dichloropropane ND 5.6 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 5.6 1.1 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.6 1.1 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 125
FC287933.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-8
Lab Sample ID:FC2879-8 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.6 1.1 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.6 2.6 ug/kg
64-17-5 Ethyl Alcohol ND 450 85 ug/kg
100-41-4 Ethylbenzene ND 5.6 1.1 ug/kg
591-78-6 2-Hexanone ND 28 8.5 ug/kg
98-82-8 Isopropylbenzene ND 5.6 1.1 ug/kg
99-87-6 p-Isopropyltoluene ND 5.6 1.1 ug/kg
74-83-9 Methyl Bromide c ND 5.6 2.3 ug/kg
74-87-3 Methyl Chloride b ND 5.6 2.3 ug/kg
75-09-2 Methylene Chloride ND 23 12 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 28 8.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether c ND 5.6 1.1 ug/kg
91-20-3 Naphthalene ND 5.6 2.3 ug/kg
103-65-1 n-Propylbenzene ND 5.6 1.1 ug/kg
100-42-5 Styrene ND 5.6 1.1 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.6 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.6 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.6 1.4 ug/kg
108-88-3 Toluene ND 23 11 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.6 1.6 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.6 1.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.6 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.6 1.1 ug/kg
79-01-6 Trichloroethylene ND 5.6 1.1 ug/kg
75-69-4 Trichlorofluoromethane c ND 5.6 2.3 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.6 1.4 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.6 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.6 1.1 ug/kg
108-05-4 Vinyl Acetate ND 28 18 ug/kg
75-01-4 Vinyl Chloride b ND 5.6 1.1 ug/kg
m,p-Xylene ND 11 1.2 ug/kg
95-47-6 o-Xylene ND 5.6 1.1 ug/kg
1330-20-7 Xylene (total)ND 17 2.4 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%72-135%
2037-26-5 Toluene-D8 110%75-126%
460-00-4 4-Bromofluorobenzene 104%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 125
FC287933.8
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-8
Lab Sample ID:FC2879-8 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV and BS outside control limits high, sample is ND.
(b) Associated ICV and CCV outside control limits high, sample is ND.
(c) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 125
FC287933.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-8
Lab Sample ID:FC2879-8 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:88.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14148.D 1 02/27/23 15:35 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.53 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.0 1.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 110%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 125
FC287933.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-8
Lab Sample ID:FC2879-8 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:88.0
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37937.D 1 02/24/23 22:19 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)4.32 5.7 2.8 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 70%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 125
FC287933.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-9
Lab Sample ID:FC2879-9 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.4
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B21611.D 1 03/03/23 13:42 AL n/a n/a V2B909
Run #2
Initial Weight Final Volume
Run #1 8.38 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 140 70 ug/kg
71-43-2 Benzene ND 3.5 0.85 ug/kg
108-86-1 Bromobenzene ND 3.5 0.70 ug/kg
74-97-5 Bromochloromethane ND 3.5 1.0 ug/kg
75-27-4 Bromodichloromethane ND 3.5 0.70 ug/kg
75-25-2 Bromoform ND 3.5 0.70 ug/kg
78-93-3 2-Butanone (MEK)5.9 17 5.1 ug/kg J
104-51-8 n-Butylbenzene 1.0 3.5 0.70 ug/kg J
135-98-8 sec-Butylbenzene 1.0 3.5 0.70 ug/kg J
98-06-6 tert-Butylbenzene ND 3.5 0.70 ug/kg
56-23-5 Carbon Tetrachloride ND 3.5 0.71 ug/kg
108-90-7 Chlorobenzene ND 3.5 0.70 ug/kg
75-00-3 Chloroethane a ND 3.5 1.4 ug/kg
67-66-3 Chloroform ND 3.5 0.93 ug/kg
95-49-8 o-Chlorotoluene ND 3.5 0.70 ug/kg
106-43-4 p-Chlorotoluene ND 3.5 0.70 ug/kg
124-48-1 Dibromochloromethane ND 3.5 0.70 ug/kg
106-93-4 1,2-Dibromoethane ND 3.5 0.70 ug/kg
75-71-8 Dichlorodifluoromethane b ND 3.5 1.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.5 0.70 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.5 0.70 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.5 0.80 ug/kg
75-34-3 1,1-Dichloroethane ND 3.5 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 3.5 0.70 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.5 0.70 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.5 0.96 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.5 0.70 ug/kg
78-87-5 1,2-Dichloropropane ND 3.5 0.70 ug/kg
142-28-9 1,3-Dichloropropane ND 3.5 0.70 ug/kg
594-20-7 2,2-Dichloropropane ND 3.5 0.70 ug/kg
563-58-6 1,1-Dichloropropene ND 3.5 0.71 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.5 0.70 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 125
FC287933.9
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-9
Lab Sample ID:FC2879-9 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.4
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 3.5 0.70 ug/kg
108-20-3 Di-Isopropyl Ether ND 3.5 1.6 ug/kg
64-17-5 Ethyl Alcohol ND 280 52 ug/kg
100-41-4 Ethylbenzene 5.4 3.5 0.70 ug/kg
591-78-6 2-Hexanone ND 17 5.2 ug/kg
98-82-8 Isopropylbenzene 2.2 3.5 0.70 ug/kg J
99-87-6 p-Isopropyltoluene ND 3.5 0.70 ug/kg
74-83-9 Methyl Bromide c ND 3.5 1.4 ug/kg
74-87-3 Methyl Chloride b ND 3.5 1.4 ug/kg
75-09-2 Methylene Chloride ND 14 7.7 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 17 5.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether c ND 3.5 0.70 ug/kg
91-20-3 Naphthalene 2.1 3.5 1.4 ug/kg J
103-65-1 n-Propylbenzene 6.0 3.5 0.70 ug/kg
100-42-5 Styrene ND 3.5 0.70 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 3.5 0.72 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.5 0.70 ug/kg
127-18-4 Tetrachloroethylene ND 3.5 0.89 ug/kg
108-88-3 Toluene ND 14 7.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.5 0.98 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.5 0.70 ug/kg
71-55-6 1,1,1-Trichloroethane ND 3.5 0.70 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.5 0.70 ug/kg
79-01-6 Trichloroethylene ND 3.5 0.70 ug/kg
75-69-4 Trichlorofluoromethane c ND 3.5 1.4 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.5 0.87 ug/kg
95-63-6 1,2,4-Trimethylbenzene 25.2 3.5 0.70 ug/kg
108-67-8 1,3,5-Trimethylbenzene 8.1 3.5 0.70 ug/kg
108-05-4 Vinyl Acetate ND 17 11 ug/kg
75-01-4 Vinyl Chloride b ND 3.5 0.70 ug/kg
m,p-Xylene ND 7.0 0.77 ug/kg
95-47-6 o-Xylene ND 3.5 0.70 ug/kg
1330-20-7 Xylene (total)ND 10 1.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%75-124%
17060-07-0 1,2-Dichloroethane-D4 100%72-135%
2037-26-5 Toluene-D8 108%75-126%
460-00-4 4-Bromofluorobenzene 110%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 125
FC287933.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-9
Lab Sample ID:FC2879-9 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.4
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV and BS outside control limits high, sample is ND.
(b) Associated ICV and CCV outside control limits high, sample is ND.
(c) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 125
FC287933.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-9
Lab Sample ID:FC2879-9 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:85.4
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14149.D 1 02/27/23 16:00 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 8.12 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)2.19 4.5 1.8 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 100%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 125
FC287933.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-9
Lab Sample ID:FC2879-9 Date Sampled:02/20/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:85.4
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37938.D 1 02/24/23 22:48 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)4.44 5.9 2.9 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 68%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 125
FC287933.9
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-10
Lab Sample ID:FC2879-10 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:87.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185570.D 1 03/02/23 15:43 AL n/a n/a V3C943
Run #2
Initial Weight Final Volume
Run #1 7.82 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 150 73 ug/kg
71-43-2 Benzene ND 3.7 0.89 ug/kg
108-86-1 Bromobenzene ND 3.7 0.73 ug/kg
74-97-5 Bromochloromethane ND 3.7 1.1 ug/kg
75-27-4 Bromodichloromethane ND 3.7 0.73 ug/kg
75-25-2 Bromoform ND 3.7 0.73 ug/kg
78-93-3 2-Butanone (MEK) a ND 18 5.3 ug/kg
104-51-8 n-Butylbenzene ND 3.7 0.73 ug/kg
135-98-8 sec-Butylbenzene ND 3.7 0.73 ug/kg
98-06-6 tert-Butylbenzene ND 3.7 0.73 ug/kg
56-23-5 Carbon Tetrachloride a ND 3.7 0.75 ug/kg
108-90-7 Chlorobenzene ND 3.7 0.73 ug/kg
75-00-3 Chloroethane b ND 3.7 1.5 ug/kg
67-66-3 Chloroform ND 3.7 0.97 ug/kg
95-49-8 o-Chlorotoluene ND 3.7 0.73 ug/kg
106-43-4 p-Chlorotoluene ND 3.7 0.73 ug/kg
124-48-1 Dibromochloromethane a ND 3.7 0.73 ug/kg
106-93-4 1,2-Dibromoethane ND 3.7 0.73 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.7 1.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.7 0.73 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.7 0.73 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.7 0.84 ug/kg
