FA-28951_48153_CA_LSA_20220615

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
June 20, 2022

Ms. Sarah Brown
NCDEQ-UST Section
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, NC 28301-5043

Re: Phase I Limited Site Assessment Report
Han-Dee Hugo #97
305 Pritchard Road
Clayton, Johnston County
North Carolina
Facility ID Number: 00-0-0000037345
Incident Number: 48153
GRI Project Number: 5816

Dear Ms. Brown,

Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact Rae Brown at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Howell Clark; Sampson Bladen Oil, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Phase I Limited Site Assessment Report
Han-Dee Hugo #97
305 Pritchard Road
Clayton, Johnston County
North Carolina
Facility ID Number: 00-0-00000037345
Incident Number: 48153
GRI Project Number: 5816

Prepared for:

Howell Clark
Sampson-Bladen Oil Company, Inc.
Post Office Box 469
Clinton, North Carolina 28328

June 15, 2022

Rae Troiano Brown, P.G.
Project Manager
AJ Discepolo, GIT
Staff Scientist

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
ii
EXECUTIVE SUMMARY
The Han-Dee Hugo #97 site is located at 305 Pritchard Road in Clayton, Johnston County, North Carolina.
The property operates as a petroleum retail facility and convenience store. The site is covered by concrete
and asphalt. One 15,000-gallon gasoline UST, one 8,000-gallon gasoline UST, and one 8,000-gallon diesel
UST are located at the site with four associated gasoline and two gasoline/diesel dispenser islands.

On October 21, 2021, during a site assessment for property refinancing, a release was confirmed following
the receipt of soil laboratory results. Concentrations of benzo(a)anthracene and benzopyrene that
exceeded soil-to-water MCCs were reported. Based on the soil results, NCDEQ required additional
assessment.

In April 2022, a receptor survey was conducted. The surrounding properties are commercial, residential,
highway business, office institutional, mixed use, and public/institutional. No private wells are located
within 1,000 feet of the site. Public water is available to the subject site and to all surrounding properties.
No surface water bodies were identified within a 500-foot radius of the site.

On April 19, 2022, one monitoring well (MW-1) was installed in the former location of TMW-5-20’, the
location of soil contamination identified during previous environmental assessment activities conducted
in September 2021. Soil samples were collected at 10-foot intervals during the installation of monitoring
well MW-1. No reported concentrations exceeded the soil-to-water MCCs.

Please note that on April 19 and 25, 2022, no ground water was measured in MW-1; therefore, no ground
water samples were collected.

Based on the lack of receptors, the site should be classified as low risk. Contaminant concentrations
reported in TMW-5-20’ exceeded the soil-to-water MCC; therefore, public notice should be completed
and no further action should be required. An NRP is not required as none of the estimated concentrations
exceeded the residential SCLs.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
iii
SITE INFORMATION
1. Site Identification
 Han-Dee Hugo #97 (Facility ID 00-0-00000037345)
 Incident Number 48153
 Risk Classification – Pending
 Location of Source Area: 305 Pritchard Road
Clayton, NC 27410
Johnston County (Figure 1)
35.694444 °N, 78.420765 °W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner (Table 1)
Sampson-Bladen Oil Company, Inc.
Post Office Box 469
Clinton, NC 28329
[e-mail]
910-592-4177

UST Operator
Sampson-Bladen Oil Company, Inc.
Post Office Box 469
Clinton, NC 28329
[e-mail]
919-270-9379

Property Owner
Sampson-Bladen Oil Company, Inc.
Post Office Box 469
Clinton, NC 28329
[e-mail]
910-592-4177

Property Occupant
Sampson-Bladen Oil Company, Inc.
Post Office Box 469
Clinton, NC 28329
[e-mail]
910-592-4177

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered on October 21,2021.
 An unknown amount of product was released from the leaking UST System.
 One 15,000-gallon gasoline, one 8,000-gallon gasoline and one 8,000-gallon diesel USTs are in use at
the site (Table 2).

Certification:

I, Rae Troiano Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
iv
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... ii
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iv
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................6
6. LIMITATIONS ........................................................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Soil Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results

APPENDICES
Appendix A: Johnston County Property Cards
Appendix B: Well Construction Records
Appendix C: State Correspondence
Appendix D: Laboratory Analytical Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A
If YES, describe.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
2
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? N/A

MW-1 was installed to 40 feet bgs but yielded no water.

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility (Figure 2).

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility in the near future.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
3
7. What is the zoning status of the property?
According to the Town of Clayton Official Zoning Map, the site is zoned PD-MU (Planned
Development-Mixed Use).

8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store in the near future.

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 20 Simmental Court, located approximately 360 feet northwest
of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Riverwood Elementary School is located at 801 New Garden Road, approximately 220 feet south
of the source area at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Town of Clayton Zoning Map, the surrounding areas are zoned Highway business
(B-3), Planned development mixed use (PD-MU), residential (R) and office institutional (O-I).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of mixed-use, public/institutional and residential. Land
use information has been included as Table 3. A zoning map has been included as Figure 2B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on April 19, 2022. Five active water supply wells were identified
within a 1,500-foot radius of the site. None of the wells identified are located within 1,000-feet
of the site. A Site Vicinity Map showing property boundaries for the site and surrounding

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
4
properties has been included as Figure 2A. Water supply well information has been provided in
Table 4.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by the Town of Clayton.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
No surface water bodies were observed within 1,500 feet of the source area.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On May 17, 2022, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along Pritchard Road and Covered Bridge Road and several
underground utility lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners
are attached as Appendix A.

3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Raleigh Belt. The bedrock
is generally described as foliated to massive granitic rock. The soil samples collected during well
installation activities were red and tan silty clays to silt. The depth to ground water during the April 2022
gauging event was greater than 40 feet bgs. A copy of the well construction record has been included as
Appendix B. A Site Map is included as Figure 3. Well construction and gauging information is presented

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
5
in Table 6. Photos of the newly installed monitoring well is shown below:

4. SITE INVESTIGATION
On September 16, 2021, during a site assessment for property refinancing, GRI personnel installed six soil
borings (TMW-1 through TMW-6) around the UST basin and dispenser areas. Based on field observations,
the soil at the site was found to consist primarily of silts to approximately 49 feet below bgs the terminal
depth of TMW-2. All remaining boring locations were drilled to 20 feet using direct push technology. No
ground water was encountered; therefore, soil samples were collected from TMW-1-20’ through TMW-
6-20’ approximately 20 feet BGS and submitted for laboratory analysis of VOCs by EPA Method 8260 and
semi-VOCs by EPA Method 8270. No petroleum odors were observed in any of the soil samples collected.
Estimated concentrations of benzo(a)anthracene and benzo(a)pyrene reported in the soil sample
collected from TMW-5-20’ exceeded the soil-to-water MCCs as specified in 15A NCAC 02L.0202. None of
the concentrations exceeded the residential SCLs. Locations of the soil samples are shown on Figure 4
and a summary of the soil laboratory results are show in Table 7. Based on these results, the NCDEQ
requested an LSA. A copy of the NORR has been included in Appendix C.

On April 19, 2022, one monitoring well (MW-1) was installed by a North Carolina licensed well contractor.
MW-1 was installed to a total depth of 40 feet bgs with a 25-foot screened interval set to bracket the
water table at the time of installation in the vicinity of TMW-5, the location with soil contamination
identified during September 2021 site assessment.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
6

1. Soil Sampling:
On April 19, 2022, three soil samples (SB-1 10’, SB-2 20’, SB-3 30’) were collected at 10-foot intervals
during the installation of monitoring well MW-1. The soil samples were submitted for analysis of VPH
by the MADEP method. Soil samples (SB-1 10’ and SB-3 30’) were also submitted for analysis of VOCs
by EPA Method 8260B/8270.

No reported contaminant concentrations exceeded the soil-to-water MCCs. A Soil Quality Map has
been included as Figure 4. A summary of the soil sample analytical results is presented in Table 7. A
copy of the laboratory analytical report from the April 2022 soil sampling event has been included in
Appendix D. A copy of the current soil sampling data collected during the LSA activities is shown
below:
Sample ID Sample Depth (ft-BGS) Benzene Toluene Ethylbenzene Total Xylenes MTBE Naphthalene Soil to Water MCC (mg/kg) 4.3 4.9 4.6 0.091 0.091 0.16
Residential SCL (mg/kg) 1,200 1,560 3,129 350 350 313
SB-1-10’ 10 <0.0013 <0.011 <0.0011 <0.0022 <0.0011 <0.0021
SB-2-20’ 20 <0.0015 <0.012 <0.0012 <0.0025 <0.0011 <0.34
SB-3-30’ 30 <0.0015 <0.012 <0.0012 <0.0025 <0.0012 <0.0024

2. Ground Water Sampling:
On April 19 and 25, 2022, no water was measured in MW-1; therefore, no ground water samples were
collected.

3. Quality Control:
The soil samples were immediately placed in laboratory-supplied containers after collection, which
were then placed in iced coolers. New disposable bailers were used to sample the monitoring well
and new nitrile gloves were worn during soil and ground water sampling. Samples were logged using
proper chain-of-custody procedures. The samples were transported to a North Carolina certified
laboratory for analysis.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, residential, office and public/institutional properties.
 In April 2022, a receptor survey was conducted. No potable wells were identified within 1,000
feet of the site. Public water is available to the subject site and to all surrounding properties. No
surface water bodies were identified within 500 feet of the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: June 15, 2022 Han-Dee Hugo #97
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 5816
7
 In September 2021, during a site assessment for refinancing, estimated concentrations of
benzo(a)anthracene and benzo(a)pyrene in the soil sample TMW-5-20’ exceeded the soil-to-
water MCCs.
 April 19, 2022, during installation of MW-1 in the former location of TMW-5-20’, soil samples
were collected at 10-foot intervals to 30 feet bgs. No reported contaminant concentrations
exceeded the soil-to-water MCCs.
 On April 19 and 25, 2022, no ground water was present in MW-1; therefore, no ground water
samples were collected.
 Based on the lack of soil-to-water MCC violations in any of the soil samples collected during the
LSA, it was deemed unnecessary to install MW-1 deeper.
 Based on the lack of receptors, the site should be classified as low risk. Contaminant
concentrations reported in TMW-5-20’ exceeded the soil-to-water MCC; therefore, public notice
should be completed and no further action should be required. An NRP is not required as none
of the estimated concentrations exceeded the residential SCLs.

