FA-233_6601_CA_MRP_20230406

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
April 6, 2023

Mr. Nathan Beauchamp
NCDEQ-UST Section
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, NC 28301-5043

Re: Ground Water Monitoring Report
February 2023
Former Roseboro BP
270 E. Martin Luther King Jr. Boulevard
Roseboro, Sampson County
North Carolina
Facility ID Number: 0-00-0000008172
Incident Number: 06601
GRI Project Number: 2059

Dear Mr. Beauchamp,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Rae Brown at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Greg Owen; Wellman Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
February 2023
Former Roseboro BP
270 E. Dr. Martin Luther King Jr. Blvd.
Roseboro, Sampson County
North Carolina
Facility ID Number: 0-00-0000008172
Incident Number: 06601
GRI Project Number: 2059

Prepared for:

Mr. Greg Owen
Wellman Oil Company, Inc.
716 Warsaw Road
Clinton, NC 28328

April 6, 2023

Rae Troiano Brown, P.G.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
ii
EXECUTIVE SUMMARY
Former Roseboro BP is located at 270 E. Dr. Martin Luther King Jr. Blvd. in Roseboro, Sampson County,
North Carolina. The site is currently owned by William H. Owen and is operated by Xpress Car Wash. In
1991, a UST release at the site was discovered during repairs to a public water line located along the north
side of North Carolina Highway 24. In November 1993, a vacuum extraction and air sparging system was
installed at the site that operated until October 1996 when the site priority ranking was lowered by the
NCDEQ and the cleanup was suspended. No USTs have been operated at the site since 2003.

The adjoining properties are a mixture of residential and commercial properties. A municipal water supply
well (WSW-7) for the Town of Roseboro is located approximately 1,600 feet from the site. All structures
within 1,000 feet of the source area are serviced by a municipal water supply system. The site was ranked
high risk because of the municipal water supply well.

In January 2010, a second plume on the Roseboro BP site was reported. However, no definitive evidence
exists that the free product from the Roseboro BP release migrated off site, and ground water
contamination reported in adjacent property wells may be from the EPCO 3-Way Food Mart release. In
2014, petroleum constituent concentrations which exceeded MCCs in soil samples collected at depths of
4 – 5 feet BGS were reported at the EPCO Food Mart in the Phase I and Limited Phase II Environmental
Site Assessment report (depths to water were 10 feet BGS). In the 2015 Site Check report, EPCO MW-103
(which is located down-gradient of the EPCO UST basin) reported a concentration of benzene of 4,400
g/L.

On February 14, 2023, seven Type II monitoring wells (MW-20, MW-22, MW-35, MW-43, MW-44, EPCO-
MW-101, and EPCO-MW-102) and one telescoping well (DMW-3) were gauged, purged, and/or sampled.
MW-2R had an obstruction at approximately 4.86 feet below TOC and neither a depth-to-water
measurement nor a ground water sample could be collected. Free product was measured in monitoring
wells EPCO-MW-101 and EPCO-MW-102 located at the EPCO 3-Way Food Mart.

Ground water samples were collected from MW-20, MW-22, MW-35, MW-43, MW-44, and DMW-3.
Contaminant concentrations in water samples collected from MW-43 and MW-44 exceeded the MACs.
All of the reported contaminant concentrations were below the GCLs. An estimated concentration of
MTBE not exceeding the MAC was reported in the ground water sample collected from WSW-7.

The total contaminant mass at the site has decreased by 60.4% since 2015.

No free product has been reported at the site since 2009. No contaminant concentrations have exceeded
GCLs since 2019. Based on this information, the site risk should be reduced to low; and, subsequent to
filing a notice of residual petroleum and completing public notice, the incident should be closed.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
iii
SITE INFORMATION
1. Site Identification
 Former Roseboro BP (Facility ID 0-00-0000008172)
 Incident Number 06601 – High Risk (H151D)
 Location of Source Area: 270 E. Dr. Martin Luther King Jr. Blvd.
Roseboro, NC 28314
Sampson County
34.9553060°N, 78.5101110°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Wellman Oil Co., Inc.
P.O. Box 780
Clinton, North Carolina 28328
Email: [e-mail]
Phone No. 910.590.3040

UST/AST Operator
Wellman Oil Co., Inc.
P.O. Box 780
Clinton, North Carolina 28328
Email: [e-mail]
Phone No. 910.590.3040

Property Owner
William H. Owen
P.O. Box 780
Clinton, North Carolina 28328
Email: Unknown
Phone No. 910.590.3040

Property Occupant
Xpress Car Wash
270 NC Highway 24
Clinton, North Carolina 28328
Email: Unknown
Phone No. Unknown
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
[phone]
3. Information about Release
 In 1991, a release was discovered during the repair of a public water line located in the NCDOT
right-of-way.
 An unknown amount of product was released from the premium gasoline product line.
 One 3,000-gallon gasoline UST, two 2,000-gallon gasoline USTs, one 550-gallon diesel UST, one
550-gallon heating oil UST, one 550-gallon used oil UST, and one 3,000-gallon UST (contents
unknown) were removed from the site in June 1993. Two 3,000-gallon gasoline USTs and one
6,000-gallon gasoline UST were removed from the site on April 23, 2003.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
MNA: Monitored Natural Attenuation
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... ii
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
3.0 FREE PRODUCT REMOVAL ........................................................................................................5
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................6
5.0 CONCLUSIONS .........................................................................................................................6
6.0 LIMITATIONS ...........................................................................................................................6
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 3A: Detail Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Water Supply Well Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Summary of MNA Parameter Readings

APPENDICES
Appendix A: State Correspondence
Appendix B: Historical Cross Sections
Appendix C: Laboratory Analytical Report
Appendix D: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the February 2023 ground water sampling event at the Former Roseboro BP
site, located at 270 E. Dr. Martin Luther King Jr. Blvd. in Roseboro, Sampson County, North Carolina
(Figures 1, 2, 3, and 3A). These activities were conducted in accordance with GRI Proposal No. 22-884,
which was submitted to NCDEQ on January 11, 2023, and was approved as Task Authorization No. 6601-
45 on January 12, 2023. State correspondence is included as Appendix A.

The site is currently owned by William H. Owen and is operated by Xpress Car Wash. In 1991, a release at
the site was discovered during repairs to a public water line located on-site along the north side of North
Carolina Highway 24. Subsequent tightness testing of the on-site UST system indicated that the release
was from a premium unleaded gasoline product line. In November 1993, a vacuum extraction and air
sparging system was installed at the site that operated until October 1996 when the site priority ranking
was lowered by the NCDEQ and the cleanup was suspended. No USTs have operated at the site since
2003. UST owner/operator information and UST system information are included as Tables 1 and 2,
respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of residential and commercial properties. The site contains
one building (car wash) and is primarily capped with concrete and asphalt. The overall topography at the
site is relatively flat. Twenty-six Type II monitoring wells, six Type III monitoring wells, and four recovery

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
2
wells were installed during previous ground water assessment activities. A Site Map showing the locations
of the monitoring wells has been included as Figure 3 and a detailed Site Map is included as Figure 3A.
Historical cross-sections that include soil data and estimated contaminant contours are included as
Appendix B.

A municipal water supply well (WSW-7) for the Town of Roseboro is located approximately 1,600 feet
from the site. All structures within 1,000 feet of the source area are serviced by a municipal water supply
system. Adjacent property owner information and well owner information is presented in Tables 3 and
4, respectively.

In the 2004 CAP, three phases were proposed. In Phase I, water supply wells were to be abandoned and
MMPE events were to be implemented as necessary to remove free product and reduce dissolved phase
contaminant concentrations. A six-month monitoring program was to be conducted with monthly
analysis of the municipal well and quarterly analysis of the monitoring wells.

In Phase II, packer tests were to be conducted on the municipal well to determine permanent placement
for uncontaminated ground water zone. A similar monitoring program to the first phase was to be
implemented.

If the first and second phases failed, in the Phase III, a granular activated carbon filtration system would
be installed to reduce contaminant concentrations to applicable standards. A long-term sampling
program would be required to monitor the plume migration and potential carbon breakthrough.

Please note that the CAP was not implemented; and, therefore, no milestones have been established for
the site.

In 2003, all the USTs were removed from the Roseboro BP site. In January 2010, a second plume on the
Roseboro site was reported. However, no definitive evidence exists that the free product found in
monitoring wells (MW-101 and MW-102) on the adjacent property, EPCO 3-Way Food Mart, originated
from Roseboro BP. Monitoring wells EPCO-MW-101 and EPCO-MW-102 were installed as part of the
EPCO 3-Way Food Mart site assessment. Two monitoring wells (MW-43 and MW-44) were installed at
Roseboro BP site to evaluate whether or not free product present at the Roseboro BP site could have
migrated offsite. Historic gauging of MW-43 and MW-44 has not detected free product. Free product in
MW-2R at the Roseboro BP site has not been present since 2009.

In 2002, USTs were installed at EPCO 3-Way Food Mart and no release was reported to the NCDEQ at the
time of installation. Therefore, if the former air sparge system at the Roseboro BP site which operated
from 1993 to 1996 “pushed” free product onto the EPCO 3-Way Food Mart site, then the free product
would have been discovered during the UST installation. Petroleum constituent concentrations which
exceeded MCCs in soil samples collected at depths of 4 – 5 feet from the EPCO 3-Way Food Mart site were
reported in a EPCO Food Mart Phase I and Limited Phase II Environmental Site Assessment report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
3
(December 28, 2014); depth to ground water is typically 10 – 12 feet below ground surface. In addition,
in the Site Check Report (February 26, 2015) for the EPCO 3-Way Food Mart property, EPCO MW-103
(which is located down-gradient of the EPCO 3-Way Food Mart UST basin) reported a concentration of
benzene of 4,400 g/L and the hydraulic gradient reported was 0.00091 feet per foot which is extremely
flat and undoubtedly subject to lithologic heterogeneities. This evidence would indicate that the free
product on the EPCO 3-Way Food Mart property could be originating from a release on the EPCO 3-Way
Food Mart property.

Please note that some of the information contained in this report was obtained under the supervision of
Clark Environmental Services, Inc. (Clark), the previous consultant on the project until GRI was retained in
March 2004. Although GRI cannot verify the accuracy of their information, for the purpose of this report
it is assumed to be correct, and any inferences or interpretations made by GRI based on data that may be
incorrect are not the responsibility of GRI. Please refer to earlier submittals for additional information
regarding assessment activities.

In January 2022, GRI conducted an updated receptor survey. All structures within 1,000 feet of the source
area are serviced by a municipal water supply system. No surface water bodies were identified within a
500-foot radius of the site. Adjacent property owner information is shown on Table 3 and water supply
well information is shown on Table 4. Potable well locations are shown on Figure 2.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On February 14, 2023, seven Type II monitoring wells (MW-20, MW-22, MW-35, MW-43, MW-44, EPCO-
MW-101, and EPCO-MW-102) and one telescoping well (DMW-3) were gauged, purged, and/or sampled.
Free product was measured in monitoring wells EPCO-MW-101 (0.04 feet) and EPCO-MW-102 (0.36 feet)
located at the EPCO 3-Way Food Mart site. MW-2R had an obstruction at approximately 4.86 feet below
TOC and neither a depth-to-water measurement nor a ground water sample could be collected.

Depths to ground water in the Type II monitoring wells ranged from 11.97 feet to 14.71 feet below TOC.
Ground water elevations in the Type II monitoring wells ranged from 116.01 to 113.69 feet. Ground water
flow was generally to the northeast with a horizontal gradient of approximately 0.01 feet per foot. The
vertical gradient between paired wells MW-35 and DMW-3 was approximately 0.024 feet per foot in the
downward direction. Well construction and gauging information is presented in Table 5. A Water Table
Surface Map based on the Type II monitoring wells is included as Figure 4. A summary of the current
ground water gauging data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
4
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-2R 5 – 15 15 128.76 NM NM NM
MW-20 10 – 20 20 128.40 14.71 0.00 113.69
MW-22 10 – 20 20 128.04 13.58 0.00 114.46
MW-35 15 – 20 20 128.05 12.04 0.00 116.01
MW-43 5 – 20 20 128.24 14.11 0.00 114.13
MW-44 5 – 20 20 127.10 13.02 0.00 114.08
DMW-3 40 – 45 45 128.22 13.96 0.00 114.26
EPCO MW-101 8 – 18 18 126.46 12.08 0.04 114.41
EPCO MW-102 8 – 18 18 125.85 11.97 0.36 114.19

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B from MW-20, MW-22, MW-35, MW-43, MW-44, DMW-3, and WSW-7.
Concentrations of benzene, toluene, xylenes, MTBE, naphthalene, TAA, n-propylbenzene, and/or 1,2,4-
trimethylbenzene reported in the ground water samples collected from MW-43 and MW-44 exceeded the
MACs. All of the reported contaminant concentrations were below the GCLs. An estimated concentration
of MTBE not exceeding the MAC was reported in the ground water sample collected from WSW-7.

A summary of the analytical results for ground water samples collected on February 14, 2023 is presented
in Table 6. A summary of the MNA parameter readings collected from each of the sampled monitoring
wells is presented in Table 7. A Ground Water Quality Map based on the February 2023 data is included
as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the
monitoring wells during the February 2023 sampling event is included as Appendix C. A summary of the
current ground water analytical data is shown below:

Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-2R NS NS NS NS NS NS
MW-20 0.868 4.7 1.37 7.14 <0.140 <0.470
MW-22 0.330 J 1.72 0.59 2.85 <0.140 <0.470
MW-35 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-43 1,640 2,740 597 2,730 <14.0 <47.0
MW-44 219 7.61 62.8 167 J 30 46
DMW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
WSW-7 <0.180 <0.220 <0.170 <0.210 0.706 J <0.470
EPCO MW-101 FP FP FP FP FP FP
EPCO MW-102 FP FP FP FP FP FP

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations as well as the maximum historical water column height from the 2015 water

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
5
sampling event. A theoretical contaminant mass area was calculated around MW-2R, MW-43, and MW-
44 and used in the contaminant mass calculations. The total contaminant mass at the site has decreased
60.4% since 2015. Please note that since MW-2R was not sampled during this event, only the contaminant
concentrations of MW-43 and MW-44 were used for the February 2023 contaminant mass calculations.
Contaminant mass calculations are included as Appendix D. A map of the contaminant mass areas is
included as Figure 6. A chart depicting the overall trend in contaminant mass is shown below:

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately four to thirteen feet BGS.
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in monitoring wells MW-2R and MW-42. Please note, that
MW-42 is located off-site at another gasoline station.

AFVR events were conducted in MW-2R in 2008 and 2009; and, in 2010, an MMPE event was conducted
in MW-2R. Free product has not been present in MW-2R since 2009.

0.00
5.00
10.00
15.00
20.00
0.00
5,000.00
10,000.00
15,000.00
20,000.00
25,000.00
Average Water Column Height (ft)Contaminant Mass (grams)Time
Total Contaminant Mass vs. Time
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
Contaminant Mass Water Column Height (ft)Linear (Contaminant Mass)

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
6
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
In November 1993, a vacuum extraction and air sparging system was installed at the site that operated
until October 1996 when the site priority ranking was lowered by the NCDEQ and the cleanup was
suspended.

In 2004, a three phase CAP was proposed. Please note that the CAP was not implemented; and, therefore,
no milestones or natural attenuation plan has been established.
5.0 CONCLUSIONS
 the Former Roseboro BP is operated by Xpress Car Wash. In 2003, all the USTs were removed
from the Roseboro BP site.
 On February 14, 2023, seven Type II monitoring wells and one telescoping well were gauged,
purged, and/or sampled. MW-2R had an obstruction at approximately 4.86 feet below TOC and
neither a depth-to-water measurement nor a ground water sample could be collected.
 Free product was measured in monitoring wells EPCO-MW-101 (0.04 feet) and EPCO-MW-102
(0.36 feet). Free product at the EPCO 3-Way Food Mart should not be attributed to Roseboro BP
and should be the responsibility of EPCO 3-Way Food Mart.
 Ground water elevations in the Type II monitoring wells ranged from 116.01 to 113.69 feet.
Ground water flow was generally to the northeast with a horizontal gradient of approximately
0.01 feet per foot. The vertical gradient between paired wells MW-35 and DMW-3 was
approximately 0.024 feet per foot in the downward direction.
 The concentrations of benzene, toluene, xylenes, MTBE, naphthalene, TAA, n-propylbenzene,
and/or 1,2,4-trimethylbenzene reported in the ground water samples collected from MW-43 and
MW-44 exceeded the MACs. All of the reported contaminant concentrations were below the
GCLs.
 A theoretical contaminant mass area was calculated around MW-2R, MW-43, and MW-44 and
used in the contaminant mass calculations. The total contaminant mass at the site has decreased
60.4% since 2015.
 An estimated concentration of MTBE not exceeding the MAC was reported in the ground water
sample collected from WSW-7.
 No USTs have operated at the site since 2003. According to the updated receptor survey
conducted in January 2022, all structures within 1,000 feet of the source area are serviced by a
municipal water supply system. No free product has been reported at the site since 2009. No
contaminant concentrations have exceeded GCLs since 2019. Based on this information, the site
risk should be reduced to low; and, subsequent to filing a notice of residual petroleum and
completing public notice, the incident should be closed.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Wellman Oil Company, Inc. for specific application
to the referenced site in Sampson County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 6, 2023 Former Roseboro BP
Project Manager: Rae Troiano Brown, P.G. GRI Project No. 2059
7
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Rae Troiano Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
SITEN EAST STBROAD STW N O R T H S T
E C L IN T O N S T
C U L B R E T H S T
N WEST STNE RAI
LROAD ST
E R O S E B O R O S TE NORTH STOAK ST
E DR MARTIN L KING JR BLVD
W C L IN T O N S T
MAPLE ST
PEARL STLEGION STSU M NER A V E CYPRESS STNATI
ONAL
STE P L E A S A N T S T HOBBS STN CHURCH STBULLARD ST
W DR MARTIN L KING JR BLVD
PARK DRNW RAI
L
ROAD STMCPHERSON STBOWEN STN BROAD STS HALL STS EAST STN HALL
STHERRING STB U T L E R S T
E R O S E B O R O S TBROAD STFIGURE 2: SITE VICINITY MAPROSEBORO BPHIGHWAY 24 EASTROSEBORO, SAMPSON COUNTYNORTH CAROLINAINCIDENT NO. 6601GRI NO. 2059
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 17, 2022
³
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS 250-FOOT RADIUS
500-FOOT RADIUS
LEGEND
ncrivers
Centerlines
nc_sampson_parcels_poly