75-34-3 1,1-Dichloroethane ND 3.7 1.3 ug/kg
107-06-2 1,2-Dichloroethane a ND 3.7 0.73 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.7 0.73 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.7 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.7 0.73 ug/kg
78-87-5 1,2-Dichloropropane ND 3.7 0.73 ug/kg
142-28-9 1,3-Dichloropropane ND 3.7 0.73 ug/kg
594-20-7 2,2-Dichloropropane ND 3.7 0.73 ug/kg
563-58-6 1,1-Dichloropropene ND 3.7 0.75 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.7 0.73 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 125
FC287933.10
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-10
Lab Sample ID:FC2879-10 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:87.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 3.7 0.73 ug/kg
108-20-3 Di-Isopropyl Ether ND 3.7 1.7 ug/kg
64-17-5 Ethyl Alcohol a ND 290 55 ug/kg
100-41-4 Ethylbenzene ND 3.7 0.73 ug/kg
591-78-6 2-Hexanone a ND 18 5.5 ug/kg
98-82-8 Isopropylbenzene ND 3.7 0.73 ug/kg
99-87-6 p-Isopropyltoluene ND 3.7 0.73 ug/kg
74-83-9 Methyl Bromide ND 3.7 1.5 ug/kg
74-87-3 Methyl Chloride ND 3.7 1.5 ug/kg
75-09-2 Methylene Chloride a ND 15 8.1 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 18 5.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether a ND 3.7 0.73 ug/kg
91-20-3 Naphthalene ND 3.7 1.5 ug/kg
103-65-1 n-Propylbenzene ND 3.7 0.73 ug/kg
100-42-5 Styrene ND 3.7 0.73 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane a ND 3.7 0.75 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.7 0.73 ug/kg
127-18-4 Tetrachloroethylene ND 3.7 0.94 ug/kg
108-88-3 Toluene ND 15 7.3 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.7 1.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.7 0.73 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 3.7 0.73 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.7 0.73 ug/kg
79-01-6 Trichloroethylene ND 3.7 0.73 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.7 1.5 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.7 0.92 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.7 0.73 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.7 0.73 ug/kg
108-05-4 Vinyl Acetate c ND 18 12 ug/kg
75-01-4 Vinyl Chloride ND 3.7 0.73 ug/kg
m,p-Xylene ND 7.3 0.81 ug/kg
95-47-6 o-Xylene ND 3.7 0.73 ug/kg
1330-20-7 Xylene (total)ND 11 1.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 100%75-126%
460-00-4 4-Bromofluorobenzene 94%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 125
FC287933.10
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-10
Lab Sample ID:FC2879-10 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:87.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated BS recovery outside control limits low.
(c) Associated ICV and CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 125
FC287933.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-10
Lab Sample ID:FC2879-10 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:87.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14150.D 1 02/27/23 16:24 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.07 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.8 1.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 125
FC287933.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-10
Lab Sample ID:FC2879-10 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:87.3
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37939.D 1 02/24/23 23:18 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)5.27 5.7 2.8 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 71%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 125
FC287933.10
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-11
Lab Sample ID:FC2879-11 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3C185571.D 1 03/02/23 16:08 AL n/a n/a V3C943
Run #2
Initial Weight Final Volume
Run #1 8.33 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a ND 140 70 ug/kg
71-43-2 Benzene ND 3.5 0.86 ug/kg
108-86-1 Bromobenzene ND 3.5 0.70 ug/kg
74-97-5 Bromochloromethane ND 3.5 1.0 ug/kg
75-27-4 Bromodichloromethane ND 3.5 0.70 ug/kg
75-25-2 Bromoform ND 3.5 0.70 ug/kg
78-93-3 2-Butanone (MEK) a ND 18 5.1 ug/kg
104-51-8 n-Butylbenzene ND 3.5 0.70 ug/kg
135-98-8 sec-Butylbenzene ND 3.5 0.70 ug/kg
98-06-6 tert-Butylbenzene ND 3.5 0.70 ug/kg
56-23-5 Carbon Tetrachloride a ND 3.5 0.72 ug/kg
108-90-7 Chlorobenzene ND 3.5 0.70 ug/kg
75-00-3 Chloroethane b ND 3.5 1.4 ug/kg
67-66-3 Chloroform ND 3.5 0.94 ug/kg
95-49-8 o-Chlorotoluene ND 3.5 0.70 ug/kg
106-43-4 p-Chlorotoluene ND 3.5 0.70 ug/kg
124-48-1 Dibromochloromethane a ND 3.5 0.70 ug/kg
106-93-4 1,2-Dibromoethane ND 3.5 0.70 ug/kg
75-71-8 Dichlorodifluoromethane a ND 3.5 1.4 ug/kg
95-50-1 1,2-Dichlorobenzene ND 3.5 0.70 ug/kg
541-73-1 1,3-Dichlorobenzene ND 3.5 0.70 ug/kg
106-46-7 1,4-Dichlorobenzene ND 3.5 0.81 ug/kg
75-34-3 1,1-Dichloroethane ND 3.5 1.2 ug/kg
107-06-2 1,2-Dichloroethane a ND 3.5 0.70 ug/kg
75-35-4 1,1-Dichloroethylene ND 3.5 0.70 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.5 0.97 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.5 0.70 ug/kg
78-87-5 1,2-Dichloropropane ND 3.5 0.70 ug/kg
142-28-9 1,3-Dichloropropane ND 3.5 0.70 ug/kg
594-20-7 2,2-Dichloropropane ND 3.5 0.70 ug/kg
563-58-6 1,1-Dichloropropene ND 3.5 0.72 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.5 0.70 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
58 of 125
FC287933.11
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-11
Lab Sample ID:FC2879-11 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 3.5 0.70 ug/kg
108-20-3 Di-Isopropyl Ether ND 3.5 1.6 ug/kg
64-17-5 Ethyl Alcohol a ND 280 53 ug/kg
100-41-4 Ethylbenzene ND 3.5 0.70 ug/kg
591-78-6 2-Hexanone a ND 18 5.3 ug/kg
98-82-8 Isopropylbenzene ND 3.5 0.70 ug/kg
99-87-6 p-Isopropyltoluene ND 3.5 0.70 ug/kg
74-83-9 Methyl Bromide ND 3.5 1.4 ug/kg
74-87-3 Methyl Chloride ND 3.5 1.4 ug/kg
75-09-2 Methylene Chloride a ND 14 7.7 ug/kg
108-10-1 4-Methyl-2-pentanone (MIB a ND 18 5.3 ug/kg
1634-04-4 Methyl Tert Butyl Ether a ND 3.5 0.70 ug/kg
91-20-3 Naphthalene ND 3.5 1.4 ug/kg
103-65-1 n-Propylbenzene ND 3.5 0.70 ug/kg
100-42-5 Styrene ND 3.5 0.70 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane a ND 3.5 0.73 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.5 0.70 ug/kg
127-18-4 Tetrachloroethylene ND 3.5 0.90 ug/kg
108-88-3 Toluene ND 14 7.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 3.5 0.99 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 3.5 0.70 ug/kg
71-55-6 1,1,1-Trichloroethane a ND 3.5 0.70 ug/kg
79-00-5 1,1,2-Trichloroethane ND 3.5 0.70 ug/kg
79-01-6 Trichloroethylene ND 3.5 0.70 ug/kg
75-69-4 Trichlorofluoromethane a ND 3.5 1.4 ug/kg
96-18-4 1,2,3-Trichloropropane ND 3.5 0.88 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 3.5 0.70 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 3.5 0.70 ug/kg
108-05-4 Vinyl Acetate c ND 18 12 ug/kg
75-01-4 Vinyl Chloride ND 3.5 0.70 ug/kg
m,p-Xylene ND 7.0 0.77 ug/kg
95-47-6 o-Xylene ND 3.5 0.70 ug/kg
1330-20-7 Xylene (total)ND 11 1.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 116%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
59 of 125
FC287933.11
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-11
Lab Sample ID:FC2879-11 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:85.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside control limits high, sample is ND.
(b) Associated BS recovery outside control limits low.
(c) Associated ICV and CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
60 of 125
FC287933.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-11
Lab Sample ID:FC2879-11 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:85.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14151.D 1 02/27/23 16:48 JR n/a n/a G1U617
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.59 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.3 2.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 96%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
61 of 125
FC287933.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-11
Lab Sample ID:FC2879-11 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:85.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37940.D 1 02/24/23 23:47 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)4.10 5.8 2.9 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 69%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
62 of 125
FC287933.11
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-17
Lab Sample ID:FC2879-12 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B21612.D 1 03/03/23 14:07 AL n/a n/a V2B909
Run #2
Initial Weight Final Volume
Run #1 6.18 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 261 180 92 ug/kg
71-43-2 Benzene 1.6 4.6 1.1 ug/kg J
108-86-1 Bromobenzene ND 4.6 0.92 ug/kg
74-97-5 Bromochloromethane ND 4.6 1.4 ug/kg
75-27-4 Bromodichloromethane ND 4.6 0.92 ug/kg
75-25-2 Bromoform ND 4.6 0.92 ug/kg
78-93-3 2-Butanone (MEK)52.0 23 6.7 ug/kg
104-51-8 n-Butylbenzene ND 4.6 0.92 ug/kg
135-98-8 sec-Butylbenzene ND 4.6 0.92 ug/kg
98-06-6 tert-Butylbenzene ND 4.6 0.92 ug/kg
56-23-5 Carbon Tetrachloride ND 4.6 0.94 ug/kg
108-90-7 Chlorobenzene ND 4.6 0.92 ug/kg
75-00-3 Chloroethane a ND 4.6 1.8 ug/kg
67-66-3 Chloroform ND 4.6 1.2 ug/kg
95-49-8 o-Chlorotoluene ND 4.6 0.92 ug/kg
106-43-4 p-Chlorotoluene ND 4.6 0.92 ug/kg
124-48-1 Dibromochloromethane ND 4.6 0.92 ug/kg
106-93-4 1,2-Dibromoethane ND 4.6 0.92 ug/kg