6. LIMITATIONS
This report has been prepared for the exclusive use of Sampson-Bladen Oil Company, Inc. for specific
application to the referenced site in Johnston County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site Location Han-Dee Hugo #97304 Pritchard RoadClayton North CarolinaJohnston CountyIncident No. 48153GRI Project No. 5816500 M2000 FTDate: 06/13/2022 Location: 35.694444° N -78.420765° W Dad
"J
"J
"J
"J
"J
SITE
177000-17-7221
177000-36-6724
177000-28-3331
177000-27-6207
177000-26-3738
177000-18-6465
177000-18-5117
177000-27-5130
177000-26-4958
177000-28-0238
PRITCHARD RD MEDLIN RDC O V E R E D B R ID G E R DATHLETIC CLUB BLVDEL
W
A
Y D
R
STETS
O
N LN
SWANN TRLM A N N IN G D R
PAYTON DRC O L LIN S W O R TH D R BRIDGEPORT CIRDOE LN
HUTSON LNM A R IN O P LB
ALL
A
N
C
E
R W
A
Y
G
E
LB
VIE
H PL
FAWN LNWRANGLER DRRIVERWOOD RANCH BLVDWA
T
E
RF
I
E
L
D
DRSTANSBURY LNSIMMENTAL CTFIGURE 2A: SITE VICINITY MAPHAN-DEE HUGO#97304 PRITCHARD ROADCLAYTON, JOHNSTON COUNTYNORTH CAROLINAINCIDENT NO. 48153GRI NO. 5816
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 18, 20221,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
500-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
Street Centerlines
Hydrology
Well Owners and Adjacent Properties
Johnston County NC parcels_2020
1
1 Land Use Code
"J
"J
"J
"J
"J
SITEPRITCHARD RD MEDLIN RDC O V E R E D B R ID G E R DATHLETIC CLUB BLVDEL
W
A
Y D
R
STETS
O
N LN
SWANN TRLM A N N IN G D R
PAYTON DRC O L LIN S W O R TH D R BRIDGEPORT CIRDOE LN
HUTSON LNM A R IN O P LB
ALL
A
N
C
E
R W
A
Y
G
E
LB
VIE
H PL
FAWN LNWRANGLER DRRIVERWOOD RANCH BLVDWA
T
E
RF
I
E
L
D
DRSTANSBURY LNSIMMENTAL CTFIGURE 2B: ZONING MAPHAN-DEE HUGO#97304 PRITCHARD ROADCLAYTON, JOHNSTON COUNTYNORTH CAROLINAINCIDENT NO. 48153GRI NO. 5816
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 18, 20221,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
500-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
Street Centerlines
Hydrology
ZONING - R-6
ZONING - B-1
ZONING - O-I
ZONING - B-3
ZONING - R-8
ZONING - R-E
ZONING - PD-MU
ZONING - R-10
Johnston County NC parcels_2020

TABLES
UST ID Number 1A-3 Facility ID Number
Owner or Operator?
Owner
00-0-0000037345
TABLE 1
UST OWNER/OPERATOR INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
Post Office Box 469, Clinton, NC 28328 910-862-2650
Name of Owner Dates of Ownership
Sampson-Bladen Oil Company, Inc. 11/01/2011 - Current
Address Telephone Number
Page 1 of 1
Date: 05/17/22
Was Release
Associated
with UST
System?
(Yes / No)
1A Gasoline NA 8,000 5/1/1997 Single Wall FRP 8' x 21' 4" Single Wall FRP Current No
1B Gasoline NA 12,000 5/1/1997 Single Wall FRP 8' x 21' 4" Single Wall FRP Current Yes
2 Kerosene NA 2,500 5/1/1997 Single Wall FRP 8' x 21' 4" Single Wall FRP Current No
3 Diesel NA 6,000 1/15/1999 Single Wall FRP 8' x 21' 4" Other Current No
TABLE 2
UST SYSTEM INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 00-0-00000373545
Page 1 of 1
Date: 05/17/22 Facility ID # : 00-0-0000037345
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Riverwood Elementary &
Middle R-10 School
204 Athletic Club
Clayton, NC 27527 ~200
n/a PD-MU
Planned Development-
Mixed Use n/a ~0
3 n/a B-3 Highway buisness n/a ~100
n/a O-I Office-Institutional n/a ~700
n/a R-E Residential-Estate n/a ~1,000
n/a R-6 Single Family Residential n/a ~1,500
n/a B-1 Central Buisness n/a ~1,550
Note:
• Properties are keyed to Figure 3.
TABLE 3
LAND USE INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
Page 1 of 1
Facility ID # : 00-0-0000037345
Well ID. Parcel ID No. Well Owner Mailing Address Well Address
Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
WSW-1 16I02008B Gary Daniel Weaver
2907 Schooner Lane
Grimesland, NC 27837
4083 Covered Bridge Road
Clayton, NC 27527 Active Non-Potable Yes No ~1,200' SW
WSW-2 16I02008I Shirley G Weaver Life Estate
4025 Covered Bridge Road
Clayton, NC 27527
4025 Covered Bridge Road
Clayton, NC 27527 Active Potable Yes No ~1,400' SW
WSW-3 16I02008C Del Peepers
3991 Covered Bridge Road
Clayton, NC 27527
3991 Covered Bridge Road
Clayton, NC 27527 Active Non-Potable Yes No ~1,485' SW
WSW-4 16I02008D Dorothy Gazaway
3941 Covered Bridge Road
Clayton, NC 27527
3941 Covered Bridge Road
Clayton, NC 27527 Active Potable Yes No ~1,650' SW
WSW-5 16I01014F Timothy Smith
4080 Covered Bridge Road
Clayton, NC 27527
4080 Covered Bridge Road
Clayton, NC 27527 Active Potable Yes No ~1,550' SW
Notes:
• Receptors are shown on Figure 3.
• n/a: not applicable.
Unknown
Unknown
Unknown
Unknown
Unknown
TABLE 4
RECEPTOR INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
Date: 05/17/22
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
Page 1 of 1
Date: 05/17/22 Facility ID #: 00-0-0000037345
PIN Number Property Owner Name Property Owner Address
16I02047V Sampson-Bladen Oil Company, Inc.
Post office Box 469
Clinton, NC 28329-0469
16I02053P Riverwood Ranch Townhomes, LLC.
1375 East 9th Street Suite 200
Cleveland, OH 44114-1739
16I02047U Riverwood Land Company, LLC.
Post Office Box 31827
Raleigh, NC 27622-0000
16I02008A Zogreo, LLC. &Wilder Investors LLS.
1201 Edwards Mill Road Suite 300
Raleigh, NC 27607-0180
16I02047T Gandhi at Riverwood, LLC.
9201 Leesville Road
Raleigh, NC 27613-0000
16I02008Z County of Johnston
Post Office Box 1049
Smithfield, NC 27577
Note:
• Properties are keyed to Figure 2.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
Page 1 of 1
Date: 05/27/22 Facility ID #: 00-0-0000035425
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
04/19/22 Dry --- NA
04/25/22 Dry --- NA
Notes:
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
Han-Dee Hugo #97 (INCIDENT NO. 48153)
MW-1 04/19/22 15 15-40 40 NM
Page 1 of 1
Date: 05/26/22
Sample ID Date Collected
(mm/dd/yy)
Sample
Depth
(feet)
0.0072 5.4 8 6 0.085 0.2 0.17 0.058 68 540 31 540 NE 31
12 1,250 60.3 3,120 156 5.5 6.6 0.66 625 1,560 469 1,560 31,200 469
SB-1 10' 04/19/2022 10 <0.0013 <0.011 <0.0011 <0.0022 <0.0011 <0.0021 0.0248 J <0.023 <3.2 <3.2 <3.2 <3.0 6.72 J 7.42 J
SB-2 20' 04/19/2022 20 NR NR NR NR NR NR NR NR <4.0 <4.0 <4.0 <3.3 <3.3 <5.2
SB-3 30' 04/19/2022 30 <0.0015 <0.012 <0.0012 <0.0025 <0.0012 <0.0024 <0.022 <0.026 <3.1 <3.1 <3.1 <3.3 <3.3 <5.3
TMW-1-20' 9/16/2021 20 <0.0009 <0.001 <0.0009 <0.0007 <0.0009 0.004 J <0.208 <0.220 NR NR NR NR NR NR
TMW-2-20' 9/16/2021 20 <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 0.002 J <0.190 <0.201 NR NR NR NR NR NR
TMW-3-20' 9/16/2021 20 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 <0.176 <0.186 NR NR NR NR NR NR
TMW-4-20' 9/16/2021 20 <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 <0.182 <0.193 NR NR NR NR NR NR
TMW-5-20' 9/16/2021 20 <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 0.195 J 0.268 J NR NR NR NR NR NR
TMW-6-20' 9/16/2021 20 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 <0.171 <0.181 NR NR NR NR NR NR
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• MCC: Maximum Soil Contaminant Concentration level as specified by T 15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report
• Concentrations in bold face type exceeded the soil to ground water MCCs.
• NE: Not Established
• J: Estimated value.
• NR: Not Requested
TABLE 7
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
Han-Dee Hugo #97 (INCIDENT NO. 48153)
Facility ID #: 00-0-0000037345
MADEP EPH
Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl-ether (MTBE)Analytical Method SW846 8260D MADEP VPH
Soil to Water MCC (mg/kg)
Residential Soil Cleanup Level (mg/kg)C9-C18 AliphaticsC19-C36 AliphaticsC11-C22 AromaticsC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsBenzo(a)pyreneBenzo(a)anthraceneNaphthalene

