FA-27949_47245_CA_LTRRPT_20230406

1044 Washington Street
Raleigh, NC 27605
[phone]

www.CatlinUSA.com
Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA

E N V I RO N M E N TA L | C I V I L | G E O T E C H N I C A L

Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA | Charleston, SC

April 6, 2023

North Carolina Department of Environmental Quality (NCDEQ)
Division of Waste Management
UST Section
Attn: Mr. Mike Haseltine, L.G
127 Cardinal Drive Extension
Wilmington, NC 28405

Re: Field Activities Report – WSW-1 Sampling
NCDOT Carthage Road Oil Facility
3388 US Highway 15-501
Carthage, Moore County, North Carolina
Incident Number: 47245
NCDOT Contract Number: 7000020481
WBS Element: 42222.175
Risk Classification: High
CATLIN Project No. 220257

Dear Mr. Haseltine,

On behalf of the North Carolina Department of Transportation (NCDOT), CATLIN
Engineers and Scientists (CATLIN) is pleased to provide you with this letter report
documenting the sampling of a water supply well (WSW-1) on March 16, 2023. In an
email correspondence with Mr. Nathan Beauchamp (NCDEQ), access was granted to
sample WSW-1. The site location is illustrated on Figure 1 (Attachment A) and the water
supply well location is illustrated on Figure 2 (Attachment A). Water supply well
information is located in Table 1 (Attachment B).

Upon arrival to the site on March 16, 2023, CATLIN purged WSW-1 by allowing the spigot
to run for approximately 15 minutes. Following purging activities, a groundwater sample
was collected directly from the spigot into appropriate laboratory provided glassware,
labeled, and placed on ice in an insulated cooler. The sample was submitted to Con-Test
Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow,
Massachusetts, under proper chain of custody (COC) protocol for analysis per Standard
Method (SM) 6200B, Environmental Protection Agency (EPA) Method 625, and
Massachusetts Department of Environmental Protection (MADEP) Volatile Petroleum
Hydrocarbons (VPH).

April 6, 2023
Page 2 of 2
NCDOT; 47245_NCDOT Carthage Road Oil Facility CATLIN Engineers and Scientists
CATLIN Project No. 220257 April 2023

Laboratory analytical results for SM 6200B, EPA Method 625 and MADEP VPH revealed
all contaminant concentrations were all below the laboratory detection limits. The SM
6200B and EPA Method 625 results are summarized in Table 2 and the MADEP VPH
results are summarized in Table 3. The laboratory report and COC documentation is
included in Attachment C.

Based on the historical sampling results and fate and transport modeling data submitted
in the previous monitoring report dated October 18, 2022, along with the current WSW-1
sample results, CATLIN recommends the site be a candidate for No Further Action (NFA)
status with a Notice of Residual Petroleum (NRP) for groundwater.

Should you have any questions or require additional information, please contact Ms.
Jennifer Parish (NCDOT) at [phone] or me directly at [phone].

Sincerely,

Sean O’Neil, PE
Project Manager

CC:
Jennifer Parish (NCDOT): Electronic Copy

Attachments:
A Figures
B Tables
C Laboratory Analytical Data and Chain-of-Custody Documentation

NCDOT; 47245_NCDOT Carthage Road Oil Facility CATLIN Engineers and Scientists
CATLIN Project No. 220257 April 2023

ATTACHMENT A

FIGURES

FIGUREPROJECTTITLE
1CARTHAGE ROAD OIL FACILITY3388 US HWY 15-501CARTHAGE, NC
SITE VICINITY MAP
SITE LOCATION
PRIEST HILL RDUS HWY 15-
5
0
1
Copyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY47245220257AUG 2022 AS SHOWN KMC/SJO
FIGUREPROJECTTITLE
2CARTHAGE ROAD OIL FACILITY3388 US HWY 15-501CARTHAGE, NC
POTENTIAL RECEPTOR MAP
!(P
!(P
!(W
!(P
!(P !(P
!(P
!(P
!(P
!(P
!(P
!(W !(W
!(W
!(W!(W
!(P
!(P
!(P
!(P
SITE LOCATION
1 ,5 0 0 FEE T RADIUS
500F E ET RADIUSPRIEST HILL RDUS HWY 15-
5
0
1
POND 1
POND 2
POND 3
WSW-1
WSW-17WSW-3
WSW-10
WSW-11
WSW-18
WSW-14
WSW-12
WSW-9
WSW-8WSW-7
WSW-6
WSW-5
WSW-4
WSW-15
WSW-16
WSW-20
WSW-21
WSW-2
WSW-19
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
LEGEND
!(P PotableWater Supply Well
!(W Inactive Non-PotableWater Supply Well
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY47245220257AUG 2022 AS SHOWN KMC/SJO
NOTE: Well locations were obtained during field reconnaissance conducted on January 13, 2021 and are approximate.

NCDOT; 47245_NCDOT Carthage Road Oil Facility CATLIN Engineers and Scientists
CATLIN Project No. 220257 April 2023