75-71-8 Dichlorodifluoromethane b ND 4.6 1.8 ug/kg
95-50-1 1,2-Dichlorobenzene ND 4.6 0.92 ug/kg
541-73-1 1,3-Dichlorobenzene ND 4.6 0.92 ug/kg
106-46-7 1,4-Dichlorobenzene ND 4.6 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 4.6 1.6 ug/kg
107-06-2 1,2-Dichloroethane ND 4.6 0.92 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.6 0.92 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.6 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.6 0.92 ug/kg
78-87-5 1,2-Dichloropropane ND 4.6 0.92 ug/kg
142-28-9 1,3-Dichloropropane ND 4.6 0.92 ug/kg
594-20-7 2,2-Dichloropropane ND 4.6 0.92 ug/kg
563-58-6 1,1-Dichloropropene ND 4.6 0.94 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.6 0.92 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
63 of 125
FC287933.12
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-17
Lab Sample ID:FC2879-12 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.6 0.92 ug/kg
108-20-3 Di-Isopropyl Ether ND 4.6 2.1 ug/kg
64-17-5 Ethyl Alcohol 189 370 69 ug/kg J
100-41-4 Ethylbenzene ND 4.6 0.92 ug/kg
591-78-6 2-Hexanone ND 23 6.9 ug/kg
98-82-8 Isopropylbenzene ND 4.6 0.92 ug/kg
99-87-6 p-Isopropyltoluene ND 4.6 0.92 ug/kg
74-83-9 Methyl Bromide c ND 4.6 1.8 ug/kg
74-87-3 Methyl Chloride b ND 4.6 1.8 ug/kg
75-09-2 Methylene Chloride ND 18 10 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 23 6.9 ug/kg
1634-04-4 Methyl Tert Butyl Ether c ND 4.6 0.92 ug/kg
91-20-3 Naphthalene ND 4.6 1.8 ug/kg
103-65-1 n-Propylbenzene ND 4.6 0.92 ug/kg
100-42-5 Styrene ND 4.6 0.92 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 4.6 0.94 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.6 0.92 ug/kg
127-18-4 Tetrachloroethylene ND 4.6 1.2 ug/kg
108-88-3 Toluene ND 18 9.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 4.6 1.3 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 4.6 0.92 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.6 0.92 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.6 0.92 ug/kg
79-01-6 Trichloroethylene ND 4.6 0.92 ug/kg
75-69-4 Trichlorofluoromethane c ND 4.6 1.8 ug/kg
96-18-4 1,2,3-Trichloropropane ND 4.6 1.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 4.6 0.92 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 4.6 0.92 ug/kg
108-05-4 Vinyl Acetate ND 23 15 ug/kg
75-01-4 Vinyl Chloride b ND 4.6 0.92 ug/kg
m,p-Xylene ND 9.2 1.0 ug/kg
95-47-6 o-Xylene ND 4.6 0.92 ug/kg
1330-20-7 Xylene (total)ND 14 1.9 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%72-135%
2037-26-5 Toluene-D8 110%75-126%
460-00-4 4-Bromofluorobenzene 110%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
64 of 125
FC287933.12
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-17
Lab Sample ID:FC2879-12 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8260D Percent Solids:88.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV and BS outside control limits high, sample is ND.
(b) Associated ICV and CCV outside control limits high, sample is ND.
(c) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
65 of 125
FC287933.12
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-17
Lab Sample ID:FC2879-12 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C Percent Solids:88.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U14169.D 1 02/28/23 11:02 JR n/a n/a G1U618
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.80 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.6 2.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 111%56-149%
98-08-8 aaa-Trifluorotoluene 89%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
66 of 125
FC287933.12
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-17
Lab Sample ID:FC2879-12 Date Sampled:02/21/23
Matrix:SO - Soil Date Received:02/22/23
Method:SW846 8015C SW846 3546 Percent Solids:88.2
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW37941.D 1 02/25/23 00:17 EG 02/24/23 08:00 OP95605 GWW1484
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 5.7 2.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 66%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
67 of 125
FC287933.12
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
68 of 125
FC28794
FC2879: Chain of Custody
Page 1 of 3
69 of 125
FC287944.1
FC2879: Chain of Custody
Page 2 of 3
70 of 125
FC287944.1
Job Number:FC2879 Client:GES
Date / Time Received:2/22/2023 9:30:00 AM Delivery Method:FX
Project:MURPHY # 2701997
Airbill #'s:570790507267
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments FROZEN @ 1400 // 2/22/23
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.4);
Cooler 1: (2.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:NATHANS Date:Date:2/22/2023 9:30:00 AM
FC2879: Chain of Custody
Page 3 of 3
71 of 125
FC287944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
72 of 125
FC28795
Method Blank Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-MB 3C185449.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
73 of 125
FC287955.1.1
Method Blank Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-MB 3C185449.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 94%75-124%
17060-07-0 1,2-Dichloroethane-D4 101%72-135%
2037-26-5 Toluene-D8 102%75-126%
74 of 125
FC287955.1.1
Method Blank Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-MB 3C185449.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 96%71-133%
75 of 125
FC287955.1.1
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C941-MB 3C185503.D 1 02/28/23 DB n/a n/a V3C941
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%72-135%
2037-26-5 Toluene-D8 103%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
76 of 125
FC287955.1.2
Method Blank Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-MB 2B21545.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
77 of 125
FC287955.1.3
Method Blank Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-MB 2B21545.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 95%75-124%
17060-07-0 1,2-Dichloroethane-D4 99%72-135%
2037-26-5 Toluene-D8 110%75-126%
78 of 125
FC287955.1.3
Method Blank Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-MB 2B21545.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 107%71-133%
79 of 125
FC287955.1.3
Method Blank Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-MB 3C185559.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
80 of 125
FC287955.1.4
Method Blank Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-MB 3C185559.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride a 21.4 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 110%72-135%
2037-26-5 Toluene-D8 102%75-126%
81 of 125
FC287955.1.4
Method Blank Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-MB 3C185559.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%71-133%
(a) Suspected laboratory contaminant.
82 of 125
FC287955.1.4
Method Blank Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-MB 2B21605.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
83 of 125
FC287955.1.5
Method Blank Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-MB 2B21605.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 95%75-124%
17060-07-0 1,2-Dichloroethane-D4 102%72-135%
2037-26-5 Toluene-D8 109%75-126%
84 of 125
FC287955.1.5
Method Blank Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-MB 2B21605.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 108%71-133%
85 of 125
FC287955.1.5
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C945-MB 3C185616.D 1 03/04/23 AL n/a n/a V3C945
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7
CAS No.Compound Result RL MDL Units Q
108-88-3 Toluene ND 20 10 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 110%72-135%
2037-26-5 Toluene-D8 100%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
86 of 125
FC287955.1.6
Blank Spike Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-BS 3C185447.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 285 114 61-152
71-43-2 Benzene 50 48.9 98 76-126
108-86-1 Bromobenzene 50 52.4 105 76-122
74-97-5 Bromochloromethane 50 51.2 102 77-120
75-27-4 Bromodichloromethane 50 47.2 94 74-130
75-25-2 Bromoform 50 49.1 98 76-127
78-93-3 2-Butanone (MEK)250 246 98 75-137
104-51-8 n-Butylbenzene 50 50.9 102 71-128
135-98-8 sec-Butylbenzene 50 47.2 94 79-135
98-06-6 tert-Butylbenzene 50 47.9 96 77-133
56-23-5 Carbon Tetrachloride 50 49.8 100 78-133
108-90-7 Chlorobenzene 50 53.2 106 81-129
75-00-3 Chloroethane 50 30.0 60* a 68-133
67-66-3 Chloroform 50 49.0 98 72-123
95-49-8 o-Chlorotoluene 50 48.4 97 77-129
106-43-4 p-Chlorotoluene 50 47.5 95 80-134
124-48-1 Dibromochloromethane 50 55.9 112 76-127
106-93-4 1,2-Dibromoethane 50 53.8 108 77-126
75-71-8 Dichlorodifluoromethane 50 74.2 148 68-168
95-50-1 1,2-Dichlorobenzene 50 49.6 99 80-129
541-73-1 1,3-Dichlorobenzene 50 49.4 99 81-129
106-46-7 1,4-Dichlorobenzene 50 50.0 100 76-130
75-34-3 1,1-Dichloroethane 50 46.9 94 73-125
107-06-2 1,2-Dichloroethane 50 48.7 97 74-128
75-35-4 1,1-Dichloroethylene 50 47.9 96 81-136
156-59-2 cis-1,2-Dichloroethylene 50 48.0 96 74-126
156-60-5 trans-1,2-Dichloroethylene 50 47.7 95 70-127
78-87-5 1,2-Dichloropropane 50 49.9 100 74-125
142-28-9 1,3-Dichloropropane 50 52.6 105 76-122
594-20-7 2,2-Dichloropropane 50 51.0 102 77-133
563-58-6 1,1-Dichloropropene 50 50.3 101 75-130
10061-01-5 cis-1,3-Dichloropropene 50 49.8 100 80-123
10061-02-6 trans-1,3-Dichloropropene 50 49.8 100 75-131
108-20-3 Di-Isopropyl Ether 50 47.0 94 75-122
64-17-5 Ethyl Alcohol 1000 1120 112 53-154
100-41-4 Ethylbenzene 50 52.6 105 77-123
* = Outside of Control Limits.
87 of 125
FC287955.2.1