APPENDICES

APPENDIX A
County Parcel Records

* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:10060 - 1 in. = 838.33 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02046B
Tag:16I02046B
NCPin:177000-18-0722
Mapsheet No:1770
Owner Name 1:ZOGREO, LLC
Owner Name 2:WILDER INVESTORS LLS
Mail Address 1:1201 EDWARDS MILL RD
Mail Address 2:Suite 300
Mail Address 3:RALEIGH, NC 27607-0180
Site Address 1:
Site Address 2:
Book:03988
Page:0123
Market Value:571590
Assessed Acreage:8.310
Calc. Acreage:8.330
Sales Price:0
Sale Date:2011-06-01
Powered by TCPDF (www.tcpdf.org)
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:10060 - 1 in. = 838.33 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02008A
Tag:16I02008A
NCPin:177000-18-6465
Mapsheet No:1770
Owner Name 1:ZOGREO, LLC
Owner Name 2:WILDER INVESTORS LLS
Mail Address 1:1201 EDWARDS MILL RD
Mail Address 2:Suite 300
Mail Address 3:RALEIGH, NC 27607-0180
Site Address 1:2165 PRITCHARD RD
Site Address 2:CLAYTON, NC 27520-
Book:04804
Page:0887
Market Value:326260
Assessed Acreage:2.140
Calc. Acreage:2.150
Sales Price:0
Sale Date:2016-07-29
Powered by TCPDF (www.tcpdf.org)
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:10060 - 1 in. = 838.33 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02047V
Tag:16I02047V
NCPin:177000-28-0238
Mapsheet No:1770
Owner Name 1:SAMPSON - BLADEN OIL
COMPANY, INCORPORATED
Owner Name 2:
Mail Address 1:
Mail Address 2:PO BOX 469
Mail Address 3:CLINTON, NC 28329-0469
Site Address 1:
Site Address 2:
Book:06068
Page:0591
Market Value:1660030
Assessed Acreage:1.300
Calc. Acreage:1.300
Sales Price:0
Sale Date:2021-10-04
Powered by TCPDF (www.tcpdf.org)
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:10060 - 1 in. = 838.33 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02008Z
Tag:16I02008Z
NCPin:177000-17-7221
Mapsheet No:1770
Owner Name 1:COUNTY OF JOHNSTON
Owner Name 2:
Mail Address 1:
Mail Address 2:PO BOX 1049
Mail Address 3:SMITHFIELD, NC 27577-0000
Site Address 1:108 ATHLETIC CLUB BLVD
Site Address 2:CLAYTON, NC 27527-
Book:01823
Page:0286
Market Value:25919930
Assessed Acreage:45.700
Calc. Acreage:45.390
Sales Price:0
Sale Date:1999-05-03
Result 2
id:16I02008Z
Tag:16I02008Z
NCPin:177000-17-7221
Mapsheet No:1770
Owner Name 1:COUNTY OF JOHNSTON
Owner Name 2:
Mail Address 1:
Mail Address 2:PO BOX 1049
Mail Address 3:SMITHFIELD, NC 27577-0000
Site Address 1:204 ATHLETIC CLUB BLVD
Site Address 2:CLAYTON, NC 27527-
Book:01823
Page:0286
Market Value:25919930
Assessed Acreage:45.700
Calc. Acreage:45.390
Sales Price:0
Sale Date:1999-05-03
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Powered by TCPDF (www.tcpdf.org)
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:10060 - 1 in. = 838.33 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02009C
Tag:16I02009C
NCPin:177000-07-9827
Mapsheet No:1770
Owner Name 1:FSC I LLC
Owner Name 2:
Mail Address 1:400 RIVERWOOD DR
Mail Address 2:
Mail Address 3:CLAYTON, NC 27527-0000
Site Address 1:205 ATHLETIC CLUB BLVD
Site Address 2:CLAYTON, NC 27527-
Book:04542
Page:0710
Market Value:2289340
Assessed Acreage:7.960
Calc. Acreage:8.030
Sales Price:0
Sale Date:2014-12-31
Powered by TCPDF (www.tcpdf.org)
* * * DISCLAIMER * * *
Johnston County assumes no legal responsibility for the information represented here.
Scale: 1:1257 - 1 in. = 104.79 feet
(The scale is only accurate when printed landscape on a 8 1/2 x 11 size sheet with no page scaling.)Johnston County GIS
June 14, 2022
Result 1
id:16I02047T
Tag:16I02047T
NCPin:177000-18-5117
Mapsheet No:1770
Owner Name 1:GANDHI AT RIVERWOOD LLC
Owner Name 2:
Mail Address 1:9201 LEESVILLE RD, STE 201
Mail Address 2:
Mail Address 3:RALEIGH, NC 27613-0000
Site Address 1:304 PRITCHARD RD
Site Address 2:CLAYTON, NC 27527-
Book:03777
Page:0480
Market Value:147230
Assessed Acreage:1.690
Calc. Acreage:1.680
Sales Price:360000
Sale Date:2009-11-06
Powered by TCPDF (www.tcpdf.org)

APPENDIX B
Well Construction Record

WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX C
State Correspondence
North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville,
NC 28301 | [phone]
December 10, 2021
Sampson-Bladen Oil Company Inc.
Mr. Howell Clark
PO BOX 469
Clinton, NC 28328
Re: Notice of Regulatory Requirements
15A NCAC 2L .0404 and 2L .0405
Risk-based Assessment and Corrective Action for
Commercial Petroleum Underground Storage Tanks
Han-Dee Hugo #97
304PritchardRoad
Johnston County
Incident Number: 48153
Risk Classification: Pending
Dear Mr. Clark:
Information received by this regional office of the Underground Storage Tank Section, Division of
Waste Management, on October 25, 2021, confirms a release or discharge from a petroleum underground
storage tank (UST) system at the above-referenced location. Records indicate that you are the owner or
operator of this UST system. Therefore, as a responsible party, you must comply with the initial response
and abatement action requirements of the Title 15A of the North Carolina Administrative Code (NCAC),
Subchapter 2L .0404 and, if applicable, the assessment and reporting requirements of Title 15A NCAC 2L
.0405, within the timeframes specified in the attached rules. (Be aware that if Title 15A NCAC 2L .0405
is applicable, you must comply with its requirements even if you do not receive formal notification from
the UST Section.)
Initial abatement action requirements include the preparation and submittal of an Initial Abatement
Action (IAA) Report, in accordance with Title 15A NCAC 2L .0404 and the most recent version of the
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases, within
90 days of discovery of the release.
Because a release or discharge has been confirmed, a Licensed Geologist or a Professional
Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to
the Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and 2L
.0111(b).
Please note that before you sell, transfer, or request a “No Further Action” determination for a
property that has not been remediated to below “unrestricted use” standards, you must file a Notice of
Residual Petroleum ("Notice") with the Register of Deeds in the county where the property is located (North
Carolina General Statutes 143B-279.9 and 143B-279.11).
5816 Received FEB 14 2022
North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville,
NC 28301 | [phone]
Failure to comply with the State's rules in the manner and time specified may result in the
assessment of civil penalties and/or the use of other enforcement mechanisms.
If you have any questions regarding trust fund eligibility or reimbursement from the Commercial
Leaking Petroleum Underground Storage Tank Cleanup Funds, please contact the UST Section Trust Fund
Branch at [phone]. If you have any questions regarding the actions that must be taken or the rules
mentioned in this letter, please contact me at the address or telephone number listed below.
Enclosures: Title 15A NCAC 2L .0404 and 2L .0405
cc: Marilyn Pearson, Johnston County Health Department Director (email only)
Rae Brown, Geological Resources, Inc. (email only)
Fayetteville Regional Office | 225 Green St | #714 Systel Building | Fayetteville, NC 28301 | [phone]
IAA noncomm high NOR 0617.dotx
Sincerely,
Sarah Brown
Environmental Specialist II
Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ
Site Name City / County /Johnston Incident #48153
Resp Pty Name / Contact Incident Mgr Region RAL
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #0
Consultant / Project Mgr /Rae T Brown
Telephone / Fax Number /Task Authorization Number:1 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:Pending RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
2.600 1 /site Y $6,919.00 y $6,919.00 $6,919.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$6,919.00 $6,919.00 TOTAL:
Total Standard Costs (Not Third Party)$6,919.00 $6,919.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:2/15/22 by:(PM)(Reserved for RO)
RO Review:3/7/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 3/17/2022
CO Review:3/11/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 8/1/2020
RTB
Proposed
Units / Type
(Consultant)
Sarah Brown
ActiveFALSE
22-125 Mar-22
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
mpson-Bladen Oill Compa
Geological Resources, Inc.
DIRECTED COSTS
Clayton
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Han-Hugo 97
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have beencompletedwithin12monthsofthecompletiondateoftheFIRSTcompletedtasktoremainwithintheStatuteofLimitations.All ePATAs submittedwithin aclaim are closed with thatclaim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
SBB
HB
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
NCDEQ Registered Tank Report
Facility Id 00-0-0000037345
Facility Name HANDEE HUGO 97
Address PRITCHARD ROAD AND E ATHLETIC BL
City CLAYTON State NC
Zip 27527County Johnston
Latitude 35.694484Longitude-78.420461
Tank Owner SAMPSON-BLADEN OIL COMPAN
Address PO BOX 469 / 932 US 421 N
City CLINTON
State NC Zip 28328-0469
Tank Information
Tank Id Product Name Capacity Installation Date Perm Close Date Tank Construction Piping Construction OverFill Protection Spill Protection Tank Status
1A Gasoline, Gas Mix 8000 12/28/2011 Double Wall FRP DW Flexible Piping Auto Shutoff Device Catchment Basin Current
1B Gasoline, Gas Mix 15000 12/28/2011 Double Wall FRP DW Flexible Piping Auto Shutoff Device Catchment Basin Current
1C Diesel 8000 12/28/2011 Double Wall FRP DW Flexible Piping Auto Shutoff Device Catchment Basin Current
Monday, August 16, 2021 Page 1 of 1