ATTACHMENT B

TABLES

Page 1 of 2
TABLE 1
Well #Property Address Parcel
Number
Owner Name
(Last, First MI)
Owner Mailing
Address
Well
Use
Distance
from
Source
Area (ft.)
Comment
WSW-1 3344 US HWY 15/501 00004544 Lewis, Tyler M 3344 US HWY 15/501
Carthage, NC 28327 potable 290 / E Well behind house to northwestern
corner. No municipal water available.
WSW-2 159 Muse Road 00005182 Phillips, John F 159 Muse Road
Carthage, NC 28327 potable 1,171 / ENE Well on southen side of house.
WSW-3 3323 US HWY 15/501 99000508 Faircloth, Stanley R Jr.3323 US HWY 15/501
Carthage, NC 28327 potable 620 / SE
Owner said there is no municipal water.
Well is visible in yard. Confirmed by
Town of Carthage.
WSW-6 489 Union Church Road 00006919 Whitaker, Linda H 489 Union Church Road
Carthage, NC 28327 inactive 1,313 / S
Per Linda Whitaker only municipal
water is used. Confirmed by Town of
Carthage.
WSW-7 491 Union Church Road 00002265 Flinchum, Lawrence A 491 Union Church Road
Carthage, NC 28327 inactive 1,203 / S On municpal water per resident.
Confirmed by Town of Carthage.
WSW-8 832 Stage Road 00001130 Frye, Robin A 832 Stage Road
Carthage, NC 28327 potable 1,157 / S Well visible on property, assumed
potable.
WSW-9 820 Stage Road 00006678 Roybal, Robert H 820 Stage Road
Carthage, NC 28327 potable 1,311 / S Well visible on property, assumed
potable.
WSW-10 790 Stage Road 20070574 Tyner, Robert A 790 Stage Road
Carthage, NC 28327 potable 1,332 / SSE According to Town of Carthage, no
municipal water provided to property.
WSW-16 3520 US HWY 15/501 00001452 Cockman, Richard J 3520 US HWY 15/501
Carthage, NC 28327 potable 1,430 / WSW Historical records indicate well at
parcel. No municipal water available.
WSW-17 3263 US HWY 15/501 00002035 Dutton, Tammy 3363 US HWY 15/501
Carthage, NC 28327 potable 1,075 / ESE Wellhouse visible from driveway to
western side of property.
WSW-19 3229 US HWY 15/501 95000724 Dutton, Jeremy C 3229 US HWY 15/501
Carthage, NC 28327 potable 1,489 / ESE Well to the left of entry road to property.
WSW-20 784 Priest Hill Road 00004990 Sanders, Alecia 784 Priest Hill Road
Carthage, NC 28327 potable 1,440 / N No available municipal water.
WSW-21 815 Priest Hill Road 00005832 Milcendeau, Patrick;
Milcendeau, Jo F
5460 US HWY 1 N.
Vass, NC 28394 potable 971 / N Well spotted in front yard. Per Town of
Carthage, no municipal water available.
PUBLIC AND PRIVATE WATER SUPPLY WELL AND OTHER RECEPTOR INFORMATION
Incident Name and No.: NCDOT Carthage Road Oil Facility - 47245
NCDOT; 47254_Carthage Road Oil Facility; T2_Receptor Survey
CATLIN Project No. 220257
CATLIN Engineers and Scientists
April 2023
Page 2 of 2
TABLE 1
PUBLIC AND PRIVATE WATER SUPPLY WELL AND OTHER RECEPTOR INFORMATION
Incident Name and No.: NCDOT Carthage Road Oil Facility - 47245
Surface
Water Property Address Parcel
Number
Owner Name
(Last, First MI)
Owner Mailing
Address Comment
Pond #1 1020 Priest Hill Road 0004746 North Carolina State
Highway Commision
902 N Sandhills Blvd.,
Aberdeen, NC 28315 See Figure 2 for location
Pond #2 Union Church Road 00001713 Gulledge, William T PO Box 97
Vass, NC 28394 See Figure 2 for location
Pond #3 Priest Hill Road 00005832 Milcendeau, Patrick 5460 US HWY 1
Vass, NC 28394 See Figure 2 for location
NOTE: Information obtained from Town of Carthage Public works on April 27, 2021 and field survey conducted on January 13, 2021.
586 / NNE
Distance from Source
Area (ft.)
1,160 / WSW
1,264 / SW
NCDOT; 47254_Carthage Road Oil Facility; T2_Receptor Survey
CATLIN Project No. 220257
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 2
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B & EPA METHOD 625.1
Incident Name and No.: NCDOT Carthage Road Oil Facility - 47245
625.1
Well
ID
Sample
ID
Date
Collected
11/23/2021 6.5 1.5 4.4 <2.0 1.2 4.1 30.3 5.7 63.2 BRL BRL
7/19/2022 8.4 1.3 5.9 3.6 1.2 4.9 44.6 8.9 91.6 BRL NA
11/23/2021 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.50 BRL BRL
7/19/2022 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.50 BRL NA
11/23/2021 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.50 BRL BRL
7/19/2022 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.50 BRL NA
WSW-1 WSW-1 3/16/2023 <0.18 <0.22 <0.15 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BRL BRL
All results in micrograms per liter (µg/L).
BRL = Below Reporting Limit
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than reporting limit or detection limit
EPA = Environmental Protection Agency
SM = Standard Method
NA = Not Analyzed
24,100
400
50,000
500
Varies
Varies
Varies
VariesTotal XylenesAll other SM 6200B AnalytesAll EPA Method 625.1 Analytes28,500
400
Analytical Method SM 6200B
Contaminant of
Concern
BenzeneEthylbenzeneIsopropylbenzene (Cumene)n-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMW-01R MW-1R NaphthaleneGCL (µg/L)
2L GWQS (µg/L)
5,000
1
MW-3 MW-3
MW-05R MW-5R
260,000
600
80,000
600
30,500
70
26,100
70
6,000
6
NCDOT; 47254_Carthage Road Oil Facility; T5_GW Lab Results 6200B & 625.1
CATLIN Project No. 220257
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 3
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS - MADEP EPH & VPH
Incident Name and No.: NCDOT Carthage Road Oil Facility - 47245
Well
ID
Sample
ID
Date
Collected
11/23/2021 <100 <100 <100 606 210 118 606 <310*<100 <218*
7/19/2022 NA NA NA 865 273 209 865 N/A N/A N/A
11/23/2021 <100 <100 <100 <50.0 <50.0 <50.0 <50.0 <150.0 <100 <150.0
7/19/2022 NA NA NA <50.0 <50.0 <50.0 <50.0 N/A N/A N/A
11/23/2021 <100 322 <100 <50.0 <50.0 <50.0 <50.0 <150.0 322 <150.0
7/19/2022 NA NA NA <50.0 <50.0 <50.0 <50.0 N/A N/A N/A
WSW-1 WSW-1 3/16/2023 NA NA NA <100 <100 <100 <100 N/A N/A N/A
All results in micrograms per liter (µg/L).
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than reporting limit
* = The value represents the sum of the reported practical quantitation limit of one analyte and the detected concentration of the other analyte
MADEP = Massachusetts Department of Environmental Protection
EPH = Extractable Petroleum Hydrocarbons
VPH = Volatile Petroleum Hydrocarbons
NE = Not Established
NA= Not Analyzed
N/A = Not Applicable C9-C22 AromaticsAnalytical Method MADEP EPH MADEP VPH Combined EPH & VPH Fractions
Contaminant of
Concern
C9-C18 AliphaticsC19-C36 AliphaticsC11-C22 AromaticsC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsNE
200
GCL (µg/L)
2L GWQS (µg/L)
NE
700
NE
10,000
NE
200
NE
400
NE
700
NE
200
NE
400
NE
700
NE
10,000
MW-01R MW-1R
MW-3 MW-3
MW-05R MW-5R
NCDOT; 47254_Carthage Road Oil Facility; T6_GW Lab Results MADEP
CATLIN Project No. 220257
CATLIN Engineers and Scientists
April 2023

NCDOT; 47245_NCDOT Carthage Road Oil Facility CATLIN Engineers and Scientists
CATLIN Project No. 220257 April 2023

