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GROUND WATER MONITORING REPORT
JUNE 2017
HAN-DEE HUGO #5
1210 NORTH MAIN STREET
BLADENBORO, BLADEN COUNTY
FACILITY ID NO. 0-023752
GROUNDWATER INCIDENT NO. 29175
GRI PROJECT NO. 3142
Prepared For:
Sampson-Bladen Oil Company, Inc.
Post Office 160
Elizabethtown, North Carolina 28337
Prepared by:
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
(704) 845-4010
August 14, 2017
Holden McClenney Rae Troiano Brown, P.G.
Staff Scientist Project Manager
704.698.1254
EXECUTIVE SUMMARY
Han-Dee Hugo #5 is located at 1210 North Main Street in Bladenboro, Bladen County, North Carolina.
The site is currently an active petroleum retail facility and convenience store. Three 8,000-gallon
gasoline USTs, one 8,000-gallon fuel oil, one 8,000-gallon diesel, and one 2,000-gallon kerosene USTs
are in use at the site.
A release at the site was discovered during Environmental Site Assessment activities. Contaminated soil
was discovered during site renovations in May and June 2012. A total of 2,162.49 tons of soil was
removed from the site.
The site is ranked as high risk because one potable water supply well (WSW-7) was identified within
1,000-radius of the site. Another water supply well (WSW-10) was identified within a 1,500-foot radius
of the subject site. Three irrigation wells (WSW-1, WSW-2, and WSW-5) were confirmed within 1,000
feet of the site. There are no water supply wells within 250 feet of the site. Municipal water is available
to all properties in the area. A well abandonment agreement was sent to the owner of WSW-7 who
denied abandoning her well and connecting to municipal water.
On June 6, 2017, GRI personnel installed five Type II monitoring wells at the site to assess the Gross
Contaminant Level plume in the vicinity of MW-11. On June 20, 2017, five Type II monitoring wells
and one Type III monitoring well were gauged, purged, and sampled. Free product was not measured in
any monitoring well during the June 2017 sampling event. Concentrations of individual BTEX
constituents, MTBE, naphthalene and/or di-isopropyl ether that exceeded the maximum allowable
concentrations specified in T15A NCAC 2L.0202 were reported in the ground water samples collected
from MW-14, MW-15, MW-16, MW-17 and MW-18. None of the report contaminant concentrations
exceeded GCLs.
Based on this information, the site risk classification should remain high risk due to GCL concentrations.
GRI recommends conducting a ground water assessment in six months to include nutrient analysis.
Subsequent to the assessment, a corrective action feasibility study should be conducted for the site.
TABLE OF CONTENTS
1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1
3.0 GROUND WATER SAMPLING ACTIVITIES ......................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 2
5.0 LIMITATIONS .............................................................................................................................. 3
FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Water Quality Map
TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: Laboratory Report – Ground Water Samples
Appendix B: Monitoring Well Construction Records
1
1.0 SITE HISTORY AND CHARACTERIZATION
Han-Dee Hugo #5 is located at 1210 North Main Street in Bladenboro, Bladen County, North Carolina
(Figure 1). The site is currently an active petroleum retail facility and convenience store. Three 8,000-
gallon gasoline, one 8,000-gallon fuel oil, one 8,000-gallon diesel, and one 2,000-gallon kerosene USTs
are in use at the site.
According to the Phase II Limited Site Assessment (LSA) Report (April 25, 2005) submitted by CBM
Environmental Services, Inc., a release at the site was discovered during Environmental Site Assessment
activities. Four shallow monitoring wells (MW-1 through MW-4) and one deep monitoring well (TW-1)
were installed during LSA activities. Contaminated soil was discovered during site renovations in May
and June 2012. A total of 2,162.49 tons of soil was removed from the site. GRI submitted an Initial
Action Abatement Report on August 27, 2012. In December 2012 and January 2013, during the
Comprehensive Site Assessment (CSA), monitoring wells MW-1R, MW-2R, MW-4R, MW-5 through
MW-13, and TW-1R were installed. The CSA report was submitted by GRI in May 2013. Monitoring
wells MW-14 through MW-18 were installed on June 6, 2017.
The site is ranked as high risk because one potable water supply well (WSW-7) was identified within
1,000-radius of the site. Another water supply well (WSW-10) was identified within a 1,500-foot radius
of the subject site. Three irrigation wells (WSW-1, WSW-2, and WSW-5) were confirmed within 1,000
feet of the site. There are no water supply wells within 250 feet of the site. Municipal water is available
to all properties in the area. In October 2013, a well abandonment agreement was sent to the owner of
WSW-7 who denied abandoning her well and connecting to municipal water. Site Vicinity Map showing
the locations of water supply wells is included as Figure 2. A Site Map showing the locations of the
monitoring wells and the structures on-site and on surrounding properties has been included as Figure 3.