TABLES
UST ID Number 8, 8A & 9 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 2-7 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
FORMER ROSEBORO BP (INCIDENT NO. 06601)
00-0-0000008172
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
Wellman Oil Co., Inc 07/01/1993 - 04/23/2003
Address Telephone Number
716 Warsaw Rd, Clinton, NC 28328 910-592-4135
0-008172
Name of Owner or Operator Dates of Ownership / Operation
Unknown 04/22/1985 - 06/24/1993
Address Telephone Number
Unknown Unknown
Unknown Unknown
0-008172
Name of Owner or Operator Dates of Ownership / Operation
Unknown 04/29/1957 - 06/24/1993
Page 1 of 1
Date: 11/27/19
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 3,000 04/22/1985 Single Wall Steel 5' 4" x 18' Single Wall Steel Removed Unknown
2 Unknown Unknown 3,000 04/29/1957 Single Wall Steel 5' 4" x 18' Single Wall Steel Removed Unknown
3 Gasoline Gasoline 2,000 04/29/1957 Single Wall Steel 5' 4" x 12' Single Wall Steel Removed Unknown
4 Gasoline Gasoline 2,000 04/29/1957 Single Wall Steel 5' 4" x 12' Single Wall Steel Removed Unknown
5 Diesel Diesel 550 04/29/1957 Single Wall Steel 3'10" x 6'2" Single Wall Steel Removed Unknown
6 Heating Oil Heating Oil 550 04/29/1957 Single Wall Steel 3'10" x 6'2" Single Wall Steel Removed Unknown
7 Oil, Mixed Oil, Mixed 550 04/29/1957 Single Wall Steel 3'10" x 6'2" Single Wall Steel Removed Unknown
8 Gasoline Gasoline 3,000 07/01/1993 Single Wall Steel 5' 4" x 18' Single Wall FRP Removed Unknown
8A Gasoline Gasoline 3,000 07/01/1993 Single Wall Steel 5' 4" x 18' Single Wall FRP Removed Unknown
9 Gasoline Gasoline 6,000 07/01/1993 Single Wall Steel 8' x 16' Single Wall FRP Removed Unknown
Notes:
• FRP: Fiberglass reinforced plastic.
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
FORMER ROSEBORO BP (INCIDENT NO. 06601)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Facility ID # : 00-0-0000008172
Page 1 of 1
Date: 03/18/2022 Facility ID # : 00-0-0000008172
Parcel Number Owner Name Address
08076208501 (Site) William H. Owen
270 E Dr. Martin Luther King Blvd
Roseboro, NC 28382
08012524505 Wade Cary Holdings, LLC
205 E. Dr. Martin Luther King Jr Blvd
Roseboro, NC 28382
08111124002 Phuong Thi Phu
301 East NC 24 Highway Roseboro,
NC 28382
08095444003 First Citizens Bank & Trust Co.
304 E. Dr. Martin Luther King Blvd
Roseboro, NC 28382
08104638502 M. B. Barefoot
446 National Street Roseboro,
NC 28382
08026088001 Felix Huong Tran
206 E. Dr. Martin Luther King Jr Blvd
Roseboro, NC 28382
08029312501 Jie Yang
306 North East Street Roseboro,
NC 28382
08058981101 Lakewood Plaza II East North Street
Note:
• Properties are keyed to Figure 2.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
FORMER ROSEBORO BP (INCIDENT NO. 06601)
Page 1 of 1
Facility ID # : 00-0-0000008172
Well ID. Parcel ID No. Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Well Depth
(ft)
Connected to
Municipal Water
Yes/No
Distance from
source area of
release
(ft.)
WSW-1 1904 Skibo Road
Rayetteville, NC 28314
320 Maple Street
Roseboro, NC 28382
Abandoned
(06/29/06)48 Yes ~860' NE
WSW-2 320 Maple Street
Roseboro, NC 28382
320 Maple Street
Roseboro, NC 28382
Abandoned
(06/29/06)20 Yes ~853' NE
WSW-3 08004244001 John Jones
312 Oak Street
Roseboro, NC 28382
313 Oak Street
Roseboro, NC 28382
Abandoned
(06/29/06)18 Yes ~885' NE
WSW-4 08050096002 James Elton Hudson
408 Maple Street
Roseboro, NC 28382
504 Hobbs Street
Roseboro, NC 28381
Abandoned
(06/29/06)12 Yes ~1,167' NE
WSW-5 08050096001 James Elton Hudson
Hobbs Street
Roseboro, NC 28381
Hobbs Street
Roseboro, NC 28382
Abandoned
(06/29/06)16 Yes ~1,326' NE
WSW-6 08089532001 Gary W. Culbreth
3606 Elizabethtown Hwy
Roseboro, NC 28382
413 Oak Street
Roseboro, NC 28382 Irrigation 70 Yes ~1,047' E
WSW-7 08010119503 The Town of Roseboro
P.O. Box 848
Roseboro, NC 28382
611 Cypress Street
Roseboro, NC 28382 Potable 270 NA ~1,600' NE
WSW-8 08008008001 Elim Rivera
412 Oak Street
Roseboro, NC 28382
412 Oak Street
Roseboro, NC 28382 Not In Use Unknown Yes ~1,025' E
WSW-9 08001928001 Christopher Paul Pittman
314 Sumner Ave
Roseboro, NC 28382
314 Sumner Ave
Roseboro, NC 28382 Irrigation 15 Yes ~788' North
WSW-10 08115016003 Nicolas Turrubiartez, Jr.
3932 Andrews Chapel Road
Roseboro, NC 28382
309 Oak Street
Roseboro, NC 28382 Not In Use 17 Yes ~490' NE
Note:
• Water supply wells are keyed to Figure 2.
• Water supply well information from 2006; updated 2022.
• NA: Not applicable.
8046588001 Agustin Alvarez
TABLE 4
WATER SUPPLY WELL INFORMATION
FORMER ROSEBORO BP (INCIDENT NO. 06601)
Date: 3/18/2022
Page 1 of 1
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
05/12/04 10.57 0.00 117.80
06/01/06 NM NM NM
05/12/04 9.65 0.02 119.13
05/31/06 14.40 1.98 116.06
09/05/06 12.66 0.03 116.13
06/19/07 12.42 0.19 116.50
12/06/07 14.82 0.16 114.08
02/14/08 14.22 0.23 114.74 Before AFVR
02/14/08 14.94 0.00 113.82 After AFVR
05/20/08 11.33 0.04 117.46
11/06/08 12.47 0.05 116.33
05/27/09 9.22 0.00 119.54 Before AFVR
05/27/09 11.35 0.00 117.41 After AFVR
05/28/09 10.67 0.00 118.09
12/03/09 13.73 0.03 115.06
05/10/10 9.90 0.00 118.86 Before MMPE
05/14/10 13.81 0.00 114.95 After MMPE
06/16/10 11.09 0.00 117.67
12/09/10 13.20 0.00 115.56
06/01/11 DRY -- --
11/08/11 DRY -- --
06/06/12 DRY -- --
12/05/12 DRY -- --
06/04/13 13.95 0.00 114.81
12/02/13 13.97 0.00 114.79
06/18/14 12.03 0.00 116.73
12/08/14 13.53 0.00 115.23
06/03/15 11.31 0.00 117.45
12/15/15 11.16 0.00 117.60
06/08/16 11.50 0.00 117.26
02/20/17 11.76 0.00 117.00
05/16/18 12.68 0.00 116.08
11/13/18 12.58 0.00 116.18
11/07/19 13.23 0.00 115.53
11/04/20 11.62 0.00 117.14
01/04/22 11.84 0.00 116.92
02/14/23 NM NM NM Obstructed
05/12/04 10.54 0.00 117.63
06/01/06 NM NM NM
05/12/04 10.72 0.00 118.36
05/31/06 13.57 0.00 115.51
09/05/06 12.31 0.00 116.77
06/19/07 13.24 0.00 115.84
12/06/07 14.86 0.00 114.22
05/20/08 13.05 0.00 116.03
11/06/08 13.25 0.00 115.83
05/28/09 11.83 0.00 117.25
12/03/09 14.21 0.00 114.87
06/16/10 11.95 0.00 117.13
12/09/10 13.70 0.00 115.38
06/01/11 13.20 0.00 115.88
11/08/11 14.34 0.00 114.74
06/06/12 14.03 0.00 115.05
12/05/12 15.03 0.00 114.05
06/04/13 14.31 0.00 114.77
12/02/13 14.56 0.00 114.52
06/18/14 12.75 0.00 116.33
12/08/14 14.09 0.00 114.99
06/03/15 12.10 0.00 116.98
12/15/15 11.98 0.00 117.10
02/20/17 13.19 0.00 115.89
05/16/18 13.35 0.00 115.73
11/13/18 13.31 0.00 115.77
11/07/19 13.91 0.00 115.17
MW-1R 7 7 - 17 17 128.37
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
MW-3R 7 7 - 17 17 128.17
MW-2R 5 5 - 15 15 128.76
MW-11 10 10 - 20 20 129.08
Page 1 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 11.33 0.00 117.69
05/31/06 13.55 0.00 115.47
09/05/06 13.13 0.00 115.89
06/19/07 13.64 0.00 115.38
12/06/07 14.83 0.00 114.19
05/20/08 13.01 0.00 116.01
11/06/08 13.23 0.00 115.79
05/28/09 11.86 0.00 117.16
12/03/09 14.19 0.00 114.83
06/16/10 12.04 0.00 116.98
12/09/10 13.70 0.00 115.32
06/01/11 13.12 0.00 115.90
11/08/11 14.30 0.00 114.72
06/06/12 14.00 0.00 115.02
12/05/12 15.00 0.00 114.02
06/04/13 14.42 0.00 114.60
12/02/13 14.54 0.00 114.48
06/18/14 12.24 0.00 116.78
12/08/14 14.06 0.00 114.96
06/03/15 12.09 0.00 116.93
12/15/15 11.93 0.00 117.09
06/08/16 12.35 0.00 116.67
02/20/17 13.14 0.00 115.88
05/16/18 13.32 0.00 115.70
11/13/18 13.27 0.00 115.75
11/07/19 13.89 0.00 115.13
05/12/04 10.11 0.00 118.62
05/31/06 12.59 0.00 116.14
06/19/07 11.61 0.00 117.12
12/06/07 NM NM NM
05/20/08 11.84 0.00 116.89
11/06/08 11.99 0.00 116.74
05/28/09 10.50 0.00 118.23
12/03/09 13.08 0.00 115.65
06/16/10 10.80 0.00 117.93
12/09/10 12.51 0.00 116.22
06/01/11 NM NM NM
11/08/11 13.54 0.00 115.19
06/06/12 13.35 0.00 115.38
12/05/12 14.26 0.00 114.47
06/04/13 13.71 0.00 115.02
12/02/13 13.72 0.00 115.01
06/18/14 11.33 0.00 117.40
12/08/14 13.24 0.00 115.49
06/03/15 11.07 0.00 117.66
12/15/15 11.15 0.00 117.58
06/08/16 11.48 0.00 117.25
02/20/17 12.42 0.00 116.31
05/16/18 12.50 0.00 116.23
11/13/18 12.94 0.00 115.79
11/07/19 Dry Dry Dry
MW-12 10 10 - 20 20 129.02
MW-17 7 7 - 20 20 128.73
Page 2 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 5.28 0.00 124.86
06/01/06 7.17 0.00 122.97
09/05/06 4.34 0.00 125.80
06/25/07 Dry -- --
12/06/07 NM NM NM
12/03/09 5.60 0.00 124.54
06/16/10 5.84 0.00 124.30
12/09/10 8.00 0.00 122.14
06/01/11 7.02 0.00 123.12
11/08/11 7.12 0.00 123.02
06/06/12 6.00 0.00 124.14
12/05/12 NM 0.00 NM
06/04/13 6.74 0.00 123.40
12/02/13 6.93 0.00 123.21
06/18/14 7.41 0.00 122.73
12/08/14 7.36 0.00 122.78
06/03/15 6.56 0.00 123.58
12/15/15 NM NM NM
02/20/17 7.09 0.00 123.05
05/16/18 7.03 0.00 123.11
11/13/18 5.95 0.00 124.19
11/07/19 NM NM NM
05/12/04 NM NM NM
06/01/06 NM NM NM
12/05/12 13.90 0.00 114.50
06/04/13 13.72 0.00 114.68
12/02/13 14.83 0.00 113.57
06/18/14 11.99 0.00 116.41
12/08/14 13.36 0.00 115.04
06/03/15 11.35 0.00 117.05
12/15/15 11.30 0.00 117.10
06/08/16 11.64 0.00 116.76
02/20/17 12.43 0.00 115.97
05/16/18 12.61 0.00 115.79
11/13/18 12.60 0.00 115.80
11/07/19 13.19 0.00 115.21
11/04/20 12.38 0.00 116.02
01/04/22 13.98 0.00 114.42
02/14/23 14.71 0.00 113.69
05/12/04 10.73 0.00 117.74
05/31/06 13.03 0.00 115.44
09/05/06 8.32 0.00 120.15
06/25/07 12.64 0.00 115.83
12/06/07 NM NM NM
MW-19 2 2 - 10 10 130.14
MW-21 10 10 - 20 20 128.47
MW-20 10 10 - 20 20 128.4
Page 3 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 10.44 0.00 117.60
06/01/06 12.72 0.00 115.32
09/05/06 9.73 0.00 118.31
06/25/07 12.17 0.00 115.87
12/06/07 13.97 0.00 114.07
05/20/08 12.19 0.00 115.85
11/06/08 12.37 0.00 115.67
05/28/09 11.09 0.00 116.95
12/03/09 12.82 0.00 115.22
06/16/10 11.29 0.00 116.75
12/09/10 12.88 0.00 115.16
06/01/11 12.34 0.00 115.70
11/08/11 13.47 0.00 114.57
06/06/12 13.13 0.00 114.91
12/05/12 14.20 0.00 113.84
06/04/13 13.60 0.00 114.44
12/02/13 13.67 0.00 114.37
06/18/14 11.96 0.00 116.08
12/08/14 13.26 0.00 114.78
06/03/15 11.35 0.00 116.69
12/15/15 11.11 0.00 116.93
02/20/17 12.23 0.00 115.81
05/16/18 12.50 0.00 115.54
11/13/18 12.03 0.00 116.01
11/07/19 13.01 0.00 115.03
11/04/20 11.58 0.00 116.46
01/04/22 13.28 0.00 114.76
02/14/23 13.58 0.00 114.46
05/12/04 12.73 0.00 117.99
05/31/06 14.95 0.00 115.79
06/19/07 14.35 0.00 116.39
12/06/07 16.25 0.00 114.49
05/20/08 14.39 0.00 116.35
11/06/08 14.62 0.00 116.12
05/28/09 13.16 0.00 117.58
12/03/09 15.68 0.00 115.06
06/16/10 13.42 0.00 117.32
12/09/10 15.14 0.00 115.60
06/01/11 14.57 0.00 116.17
11/08/11 15.74 0.00 115.00
06/06/12 15.50 0.00 115.24
12/05/12 16.73 0.00 114.01
06/04/13 15.94 0.00 114.80
12/02/13 15.96 0.00 114.78
06/18/14 14.04 0.00 116.70
12/08/14 15.48 0.00 115.26
06/03/15 13.37 0.00 117.37
12/15/15 13.38 0.00 117.36
06/08/16 13.70 0.00 117.04
02/20/17 14.58 0.00 116.16
05/16/18 14.74 0.00 116.00
11/13/18 14.72 0.00 116.02
11/07/19 15.21 0.00 115.53
MW-25 10 10 - 20 20 130.74
MW-22 10 10 - 20 20 128.04
Page 4 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 12.12 0.00 117.60
05/31/06 14.35 0.00 115.37
06/19/07 11.59 0.00 118.13
12/06/07 NM NM NM
05/20/08 13.82 0.00 115.90
11/06/08 14.03 0.00 115.69
05/28/09 12.71 0.00 117.01
12/03/09 15.17 0.00 114.55
06/16/10 12.97 0.00 116.75
12/09/10 14.50 0.00 115.22
06/01/11 14.00 0.00 115.72
11/08/11 15.13 0.00 114.59
06/06/12 14.76 0.00 114.96
12/05/12 15.80 0.00 113.92
06/04/13 15.22 0.00 114.50
12/02/13 15.31 0.00 114.41
06/18/14 13.58 0.00 116.14
12/08/14 14.86 0.00 114.86
06/03/15 12.92 0.00 116.80
12/15/15 NM NM NM
05/12/04 8.67 0.00 117.38
05/31/06 10.92 0.00 115.13
09/05/06 10.21 0.00 115.84
06/19/07 10.58 0.00 115.47
12/06/07 12.21 0.00 113.84
05/20/08 10.37 0.00 115.68
11/06/08 10.62 0.00 115.43
05/28/09 9.31 0.00 116.74
12/03/09 11.50 0.00 114.55
06/16/10 9.41 0.00 116.64
12/09/10 11.09 0.00 114.96
06/01/11 10.58 0.00 115.47
11/08/11 11.66 0.00 114.39
06/06/12 11.24 0.00 114.81
12/05/12 12.37 0.00 113.68
06/04/13 11.71 0.00 114.34
12/02/13 11.88 0.00 114.17
06/18/14 10.21 0.00 115.84
12/08/14 11.47 0.00 114.58
06/03/15 9.61 0.00 116.44
12/15/15 NM NM NM
02/20/17 10.46 0.00 115.59
05/16/18 10.68 0.00 115.37
11/13/18 10.56 0.00 115.49
11/07/19 11.30 0.00 114.75
MW-27 7 7 - 17 17 126.05
MW-26 7 7 - 17 17 129.72
Page 5 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 8.61 0.00 117.31
05/31/06 10.86 0.00 115.06
09/05/06 10.28 0.00 115.64
06/21/07 10.50 0.00 115.42
12/06/07 12.09 0.00 113.83
05/20/08 10.32 0.00 115.60
11/06/08 10.57 0.00 115.35
05/28/09 9.29 0.00 116.63
12/03/09 11.40 0.00 114.52
06/16/10 9.35 0.00 116.57
12/09/10 11.04 0.00 114.88
06/01/11 10.53 0.00 115.39
11/08/11 11.59 0.00 114.33
06/06/12 11.20 0.00 114.72
12/05/12 12.33 0.00 113.59
06/04/13 11.64 0.00 114.28
12/02/13 11.82 0.00 114.10
06/18/14 10.19 0.00 115.73
12/08/14 11.42 0.00 114.50
06/03/15 9.59 0.00 116.33
12/15/15 9.32 0.00 116.60
06/08/16 9.74 0.00 116.18
02/20/17 10.42 0.00 115.50
05/16/18 10.65 0.00 115.27
11/13/18 10.59 0.00 115.33
11/07/19 11.22 0.00 114.70
05/12/04 12.73 0.00 118.06
05/31/06 14.93 0.00 115.86
06/19/07 14.56 0.00 116.23
12/06/07 NM 0.00 NM
12/03/09 15.27 0.00 115.52
06/16/10 13.37 0.00 117.42
12/09/10 15.14 0.00 115.65
06/01/11 14.54 0.00 116.25
11/08/11 15.72 0.00 115.07
06/06/12 15.27 0.00 115.52
12/05/12 16.45 0.00 114.34
06/04/13 15.93 0.00 114.86
12/02/13 15.95 0.00 114.84
06/18/14 14.01 0.00 116.78
12/08/14 15.46 0.00 115.33
06/03/15 13.33 0.00 117.46
12/15/15 NM NM NM
05/12/04 10.51 0.00 120.87
05/31/06 15.67 0.00 115.71
06/19/07 12.83 0.00 118.55
12/06/07 NM NM NM
05/20/08 15.16 0.00 116.22
11/06/08 15.35 0.00 116.03
05/28/09 14.92 0.00 116.46
12/03/09 13.93 0.00 117.45
06/16/10 13.33 0.00 118.05
12/09/10 15.84 0.00 115.54
06/01/11 15.32 0.00 116.06
11/08/11 16.25 0.00 115.13
06/06/12 15.74 0.00 115.64
12/05/12 17.17 0.00 114.21
06/04/13 16.65 0.00 114.73
12/02/13 16.47 0.00 114.91
06/18/14 14.82 0.00 116.56
12/08/14 16.03 0.00 115.35
06/03/15 13.33 0.00 118.05
12/15/15 NM NM NM
MW-29 7 7 - 17 17 130.79
MW-28 7 7 - 17 17 125.92
MW-30 7 7 - 17 17 131.38
Page 6 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 7.64 0.00 116.79
05/31/06 9.86 0.00 114.57
09/05/06 7.95 0.00 116.48
06/19/07 9.78 0.00 114.65
12/06/07 11.06 0.00 113.37
05/20/08 9.31 0.00 115.12
11/06/08 9.50 0.00 114.93
05/28/09 8.50 0.00 115.93
12/03/09 10.15 0.00 114.28
06/16/10 8.38 0.00 116.05
12/09/10 10.00 0.00 114.43
06/01/11 9.55 0.00 114.88
11/08/11 10.42 0.00 114.01
06/06/12 9.88 0.00 114.55
12/05/12 11.21 0.00 113.22
06/04/13 10.44 0.00 113.99
12/02/13 10.62 0.00 113.81
06/18/14 9.24 0.00 115.19
12/08/14 10.29 0.00 114.14
06/03/15 8.75 0.00 115.68
12/15/15 8.28 0.00 116.15
06/04/13 9.22 0.00 NM
06/03/15 7.48 0.00 NM
12/15/15 NM NM NM
05/12/04 7.73 0.00 114.56
05/31/06 8.97 0.00 113.32
09/05/06 5.70 0.00 116.59
06/19/07 8.88 0.00 113.41
12/06/07 10.20 0.00 112.09
05/20/08 8.24 0.00 114.05
11/06/08 8.70 0.00 113.59
05/28/09 7.74 0.00 114.55
12/03/09 11.80 0.00 110.49
06/16/10 7.34 0.00 114.95
12/09/10 9.05 0.00 113.24
06/01/11 8.62 0.00 113.67
11/08/11 9.31 0.00 112.98
06/06/12 8.64 0.00 113.65
12/05/12 NM NM NM
06/04/13 9.34 0.00 112.95
12/02/13 9.77 0.00 112.52
06/18/14 8.68 0.00 113.61
12/08/14 9.56 0.00 112.73
06/03/15 8.31 0.00 113.98
12/15/15 NM NM NM
MW-31 5 5 - 20 20 124.43
MW-32 NA NA NA NA
MW-33 5 5 - 20 20 122.29
Page 7 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 10.19 0.00 117.86
05/31/06 12.25 0.00 115.80
09/05/06 12.23 0.00 115.82
06/25/07 11.86 0.00 116.19
12/06/07 Dry -- --
05/20/08 11.83 0.00 116.22
11/06/08 11.75 0.00 116.30
05/28/09 10.28 0.00 117.77
12/03/09 8.99 0.00 119.06
06/16/10 10.81 0.00 117.24
12/09/10 10.68 0.00 117.37
06/01/11 12.60 0.00 115.45
11/08/11 13.02 0.00 115.03
06/06/12 13.77 0.00 114.28
12/05/12 12.73 0.00 115.32
06/04/13 13.94 0.00 114.11
12/02/13 13.82 0.00 114.23
06/18/14 NM NM NM
12/08/14 12.81 0.00 115.24
06/03/15 NM NM NM
12/15/15 11.70 0.00 116.35
06/08/16 9.94 0.00 118.11
02/20/17 11.43 0.00 116.62
05/16/18 12.03 0.00 116.02
11/13/18 11.81 0.00 116.24
11/07/19 12.12 0.00 115.93
11/04/20 10.65 0.00 117.40
01/04/22 12.63 0.00 115.42
02/14/23 12.04 0.00 116.01
05/12/04 7.52 0.00 117.00
05/31/06 9.77 0.00 114.75
06/19/07 9.81 0.00 114.71
12/06/07 10.95 0.00 113.57
05/20/08 9.22 0.00 115.30
11/06/08 9.51 0.00 115.01
05/28/09 8.33 0.00 116.19
12/03/09 10.17 0.00 114.35
06/16/10 8.36 0.00 116.16
12/09/10 9.91 0.00 114.61
06/01/11 9.48 0.00 115.04
11/08/11 10.40 0.00 114.12
06/06/12 9.93 0.00 114.59
12/05/12 11.18 0.00 113.34
06/04/13 10.41 0.00 114.11
12/02/13 10.63 0.00 113.89
06/18/14 9.16 0.00 115.36
12/08/14 10.27 0.00 114.25
06/03/15 8.64 0.00 115.88
12/15/15 8.26 0.00 116.26
06/08/16 8.70 0.00 115.82
02/20/17 9.27 0.00 115.25
05/16/18 9.52 0.00 115.00
11/13/18 9.38 0.00 115.14
11/07/19 10.20 0.00 114.32
11/04/20 8.74 0.00 115.78
MW-35 15 15 - 20 20 128.05
MW-36 5 5 - 20 20 124.52
Page 8 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 8.22 0.00 115.32
05/31/06 10.38 0.00 113.16