APPENDIX D
Laboratory Analytical Reports
05/26/22
Technical Report for
GRI (Geological Resources Inc.)
Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
5816
SGS Job Number: FA95037
Sampling Date: 04/19/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Rae Brown
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 05/26/22
e-Hardcopy 2.0
Automated Report
45
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 45
FA95037
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA95037-1: SB-1 10' ....................................................................................................6
3.2: FA95037-2: SB-2 20' ....................................................................................................12
3.3: FA95037-3: SB-3 30' ....................................................................................................14
Section 4: Misc. Forms ............................................................................................................20
4.1: Chain of Custody ...........................................................................................................21
Section 5: MS Volatiles - QC Data Summaries .....................................................................23
5.1: Method Blank Summary ................................................................................................24
5.2: Blank Spike Summary ...................................................................................................26
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................28
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................30
6.1: Method Blank Summary ................................................................................................31
6.2: Blank Spike Summary ...................................................................................................33
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................35
Section 7: GC Volatiles - QC Data Summaries .....................................................................37
7.1: Method Blank Summary ................................................................................................38
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................39
7.3: Duplicate Summary .......................................................................................................40
Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................41
8.1: Method Blank Summary ................................................................................................42
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................43
8.3: Duplicate Summary .......................................................................................................45 123456782 of 45
FA95037
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA95037
Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Project No: 5816
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA95037-1 04/19/22 08:07 JB 04/21/22 SO Soil SB-1 10'
FA95037-2 04/19/22 08:19 JB 04/21/22 SO Soil SB-2 20'
FA95037-3 04/19/22 08:27 JB 04/21/22 SO Soil SB-3 30'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 45
FA950371
Summary of Hits Page 1 of 1
Job Number:FA95037
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Collected:04/19/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA95037-1 SB-1 10'
Benzo(a)anthracene 0.0248 J 0.20 0.020 mg/kg SW846 8270E
Chrysene 0.0377 J 0.20 0.020 mg/kg SW846 8270E
Fluoranthene 0.118 J 0.20 0.020 mg/kg SW846 8270E
Phenanthrene 0.0336 J 0.20 0.020 mg/kg SW846 8270E
Pyrene 0.0923 J 0.20 0.023 mg/kg SW846 8270E
C11-C22 Aromatics (Unadj.)7.42 J 12 4.8 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics 7.42 J 12 4.8 mg/kg MADEP EPH REV 2.1
C19-C36 Aliphatics 6.72 J 12 3.0 mg/kg MADEP EPH REV 2.1
FA95037-2 SB-2 20'
No hits reported in this sample.
FA95037-3 SB-3 30'
No hits reported in this sample.
4 of 45
FA950372
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 45
FA950373
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8260D Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B19076.D 1 05/19/22 21:17 JG n/a n/a V2B810
Run #2 b 2B18898.D 1 04/26/22 22:23 JG n/a n/a V2B806
Initial Weight Final Volume
Run #1 5.62 g 5.0 ml
Run #2 5.12 g 5.0 ml
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 0.21 0.11 mg/kg
71-43-2 Benzene ND 0.0053 0.0013 mg/kg
75-27-4 Bromodichloromethane ND 0.0053 0.0011 mg/kg
75-25-2 Bromoform c ND 0.0053 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.026 0.0077 mg/kg
104-51-8 n-Butylbenzene ND 0.0053 0.0011 mg/kg
75-15-0 Carbon Disulfide ND 0.0053 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0053 0.0011 mg/kg
108-90-7 Chlorobenzene ND 0.0053 0.0011 mg/kg
75-00-3 Chloroethane ND 0.0053 0.0021 mg/kg
67-66-3 Chloroform ND 0.0053 0.0014 mg/kg
110-82-7 Cyclohexane ND 0.0053 0.0013 mg/kg
124-48-1 Dibromochloromethane ND 0.0053 0.0011 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0053 0.0020 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0053 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane d ND 0.0053 0.0021 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0053 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0053 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0053 0.0012 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0053 0.0019 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0053 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0053 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0053 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0053 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0053 0.0011 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
100-41-4 Ethylbenzene ND 0.0053 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.026 0.0079 mg/kg
98-82-8 Isopropylbenzene ND 0.0053 0.0011 mg/kg
79-20-9 Methyl Acetate ND 0.026 0.0094 mg/kg
74-83-9 Methyl Bromide ND 0.0053 0.0021 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8260D Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride d ND 0.0053 0.0021 mg/kg
108-87-2 Methylcyclohexane ND 0.0053 0.0018 mg/kg
75-09-2 Methylene Chloride ND 0.021 0.012 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.026 0.0079 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0053 0.0011 mg/kg
91-20-3 Naphthalene ND 0.0053 0.0021 mg/kg
103-65-1 n-Propylbenzene ND 0.0053 0.0011 mg/kg
100-42-5 Styrene ND 0.0053 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0053 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0053 0.0014 mg/kg
108-88-3 Toluene ND 0.021 0.011 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0053 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0053 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0053 0.0011 mg/kg
79-01-6 Trichloroethylene ND 0.0053 0.0011 mg/kg
75-69-4 Trichlorofluoromethane d ND 0.0053 0.0021 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0053 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0053 0.0011 mg/kg
75-01-4 Vinyl Chloride e ND 0.0053 0.0011 mg/kg
1330-20-7 Xylene (total)ND 0.016 0.0022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%110%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%117%72-135%
2037-26-5 Toluene-D8 97%94%75-126%
460-00-4 4-Bromofluorobenzene 104%103%71-133%
(a) Sample re-analyzed beyond hold time. Results reported from bisulfate preserved vial.
(b) Results reported from bisulfate preserved vial. Confirmation run.
(c) Associated CCV outside control limits low.
(d) Associated CCV outside control limits low. Confirmed by re-analysis.
(e) Associated BS recovery outside control limits low. Confirmed by re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8270E SW846 3546 Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X081070.D 1 04/26/22 07:49 WH 04/22/22 07:30 OP90880 SX3246
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 0.99 0.20 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.20 0.022 mg/kg
95-57-8 2-Chlorophenol ND 0.20 0.024 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.20 0.023 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.20 0.053 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.99 0.20 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.40 0.079 mg/kg
95-48-7 2-Methylphenol ND 0.20 0.024 mg/kg
3&4-Methylphenol ND 0.20 0.033 mg/kg
88-75-5 2-Nitrophenol b ND 0.20 0.022 mg/kg
100-02-7 4-Nitrophenol ND 0.99 0.20 mg/kg
87-86-5 Pentachlorophenol ND 0.99 0.20 mg/kg
108-95-2 Phenol ND 0.20 0.020 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.20 0.023 mg/kg
83-32-9 Acenaphthene ND 0.20 0.021 mg/kg
208-96-8 Acenaphthylene ND 0.20 0.020 mg/kg
120-12-7 Anthracene ND 0.20 0.022 mg/kg
56-55-3 Benzo(a)anthracene 0.0248 0.20 0.020 mg/kg J
50-32-8 Benzo(a)pyrene ND 0.20 0.023 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.20 0.022 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.20 0.021 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.20 0.026 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.20 0.021 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.20 0.040 mg/kg
106-47-8 4-Chloroaniline ND 0.20 0.050 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.20 0.020 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.20 0.023 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.20 0.025 mg/kg
91-58-7 2-Chloronaphthalene ND 0.20 0.020 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.20 0.020 mg/kg
218-01-9 Chrysene 0.0377 0.20 0.020 mg/kg J
53-70-3 Dibenzo(a,h)anthracene ND 0.20 0.025 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8270E SW846 3546 Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.20 0.020 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.20 0.047 mg/kg
84-66-2 Diethyl Phthalate ND 0.40 0.040 mg/kg
131-11-3 Dimethyl Phthalate ND 0.20 0.040 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.20 0.040 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.40 0.079 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.20 0.020 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.20 0.026 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.40 0.040 mg/kg
206-44-0 Fluoranthene 0.118 0.20 0.020 mg/kg J
86-73-7 Fluorene ND 0.20 0.021 mg/kg