ATTACHMENT C

LABORATORY ANALYTICAL DATA AND CHAIN-OF-CUSTODY DOCUMENTATION
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 24, 2023
Sean O’Neil
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
Project Location: Carthage, NC
Client Job Number:
Project Number: 220257
Laboratory Work Order Number: 23C1954
Enclosed are results of analyses for samples as received by the laboratory on March 17, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 6
23C1954-01 6
Sample Preparation Information 11
QC Data 12
Volatile Organic Compounds by GC/MS 12
B334676 12
Semivolatile Organic Compounds by - GC/MS 16
B334530 16
Petroleum Hydrocarbons Analyses - VPH 20
B334595 20
Flag/Qualifier Summary 22
Certifications 23
Chain of Custody/Sample Receipt 27
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/24/2023
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
ATTN: Sean O’Neil
220257
23C1954
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Carthage, NC
230316-5
WSW-1 23C1954-01 Ground Water 625.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-23 6200B
[TOC_1]Sample Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only adjusted hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
625.1
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2-Chloronaphthalene
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1
Benzidine
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1
Benzyl alcohol
B334530-BLK1, B334530-BS1, B334530-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Benzidine
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1, S084768-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Benzidine
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1, S084768-CCV1
Benzyl alcohol
B334530-BLK1, B334530-BS1, B334530-BSD1, S084768-CCV2
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
N-Nitrosodimethylamine
23C1954-01[WSW-1], B334530-BLK1, B334530-BS1, B334530-BSD1, S084768-CCV1
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/17/2023
Work Order: 23C1954Sample Description:Project Location: Carthage, NC
Sample ID: 23C1954-01
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 3/16/2023 14:55
[TOC_2]23C1954-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/21/23 11:41 MFFg/L2.0 3/21/23SM21-23 6200B1Acetone
ND 0.50 3/21/23 11:41 MFFg/L0.18 3/21/23SM21-23 6200B1Benzene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B1Bromobenzene
ND 0.50 3/21/23 11:41 MFFg/L0.28 3/21/23SM21-23 6200B1Bromochloromethane
ND 0.50 3/21/23 11:41 MFFg/L0.16 3/21/23SM21-23 6200B1Bromodichloromethane
ND 0.50 3/21/23 11:41 MFFg/L0.41 3/21/23SM21-23 6200B1Bromoform
ND 2.0 3/21/23 11:41 MFFg/L1.3 3/21/23SM21-23 6200B1Bromomethane
ND 5.0 3/21/23 11:41 MFFg/L1.7 3/21/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B1n-Butylbenzene
ND 0.50 3/21/23 11:41 MFFg/L0.13 3/21/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 3/21/23 11:41 MFFg/L0.16 3/21/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 3/21/23 11:41 MFFg/L0.12 3/21/23SM21-23 6200B1Chlorobenzene
ND 50 3/21/23 11:41 MFFg/L20 3/21/23SM21-23 6200B1Ethanol
ND 0.50 3/21/23 11:41 MFFg/L0.20 3/21/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 3/21/23 11:41 MFFg/L0.34 3/21/23SM21-23 6200B1Chloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B1Chloroform
ND 0.60 3/21/23 11:41 MFFg/L0.50 3/21/23SM21-23 6200B1Chloromethane
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B12-Chlorotoluene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B14-Chlorotoluene
ND 0.50 3/21/23 11:41 MFFg/L0.16 3/21/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/21/23 11:41 MFFg/L0.13 3/21/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 3/21/23 11:41 MFFg/L0.13 3/21/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 3/21/23 11:41 MFFg/L0.16 3/21/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B11,1-Dichloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.30 3/21/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/21/23 11:41 MFFg/L0.17 3/21/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/21/23 11:41 MFFg/L0.19 3/21/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 3/21/23 11:41 MFFg/L0.12 3/21/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 3/21/23 11:41 MFFg/L0.35 3/21/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 3/21/23 11:41 MFFg/L0.16 3/21/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 3/21/23 11:41 MFFg/L0.20 3/21/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/21/23 11:41 MFFg/L0.22 3/21/23SM21-23 6200B1Ethylbenzene
ND 5.0 3/21/23 11:41 MFFg/L1.2 3/21/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/21/23 11:41 MFFg/L0.13 3/21/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/21/23 11:41 MFFg/L0.17 3/21/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/21/23 11:41 MFFg/L0.18 3/21/23SM21-23 6200B1Methylene Chloride
ND 5.0 3/21/23 11:41 MFFg/L1.3 3/21/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/17/2023
Work Order: 23C1954Sample Description:Project Location: Carthage, NC
Sample ID: 23C1954-01
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 3/16/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/21/23 11:41 MFFg/L0.38 3/21/23SM21-23 6200B1Naphthalene
ND 0.50 3/21/23 11:41 MFFg/L0.12 3/21/23SM21-23 6200B1n-Propylbenzene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B1Styrene
ND 0.50 3/21/23 11:41 MFFg/L0.14 3/21/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.17 3/21/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 3/21/23 11:41 MFFg/L0.22 3/21/23SM21-23 6200B1Toluene