09/05/06 6.87 0.00 116.67
06/19/07 10.32 0.00 113.22
12/06/07 11.64 0.00 111.90
05/20/08 9.80 0.00 113.74
11/06/08 10.01 0.00 113.53
05/28/09 9.23 0.00 114.31
12/03/09 10.50 0.00 113.04
06/16/10 8.85 0.00 114.69
12/09/10 10.48 0.00 113.06
06/01/11 10.16 0.00 113.38
11/08/11 10.79 0.00 112.75
06/06/12 10.11 0.00 113.43
12/05/12 NM NM NM
06/04/13 10.72 0.00 112.82
12/02/13 11.13 0.00 112.41
06/18/14 10.06 0.00 113.48
12/08/14 10.98 0.00 112.56
06/03/15 9.71 0.00 113.83
12/15/15 8.97 0.00 114.57
02/20/17 9.72 0.00 113.82
05/16/18 10.06 0.00 113.48
11/13/18 9.84 0.00 113.70
11/07/19 10.74 0.00 112.80
05/12/04 6.51 0.00 113.08
06/01/06 8.45 0.00 111.14
09/05/06 4.65 0.00 114.94
06/19/07 8.55 0.00 111.04
12/06/07 11.45 0.00 108.14
05/20/08 7.76 0.00 111.83
11/06/08 7.91 0.00 111.68
05/28/09 7.31 0.00 112.28
12/03/09 7.78 0.00 111.81
06/16/10 6.82 0.00 112.77
12/09/10 8.27 0.00 111.32
06/01/11 8.18 0.00 111.41
11/08/11 8.28 0.00 111.31
06/06/12 7.76 0.00 111.83
12/05/12 NM NM NM
06/04/13 8.50 0.00 111.09
12/02/13 8.79 0.00 110.80
06/18/14 8.26 0.00 111.33
12/08/14 8.94 0.00 110.65
06/03/15 8.10 0.00 111.49
12/15/15 NM NM NM
05/12/04 5.19 0.00 114.54
05/31/06 7.46 0.00 112.27
09/05/06 3.82 0.00 115.91
06/19/07 7.60 0.00 112.13
12/06/07 8.66 0.00 111.07
05/20/08 6.77 0.00 112.96
11/06/08 6.98 0.00 112.75
05/28/09 6.18 0.00 113.55
12/03/09 7.02 0.00 112.71
06/16/10 5.73 0.00 114.00
12/09/10 7.36 0.00 112.37
06/01/11 7.23 0.00 112.50
11/08/11 7.52 0.00 112.21
06/06/12 6.96 0.00 112.77
12/05/12 NM NM NM
06/04/13 7.73 0.00 112.00
12/02/13 8.05 0.00 111.68
06/18/14 7.29 0.00 112.44
12/08/14 8.12 0.00 111.61
06/03/15 6.98 0.00 112.75
12/15/15 NM NM NM
MW-37 5 5 - 20 20 123.54
MW-39 5 5 - 17 17 119.73
MW-38 3 3 - 13 13 119.59
Page 9 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 8.04 0.00 114.52
05/31/06 9.92 0.00 112.64
06/19/07 9.96 0.00 112.60
12/06/07 NM NM NM
06/04/13 10.11 0.00 112.45
12/02/13 10.46 0.00 112.10
06/18/14 9.58 0.00 112.98
12/08/14 10.35 0.00 112.21
06/03/15 9.26 0.00 113.30
12/15/15 NM NM NM
05/12/04 3.63 0.00 113.17
05/31/06 5.31 0.00 111.49
06/19/07 5.31 0.00 111.49
12/06/07 6.24 0.00 110.56
05/20/08 4.65 0.00 112.15
11/06/08 4.83 0.00 111.97
05/28/09 4.21 0.00 112.59
12/03/09 4.87 0.00 111.93
06/16/10 3.95 0.00 112.85
12/09/10 5.00 0.00 111.80
06/01/11 5.00 0.00 111.80
11/08/11 5.20 0.00 111.60
06/06/12 4.75 0.00 112.05
12/05/12 6.10 0.00 110.70
06/04/13 5.23 0.00 111.57
12/02/13 5.49 0.00 111.31
06/18/14 4.93 0.00 111.87
12/08/14 5.56 0.00 111.24
06/03/15 4.70 0.00 112.10
12/15/15 NM NM NM
06/06/12 15.50 0.45 114.26
12/05/12 14.98 0.68 113.81
06/04/13 12.94 0.00 116.43
12/02/13 13.81 0.06 115.61
06/18/14 12.92 NM NM
06/24/14 12.92 1.71 117.92
12/08/14 9.04 0.04 120.36
06/03/15 8.68 0.00 120.69
12/15/15 9.69 0.00 119.68
06/08/16 9.09 0.00 120.28
12/15/15 11.07 0.00 117.17
06/08/16 11.37 0.00 116.87
02/20/17 12.26 0.00 115.98
05/16/18 12.39 0.00 115.85
11/13/18 12.37 0.00 115.87
11/07/19 12.88 0.00 115.36
11/04/20 11.43 0.00 116.81
01/04/22 13.18 0.00 115.06
02/14/23 14.11 0.00 114.13
12/15/15 10.02 0.00 117.08
06/08/16 10.40 0.00 116.70
02/20/17 11.19 0.00 115.91
05/16/18 11.39 0.00 115.71
11/13/18 11.37 0.00 115.73
11/07/19 11.81 0.00 115.29
11/04/20 10.42 0.00 116.68
01/04/22 12.16 0.00 114.94
02/14/23 13.02 0.00 114.08
05/12/04 9.74 0.00 112.89
05/31/06 11.57 0.00 111.06
05/12/04 7.53 0.00 117.62
05/31/06 9.56 0.00 115.59
MW-41 5 5 - 17 17 116.80
MW-40 5 5 - 17 17 122.56
MW-42 5.5 5.5 - 15.5 15.5 129.37
MW-43 5 5 - 20 20 128.24
DMW-2 39 39 - 44 44 125.15
DMW-1 40 40 - 45 45 122.63
127.10MW-44 5 5 - 20 20
Page 10 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 10.47 0.00 117.75
05/31/06 12.60 0.00 115.62
06/19/07 11.98 0.00 116.24
12/06/07 NM NM NM
12/05/12 13.98 0.00 114.24
06/04/13 13.51 0.00 114.71
12/02/13 13.43 0.00 114.79
06/18/14 11.61 0.00 116.61
12/08/14 13.11 0.00 115.11
06/03/15 10.93 0.00 117.29
12/15/15 10.86 0.00 117.36
06/08/16 11.21 0.00 117.01
02/20/17 12.11 0.00 116.11
05/16/18 12.28 0.00 115.94
11/13/18 12.26 0.00 115.96
11/07/19 12.78 0.00 115.44
11/04/20 11.26 0.00 116.96
01/04/22 13.02 0.00 115.20
02/14/23 13.96 0.00 114.26
05/12/04 7.35 0.00 117.51
05/31/06 9.22 0.00 115.64
09/05/06 9.24 0.00 115.62
06/19/07 8.97 0.00 115.89
12/06/07 10.60 0.00 114.26
05/20/08 9.06 0.00 115.80
11/06/08 9.02 0.00 115.84
05/28/09 7.51 0.00 117.35
12/03/09 10.01 0.00 114.85
06/16/10 7.93 0.00 116.93
12/09/10 9.49 0.00 115.37
06/01/11 9.05 0.00 115.81
11/08/11 10.17 0.00 114.69
06/06/12 9.87 0.00 114.99
12/05/12 NM NM NM
06/04/13 10.41 0.00 114.45
12/02/13 10.28 0.00 114.58
06/18/14 8.52 0.00 116.34
12/08/14 10.00 0.00 114.86
06/03/15 7.84 0.00 117.02
12/15/15 NM NM NM
05/12/04 11.01 0.00 112.71
05/31/06 12.84 0.00 110.88
09/05/06 11.13 0.00 112.59
06/19/07 12.88 0.00 110.84
12/06/07 13.97 0.00 109.75
05/20/08 12.17 0.00 111.55
11/06/08 12.28 0.00 111.44
05/28/09 11.65 0.00 112.07
12/03/09 12.39 0.00 111.33
06/16/10 11.26 0.00 112.46
12/09/10 12.60 0.00 111.12
06/01/11 12.60 0.00 111.12
11/08/11 12.93 0.00 110.79
06/06/12 12.60 0.00 111.12
12/05/12 NM NM NM
06/04/13 13.11 0.00 110.61
12/02/13 13.67 0.00 110.05
06/18/14 13.08 0.00 110.64
12/08/14 14.69 0.00 109.03
06/03/15 13.12 0.00 110.60
12/15/15 NM NM NM
DMW-4 40 40 - 45 45 124.86
DMW-5 41 41 - 46 46 123.72
DMW-3 40 40 -45 45 128.22
Page 11 of 12
Date: 02/24/2023 Facility ID#: 00-0-0000008172
Well No.
Date
Gauged
(mm/dd/yy)
Constructed
Well Depth
(ft. BGS)
Screened
Interval
(ft. BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Elevation
Depth to
Ground Water
(ft. BGS)
Free Product
Thickness (ft.)
Ground Water
Elevation (ft.)Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
05/12/04 11.07 0.00 111.65
05/31/06 12.78 0.00 109.94
06/19/07 12.93 0.00 109.79
12/06/07 NM NM NM
12/05/12 13.93 0.00 108.79
06/04/13 13.00 0.00 109.72
12/02/13 13.73 0.00 108.99
06/18/14 13.23 0.00 109.49
12/08/14 15.93 0.00 106.79
06/03/15 13.65 0.00 109.07
12/15/15 NM NM NM
05/12/04 15.03 0.00 104.60
06/01/06 16.94 0.00 102.69
05/12/04 8.79 0.00 111.00
06/01/06 10.56 0.00 109.23
09/05/06 7.44 0.00 112.35
06/19/07 10.50 0.00 109.29
12/06/07 9.36 0.00 110.43
05/20/08 9.53 0.00 110.26
11/06/08 9.72 0.00 110.07
05/28/09 9.14 0.00 110.65
12/03/09 9.96 0.00 109.83
06/16/10 8.23 0.00 111.56
12/09/10 10.01 0.00 109.78
06/01/11 9.98 0.00 109.81
11/08/11 10.39 0.00 109.40
06/06/12 10.05 0.00 109.74
12/05/12 NM NM NM
06/04/13 10.63 0.00 109.16
12/02/13 11.71 0.00 108.08
06/18/14 11.21 0.00 108.58
12/08/14 13.71 0.00 106.08
06/03/15 11.72 0.00 108.07
12/15/15 NM NM NM
05/12/04 7.32 0.00 112.55
05/31/06 9.30 0.00 110.57
09/05/06 6.22 0.00 113.65
06/19/07 9.32 0.00 110.55
12/06/07 10.20 0.00 109.67
05/20/08 8.42 0.00 111.45
11/06/08 8.53 0.00 111.34
05/28/09 7.90 0.00 111.97
12/03/09 8.61 0.00 111.26
06/16/10 7.23 0.00 112.64
12/09/10 8.89 0.00 110.98
06/01/11 8.89 0.00 110.98
11/08/11 9.13 0.00 110.74
06/06/12 8.73 0.00 111.14
12/05/12 NM NM NM
06/04/13 9.35 0.00 110.52
12/02/13 9.74 0.00 110.13
06/18/14 9.26 0.00 110.61
12/08/14 10.77 0.00 109.10
06/03/15 9.41 0.00 110.46
12/15/15 NM NM NM
01/04/22 10.70 0.00 115.76
02/14/23 12.08 0.04 114.41
01/04/22 11.82 0.00 114.03
02/14/23 11.97 0.36 114.19
Notes:
• Ground water elevations relative to mean sea level; data reported in feet.
• Ground water elevations corrected for presence of free product with assumed density of 0.8581, if applicable.
• NM: Not measured.
• DMW-1, DMW-2 and DMW-7 were abandoned 06/29/06.
DMW-6 40.7 40.7 - 45.7 45.7 122.72
• During the December 5, 2012 monitoring event: MW-1R and MW-3R were covered; MW-21 could not be located; MW-20
was located and sampled instead.
DMW-8 40 40 - 45 45 119.79
DMW-7 65 65 - 70 70 119.63
8 8 - 18 18 125.85EPCO-102
EPCO-101 8 8 - 18 18 126.46
DMW-9 40 40 - 45 45 119.87
Page 12 of 12
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100
08/28/02 140 880 310 1,480 <100 60.0 NR NR NR NR NR
05/12/04 2,800 4,400 1,700 4,400 7,000 370 NR NR NR NR NR
05/31/06 NS NS NS NS NS NS NS NS NS NS NS
08/28/02 140 <10 370.00 <40 28.0 56.0 NR NR NR NR NR
05/12/04 FP FP FP FP FP FP FP FP FP FP FP
05/31/06 FP FP FP FP FP FP FP FP FP FP FP
09/06/06 FP FP FP FP FP FP FP FP FP FP FP
06/19/07 FP FP FP FP FP FP FP FP FP FP FP
12/06/07 FP FP FP FP FP FP FP FP FP FP FP
05/20/08 FP FP FP FP FP FP FP FP FP FP FP
11/06/08 FP FP FP FP FP FP FP FP FP FP FP
05/28/09 642 413 3,860 9,690 <33.0 1,190 <33.0 353 893 6,920 1,910
12/03/09 FP FP FP FP FP FP FP FP FP FP FP
06/16/10 339 155 2,720 5,990 88.5 1,480 <4.40 300 720 930 1,500
12/09/10 582 51.5 J 2,360 3,450 123 1,120 <22.0 235 508 3,630 747
06/01/11 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/05/12 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
06/04/13 515 80.4 63.8 1,680 101 804 <2.5 56.6 175 1,240 748
12/02/13 1,130 444 562 3,330 84.1 799 <2.5 38.7 96.7 1,880 887
06/19/14 434 381 1,880 3,320 49.2 832 <2.0 298 898 3,240 786
12/09/14 545 81.3 855 1,890 57.1 779 <10 78.4 228 2,070 682
06/04/15 223 35.2 1,370 2,120 38.6 956 <8.2 163 454 2,070 721
12/15/15 517 61.3 1,620 3,070 73.0 1,240 <1.6 114 259 2,070 650
06/08/16 250 13.1 650 269 34.6 1,330 <2.5 89.2 209 160 202
02/20/17 647 74.7 1,480 3,400 55.8 1,140 <3.1 64.8 134 1,410 638
05/16/18 461 15.9 1,190 99.2 42.7 1,200 NR NR NR NR NR
11/13/18 170 14.5 613 97.5 <1.3 684 NR NR NR NR NR
11/07/19 163 6.8 J 403 27.1 J 19.5 798 NR NR NR NR NR
11/04/20 26.7 0.97 J 27.9 9.7 11.2 226 NR NR NR NR NR
01/04/22 58.3 <13 28.5 J <25 20.1 J 291 NR NR NR NR NR
02/14/23 NS NS NS NS NS NS NS NS NS NS NS
04/16/97 12.0 138 36 140 16 NR NR NR NR NR NR
05/12/04 620 120 96 390 160 <100 NR NR NR NR NR
05/31/06 NS NS NS NS NS NS NS NS NS NS NS
06/16/10 NS NS NS NS NS NS NS NS NS NS NS
08/28/02 8.0 <1 1 3 2 <1 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 68.2 0.520 8.12 5.89 200 2.75 NR NR NR NR NR
12/06/07 79.5 1.44 13.8 26.6 153 6.29 <0.500 2.12 1.05 11.5 1.73
05/20/08 84.9 0.880I 0.470I 8.04 129 2.56 <1.0 0.560I <1.0 4.79 <1.0
11/06/08 250 4.4 J 26 110 160 6.60 B 1.10 J <0.75 3.2 J 27 3.1 J
05/28/09 33.5 0.836 J 1.90 J 4.41 31.1 1.38 J <0.330 0.390 J <0.330 2.04 <0.330
12/03/09 16.6 <0.190 2.65 5.94 16.8 1.16 <0.220 0.369 J 0.358 J 2.86 0.469 J
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 27.9 <0.380 3.65 1.40 J 86.3 4.15 <0.440 1.86 J <0.440 1.50 J <0.360
06/01/11 21.9 0.44 J 0.91 0.86 J 64.0 1.6 0.21 J 0.19 J 0.13 J 0.59 <0.10
11/08/11 165 2.6 57.3 25.6 100 15.5 2.40 3.3 4.8 31.4 1.8
06/06/12 196 4.3 48.0 62.0 84.1 9.70 1.60 J 2.2 J 3.2 23.2 1.9 J
12/05/12 433 6.6 147 213 226 37.6 5.40 5.6 11.7 56.7 8.6
06/04/13 133 1.4 41.2 17.39 115 15.9 3.00 2.1 3.5 7.5 0.79
12/02/13 299 6.4 80.7 89.3 192 26.1 4.70 4.0 6.6 32.4 3.3
06/19/14 438 8.7 75.9 65.5 167 39.2 3.90 6.0 7.9 36.0 3.6
12/09/14 397 7.8 J 105 178 104 34.3 3.40 J 4.7 J 8.8 J 63.7 13
06/04/15 13.1 <0.17 1.2 <0.43 18.7 2.1 0.23 J 0.43 J <0.16 0.81 <0.14
12/15/15 0.74 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 0.15 J <0.14
02/20/17 55.6 0.85 7.1 4.6 15.6 2.8 0.45 J 0.59 0.87 2.6 <0.13
05/16/18 73.3 0.68 2 2.2 33.6 16.2 NR NR NR NR NR
11/13/18 17.8 <0.13 2.4 0.48 J 3.6 0.86 NR NR NR NR NR
11/07/19 143 4.7 43.5 87.5 20.2 13.2 NR NR NR NR NRBenzeneMW-3R
MAC (µg/l)
GCL (µg/l)
MW-1R
MW-11
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzeneMW-2R
Page 1 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 960 66 47 210 <80 <40 NR NR NR NR NR
05/12/04 380 140 72 320 100 24.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 14 <2.0 NR NR NR NR NR
09/06/06 5.2 <1.0 <1.0 <3.0 1.6 <2.0 NR NR NR NR NR
06/21/07 741 543 183 526 255 <50.0 NR NR NR NR NR
12/06/07 561 23.1 86.3 121 94.1 31.6 <0.500 7.69 12.9 104 23
05/20/08 479 12.2 142 362 153 27.5 4.32 4.54 9.04V 101 6.03
11/06/08 350 3.6 32 3.7 99.0 14 B 3.80 7.4 5.3 20 0.14 J
05/28/09 148 1.25 19.0 7.51 55.0 14.7 1.54 3.30 2.41 29.8 2.14
12/03/09 9.32 <0.190 7.42 6.20 1.12 3.27 <0.220 1.07 2.39 12.1 2.32
06/16/10 167 3.08 J 22.0 10.2 54.6 8.55 1.34 J 2.14 J 1.99 J 14.4 0.776 J
12/09/10 208 2.67 J 38.0 37.8 88.0 28.3 <1.10 6.12 3.81 J 58.1 5.54
06/01/11 216 1.5 28.6 14.71 80.0 28.5 2.0 4.3 5.1 41.1 3.7
11/08/11 457 22.2 93.8 68.7 69.0 37.1 1.4 J 10.6 18.1 80.6 10.8
06/06/12 655 6.5 93.5 16.2 52.2 53.8 <1.6 13.0 19.8 52.8 3.6 J
12/05/12 531 9.2 J 121 81.1 38.1 43.5 <2.0 7.5 J 16.0 50.5 9.2 J
06/04/13 324 3.0 49.2 11.23 24.4 44.8 0.42 J 6.2 7.5 13.6 0.96
12/02/13 326 4.2 75.4 52.9 18.6 48.6 0.59 9.8 13.8 28.7 6.8
06/19/14 179 3.6 47.3 24.4 11.4 28.7 0.48 J 5.0 5.0 9.9 2.0
12/09/14 592 106 191 290 18.2 65.6 <2.5 9.0 J 22.7 87.5 26.8
06/04/15 159 1.2 33.9 5.2 25.8 15.0 0.85 2.1 2.8 2.8 0.39 J
12/15/15 360 5.4 81.6 3.8 26.5 38.1 0.9 3.7 6.7 4.6 <0.14
06/08/16 320 31 74.5 59.5 52.4 32.8 2.0 J 3.8 J 6.5 35.5 5.2
02/20/17 244 4.8 J 36.5 6.7 J 19.9 41.6 <1.3 1.8 J 3.8 J 8.5 <1.3
05/16/18 139 1.8 J 44.4 12.7 5.7 31.5 NR NR NR NR NR
11/13/18 243 10.3 87.2 29.6 4.0 J 32.0 NR NR NR NR NR
11/07/19 224 3.0 J 54.6 23.7 14.3 21.5 NR NR NR NR NR
08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 6.1 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 4.7 <2.0 NR NR NR NR NR
06/21/07 <0.500 <0.500 <0.500 <0.500 1.15 <0.500 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
05/20/08 <1.0 <1.0 <1.0 1.68I 0.540I 1.10 <1.0 <1.0 <1.0 0.680I <1.0
11/06/08 <0.11 <0.10 0.27 J 1.2 J 0.66 J 0.80 JB <0.10 <0.15 <0.11 0.40 J <0.13
05/28/09 0.222 J <0.330 <0.670 <1.33 5.90 <1.00 <0.330 <0.330 <0.330 0.343 J <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 0.483 J <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 5.63 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 0.286 J 0.617 J <0.250 <0.500 <0.220 <0.150 <0.220 0.543 J 0.189 J
06/01/11 32.9 169 31.0 114.3 <0.13 6.10 <0.16 1.1 2.7 12.2 3.2
11/08/11 31.9 53.3 26.9 97.3 <0.13 5.6 <0.16 1.2 2.7 12.1 3.1
06/06/12 18.8 31.4 14.2 70.0 <0.13 3.1 <0.16 0.69 1.3 8.6 2.2
12/05/12 47.5 199 64.4 224 <0.20 12.2 <0.20 2.1 6.4 26.0 6.1
06/04/13 23.6 101 28.9 109 <0.10 6.50 <0.10 1.1 2.8 12.9 3.1
12/02/13 10.1 49.7 13.5 51.2 <0.10 2.2 <0.10 0.38 J 1.2 4.5 1.2
06/19/14 <0.10 <0.10 <0.10 <0.20 3.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 63.5 530 94 446 <2.5 17.7 <2.5 2.8 J 8.0 J 50.8 12.8 J
06/04/15 12.2 39.5 15.1 56 <0.16 4.6 <0.16 0.74 1.9 8.9 1.8
12/15/15 18.4 49.6 26.8 94.6 <0.16 7.10 <0.16 1 2.9 15 1.7
06/08/16 10.8 65.8 8.1 37.2 <0.13 1.9 <0.13 0.36 J 0.63 2.8 0.65
02/20/17 1.40 6.4 1.5 5.7 <0.13 0.36 J <0.13 <0.13 <0.13 0.73 0.24 J
05/16/18 0.19 J 0.43 J <0.13 0.53 J <0.13 <0.13 NR NR NR NR NR
11/13/18 41.0 357 69.1 344 <1.3 16.5 NR NR NR NR NR
MW-17
MW-12
Page 2 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
06/01/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/25/07 Dry Dry Dry Dry Dry Dry NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
12/03/09 <0.140 <0.190 <0.150 1.41 <0.250 <0.500 <0.220 <0.150 <0.220 0.646 J 0.585 J
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 0.479 J 0.968 J <0.250 <0.500 <0.220 <0.150 <0.220 1.05 0.336 J
06/01/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.15 J <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 0.87 J <0.10 1.1 <0.10 <0.10 <0.10 3.2 2.0
06/19/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
02/20/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
08/28/02 330 15 40 158 110 <10 NR NR NR NR NR
05/12/04 NS NS NS NS NS NS NS NS NS NS NS
06/01/06 NS NS NS NS NS NS NS NS NS NS NS
12/05/12 103 2.3 22.7 18.9 57.8 6.80 0.37 J 1.4 1.5 5.0 0.62
06/04/13 23.2 0.43 J 12.6 0.36 J 39.3 8.00 0.20 J 1.0 1.2 0.48 J <0.10
12/02/13 6.5 0.30 J 3.3 0.63 J 29.5 4.5 0.22 J 0.52 0.24 J 0.23 J <0.10
06/19/14 37.0 0.27 J 5.9 0.54 J 45.5 5.9 0.29 J 1.1 0.51 0.50 <0.10
12/09/14 914 1,660 246 1,080 87.7 48.7 J <10 <10 18.4 J 121 27.5 J
06/04/15 234 16.5 68.1 161 18.2 17.2 0.23 J 2.8 5.1 30.6 4.1
12/15/15 186 21.9 54.6 101 15 17.6 0.21 J 2.3 3.7 24.7 2
06/08/16 179 8.6 77.2 183 3.9 17.9 <0.13 3.1 5 28.7 3.6
02/20/17 451 36.1 160 245 24.9 37.0 <2.5 4.0 J 6.5 J 76.2 8.5 J
05/16/18 268 2.7 38.8 46.6 28.4 25.0 NR NR NR NR NR
11/13/18 66.5 8.3 11.5 10.4 10.8 8.20 NR NR NR NR NR
11/07/19 430 40.0 187 469 6.2 46.1 NR NR NR NR NR
11/04/20 57.5 0.30 J 2.9 0.92 J 5.8 2.0 NR NR NR NR NR
01/04/22 64.6 <13 31.0 J 29.8 J <13 <13 NR NR NR NR NR
02/14/23 0.868 4.7 1.37 7.14 <0.140 <0.470 <0.150 <0.180 0.364 J 2.29 0.752
08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 1.60 <1.0 16 5.3 <1.0 8.50 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/25/07 NS NS NS NS NS NS NS NS NS NS NS
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/18/14 NS NS NS NS NS NS NS NS NS NS NS
12/09/14 NS NS NS NS NS NS NS NS NS NS NS
06/03/15 NS NS NS NS NS NS NS NS NS NS NS
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
MW-19
MW-21
MW-20