In addition, concentrations of benzene and MTBE reported in MW-11 have exceeded the gross
contaminant levels (GCLs) since 2013.
2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water sampling activities conducted at the
site. The activities were conducted in accordance with GRI Proposal Number 17-337 which was
submitted to the NCDEQ on May 23, 2017, and approved as Task Authorization Number 29175-9 on
June 15, 2017. The current scope of work includes obtaining current ground water quality data for the
GLC plume assessment in the vicinity of MW-11.
2
3.0 MONITORING WELL INSTALLATION
On June 6, 2017, GRI personnel installed five Type II monitoring wells (MW-14 through MW-18) to a
total depth of fifteen feet below ground surface utilizing a mobile drill rig with six inch solid stem augers.
Locations of the monitoring wells are shown on Figure 3. A summary of well construction information
is presented in Table 1. Well installation records are included in Appendix A.
4.0 GROUND WATER SAMPLING ACTIVITIES
4.1 Site Hydrogeology
On June 20, 2017, monitoring wells MW-14 through MW-18 were gauged, purged and/or sampled. The
depths to ground water in the Type II monitoring wells during the June 2017 sampling event ranged from
5.61 to 6.36 feet below the tops of well casings. Ground water elevations in the newly installed Type II
monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from
95.73 to 96.40 feet. The locations of the monitoring wells are shown on Figure 3. A Water Table
Surface Map based on data obtained from the Type II wells in June 2017 is included as Figure 4. A
summary of well construction and gauging information is presented in Table 1.
4.2 Ground Water Sampling
Laboratory analyses were performed on the ground water samples collected from the monitoring wells
and water supply well during the June 2017 sampling event for volatile organic compounds by EPA
Method 602.
Concentrations of individual BTEX constituents, MTBE, naphthalene and/or di-isopropyl ether that
exceeded the maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were
reported in the ground water samples collected from MW-14, MW-15, MW-16, MW-17 and MW-18.
None of the reported contaminant concentrations exceeded the GCLs. A Ground Water Quality Map
based on data from the June 20, 2017, sampling event has been included as Figure 5. A summary of
ground water sampling analytical results is presented in Table 2. A complete laboratory report has been
included in Appendix B.
5.0 CONCLUSIONS AND RECOMMENDATIONS
In July 2017, five monitoring wells (MW-14 through MW-18) were installed in the vicinity of
MW-11 in order to assess the GCL plume.
Concentrations of individual BTEX constituents, MTBE, naphthalene and/or di-isopropyl ether
that exceeded the MACs were reported in the ground water samples collected from MW-14,
3
MW-15, MW-16, MW-17 and MW-18.
None of the reported contaminant concentrations exceeded the GCLs.
Based on this information, the site risk classification should remain high risk due to GCL
concentrations. GRI recommends conducting a ground water assessment in six months to
include nutrient analysis. Subsequent to the assessment, a corrective action feasibility study
should be conducted for the site.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Sampson-Bladen Oil Company, Inc. for specific
application to the referenced site in Bladen County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by the NCDEQ and with resources adequate only
for that scope of work. Our findings have been developed in accordance with generally accepted
standards of geology and hydrogeology practices in the State of North Carolina, available information,
and our professional judgment. No other warranty is expressed or implied.