ND 1.0 3/21/23 11:41 MFFg/L0.34 3/21/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 1.0 3/21/23 11:41 MFFg/L0.30 3/21/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.19 3/21/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 3/21/23 11:41 MFFg/L0.17 3/21/23SM21-23 6200B1Trichloroethylene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/21/23 11:41 MFFg/L0.28 3/21/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 3/21/23 11:41 MFFg/L0.20 3/21/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 3/21/23 11:41 MFFg/L0.15 3/21/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 3/21/23 11:41 MFFg/L1.7 3/21/23SM21-23 6200B1Vinyl Acetate
ND 0.50 3/21/23 11:41 MFFg/L0.24 3/21/23SM21-23 6200B1Vinyl Chloride
ND 1.0 3/21/23 11:41 MFFg/L0.49 3/21/23SM21-23 6200B1m+p Xylene
ND 0.50 3/21/23 11:41 MFFg/L0.24 3/21/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 113 3/21/23 11:4170-130
Toluene-d8 103 3/21/23 11:4170-130
4-Bromofluorobenzene 93.1 3/21/23 11:4170-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/17/2023
Work Order: 23C1954Sample Description:Project Location: Carthage, NC
Sample ID: 23C1954-01
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 3/16/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.530 4.93 3/20/23 15:23 AR2g/L0.530 3/17/23625.11Acenaphthene
<0.551 4.93 3/20/23 15:23 AR2g/L0.551 3/17/23625.11Acenaphthylene
<0.490 4.93 3/20/23 15:23 AR2g/L0.490 3/17/23625.11Anthracene
<10.2 19.7 3/20/23 15:23 AR2g/L10.2 3/17/23625.11L-04, R-05, V-04,
V-05
Benzidine
<0.454 4.93 3/20/23 15:23 AR2g/L0.454 3/17/23625.11Benzo(a)anthracene
<0.688 4.93 3/20/23 15:23 AR2g/L0.688 3/17/23625.11Benzo(a)pyrene
<0.539 4.93 3/20/23 15:23 AR2g/L0.539 3/17/23625.11Benzo(b)fluoranthene
<0.670 4.93 3/20/23 15:23 AR2g/L0.670 3/17/23625.11Benzo(g,h,i)perylene
<0.622 4.93 3/20/23 15:23 AR2g/L0.622 3/17/23625.11Benzo(k)fluoranthene
<0.517 9.85 3/20/23 15:23 AR2g/L0.517 3/17/23625.114-Bromophenylphenylether
<0.650 9.85 3/20/23 15:23 AR2g/L0.650 3/17/23625.11Butylbenzylphthalate
<0.515 9.85 3/20/23 15:23 AR2g/L0.515 3/17/23625.114-Chloro-3-methylphenol
<0.418 9.85 3/20/23 15:23 AR2g/L0.418 3/17/23625.11Bis(2-chloroethoxy)methane
<0.488 9.85 3/20/23 15:23 AR2g/L0.488 3/17/23625.11Bis(2-chloroethyl)ether
<0.633 9.85 3/20/23 15:23 AR2g/L0.633 3/17/23625.11Bis(2-chloroisopropyl)ether
<0.513 9.85 3/20/23 15:23 AR2g/L0.513 3/17/23625.11L-042-Chloronaphthalene
<0.450 9.85 3/20/23 15:23 AR2g/L0.450 3/17/23625.112-Chlorophenol
<0.543 9.85 3/20/23 15:23 AR2g/L0.543 3/17/23625.114-Chlorophenylphenylether
<0.438 4.93 3/20/23 15:23 AR2g/L0.438 3/17/23625.11Chrysene
<0.729 4.93 3/20/23 15:23 AR2g/L0.729 3/17/23625.11Dibenz(a,h)anthracene
<0.486 9.85 3/20/23 15:23 AR2g/L0.486 3/17/23625.11Di-n-butylphthalate
<0.631 4.93 3/20/23 15:23 AR2g/L0.631 3/17/23625.111,3-Dichlorobenzene
<0.613 4.93 3/20/23 15:23 AR2g/L0.613 3/17/23625.111,4-Dichlorobenzene
<0.628 4.93 3/20/23 15:23 AR2g/L0.628 3/17/23625.111,2-Dichlorobenzene
<0.768 9.85 3/20/23 15:23 AR2g/L0.768 3/17/23625.113,3-Dichlorobenzidine
<0.484 9.85 3/20/23 15:23 AR2g/L0.484 3/17/23625.112,4-Dichlorophenol
<0.409 9.85 3/20/23 15:23 AR2g/L0.409 3/17/23625.11Diethylphthalate
<0.497 9.85 3/20/23 15:23 AR2g/L0.497 3/17/23625.112,4-Dimethylphenol
<0.379 9.85 3/20/23 15:23 AR2g/L0.379 3/17/23625.11Dimethylphthalate
<8.38 9.85 3/20/23 15:23 AR2g/L8.38 3/17/23625.114,6-Dinitro-2-methylphenol
<8.34 9.85 3/20/23 15:23 AR2g/L8.34 3/17/23625.112,4-Dinitrophenol
<0.663 9.85 3/20/23 15:23 AR2g/L0.663 3/17/23625.112,4-Dinitrotoluene
<0.554 9.85 3/20/23 15:23 AR2g/L0.554 3/17/23625.112,6-Dinitrotoluene
<3.07 9.85 3/20/23 15:23 AR2g/L3.07 3/17/23625.11Di-n-octylphthalate
<0.563 9.85 3/20/23 15:23 AR2g/L0.563 3/17/23625.111,2-Diphenylhydrazine/Azobenzene
<0.825 9.85 3/20/23 15:23 AR2g/L0.825 3/17/23625.11Bis(2-Ethylhexyl)phthalate
<0.473 4.93 3/20/23 15:23 AR2g/L0.473 3/17/23625.11Fluoranthene
<0.531 4.93 3/20/23 15:23 AR2g/L0.531 3/17/23625.11Fluorene
<0.574 9.85 3/20/23 15:23 AR2g/L0.574 3/17/23625.11Hexachlorobenzene
<0.736 9.85 3/20/23 15:23 AR2g/L0.736 3/17/23625.11Hexachlorobutadiene
<5.88 9.85 3/20/23 15:23 AR2g/L5.88 3/17/23625.11Hexachlorocyclopentadiene
<0.706 9.85 3/20/23 15:23 AR2g/L0.706 3/17/23625.11Hexachloroethane
<0.773 4.93 3/20/23 15:23 AR2g/L0.773 3/17/23625.11Indeno(1,2,3-cd)pyrene
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/17/2023
Work Order: 23C1954Sample Description:Project Location: Carthage, NC
Sample ID: 23C1954-01
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 3/16/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
<0.510 9.85 3/20/23 15:23 AR2g/L0.510 3/17/23625.11Isophorone
<0.588 4.93 3/20/23 15:23 AR2g/L0.588 3/17/23625.11Naphthalene
<0.571 9.85 3/20/23 15:23 AR2g/L0.571 3/17/23625.11Nitrobenzene
<0.505 9.85 3/20/23 15:23 AR2g/L0.505 3/17/23625.112-Nitrophenol
<1.90 9.85 3/20/23 15:23 AR2g/L1.90 3/17/23625.114-Nitrophenol
<0.558 9.85 3/20/23 15:23 AR2g/L0.558 3/17/23625.11V-06N-Nitrosodimethylamine
<0.427 9.85 3/20/23 15:23 AR2g/L0.427 3/17/23625.11N-Nitrosodiphenylamine/Diphenylamine
<0.566 9.85 3/20/23 15:23 AR2g/L0.566 3/17/23625.11N-Nitrosodi-n-propylamine
<0.657 9.85 3/20/23 15:23 AR2g/L0.657 3/17/23625.11Pentachlorophenol
<0.665 4.93 3/20/23 15:23 AR2g/L0.665 3/17/23625.112-Methylnaphthalene
<0.506 4.93 3/20/23 15:23 AR2g/L0.506 3/17/23625.11Phenanthrene
<0.481 9.85 3/20/23 15:23 AR2g/L0.481 3/17/23625.112-Methylphenol
<0.188 9.85 3/20/23 15:23 AR2g/L0.188 3/17/23625.11Phenol
<0.428 19.7 3/20/23 15:23 AR2g/L0.428 3/17/23625.113/4-Methylphenol
<0.646 4.93 3/20/23 15:23 AR2g/L0.646 3/17/23625.11Pyrene
<0.653 4.93 3/20/23 15:23 AR2g/L0.653 3/17/23625.111,2,4-Trichlorobenzene
<0.464 9.85 3/20/23 15:23 AR2g/L0.464 3/17/23625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 33.2 3/20/23 15:2315-110
Phenol-d6 24.8 3/20/23 15:2315-110
Nitrobenzene-d5 65.3 3/20/23 15:2330-130
2-Fluorobiphenyl 65.6 3/20/23 15:2330-130
2,4,6-Tribromophenol 76.9 3/20/23 15:2315-110
p-Terphenyl-d14 81.2 3/20/23 15:2330-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/17/2023
Work Order: 23C1954Sample Description:Project Location: Carthage, NC