Page 3 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/13/04 1.10 <1.0 <1.0 <2.0 5.4 <2.0 NR NR NR NR NR
06/01/06 <1.0 <1.0 <1.0 <3.0 21.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/25/07 <1.00 <1.00 <1.00 <3.00 102 <5.00 NR NR NR NR NR
12/06/07 36.8 <0.500 2.89 1.98 183 <5.00 1.87 1.85 <0.500 4.31 <0.500
05/20/08 124 12.5 10.5 24.0 96.6 2.56 0.310I 1.27 2.09V 8.39 0.860I
11/06/08 26.0 0.16 J 1.4 0.20 J 140 1.4 B 0.56 J 0.95 J 0.15 J 1.5 <0.13
05/28/09 58.1 2.57 8.56 12.4 70.2 2.53 <0.330 0.847 J 0.546 J 5.36 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 50.3 0.346 J 3.61 1.46 57.6 1.40 0.290 J 0.500J 0.248 J 1.71 <0.180
12/09/10 14.9 0.199 J 1.30 <0.220 84.4 2.87 <0.220 1.05 <0.220 0.153 J <0.180
06/01/11 2.2 <0.13 0.44 J <0.30 33.7 0.19 J <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 40.4 1.1 14.5 3.9 88.8 3.1 1.20 1.7 1.5 2.6 0.17 J
06/06/12 21.5 0.26 J 0.27 J 1.7 8.9 0.38 J <0.16 0.13 J <0.11 0.67 <0.10
12/05/12 66.0 0.83 21.3 6.3 128 11.8 2.20 1.9 2.5 5.5 0.45 J
06/04/13 1.60 <0.10 0.14 J <0.22 11.2 0.22 J 0.15 J <0.10 <0.10 <0.10 <0.10
12/02/13 0.28 J <0.10 0.18 J <0.22 29.3 0.20 J 0.42 J <0.10 <0.10 <0.10 <0.10
06/19/14 167 21.0 23.2 20.2 88.1 7.70 1.70 1.6 2.1 12.7 0.61
12/09/14 206 15.9 49 84.4 128 14.2 2.9 J 2.5 J 3.7 J 29.1 4.0 J
06/04/15 26.6 2.3 2.6 3.5 20.7 2.2 <0.16 0.39 J 0.31 J 0.89 <0.14
12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
02/20/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 13.3 0.15 J 0.85 0.97 J 3.3 4.6 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/07/19 21.7 0.78 6.1 2.9 18.3 2.8 NR NR NR NR NR
11/04/20 13.7 0.94 4.1 1.8 6.5 0.77 NR NR NR NR NR
01/04/22 11.6 0.29 J 4.7 0.40 J 2 1.5 NR NR NR NR NR
02/14/23 0.330 J 1.72 0.59 2.85 <0.140 <0.470 <0.150 <0.180 <0.190 0.96 0.284 J
09/10/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 22 97 180 840 <1.0 53.0 NR NR NR NR NR
05/31/06 <10 29 260 1,320 <10 92.0 NR NR NR NR NR
06/21/07 14.5 180 253 1,140 1.82 102 NR NR NR NR NR
12/06/07 23.1 107 624 2,840 1.92 116 <0.500 23.0 55.5 474 111
05/20/08 1.72 8.46 77.4 309 <1.0 11.6 <1.0 2.51 6.71V 48.9 9.72
11/06/08 7.30 47 120 540 <0.10 30 B <0.10 11 14 110 24
05/28/09 11.8 23.3 120 539 <0.660 38.6 <0.660 8.32 17.5 138 35.2
12/03/09 44.0 126 681 2,640 <1.25 163 <1.10 34.9 75.5 584 156
06/16/10 5.84 29.6 115 525 0.669 J 27.6 <0.440 5.34 9.63 104 22.1
12/09/10 5.15 J 37.6 205 925 <2.50 57.6 <2.20 13.7 16.3 168 35.9
06/01/11 10.4 41.0 214 690 0.90 55.7 <0.16 16.0 26.9 148 16.9
11/08/11 41.2 131 636 2,490 4.5 J 185 <1.3 42.6 88.6 702 153
06/06/12 27.5 10.8 242 853 4.6 84.9 <0.82 22.8 44.0 352 67.8
12/05/12 28.4 13.8 211 661 6.0 71.1 <1.0 16.8 39.7 292 51.6
06/04/13 14.7 1.5 46.4 112 4.1 27.8 <0.10 7.8 12.8 69.6 8.9
12/02/13 7.70 0.25 J 0.25 J 2.4 3.4 2.0 <0.10 0.38 J <0.10 4.2 0.19 J
06/19/14 8.70 <0.10 0.84 0.37 J 5.6 2.0 <0.10 0.55 0.27 J 0.19 J <0.10
12/09/14 19.9 80.2 217 982 2.6 J 80.5 <2.5 16.3 34 332 60.6
06/04/15 5.50 7.7 56.6 179 0.53 29.6 <0.16 5.4 9.6 56.9 9.8
12/15/15 4.10 5.5 28 139 0.64 19.1 <0.16 3.6 6.2 49.6 9.5
06/08/16 4.60 J 51.4 228 1,190 <1.3 76.2 <1.3 11.2 24.5 240 44.5
02/20/17 5.60 8.4 79.3 262 0.20 J 54.7 <0.13 9.7 15.2 160 17.1
05/16/18 0.91 <0.13 0.75 0.85 J 0.20 J 1.1 NR NR NR NR NR
11/13/18 15.1 21.9 192 688 <1.3 75.0 NR NR NR NR NR
11/07/19 5.0 16.6 266 1,110 <1.3 82.6 NR NR NR NR NR
MW-25
MW-22
Page 4 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 4.80 <1.0 <1.0 <2.0 14 <2.0 NR NR NR NR NR
05/31/06 220 2.6 2.5 2.4 74.0 6.90 NR NR NR NR NR
06/21/07 161 0.960 3.28 1.58 68.5 2.78 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
05/20/08 52.4 <1.0 <1.0 1.77I 22.8 1.22 <1.0 1.20 <1.0 0.650I <1.0
11/06/08 44.0 0.31 J 0.30 J 0.99 J 43.0 0.49 JB <0.20 2.0 J <0.22 0.27 J <0.26
05/28/09 5.71 0.415 J <0.670 <1.33 46.5 2.57 <0.330 3.73 <0.330 <0.330 1.25
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 3.35 <0.190 0.388 J <0.220 15.5 0.926 J <0.220 0.641 J <0.220 <0.150 <0.180
12/09/10 0.325 J <0.190 0.309 J 0.647 J 37.7 1.73 <0.220 2.71 <0.220 <0.150 <0.180
06/01/11 0.48 J <0.13 <0.15 <0.30 26.7 0.33 J <0.16 1.0 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 0.27 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 0.16 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/19/14 <0.10 <0.10 <0.10 <0.20 0.23 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 0.31 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/15 <0.17 <0.17 <0.15 <0.43 0.42 J <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
08/28/02 5.00 <1 <1 <4 9 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 7.40 8.0 65 210 1.7 25.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 0.560 <0.500 1.07 <0.500 <0.500 1.92 NR NR NR NR NR
12/06/07 46.0 47.7 252 844 11.2 78.3 <0.500 18.4 29.2 265 21.4
05/20/08 7.00 1.12 96.1 42.5 1.15 22.3 <1.0 4.46 7.73V 46.1 0.650I
11/06/08 4.30 0.49 J 15 2.1 J 0.66 J 10 B <0.10 4.6 1.1 24 <0.13
05/28/09 0.901 J <0.330 0.842 J <1.33 <0.330 7.49 <0.330 1.70 <0.330 0.378 J <0.330
12/03/09 0.862 J <0.190 <0.150 <0.220 1.07 <0.500 <0.220 <0.150 <0.220 0.563 J <0.180
06/16/10 5.82 0.724 J 17.4 <0.220 1.02 15.7 <0.220 3.91 1.34 1.35 <0.180
12/09/10 6.87 5.00 47.9 47.4 1.39 J 26.7 <0.440 5.40 3.26 44.3 1.92 J
06/01/11 2.90 1.1 25.3 28.3 0.34 J 28.1 <0.16 5.0 2.1 18.8 <0.10
11/08/11 3.70 0.21 J 2.0 1.8 3.3 11.7 <0.16 2.3 <0.11 6.5 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 2.7 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 5.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 3.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 2.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 3.6 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 2.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/15 0.18 J <0.17 <0.15 <0.43 0.33 J 0.30 J <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
02/20/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <0.13 <0.13 <0.13 <0.25 0.45 J <0.13 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/07/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
MW-26
MW-27
Page 5 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 780 <40 67 320 100 <40 NR NR NR NR NR
05/12/04 1.40 <1.0 <1.0 <2.0 9.4 <2.0 NR NR NR NR NR
05/31/06 100 <1.0 1.4 1.5 59.0 5.7 NR NR NR NR NR
09/06/06 220 <5.0 <5.0 12 78.0 <10 NR NR NR NR NR
06/21/07 651 80.0 92.0 160 292 <50.0 NR NR NR NR NR
12/06/07 682 50.4 89.3 145 125 47.6 <0.500 12.9 11.5 139 13.2
05/20/08 84.8 1.15 5.16 5.52 36.2 5.99 <1.0 1.62 2.42V 16.3 0.660I
11/06/08 88.0 0.55 J 2.5 1.0 J 58.0 2.3 B 0.96 J 1.8 0.16 J 12 0.16 J
05/28/09 83.7 1.34 10.0 3.57 J 54.4 5.90 0.942 J 1.22 0.987 J 10.2 <0.330
12/03/09 328 6.81 46.4 28.3 68.8 32.5 <0.220 11.5 5.68 65.8 2.30
06/16/10 57.6 0.315 J 2.14 <0.220 44.8 3.64 0.515 J 0.722 J 0.253 J 4.47 <0.180
12/09/10 132 <0.380 13.3 <0.440 64.9 11.4 <0.440 4.08 1.40 J 9.73 <0.360
06/01/11 27.7 0.14 J 1.9 <0.30 40.5 2.3 0.46 J 0.34 J 0.20 J <0.10 <0.10
11/08/11 315 4.7 69.9 39.6 57.3 48.8 1.20 18.6 16.6 29.9 5.8
06/06/12 65.4 1.3 J 20.3 <3.0 51.5 8.2 <1.6 4.2 J 3.6 J <1.0 <1.0
12/05/12 254 2.2 J 25.9 12.1 281 19.8 <1.0 5.8 3.4 J 7.7 2.8 J
06/04/13 122 1.0 20.8 3.8 193 16.1 0.50 6.4 2.9 4.6 0.47 J
12/02/13 226 2.1 J 36.0 19.4 303 18.6 <1.0 4.4 J 3.5 J 6.8 3.0 J
06/18/14 9.90 <0.10 3.1 <0.20 89.2 4.9 0.11 J 1.5 0.75 <0.10 <0.10
12/09/14 47.1 0.84 J 88.2 16.5 107 35.4 0.37 J 18.4 25.5 23.5 4.8
06/04/15 38.0 0.7 2.2 0.61 J 28.6 3.9 0.33 J 0.55 0.36 J 2.8 <0.14
12/15/15 1.60 <0.17 0.15 J <0.43 4.9 0.39 J <0.16 <0.12 <0.16 0.22 J <0.14
06/08/16 5.70 <0.13 0.30 J <0.31 15.7 1 0.33 J 0.16 J <0.13 <0.13 <0.13
02/20/17 0.24 J <0.13 <0.13 <0.25 3.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 1.60 <0.13 0.36 J <0.25 14.4 0.29 J NR NR NR NR NR
11/13/18 0.25 J <0.13 0.22 J <0.25 1.5 0.25 J NR NR NR NR NR
11/07/19 192 10.3 48.6 9.8 17.4 28.2 NR NR NR NR NR
09/10/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 1.90 <1.0 1.1 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 50.0 3 18 11 3.9 45.0 NR NR NR NR NR
06/19/07 66.2 3.00 43.5 30.4 11.1 39.4 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
12/03/09 0.309 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 0.576 J <0.180
06/16/10 <0.140 1.23 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 31.7 <0.190 0.485 J 1.30 9.82 0.735 J <0.220 0.726 J 0.256 J 1.21 <0.180
06/01/11 0.48 J <0.13 <0.15 <0.30 1.3 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 2.9 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 18.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 1.6 0.27 J <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 6.90 <0.10 <0.10 <0.22 13.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/19/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 0.43 J 0.23 J 2.1 <0.10 <0.10 0.20 J 1.2 1.1
06/04/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
MW-29
MW-28
Page 6 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene09/10/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 6.00 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 39.0 <1.0 <1.0 1.3 2.9 7.30 NR NR NR NR NR
06/19/07 69.2 1.61 0.700 1.22 7.16 2.10 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
05/20/08 14.3 <1.0 <1.0 1.48I 2.01 1.02 0.450I 0.710I <1.0 0.650I <1.0
11/06/08 2.90 0.60 J <0.13 0.40 J 0.16 J 0.19 JB <0.10 <0.15 <0.11 0.11 J <0.13
05/28/09 5.97 0.516 J <0.670 <1.33 0.949 J <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 0.40 J <0.13 <0.15 <0.30 0.82 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 0.14 J <0.10 <0.10 <0.22 11.9 <0.15 0.26 J <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/19/14 <0.10 53.3 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/15 <0.17 5.2 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
08/28/02 <1 <1 <1 <4 73.0 <1 NR NR NR NR NR
05/12/04 230 <1.0 <1.0 <2.0 3,500 <2.0 NR NR NR NR NR
05/31/06 <5.0 <5.0 <5.0 <15.0 170 <10 NR NR NR NR NR
09/06/06 <5.0 <5.0 <5.0 <15.0 71.0 <10 NR NR NR NR NR
06/21/07 80.8 <0.500 <0.500 <5.00 1,010 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 61.1 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 8.00 <1.0 <1.0 <30 376 <10 <10 <10 <10 2.70I <10
11/06/08 3.80 <0.38 <0.30 <0.24 150 <0.14 <0.22 <0.24 <0.44 <0.28 <0.26
05/28/09 42.0 <1.65 4.15 J 12.8 J 886 6.23 J <1.65 <1.65 <1.65 6.43 <1.65
12/03/09 <0.140 <0.190 <0.150 <0.220 21.1 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 11.4 <1.90 <1.50 2.54 J 468 <5.00 <2.20 <1.50 <2.20 <1.50 <1.80
12/09/10 39.4 <0.380 <0.300 <0.440 301 <1.00 <0.440 <0.300 <0.440 <0.300 <0.360
06/01/11 2.40 <0.13 <0.15 <0.30 13.9 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 8.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 6.8 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 2.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 8.50 <0.10 <0.10 <0.20 58.8 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 8.60 <0.10 <0.10 <0.20 22.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 9.80 <0.17 <0.15 <0.43 73.3 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 <0.17 <0.17 <0.15 <0.43
0.22 J <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 NS NS NS NS NS NS NS NS NS NS NS
06/03/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
MW-30
MW-31
MW-32
Page 7 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene08/28/02 <1 <1 <1 <4 10 <1 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 2.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 1.3 <2.0 NR NR NR NR NR
06/19/07 <0.500 <0.500 <0.500 <0.500 4.04 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 4.15 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 1.79 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 2.5 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/28/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 1.23 0.407 J
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 1.53 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 0.27 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 12.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 7.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 1.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 1.8 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
11/19/02 1,200 <50 <50 <200 120 NR NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 4.0 <2.0 NR NR NR NR NR
09/06/06 1.70 <1.0 <1.0 <3.0 7.5 <2.0 NR NR NR NR NR
06/25/07 215 67.2 22.0 31.1 12.6 <5.00 NR NR NR NR NR
12/06/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
05/20/08 <1.0 <1.0 <1.0 <3.0 17.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 130 2.1 4.5 1.3 J 12 0.10 JB 1.40 0.56 J 0.23 J 2.1 <0.13
05/28/09 <0.200 <0.330 <0.670 <1.33 1.42 <1.00 <0.330 <0.330 <0.330 0.927 J 0.387 J
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 0.211 J <0.190 <0.150 <0.220 1.47 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 46.9 2.21 4.14 5.03 1.96 J <1.00 <0.440 1.59 J 0.593 J 3.33 0.811 J
06/01/11 <0.13 <0.13 <0.15 <0.30 0.29 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 2.00 <0.13 <0.15 <0.30 0.97 <0.10 0.25 J <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 0.16 J <0.15 <0.30 0.81 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 6.90 <0.10 0.66 <0.22 1.0 <0.15 0.22 J <0.10 <0.10 <0.10 <0.10
06/04/13 0.14 J <0.10 0.11 J <0.22 0.22 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 0.75 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/19/14 0.27 J 0.33 J 0.17 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 0.82 0.17 J <0.10 <0.20 0.24 J 0.31 J <0.10 <0.10 <0.10 0.29 J 0.16 J
06/04/15 0.25 J <0.17 <0.15 <0.43 <0.16 0.25 J <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 0.9 <0.17 <0.15 <0.43 0.34 J <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/08/16 0.27 J <0.13 0.39 J <0.31 4.7 0.24 J <0.13 <0.13 <0.13 <0.13 <0.13
02/20/17 <0.13 <0.13 <0.13 <0.25 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/07/19 0.43 J <0.13 <0.13 <0.25 0.37 J <0.13 NR NR NR NR NR
11/04/20 0.25 J <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
01/04/22 <25 <25 <25 <50 <25 26.9 J NR NR NR NR NR
02/14/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.150 <0.180 <0.190 <0.190 <0.190
MW-33
MW-35
Page 8 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene03/21/03 4.00 <1 1 <4 5,300 5 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 1,100 <2.0 NR NR NR NR NR
05/31/06 200 <25 <25 <75 6,300 <50 NR NR NR NR NR
06/21/07 445 <50.0 <50.0 107 5,000 <50.0 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 6,040 <5.00 <0.500 2.2 <0.500 <0.500 <0.500
05/20/08 44.0 3.25 2.72 7.58 4,140 2.61 0.960I 4.81 1.87V 3.95 0.550I
11/06/08 26 J <9.5 <7.5 <6.0 3,700 9.20 J <5.5 <6.0 <11 7.5 J 6.7 J
05/28/09 71.7 <3.30 <6.70 27.1 J 1,160 <10.0 <3.30 4.14 J <3.30 17.5 <3.30
12/03/09 <0.140 <0.190 <0.150 <0.220 576 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 52.8 <3.80 3.27 J 13.2 J 1,120 <10.0 <4.40 <3.00 <4.40 8.10 J 3.79 J
12/09/10 166 2.69 J 19.1 52.9 1,070 21.4 <2.20 <1.50 <2.20 26.0 3.78 J
06/01/11 46.6 1.3 1.6 5.8 971 4.9 0.70 1.7 0.18 J 3.6 <0.10
11/08/11 <2.6 <2.6 6.4 J 22.6 J 848 3.8 J <3.3 <2.0 <2.1 5.4 J <2.0
06/06/12 <0.13 <0.13 <0.15 <0.30 179 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.50 <0.50 <0.50 <1.1 1,110 <0.74 <0.50 <0.50 <0.50 <0.50 <0.50
06/04/13 0.23 J <0.10 <0.10 <0.22 989 <0.15 0.23 J <0.10 <0.10 <0.10 <0.10
12/02/13 1.50 J <1.0 <1.0 <2.2 399 2.2 J <1.0 <1.0 <1.0 <1.0 <1.0
06/18/14 1.40 <0.10 0.56 0.54 J 308 0.61 0.25 J 0.28 J <0.10 0.29 J <0.10
12/09/14 0.17 J <0.10 <0.10 <0.20 294 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 104 1.3 18.6 5 151 16.5 0.26 J 3.9 2.8 13.2 0.26 J
12/15/15 <0.17 <0.17 <0.15 <0.43 149 0.56 0.19 J <0.12 <0.16 <0.14 <0.14
06/08/16 8.10 0.37 J 3.9 <0.31 59.8 2.2 0.14 J 0.78 0.46 J 0.30 J <0.13
02/20/17 <0.13 <0.13 <0.13 <0.25 16.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <0.13 <0.13 <0.13 <0.25 2.9 <0.13 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 1.9 <0.13 NR NR NR NR NR
11/07/19 <0.13 <0.13 <0.13 <0.25 0.26 J <0.13 NR NR NR NR NR
11/04/20 11.6 0.54 2.6 1.3 J 18.7 4 NR NR NR NR NR
03/21/03 14.0 <1 <1 <4 420 <1 NR NR NR NR NR
05/13/04 5.10 <1.0 <1.0 <2.0 450 <2.0 NR NR NR NR NR
05/31/06 <10 <10 <10 <30 310 <20 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 8.7 <2.0 NR NR NR NR NR
06/19/07 4.33 <0.500 <0.500 <0.500 548 <0.500 NR NR NR NR NR
12/06/07 5.55 <0.500 <0.500 <1.00 1,500 <5.00 1.22 <0.500 <0.500 <0.500 <0.500
05/20/08 1.33 <1.0 <1.0 <3.0 668 0.900I 1.16 0.970I <1.0 <1.0 <1.0
11/06/08 <1.4 <1.9 <1.5 <1.2 700 <0.70 <1.1 <1.2 <2.2 <1.4 <1.3
05/28/09 <1.00 <1.65 <3.35 <6.65 382 <5.00 <1.65 <1.65 <1.65 <1.65 <1.65
12/03/09 0.795 J <0.190 <0.150 <0.220 626 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 0.392 J <0.190 <0.150 <0.220 401 <0.500 0.848 J 0.200 J <0.220 <0.150 <0.180