Blank Spike Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-BS 3C185447.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 264 106 72-133
98-82-8 Isopropylbenzene 50 52.7 105 80-136
99-87-6 p-Isopropyltoluene 50 47.6 95 77-131
74-83-9 Methyl Bromide 50 55.9 112 65-139
74-87-3 Methyl Chloride 50 50.8 102 71-144
75-09-2 Methylene Chloride 50 47.8 96 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 272 109 76-132
1634-04-4 Methyl Tert Butyl Ether 50 53.6 107 77-120
91-20-3 Naphthalene 50 52.6 105 79-129
103-65-1 n-Propylbenzene 50 48.5 97 80-135
100-42-5 Styrene 50 54.9 110 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 54.5 109 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 49.9 100 71-126
127-18-4 Tetrachloroethylene 50 56.1 112 79-130
108-88-3 Toluene 50 52.5 105 76-124
87-61-6 1,2,3-Trichlorobenzene 50 52.1 104 77-128
120-82-1 1,2,4-Trichlorobenzene 50 52.2 104 78-130
71-55-6 1,1,1-Trichloroethane 50 50.1 100 70-129
79-00-5 1,1,2-Trichloroethane 50 52.2 104 74-124
79-01-6 Trichloroethylene 50 49.3 99 75-128
75-69-4 Trichlorofluoromethane 50 53.4 107 73-145
96-18-4 1,2,3-Trichloropropane 50 53.6 107 74-127
95-63-6 1,2,4-Trimethylbenzene 50 49.0 98 74-123
108-67-8 1,3,5-Trimethylbenzene 50 50.1 100 73-122
108-05-4 Vinyl Acetate 250 260 104 48-164
75-01-4 Vinyl Chloride 50 52.9 106 76-141
m,p-Xylene 100 107 107 80-128
95-47-6 o-Xylene 50 52.1 104 80-132
1330-20-7 Xylene (total)150 159 106 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 99%72-135%
2037-26-5 Toluene-D8 106%75-126%
* = Outside of Control Limits.
88 of 125
FC287955.2.1
Blank Spike Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C939-BS 3C185447.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
(a) Sporadic marginal failure.
* = Outside of Control Limits.
89 of 125
FC287955.2.1
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C941-BS 3C185501.D 1 02/28/23 DB n/a n/a V3C941
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 103%72-135%
2037-26-5 Toluene-D8 103%75-126%
460-00-4 4-Bromofluorobenzene 96%71-133%
* = Outside of Control Limits.
90 of 125
FC287955.2.2
Blank Spike Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-BS a 2B21543.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 292 117 61-152
71-43-2 Benzene 50 51.2 102 76-126
108-86-1 Bromobenzene 50 45.6 91 76-122
74-97-5 Bromochloromethane 50 50.8 102 77-120
75-27-4 Bromodichloromethane 50 55.6 111 74-130
75-25-2 Bromoform 50 52.6 105 76-127
78-93-3 2-Butanone (MEK)250 269 108 75-137
104-51-8 n-Butylbenzene 50 47.7 95 71-128
135-98-8 sec-Butylbenzene 50 47.4 95 79-135
98-06-6 tert-Butylbenzene 50 46.9 94 77-133
56-23-5 Carbon Tetrachloride 50 58.2 116 78-133
108-90-7 Chlorobenzene 50 50.3 101 81-129
75-00-3 Chloroethane 50 69.2 138*68-133
67-66-3 Chloroform 50 52.2 104 72-123
95-49-8 o-Chlorotoluene 50 46.8 94 77-129
106-43-4 p-Chlorotoluene 50 46.0 92 80-134
124-48-1 Dibromochloromethane 50 52.0 104 76-127
106-93-4 1,2-Dibromoethane 50 49.2 98 77-126
75-71-8 Dichlorodifluoromethane 50 77.9 156 68-168
95-50-1 1,2-Dichlorobenzene 50 45.8 92 80-129
541-73-1 1,3-Dichlorobenzene 50 46.2 92 81-129
106-46-7 1,4-Dichlorobenzene 50 48.0 96 76-130
75-34-3 1,1-Dichloroethane 50 52.9 106 73-125
107-06-2 1,2-Dichloroethane 50 51.1 102 74-128
75-35-4 1,1-Dichloroethylene 50 55.9 112 81-136
156-59-2 cis-1,2-Dichloroethylene 50 51.3 103 74-126
156-60-5 trans-1,2-Dichloroethylene 50 55.9 112 70-127
78-87-5 1,2-Dichloropropane 50 51.2 102 74-125
142-28-9 1,3-Dichloropropane 50 48.1 96 76-122
594-20-7 2,2-Dichloropropane 50 55.2 110 77-133
563-58-6 1,1-Dichloropropene 50 51.6 103 75-130
10061-01-5 cis-1,3-Dichloropropene 50 54.3 109 80-123
10061-02-6 trans-1,3-Dichloropropene 50 52.6 105 75-131
108-20-3 Di-Isopropyl Ether 50 54.2 108 75-122
64-17-5 Ethyl Alcohol 1000 1140 114 53-154
100-41-4 Ethylbenzene 50 51.1 102 77-123
* = Outside of Control Limits.
91 of 125
FC287955.2.3
Blank Spike Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-BS a 2B21543.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 262 105 72-133
98-82-8 Isopropylbenzene 50 50.0 100 80-136
99-87-6 p-Isopropyltoluene 50 47.7 95 77-131
74-83-9 Methyl Bromide 50 69.8 140*65-139
74-87-3 Methyl Chloride 50 64.2 128 71-144
75-09-2 Methylene Chloride 50 49.6 99 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 261 104 76-132
1634-04-4 Methyl Tert Butyl Ether 50 54.2 108 77-120
91-20-3 Naphthalene 50 46.1 92 79-129
103-65-1 n-Propylbenzene 50 46.8 94 80-135
100-42-5 Styrene 50 51.8 104 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 52.6 105 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 46.6 93 71-126
127-18-4 Tetrachloroethylene 50 49.4 99 79-130
108-88-3 Toluene 50 47.8 96 76-124
87-61-6 1,2,3-Trichlorobenzene 50 45.7 91 77-128
120-82-1 1,2,4-Trichlorobenzene 50 47.7 95 78-130
71-55-6 1,1,1-Trichloroethane 50 55.0 110 70-129
79-00-5 1,1,2-Trichloroethane 50 48.8 98 74-124
79-01-6 Trichloroethylene 50 51.1 102 75-128
75-69-4 Trichlorofluoromethane 50 63.9 128 73-145
96-18-4 1,2,3-Trichloropropane 50 45.1 90 74-127
95-63-6 1,2,4-Trimethylbenzene 50 48.4 97 74-123
108-67-8 1,3,5-Trimethylbenzene 50 47.3 95 73-122
108-05-4 Vinyl Acetate 250 297 119 48-164
75-01-4 Vinyl Chloride 50 65.1 130 76-141
m,p-Xylene 100 108 108 80-128
95-47-6 o-Xylene 50 49.8 100 80-132
1330-20-7 Xylene (total)150 158 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 105%75-124%
17060-07-0 1,2-Dichloroethane-D4 103%72-135%
2037-26-5 Toluene-D8 96%75-126%
* = Outside of Control Limits.
92 of 125
FC287955.2.3
Blank Spike Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B907-BS a 2B21543.D 1 03/01/23 AL n/a n/a V2B907
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-4, FC2879-5
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 90%71-133%
(a) No MS/MSD available for this run.
* = Outside of Control Limits.
93 of 125
FC287955.2.3
Blank Spike Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-BS 3C185557.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 274 110 61-152
71-43-2 Benzene 50 47.1 94 76-126
108-86-1 Bromobenzene 50 49.4 99 76-122
74-97-5 Bromochloromethane 50 51.2 102 77-120
75-27-4 Bromodichloromethane 50 52.0 104 74-130
75-25-2 Bromoform 50 51.7 103 76-127
78-93-3 2-Butanone (MEK)250 240 96 75-137
104-51-8 n-Butylbenzene 50 48.5 97 71-128
135-98-8 sec-Butylbenzene 50 49.0 98 79-135
98-06-6 tert-Butylbenzene 50 50.1 100 77-133
56-23-5 Carbon Tetrachloride 50 53.9 108 78-133
108-90-7 Chlorobenzene 50 51.2 102 81-129
75-00-3 Chloroethane 50 32.2 64* a 68-133
67-66-3 Chloroform 50 50.8 102 72-123
95-49-8 o-Chlorotoluene 50 48.5 97 77-129
106-43-4 p-Chlorotoluene 50 47.7 95 80-134
124-48-1 Dibromochloromethane 50 55.4 111 76-127
106-93-4 1,2-Dibromoethane 50 52.5 105 77-126
75-71-8 Dichlorodifluoromethane 50 45.8 92 68-168
95-50-1 1,2-Dichlorobenzene 50 50.2 100 80-129
541-73-1 1,3-Dichlorobenzene 50 50.2 100 81-129
106-46-7 1,4-Dichlorobenzene 50 49.0 98 76-130
75-34-3 1,1-Dichloroethane 50 48.4 97 73-125
107-06-2 1,2-Dichloroethane 50 52.0 104 74-128
75-35-4 1,1-Dichloroethylene 50 48.4 97 81-136
156-59-2 cis-1,2-Dichloroethylene 50 48.8 98 74-126
156-60-5 trans-1,2-Dichloroethylene 50 48.4 97 70-127
78-87-5 1,2-Dichloropropane 50 46.5 93 74-125
142-28-9 1,3-Dichloropropane 50 47.9 96 76-122
594-20-7 2,2-Dichloropropane 50 50.0 100 77-133
563-58-6 1,1-Dichloropropene 50 49.8 100 75-130
10061-01-5 cis-1,3-Dichloropropene 50 49.7 99 80-123
10061-02-6 trans-1,3-Dichloropropene 50 52.9 106 75-131
108-20-3 Di-Isopropyl Ether 50 48.5 97 75-122
64-17-5 Ethyl Alcohol 1000 985 99 53-154
100-41-4 Ethylbenzene 50 50.6 101 77-123
* = Outside of Control Limits.
94 of 125
FC287955.2.4
Blank Spike Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-BS 3C185557.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 250 100 72-133
98-82-8 Isopropylbenzene 50 51.9 104 80-136
99-87-6 p-Isopropyltoluene 50 48.4 97 77-131
74-83-9 Methyl Bromide 50 47.9 96 65-139
74-87-3 Methyl Chloride 50 45.4 91 71-144
75-09-2 Methylene Chloride 50 46.1 92 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 269 108 76-132
1634-04-4 Methyl Tert Butyl Ether 50 50.0 100 77-120
91-20-3 Naphthalene 50 52.1 104 79-129
103-65-1 n-Propylbenzene 50 48.0 96 80-135
100-42-5 Styrene 50 51.9 104 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 55.2 110 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 48.5 97 71-126
127-18-4 Tetrachloroethylene 50 53.3 107 79-130
108-88-3 Toluene 50 49.2 98 76-124
87-61-6 1,2,3-Trichlorobenzene 50 52.0 104 77-128
120-82-1 1,2,4-Trichlorobenzene 50 53.4 107 78-130
71-55-6 1,1,1-Trichloroethane 50 53.3 107 70-129
79-00-5 1,1,2-Trichloroethane 50 50.7 101 74-124
79-01-6 Trichloroethylene 50 50.3 101 75-128
75-69-4 Trichlorofluoromethane 50 50.9 102 73-145
96-18-4 1,2,3-Trichloropropane 50 49.0 98 74-127
95-63-6 1,2,4-Trimethylbenzene 50 48.6 97 74-123
108-67-8 1,3,5-Trimethylbenzene 50 48.6 97 73-122
108-05-4 Vinyl Acetate 250 321 128 48-164
75-01-4 Vinyl Chloride 50 44.3 89 76-141
m,p-Xylene 100 103 103 80-128
95-47-6 o-Xylene 50 51.6 103 80-132
1330-20-7 Xylene (total)150 155 103 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 101%75-126%
* = Outside of Control Limits.
95 of 125
FC287955.2.4
Blank Spike Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C943-BS 3C185557.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
(a) Sporadic marginal failure.
* = Outside of Control Limits.
96 of 125
FC287955.2.4
Blank Spike Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-BS 2B21603.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 286 114 61-152