Sample ID: 23C1954-01
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 3/16/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 3/20/23 17:17 EEHg/L 3/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 3/20/23 17:17 EEHg/L 3/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 3/20/23 17:17 EEHg/L 3/17/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)91.7 3/20/23 17:1770-130
2,5-Dibromotoluene (PID)91.6 3/20/23 17:1770-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3510C Analytical Method: 625.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B334530 03/17/231020 1.0023C1954-01 [WSW-1]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B334595 03/17/235 5.0023C1954-01 [WSW-1]
Prep Method: SW-846 5030B Analytical Method: SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B334676 03/21/235 5.0023C1954-01 [WSW-1]
[TOC_1]Sample Preparation Information[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B334676 - SW-846 5030B
[TOC_3]B334676[TOC]
Blank (B334676-BLK1) Prepared & Analyzed: 03/21/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B334676 - SW-846 5030B
Blank (B334676-BLK1) Prepared & Analyzed: 03/21/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11528.7
g/L 25.0 70-130Surrogate: Toluene-d8 10225.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.223.8
LCS (B334676-BS1) Prepared & Analyzed: 03/21/23
Acetone g/L50 200 70-130107214
Benzene g/L0.50 20.0 70-13010821.6
Bromobenzene g/L0.50 20.0 70-13010120.2
Bromochloromethane g/L0.50 20.0 70-13012124.2
Bromodichloromethane g/L0.50 20.0 70-13010220.5
Bromoform g/L0.50 20.0 70-13077.115.4
Bromomethane g/L2.0 20.0 60-14090.418.1
2-Butanone (MEK)g/L5.0 200 70-130113226
n-Butylbenzene g/L0.50 20.0 70-13010420.9
sec-Butylbenzene g/L0.50 20.0 70-13010821.6
tert-Butylbenzene g/L0.50 20.0 70-13010020.1
Carbon Tetrachloride g/L0.50 20.0 70-13098.919.8
Chlorobenzene g/L0.50 20.0 70-13098.219.6
Ethanol g/L50 200 70-130105209
Chlorodibromomethane g/L0.50 20.0 70-13088.417.7
Chloroethane g/L0.50 20.0 60-14090.418.1
Chloroform g/L0.50 20.0 70-13010521.0
Chloromethane g/L0.60 20.0 60-14077.515.5
2-Chlorotoluene g/L0.50 20.0 70-13097.019.4
4-Chlorotoluene g/L0.50 20.0 70-13099.319.9
1,2-Dibromoethane (EDB)g/L0.50 20.0 70-13097.419.5
1,2-Dichlorobenzene g/L0.50 20.0 70-13010120.2
1,3-Dichlorobenzene g/L0.50 20.0 70-13010420.8
1,4-Dichlorobenzene g/L0.50 20.0 70-13098.819.8
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 60-14011923.9
1,1-Dichloroethane g/L0.50 20.0 70-13010921.7
1,2-Dichloroethane g/L0.50 20.0 70-13010821.5
1,1-Dichloroethylene g/L0.50 20.0 70-13011422.8
cis-1,2-Dichloroethylene g/L0.50 20.0 70-13011122.1
trans-1,2-Dichloroethylene g/L0.50 20.0 70-13010220.4
1,2-Dichloropropane g/L0.50 20.0 70-13010621.2
1,3-Dichloropropane g/L0.50 20.0 70-13010120.2
2,2-Dichloropropane g/L0.50 20.0 70-13010921.8
1,1-Dichloropropene g/L0.50 20.0 70-13010420.7
cis-1,3-Dichloropropene g/L0.50 20.0 70-13010520.9
trans-1,3-Dichloropropene g/L0.50 20.0 70-13011222.5
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B334676 - SW-846 5030B
LCS (B334676-BS1) Prepared & Analyzed: 03/21/23
Diisopropyl Ether (DIPE)g/L0.50 20.0 70-13012224.4
Ethylbenzene g/L0.50 20.0 70-13010320.7
2-Hexanone (MBK)g/L5.0 200 70-13097.8196
Isopropylbenzene (Cumene)g/L0.50 20.0 70-13010020.1
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 70-13010521.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 70-13097.019.4
Methylene Chloride g/L5.0 20.0 70-13011022.0
4-Methyl-2-pentanone (MIBK)g/L5.0 200 70-13098.5197
Naphthalene g/L0.50 20.0 70-13085.817.2
n-Propylbenzene g/L0.50 20.0 70-13010320.6
Styrene g/L0.50 20.0 70-13099.019.8
1,1,2,2-Tetrachloroethane g/L0.50 20.0 70-13089.617.9
Tetrachloroethylene g/L0.50 20.0 70-13010120.1
Toluene g/L0.50 20.0 70-13010220.3
1,2,3-Trichlorobenzene g/L1.0 20.0 70-13093.618.7
1,2,4-Trichlorobenzene g/L0.50 20.0 70-13010320.6
1,1,1-Trichloroethane g/L0.50 20.0 70-13010621.2
1,1,2-Trichloroethane g/L0.50 20.0 70-13010020.1
Trichloroethylene g/L0.50 20.0 70-13010220.4
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 70-13010921.8
1,2,3-Trichloropropane g/L0.50 20.0 70-13011022.0
1,2,4-Trimethylbenzene g/L0.50 20.0 70-13098.619.7
1,3,5-Trimethylbenzene g/L0.50 20.0 70-13097.319.5
Vinyl Acetate g/L20 200 70-13096.0192
Vinyl Chloride g/L0.50 20.0 60-14010621.1
m+p Xylene g/L1.0 40.0 70-13010040.2
o-Xylene g/L0.50 20.0 70-13010120.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11428.4
g/L 25.0 70-130Surrogate: Toluene-d8 10325.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.523.9
LCS Dup (B334676-BSD1) Prepared & Analyzed: 03/21/23
Acetone g/L50 200 2570-130101 5.35203
Benzene g/L0.50 20.0 2570-130108 0.092321.7
Bromobenzene g/L0.50 20.0 2570-13097.6 3.2819.5
Bromochloromethane g/L0.50 20.0 2570-130122 0.61724.4
Bromodichloromethane g/L0.50 20.0 2570-130102 0.048820.5
Bromoform g/L0.50 20.0 2570-13076.2 1.2415.2
Bromomethane g/L2.0 20.0 2560-140101 10.820.2
2-Butanone (MEK)g/L5.0 200 2570-130106 6.22213
n-Butylbenzene g/L0.50 20.0 2570-130105 1.0521.1
sec-Butylbenzene g/L0.50 20.0 2570-130112 3.8622.5
tert-Butylbenzene g/L0.50 20.0 2570-130103 2.8520.6
Carbon Tetrachloride g/L0.50 20.0 2570-13096.0 3.0319.2
Chlorobenzene g/L0.50 20.0 2570-13098.6 0.35619.7
Ethanol g/L50 200 2570-130125 18.0251
Chlorodibromomethane g/L0.50 20.0 2570-13090.6 2.4018.1
Chloroethane g/L0.50 20.0 2560-14091.0 0.66218.2
Chloroform g/L0.50 20.0 2570-130107 2.1321.4
Chloromethane g/L0.60 20.0 2560-14083.8 7.8716.8
2-Chlorotoluene g/L0.50 20.0 2570-13096.0 0.93319.2
4-Chlorotoluene g/L0.50 20.0 2570-13099.8 0.50220.0
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B334676 - SW-846 5030B
LCS Dup (B334676-BSD1) Prepared & Analyzed: 03/21/23
1,2-Dibromoethane (EDB)g/L0.50 20.0 2570-13098.4 1.0219.7
1,2-Dichlorobenzene g/L0.50 20.0 2570-130105 3.6520.9