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
FIGURES
"J
"J
"J
"J
!H !H
!H
DJ
DJ
DJ
SITE
WSW-4
WSW-2WSW-1
WSW-8
WSW-5
WSW-10WSW-9
WSW-7
WSW-6
WSW-3 026918412138
026919518241
026919519908
026900335297
026918421198
026918416682
026900510413
026919510613
026918317226
026918419103
026919501759
026918328376
026919504833
026900329557
026900510546
026919513035
026919520174
MAIN STSUNSET PARK RDINDUSTRIAL DR
CDR FRANK ELKINS MEMORIAL HWY
RONALD BRITT RDNC 131 HWYJ R BRITT RDTODD BRITT CTTULIP DRHOLLY BRITT CTS A N D S L N
N C 24 2 H W YWateree CreekFIGURE 2: SITE VICINITY MAPHANDEE HUGO #51210 N. MAIN STREETBLADENBORO, BLADEN COUNTYNORTH CAROLINAINCIDENT NO. 29175GRI PROJECT NO. 3142
PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 3, 2012
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
LEGEND
DJ Water Supply Well (Abandoned)
!H Irrigation Well
"J Water Supply Well
Hydrography
centerlines
Parcels
026918416682 PIN Number
TABLES
Date: 07/28/1704/04/05 3.35 --- 96.6505/30/12 3.10 --- 96.9001/04/13 2.30 --- 97.7009/23/13 4.49 --- 95.5109/27/13 4.90 --- 95.1010/28/13 5.90 --- 94.1006/10/14 3.01 --- 96.9912/15/14 3.77 --- 96.2306/16/15 3.94 --- 96.0603/13/17 3.11 --- 96.8904/04/05 6.35 --- 97.0305/30/12 NM --- NMMW-1R 100.00155 - 15DestroyedDestroyed103.382 2 - 12 12100.00MW-1MW-22 2 - 1202/25/0503/10/0512Top of Casing Elevation (ft.)01/02/13WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)5TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)Page 1 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)01/04/13 5.68 --- 96.5309/23/13 6.46 --- 95.7509/27/13 6.80 --- 95.4110/28/13 8.03 --- 94.1806/10/14 4.34 --- 97.8712/15/14 6.36 --- 95.8506/16/15 6.16 --- 96.0503/13/17 5.80 --- 96.4104/04/05 5.70 --- 97.4505/30/12 5.46 --- 97.6901/04/13 5.08 --- 96.7810/28/13 6.75 --- 95.1106/10/14 4.58 --- 97.2812/15/14 5.68 --- 96.1806/16/15 5.31 --- 96.5503/13/17 5.27 --- 96.5904/04/05 5.68 --- 96.7105/30/12 4.60 --- 97.79101.86144 - 14403/31/05102.21155 - 15512/20/12MW-2RMW-3Destroyed102.3903/31/05 144 - 144MW-4103.15Page 2 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)01/04/13 4.74 --- 96.8609/23/13 5.38 --- 96.22 Before MMPE09/27/13 9.75 --- 91.85 After MMPE10/28/13 6.96 --- 94.6404/28/14 3.71 --- 97.89 Before MMPE05/02/14 6.51 --- 95.09 After MMPE06/10/14 4.62 --- 96.9811/10/14 6.05 --- 95.55 Before MMPE11/14/14 7.34 --- 94.26 After MMPE12/15/14 5.62 --- 95.9806/16/15 5.28 --- 96.3203/13/17 4.98 --- 96.6201/04/13 4.28 --- 97.2710/28/13 7.73 --- 93.8206/10/14 4.31 --- 97.2412/15/14 5.24 --- 96.3106/16/15 4.81 --- 96.74MW-4RMW-5 12/20/12 5 5 - 15 15155 - 15512/20/12101.55101.60Page 3 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)01/04/13 5.28 --- 96.5510/28/13 7.89 --- 93.9406/10/14 4.45 --- 97.3812/15/14 5.81 --- 96.0206/16/15 5.39 --- 96.4401/04/13 2.92 --- 97.0810/28/13 5.88 --- 94.1206/10/14 3.23 --- 96.7712/15/14 3.86 --- 96.1406/16/15 3.86 --- 96.1403/13/17 3.23 --- 96.7701/04/13 3.24 --- 97.0210/28/13 6.21 --- 94.0506/10/14 3.78 --- 96.4812/15/14 4.26 --- 96.0006/16/15 4.55 --- 95.7103/13/17 4.01 --- 96.25100.26155 - 15512/20/12MW-8101.83155 - 155MW-6 12/20/12 2 2 - 12 1212/20/12MW-7 100.00Page 4 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)01/04/13 1.85 --- 97.5210/28/13 5.19 --- 94.1806/10/14 2.87 --- 96.5012/15/14 3.19 --- 96.1806/16/15 3.53 --- 95.8403/13/17 1.89 --- 97.4801/04/13 2.00 --- 97.3210/28/13 5.24 --- 94.0806/10/14 2.72 --- 96.6012/15/14 NM --- NM06/16/15 3.49 --- 95.8303/13/17 2.71 --- 96.6199.3215MW-95 - 15512/20/12MW-1099.37155 - 15512/20/12Page 5 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)01/04/13 5.30 --- 96.8909/23/13 7.03 --- 95.16 Before MMPE09/27/13 10.90 --- 91.29 After MMPE10/28/13 8.44 --- 93.7504/28/14 5.14 --- 97.05 Before MMPE05/02/14 9.31 --- 92.88 After MMPE06/10/14 5.85 --- 96.3411/10/14 7.43 --- 94.76 Before MMPE11/14/14 9.92 --- 92.27 After MMPE12/15/14 6.51 --- 95.6806/16/15 6.73 --- 95.4603/13/17 6.15 --- 96.0401/04/13 0.88 --- 98.0710/28/13 5.14 --- 93.8106/10/14 2.18 --- 96.7712/15/14 2.98 --- 95.9706/16/15 3.13 --- 95.8201/04/13 1.68 --- 98.3110/28/13 5.39 --- 94.6006/10/14 2.83 --- 97.1612/15/14 3.43 --- 96.5606/16/15 3.24 --- 96.75102.19155 - 15512/20/12MW-117 98.95MW-13 12/20/12 2 2 - 7 7 99.99MW-12 12/20/12 2 2 - 7Page 6 of 7
Date: 07/28/17Top of Casing Elevation (ft.)WellInstallationDate(mm/dd/yy)CommentsGroundWaterElevation (ft.)TABLE 1WELL CONSTRUCTION AND GAUGING INFORMATIONHAN-DEE HUGO #5 (INCIDENT NO. 29175)Facility ID # : 0-023752Well IDDateWaterLevelMeasured(mm/dd/yy)WellCasingDepth(ft. BGS)Screened Interval (x to y ft. BGS)Bottomof Well(ft. BGS)Depth toWater fromTop of Casing(feet)Free Product Thickness (ft.)MW-14 07/06/17 07/20/17 5 5-15 15 101.91 6.09 --- 95.82MW-15 07/06/17 07/20/17 5 5-15 15 102.09 6.36 --- 95.73MW-16 07/06/17 07/20/17 5 5-15 15 102.37 6.34 --- 96.03MW-17 07/06/17 07/20/17 5 5-15 15 102.39 5.99 --- 96.40MW-18 07/06/17 07/20/17 5 5-15 15 101.85 5.61 --- 96.2404/04/05 7.77 --- 95.6405/30/12 NM --- NM10/28/13 9.81 --- 93.6001/04/13 6.68 --- 95.1806/10/14 7.29 --- 94.5712/15/14 8.09 --- 93.7706/16/15 8.28 --- 93.5803/13/17 6.26 --- 95.60Notes:• NA: Data not available.• NM: Not Measured.• Top of Casing information obtained from report titled 'Phase II LSA', dated 2005by CBM Environmental Services, Inc. • Well construction details obtained from historical well logs.01/03/13TW-1R 101.864843 - 4843Destroyed103.41• ft BGS : feet below ground surface.03/31/05TW-1 4843 - 4843Page 7 of 7
Date: 07/31/17
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70
5,000 260,000 84,500 85,500 20,000 6,000 70,000
02/28/05 1.2 0.44 J 3.7 0.43 J 60 6.6 NR
05/30/12 <0.13 0.21 J 0.88 0.47 J 12.2 29.7 1.1
01/04/13 84.5 323 32.5 215 2.1 16.8 0.20 J
10/28/13 0.65 0.49 J 7.8 1.5 7.8 38.8 1.4
06/10/14 37.5 1.7 3.5 24.5 1.9 0.65 0.52
12/15/14 <0.10 0.17 J 0.79 0.30 J 1.8 2.1 0.35 J
06/17/15 162 127 24.8 192 4.5 30.8 <0.80
03/13/17 0.33 J 0.35 J 3.0 2.0 2.8 78.6 0.34 J
MW-2 03/15/05 330 370 130 390 4,500 8.1 J NR
01/04/13 38.4 0.93 1.3 6.5 292 57.0 1.3
10/28/13 25.6 1.8 1.1 J 4.1 104 57.1 0.54 J
06/10/14 21.6 8.6 1.9 2.7 149 48.6 0.66
12/15/14 14.9 0.72 0.61 1.0 J 93.2 39.9 0.43 J
06/16/15 12.6 1.4 0.63 1.4 J 97.6 35.9 0.44 J
03/13/17 2.3 0.28 J 0.24 J 0.39 J 46.0 30.9 0.26 J
04/05/05 3.2 9 2.0 8.5 450 13 NR
05/30/12 0.56 0.20 J <0.15 0.33 J 120 8.8 0.79
01/04/13 1.8 0.25 J 0.13 J 0.35 J 95.9 5.4 1.5
10/28/13 0.72 <0.10 <0.10 <0.22 54.1 3.7 0.7
06/10/14 0.54 <0.10 <0.10 <0.20 49.1 4.7 0.85
12/15/14 <0.10 <0.10 <0.10 <0.20 13.8 2.3 0.27 J
06/17/15 <0.17 <0.17 <0.15 <0.43 <0.16 0.24 J <0.16
03/13/17 <0.13 0.13 J <0.13 <0.25 7.9 1.5 <0.13
04/05/05 6,500 2,100 2,000 10,400 140,000 520 NR
05/30/12 12,000 33,300 1,410 16,500 409,000 776 9,810
01/04/13 1,430 1,480 166 1,100 27,500 67.2 J 696
10/28/13 2,200 2,300 512 2,009 7,130 119 1,240
06/10/14 624 572 157 494 1,800 46.6 455
12/15/14 1,190 300 205 187 5,990 45.9 509
06/17/15 1,370 141 249 336 774 54.8 979
03/13/17 587 22.00 49.0 40.1 74.8 69.9 598