118-74-1 Hexachlorobenzene ND 0.20 0.020 mg/kg
87-68-3 Hexachlorobutadiene ND 0.20 0.020 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.20 0.040 mg/kg
67-72-1 Hexachloroethane ND 0.20 0.023 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 0.024 mg/kg
78-59-1 Isophorone ND 0.20 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.20 0.020 mg/kg
91-57-6 2-Methylnaphthalene ND 0.20 0.020 mg/kg
91-20-3 Naphthalene ND 0.20 0.020 mg/kg
98-95-3 Nitrobenzene ND 0.20 0.020 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.20 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.20 0.021 mg/kg
85-01-8 Phenanthrene 0.0336 0.20 0.020 mg/kg J
129-00-0 Pyrene 0.0923 0.20 0.023 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 89%40-102%
4165-62-2 Phenol-d5 87%41-100%
118-79-6 2,4,6-Tribromophenol 78%42-108%
4165-60-0 Nitrobenzene-d5 77%40-105%
321-60-8 2-Fluorobiphenyl 84%43-107%
1718-51-0 Terphenyl-d14 101%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP VPH REV 2.1 Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U9880.D 1 04/29/22 15:25 JR n/a n/a G1U438
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 3.77 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.090 0.090 mg/kg
100-41-4 Ethylbenzene ND 0.18 0.090 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.18 0.090 mg/kg
91-20-3 Naphthalene ND 0.45 0.27 mg/kg
108-88-3 Toluene ND 0.18 0.090 mg/kg
m,p-Xylene ND 0.36 0.18 mg/kg
95-47-6 o-Xylene ND 0.18 0.090 mg/kg
C5- C8 Aliphatics (Unadj.)ND 9.0 3.2 mg/kg
C9- C12 Aliphatics (Unadj.)ND 9.0 3.2 mg/kg
C9- C10 Aromatics (Unadj.)ND 9.0 3.2 mg/kg
C5- C8 Aliphatics ND 9.0 3.2 mg/kg
C9- C12 Aliphatics ND 9.0 3.2 mg/kg
C9- C10 Aromatics ND 9.0 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 288% a 70-130%
460-00-4 BFB 270% a 70-130%
(a) Outside control limits, Sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-1 10'
Lab Sample ID:FA95037-1 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:84.0
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN038133.D 1 04/26/22 19:07 AF 04/25/22 10:00 OP90914 GNN1783
Run #2
Initial Weight Final Volume
Run #1 20.0 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.24 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.24 0.12 mg/kg
120-12-7 Anthracene ND 0.24 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.24 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.24 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.24 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.24 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.24 0.12 mg/kg
218-01-9 Chrysene ND 0.24 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.24 0.12 mg/kg
206-44-0 Fluoranthene ND 0.24 0.12 mg/kg
86-73-7 Fluorene ND 0.24 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.24 0.12 mg/kg
91-57-6 2-Methylnaphthalene ND 0.24 0.12 mg/kg
91-20-3 Naphthalene ND 0.24 0.12 mg/kg
85-01-8 Phenanthrene ND 0.24 0.12 mg/kg
129-00-0 Pyrene ND 0.24 0.12 mg/kg
C11-C22 Aromatics (Unadj.)7.42 12 4.8 mg/kg J
C11-C22 Aromatics 7.42 12 4.8 mg/kg J
C9-C18 Aliphatics ND 12 3.0 mg/kg
C19-C36 Aliphatics 6.72 12 3.0 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 58% a 40-140%
580-13-2 2-Bromonaphthalene 78%40-140%
84-15-1 o-Terphenyl 62% a 40-140%
321-60-8 2-Fluorobiphenyl 71%40-140%
(a) Surrogate recoveries corrected for double spike.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 45
FA9503733.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-2 20'
Lab Sample ID:FA95037-2 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP VPH REV 2.1 Percent Solids:76.4
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U9881.D 1 04/29/22 15:55 JR n/a n/a G1U438
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 3.38 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.11 0.11 mg/kg
100-41-4 Ethylbenzene ND 0.23 0.11 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.23 0.11 mg/kg
91-20-3 Naphthalene ND 0.57 0.34 mg/kg
108-88-3 Toluene ND 0.23 0.11 mg/kg
m,p-Xylene ND 0.46 0.23 mg/kg
95-47-6 o-Xylene ND 0.23 0.11 mg/kg
C5- C8 Aliphatics (Unadj.)ND 11 4.0 mg/kg
C9- C12 Aliphatics (Unadj.)ND 11 4.0 mg/kg
C9- C10 Aromatics (Unadj.)ND 11 4.0 mg/kg
C5- C8 Aliphatics ND 11 4.0 mg/kg
C9- C12 Aliphatics ND 11 4.0 mg/kg
C9- C10 Aromatics ND 11 4.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 336% a 70-130%
460-00-4 BFB 309% a 70-130%
(a) Outside control limits, Sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 45
FA9503733.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-2 20'
Lab Sample ID:FA95037-2 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:76.4
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN038166.D 1 04/27/22 11:44 AF 04/25/22 10:00 OP90914 GNN1783
Run #2
Initial Weight Final Volume
Run #1 20.1 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.26 0.13 mg/kg
208-96-8 Acenaphthylene ND 0.26 0.13 mg/kg
120-12-7 Anthracene ND 0.26 0.13 mg/kg
56-55-3 Benzo(a)anthracene ND 0.26 0.13 mg/kg
50-32-8 Benzo(a)pyrene ND 0.26 0.13 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.26 0.13 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.26 0.13 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.26 0.13 mg/kg
218-01-9 Chrysene ND 0.26 0.13 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.26 0.13 mg/kg
206-44-0 Fluoranthene ND 0.26 0.13 mg/kg
86-73-7 Fluorene ND 0.26 0.13 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.13 mg/kg
91-57-6 2-Methylnaphthalene ND 0.26 0.13 mg/kg
91-20-3 Naphthalene ND 0.26 0.13 mg/kg
85-01-8 Phenanthrene ND 0.26 0.13 mg/kg
129-00-0 Pyrene ND 0.26 0.13 mg/kg
C11-C22 Aromatics (Unadj.)ND 13 5.2 mg/kg
C11-C22 Aromatics ND 13 5.2 mg/kg
C9-C18 Aliphatics ND 13 3.3 mg/kg
C19-C36 Aliphatics ND 13 3.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 50% a 40-140%
580-13-2 2-Bromonaphthalene 108%40-140%
84-15-1 o-Terphenyl 58% a 40-140%
321-60-8 2-Fluorobiphenyl 100%40-140%
(a) Surrogate recoveries corrected for double spike.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 45
FA9503733.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8260D Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B19075.D 1 05/19/22 20:52 JG n/a n/a V2B810
Run #2 b 2B18899.D 1 04/26/22 22:47 JG n/a n/a V2B806
Initial Weight Final Volume
Run #1 5.46 g 5.0 ml
Run #2 5.05 g 5.0 ml
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 0.24 0.12 mg/kg
71-43-2 Benzene ND 0.0061 0.0015 mg/kg
75-27-4 Bromodichloromethane ND 0.0061 0.0012 mg/kg
75-25-2 Bromoform c ND 0.0061 0.0012 mg/kg
78-93-3 2-Butanone (MEK)ND 0.030 0.0088 mg/kg
104-51-8 n-Butylbenzene ND 0.0061 0.0012 mg/kg
75-15-0 Carbon Disulfide ND 0.0061 0.0012 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0061 0.0012 mg/kg
108-90-7 Chlorobenzene ND 0.0061 0.0012 mg/kg
75-00-3 Chloroethane ND 0.0061 0.0024 mg/kg
67-66-3 Chloroform ND 0.0061 0.0016 mg/kg
110-82-7 Cyclohexane ND 0.0061 0.0015 mg/kg
124-48-1 Dibromochloromethane ND 0.0061 0.0012 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0061 0.0023 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0061 0.0012 mg/kg
75-71-8 Dichlorodifluoromethane d ND 0.0061 0.0024 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0061 0.0012 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0061 0.0012 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0061 0.0014 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0061 0.0021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0061 0.0012 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0061 0.0012 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0061 0.0017 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0061 0.0012 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0061 0.0012 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0061 0.0012 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0061 0.0012 mg/kg
100-41-4 Ethylbenzene ND 0.0061 0.0012 mg/kg
591-78-6 2-Hexanone ND 0.030 0.0091 mg/kg
98-82-8 Isopropylbenzene ND 0.0061 0.0012 mg/kg
79-20-9 Methyl Acetate ND 0.030 0.011 mg/kg
74-83-9 Methyl Bromide ND 0.0061 0.0024 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 45
FA9503733.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8260D Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride d ND 0.0061 0.0024 mg/kg
108-87-2 Methylcyclohexane ND 0.0061 0.0021 mg/kg
75-09-2 Methylene Chloride ND 0.024 0.013 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.030 0.0091 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0061 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0061 0.0024 mg/kg
103-65-1 n-Propylbenzene ND 0.0061 0.0012 mg/kg
100-42-5 Styrene ND 0.0061 0.0012 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0061 0.0012 mg/kg
127-18-4 Tetrachloroethylene ND 0.0061 0.0016 mg/kg
108-88-3 Toluene ND 0.024 0.012 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0061 0.0012 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0061 0.0012 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0061 0.0012 mg/kg
79-01-6 Trichloroethylene ND 0.0061 0.0012 mg/kg
75-69-4 Trichlorofluoromethane d ND 0.0061 0.0024 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0061 0.0012 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0061 0.0012 mg/kg
75-01-4 Vinyl Chloride e ND 0.0061 0.0012 mg/kg
1330-20-7 Xylene (total)ND 0.018 0.0025 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%110%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%120%72-135%
2037-26-5 Toluene-D8 96%93%75-126%
460-00-4 4-Bromofluorobenzene 98%97%71-133%
(a) Sample re-analyzed beyond hold time. Results reported from bisulfate preserved vial.
(b) Results reported from bisulfate preserved vial. Confirmation run.
(c) Associated CCV outside control limits low.
(d) Associated CCV outside control limits low. Confirmed by re-analysis.
(e) Associated BS recovery outside control limits low. Confirmed by re-analysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 45
FA9503733.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8270E SW846 3546 Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X081073.D 1 04/26/22 09:04 WH 04/22/22 07:30 OP90880 SX3246
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 1.1 0.22 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.22 0.025 mg/kg