1,3-Dichlorobenzene g/L0.50 20.0 2570-130106 2.0421.3
1,4-Dichlorobenzene g/L0.50 20.0 2570-13099.2 0.35319.8
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 2560-140118 1.3523.6
1,1-Dichloroethane g/L0.50 20.0 2570-130107 1.1621.5
1,2-Dichloroethane g/L0.50 20.0 2570-130107 0.55921.4
1,1-Dichloroethylene g/L0.50 20.0 2570-130110 3.0822.1
cis-1,2-Dichloroethylene g/L0.50 20.0 2570-130112 1.4422.4
trans-1,2-Dichloroethylene g/L0.50 20.0 2570-130101 1.0320.2
1,2-Dichloropropane g/L0.50 20.0 2570-130107 1.1721.5
1,3-Dichloropropane g/L0.50 20.0 2570-130101 0.24820.2
2,2-Dichloropropane g/L0.50 20.0 2570-130111 1.5522.1
1,1-Dichloropropene g/L0.50 20.0 2570-130105 1.5821.0
cis-1,3-Dichloropropene g/L0.50 20.0 2570-130105 0.095620.9
trans-1,3-Dichloropropene g/L0.50 20.0 2570-130108 4.0421.6
Diisopropyl Ether (DIPE)g/L0.50 20.0 2570-130123 0.77624.6
Ethylbenzene g/L0.50 20.0 2570-130104 0.67520.8
2-Hexanone (MBK)g/L5.0 200 2570-13090.8 7.43182
Isopropylbenzene (Cumene)g/L0.50 20.0 2570-13099.8 0.69920.0
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 2570-130105 0.23721.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 2570-13094.6 2.5118.9
Methylene Chloride g/L5.0 20.0 2570-130110 0.63622.1
4-Methyl-2-pentanone (MIBK)g/L5.0 200 2570-13095.7 2.88191
Naphthalene g/L0.50 20.0 2570-13089.2 3.9417.8
n-Propylbenzene g/L0.50 20.0 2570-130103 0.19420.7
Styrene g/L0.50 20.0 2570-13099.7 0.75519.9
1,1,2,2-Tetrachloroethane g/L0.50 20.0 2570-13090.4 0.94418.1
Tetrachloroethylene g/L0.50 20.0 2570-130103 2.5020.6
Toluene g/L0.50 20.0 2570-130101 0.49320.2
1,2,3-Trichlorobenzene g/L1.0 20.0 2570-130100 6.9620.1
1,2,4-Trichlorobenzene g/L0.50 20.0 2570-130106 2.9221.2
1,1,1-Trichloroethane g/L0.50 20.0 2570-130104 2.3420.7
1,1,2-Trichloroethane g/L0.50 20.0 2570-13099.8 0.69920.0
Trichloroethylene g/L0.50 20.0 2570-13099.0 3.0819.8
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 2570-130106 2.7021.2
1,2,3-Trichloropropane g/L0.50 20.0 2570-130106 3.4321.2
1,2,4-Trimethylbenzene g/L0.50 20.0 2570-13099.6 1.0119.9
1,3,5-Trimethylbenzene g/L0.50 20.0 2570-13097.6 0.35919.5
Vinyl Acetate g/L20 200 2570-13093.1 3.02186
Vinyl Chloride g/L0.50 20.0 2560-140105 0.14221.1
m+p Xylene g/L1.0 40.0 2570-130100 0.22440.1
o-Xylene g/L0.50 20.0 2570-13099.7 1.7419.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11228.1
g/L 25.0 70-130Surrogate: Toluene-d8 10426.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.224.3
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by - GC/MS[TOC]
Batch B334530 - SW-846 3510C
[TOC_3]B334530[TOC]
Blank (B334530-BLK1) Prepared: 03/17/23 Analyzed: 03/20/23
Benzyl alcohol g/L10.0 L-04, V-05ND
Acenaphthene g/L5.00ND
Acenaphthylene g/L5.00ND
Anthracene g/L5.00ND
Benzidine g/L20.0 L-04, R-05, V-04,
V-05
ND
Benzo(a)anthracene g/L5.00ND
Benzo(a)pyrene g/L5.00ND
Benzo(b)fluoranthene g/L5.00ND
Benzo(g,h,i)perylene g/L5.00ND
Benzo(k)fluoranthene g/L5.00ND
4-Bromophenylphenylether g/L10.0ND
Butylbenzylphthalate g/L10.0ND
4-Chloro-3-methylphenol g/L10.0ND
Bis(2-chloroethoxy)methane g/L10.0ND
Bis(2-chloroethyl)ether g/L10.0ND
Bis(2-chloroisopropyl)ether g/L10.0ND
2-Chloronaphthalene g/L10.0 L-04ND
2-Chlorophenol g/L10.0ND
4-Chlorophenylphenylether g/L10.0ND
Chrysene g/L5.00ND
Dibenz(a,h)anthracene g/L5.00ND
Di-n-butylphthalate g/L10.0ND
1,3-Dichlorobenzene g/L5.00ND
1,4-Dichlorobenzene g/L5.00ND
1,2-Dichlorobenzene g/L5.00ND
3,3-Dichlorobenzidine g/L10.0ND
2,4-Dichlorophenol g/L10.0ND
Diethylphthalate g/L10.0ND
2,4-Dimethylphenol g/L10.0ND
Dimethylphthalate g/L10.0ND
4,6-Dinitro-2-methylphenol g/L10.0ND
2,4-Dinitrophenol g/L10.0ND
2,4-Dinitrotoluene g/L10.0ND
2,6-Dinitrotoluene g/L10.0ND
Di-n-octylphthalate g/L10.0ND
1,2-Diphenylhydrazine/Azobenzene g/L10.0ND
Bis(2-Ethylhexyl)phthalate g/L10.0ND
Fluoranthene g/L5.00ND
Fluorene g/L5.00ND
Hexachlorobenzene g/L10.0ND
Hexachlorobutadiene g/L10.0ND
Hexachlorocyclopentadiene g/L10.0ND
Hexachloroethane g/L10.0ND
Indeno(1,2,3-cd)pyrene g/L5.00ND
Isophorone g/L10.0ND
Naphthalene g/L5.00ND
Nitrobenzene g/L10.0ND
2-Nitrophenol g/L10.0ND
4-Nitrophenol g/L10.0ND
N-Nitrosodimethylamine g/L10.0 V-06ND
N-Nitrosodiphenylamine/Diphenylamine g/L10.0ND
N-Nitrosodi-n-propylamine g/L10.0ND
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B334530 - SW-846 3510C
Blank (B334530-BLK1) Prepared: 03/17/23 Analyzed: 03/20/23
Pentachlorophenol g/L10.0ND
2-Methylnaphthalene g/L5.00ND
Phenanthrene g/L5.00ND
2-Methylphenol g/L10.0ND
Phenol g/L10.0ND
3/4-Methylphenol g/L20.0ND
Pyrene g/L5.00ND
1,2,4-Trichlorobenzene g/L5.00ND
2,4,6-Trichlorophenol g/L10.0ND
g/L 200 15-110Surrogate: 2-Fluorophenol 34.168.2
g/L 200 15-110Surrogate: Phenol-d6 25.250.5
g/L 100 30-130Surrogate: Nitrobenzene-d5 70.170.1
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 71.271.2
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 84.3169
g/L 100 30-130Surrogate: p-Terphenyl-d14 87.287.2
LCS (B334530-BS1) Prepared: 03/17/23 Analyzed: 03/20/23
Benzyl alcohol g/L10.0 50.0 L-04, V-0566.833.4
Acenaphthene g/L5.00 50.0 47-14571.235.6
Acenaphthylene g/L5.00 50.0 33-14567.333.6
Anthracene g/L5.00 50.0 27-13375.037.5
Benzidine g/L0.00 50.0 L-04, R-05, V-04,
V-05
40-140*ND
Benzo(a)anthracene g/L5.00 50.0 33-14372.636.3
Benzo(a)pyrene g/L5.00 50.0 17-16369.134.5
Benzo(b)fluoranthene g/L5.00 50.0 24-15974.337.1
Benzo(g,h,i)perylene g/L5.00 50.0 10-21988.944.4
Benzo(k)fluoranthene g/L5.00 50.0 11-16277.939.0
4-Bromophenylphenylether g/L10.0 50.0 53-12766.333.1
Butylbenzylphthalate g/L10.0 50.0 10-15269.935.0
4-Chloro-3-methylphenol g/L10.0 50.0 22-14767.133.6
Bis(2-chloroethoxy)methane g/L10.0 50.0 33-18465.332.6
Bis(2-chloroethyl)ether g/L10.0 50.0 12-15871.535.7
Bis(2-chloroisopropyl)ether g/L10.0 50.0 36-16688.544.3
2-Chloronaphthalene g/L10.0 50.0 L-0460-12056.8 *28.4
2-Chlorophenol g/L10.0 50.0 23-13459.329.7