71-43-2 Benzene 50 52.6 105 76-126
108-86-1 Bromobenzene 50 51.5 103 76-122
74-97-5 Bromochloromethane 50 53.5 107 77-120
75-27-4 Bromodichloromethane 50 56.4 113 74-130
75-25-2 Bromoform 50 53.7 107 76-127
78-93-3 2-Butanone (MEK)250 268 107 75-137
104-51-8 n-Butylbenzene 50 52.9 106 71-128
135-98-8 sec-Butylbenzene 50 52.3 105 79-135
98-06-6 tert-Butylbenzene 50 52.2 104 77-133
56-23-5 Carbon Tetrachloride 50 54.8 110 78-133
108-90-7 Chlorobenzene 50 52.3 105 81-129
75-00-3 Chloroethane 50 68.0 136*68-133
67-66-3 Chloroform 50 53.4 107 72-123
95-49-8 o-Chlorotoluene 50 52.7 105 77-129
106-43-4 p-Chlorotoluene 50 51.8 104 80-134
124-48-1 Dibromochloromethane 50 52.4 105 76-127
106-93-4 1,2-Dibromoethane 50 52.9 106 77-126
75-71-8 Dichlorodifluoromethane 50 75.9 152 68-168
95-50-1 1,2-Dichlorobenzene 50 51.5 103 80-129
541-73-1 1,3-Dichlorobenzene 50 51.6 103 81-129
106-46-7 1,4-Dichlorobenzene 50 52.6 105 76-130
75-34-3 1,1-Dichloroethane 50 53.2 106 73-125
107-06-2 1,2-Dichloroethane 50 54.2 108 74-128
75-35-4 1,1-Dichloroethylene 50 56.5 113 81-136
156-59-2 cis-1,2-Dichloroethylene 50 52.1 104 74-126
156-60-5 trans-1,2-Dichloroethylene 50 56.5 113 70-127
78-87-5 1,2-Dichloropropane 50 53.4 107 74-125
142-28-9 1,3-Dichloropropane 50 50.8 102 76-122
594-20-7 2,2-Dichloropropane 50 55.3 111 77-133
563-58-6 1,1-Dichloropropene 50 52.1 104 75-130
10061-01-5 cis-1,3-Dichloropropene 50 55.1 110 80-123
10061-02-6 trans-1,3-Dichloropropene 50 56.1 112 75-131
108-20-3 Di-Isopropyl Ether 50 54.7 109 75-122
64-17-5 Ethyl Alcohol 1000 1180 118 53-154
100-41-4 Ethylbenzene 50 52.8 106 77-123
* = Outside of Control Limits.
97 of 125
FC287955.2.5
Blank Spike Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-BS 2B21603.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 272 109 72-133
98-82-8 Isopropylbenzene 50 51.9 104 80-136
99-87-6 p-Isopropyltoluene 50 53.2 106 77-131
74-83-9 Methyl Bromide 50 66.8 134 65-139
74-87-3 Methyl Chloride 50 63.0 126 71-144
75-09-2 Methylene Chloride 50 51.1 102 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 270 108 76-132
1634-04-4 Methyl Tert Butyl Ether 50 55.2 110 77-120
91-20-3 Naphthalene 50 53.2 106 79-129
103-65-1 n-Propylbenzene 50 51.8 104 80-135
100-42-5 Styrene 50 52.3 105 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 55.1 110 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 53.0 106 71-126
127-18-4 Tetrachloroethylene 50 50.7 101 79-130
108-88-3 Toluene 50 50.1 100 76-124
87-61-6 1,2,3-Trichlorobenzene 50 52.5 105 77-128
120-82-1 1,2,4-Trichlorobenzene 50 53.1 106 78-130
71-55-6 1,1,1-Trichloroethane 50 53.8 108 70-129
79-00-5 1,1,2-Trichloroethane 50 51.5 103 74-124
79-01-6 Trichloroethylene 50 52.7 105 75-128
75-69-4 Trichlorofluoromethane 50 63.9 128 73-145
96-18-4 1,2,3-Trichloropropane 50 51.9 104 74-127
95-63-6 1,2,4-Trimethylbenzene 50 54.0 108 74-123
108-67-8 1,3,5-Trimethylbenzene 50 52.9 106 73-122
108-05-4 Vinyl Acetate 250 312 125 48-164
75-01-4 Vinyl Chloride 50 66.7 133 76-141
m,p-Xylene 100 107 107 80-128
95-47-6 o-Xylene 50 52.1 104 80-132
1330-20-7 Xylene (total)150 160 107 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
2037-26-5 Toluene-D8 95%75-126%
* = Outside of Control Limits.
98 of 125
FC287955.2.5
Blank Spike Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B909-BS 2B21603.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 96%71-133%
* = Outside of Control Limits.
99 of 125
FC287955.2.5
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C945-BS a 3C185614.D 1 03/04/23 AL n/a n/a V3C945
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
108-88-3 Toluene 50 54.0 108 76-124
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%72-135%
2037-26-5 Toluene-D8 101%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
(a) No MSD available for this run.
* = Outside of Control Limits.
100 of 125
FC287955.2.6
Matrix Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2958-14MS 3C185638.D 1 03/04/23 AL n/a n/a V3C945
FC2958-14 a 3C185621.D 1 03/04/23 AL n/a n/a V3C945
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7
FC2958-14 Spike MS MS
CAS No.Compound ug/kg Q ug/kg ug/kg %Limits
108-88-3 Toluene ND 48.3 49.6 103 76-124
CAS No.Surrogate Recoveries MS FC2958-14 Limits
1868-53-7 Dibromofluoromethane 99%99%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%112%72-135%
2037-26-5 Toluene-D8 103%101%75-126%
460-00-4 4-Bromofluorobenzene 97%94%71-133%
(a) Confirmation run.
* = Outside of Control Limits.
101 of 125
FC287955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2909-1MS 3C185468.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1MSD 3C185469.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1 3C185454.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
FC2909-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 290 247 85 274 209 76 17 61-152/27
71-43-2 Benzene ND 57.9 47.1 81 54.9 40.9 75*14 76-126/26
108-86-1 Bromobenzene ND 57.9 37.2 64*54.9 30.6 56*19 76-122/32
74-97-5 Bromochloromethane ND 57.9 49.8 86 54.9 43.7 80 13 77-120/24
75-27-4 Bromodichloromethane ND 57.9 43.0 74 54.9 37.8 69*13 74-130/25
75-25-2 Bromoform ND 57.9 37.4 65*54.9 33.6 61*11 76-127/26
78-93-3 2-Butanone (MEK)ND 290 228 79 274 197 72*15 75-137/25
104-51-8 n-Butylbenzene ND 57.9 28.2 49*54.9 23.0 42*20 71-128/35
135-98-8 sec-Butylbenzene ND 57.9 31.9 55*54.9 26.6 48*18 79-135/34
98-06-6 tert-Butylbenzene ND 57.9 36.5 63*54.9 30.6 56*18 77-133/34
56-23-5 Carbon Tetrachloride ND 57.9 45.7 79 54.9 40.3 73*13 78-133/29
108-90-7 Chlorobenzene ND 57.9 41.5 72*54.9 35.2 64*16 81-129/29
75-00-3 Chloroethane ND 57.9 35.2 61*54.9 34.2 62*3 68-133/29
67-66-3 Chloroform ND 57.9 48.6 84 54.9 43.2 79 12 72-123/26
95-49-8 o-Chlorotoluene ND 57.9 34.3 59*54.9 28.4 52*19 77-129/33
106-43-4 p-Chlorotoluene ND 57.9 31.0 54*54.9 25.5 46*19 80-134/33
124-48-1 Dibromochloromethane ND 57.9 47.1 81 54.9 39.8 73*17 76-127/27
106-93-4 1,2-Dibromoethane ND 57.9 48.3 83 54.9 42.2 77 13 77-126/26
75-71-8 Dichlorodifluoromethane ND 57.9 81.8 141 54.9 71.6 130 13 68-168/29
95-50-1 1,2-Dichlorobenzene ND 57.9 28.6 49*54.9 23.2 42*21 80-129/32
541-73-1 1,3-Dichlorobenzene ND 57.9 27.7 48*54.9 22.8 42*19 81-129/33
106-46-7 1,4-Dichlorobenzene ND 57.9 27.9 48*54.9 22.9 42*20 76-130/32
75-34-3 1,1-Dichloroethane ND 57.9 47.6 82 54.9 42.2 77 12 73-125/27
107-06-2 1,2-Dichloroethane ND 57.9 48.2 83 54.9 42.2 77 13 74-128/23
75-35-4 1,1-Dichloroethylene ND 57.9 48.8 84 54.9 43.1 79*12 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 57.9 46.9 81 54.9 41.3 75 13 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 57.9 47.7 82 54.9 41.4 75 14 70-127/27
78-87-5 1,2-Dichloropropane ND 57.9 49.4 85 54.9 42.7 78 15 74-125/25
142-28-9 1,3-Dichloropropane ND 57.9 52.5 91 54.9 45.1 82 15 76-122/26
594-20-7 2,2-Dichloropropane ND 57.9 51.9 90 54.9 45.5 83 13 77-133/28
563-58-6 1,1-Dichloropropene ND 57.9 45.8 79 54.9 39.8 73*14 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 57.9 43.1 74*54.9 37.5 68*14 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 57.9 41.8 72*54.9 35.7 65*16 75-131/28
108-20-3 Di-Isopropyl Ether ND 57.9 48.8 84 54.9 42.8 78 13 75-122/25
64-17-5 Ethyl Alcohol ND 1160 1330 115 1100 1220 111 9 53-154/42
100-41-4 Ethylbenzene ND 57.9 43.2 75*54.9 36.9 67*16 77-123/31
* = Outside of Control Limits.
102 of 125
FC287955.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2909-1MS 3C185468.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1MSD 3C185469.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1 3C185454.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
FC2909-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 290 219 76 274 184 67*17 72-133/26
98-82-8 Isopropylbenzene ND 57.9 42.0 73*54.9 35.0 64*18 80-136/32
99-87-6 p-Isopropyltoluene ND 57.9 31.4 54*54.9 25.8 47*20 77-131/34
74-83-9 Methyl Bromide ND 57.9 60.0 104 54.9 48.3 88 22 65-139/31
74-87-3 Methyl Chloride ND 57.9 56.1 97 54.9 51.2 93 9 71-144/27
75-09-2 Methylene Chloride ND 57.9 77.0 133 54.9 69.6 127 10 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 290 259 89 274 224 82 14 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 57.9 54.2 94 54.9 47.9 87 12 77-120/24
91-20-3 Naphthalene ND 57.9 21.3 37*54.9 17.3 32*21 79-129/33
103-65-1 n-Propylbenzene ND 57.9 35.0 60*54.9 29.0 53*19 80-135/33
100-42-5 Styrene ND 57.9 38.2 66*54.9 31.4 57*20 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 57.9 48.0 83 54.9 40.6 74*17 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 57.9 43.1 74 54.9 37.0 67*15 71-126/30
127-18-4 Tetrachloroethylene ND 57.9 44.4 77*54.9 37.4 68*17 79-130/31
108-88-3 Toluene ND 57.9 46.4 80 54.9 39.7 72*16 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 57.9 19.4 33*54.9 15.6 28*22 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 57.9 19.2 33*54.9 14.8 27*26 78-130/34
71-55-6 1,1,1-Trichloroethane ND 57.9 49.9 86 54.9 42.7 78 16 70-129/27
79-00-5 1,1,2-Trichloroethane ND 57.9 49.6 86 54.9 43.9 80 12 74-124/28
79-01-6 Trichloroethylene ND 57.9 44.8 77 54.9 38.1 69*16 75-128/27
75-69-4 Trichlorofluoromethane ND 57.9 51.2 88 54.9 45.7 83 11 73-145/31
96-18-4 1,2,3-Trichloropropane ND 57.9 47.0 81 54.9 40.4 74 15 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 57.9 34.4 59*54.9 28.5 52*19 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 57.9 36.7 63*54.9 30.2 55*19 73-122/33
108-05-4 Vinyl Acetate ND 290 ND 0*274 ND 0*nc 48-164/37
75-01-4 Vinyl Chloride ND 57.9 55.6 96 54.9 50.4 92 10 76-141/27
m,p-Xylene ND 116 85.7 74*110 72.0 66*17 80-128/30
95-47-6 o-Xylene ND 57.9 42.7 74*54.9 35.4 65*19 80-132/30