95-57-8 2-Chlorophenol ND 0.22 0.027 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.22 0.025 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.22 0.058 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.1 0.22 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.44 0.088 mg/kg
95-48-7 2-Methylphenol ND 0.22 0.026 mg/kg
3&4-Methylphenol ND 0.22 0.036 mg/kg
88-75-5 2-Nitrophenol b ND 0.22 0.024 mg/kg
100-02-7 4-Nitrophenol ND 1.1 0.22 mg/kg
87-86-5 Pentachlorophenol ND 1.1 0.22 mg/kg
108-95-2 Phenol ND 0.22 0.022 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.22 0.025 mg/kg
83-32-9 Acenaphthene ND 0.22 0.023 mg/kg
208-96-8 Acenaphthylene ND 0.22 0.022 mg/kg
120-12-7 Anthracene ND 0.22 0.025 mg/kg
56-55-3 Benzo(a)anthracene ND 0.22 0.022 mg/kg
50-32-8 Benzo(a)pyrene ND 0.22 0.026 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.22 0.024 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.22 0.023 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.22 0.029 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.22 0.023 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.22 0.044 mg/kg
106-47-8 4-Chloroaniline ND 0.22 0.055 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.22 0.022 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.22 0.025 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.22 0.028 mg/kg
91-58-7 2-Chloronaphthalene ND 0.22 0.022 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.22 0.022 mg/kg
218-01-9 Chrysene ND 0.22 0.022 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.22 0.027 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 45
FA9503733.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:SW846 8270E SW846 3546 Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.22 0.022 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.22 0.052 mg/kg
84-66-2 Diethyl Phthalate ND 0.44 0.044 mg/kg
131-11-3 Dimethyl Phthalate ND 0.22 0.044 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.22 0.044 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.44 0.088 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.22 0.022 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.22 0.028 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.44 0.044 mg/kg
206-44-0 Fluoranthene ND 0.22 0.022 mg/kg
86-73-7 Fluorene ND 0.22 0.023 mg/kg
118-74-1 Hexachlorobenzene ND 0.22 0.022 mg/kg
87-68-3 Hexachlorobutadiene ND 0.22 0.022 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.22 0.044 mg/kg
67-72-1 Hexachloroethane ND 0.22 0.026 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.22 0.027 mg/kg
78-59-1 Isophorone ND 0.22 0.022 mg/kg
90-12-0 1-Methylnaphthalene ND 0.22 0.022 mg/kg
91-57-6 2-Methylnaphthalene ND 0.22 0.022 mg/kg
91-20-3 Naphthalene ND 0.22 0.022 mg/kg
98-95-3 Nitrobenzene ND 0.22 0.022 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.22 0.022 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.22 0.024 mg/kg
85-01-8 Phenanthrene ND 0.22 0.022 mg/kg
129-00-0 Pyrene ND 0.22 0.025 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 75%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 66%42-108%
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 73%43-107%
1718-51-0 Terphenyl-d14 88%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 45
FA9503733.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP VPH REV 2.1 Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1U9882.D 1 04/29/22 16:25 JR n/a n/a G1U438
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.68 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.088 0.088 mg/kg
100-41-4 Ethylbenzene ND 0.18 0.088 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.18 0.088 mg/kg
91-20-3 Naphthalene ND 0.44 0.26 mg/kg
108-88-3 Toluene ND 0.18 0.088 mg/kg
m,p-Xylene ND 0.35 0.18 mg/kg
95-47-6 o-Xylene ND 0.18 0.088 mg/kg
C5- C8 Aliphatics (Unadj.)ND 8.8 3.1 mg/kg
C9- C12 Aliphatics (Unadj.)ND 8.8 3.1 mg/kg
C9- C10 Aromatics (Unadj.)ND 8.8 3.1 mg/kg
C5- C8 Aliphatics ND 8.8 3.1 mg/kg
C9- C12 Aliphatics ND 8.8 3.1 mg/kg
C9- C10 Aromatics ND 8.8 3.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 261% a 70-130%
460-00-4 BFB 249% a 70-130%
(a) Outside control limits, Sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 45
FA9503733.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-3 30'
Lab Sample ID:FA95037-3 Date Sampled:04/19/22
Matrix:SO - Soil Date Received:04/21/22
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:75.6
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN038168.D 1 04/27/22 12:44 AF 04/25/22 10:00 OP90914 GNN1783
Run #2
Initial Weight Final Volume
Run #1 20.0 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.26 0.13 mg/kg
208-96-8 Acenaphthylene ND 0.26 0.13 mg/kg
120-12-7 Anthracene ND 0.26 0.13 mg/kg
56-55-3 Benzo(a)anthracene ND 0.26 0.13 mg/kg
50-32-8 Benzo(a)pyrene ND 0.26 0.13 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.26 0.13 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.26 0.13 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.26 0.13 mg/kg
218-01-9 Chrysene ND 0.26 0.13 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.26 0.13 mg/kg
206-44-0 Fluoranthene ND 0.26 0.13 mg/kg
86-73-7 Fluorene ND 0.26 0.13 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.13 mg/kg
91-57-6 2-Methylnaphthalene ND 0.26 0.13 mg/kg
91-20-3 Naphthalene ND 0.26 0.13 mg/kg
85-01-8 Phenanthrene ND 0.26 0.13 mg/kg
129-00-0 Pyrene ND 0.26 0.13 mg/kg
C11-C22 Aromatics (Unadj.)ND 13 5.3 mg/kg
C11-C22 Aromatics ND 13 5.3 mg/kg
C9-C18 Aliphatics ND 13 3.3 mg/kg
C19-C36 Aliphatics ND 13 3.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 57% a 40-140%
580-13-2 2-Bromonaphthalene 110%40-140%
84-15-1 o-Terphenyl 64% a 40-140%
321-60-8 2-Fluorobiphenyl 102%40-140%
(a) Surrogate recoveries corrected for double spike.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 45
FA9503733.3
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
20 of 45
FA950374
FA95037: Chain of Custody
Page 1 of 2
21 of 45
FA9503744.1
Job Number:FA95037 Client:GEOLOGICAL RESOURCES INC
Date / Time Received:4/21/2022 9:30:00 AM Delivery Method:FED EX
Project:HW-DEE HUGO 97/ SF16
Airbill #'s:1009 6379 5766
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments FROZEN@ 4/21/2022 1540
IT APPEARS THAT ONE VIAL FOR SAMPLES 1,2 & 3 DO NOT HAVE ENOUGH MeOH PRESERVATIVE IN THEM.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.4);
Cooler 1: (2.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:CARLOSD Date:Date:4/21/2022 9:30:00 AM
FA95037: Chain of Custody
Page 2 of 2
22 of 45
FA9503744.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
23 of 45
FA950375
Method Blank Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B810-MB 2B19067.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
110-82-7 Cyclohexane ND 5.0 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.9 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
79-20-9 Methyl Acetate ND 25 8.9 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.7 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
24 of 45
FA9503755.1.1
Method Blank Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B810-MB 2B19067.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%72-135%
2037-26-5 Toluene-D8 98%75-126%
460-00-4 4-Bromofluorobenzene 101%71-133%
25 of 45
FA9503755.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B810-BS 2B19066.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 205 82 61-152
71-43-2 Benzene 50 46.9 94 76-126
75-27-4 Bromodichloromethane 50 43.0 86 74-130
75-25-2 Bromoform 50 40.0 80 76-127
78-93-3 2-Butanone (MEK)250 210 84 75-137
104-51-8 n-Butylbenzene 50 42.9 86 71-128
75-15-0 Carbon Disulfide 50 45.6 91 72-122
56-23-5 Carbon Tetrachloride 50 42.5 85 78-133
108-90-7 Chlorobenzene 50 44.4 89 81-129
75-00-3 Chloroethane 50 45.9 92 68-133
67-66-3 Chloroform 50 40.5 81 72-123
110-82-7 Cyclohexane 50 46.2 92 73-126
124-48-1 Dibromochloromethane 50 41.7 83 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 38.9 78 70-137
106-93-4 1,2-Dibromoethane 50 43.9 88 77-126
75-71-8 Dichlorodifluoromethane 50 35.2 70 68-168
95-50-1 1,2-Dichlorobenzene 50 43.8 88 80-129
541-73-1 1,3-Dichlorobenzene 50 46.6 93 81-129
106-46-7 1,4-Dichlorobenzene 50 44.8 90 76-130
75-34-3 1,1-Dichloroethane 50 42.8 86 73-125
107-06-2 1,2-Dichloroethane 50 41.9 84 74-128
75-35-4 1,1-Dichloroethylene 50 41.7 83 81-136
156-59-2 cis-1,2-Dichloroethylene 50 43.3 87 74-126
156-60-5 trans-1,2-Dichloroethylene 50 42.7 85 70-127
78-87-5 1,2-Dichloropropane 50 44.9 90 74-125
10061-01-5 cis-1,3-Dichloropropene 50 47.0 94 80-123
10061-02-6 trans-1,3-Dichloropropene 50 45.7 91 75-131
100-41-4 Ethylbenzene 50 45.8 92 77-123
591-78-6 2-Hexanone 250 295 118 72-133
98-82-8 Isopropylbenzene 50 45.8 92 80-136
79-20-9 Methyl Acetate 250 214 86 67-137
74-83-9 Methyl Bromide 50 41.7 83 65-139
74-87-3 Methyl Chloride 50 37.3 75 71-144
108-87-2 Methylcyclohexane 50 50.1 100 75-128
75-09-2 Methylene Chloride 50 47.0 94 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 215 86 76-132
* = Outside of Control Limits.
26 of 45
FA9503755.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B810-BS 2B19066.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 46.5 93 77-120
91-20-3 Naphthalene 50 43.6 87 79-129
103-65-1 n-Propylbenzene 50 47.0 94 80-135
100-42-5 Styrene 50 46.3 93 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 42.1 84 71-126
127-18-4 Tetrachloroethylene 50 46.6 93 79-130
108-88-3 Toluene 50 46.1 92 76-124
120-82-1 1,2,4-Trichlorobenzene 50 44.8 90 78-130
71-55-6 1,1,1-Trichloroethane 50 39.9 80 70-129
79-00-5 1,1,2-Trichloroethane 50 42.8 86 74-124
79-01-6 Trichloroethylene 50 46.4 93 75-128
75-69-4 Trichlorofluoromethane 50 40.4 81 73-145
95-63-6 1,2,4-Trimethylbenzene 50 45.3 91 74-123
108-67-8 1,3,5-Trimethylbenzene 50 47.0 94 73-122
75-01-4 Vinyl Chloride 50 35.4 71*76-141
1330-20-7 Xylene (total)150 139 93 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 95%75-124%
17060-07-0 1,2-Dichloroethane-D4 91%72-135%
2037-26-5 Toluene-D8 100%75-126%
460-00-4 4-Bromofluorobenzene 101%71-133%
* = Outside of Control Limits.
27 of 45
FA9503755.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA95355-4MS 2B19083.D 1 05/20/22 JG n/a n/a V2B810
FA95355-4MSD 2B19084.D 1 05/20/22 JG n/a n/a V2B810
FA95355-4 a 2B19080.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