01/04/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10
10/28/13 <0.10 <0.10 <0.10 <0.22 0.29 J <0.15 <0.10
06/10/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 0.45 J <0.15 <0.43 20.4 3.7 0.34 J
01/04/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
06/10/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16
01/04/13 <0.10 <0.10 <0.10 <0.22 1.5 1.3 <0.10
10/28/13 239 2.7 22.4 11.4 10.4 0.27 J 2
06/10/14 17.1 0.28 J 2.4 2.8 3.4 0.42 J 0.62
12/15/14 22.0 <0.10 2 0.81 J 7.3 1.3 1.8
06/17/15 9.3 <0.17 2.1 10.1 2.4 0.86 0.66
03/13/17 8.2 <0.13 0.16 J 0.26 J 1.6 0.78 0.34 J
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
10/28/13 0.29 J <0.10 <0.10 <0.22 3.3 0.70 0.16 J
06/10/14 6.3 <0.10 1.9 0.30 J 9.0 2.2 1.2
12/15/14 16.2 <0.10 2.7 0.80 J 10.0 6.5 1.7
06/17/15 9.4 <0.17 1.6 0.50 J 10.1 3.6 1.6
03/13/17 5.6 <0.13 1.4 0.38 J 8.7 2.6 1.4
EPA Method 6200B or EPA Method 602
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Analytical Method
Contaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneDi-isopropyl etherMW-6
2L Standard (µg/l)
GCL (µg/l)
MW-1
MW-1R
MW-3
MW-4
MW-4R
MW-5
Facility ID No. 0-023752
MW-7
MW-8
MW-2R
Page 1 of 2
Date: 07/31/17
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70
5,000 260,000 84,500 85,500 20,000 6,000 70,000
EPA Method 6200B or EPA Method 602
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Analytical Method
Contaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneDi-isopropyl ether2L Standard (µg/l)
GCL (µg/l)
Facility ID No. 0-023752
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
06/10/14 0.38 J <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 0.13 J <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16
03/13/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
06/10/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16
03/13/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13
01/04/13 8,470 34,900 2,830 15,200 75,400 392 4,470
10/28/13 12,300 42,300 1,870 11,100 52,700 230 J 4,820
06/10/14 15,800 52,600 3,210 19,700 65,900 505 6,430
12/15/14 4,830 23,400 1,780 8,730 23,900 307 1,910
06/17/15 15,400 57,100 3,450 19,300 66,300 518 6,280
03/13/17 14,200 69,000 3,520 19,600 45,200 374 J 4,680
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
10/28/13 <0.10 0.13 J <0.10 <0.22 <0.10 <0.15 <0.10
06/10/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10
10/28/13 <0.10 0.13 J <0.10 <0.22 0.15 J <0.15 <0.10
06/10/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10
06/17/15 <0.17 0.53 <0.15 <0.43 <0.16 <0.12 <0.16
MW-14 07/20/17 259 1,240 800 3,180 125 133 323
MW-15 07/20/17 1,080 6,260 1,950 10,000 256 440 119
MW-16 07/20/17 33.5 150 18.6 74.2 631 <2.5 32.9
MW-17 07/20/17 491 2,470 254 1,290 3,310 63.9 219
MW-18 07/20/17 304 454 340 1,210 23.1 151 206
TW-1 04/05/05 2.5 13 1.9 9.7 28 <1.0 NR
01/04/13 2.5 5.3 0.44 J 1.5 17.1 <0.15 1
10/28/13 <0.10 <0.10 <0.10 <0.22 0.44 J <0.15 <0.10
06/10/14 <0.10 0.20 J <0.10 <0.20 <0.10 <0.10 <0.10
12/15/14 <0.10 <0.10 <0.10 <0.20 0.29 J <0.10 <0.10
06/16/15 <0.17 <0.17 <0.15 <0.43 0.39 J <0.12 <0.16
03/13/17 <0.13 0.36 J <0.13 <0.25 <0.13 <0.13 <0.13
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• NR: Not Requested
• *: Refer to laboratory report
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no
standard has been established.
MW-13
TW-1R
MW-9
MW-10
MW-11
MW-12
Page 2 of 2
APPENDICES
APPENDIX A
Well Construction Records
APPENDIX B
Laboratory Report –Ground Water Samples
07/28/17
Technical Report for
GRI (Geological Resources Inc.)