1330-20-7 Xylene (total)ND 174 128 74*165 107 65*18 80-129/30
CAS No.Surrogate Recoveries MS MSD FC2909-1 Limits
1868-53-7 Dibromofluoromethane 96%98%96%75-124%
17060-07-0 1,2-Dichloroethane-D4 100%100%109%72-135%
2037-26-5 Toluene-D8 103%103%104%75-126%
* = Outside of Control Limits.
103 of 125
FC287955.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2909-1MS 3C185468.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1MSD 3C185469.D 1 02/24/23 AL n/a n/a V3C939
FC2909-1 3C185454.D 1 02/24/23 AL n/a n/a V3C939
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-2, FC2879-3
CAS No.Surrogate Recoveries MS MSD FC2909-1 Limits
460-00-4 4-Bromofluorobenzene 98%98%98%71-133%
* = Outside of Control Limits.
104 of 125
FC287955.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2913-10MS 3C185524.D 1 03/01/23 DB n/a n/a V3C941
FC2913-10MSD 3C185525.D 1 03/01/23 DB n/a n/a V3C941
FC2913-10 3C185508.D 1 02/28/23 DB n/a n/a V3C941
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1
FC2913-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
CAS No.Surrogate Recoveries MS MSD FC2913-10 Limits
1868-53-7 Dibromofluoromethane 103%102%102%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%108%112%72-135%
2037-26-5 Toluene-D8 103%102%103%75-126%
460-00-4 4-Bromofluorobenzene 97%96%95%71-133%
* = Outside of Control Limits.
105 of 125
FC287955.4.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3064-2MS 3C185579.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2MSD 3C185580.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2 3C185561.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
FC3064-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 140 U 256 257 100 259 259 100 1 61-152/27
71-43-2 Benzene 3.5 U 51.3 43.4 85 51.8 48.1 93 10 76-126/26
108-86-1 Bromobenzene 3.5 U 51.3 40.6 79 51.8 45.7 88 12 76-122/32
74-97-5 Bromochloromethane 3.5 U 51.3 48.0 94 51.8 52.3 101 9 77-120/24
75-27-4 Bromodichloromethane 3.5 U 51.3 45.7 89 51.8 50.6 98 10 74-130/25
75-25-2 Bromoform 3.5 U 51.3 42.0 82 51.8 47.6 92 13 76-127/26
78-93-3 2-Butanone (MEK)18 U 256 226 88 259 237 92 5 75-137/25
104-51-8 n-Butylbenzene 3.5 U 51.3 34.0 66*51.8 37.5 72 10 71-128/35
135-98-8 sec-Butylbenzene 3.5 U 51.3 36.2 71*51.8 40.3 78*11 79-135/34
98-06-6 tert-Butylbenzene 3.5 U 51.3 37.9 74*51.8 42.3 82 11 77-133/34
56-23-5 Carbon Tetrachloride 3.5 U 51.3 45.7 89 51.8 51.9 100 13 78-133/29
108-90-7 Chlorobenzene 3.5 U 51.3 44.7 87 51.8 49.5 96 10 81-129/29
75-00-3 Chloroethane 3.5 U 51.3 35.4 69 51.8 35.1 68 1 68-133/29
67-66-3 Chloroform 3.5 U 51.3 47.1 92 51.8 51.2 99 8 72-123/26
95-49-8 o-Chlorotoluene 3.5 U 51.3 38.6 75*51.8 42.5 82 10 77-129/33
106-43-4 p-Chlorotoluene 3.5 U 51.3 38.1 74*51.8 41.5 80 9 80-134/33
124-48-1 Dibromochloromethane 3.5 U 51.3 47.1 92 51.8 52.8 102 11 76-127/27
106-93-4 1,2-Dibromoethane 3.5 U 51.3 48.1 94 51.8 51.7 100 7 77-126/26
75-71-8 Dichlorodifluoromethane 3.5 U 51.3 39.4 77 51.8 44.6 86 12 68-168/29
95-50-1 1,2-Dichlorobenzene 3.5 U 51.3 37.2 73*51.8 40.7 79*9 80-129/32
541-73-1 1,3-Dichlorobenzene 3.5 U 51.3 37.1 72*51.8 41.4 80*11 81-129/33
106-46-7 1,4-Dichlorobenzene 3.5 U 51.3 37.7 74*51.8 40.8 79 8 76-130/32
75-34-3 1,1-Dichloroethane 3.5 U 51.3 44.7 87 51.8 49.6 96 10 73-125/27
107-06-2 1,2-Dichloroethane 3.5 U 51.3 48.1 94 51.8 51.9 100 8 74-128/23
75-35-4 1,1-Dichloroethylene 3.5 U 51.3 43.2 84 51.8 48.4 94 11 81-136/28
156-59-2 cis-1,2-Dichloroethylene 3.5 U 51.3 45.1 88 51.8 49.4 95 9 74-126/26
156-60-5 trans-1,2-Dichloroethylene 3.5 U 51.3 44.3 86 51.8 48.2 93 8 70-127/27
78-87-5 1,2-Dichloropropane 3.5 U 51.3 43.6 85 51.8 48.0 93 10 74-125/25
142-28-9 1,3-Dichloropropane 3.5 U 51.3 43.5 85 51.8 48.2 93 10 76-122/26
594-20-7 2,2-Dichloropropane 3.5 U 51.3 41.9 82 51.8 47.3 91 12 77-133/28
563-58-6 1,1-Dichloropropene 3.5 U 51.3 44.3 86 51.8 48.9 94 10 75-130/28
10061-01-5 cis-1,3-Dichloropropene 3.5 U 51.3 44.7 87 51.8 49.3 95 10 80-123/26
10061-02-6 trans-1,3-Dichloropropene 3.5 U 51.3 46.3 90 51.8 51.5 100 11 75-131/28
108-20-3 Di-Isopropyl Ether 3.5 U 51.3 44.2 86 51.8 49.4 95 11 75-122/25
64-17-5 Ethyl Alcohol 280 U 1030 1160 113 1040 1240 120 7 53-154/42
100-41-4 Ethylbenzene 3.5 U 51.3 43.9 86 51.8 48.7 94 10 77-123/31
* = Outside of Control Limits.
106 of 125
FC287955.4.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3064-2MS 3C185579.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2MSD 3C185580.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2 3C185561.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
FC3064-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 18 U 256 224 87 259 244 94 9 72-133/26
98-82-8 Isopropylbenzene 3.5 U 51.3 42.3 83 51.8 46.6 90 10 80-136/32
99-87-6 p-Isopropyltoluene 3.5 U 51.3 35.8 70*51.8 39.4 76*10 77-131/34
74-83-9 Methyl Bromide 3.5 U 51.3 46.5 91 51.8 52.2 101 12 65-139/31
74-87-3 Methyl Chloride 3.5 U 51.3 41.4 81 51.8 44.8 87 8 71-144/27
75-09-2 Methylene Chloride 14 U 51.3 49.8 97 51.8 52.5 101 5 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)18 U 256 251 98 259 270 104 7 76-132/26
1634-04-4 Methyl Tert Butyl Ether 3.5 U 51.3 45.1 88 51.8 51.1 99 12 77-120/24
91-20-3 Naphthalene 3.5 U 51.3 34.4 67*51.8 37.6 73*9 79-129/33
103-65-1 n-Propylbenzene 3.5 U 51.3 37.8 74*51.8 42.1 81 11 80-135/33
100-42-5 Styrene 3.5 U 51.3 43.7 85 51.8 48.4 94 10 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane 3.5 U 51.3 47.3 92 51.8 52.6 102 11 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane 3.5 U 51.3 42.9 84 51.8 47.3 91 10 71-126/30
127-18-4 Tetrachloroethylene 3.5 U 51.3 46.7 91 51.8 50.3 97 7 79-130/31
108-88-3 Toluene 14 U 51.3 44.1 86 51.8 49.3 95 11 76-124/30
87-61-6 1,2,3-Trichlorobenzene 3.5 U 51.3 30.6 60*51.8 32.7 63*7 77-128/35
120-82-1 1,2,4-Trichlorobenzene 3.5 U 51.3 31.8 62*51.8 34.5 67*8 78-130/34
71-55-6 1,1,1-Trichloroethane 3.5 U 51.3 46.7 91 51.8 52.3 101 11 70-129/27
79-00-5 1,1,2-Trichloroethane 3.5 U 51.3 47.4 92 51.8 51.9 100 9 74-124/28
79-01-6 Trichloroethylene 3.5 U 51.3 45.9 90 51.8 49.8 96 8 75-128/27
75-69-4 Trichlorofluoromethane 3.5 U 51.3 46.1 90 51.8 50.5 98 9 73-145/31
96-18-4 1,2,3-Trichloropropane 3.5 U 51.3 43.5 85 51.8 48.6 94 11 74-127/27
95-63-6 1,2,4-Trimethylbenzene 3.5 U 51.3 37.6 73*51.8 41.7 81 10 74-123/34
108-67-8 1,3,5-Trimethylbenzene 3.5 U 51.3 38.1 74 51.8 42.2 82 10 73-122/33
108-05-4 Vinyl Acetate 18 U 256 ND 0*259 ND 0*nc 48-164/37
75-01-4 Vinyl Chloride 3.5 U 51.3 41.8 82 51.8 46.5 90 11 76-141/27
m,p-Xylene 7.0 U 103 88.5 86 104 96.4 93 9 80-128/30
95-47-6 o-Xylene 3.5 U 51.3 43.0 84 51.8 48.6 94 12 80-132/30
1330-20-7 Xylene (total)11 U 154 132 86 155 145 93 9 80-129/30
CAS No.Surrogate Recoveries MS MSD FC3064-2 Limits
1868-53-7 Dibromofluoromethane 101%100%98%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%105%111%72-135%
2037-26-5 Toluene-D8 103%102%103%75-126%
* = Outside of Control Limits.
107 of 125
FC287955.4.3
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC3064-2MS 3C185579.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2MSD 3C185580.D 1 03/02/23 AL n/a n/a V3C943
FC3064-2 3C185561.D 1 03/02/23 AL n/a n/a V3C943
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-1, FC2879-6, FC2879-7, FC2879-10, FC2879-11
CAS No.Surrogate Recoveries MS MSD FC3064-2 Limits
460-00-4 4-Bromofluorobenzene 98%97%98%71-133%
* = Outside of Control Limits.
108 of 125
FC287955.4.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2964-2MS 2B21627.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2MSD 2B21628.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2 2B21615.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
FC2964-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 276 216 78 284 216 76 0 61-152/27
71-43-2 Benzene ND 55.2 54.7 99 56.9 59.2 104 8 76-126/26
108-86-1 Bromobenzene ND 55.2 51.8 94 56.9 55.4 97 7 76-122/32
74-97-5 Bromochloromethane ND 55.2 53.5 97 56.9 56.6 99 6 77-120/24
75-27-4 Bromodichloromethane ND 55.2 53.9 98 56.9 60.6 107 12 74-130/25
75-25-2 Bromoform ND 55.2 41.5 75*56.9 45.8 80 10 76-127/26
78-93-3 2-Butanone (MEK)ND 276 188 68*284 193 68*3 75-137/25
104-51-8 n-Butylbenzene ND 55.2 48.1 87 56.9 53.7 94 11 71-128/35
135-98-8 sec-Butylbenzene ND 55.2 53.0 96 56.9 59.4 104 11 79-135/34
98-06-6 tert-Butylbenzene ND 55.2 55.2 100 56.9 60.5 106 9 77-133/34
56-23-5 Carbon Tetrachloride ND 55.2 57.2 104 56.9 61.4 108 7 78-133/29
108-90-7 Chlorobenzene ND 55.2 52.8 96 56.9 57.3 101 8 81-129/29
75-00-3 Chloroethane ND 55.2 73.8 134*56.9 78.1 137*6 68-133/29
67-66-3 Chloroform ND 55.2 57.1 103 56.9 61.0 107 7 72-123/26
95-49-8 o-Chlorotoluene ND 55.2 53.5 97 56.9 58.6 103 9 77-129/33
106-43-4 p-Chlorotoluene ND 55.2 51.8 94 56.9 57.1 100 10 80-134/33
124-48-1 Dibromochloromethane ND 55.2 48.6 88 56.9 53.2 93 9 76-127/27
106-93-4 1,2-Dibromoethane ND 55.2 46.8 85 56.9 51.0 90 9 77-126/26
75-71-8 Dichlorodifluoromethane ND 55.2 67.6 122 56.9 75.3 132 11 68-168/29
95-50-1 1,2-Dichlorobenzene ND 55.2 47.4 86 56.9 52.1 92 9 80-129/32
541-73-1 1,3-Dichlorobenzene ND 55.2 49.1 89 56.9 53.9 95 9 81-129/33
106-46-7 1,4-Dichlorobenzene ND 55.2 48.6 88 56.9 54.4 96 11 76-130/32
75-34-3 1,1-Dichloroethane ND 55.2 58.5 106 56.9 60.5 106 3 73-125/27
107-06-2 1,2-Dichloroethane ND 55.2 52.7 95 56.9 56.7 100 7 74-128/23
75-35-4 1,1-Dichloroethylene ND 55.2 59.4 108 56.9 63.5 112 7 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 55.2 54.6 99 56.9 59.0 104 8 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 55.2 59.4 108 56.9 63.5 112 7 70-127/27
78-87-5 1,2-Dichloropropane ND 55.2 54.3 98 56.9 59.4 104 9 74-125/25