4-Chlorophenylphenylether g/L10.0 50.0 25-15870.035.0
Chrysene g/L5.00 50.0 17-16871.535.8
Dibenz(a,h)anthracene g/L5.00 50.0 10-22778.539.3
Di-n-butylphthalate g/L10.0 50.0 10-12075.537.8
1,3-Dichlorobenzene g/L5.00 50.0 10-17248.224.1
1,4-Dichlorobenzene g/L5.00 50.0 20-12449.424.7
1,2-Dichlorobenzene g/L5.00 50.0 32-12954.727.4
3,3-Dichlorobenzidine g/L10.0 50.0 10-26261.130.5
2,4-Dichlorophenol g/L10.0 50.0 39-13564.032.0
Diethylphthalate g/L10.0 50.0 10-12074.937.4
2,4-Dimethylphenol g/L10.0 50.0 32-12068.434.2
Dimethylphthalate g/L10.0 50.0 10-12069.634.8
4,6-Dinitro-2-methylphenol g/L10.0 50.0 10-18196.248.1
2,4-Dinitrophenol g/L10.0 50.0 10-19110150.6
2,4-Dinitrotoluene g/L10.0 50.0 39-13991.745.8
2,6-Dinitrotoluene g/L10.0 50.0 50-15885.542.7
Di-n-octylphthalate g/L10.0 50.0 4-14663.231.6
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B334530 - SW-846 3510C
LCS (B334530-BS1) Prepared: 03/17/23 Analyzed: 03/20/23
1,2-Diphenylhydrazine/Azobenzene g/L10.0 50.0 40-14072.436.2
Bis(2-Ethylhexyl)phthalate g/L10.0 50.0 8-15867.433.7
Fluoranthene g/L5.00 50.0 26-13777.838.9
Fluorene g/L5.00 50.0 59-12174.637.3
Hexachlorobenzene g/L10.0 50.0 10-15272.436.2
Hexachlorobutadiene g/L10.0 50.0 24-12049.124.5
Hexachlorocyclopentadiene g/L10.0 50.0 40-14060.430.2
Hexachloroethane g/L10.0 50.0 40-12051.725.9
Indeno(1,2,3-cd)pyrene g/L5.00 50.0 10-17180.540.2
Isophorone g/L10.0 50.0 21-19674.737.3
Naphthalene g/L5.00 50.0 21-13363.731.9
Nitrobenzene g/L10.0 50.0 35-18073.336.6
2-Nitrophenol g/L10.0 50.0 29-18269.734.8
4-Nitrophenol g/L10.0 50.0 10-13269.534.8
N-Nitrosodimethylamine g/L10.0 50.0 V-0640-14051.125.5
N-Nitrosodiphenylamine/Diphenylamine g/L10.0 50.0 40-14071.035.5
N-Nitrosodi-n-propylamine g/L10.0 50.0 10-23075.537.7
Pentachlorophenol g/L10.0 50.0 14-17669.834.9
2-Methylnaphthalene g/L5.00 50.0 40-14057.328.7
Phenanthrene g/L5.00 50.0 54-12073.936.9
2-Methylphenol g/L10.0 50.0 40-14063.731.9
Phenol g/L10.0 50.0 5-12048.724.4
3/4-Methylphenol g/L20.0 50.0 40-14069.734.9
Pyrene g/L5.00 50.0 52-12083.841.9
1,2,4-Trichlorobenzene g/L5.00 50.0 44-14255.627.8
2,4,6-Trichlorophenol g/L10.0 50.0 37-14469.334.7
g/L 200 15-110Surrogate: 2-Fluorophenol 56.4113
g/L 200 15-110Surrogate: Phenol-d6 48.697.1
g/L 100 30-130Surrogate: Nitrobenzene-d5 81.881.8
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 75.475.4
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 89.0178
g/L 100 30-130Surrogate: p-Terphenyl-d14 90.990.9
LCS Dup (B334530-BSD1) Prepared: 03/17/23 Analyzed: 03/20/23
Benzyl alcohol g/L10.0 50.0 20 L-04, V-0565.8 1.5132.9
Acenaphthene g/L5.00 50.0 4847-14573.9 3.6736.9
Acenaphthylene g/L5.00 50.0 7433-14571.5 6.0335.7
Anthracene g/L5.00 50.0 6627-13377.0 2.5838.5
Benzidine g/L0.00 50.0 30 L-04, R-05, V-04,
V-05
40-1406.50 200**3.25
Benzo(a)anthracene g/L5.00 50.0 5333-14373.8 1.6736.9
Benzo(a)pyrene g/L5.00 50.0 7217-16370.2 1.6135.1
Benzo(b)fluoranthene g/L5.00 50.0 7124-15974.4 0.13537.2
Benzo(g,h,i)perylene g/L5.00 50.0 9710-21983.5 6.2941.7
Benzo(k)fluoranthene g/L5.00 50.0 6311-16277.2 0.90238.6
4-Bromophenylphenylether g/L10.0 50.0 4353-12768.7 3.5634.3
Butylbenzylphthalate g/L10.0 50.0 6010-15278.2 11.239.1
4-Chloro-3-methylphenol g/L10.0 50.0 7322-14777.6 14.538.8
Bis(2-chloroethoxy)methane g/L10.0 50.0 5433-18467.1 2.7233.5
Bis(2-chloroethyl)ether g/L10.0 50.0 10812-15871.4 0.084035.7
Bis(2-chloroisopropyl)ether g/L10.0 50.0 7636-16681.3 8.5540.6
2-Chloronaphthalene g/L10.0 50.0 24 L-0460-12056.9 0.106*28.4
2-Chlorophenol g/L10.0 50.0 6123-13458.1 2.0429.1
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B334530 - SW-846 3510C
LCS Dup (B334530-BSD1) Prepared: 03/17/23 Analyzed: 03/20/23
4-Chlorophenylphenylether g/L10.0 50.0 6125-15870.3 0.48535.2
Chrysene g/L5.00 50.0 8717-16872.2 1.0036.1
Dibenz(a,h)anthracene g/L5.00 50.0 12610-22777.4 1.5138.7
Di-n-butylphthalate g/L10.0 50.0 4710-12074.7 1.1437.3
1,3-Dichlorobenzene g/L5.00 50.0 3010-17251.8 7.3225.9
1,4-Dichlorobenzene g/L5.00 50.0 3020-12454.2 9.3127.1
1,2-Dichlorobenzene g/L5.00 50.0 3032-12956.6 3.4528.3
3,3-Dichlorobenzidine g/L10.0 50.0 10810-26273.7 18.736.8
2,4-Dichlorophenol g/L10.0 50.0 5039-13570.1 9.0735.0
Diethylphthalate g/L10.0 50.0 10010-12077.0 2.7938.5
2,4-Dimethylphenol g/L10.0 50.0 5832-12069.0 0.90334.5
Dimethylphthalate g/L10.0 50.0 18310-12073.8 5.9436.9
4,6-Dinitro-2-methylphenol g/L10.0 50.0 20310-181103 6.6951.4
2,4-Dinitrophenol g/L10.0 50.0 13210-191105 3.5152.4
2,4-Dinitrotoluene g/L10.0 50.0 4239-13992.4 0.76146.2
2,6-Dinitrotoluene g/L10.0 50.0 4850-15888.3 3.2044.1
Di-n-octylphthalate g/L10.0 50.0 694-14659.9 5.3930.0
1,2-Diphenylhydrazine/Azobenzene g/L10.0 50.0 3040-14081.9 12.341.0
Bis(2-Ethylhexyl)phthalate g/L10.0 50.0 828-15868.3 1.3034.1
Fluoranthene g/L5.00 50.0 6626-13780.4 3.3640.2
Fluorene g/L5.00 50.0 3859-12176.5 2.4638.2
Hexachlorobenzene g/L10.0 50.0 5510-15276.6 5.5938.3
Hexachlorobutadiene g/L10.0 50.0 6224-12059.7 19.629.9
Hexachlorocyclopentadiene g/L10.0 50.0 3040-14061.0 1.0230.5
Hexachloroethane g/L10.0 50.0 5240-12055.0 6.0427.5
Indeno(1,2,3-cd)pyrene g/L5.00 50.0 9910-17177.9 3.2639.0
Isophorone g/L10.0 50.0 9321-19679.9 6.8140.0
Naphthalene g/L5.00 50.0 6521-13366.1 3.7033.1
Nitrobenzene g/L10.0 50.0 6235-18079.0 7.4939.5
2-Nitrophenol g/L10.0 50.0 5529-18271.5 2.6335.8
4-Nitrophenol g/L10.0 50.0 13110-13248.5 35.724.2
N-Nitrosodimethylamine g/L10.0 50.0 30 V-0640-14054.1 5.8227.1
N-Nitrosodiphenylamine/Diphenylamine g/L10.0 50.0 3040-14075.0 5.5337.5
N-Nitrosodi-n-propylamine g/L10.0 50.0 8710-23072.4 4.1136.2
Pentachlorophenol g/L10.0 50.0 8614-17671.4 2.1835.7
2-Methylnaphthalene g/L5.00 50.0 3040-14068.3 17.434.1
Phenanthrene g/L5.00 50.0 3954-12075.2 1.8237.6
2-Methylphenol g/L10.0 50.0 3040-14054.7 15.227.4
Phenol g/L10.0 50.0 645-12030.2 46.815.1
3/4-Methylphenol g/L20.0 50.0 3040-14059.0 16.829.5