12/09/10 <0.700 <0.950 <0.750 <1.10 248 <2.50 <1.10 <0.750 <1.10 <0.750 <0.900
06/01/11 <0.13 <0.13 <0.15 <0.30 108 <0.10 0.20 J <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 247 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 98.0 0.17 J <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 0.70 <0.10 <0.10 <0.22 464 <0.15 0.23 J <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 72.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 0.72 <0.10 <0.10 <0.20 567 <0.10 0.26 J <0.10 <0.10 <0.10 <0.10
12/09/14 0.55 <0.10 <0.10 <0.20 248 <0.10 0.15 J <0.10 <0.10 <0.10 <0.10
06/03/15 0.52 <0.17 <0.15 <0.43 204 <0.12 0.19 J <0.12 <0.16 <0.14 <0.14
12/15/15 0.42 J <0.17 <0.15 <0.43 134 E 0.22 J <0.16 <0.12 <0.16 <0.14 <0.14
02/20/17 <0.13 <0.13 <0.13 <0.25 40.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <0.13 <0.13 <0.13 <0.25 24.9 <0.13 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/07/19 0.17 J 0.23 J <0.13 <0.25 34.4 <0.13 NR NR NR NR NR
MW-37
MW-36
Page 9 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene05/02/03 <1 <0.5 <0.5 <2 4.6 NR NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 3.1 <2.0 NR NR NR NR NR
06/01/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 <0.500 <0.500 <0.500 <0.500 2.36 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 6.95 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 <0.25 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/27/09 <0.200 <0.330 <0.670 <1.33 0.385 J <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 0.440 J <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 1.49 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 0.342 J <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 1.2 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 0.48 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.35 J <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 0.89 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 0.51 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 0.52 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
09/05/03 2.80 <1.0 <1.0 <4.0 3 <1.0 NR NR NR NR NR
05/13/04 8.80 <1.0 <1.0 <2.0 7.2 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 0.940 <0.500 <0.500 <0.500 5.71 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 0.510I <1.0 <1.0 <3.0 3.76 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 <0.25 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/28/09 <0.200 <0.330 <0.670 <1.33 5.18 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 0.946 J <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 1.08 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 4.14 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 6.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 1.8 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 1.9 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
09/05/03 <1.0 <1.0 <1.0 <4.0 <2.0 <1.0 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 27.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/19/07 <0.500 <0.500 <0.500 <0.500 1.83 <0.500 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
06/16/10 NS NS NS NS NS NS NS NS NS NS NS
12/09/10 NS NS NS NS NS NS NS NS NS NS NS
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
MW-38
MW-39
MW-40
Page 10 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene09/05/03 <10 <10 <10 <40 760 <10 NR NR NR NR NR
05/13/04 1.60 <1.0 <1.0 <2.0 1,500 <2.0 NR NR NR NR NR
05/31/06 <50 <50 <50 <150 850 <100 NR NR NR NR NR
06/19/07 <0.500 <0.500 <0.500 <0.500 223 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 30.6 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 67.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 68.0 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/28/09 0.390 J <0.330 <0.670 <1.33 304 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 24.9 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <1.40 <1.90 <1.50 <2.20 573 <5.00 <2.20 <1.50 <2.20 <1.50 <1.80
12/09/10 0.278 J <0.190 <0.150 <0.220 181 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 53.4 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 26.6 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 0.53 <0.13 <0.15 <0.30 78.0 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 10.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 5.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 3.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 4.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/09/14 <0.10 <0.10 <0.10 <0.20 1.5 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 3.5 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
06/06/12 FP FP FP FP FP FP FP FP FP FP FP
12/05/12 FP FP FP FP FP FP FP FP FP FP FP
06/04/13 77.1 5,210 1,680 9,230 <5.0 347 <5.0 79.0 267 1,700 471
12/02/13 FP FP FP FP FP FP FP FP FP FP FP
06/18/14 FP FP FP FP FP FP FP FP FP FP FP
12/09/14 FP FP FP FP FP FP FP FP FP FP FP
06/04/15 0.23 J 1.3 1.1 3.5 <0.16 <0.12 <0.16 <0.12 <0.16 1.7 0.45 J
12/15/15 <0.17 <0.17 0.52 1.4 J <0.16 0.59 <0.16 <0.12 0.22 J 1 0.30 J
06/08/16 NS NS NS NS NS NS NS NS NS NS NS
12/15/15 1,090 4,460 1,170 5,670 73.6 263 <16 88.9 304 1,790 480
06/08/16 2,110 5,880 798 3,970 <13 180 <13 47.2 J 151 938 262
02/20/17 8,020 15,500 1,560 6,950 198 J 290 <63 <63 111 J 779 205 J
05/16/18 8,940 20,500 1,990 8,340 396 812 NR NR NR NR NR
11/13/18 3,480 7,690 945 4,570 74.1 J 146 NR NR NR NR NR
11/07/19 5,540 13,800 1,440 6,880 92.0 J 354 NR NR NR NR NR
11/04/20 2,880 7,610 964 4,690 <25 136 NR NR NR NR NR
01/04/22 1,710 3,640 659 3,160 <13 152 NR NR NR NR NR
02/14/23 1,640 2,740 597 2,730 <14.0 <47.0 <15.0 33.5 J 85.4 524 156
12/15/15 1,180 129 1,000 2,430 611 380 <4.1 87.5 173 1,080 310
06/08/16 603 44.3 330 939 290 138 <1.3 35.7 52.4 452 113
02/20/17 269 16.7 54.3 282 80.1 34.3 <1.3 5.3 6.1 109 21.2
05/16/18 232 6.5 24.1 98.6 71.0 30.1 NR NR NR NR NR
11/13/18 584 42.5 392 1,030 169 142 NR NR NR NR NR
11/07/19 480 16.1 189 678 107 68.4 NR NR NR NR NR
11/04/20 252 8.2 132 471 71.1 83.2 NR NR NR NR NR
01/04/22 600 25.7 J 370 1,180 121 156 NR NR NR NR NR
02/14/23 219 7.61 62.8 167 J 30 46 <1.50 8.7 8.47 71.8 28.1
08/28/02 2.00 <1.0 <1.0 <4.0 14 <1 NR NR NR NR NR
05/13/04 14.0 <1.0 <1.0 <2.0 59.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 5.9 <2.0 NR NR NR NR NR
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
08/28/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
MW-41
MW-42
DMW-2
MW-43
DMW-1
MW-44
Page 11 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene11/19/02 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.20 J <0.10 <0.10 <0.10 <0.10 <0.10
06/19/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.32 J <0.10 <0.10 <0.10 0.32 J 0.19 J
06/04/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/08/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
02/20/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/16/18 <63 <63 <63 <130 <63 <63 NR NR NR NR NR
11/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/07/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
11/04/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR
01/04/22 <25 <25 40.5 J 282 J <25 564 NR NR NR NR NR
02/14/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.150 <0.180 <0.190 <0.190 <0.180
03/21/03 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/12/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/21/07 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 <0.25 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/28/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
DMW-4
DMW-3
Page 12 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene07/15/03 <1 <1 <1 <4 <2 <1 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 1.5 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 2.8 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 4.8 <2.0 NR NR NR NR NR
06/19/07 <0.500 <0.500 <0.500 <0.500 7.02 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 9.49 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 8.63 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 9.9 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/28/09 <0.200 <0.330 <0.670 <1.33 10.1 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 10.2 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 11.5 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 15.3 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 18.4 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 23.0 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 20.8 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 23.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 47.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 32.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 55.5 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 47.2 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
09/05/03 <1.0 <1.0 <1.0 <4.0 <2.0 <1.0 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
05/31/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
06/19/07 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR
12/06/07 NS NS NS NS NS NS NS NS NS NS NS
12/05/12 <0.10 <0.10 <0.10 <0.22 0.62 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 1.8 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 0.76 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 3.7 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
09/05/03 <1.0 <1.0 <1.0 <4.0 <2.0 <1.0 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NR NR NR NR NR
06/01/06 <1.0 <1.0 <1.0 <3.0 <1.0 <2.0 NR NR NR NR NR
09/05/03 <1.0 <1.0 <1.0 <4.0 8.6 <1.0 NR NR NR NR NR
05/13/04 <1.0 <1.0 <1.0 <2.0 9.9 <2.0 NR NR NR NR NR
06/01/06 <1.0 <1.0 <1.0 <3.0 15 <2.0 NR NR NR NR NR
09/06/06 <1.0 <1.0 <1.0 <3.0 14 <2.0 NR NR NR NR NR
06/21/07 <0.500 <0.500 <0.500 <0.500 19.6 <0.500 NR NR NR NR NR
12/06/07 <0.500 <0.500 <0.500 <1.00 0.86 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 19.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 18 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/27/09 <0.200 <0.330 <0.670 <1.33 21.7 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 17.5 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 17.3 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 18.4 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 17.6 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 15.2 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/07/12 <0.13 <0.13 <0.15 <0.30 15.0 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 7.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 7.7 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 16.5 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 0.18 J <0.10 <0.10 <0.20 12.5 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 14.8 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
DMW-7
DMW-5
DMW-8
DMW-6
Page 13 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene09/05/03 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
05/13/04 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
05/31/06 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
09/06/06 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
06/21/07 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
12/06/07 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.1 <1.2 <1.3 <1.4 <1.6 <1.12 <1.10 <1.13 <1.15 <1.14
11/06/08 <0.14 <0.15 <0.16 <0.17 <0.18 <0.20 <0.26 <0.24 <0.27 <0.29 <0.28
05/28/09 <0.200 <0.330 <0.670 <1.33 10.9 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 9.57 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 10.5 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 11.8 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 11.6 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 8.2 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/06/12 <0.13 <0.13 <0.15 <0.30 8.5 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 NS NS NS NS NS NS NS NS NS NS NS
06/04/13 <0.10 <0.10 <0.10 <0.22 7.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 4.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 7.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 7.6 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 7.2 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 NS NS NS NS NS NS NS NS NS NS NS
12/06/07 <0.500 <0.500 <0.500 <1.00 3.04 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 2.35 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 1.7 <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/27/09 <0.200 <0.330 <0.670 <1.33 1.72 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 1.44 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 1.22 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 1.51 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 1.5 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 0.47 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
02/21/12 <0.13 <0.13 <0.15 <0.30 1.6 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/07/12 <0.13 <0.13 <0.15 <0.30 1.4 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 1.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 2.8 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 1.5 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 0.32 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 3.1 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 <0.17 <0.17 <0.15 <0.43 2.1 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
05/20/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
11/06/08 <0.14 <0.19 <0.15 <0.12 0.50 J <0.070 <0.11 <0.12 <0.22 <0.14 <0.13
05/27/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <0.330 <0.330
12/03/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/16/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/09/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/01/11 <0.13 <0.13 <0.15 <0.30 0.35 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/08/11 <0.13 <0.13 <0.15 <0.30 0.46 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
02/21/12 <0.13 <0.13 <0.15 <0.30 0.38 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
06/07/12 <0.13 <0.13 <0.15 <0.30 0.47 J <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
12/05/12 <0.10 <0.10 <0.10 <0.22 0.70 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/04/13 <0.10 <0.10 <0.10 <0.22 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
12/02/13 <0.10 <0.10 <0.10 <0.22 0.54 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
06/18/14 <0.10 <0.10 <0.10 <0.20 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
12/08/14 <0.10 <0.10 <0.10 <0.20 0.49 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
06/03/15 <0.17 <0.17 <0.15 <0.43 0.76 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
12/15/15 <0.17 <0.17 <0.15 <0.43 1.1 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
02/24/23 <0.180 <0.220 <0.170 <0.210 0.706 J <0.470 <0.150 <0.180 <0.190 <0.190 <0.180
01/04/22 790 694 2,040 7,370 <6.3 682 NR NR NR NR NR
02/14/23 FP FP FP FP FP FP FP FP FP FP FP
DMW-9
WSW-7 (Pre)
EPCO MW-101
WSW-7 (Post)
Page 14 of 15
Date: 2/24/23 Facility ID#: 00-0-0000008172
Contaminant
of Concern
→
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 400 30,500 26,100 28,500 24,100BenzeneMAC (µg/l)
GCL (µg/l)
TABLE 6
SUMMARY OF LABORATORY ANALYTICAL RESULTS - GROUND WATER SAMPLES
FORMER ROSEBORO BP (INCIDENT NO. 6601)n-PropylbenzeneAnalytical Method →1,3,5-TrimethylbenzeneXylenesTolueneSample ID MTBENaphthaleneEPA Method 6200B / EPA 602
Isopropylbenzene1,2-Dichloroethane1,2,4-TrimethylbenzeneEthylbenzene01/04/22 3,550 84,600 91,200 830,000 <130 230,000 NR NR NR NR NR
02/14/23 FP FP FP FP FP FP FP FP FP FP FP
Notes:
• < : Less than the reporting limit specified in the laboratory report.
• Results reported in µg/l (micrograms per liter).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• FP : Free product; NR: Not requested; NS: Not sampled.
• J: Estimated value; E: Value exceeds calibration range
• The following petroleum constituent was reported to exceed the MAC: TAA in MW-44 on 02/14/23
• Refer to the laboratory analytical report for concentrations of compounds detected at levels below the MAC.
• Concentrations in italics exceed the GCL.
• Concentrations in bold face type exceed the MAC.
• GCL : Gross contamination level.
EPCO MW-102
Page 15 of 15
Date: 2/27/23 Facility ID#: 00-0-0000008172
Monitoring
Wells
Date
Collected
(mm/dd/yy)
DO (mg/L) pH Temp(oC) Conductivity
Oxidation-
Reduction
Potential
(mV)
MW-20 02/14/23 1.64 5.87 17.63 60 111.9
MW-22 02/14/23 1.41 5.09 15.77 61 182.7
MW-35 02/14/23 3.06 7.25 19.32 311 161.9
MW-43 02/14/23 1.83 6.11 18.99 225 -11.7
MW-44 02/14/23 1.61 6.14 19.10 213 30.0
DMW-3 02/14/23 2.46 7.77 18.81 97 166.5