Handee Hugo 5; 1210 N Main St, Bladenboro, NC
29175/3142
SGS Accutest Job Number: FA46038
Sampling Date: 07/20/17
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
rtb@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com;
jjr@geologicalresourcesinc.com; nml@geologicalresourcesinc.com
ATTN: Rae Brown
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Southeast 07/28/17
e-Hardcopy 2.0
Automated Report
21
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
1 of 21
FA46038
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA46038-1: MW-14 ......................................................................................................7
3.2: FA46038-2: MW-15 ......................................................................................................8
3.3: FA46038-3: MW-16 ......................................................................................................9
3.4: FA46038-4: MW-17 ......................................................................................................10
3.5: FA46038-5: MW-18 ......................................................................................................11
Section 4: Misc. Forms ............................................................................................................12
4.1: Chain of Custody ...........................................................................................................13
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................15
5.1: Method Blank Summary ................................................................................................16
5.2: Blank Spike Summary ...................................................................................................18
5.3: Matrix Spike Summary ..................................................................................................20
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................21 123452 of 21
FA46038
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA46038
Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Project No: 29175/3142
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA46038-1 07/20/17 08:38 ZC 07/21/17 AQ Ground Water MW-14
FA46038-2 07/20/17 08:31 ZC 07/21/17 AQ Ground Water MW-15
FA46038-3 07/20/17 09:03 ZC 07/21/17 AQ Ground Water MW-16
FA46038-4 07/20/17 08:55 ZC 07/21/17 AQ Ground Water MW-17
FA46038-5 07/20/17 08:48 ZC 07/21/17 AQ Ground Water MW-18
3 of 21
FA460381
Summary of Hits Page 1 of 2
Job Number:FA46038
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:07/20/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA46038-1 MW-14
Benzene 259 13 3.1 ug/l SM 6200B
Di-Isopropyl Ether 323 13 3.1 ug/l SM 6200B
Ethylbenzene 800 13 3.1 ug/l SM 6200B
Methyl Tert Butyl Ether 125 13 3.1 ug/l SM 6200B
Naphthalene 133 13 3.1 ug/l SM 6200B
Toluene 1240 13 3.1 ug/l SM 6200B
Xylene (total)3180 150 25 ug/l SM 6200B
FA46038-2 MW-15
Benzene 1080 25 6.3 ug/l SM 6200B
Di-Isopropyl Ether 119 25 6.3 ug/l SM 6200B
Ethylbenzene 1950 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether 256 25 6.3 ug/l SM 6200B
Naphthalene 440 25 6.3 ug/l SM 6200B
Toluene 6260 130 31 ug/l SM 6200B
Xylene (total)10000 380 63 ug/l SM 6200B
FA46038-3 MW-16
Benzene 33.5 10 2.5 ug/l SM 6200B
Di-Isopropyl Ether 32.9 10 2.5 ug/l SM 6200B
Ethylbenzene 18.6 10 2.5 ug/l SM 6200B
Methyl Tert Butyl Ether 631 10 2.5 ug/l SM 6200B
Toluene 150 10 2.5 ug/l SM 6200B
Xylene (total)74.2 30 5.0 ug/l SM 6200B
FA46038-4 MW-17
Benzene 491 50 13 ug/l SM 6200B
Di-Isopropyl Ether 219 50 13 ug/l SM 6200B
Ethylbenzene 254 50 13 ug/l SM 6200B
Methyl Tert Butyl Ether 3310 50 13 ug/l SM 6200B
Naphthalene 63.9 50 13 ug/l SM 6200B
Toluene 2470 50 13 ug/l SM 6200B
Xylene (total)1290 150 25 ug/l SM 6200B
FA46038-5 MW-18
Benzene 304 5.0 1.3 ug/l SM 6200B
Di-Isopropyl Ether 206 5.0 1.3 ug/l SM 6200B
Ethylbenzene 340 5.0 1.3 ug/l SM 6200B
Methyl Tert Butyl Ether 23.1 5.0 1.3 ug/l SM 6200B
4 of 21
FA460382
Summary of Hits Page 2 of 2
Job Number:FA46038
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:07/20/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 151 5.0 1.3 ug/l SM 6200B
Toluene 454 50 13 ug/l SM 6200B
Xylene (total)1210 150 25 ug/l SM 6200B
5 of 21
FA460382
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
6 of 21
FA460383
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-14
Lab Sample ID:FA46038-1 Date Sampled:07/20/17
Matrix:AQ - Ground Water Date Received:07/21/17
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E054090.D 25 07/26/17 18:03 TD n/a n/a VE1807