FA95355-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 620 326 357 -81*316 368 -80*3 61-152/27
71-43-2 Benzene 20.4 65.3 60.9 62*63.2 59.0 61*3 76-126/26
75-27-4 Bromodichloromethane ND 65.3 57.3 88 63.2 53.4 85 7 74-130/25
75-25-2 Bromoform ND 65.3 44.7 68*63.2 42.2 67*6 76-127/26
78-93-3 2-Butanone (MEK)279 326 251 -9*316 263 -5*5 75-137/25
104-51-8 n-Butylbenzene ND 65.3 48.9 75 63.2 55.1 87 12 71-128/35
75-15-0 Carbon Disulfide ND 65.3 59.2 91 63.2 56.1 89 5 72-122/29
56-23-5 Carbon Tetrachloride ND 65.3 61.0 93 63.2 56.4 89 8 78-133/29
108-90-7 Chlorobenzene ND 65.3 54.1 83 63.2 54.3 86 0 81-129/29
75-00-3 Chloroethane ND 65.3 55.8 86 63.2 52.8 84 6 68-133/29
67-66-3 Chloroform ND 65.3 55.6 85 63.2 51.8 82 7 72-123/26
110-82-7 Cyclohexane ND 65.3 62.9 96 63.2 60.4 96 4 73-126/32
124-48-1 Dibromochloromethane ND 65.3 50.8 78 63.2 48.2 76 5 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 65.3 38.0 58*63.2 39.6 63*4 70-137/29
106-93-4 1,2-Dibromoethane 5.4 J 65.3 49.8 68*63.2 49.8 70*0 77-126/26
75-71-8 Dichlorodifluoromethane ND 65.3 52.1 80 63.2 45.8 72 13 68-168/29
95-50-1 1,2-Dichlorobenzene ND 65.3 49.3 76*63.2 50.9 81 3 80-129/32
541-73-1 1,3-Dichlorobenzene ND 65.3 54.3 83 63.2 56.6 90 4 81-129/33
106-46-7 1,4-Dichlorobenzene ND 65.3 51.2 78 63.2 54.1 86 6 76-130/32
75-34-3 1,1-Dichloroethane ND 65.3 57.1 87 63.2 53.6 85 6 73-125/27
107-06-2 1,2-Dichloroethane 6.9 65.3 55.0 74 63.2 51.8 71*6 74-128/23
75-35-4 1,1-Dichloroethylene ND 65.3 59.1 91 63.2 54.8 87 8 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 65.3 56.4 86 63.2 53.8 85 5 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 65.3 57.7 88 63.2 54.7 87 5 70-127/27
78-87-5 1,2-Dichloropropane ND 65.3 57.3 88 63.2 54.8 87 4 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND 65.3 56.8 87 63.2 54.8 87 4 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 65.3 52.6 81 63.2 51.2 81 3 75-131/28
100-41-4 Ethylbenzene ND 65.3 57.8 89 63.2 59.5 94 3 77-123/31
591-78-6 2-Hexanone 100 326 316 66*316 329 72 4 72-133/26
98-82-8 Isopropylbenzene ND 65.3 56.8 87 63.2 59.8 95 5 80-136/32
79-20-9 Methyl Acetate ND 326 268 82 316 289 91 8 67-137/30
74-83-9 Methyl Bromide ND 65.3 51.7 79 63.2 48.9 77 6 65-139/31
74-87-3 Methyl Chloride ND 65.3 57.5 88 63.2 54.2 86 6 71-144/27
108-87-2 Methylcyclohexane ND 65.3 68.1 104 63.2 65.9 104 3 75-128/31
75-09-2 Methylene Chloride ND 65.3 91.4 140*63.2 80.6 128 13 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)38.6 326 216 54*316 222 58*3 76-132/26
* = Outside of Control Limits.
28 of 45
FA9503755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA95355-4MS 2B19083.D 1 05/20/22 JG n/a n/a V2B810
FA95355-4MSD 2B19084.D 1 05/20/22 JG n/a n/a V2B810
FA95355-4 a 2B19080.D 1 05/19/22 JG n/a n/a V2B810
The QC reported here applies to the following samples:Method: SW846 8260D
FA95037-1, FA95037-3
FA95355-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 2030 E 65.3 412 -2479* b63.2 643 -2195* b44*77-120/24
91-20-3 Naphthalene 9.4 65.3 48.2 59*63.2 51.9 67*7 79-129/33
103-65-1 n-Propylbenzene ND 65.3 56.0 86 63.2 61.1 97 9 80-135/33
100-42-5 Styrene ND 65.3 56.6 87 63.2 57.2 91 1 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND 65.3 43.7 67*63.2 43.7 69*0 71-126/30
127-18-4 Tetrachloroethylene ND 65.3 60.6 93 63.2 62.4 99 3 79-130/31
108-88-3 Toluene 26.3 65.3 59.9 51*63.2 61.6 56*3 76-124/30
120-82-1 1,2,4-Trichlorobenzene ND 65.3 50.1 77*63.2 53.0 84 6 78-130/34
71-55-6 1,1,1-Trichloroethane ND 65.3 57.8 89 63.2 53.4 85 8 70-129/27
79-00-5 1,1,2-Trichloroethane ND 65.3 49.7 76 63.2 49.1 78 1 74-124/28
79-01-6 Trichloroethylene ND 65.3 64.6 99 63.2 62.5 99 3 75-128/27
75-69-4 Trichlorofluoromethane ND 65.3 60.7 93 63.2 54.6 86 11 73-145/31
95-63-6 1,2,4-Trimethylbenzene 2.9 J 65.3 55.7 81 63.2 63.5 96 13 74-123/34
108-67-8 1,3,5-Trimethylbenzene 1.8 J 65.3 56.4 84 63.2 62.6 96 10 73-122/33
75-01-4 Vinyl Chloride ND 65.3 44.5 68*63.2 43.2 68*3 76-141/27
1330-20-7 Xylene (total)16.4 J 196 177 82 190 187 90 5 80-129/30
CAS No.Surrogate Recoveries MS MSD FA95355-4 Limits
1868-53-7 Dibromofluoromethane 97%97%105%75-124%
17060-07-0 1,2-Dichloroethane-D4 93%91%113%72-135%
2037-26-5 Toluene-D8 101%102%104%75-126%
460-00-4 4-Bromofluorobenzene 99%98%94%71-133%
(a) Sample re-analyzed beyond hold time. Results reported from bisulfate preserved vial.
(b) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
29 of 45
FA9503755.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
30 of 45
FA950376
Method Blank Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-MB X081064.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
31 of 45
FA9503766.1.1
Method Blank Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-MB X081064.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 90%40-102%
4165-62-2 Phenol-d5 89%41-100%
118-79-6 2,4,6-Tribromophenol 78%42-108%
4165-60-0 Nitrobenzene-d5 80%40-105%
321-60-8 2-Fluorobiphenyl 85%43-107%
1718-51-0 Terphenyl-d14 101%45-119%
32 of 45
FA9503766.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-BS X081063.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 3830 115 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1530 92 52-108
95-57-8 2-Chlorophenol 1670 1720 103 48-104
120-83-2 2,4-Dichlorophenol 1670 1710 103 51-105
105-67-9 2,4-Dimethylphenol 1670 1340 80 43-96
51-28-5 2,4-Dinitrophenol 3330 2750 83 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3180 95 64-121
95-48-7 2-Methylphenol 1670 1590 95 46-107
3&4-Methylphenol 3330 3270 98 44-111
88-75-5 2-Nitrophenol 1670 1780 107*49-104
100-02-7 4-Nitrophenol 3330 2710 81 56-116
87-86-5 Pentachlorophenol 3330 3080 92 61-114
108-95-2 Phenol 1670 1520 91 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1710 103 56-109
83-32-9 Acenaphthene 1670 1420 85 56-109
208-96-8 Acenaphthylene 1670 1460 88 56-106
120-12-7 Anthracene 1670 1300 78 61-110
56-55-3 Benzo(a)anthracene 1670 1500 90 66-111
50-32-8 Benzo(a)pyrene 1670 1480 89 59-104
205-99-2 Benzo(b)fluoranthene 1670 1590 95 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1490 89 67-113
207-08-9 Benzo(k)fluoranthene 1670 1720 103 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1500 90 62-110
85-68-7 Butyl benzyl phthalate 1670 1630 98 65-113
106-47-8 4-Chloroaniline 1670 616 74 30-115
111-91-1 bis(2-Chloroethoxy)methane 835 1410 85 48-105
111-44-4 bis(2-Chloroethyl)ether 835 1540 92 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 1640 98 40-110
91-58-7 2-Chloronaphthalene 1670 1480 89 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1460 88 58-106
218-01-9 Chrysene 1670 1600 96 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1530 92 68-115
132-64-9 Dibenzofuran 835 753 90 a 57-108
91-94-1 3,3'-Dichlorobenzidine 835 647 78 a 36-114
84-66-2 Diethyl Phthalate 1670 1470 88 61-109
131-11-3 Dimethyl Phthalate 1670 1490 89 59-108
* = Outside of Control Limits.
33 of 45
FA9503766.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-BS X081063.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1640 98 64-119
84-74-2 Di-n-butyl Phthalate 1670 1530 92 63-108
121-14-2 2,4-Dinitrotoluene 1670 1630 98 59-109
606-20-2 2,6-Dinitrotoluene 1670 1610 97 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1530 92 64-115
206-44-0 Fluoranthene 1670 1500 90 60-108
86-73-7 Fluorene 1670 1510 91 58-109
118-74-1 Hexachlorobenzene 1670 1450 87 59-111
87-68-3 Hexachlorobutadiene 1670 1460 88 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1400 84 49-110
67-72-1 Hexachloroethane 1670 1430 86 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1450 87 66-116
78-59-1 Isophorone 1670 1440 86 42-89
90-12-0 1-Methylnaphthalene 1670 1470 88 49-106
91-57-6 2-Methylnaphthalene 1670 800 96 47-106
91-20-3 Naphthalene 1670 1450 87 44-104
98-95-3 Nitrobenzene 1670 1380 83 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1550 93 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1470 88 62-110
85-01-8 Phenanthrene 1670 1410 85 63-111
129-00-0 Pyrene 1670 1500 90 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 98%40-102%
4165-62-2 Phenol-d5 96%41-100%
118-79-6 2,4,6-Tribromophenol 83%42-108%
4165-60-0 Nitrobenzene-d5 81%40-105%
321-60-8 2-Fluorobiphenyl 86%43-107%
1718-51-0 Terphenyl-d14 95%45-119%
(a) Spike recoveries calculated from actual spike mix concentration.
* = Outside of Control Limits.
34 of 45
FA9503766.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-MS X081071.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
OP90880-MSD X081072.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
FA95037-1 X081070.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
FA95037-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 3960 3990 101 3940 4270 108 7 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 1980 1590 80 1970 1700 86 7 52-108/21
95-57-8 2-Chlorophenol ND 1980 1530 77 1970 1650 84 8 48-104/26
120-83-2 2,4-Dichlorophenol ND 1980 1700 86 1970 1810 92 6 51-105/27
105-67-9 2,4-Dimethylphenol ND 1980 1380 70 1970 1490 76 8 43-96/23
51-28-5 2,4-Dinitrophenol ND 3960 2400 61 3940 2730 69 13 40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 3960 3030 77 3940 3350 85 10 64-121/29
95-48-7 2-Methylphenol ND 1980 1460 74 1970 1560 79 7 46-107/24
3&4-Methylphenol ND 3960 2990 76 3940 3240 82 8 44-111/24
88-75-5 2-Nitrophenol ND 1980 1720 87 1970 1870 95 8 49-104/27
100-02-7 4-Nitrophenol ND 3960 2960 75 3940 3190 81 7 56-116/23
87-86-5 Pentachlorophenol ND 3960 3440 87 3940 3720 94 8 61-114/23
108-95-2 Phenol ND 1980 1360 69 1970 1480 75 8 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 1980 1830 93 1970 1970 100 7 56-109/25
83-32-9 Acenaphthene ND 1980 1520 77 1970 1600 81 5 56-109/23
208-96-8 Acenaphthylene ND 1980 1580 80 1970 1650 84 4 56-106/23
120-12-7 Anthracene ND 1980 1430 72 1970 1540 78 7 61-110/21
56-55-3 Benzo(a)anthracene 24.8 J 1980 1690 84 1970 1820 91 7 66-111/23
50-32-8 Benzo(a)pyrene ND 1980 1690 85 1970 1790 91 6 59-104/23
205-99-2 Benzo(b)fluoranthene ND 1980 1800 91 1970 1890 96 5 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1980 1760 89 1970 1920 97 9 67-113/21
207-08-9 Benzo(k)fluoranthene ND 1980 1820 92 1970 1970 100 8 67-114/22
101-55-3 4-Bromophenyl phenyl ether ND 1980 1620 82 1970 1780 90 9 62-110/21
85-68-7 Butyl benzyl phthalate ND 1980 1910 97 1970 2090 106 9 65-113/20