TABLE 7
SUMMARY OF MNA PARAMETER READINGS
FORMER ROSEBORO BP (INCIDENT NO. 6601)
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

North Carolina Department of Environmental Quality | Division of Waste Management
Wilmington Regional Office | 127 Cardinal Drive Extension | Wilmington, NC 28405 |
[phone]

April 8, 2022

Mr. Greg Owen
Wellman Oil Company, Inc.
716 Warsaw Road
Clinton, NC 28328

Re: Review of Groundwater Monitoring Report (March 2022)
Former Roseboro BP Station
270 E. Dr. Martin Luther King Jr. Blvd.
Roseboro, Sampson County
Incident Numbers: 6601
Risk Classification: Intermediate
Ranking: H 151 D

Dear Mr. Owen:

The Underground Storage Tank Section of the Division of Waste Management has reviewed the
Groundwater Monitoring Report dated March 31, 2022. The report will be maintained in the Fayetteville
Regional Office.

We generally concur with the recommendations provided in the reviewed report. The following are
provided for your consideration;

• The most recent Risk Ranking Assessment for incident #6601 was performed in April 2018. At
that time, the risk assigned for incident #6601 was high. Pursuant to Title 15A NCAC 2L
.0407(a) you have a continuing obligation to notify the Department of Environmental Quality of
any changes that might affect the risk or land use classifications that have been assigned.

• The data selected for the contaminant mass calculations and graph do not utilize data for all dates
available for MW-2R, MW-43, and MW-44 between December 2015 and January 2022, and do
not present compound specific contaminant mass calculations reflecting 2L exceedances. In
addition, a historical contaminant concentration vs. time vs. groundwater graph was not provided.
The contaminant mass calculations should be amended and both graphs included in future reports.

• A file review of available reporting for this site and the adjacent downgradient facility, incident
#29932, has been performed. Work conducted by Clark Environmental Services between 1991
and 1994 included downgradient wells MW-13, MW-14, and MW-15, as well as a former
vacuum sparge system, active between 1993 and 1996. These features were located along the
western property boundary of the present day EPCO 3-Way Food Mart prior to the initial
development of the property in approximately 1999. The file indicates plume migration to the
EPCO 3-Way Food Mart from an upgradient source and is available for review.

2059 Received APR 11 2022

North Carolina Department of Environmental Quality | Division of Waste Management
Wilmington Regional Office | 127 Cardinal Drive Extension | Wilmington, NC 28405 |
[phone]

• The recommended annual groundwater sampling should include MW-2R, MW-20, MW-22,
MW-35, MW-43, MW-44, EPCO-101, EPCO-102, DMW-3, and WSW-7. Depth to
product/water measurements should be collected from MW-2R, MW-20, MW-22, MW-35, MW-
43, MW-44, EPCO-101, and EPCO-102 at the time of sampling.

The next annual groundwater monitoring event should be scheduled for January 2023.

If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking
Petroleum Underground Storage Tank Cleanup Funds, please contact the UST Section Trust Fund Branch
at [phone].

If you have any questions regarding the above please contact me at [e-mail], (910) 796-
7402 or the address listed below.

Sincerely,

Rhonda Olson
Hydrogeologist
Wilmington Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Rae Brown, Geological Resources, Inc. (electronic copy only)
Site Name City / County /Sampson Incident #6601
Resp Pty Name / Contact Incident Mgr Region FAY
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #44
Consultant / Project Mgr /Rae Troiano BrownTelephone / Fax Number /Task Authorization Number:45 ChangeOrd:No
Project Mgr Email Site Risk / Rank / Abatement:H151D RRA Date:4/16/2018
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached? [ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO IM AuthProposed
Rate/Price
(Consultant)RO Supv. AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 9 /wells Y $110.00 y $990.00 $990.00 /
4.090 #240 10 / samples Y $94.00 y $940.00 $940.00 /
4.091 1 /shipment Y $60.00 y $60.00 $60.00 /
6.090 1 / report Y $1,125.00 y $1,125.00 $1,125.00 /
12.050 1 / trip Y $250.00 y $250.00 $250.00 /
12.055 1 / trip Y $50.00 y $50.00 $50.00 /
4.041 1 / well Y $75.00 y $75.00 $75.00 /
4.090 #271 1 / sample Y $66.00 y $66.00 $66.00 /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
/ /
Requested Preapproved Claimed 3
TOTAL:$3,556.00 $3,556.00 TOTAL:
Total Standard Costs (Not Third Party)$3,556.00 $3,556.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:1/11/23 by:(PM)(Reserved for RO)
RO Review: 1/12/23 by: (IM) Joint UST Preapproval Confirmed By:Date1
RO Supv. Review: 1/12/23 by: (STF) RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submittedin the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
RTB
Proposed
Units / Type
(Consultant)
Nathan Beauchamp
ActiveYES
22-884 January 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Wellman Oil Company, Inc
Geological Resources, Inc.
DIRECTED - CAB ONLY
Roseboro
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010 (Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Roseboro BP
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposedactivities.If, following completion of this ePATA,you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of thecompletion date ofthe FIRST completed taskto remain within the Statuteof Limitations. All ePATAs submitted within a claim are closed with thatclaim, and may not be re-used in a separate submittal, even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
NJB
MHH
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality - Division of Waste Management
Type text here 1/12/2023
1/12/23
North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville, NC 28301 | [phone]
January 20, 2022
Mr. Greg Owen
Wellman Oil Company, Inc.
716 Warsaw Road
Clinton, NC 28328
Re: Review of Groundwater Monitoring Report (March
2022) Former Roseboro BP Station
270 E. Dr. Martin Luther King Jr. Blvd.
Roseboro, Sampson County
Incident Number: 6601
Risk Classification: Intermediate
Ranking: H 151 D
Dear Mr. Owen:
The UST Section, Division of Waste Management, is in receipt of the Groundwater Monitoring Report dated March 31, 2022. The report has been reviewed and will be maintained in the Fayetteville Regional Office.
The UST Section generally concurs with the recommendations provided in the report. However, in order to evaluate future cleanup options, please include the following in the next Groundwater Monitoring Report and other pertinent items provided in the Comprehensive Appendices for Corrective Action Guidelines (Appendix A and B):
•Pictures and measurements of MW-43 showing the location and proximity to objects that
may obstruct excavation.
•Figure(s) that includes potential extent of excavation around MW-43 hot spot.
•Updated geologic cross-sections that include all soil data and contaminants of concern
isoconcentration contours.
•Figure that includes historical extent of free product.
•A graph that depicts historical contaminant concentration vs. time vs. groundwater.
•Gauge additional offsite wells needed to provide more detailed groundwater
potentiometric maps.
We are aware of your concerns regarding incident #29932. That incident is also under further review.

North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville, NC 28301 | [phone]

If you have questions regarding the information contained in this letter, please contact me at the address or
telephone number listed below.

Sincerely,

Nathan Beauchamp
Hydrogeologist
Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Rae Troiano Brown / GRI (electronic copy only)

Fayetteville Regional Office | 225 Green St | #714 Systel Building | Fayetteville, NC 28301 | [phone]

APPENDIX B
Historical Cross Sections

APPENDIX C
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/21/2023
Geological Resources, Inc. Rae Brown
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-046-0007 Client Project Description: Roseboro BP
GRI #2059
Dear Rae Brown:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/15/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 65
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-046-0007
Page 2 of 65
Report Number:
Sample Summary Table
Client Project Description:
23-046-0007
Roseboro BP
GRI #2059
Lab No Client Sample ID Matrix Date Collected Date Received
02/14/2023 09:35Aqueous 99789 Trip Blank 02/15/2023 11:00
02/14/2023 10:37Aqueous 99790 DMW-3 02/15/2023 11:00
02/14/2023 10:51Aqueous 99791 MW-35 02/15/2023 11:00
02/14/2023 11:06Aqueous 99792 MW-43 02/15/2023 11:00
02/14/2023 11:24Aqueous 99793 MW-44 02/15/2023 11:00
02/14/2023 11:42Aqueous 99794 MW-20 02/15/2023 11:00
02/14/2023 12:03Aqueous 99795 MW-22 02/15/2023 11:00
02/14/2023 12:27Aqueous 99796 WSW-7 02/15/2023 11:00
Page 3 of 65
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-046-0007
Report Limit
Project:Roseboro BP
V 99792MW-43
1640 02/16/2023 21:366200BBenzeneµg/L 18.0
597 02/16/2023 21:366200BEthylbenzeneµg/L 17.0
J33.5 02/16/2023 21:366200BIsopropylbenzeneµg/L 18.0
85.4 02/16/2023 21:366200Bn-Propylbenzene µg/L 19.0
2740 02/16/2023 21:366200BTolueneµg/L 22.0
524 02/16/2023 21:366200B1,2,4-Trimethylbenzene µg/L 19.0
156 02/16/2023 21:366200B1,3,5-Trimethylbenzene µg/L 18.0
687 02/16/2023 21:366200Bo-Xylene µg/L 21.0
2040 02/16/2023 21:366200Bm,p-Xylene µg/L 42.0
2730 02/16/2023 21:366200BXylene (Total)µg/L 21.0
V 99793MW-44
219 02/17/2023 20:306200BBenzeneµg/L 1.80
62.8 02/17/2023 20:306200BEthylbenzeneµg/L 1.70
8.70 02/17/2023 20:306200BIsopropylbenzeneµg/L 1.80
30.0 02/17/2023 20:306200BMethyl tert-butyl ether (MTBE)µg/L 1.40
46.0 02/17/2023 20:306200BNaphthaleneµg/L 4.70
8.47 02/17/2023 20:306200Bn-Propylbenzene µg/L 1.90
160 02/17/2023 20:306200Btert-Amyl Alcohol (TAA)µg/L 19.0
7.61 02/17/2023 20:306200BTolueneµg/L 2.20
71.8 02/17/2023 20:306200B1,2,4-Trimethylbenzene µg/L 1.90
28.1 02/17/2023 20:306200B1,3,5-Trimethylbenzene µg/L 1.80
J2.82 02/17/2023 20:306200Bo-Xylene µg/L 2.10
164 02/17/2023 20:306200Bm,p-Xylene µg/L 4.20
J16702/17/2023 20:306200BXylene (Total)µg/L 2.10
V 99794MW-20
0.868 02/16/2023 14:476200BBenzeneµg/L 0.180
1.37 02/16/2023 14:476200BEthylbenzeneµg/L 0.170
J0.364 02/16/2023 14:476200Bn-Propylbenzene µg/L 0.190
4.70 02/16/2023 14:476200BTolueneµg/L 0.220
2.29 02/16/2023 14:476200B1,2,4-Trimethylbenzene µg/L 0.190
0.752 02/16/2023 14:476200B1,3,5-Trimethylbenzene µg/L 0.180
1.90 02/16/2023 14:476200Bo-Xylene µg/L 0.210
5.24 02/16/2023 14:476200Bm,p-Xylene µg/L 0.420
7.14 02/16/2023 14:476200BXylene (Total)µg/L 0.210
Page 4 of 65
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-046-0007
Report Limit
Project:Roseboro BP
V 99795MW-22
J0.330 02/16/2023 15:116200BBenzeneµg/L 0.180
0.590 02/16/2023 15:116200BEthylbenzeneµg/L 0.170
1.72 02/16/2023 15:116200BTolueneµg/L 0.220
0.960 02/16/2023 15:116200B1,2,4-Trimethylbenzene µg/L 0.190
J0.284 02/16/2023 15:116200B1,3,5-Trimethylbenzene µg/L 0.180
0.727 02/16/2023 15:116200Bo-Xylene µg/L 0.210
2.12 02/16/2023 15:116200Bm,p-Xylene µg/L 0.420
2.85 02/16/2023 15:116200BXylene (Total)µg/L 0.210
V 99796WSW-7
J0.706 02/16/2023 15:356200BMethyl tert-butyl ether (MTBE)µg/L 0.140
Page 5 of 65

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Roseboro BP Lab Report Number: 23-046-0007
Date: 2/21/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Carbon Tetrachloride QC Batch No: V29854/V29853
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: tert-Amyl alcohol QC Batch No: V29854/V29853
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Vinyl acetate QC Batch No: V29854/V29853
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Vinyl acetate QC Batch No: V29910/V29853
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.