Run #2 E054024.D 100 07/24/17 17:39 TD n/a n/a VE1805
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 259 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
108-20-3 Di-Isopropyl Ether 323 13 3.1 ug/l
100-41-4 Ethylbenzene 800 13 3.1 ug/l
1634-04-4 Methyl Tert Butyl Ether 125 13 3.1 ug/l
91-20-3 Naphthalene 133 13 3.1 ug/l
108-88-3 Toluene 1240 13 3.1 ug/l
1330-20-7 Xylene (total)3180 a 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%101%70-130%
2037-26-5 Toluene-D8 106%105%70-130%
460-00-4 4-Bromofluorobenzene 104%105%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 21
FA4603833.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-15
Lab Sample ID:FA46038-2 Date Sampled:07/20/17
Matrix:AQ - Ground Water Date Received:07/21/17
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E054025.D 50 07/24/17 18:01 TD n/a n/a VE1805
Run #2 E054084.D 250 07/26/17 15:27 TD n/a n/a VE1807
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1080 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
108-20-3 Di-Isopropyl Ether 119 25 6.3 ug/l
100-41-4 Ethylbenzene 1950 25 6.3 ug/l
1634-04-4 Methyl Tert Butyl Ether 256 25 6.3 ug/l
91-20-3 Naphthalene 440 25 6.3 ug/l
108-88-3 Toluene 6260 a 130 31 ug/l
1330-20-7 Xylene (total)10000 a 380 63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%101%70-130%
2037-26-5 Toluene-D8 104%106%70-130%
460-00-4 4-Bromofluorobenzene 103%104%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 21
FA4603833.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-16
Lab Sample ID:FA46038-3 Date Sampled:07/20/17
Matrix:AQ - Ground Water Date Received:07/21/17
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E054094.D 20 07/26/17 19:33 TD n/a n/a VE1807
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 33.5 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
108-20-3 Di-Isopropyl Ether 32.9 10 2.5 ug/l
100-41-4 Ethylbenzene 18.6 10 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether 631 10 2.5 ug/l
91-20-3 Naphthalene ND 10 2.5 ug/l
108-88-3 Toluene 150 10 2.5 ug/l
1330-20-7 Xylene (total)74.2 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 21
FA4603833.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-17
Lab Sample ID:FA46038-4 Date Sampled:07/20/17
Matrix:AQ - Ground Water Date Received:07/21/17
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E054027.D 1 07/24/17 18:46 TD n/a n/a VE1805
Run #2 E054085.D 100 07/26/17 16:12 TD n/a n/a VE1807
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 491 a 50 13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether 219 a 50 13 ug/l
100-41-4 Ethylbenzene 254 a 50 13 ug/l
1634-04-4 Methyl Tert Butyl Ether 3310 a 50 13 ug/l
91-20-3 Naphthalene 63.9 a 50 13 ug/l
108-88-3 Toluene 2470 a 50 13 ug/l
1330-20-7 Xylene (total)1290 a 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 88%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%100%70-130%
2037-26-5 Toluene-D8 95%106%70-130%
460-00-4 4-Bromofluorobenzene 103%103%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 21
FA4603833.4
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-18
Lab Sample ID:FA46038-5 Date Sampled:07/20/17
Matrix:AQ - Ground Water Date Received:07/21/17
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E054089.D 10 07/26/17 17:41 TD n/a n/a VE1807
Run #2 E054028.D 100 07/24/17 19:08 TD n/a n/a VE1805
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 304 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
108-20-3 Di-Isopropyl Ether 206 5.0 1.3 ug/l
100-41-4 Ethylbenzene 340 5.0 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether 23.1 5.0 1.3 ug/l
91-20-3 Naphthalene 151 5.0 1.3 ug/l
108-88-3 Toluene 454 a 50 13 ug/l
1330-20-7 Xylene (total)1210 a 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%101%70-130%
2037-26-5 Toluene-D8 103%105%70-130%
460-00-4 4-Bromofluorobenzene 104%109%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 21
FA4603833.5
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
12 of 21
FA460384
FA46038: Chain of Custody
Page 1 of 2
13 of 21
FA4603844.1
Job Number:FA46038 Client:GRI
Date / Time Received:7/21/2017 9:30:00 AM Delivery Method:FX
Project:HAN DEE
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Accutest Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.8);
Cooler 1: (2.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH P.H Date:7/21/2017Date:7/21/2017 9:30:00 AM
FA46038: Chain of Custody
Page 2 of 2
14 of 21
FA4603844.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
15 of 21
FA460385