106-47-8 4-Chloroaniline ND 1980 488 25*1970 683 35 33*30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1980 1390 70 1970 1500 76 8 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1980 1370 69 1970 1480 75 8 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1980 1470 74 1970 1610 82 9 40-110/25
91-58-7 2-Chloronaphthalene ND 1980 1580 80 1970 1640 83 4 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 1980 1540 78 1970 1650 84 7 58-106/21
218-01-9 Chrysene 37.7 J 1980 1790 89 1970 1950 97 9 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1980 1770 90 1970 1940 98 9 68-115/23
132-64-9 Dibenzofuran ND 990 793 80 a 990 835 84 a 5 57-108/22
91-94-1 3,3'-Dichlorobenzidine ND 990 666 68 a 990 853 86 a 25 36-114/28
84-66-2 Diethyl Phthalate ND 1980 1600 81 1970 1710 87 7 61-109/20
131-11-3 Dimethyl Phthalate ND 1980 1630 82 1970 1720 87 5 59-108/20
* = Outside of Control Limits.
35 of 45
FA9503766.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90880-MS X081071.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
OP90880-MSD X081072.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
FA95037-1 X081070.D 1 04/26/22 WH 04/22/22 OP90880 SX3246
The QC reported here applies to the following samples:Method: SW846 8270E
FA95037-1, FA95037-3
FA95037-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
117-84-0 Di-n-octyl Phthalate ND 1980 1900 96 1970 2060 105 8 64-119/21
84-74-2 Di-n-butyl Phthalate ND 1980 1710 86 1970 1850 94 8 63-108/19
121-14-2 2,4-Dinitrotoluene ND 1980 1720 87 1970 1900 96 10 59-109/20
606-20-2 2,6-Dinitrotoluene ND 1980 1680 85 1970 1810 92 7 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 1980 1760 89 1970 1960 99 11 64-115/23
206-44-0 Fluoranthene 118 J 1980 1690 79 1970 1770 84 5 60-108/25
86-73-7 Fluorene ND 1980 1610 81 1970 1730 88 7 58-109/21
118-74-1 Hexachlorobenzene ND 1980 1580 80 1970 1690 86 7 59-111/21
87-68-3 Hexachlorobutadiene ND 1980 1420 72 1970 1480 75 4 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1980 1270 64 1970 1370 70 8 49-110/31
67-72-1 Hexachloroethane ND 1980 1290 65 1970 1380 70 7 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1980 1740 88 1970 1900 96 9 66-116/22
78-59-1 Isophorone ND 1980 1440 73 1970 1560 79 8 42-89/22
90-12-0 1-Methylnaphthalene ND 1980 1490 75 1970 1570 80 5 49-106/26
91-57-6 2-Methylnaphthalene ND 1980 780 39*1970 813 41*4 47-106/27
91-20-3 Naphthalene ND 1980 1430 72 1970 1520 77 6 44-104/27
98-95-3 Nitrobenzene ND 1980 1350 68 1970 1460 74 8 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1980 1420 72 1970 1530 78 7 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1980 1640 83 1970 1770 90 8 62-110/21
85-01-8 Phenanthrene 33.6 J 1980 1580 78 1970 1690 84 7 63-111/22
129-00-0 Pyrene 92.3 J 1980 1800 86 1970 1940 94 7 65-115/25
CAS No.Surrogate Recoveries MS MSD FA95037-1 Limits
367-12-4 2-Fluorophenol 73%79%89%40-102%
4165-62-2 Phenol-d5 72%78%87%41-100%
118-79-6 2,4,6-Tribromophenol 74%81%78%42-108%
4165-60-0 Nitrobenzene-d5 66%72%77%40-105%
321-60-8 2-Fluorobiphenyl 76%81%84%43-107%
1718-51-0 Terphenyl-d14 90%99%101%45-119%
(a) Spike recoveries calculated from actual spike mix concentration.
* = Outside of Control Limits.
36 of 45
FA9503766.3.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
37 of 45
FA950377
Method Blank Summary Page 1 of 1
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U438-MB 1U9876.D 1 04/29/22 JR n/a n/a G1U438
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 51 51 ug/kg
100-41-4 Ethylbenzene ND 100 51 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 100 51 ug/kg
91-20-3 Naphthalene ND 260 150 ug/kg
108-88-3 Toluene ND 100 51 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene ND 100 51 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg
C5- C8 Aliphatics ND 5100 1800 ug/kg
C9- C12 Aliphatics ND 5100 1800 ug/kg
C9- C10 Aromatics ND 5100 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 128%70-130%
460-00-4 BFB 126%70-130%
38 of 45
FA9503777.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1U438-BS 1U9874.D 1 04/29/22 JR n/a n/a G1U438
G1U438-BSD 1U9875.D 1 04/29/22 JR n/a n/a G1U438
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 4160 3720 89 4110 99 10 70-130/25
100-41-4 Ethylbenzene 4160 3710 89 4160 100 11 70-130/25
1634-04-4 Methyl Tert Butyl Ether 4160 3640 87 4100 99 12 70-130/25
91-20-3 Naphthalene 4160 3700 89 4030 97 9 70-130/25
108-88-3 Toluene 4160 3740 90 4140 99 10 70-130/25
m,p-Xylene 8320 7770 93 8560 103 10 70-130/25
95-47-6 o-Xylene 4160 3760 90 4200 101 11 70-130/25
C5- C8 Aliphatics (Unadj.)12500 10900 87 12000 96 10 70-130/25
C9- C12 Aliphatics (Unadj.)8320 7370 89 7980 96 8 70-130/25
C9- C10 Aromatics (Unadj.)4160 3720 89 4210 101 12 70-130/25
C9- C10 Aromatics 4160 3720 89 4210 101 12 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 118%124%70-130%
460-00-4 BFB 121%127%70-130%
* = Outside of Control Limits.
39 of 45
FA9503777.2.1
Duplicate Summary Page 1 of 1
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA94951-1DUP 1U9878.D 1 04/29/22 JR n/a n/a G1U438
FA94951-1 a 1U9877.D 1 04/29/22 JR n/a n/a G1U438
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
FA94951-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
71-43-2 Benzene 80.5 73.5 9 50
100-41-4 Ethylbenzene 1780 1830 3 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene 3030 2720 11 50
108-88-3 Toluene 1780 1780 0 50
m,p-Xylene 11000 11100 1 50
95-47-6 o-Xylene 6830 6880 1 50
C5- C8 Aliphatics (Unadj.)18500 18800 2 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)132000 E 131000 E 1 50
C5- C8 Aliphatics 16600 17000 2 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics 132000 E 131000 E 1 50
CAS No.Surrogate Recoveries DUP FA94951-1 Limits
460-00-4 BFB 172%* c 166%* b 70-130%
460-00-4 BFB 145%* c 148%* b 70-130%
(a) Confirmation run.
(b) Outside control limits due to matrix interference.
(c) Outside control limits due to low methanol level.
* = Outside of Control Limits.
40 of 45
FA9503777.3.1
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 8
41 of 45
FA950378
Method Blank Summary Page 1 of 1
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90914-MB NN038122.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 4000 ug/kg
C11-C22 Aromatics ND 10000 4000 ug/kg
C9-C18 Aliphatics ND 10000 2500 ug/kg
C19-C36 Aliphatics ND 10000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 68% a 40-140%
580-13-2 2-Bromonaphthalene 103%40-140%
84-15-1 o-Terphenyl 72% a 40-140%
321-60-8 2-Fluorobiphenyl 98%40-140%
(a) Surrogate recoveries corrected for double spike.
42 of 45
FA9503788.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90914-BS NN038123.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
OP90914-BSD NN038124.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 3550 71 2860 57 22 40-140/30
208-96-8 Acenaphthylene 5000 3550 71 2850 57 22 40-140/30
120-12-7 Anthracene 5000 3730 75 3100 62 18 40-140/30
56-55-3 Benzo(a)anthracene 5000 4250 85 3560 71 18 40-140/30
50-32-8 Benzo(a)pyrene 5000 4280 86 3580 72 18 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 4430 89 3670 73 19 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 4070 81 3360 67 19 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 3700 74 3080 62 18 40-140/30
218-01-9 Chrysene 5000 3990 80 3330 67 18 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 4400 88 3630 73 19 40-140/30
206-44-0 Fluoranthene 5000 3890 78 3220 64 19 40-140/30
86-73-7 Fluorene 5000 3670 73 2980 60 21 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 4200 84 3470 69 19 40-140/30
91-57-6 2-Methylnaphthalene 5000 3110 62 2430 49 25 40-140/30
91-20-3 Naphthalene 5000 2940 59 2240 45 27 40-140/30
85-01-8 Phenanthrene 5000 3800 76 3120 62 20 40-140/30
129-00-0 Pyrene 5000 4030 81 3340 67 19 40-140/30
C11-C22 Aromatics (Unadj.)85000 67500 79 56300 66 18 40-140/30
C9-C18 Aliphatics 30000 21400 71 21700 72 1 40-140/30
C19-C36 Aliphatics 40000 33700 84 35000 88 4 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 64% a 67% a 40-140%
580-13-2 2-Bromonaphthalene 108%75%40-140%
84-15-1 o-Terphenyl 79% a 66% a 40-140%
321-60-8 2-Fluorobiphenyl 101%69%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP90914-BS 2-Methylnaphthalene 3110 ND 0.0%5.0
OP90914-BS Naphthalene 2940 ND 0.0%5.0
OP90914-BSD 2-Methylnaphthalene 2430 ND 0.0%5.0
OP90914-BSD Naphthalene 2240 ND 0.0%5.0
* = Outside of Control Limits.
43 of 45
FA9503788.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90914-BS NN038123.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
OP90914-BSD NN038124.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
(a) Surrogate recoveries corrected for double spike.
* = Outside of Control Limits.
44 of 45
FA9503788.2.1
Duplicate Summary Page 1 of 1
Job Number:FA95037
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 97; 304 Pritchard Rd, Clayton, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP90914-DUP NN038125.D 1 04/26/22 AF 04/25/22 OP90914 GNN1783
FA95037-2 NN038166.D 1 04/27/22 AF 04/25/22 OP90914 GNN1783
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA95037-1, FA95037-2, FA95037-3
FA95037-2 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 a
208-96-8 Acenaphthylene ND ND nc 30 a
120-12-7 Anthracene ND ND nc 30 a
56-55-3 Benzo(a)anthracene ND ND nc 30 a
50-32-8 Benzo(a)pyrene ND ND nc 30 a
205-99-2 Benzo(b)fluoranthene ND ND nc 30 a
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a
207-08-9 Benzo(k)fluoranthene ND ND nc 30 a
218-01-9 Chrysene ND ND nc 30 a
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a
206-44-0 Fluoranthene ND ND nc 30 a
86-73-7 Fluorene ND ND nc 30 a
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a
91-57-6 2-Methylnaphthalene ND ND nc 30 a
91-20-3 Naphthalene ND ND nc 30 a
85-01-8 Phenanthrene ND ND nc 30 a
129-00-0 Pyrene ND ND nc 30 a
C11-C22 Aromatics (Unadj.)ND ND nc 30 a
C11-C22 Aromatics ND ND nc 30 a
C9-C18 Aliphatics ND ND nc 30 a
C19-C36 Aliphatics ND ND nc 30 a
CAS No.Surrogate Recoveries DUP FA95037-2 Limits
3386-33-2 1-Chlorooctadecane 46% b 50% b 40-140%
580-13-2 2-Bromonaphthalene 104%108%40-140%
84-15-1 o-Terphenyl 60% b 58% b 40-140%
321-60-8 2-Fluorobiphenyl 97%100%40-140%
(a) Advisory control limits.
(b) Surrogate recoveries corrected for double spike.
* = Outside of Control Limits.
45 of 45
FA9503788.3.1