Pyrene g/L5.00 50.0 4952-12082.1 2.0541.0
1,2,4-Trichlorobenzene g/L5.00 50.0 5044-14261.3 9.6230.6
2,4,6-Trichlorophenol g/L10.0 50.0 5837-14469.4 0.057734.7
g/L 200 15-110Surrogate: 2-Fluorophenol 38.877.5
g/L 200 15-110Surrogate: Phenol-d6 29.559.0
g/L 100 30-130Surrogate: Nitrobenzene-d5 85.985.9
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 74.974.9
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 85.8172
g/L 100 30-130Surrogate: p-Terphenyl-d14 92.892.8
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B334595 - MA VPH
[TOC_3]B334595[TOC]
Blank (B334595-BLK1) Prepared & Analyzed: 03/20/23
C5-C8 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)80.432.2
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)80.732.3
LCS (B334595-BS1) Prepared & Analyzed: 03/20/23
C9-C10 Aromatics g/L100 50.0 70-13099.950.0
Benzene g/L1.0 50.0 70-13010250.9
Butylcyclohexane g/L1.0 50.0 70-13010954.3
Decane g/L1.0 50.0 70-13081.040.5
Ethylbenzene g/L1.0 50.0 70-13010250.9
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 70-13010251.0
2-Methylpentane g/L1.0 50.0 70-13010552.6
Naphthalene g/L5.0 50.0 70-13089.444.7
Nonane g/L1.0 50.0 70-13010954.7
Pentane g/L1.0 50.0 70-13010351.4
Toluene g/L1.0 50.0 70-13010150.6
1,2,4-Trimethylbenzene g/L1.0 50.0 70-13099.950.0
2,2,4-Trimethylpentane g/L1.0 50.0 70-13092.646.3
m+p Xylene g/L2.0 100 70-130102102
o-Xylene g/L1.0 50.0 70-13010351.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)97.839.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)99.940.0
LCS Dup (B334595-BSD1) Prepared & Analyzed: 03/20/23
C9-C10 Aromatics g/L100 50.0 2570-130102 1.6650.8
Benzene g/L1.0 50.0 2570-130104 2.2852.1
Butylcyclohexane g/L1.0 50.0 2570-130109 0.13154.3
Decane g/L1.0 50.0 2570-13081.2 0.22240.6
Ethylbenzene g/L1.0 50.0 2570-130104 2.0151.9
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 2570-130103 0.56351.3
2-Methylpentane g/L1.0 50.0 2570-130107 1.2853.3
Naphthalene g/L5.0 50.0 2570-13088.6 0.84344.3
Nonane g/L1.0 50.0 2570-130110 0.18354.8
Pentane g/L1.0 50.0 2570-130106 2.8452.8
Toluene g/L1.0 50.0 2570-130103 1.6951.4
1,2,4-Trimethylbenzene g/L1.0 50.0 2570-130102 1.6650.8
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B334595 - MA VPH
LCS Dup (B334595-BSD1) Prepared & Analyzed: 03/20/23
2,2,4-Trimethylpentane g/L1.0 50.0 2570-13093.4 0.86746.7
m+p Xylene g/L2.0 100 2570-130104 1.93104
o-Xylene g/L1.0 50.0 2570-130105 2.2552.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.937.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)94.337.7
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
[TOC_1]Flag/Qualifier Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthene
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthylene
CT,MA,NH,NY,NC,RI,ME,VAAnthracene
CT,MA,NH,NY,NC,RI,ME,VABenzidine
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)anthracene
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)pyrene
CT,MA,NH,NY,NC,RI,ME,VABenzo(b)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VABenzo(g,h,i)perylene
CT,MA,NH,NY,NC,RI,ME,VABenzo(k)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VA4-Bromophenylphenylether
CT,MA,NH,NY,NC,RI,ME,VAButylbenzylphthalate
CT,MA,NH,NY,NC,RI,VA4-Chloro-3-methylphenol
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethoxy)methane
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethyl)ether
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroisopropyl)ether
CT,MA,NH,NY,NC,RI,ME,VA2-Chloronaphthalene
CT,MA,NH,NY,NC,RI,ME,VA2-Chlorophenol
CT,MA,NH,NY,NC,RI,ME,VA4-Chlorophenylphenylether
CT,MA,NH,NY,NC,RI,ME,VAChrysene
CT,MA,NH,NY,NC,RI,ME,VADibenz(a,h)anthracene
CT,MA,NH,NY,NC,RI,ME,VADi-n-butylphthalate
MA,NC1,3-Dichlorobenzene
MA,NC1,4-Dichlorobenzene
MA,NC1,2-Dichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA3,3-Dichlorobenzidine
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dichlorophenol
CT,MA,NH,NY,NC,RI,ME,VADiethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dimethylphenol
CT,MA,NH,NY,NC,RI,ME,VADimethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA4,6-Dinitro-2-methylphenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrophenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VA2,6-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VADi-n-octylphthalate
NC1,2-Diphenylhydrazine/Azobenzene
CT,MA,NH,NY,NC,RI,ME,VABis(2-Ethylhexyl)phthalate
CT,MA,NH,NY,NC,RI,ME,VAFluoranthene
CT,MA,NH,NY,NC,RI,ME,VAFluorene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobenzene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobutadiene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorocyclopentadiene
CT,MA,NH,NY,NC,RI,ME,VAHexachloroethane
CT,MA,NH,NY,NC,RI,ME,VAIndeno(1,2,3-cd)pyrene
CT,MA,NH,NY,NC,RI,ME,VAIsophorone
CT,MA,NH,NY,NC,RI,ME,VANaphthalene
CT,MA,NH,NY,NC,RI,ME,VANitrobenzene
CT,MA,NH,NY,NC,RI,ME,VA2-Nitrophenol
[TOC_1]Certifications[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VA4-Nitrophenol
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodimethylamine
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodi-n-propylamine
CT,MA,NH,NY,NC,RI,ME,VAPentachlorophenol
NY,NC2-Methylnaphthalene
CT,MA,NH,NY,NC,RI,ME,VAPhenanthrene
NY,NC2-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPhenol
NY,NC3/4-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPyrene
CT,MA,NH,NY,NC,RI,ME,VA1,2,4-Trichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
M-MA100Massachusetts DEPMA 06/30/2023
PH-0821Connecticut Department of Public HealthCT 12/31/2024
10899 NELAPNew York State Department of HealthNY 04/1/2023
2516 NELAPNew Hampshire Environmental LabNH 02/5/2024
LAO00373Rhode Island Department of HealthRI 12/30/2023
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
460217Commonwealth of VirginiaVA 12/14/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023