Method Blank Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1805-MB E054007.D 1 07/24/17 TD n/a n/a VE1805
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-4, FA46038-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
16 of 21
FA4603855.1.1
Method Blank Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1807-MB E054075.D 1 07/26/17 TD n/a n/a VE1807
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-3, FA46038-4, FA46038-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
17 of 21
FA4603855.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1805-BS E054020.D 1 07/24/17 TD n/a n/a VE1805
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-4, FA46038-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.7 107 70-130
108-90-7 Chlorobenzene 10 10.5 105 70-130
95-50-1 1,2-Dichlorobenzene 10 10.8 108 70-130
541-73-1 1,3-Dichlorobenzene 10 10.5 105 70-130
106-46-7 1,4-Dichlorobenzene 10 10.3 103 70-130
108-20-3 Di-Isopropyl Ether 10 11.1 111 70-130
100-41-4 Ethylbenzene 10 10.5 105 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.2 112 70-130
91-20-3 Naphthalene 10 9.9 99 70-130
108-88-3 Toluene 10 10.4 104 70-130
1330-20-7 Xylene (total)30 30.6 102 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
18 of 21
FA4603855.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1807-BS E054074.D 1 07/26/17 TD n/a n/a VE1807
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-3, FA46038-4, FA46038-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 7.5 75 70-130
108-90-7 Chlorobenzene 10 7.4 74 70-130
95-50-1 1,2-Dichlorobenzene 10 7.5 75 70-130
541-73-1 1,3-Dichlorobenzene 10 7.6 76 70-130
106-46-7 1,4-Dichlorobenzene 10 7.1 71 70-130
108-20-3 Di-Isopropyl Ether 10 7.3 73 70-130
100-41-4 Ethylbenzene 10 7.5 75 70-130
1634-04-4 Methyl Tert Butyl Ether 10 7.3 73 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
108-88-3 Toluene 10 7.6 76 70-130
1330-20-7 Xylene (total)30 22.3 74 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
19 of 21
FA4603855.2.2
Matrix Spike Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA46038-1MS E054032.D 100 07/24/17 TD n/a n/a VE1805
FA46038-1 E054024.D 100 07/24/17 TD n/a n/a VE1805
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-4, FA46038-5
FA46038-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 274 1000 1250 98 70-130
108-90-7 Chlorobenzene ND 1000 971 97 70-130
95-50-1 1,2-Dichlorobenzene ND 1000 936 94 70-130
541-73-1 1,3-Dichlorobenzene ND 1000 967 97 70-130
106-46-7 1,4-Dichlorobenzene ND 1000 936 94 70-130
108-20-3 Di-Isopropyl Ether 326 1000 1300 97 70-130
100-41-4 Ethylbenzene 742 1000 1760 102 70-130
1634-04-4 Methyl Tert Butyl Ether 127 1000 1070 94 70-130
91-20-3 Naphthalene 256 1000 956 70 70-130
108-88-3 Toluene 1150 1000 2140 99 70-130
1330-20-7 Xylene (total)3180 3000 6190 100 70-130
CAS No.Surrogate Recoveries MS FA46038-1 Limits
1868-53-7 Dibromofluoromethane 97%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%101%70-130%
2037-26-5 Toluene-D8 101%105%70-130%
460-00-4 4-Bromofluorobenzene 105%105%70-130%
* = Outside of Control Limits.
20 of 21
FA4603855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA46038
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA46086-1MS E054095.D 5 07/26/17 TD n/a n/a VE1807
FA46086-1MSD E054096.D 5 07/26/17 TD n/a n/a VE1807
FA46086-1 E054091.D 5 07/26/17 TD n/a n/a VE1807
The QC reported here applies to the following samples:Method: SM 6200B
FA46038-1, FA46038-2, FA46038-3, FA46038-4, FA46038-5
FA46086-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 45.7 91 50 46.7 93 2 70-130/20
108-90-7 Chlorobenzene ND 50 44.6 89 50 45.4 91 2 70-130/20
95-50-1 1,2-Dichlorobenzene ND 50 45.8 92 50 46.6 93 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 46.3 93 50 46.8 94 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 44.2 88 50 44.7 89 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 44.6 89 50 45.4 91 2 70-130/20
100-41-4 Ethylbenzene ND 50 46.0 92 50 46.9 94 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 90.1 50 123 66*50 125 70 2 70-130/20
91-20-3 Naphthalene 2.2 J 50 40.5 77 50 46.9 89 15 70-130/20
108-88-3 Toluene ND 50 45.9 92 50 47.1 94 3 70-130/20
1330-20-7 Xylene (total)ND 150 139 93 150 141 94 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA46086-1 Limits
1868-53-7 Dibromofluoromethane 99%99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%100%102%70-130%
2037-26-5 Toluene-D8 101%101%106%70-130%
460-00-4 4-Bromofluorobenzene 103%101%106%70-130%
* = Outside of Control Limits.
21 of 21
FA4603855.4.1