142-28-9 1,3-Dichloropropane ND 55.2 48.9 89 56.9 52.7 93 7 76-122/26
594-20-7 2,2-Dichloropropane ND 55.2 56.1 102 56.9 59.5 105 6 77-133/28
563-58-6 1,1-Dichloropropene ND 55.2 55.8 101 56.9 58.8 103 5 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 55.2 52.6 95 56.9 58.7 103 11 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 55.2 51.2 93 56.9 56.8 100 10 75-131/28
108-20-3 Di-Isopropyl Ether ND 55.2 59.6 108 56.9 61.2 108 3 75-122/25
64-17-5 Ethyl Alcohol ND 1100 723 65 1140 792 70 9 53-154/42
100-41-4 Ethylbenzene ND 55.2 54.6 99 56.9 59.5 105 9 77-123/31
* = Outside of Control Limits.
109 of 125
FC287955.4.4
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2964-2MS 2B21627.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2MSD 2B21628.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2 2B21615.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
FC2964-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 276 177 64*284 188 66*6 72-133/26
98-82-8 Isopropylbenzene ND 55.2 52.3 95 56.9 58.1 102 11 80-136/32
99-87-6 p-Isopropyltoluene ND 55.2 52.8 96 56.9 58.6 103 10 77-131/34
74-83-9 Methyl Bromide ND 55.2 65.7 119 56.9 73.6 129 11 65-139/31
74-87-3 Methyl Chloride ND 55.2 66.2 120 56.9 71.4 125 8 71-144/27
75-09-2 Methylene Chloride ND 55.2 62.1 112 56.9 64.3 113 3 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 276 194 70*284 204 72*5 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 55.2 53.3 96 56.9 53.8 95 1 77-120/24
91-20-3 Naphthalene ND 55.2 33.3 60*56.9 36.4 64*9 79-129/33
103-65-1 n-Propylbenzene ND 55.2 54.1 98 56.9 59.4 104 9 80-135/33
100-42-5 Styrene ND 55.2 50.4 91 56.9 55.5 98 10 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 55.2 54.1 98 56.9 60.3 106 11 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 55.2 44.1 80 56.9 48.1 85 9 71-126/30
127-18-4 Tetrachloroethylene ND 55.2 52.8 96 56.9 57.3 101 8 79-130/31
108-88-3 Toluene ND 55.2 53.7 97 56.9 58.2 102 8 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 55.2 37.6 68*56.9 43.0 76*13 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 55.2 40.3 73*56.9 45.2 79 11 78-130/34
71-55-6 1,1,1-Trichloroethane ND 55.2 58.7 106 56.9 60.8 107 4 70-129/27
79-00-5 1,1,2-Trichloroethane ND 55.2 48.6 88 56.9 52.6 92 8 74-124/28
79-01-6 Trichloroethylene ND 55.2 54.3 98 56.9 59.7 105 9 75-128/27
75-69-4 Trichlorofluoromethane ND 55.2 66.6 121 56.9 69.1 121 4 73-145/31
96-18-4 1,2,3-Trichloropropane ND 55.2 41.8 76 56.9 44.9 79 7 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 55.2 55.1 100 56.9 60.3 106 9 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 55.2 54.3 98 56.9 60.3 106 10 73-122/33
108-05-4 Vinyl Acetate ND 276 55.6 20*284 41.8 15*28 48-164/37
75-01-4 Vinyl Chloride ND 55.2 66.8 121 56.9 70.3 124 5 76-141/27
m,p-Xylene ND 110 111 100 114 120 105 8 80-128/30
95-47-6 o-Xylene ND 55.2 53.7 97 56.9 58.9 104 9 80-132/30
1330-20-7 Xylene (total)ND 166 165 100 171 179 105 8 80-129/30
CAS No.Surrogate Recoveries MS MSD FC2964-2 Limits
1868-53-7 Dibromofluoromethane 103%98%94%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%95%103%72-135%
2037-26-5 Toluene-D8 100%101%111%75-126%
* = Outside of Control Limits.
110 of 125
FC287955.4.4
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2964-2MS 2B21627.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2MSD 2B21628.D 1 03/03/23 AL n/a n/a V2B909
FC2964-2 2B21615.D 1 03/03/23 AL n/a n/a V2B909
The QC reported here applies to the following samples:Method: SW846 8260D
FC2879-7, FC2879-8, FC2879-9, FC2879-12
CAS No.Surrogate Recoveries MS MSD FC2964-2 Limits
460-00-4 4-Bromofluorobenzene 99%98%111%71-133%
* = Outside of Control Limits.
111 of 125
FC287955.4.4
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
112 of 125
FC28796
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U617-MB 1U14135.D 1 02/27/23 JR n/a n/a G1U617
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-8, FC2879-9, FC2879-10, FC2879-11
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.0 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 106%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
113 of 125
FC287966.1.1
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U618-MB 1U14168.D 1 02/28/23 JR n/a n/a G1U618
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-12
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.0 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 117%56-149%
98-08-8 aaa-Trifluorotoluene 95%66-132%
114 of 125
FC287966.1.2
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U619-MB 1U14203.D 1 03/01/23 JR n/a n/a G1U619
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-6, FC2879-7
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.0 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 128%56-149%
98-08-8 aaa-Trifluorotoluene 89%66-132%
115 of 125
FC287966.1.3
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U617-BS 1U14134.D 1 02/27/23 JR n/a n/a G1U617
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-8, FC2879-9, FC2879-10, FC2879-11
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 17.7 89 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 106%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
* = Outside of Control Limits.
116 of 125
FC287966.2.1
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U618-BS 1U14167.D 1 02/28/23 JR n/a n/a G1U618
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-12
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 17.8 89 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 118%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
* = Outside of Control Limits.
117 of 125
FC287966.2.2
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U619-BS 1U14202.D 1 03/01/23 JR n/a n/a G1U619
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-6, FC2879-7
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 17.4 87 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 129%56-149%
98-08-8 aaa-Trifluorotoluene 90%66-132%
* = Outside of Control Limits.
118 of 125
FC287966.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2879-2MS 1U14139.D 1 02/27/23 JR n/a n/a G1U617
FC2879-2MSD 1U14140.D 1 02/27/23 JR n/a n/a G1U617
FC2879-2 1U14137.D 1 02/27/23 JR n/a n/a G1U617
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-8, FC2879-9, FC2879-10, FC2879-11
FC2879-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 18.5 17.6 95 18.5 16.7 90 5 74-128/17
CAS No.Surrogate Recoveries MS MSD FC2879-2 Limits
460-00-4 4-Bromofluorobenzene 106%109%103%56-149%
98-08-8 aaa-Trifluorotoluene 96%99%94%66-132%
* = Outside of Control Limits.
119 of 125
FC287966.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2879-12MS 1U14170.D 1 02/28/23 JR n/a n/a G1U618
FC2879-12MSD 1U14171.D 1 02/28/23 JR n/a n/a G1U618
FC2879-12 1U14169.D 1 02/28/23 JR n/a n/a G1U618
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-12
FC2879-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 22.2 20.9 94 22.2 20.0 90 4 74-128/17
CAS No.Surrogate Recoveries MS MSD FC2879-12 Limits
460-00-4 4-Bromofluorobenzene 120%120%111%56-149%
98-08-8 aaa-Trifluorotoluene 94%92%89%66-132%
* = Outside of Control Limits.
120 of 125
FC287966.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2964-1MS 1U14205.D 1 03/01/23 JR n/a n/a G1U619
FC2964-1MSD 1U14206.D 1 03/01/23 JR n/a n/a G1U619
FC2964-1 1U14204.D 1 03/01/23 JR n/a n/a G1U619
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-6, FC2879-7
FC2964-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 25.3 22.3 88 25.3 23.4 93 5 74-128/17
CAS No.Surrogate Recoveries MS MSD FC2964-1 Limits
460-00-4 4-Bromofluorobenzene 123%128%121%56-149%
98-08-8 aaa-Trifluorotoluene 85%87%84%66-132%
* = Outside of Control Limits.
121 of 125
FC287966.3.3
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
122 of 125
FC28797
Method Blank Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95605-MB WW37923.D 1 02/24/23 EG 02/24/23 OP95605 GWW1484
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-6, FC2879-7, FC2879-8, FC2879-9, FC2879-10,
FC2879-11, FC2879-12
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 5.0 2.5 mg/kg
CAS No.Surrogate Recoveries Limits
84-15-1 o-Terphenyl 66%56-122%
123 of 125
FC287977.1.1
Blank Spike Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95605-BS WW37924.D 1 02/24/23 EG 02/24/23 OP95605 GWW1484
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-6, FC2879-7, FC2879-8, FC2879-9, FC2879-10,
FC2879-11, FC2879-12
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH (C10-C28)50 44.1 88 62-116
CAS No.Surrogate Recoveries BSP Limits
84-15-1 o-Terphenyl 77%56-122%
* = Outside of Control Limits.
124 of 125
FC287977.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2879
Account:MURPHY Murphy Oil USA
Project:GESSCC: Murphy USA 8549; 4993 NC-42, Garner, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95605-MS WW37946.D 1 02/25/23 EG 02/24/23 OP95605 GWW1484
OP95605-MSD WW37962.D 1 02/27/23 EG 02/24/23 OP95605 GWW1485
FC2879-1 WW37926.D 1 02/24/23 EG 02/24/23 OP95605 GWW1484
The QC reported here applies to the following samples:Method: SW846 8015C
FC2879-1, FC2879-2, FC2879-3, FC2879-4, FC2879-5, FC2879-6, FC2879-7, FC2879-8, FC2879-9, FC2879-10,
FC2879-11, FC2879-12
FC2879-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH (C10-C28)32.3 57.6 88.1 97 58.1 85.1 91 3 62-116/35
CAS No.Surrogate Recoveries MS MSD FC2879-1 Limits
84-15-1 o-Terphenyl 86%81%69%56-122%
* = Outside of Control Limits.
125 of 125
FC287977.3.1
20-Day Report
Murphy USA #8549
4993 NC Highway 42 West
Garner, NC 27529