Page 6 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99789 Matrix:
2/14/2023 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/16/23 13:54 V29854MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 13:54 V29854MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 13:54 V29854MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 13:54 V29854MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 13:54 V29854MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 13:54 V29854MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 13:54 V29854MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 13:54 V29854MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 13:54 V29854MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 13:54 V29854MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 13:54 V29854MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 13:54 V29854MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 13:54 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99789 Matrix:
2/14/2023 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 13:54 V29854MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 13:54 V29854MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 13:54 V29854MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 13:54 V29854MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 13:54 V29854MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 13:54 V29854MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 13:54 V29854MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 13:54 V29854MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 13:54 V29854MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 13:54 V29854MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 13:54 V29854MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 13:54 V29854MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 13:54 V29854MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 13:54 V29854MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 13:54 V29854MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 13:54 V29854MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 13:54 V29854MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 13:54 V29854MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 13:54 V29854MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 13:54 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99789 Matrix:
2/14/2023 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 13:54 V29854MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 13:54 V29854MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 13:54 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 13:54 V29854MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 13:54 V29854MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/16/23 13:54 V29854MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 13:54 V29854MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 13:54 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 13:54 V29854MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 13:54 V29854MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 13:54 V29854MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 13:54 V29854MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 13:54 V29854MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 13:54 V29854MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 13:54 V29854MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 02/16/23 13:54 V29854MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 13:54 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99789 Matrix:
2/14/2023 9:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/16/23 13:54 V29854
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/16/23 13:541 MSA V29854
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%02/16/23 13:541 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%02/16/23 13:541 MSA V29854
Surrogate: Toluene-d8 98.0 Limits: 70-130%02/16/23 13:541 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:DMW-3
99790 Matrix:
2/14/2023 10:37
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/16/23 16:10 6200BMSA
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: Toluene-d8 98.8 Limits: 70-130%02/16/23 16:101 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:DMW-3
99790 Matrix:
2/14/2023 10:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/16/23 16:10 V29854MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 16:10 V29854MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 16:10 V29854MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 16:10 V29854MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 16:10 V29854MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 16:10 V29854MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 16:10 V29854MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 16:10 V29854MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 16:10 V29854MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 16:10 V29854MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 16:10 V29854MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 16:10 V29854MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 16:10 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:DMW-3
99790 Matrix:
2/14/2023 10:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 16:10 V29854MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 16:10 V29854MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 16:10 V29854MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 16:10 V29854MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 16:10 V29854MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 16:10 V29854MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 16:10 V29854MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 16:10 V29854MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 16:10 V29854MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 16:10 V29854MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 16:10 V29854MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 16:10 V29854MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 16:10 V29854MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 16:10 V29854MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 16:10 V29854MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 16:10 V29854MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 16:10 V29854MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 16:10 V29854MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 16:10 V29854MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 16:10 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:DMW-3
99790 Matrix:
2/14/2023 10:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 16:10 V29854MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 16:10 V29854MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 16:10 V29854MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/16/23 16:10 V29854MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/16/23 16:10 V29854MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/16/23 16:10 V29854MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/16/23 16:10 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 16:10 V29854MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 16:10 V29854MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/16/23 16:10 V29854MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 16:10 V29854MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 16:10 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 16:10 V29854MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 16:10 V29854MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 16:10 V29854MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 16:10 V29854MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 16:10 V29854MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 16:10 V29854MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 16:10 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:DMW-3
99790 Matrix:
2/14/2023 10:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 02/16/23 16:10 V29854MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 16:10 V29854MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/16/23 16:10 V29854
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%02/16/23 16:101 MSA V29854
Surrogate: Toluene-d8 98.8 Limits: 70-130%02/16/23 16:101 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-35
99791 Matrix:
2/14/2023 10:51
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/16/23 16:37 6200BMSA
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: Dibromofluoromethane 100 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: Toluene-d8 98.6 Limits: 70-130%02/16/23 16:371 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-35
99791 Matrix:
2/14/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/16/23 16:37 V29854MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 16:37 V29854MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 16:37 V29854MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 16:37 V29854MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 16:37 V29854MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 16:37 V29854MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 16:37 V29854MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 16:37 V29854MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 16:37 V29854MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 16:37 V29854MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 16:37 V29854MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 16:37 V29854MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 16:37 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-35
99791 Matrix:
2/14/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 16:37 V29854MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 16:37 V29854MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 16:37 V29854MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 16:37 V29854MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 16:37 V29854MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 16:37 V29854MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 16:37 V29854MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 16:37 V29854MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 16:37 V29854MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 16:37 V29854MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 16:37 V29854MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 16:37 V29854MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 16:37 V29854MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 16:37 V29854MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 16:37 V29854MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 16:37 V29854MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 16:37 V29854MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 16:37 V29854MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 16:37 V29854MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 16:37 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-35
99791 Matrix:
2/14/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 16:37 V29854MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 16:37 V29854MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 16:37 V29854MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/16/23 16:37 V29854MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/16/23 16:37 V29854MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/16/23 16:37 V29854MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/16/23 16:37 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 16:37 V29854MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 16:37 V29854MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/16/23 16:37 V29854MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 16:37 V29854MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 16:37 V29854MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 16:37 V29854MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 16:37 V29854MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 16:37 V29854MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 16:37 V29854MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 16:37 V29854MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 16:37 V29854MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 16:37 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-35
99791 Matrix:
2/14/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 02/16/23 16:37 V29854MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 16:37 V29854MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/16/23 16:37 V29854
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: Dibromofluoromethane 100 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%02/16/23 16:371 MSA V29854
Surrogate: Toluene-d8 98.6 Limits: 70-130%02/16/23 16:371 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-43
99792 Matrix:
2/14/2023 11:06
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 02/16/23 21:36 6200BMSA
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: Toluene-d8 100 Limits: 70-130%02/16/23 21:36100 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-43
99792 Matrix:
2/14/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<180 µg/L 180 1000Acetone 100 02/16/23 21:36 V29854MSA
1640 µg/L 18.0 50.0Benzene 100 02/16/23 21:36 V29854MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 02/16/23 21:36 V29854MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 02/16/23 21:36 V29854MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 02/16/23 21:36 V29854MSA
<150 µg/L 150 500Bromoform 100 02/16/23 21:36 V29854MSA
<28.0 µg/L 28.0 100Bromomethane 100 02/16/23 21:36 V29854MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 02/16/23 21:36 V29854MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 02/16/23 21:36 V29854MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 02/16/23 21:36 V29854MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 02/16/23 21:36 V29854MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 02/16/23 21:36 V29854MSA
<43.0 µg/L 43.0 100Chloroethane 100 02/16/23 21:36 V29854MSA
<22.0 µg/L 22.0 50.0Chloroform 100 02/16/23 21:36 V29854MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 02/16/23 21:36 V29854MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 02/16/23 21:36 V29854MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 02/16/23 21:36 V29854MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 02/16/23 21:36 V29854MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 02/16/23 21:36 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-43
99792 Matrix:
2/14/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 02/16/23 21:36 V29854MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 02/16/23 21:36 V29854MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 02/16/23 21:36 V29854MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 02/16/23 21:36 V29854MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 02/16/23 21:36 V29854MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 02/16/23 21:36 V29854MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 02/16/23 21:36 V29854MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 02/16/23 21:36 V29854MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 02/16/23 21:36 V29854MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 02/16/23 21:36 V29854MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 02/16/23 21:36 V29854MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 02/16/23 21:36 V29854MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 02/16/23 21:36 V29854MSA
<4200 µg/L 4200 20000Ethanol 100 02/16/23 21:36 V29854MSA
597 µg/L 17.0 50.0Ethylbenzene 100 02/16/23 21:36 V29854MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 02/16/23 21:36 V29854MSA
<38.0 µg/L 38.0 1002-Hexanone 100 02/16/23 21:36 V29854MSA
33.5 J µg/L 18.0 50.0Isopropylbenzene 100 02/16/23 21:36 V29854MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 02/16/23 21:36 V29854MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 02/16/23 21:36 V29854MSA
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 02/16/23 21:36 V29854MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 02/16/23 21:36 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-43
99792 Matrix:
2/14/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
<33.0 µg/L 33.0 200Methylene Chloride 100 02/16/23 21:36 V29854MSA
<47.0 µg/L 47.0 100Naphthalene 100 02/16/23 21:36 V29854MSA
85.4 µg/L 19.0 50.0n-Propylbenzene 100 02/16/23 21:36 V29854MSA
<22.0 µg/L 22.0 50.0Styrene 100 02/16/23 21:36 V29854MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 02/16/23 21:36 V29854MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 02/16/23 21:36 V29854MSA
<190 µg/L 190 1000tert-Amyl Alcohol (TAA)100 02/16/23 21:36 V29854MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 02/16/23 21:36 V29854MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 02/16/23 21:36 V29854MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 02/16/23 21:36 V29854MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 02/16/23 21:36 V29854MSA
2740 µg/L 22.0 50.0Toluene 100 02/16/23 21:36 V29854MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 02/16/23 21:36 V29854MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 02/16/23 21:36 V29854MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 02/16/23 21:36 V29854MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 02/16/23 21:36 V29854MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 02/16/23 21:36 V29854MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 02/16/23 21:36 V29854MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 02/16/23 21:36 V29854MSA
524 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 02/16/23 21:36 V29854MSA
156 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 02/16/23 21:36 V29854MSA
<100 µg/L 100 500Vinyl Acetate 100 02/16/23 21:36 V29854MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 02/16/23 21:36 V29854MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-43
99792 Matrix:
2/14/2023 11:06
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29853 02/16/23 09:00
687 µg/L 21.0 50.0o-Xylene 100 02/16/23 21:36 V29854MSA
2040 µg/L 42.0 100m,p-Xylene 100 02/16/23 21:36 V29854MSA
2730 µg/L 21.0 50.0Xylene (Total)100 02/16/23 21:36 V29854
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%02/16/23 21:36100 MSA V29854
Surrogate: Toluene-d8 100 Limits: 70-130%02/16/23 21:36100 MSA V29854
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-44
99793 Matrix:
2/14/2023 11:24
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 02/17/23 20:30 6200BANG
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/17/23 20:3010 ANG V29910
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-44
99793 Matrix:
2/14/2023 11:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29909 02/17/23 09:00
<18.0 µg/L 18.0 100Acetone 10 02/17/23 20:30 V29910ANG
219 µg/L 1.80 5.00Benzene 10 02/17/23 20:30 V29910ANG
<2.10 µg/L 2.10 5.00Bromobenzene 10 02/17/23 20:30 V29910ANG
<4.20 µg/L 4.20 10.0Bromochloromethane 10 02/17/23 20:30 V29910ANG
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 02/17/23 20:30 V29910ANG
<15.0 µg/L 15.0 50.0Bromoform 10 02/17/23 20:30 V29910ANG
<2.80 µg/L 2.80 10.0Bromomethane 10 02/17/23 20:30 V29910ANG
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 02/17/23 20:30 V29910ANG
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 02/17/23 20:30 V29910ANG
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 02/17/23 20:30 V29910ANG
<1.90 µg/L 1.90 5.00Chlorobenzene 10 02/17/23 20:30 V29910ANG
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 02/17/23 20:30 V29910ANG
<4.30 µg/L 4.30 10.0Chloroethane 10 02/17/23 20:30 V29910ANG
<2.20 µg/L 2.20 5.00Chloroform 10 02/17/23 20:30 V29910ANG
<2.20 µg/L 2.20 5.00Chloromethane 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 02/17/23 20:30 V29910ANG
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 02/17/23 20:30 V29910ANG
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 02/17/23 20:30 V29910ANG
<2.30 µg/L 2.30 5.00Dibromomethane 10 02/17/23 20:30 V29910ANG
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 02/17/23 20:30 V29910ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-44
99793 Matrix:
2/14/2023 11:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29909 02/17/23 09:00
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 02/17/23 20:30 V29910ANG
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 02/17/23 20:30 V29910ANG
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 02/17/23 20:30 V29910ANG
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 02/17/23 20:30 V29910ANG
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 02/17/23 20:30 V29910ANG
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 02/17/23 20:30 V29910ANG
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 02/17/23 20:30 V29910ANG
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 02/17/23 20:30 V29910ANG
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 02/17/23 20:30 V29910ANG
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 02/17/23 20:30 V29910ANG
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 02/17/23 20:30 V29910ANG
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 02/17/23 20:30 V29910ANG
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 02/17/23 20:30 V29910ANG
<420 µg/L 420 2000Ethanol 10 02/17/23 20:30 V29910ANG
62.8 µg/L 1.70 5.00Ethylbenzene 10 02/17/23 20:30 V29910ANG
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 02/17/23 20:30 V29910ANG
<3.80 µg/L 3.80 10.02-Hexanone 10 02/17/23 20:30 V29910ANG
8.70 µg/L 1.80 5.00Isopropylbenzene 10 02/17/23 20:30 V29910ANG
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 02/17/23 20:30 V29910ANG
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 02/17/23 20:30 V29910ANG
30.0 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 02/17/23 20:30 V29910ANG
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 02/17/23 20:30 V29910ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-44
99793 Matrix:
2/14/2023 11:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29909 02/17/23 09:00
<3.30 µg/L 3.30 20.0Methylene Chloride 10 02/17/23 20:30 V29910ANG
46.0 µg/L 4.70 10.0Naphthalene 10 02/17/23 20:30 V29910ANG
8.47 µg/L 1.90 5.00n-Propylbenzene 10 02/17/23 20:30 V29910ANG
<2.20 µg/L 2.20 5.00Styrene 10 02/17/23 20:30 V29910ANG
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 02/17/23 20:30 V29910ANG
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 02/17/23 20:30 V29910ANG
160 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 02/17/23 20:30 V29910ANG
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 02/17/23 20:30 V29910ANG
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 02/17/23 20:30 V29910ANG
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 02/17/23 20:30 V29910ANG
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 02/17/23 20:30 V29910ANG
7.61 µg/L 2.20 5.00Toluene 10 02/17/23 20:30 V29910ANG
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 02/17/23 20:30 V29910ANG
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 02/17/23 20:30 V29910ANG
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 02/17/23 20:30 V29910ANG
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 02/17/23 20:30 V29910ANG
<1.80 µg/L 1.80 5.00Trichloroethene 10 02/17/23 20:30 V29910ANG
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 02/17/23 20:30 V29910ANG
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 02/17/23 20:30 V29910ANG
71.8 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 02/17/23 20:30 V29910ANG
28.1 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 02/17/23 20:30 V29910ANG
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 02/17/23 20:30 V29910ANG
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 02/17/23 20:30 V29910ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-44
99793 Matrix:
2/14/2023 11:24
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29909 02/17/23 09:00
2.82 J µg/L 2.10 5.00o-Xylene 10 02/17/23 20:30 V29910ANG
164 µg/L 4.20 10.0m,p-Xylene 10 02/17/23 20:30 V29910ANG
167 J µg/L 2.10 5.00Xylene (Total)10 02/17/23 20:30 V29910
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%02/17/23 20:3010 ANG V29910
Surrogate: Toluene-d8 99.4 Limits: 70-130%02/17/23 20:3010 ANG V29910
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-20
99794 Matrix:
2/14/2023 11:42
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/16/23 14:47 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: Dibromofluoromethane 89.6 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: Toluene-d8 101 Limits: 70-130%02/16/23 14:471 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-20
99794 Matrix:
2/14/2023 11:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 14:47 V29877MSA
0.868 µg/L 0.180 0.500Benzene 1 02/16/23 14:47 V29877MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 14:47 V29877MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 14:47 V29877MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 14:47 V29877MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 14:47 V29877MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 14:47 V29877MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 14:47 V29877MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 14:47 V29877MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 14:47 V29877MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 14:47 V29877MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 14:47 V29877MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 14:47 V29877MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 14:47 V29877MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 14:47 V29877MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 14:47 V29877MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 14:47 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-20
99794 Matrix:
2/14/2023 11:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 14:47 V29877MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 14:47 V29877MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 14:47 V29877MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 14:47 V29877MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 14:47 V29877MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 14:47 V29877MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 14:47 V29877MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 14:47 V29877MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 14:47 V29877MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 14:47 V29877MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 14:47 V29877MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 14:47 V29877MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 14:47 V29877MSA