Appendix D – 24-hr Release Reporting Form

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________
Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)
 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse
 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse
 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other
 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics
 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1.Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
N
NYY
N Reg
NA
3/7/2023
Commercial
Murphy USA #8549
37042
4993 NC 42 Highway West
Garner
Johnston
X
35.6112 78.5537
27529
GES conducted a site check during the week of February 20th. Lab results indicate the presence of petroleum impact.
X Soil Contamination
X
X
X
X
X

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3.
UST SYSTEM OWNER UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined
1
Aaron Williamson
From:Price, Liz <[e-mail]>
Sent:Thursday, March 9, 2023 2:42 PM
To:Daniel Dabkowski
Cc:Thomas D. Chmura; Aaron Williamson; Price, Liz
Subject:RE: [External] Murphy USA 8549 Garner, NC, UST Incident #48901
Follow Up Flag:Follow up
Flag Status:Flagged
CAUTION: This email originated from outside your organization. Exercise caution when opening attachments or clicking
links, especially from unknown senders.
Incident #48901 has been assigned to this site. Please use this incident # on future reports and correspondence for this
site.

Thank you

Liz Price
Hydrogeologist / Wilmington Regional Office
Division of Waste Management, UST Section
North Carolina Department of Environmental Quality
Office: [phone]
[e-mail]

Wilmington Regional Office Fayetteville Regional Office

DWM Site Locator DWM UST Section Website DWM Laserfiche Public Search DWM UST Permitting and
Inspection

For spills or other environmental emergencies after hours:
NC DEQ DWM Duty Phone [phone]
NC State Emergency Management 1-800-858-0368
National Response Center 1-800-424-8802

2
From: Daniel Dabkowski <[e-mail]>
Sent: Thursday, March 9, 2023 7:04 AM
To: Price, Liz <[e-mail]>
Cc: Thomas D. Chmura <[e-mail]>; Aaron Williamson <[e-mail]>
Subject: [External] Murphy USA 8549 Garner, NC UST #61 Form

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good morning Liz,

Please find attached the UST #61 form for Murphy USA #8549 located in Garner. This is being filed based on the
attached laboratory analytical data from the site check conducted the week of February 20th. If you have any questions,
please let me know.

Daniel Dabkowski
Senior Project Manager

Office: 866.765.4851 ext. 4523
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
104 Corporate Boulevard, Suite 411
West Columbia, SC 29169

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

Confidentiality Notice: This transmission (including any attachments) may contain confidential information belonging to
Groundwater & Environmental Services, Inc. and is intended only for the use of the party or entity to which it is
addressed. If you are not the intended recipient, you are hereby notified that any disclosure, copying, distribution,
retention or the taking of action in reliance on the contents of this transmission is strictly prohibited; provided, however,
the prohibition against disclosure shall not apply if the transmission is required by law to be disclosed by a governmental
intended party as a public record. If you have received this transmission in error, please immediately notify the sender
and erase all information and attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding
back to, clicking on any links or opening any attachments. If it appears suspicious delete it immediately.