1.37 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 14:47 V29877MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 14:47 V29877MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 14:47 V29877MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 14:47 V29877MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 14:47 V29877MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 14:47 V29877MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 14:47 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-20
99794 Matrix:
2/14/2023 11:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 14:47 V29877MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 14:47 V29877MSA
0.364 J µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 14:47 V29877MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 14:47 V29877MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/16/23 14:47 V29877MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/16/23 14:47 V29877MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/16/23 14:47 V29877MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/16/23 14:47 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 14:47 V29877MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 14:47 V29877MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 14:47 V29877MSA
4.70 µg/L 0.220 0.500Toluene 1 02/16/23 14:47 V29877MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 14:47 V29877MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 14:47 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 14:47 V29877MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 14:47 V29877MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 14:47 V29877MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 14:47 V29877MSA
2.29 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 14:47 V29877MSA
0.752 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 14:47 V29877MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 14:47 V29877MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 14:47 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-20
99794 Matrix:
2/14/2023 11:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
1.90 µg/L 0.210 0.500o-Xylene 1 02/16/23 14:47 V29877MSA
5.24 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 14:47 V29877MSA
7.14 µg/L 0.210 0.500Xylene (Total)1 02/16/23 14:47 V29877
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: Dibromofluoromethane 89.6 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%02/16/23 14:471 MSA V29877
Surrogate: Toluene-d8 101 Limits: 70-130%02/16/23 14:471 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-22
99795 Matrix:
2/14/2023 12:03
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/16/23 15:11 6200BMSA
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: Dibromofluoromethane 90.0 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 89.4 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: Toluene-d8 100 Limits: 70-130%02/16/23 15:111 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-22
99795 Matrix:
2/14/2023 12:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 15:11 V29877MSA
0.330 J µg/L 0.180 0.500Benzene 1 02/16/23 15:11 V29877MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 15:11 V29877MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 15:11 V29877MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 15:11 V29877MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 15:11 V29877MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 15:11 V29877MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 15:11 V29877MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 15:11 V29877MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 15:11 V29877MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 15:11 V29877MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 15:11 V29877MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 15:11 V29877MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 15:11 V29877MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 15:11 V29877MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 15:11 V29877MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 15:11 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-22
99795 Matrix:
2/14/2023 12:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 15:11 V29877MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 15:11 V29877MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 15:11 V29877MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 15:11 V29877MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 15:11 V29877MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 15:11 V29877MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 15:11 V29877MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 15:11 V29877MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 15:11 V29877MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 15:11 V29877MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 15:11 V29877MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 15:11 V29877MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 15:11 V29877MSA
0.590 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 15:11 V29877MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 15:11 V29877MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 15:11 V29877MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 15:11 V29877MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 15:11 V29877MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 15:11 V29877MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 15:11 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-22
99795 Matrix:
2/14/2023 12:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 15:11 V29877MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 15:11 V29877MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 15:11 V29877MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 15:11 V29877MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/16/23 15:11 V29877MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/16/23 15:11 V29877MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/16/23 15:11 V29877MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/16/23 15:11 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 15:11 V29877MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 15:11 V29877MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 15:11 V29877MSA
1.72 µg/L 0.220 0.500Toluene 1 02/16/23 15:11 V29877MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 15:11 V29877MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 15:11 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 15:11 V29877MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 15:11 V29877MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 15:11 V29877MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 15:11 V29877MSA
0.960 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 15:11 V29877MSA
0.284 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 15:11 V29877MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 15:11 V29877MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 15:11 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:MW-22
99795 Matrix:
2/14/2023 12:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
0.727 µg/L 0.210 0.500o-Xylene 1 02/16/23 15:11 V29877MSA
2.12 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 15:11 V29877MSA
2.85 µg/L 0.210 0.500Xylene (Total)1 02/16/23 15:11 V29877
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: Dibromofluoromethane 90.0 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 89.4 Limits: 70-130%02/16/23 15:111 MSA V29877
Surrogate: Toluene-d8 100 Limits: 70-130%02/16/23 15:111 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:WSW-7
99796 Matrix:
2/14/2023 12:27
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 02/16/23 15:35 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: Dibromofluoromethane 90.0 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: Toluene-d8 102 Limits: 70-130%02/16/23 15:351 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:WSW-7
99796 Matrix:
2/14/2023 12:27
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500Benzene 1 02/16/23 15:35 V29877MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 02/16/23 15:35 V29877MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 02/16/23 15:35 V29877MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 02/16/23 15:35 V29877MSA
<1.50 µg/L 1.50 5.00Bromoform 1 02/16/23 15:35 V29877MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 02/16/23 15:35 V29877MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 02/16/23 15:35 V29877MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 02/16/23 15:35 V29877MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 02/16/23 15:35 V29877MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.500Chloroform 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 02/16/23 15:35 V29877MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 02/16/23 15:35 V29877MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 02/16/23 15:35 V29877MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 02/16/23 15:35 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:WSW-7
99796 Matrix:
2/14/2023 12:27
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 02/16/23 15:35 V29877MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 02/16/23 15:35 V29877MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 02/16/23 15:35 V29877MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 02/16/23 15:35 V29877MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 02/16/23 15:35 V29877MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 02/16/23 15:35 V29877MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 02/16/23 15:35 V29877MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 02/16/23 15:35 V29877MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 02/16/23 15:35 V29877MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 02/16/23 15:35 V29877MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 02/16/23 15:35 V29877MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 02/16/23 15:35 V29877MSA
<42.0 µg/L 42.0 200Ethanol 1 02/16/23 15:35 V29877MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 02/16/23 15:35 V29877MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 02/16/23 15:35 V29877MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 02/16/23 15:35 V29877MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 02/16/23 15:35 V29877MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 02/16/23 15:35 V29877MSA
0.706 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 02/16/23 15:35 V29877MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 02/16/23 15:35 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:WSW-7
99796 Matrix:
2/14/2023 12:27
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 02/16/23 15:35 V29877MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 02/16/23 15:35 V29877MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.500Styrene 1 02/16/23 15:35 V29877MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 02/16/23 15:35 V29877MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 02/16/23 15:35 V29877MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 02/16/23 15:35 V29877MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 02/16/23 15:35 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 02/16/23 15:35 V29877MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 02/16/23 15:35 V29877MSA
<0.220 µg/L 0.220 0.500Toluene 1 02/16/23 15:35 V29877MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 02/16/23 15:35 V29877MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 02/16/23 15:35 V29877MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 02/16/23 15:35 V29877MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 02/16/23 15:35 V29877MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 02/16/23 15:35 V29877MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 02/16/23 15:35 V29877MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 02/16/23 15:35 V29877MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 02/16/23 15:35 V29877MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 02/16/23 15:35 V29877MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 65
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-046-0007
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
Rae Brown
Winterville
Danyale Love
Project Manager
GRI #2059 Received : 02/15/2023
Roseboro BP
Report Date : 02/21/2023
Sample ID :
Lab No :
Sampled:WSW-7
99796 Matrix:
2/14/2023 12:27
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29876 02/16/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 02/16/23 15:35 V29877MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 02/16/23 15:35 V29877MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 02/16/23 15:35 V29877
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: Dibromofluoromethane 90.0 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: 1,2-Dichloroethane - d4 90.2 Limits: 70-130%02/16/23 15:351 MSA V29877
Surrogate: Toluene-d8 102 Limits: 70-130%02/16/23 15:351 MSA V29877
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
Associated Lab Samples: 99789, 99790, 99791, 99792
LRB-V29853 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:2710.01.80<1.80µg/LAcetone
02/16/23 13:270.5000.180<0.180µg/LBenzene
02/16/23 13:270.5000.210<0.210µg/LBromobenzene
02/16/23 13:271.000.420<0.420µg/LBromochloromethane
02/16/23 13:270.5000.160<0.160µg/LBromodichloromethane
02/16/23 13:275.001.50<1.50µg/LBromoform
02/16/23 13:271.000.280<0.280µg/LBromomethane
02/16/23 13:270.5000.180<0.180µg/Ln-Butylbenzene
02/16/23 13:270.5000.200<0.200µg/Lsec-Butyl benzene
02/16/23 13:272.000.920<0.920µg/Ltert-Butyl benzene
02/16/23 13:270.5000.180<0.180µg/LCarbon Tetrachloride
02/16/23 13:270.5000.190<0.190µg/LChlorobenzene
02/16/23 13:270.5000.190<0.190µg/LChlorodibromomethane
02/16/23 13:271.000.430<0.430µg/LChloroethane
02/16/23 13:270.5000.220<0.220µg/LChloroform
02/16/23 13:270.5000.220<0.220µg/LChloromethane
02/16/23 13:270.5000.200<0.200µg/L2-Chlorotoluene
02/16/23 13:270.5000.200<0.200µg/L4-Chlorotoluene
02/16/23 13:270.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/16/23 13:272.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/16/23 13:270.5000.200<0.200µg/L1,2-Dibromoethane
02/16/23 13:270.5000.230<0.230µg/LDibromomethane
02/16/23 13:270.5000.220<0.220µg/L1,2-Dichlorobenzene
02/16/23 13:270.5000.190<0.190µg/L1,3-Dichlorobenzene
02/16/23 13:270.5000.210<0.210µg/L1,4-Dichlorobenzene
02/16/23 13:275.001.20<1.20µg/LDichlorodifluoromethane
02/16/23 13:270.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 18Date:02/21/2023 02:25 PM
Page 46 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
Associated Lab Samples: 99789, 99790, 99791, 99792
LRB-V29853 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:270.5000.150<0.150µg/L1,2-Dichloroethane
02/16/23 13:270.5000.150<0.150µg/L1,1-Dichloroethene
02/16/23 13:270.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/16/23 13:270.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/16/23 13:270.5000.190<0.190µg/L1,2-Dichloropropane
02/16/23 13:270.5000.130<0.130µg/L1,3-Dichloropropane
02/16/23 13:272.000.210<0.210µg/L2,2-Dichloropropane
02/16/23 13:270.5000.200<0.200µg/L1,1-Dichloropropene
02/16/23 13:270.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/16/23 13:270.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/16/23 13:2720042.0<42.0µg/LEthanol
02/16/23 13:270.5000.170<0.170µg/LEthylbenzene
02/16/23 13:273.000.350<0.350µg/LHexachlorobutadiene
02/16/23 13:271.000.380<0.380µg/L2-Hexanone
02/16/23 13:270.5000.180<0.180µg/LIsopropylbenzene
02/16/23 13:270.5000.089<0.089µg/L4-Isopropyl toluene
02/16/23 13:275.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/16/23 13:271.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/16/23 13:271.000.078<0.078µg/L4-Methyl-2-Pentanone
02/16/23 13:272.000.330<0.330µg/LMethylene Chloride
02/16/23 13:271.000.470<0.470µg/LNaphthalene
02/16/23 13:270.5000.190<0.190µg/Ln-Propylbenzene
02/16/23 13:270.5000.220<0.220µg/LStyrene
02/16/23 13:2710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/16/23 13:2710.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/16/23 13:2710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/16/23 13:2710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 18Date:02/21/2023 02:25 PM
Page 47 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
Associated Lab Samples: 99789, 99790, 99791, 99792
LRB-V29853 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:270.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/16/23 13:270.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/16/23 13:270.5000.220<0.220µg/LTetrachloroethene
02/16/23 13:270.5000.220<0.220µg/LToluene
02/16/23 13:270.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/16/23 13:270.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/16/23 13:270.5000.160<0.160µg/L1,1,1-Trichloroethane
02/16/23 13:270.5000.096<0.096µg/L1,1,2-Trichloroethane
02/16/23 13:270.5000.180<0.180µg/LTrichloroethene
02/16/23 13:270.5000.180<0.180µg/LTrichlorofluoromethane
02/16/23 13:270.5000.270<0.270µg/L1,2,3-Trichloropropane
02/16/23 13:270.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/16/23 13:270.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/16/23 13:275.001.00<1.00µg/LVinyl Acetate
02/16/23 13:270.5000.170<0.170µg/LVinyl Chloride
02/16/23 13:270.5000.210<0.210µg/Lo-Xylene
02/16/23 13:271.000.420<0.420µg/Lm,p-Xylene
02/16/23 13:2710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/16/23 13:274-Bromofluorobenzene (S)101 70-130
02/16/23 13:27Dibromofluoromethane (S)101 70-130
02/16/23 13:271,2-Dichloroethane - d4 (S)98.8 70-130
02/16/23 13:27Toluene-d8 (S)99.2 70-130
Page 3 of 18Date:02/21/2023 02:25 PM
Page 48 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
LCS-V29853 LCSD-V29853Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.1 97.795.038.040.0µg/LAcetone 40-160 2.8 20.0
18.8 94.096.019.220.0µg/LBenzene 70-130 2.1 20.0
18.3 91.591.518.320.0µg/LBromobenzene 70-130 0.0 20.0
18.9 94.594.018.820.0µg/LBromochloromethane 70-130 0.5 20.0
20.7 10410621.220.0µg/LBromodichloromethane 70-130 2.3 20.0
22.9 11511021.920.0µg/LBromoform 70-130 4.4 20.0
20.1 10110721.420.0µg/LBromomethane 60-140 6.2 20.0
16.7 83.586.517.320.0µg/Ln-Butylbenzene 70-130 3.5 20.0
17.1 85.588.017.620.0µg/Lsec-Butyl benzene 70-130 2.8 20.0
17.7 88.589.017.820.0µg/Ltert-Butyl benzene 70-130 0.5 20.0
18.1 90.591.518.320.0µg/LChlorobenzene 70-130 1.0 20.0
20.5 10310320.520.0µg/LChlorodibromomethane 70-130 0.0 20.0
23.4 11711723.320.0µg/LChloroethane 60-140 0.4 20.0
18.3 91.594.018.820.0µg/LChloroform 70-130 2.6 20.0
15.7 78.586.517.320.0µg/LChloromethane 60-140 9.6 20.0
19.2 96.097.019.420.0µg/L2-Chlorotoluene 70-130 1.0 20.0
18.4 92.090.518.120.0µg/L4-Chlorotoluene 70-130 1.6 20.0
18.6 93.096.019.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.1 20.0
20.5 10310120.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.9 20.0
19.8 99.097.519.520.0µg/L1,2-Dibromoethane 70-130 1.5 20.0
19.4 97.098.019.620.0µg/LDibromomethane 70-130 1.0 20.0
17.7 88.588.517.720.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0
17.6 88.086.517.320.0µg/L1,3-Dichlorobenzene 70-130 1.7 20.0
17.7 88.586.017.220.0µg/L1,4-Dichlorobenzene 70-130 2.8 20.0
18.6 93.095.019.020.0µg/LDichlorodifluoromethane 60-140 2.1 20.0
19.5 97.510020.020.0µg/L1,1-Dichloroethane 70-130 2.5 20.0
Page 4 of 18Date:02/21/2023 02:25 PM
Page 49 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
LCS-V29853 LCSD-V29853Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.6 93.094.018.820.0µg/L1,2-Dichloroethane 70-130 1.0 20.0
19.6 98.010220.420.0µg/L1,1-Dichloroethene 70-130 4.0 20.0
18.4 92.095.019.020.0µg/Lcis-1,2-Dichloroethene 70-130 3.2 20.0
18.9 94.510120.120.0µg/Ltrans-1,2-Dichloroethene 70-130 6.1 20.0
18.7 93.595.519.120.0µg/L1,2-Dichloropropane 70-130 2.1 20.0
18.6 93.094.018.820.0µg/L1,3-Dichloropropane 70-130 1.0 20.0
18.2 91.095.519.120.0µg/L2,2-Dichloropropane 70-130 4.8 20.0
20.9 10510921.820.0µg/L1,1-Dichloropropene 70-130 4.2 20.0
19.1 95.596.019.220.0µg/Lcis-1,3-Dichloropropene 70-130 0.5 20.0
19.1 95.596.019.220.0µg/Ltrans-1,3-Dichloropropene 70-130 0.5 20.0
589 118110549500µg/LEthanol 60-140 7.0 20.0
18.0 90.092.018.420.0µg/LEthylbenzene 70-130 2.1 20.0
14.5 72.572.514.520.0µg/LHexachlorobutadiene 70-130 0.0 20.0
19.2 96.096.019.220.0µg/L2-Hexanone 60-140 0.0 20.0
18.6 93.097.519.520.0µg/LIsopropylbenzene 70-130 4.7 20.0
17.2 86.088.517.720.0µg/L4-Isopropyl toluene 70-130 2.8 20.0
18.5 92.586.517.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.7 20.0
19.2 96.096.019.220.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
19.2 96.095.019.020.0µg/L4-Methyl-2-Pentanone 60-140 1.0 20.0
18.3 91.594.018.820.0µg/LMethylene Chloride 70-130 2.6 20.0
14.3 71.570.014.020.0µg/LNaphthalene 70-130 2.1 20.0
18.0 90.092.018.420.0µg/Ln-Propylbenzene 70-130 2.1 20.0
18.4 92.096.519.320.0µg/LStyrene 70-130 4.7 20.0
35.0 87.588.035.240.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.5 20.0
29.6 74.073.229.340.0µg/Ltert-Butyl formate (TBF)40-140 1.0 20.0
25.4 12797.519.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 26.2*20.0
Page 5 of 18* QC Fail Date:02/21/2023 02:25 PM
Page 50 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29854QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29853
LCS-V29853 LCSD-V29853Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.6 94.094.537.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.5 20.0
20.6 10310320.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.4 20.0
18.0 90.091.518.320.0µg/LTetrachloroethene 70-130 1.6 20.0
18.7 93.596.019.220.0µg/LToluene 70-130 2.6 20.0
14.6 73.075.515.120.0µg/L1,2,3-Trichlorobenzene 70-130 3.3 20.0
16.3 81.581.516.320.0µg/L1,2,4-Trichlorobenzene 70-130 0.0 20.0
19.4 97.010521.020.0µg/L1,1,1-Trichloroethane 70-130 7.9 20.0
18.5 92.592.518.520.0µg/L1,1,2-Trichloroethane 70-130 0.0 20.0
19.1 95.596.519.320.0µg/LTrichloroethene 70-130 1.0 20.0
20.7 10411021.920.0µg/LTrichlorofluoromethane 60-140 5.6 20.0
18.0 90.084.016.820.0µg/L1,2,3-Trichloropropane 70-130 6.8 20.0
18.0 90.088.517.720.0µg/L1,2,4-Trimethylbenzene 70-130 1.6 20.0
18.3 91.591.518.320.0µg/L1,3,5-Trimethylbenzene 70-130 0.0 20.0
27.5 138148*29.620.0µg/LVinyl Acetate 60-140 7.3 20.0
22.6 11311723.320.0µg/LVinyl Chloride 60-140 3.0 20.0
18.3 91.593.018.620.0µg/Lo-Xylene 70-130 1.6 20.0
37.7 94.297.238.940.0µg/Lm,p-Xylene 70-130 3.1 20.0
20.5 10312424.720.0µg/L3,3-Dimethyl-1-butanol 70-130 18.5 20.0
1011014-Bromofluorobenzene (S)70-130
98.499.8Dibromofluoromethane (S)70-130
97.898.81,2-Dichloroethane - d4 (S)70-130
99.499.6Toluene-d8 (S)70-130
Page 6 of 18* QC Fail Date:02/21/2023 02:25 PM
Page 51 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
Associated Lab Samples: 99794, 99795, 99796
LRB-V29876 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:3610.01.80<1.80µg/LAcetone
02/16/23 13:360.5000.180<0.180µg/LBenzene
02/16/23 13:360.5000.210<0.210µg/LBromobenzene
02/16/23 13:361.000.420<0.420µg/LBromochloromethane
02/16/23 13:360.5000.160<0.160µg/LBromodichloromethane
02/16/23 13:365.001.50<1.50µg/LBromoform
02/16/23 13:361.000.280<0.280µg/LBromomethane
02/16/23 13:360.5000.180<0.180µg/Ln-Butylbenzene
02/16/23 13:360.5000.200<0.200µg/Lsec-Butyl benzene
02/16/23 13:362.000.920<0.920µg/Ltert-Butyl benzene
02/16/23 13:360.5000.180<0.180µg/LCarbon Tetrachloride
02/16/23 13:360.5000.190<0.190µg/LChlorobenzene
02/16/23 13:360.5000.190<0.190µg/LChlorodibromomethane
02/16/23 13:361.000.430<0.430µg/LChloroethane
02/16/23 13:360.5000.220<0.220µg/LChloroform
02/16/23 13:360.5000.220<0.220µg/LChloromethane
02/16/23 13:360.5000.200<0.200µg/L2-Chlorotoluene
02/16/23 13:360.5000.200<0.200µg/L4-Chlorotoluene
02/16/23 13:360.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/16/23 13:362.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/16/23 13:360.5000.200<0.200µg/L1,2-Dibromoethane
02/16/23 13:360.5000.230<0.230µg/LDibromomethane
02/16/23 13:360.5000.220<0.220µg/L1,2-Dichlorobenzene
02/16/23 13:360.5000.190<0.190µg/L1,3-Dichlorobenzene
02/16/23 13:360.5000.210<0.210µg/L1,4-Dichlorobenzene
02/16/23 13:365.001.20<1.20µg/LDichlorodifluoromethane
02/16/23 13:360.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 18Date:02/21/2023 02:25 PM
Page 52 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
Associated Lab Samples: 99794, 99795, 99796
LRB-V29876 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:360.5000.150<0.150µg/L1,2-Dichloroethane
02/16/23 13:360.5000.150<0.150µg/L1,1-Dichloroethene
02/16/23 13:360.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/16/23 13:360.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/16/23 13:360.5000.190<0.190µg/L1,2-Dichloropropane
02/16/23 13:360.5000.130<0.130µg/L1,3-Dichloropropane
02/16/23 13:362.000.210<0.210µg/L2,2-Dichloropropane
02/16/23 13:360.5000.200<0.200µg/L1,1-Dichloropropene
02/16/23 13:360.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/16/23 13:360.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/16/23 13:3620042.0<42.0µg/LEthanol
02/16/23 13:360.5000.170<0.170µg/LEthylbenzene
02/16/23 13:363.000.350<0.350µg/LHexachlorobutadiene
02/16/23 13:361.000.380<0.380µg/L2-Hexanone
02/16/23 13:360.5000.180<0.180µg/LIsopropylbenzene
02/16/23 13:360.5000.089<0.089µg/L4-Isopropyl toluene
02/16/23 13:365.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/16/23 13:361.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/16/23 13:361.000.078<0.078µg/L4-Methyl-2-Pentanone
02/16/23 13:362.000.330<0.330µg/LMethylene Chloride
02/16/23 13:361.000.470<0.470µg/LNaphthalene
02/16/23 13:360.5000.190<0.190µg/Ln-Propylbenzene
02/16/23 13:360.5000.220<0.220µg/LStyrene
02/16/23 13:3610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/16/23 13:3610.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/16/23 13:3610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/16/23 13:3610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 18Date:02/21/2023 02:25 PM
Page 53 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
Associated Lab Samples: 99794, 99795, 99796
LRB-V29876 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/16/23 13:360.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/16/23 13:360.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/16/23 13:360.5000.220<0.220µg/LTetrachloroethene
02/16/23 13:360.5000.220<0.220µg/LToluene
02/16/23 13:360.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/16/23 13:360.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/16/23 13:360.5000.160<0.160µg/L1,1,1-Trichloroethane
02/16/23 13:360.5000.096<0.096µg/L1,1,2-Trichloroethane
02/16/23 13:360.5000.180<0.180µg/LTrichloroethene
02/16/23 13:360.5000.180<0.180µg/LTrichlorofluoromethane
02/16/23 13:360.5000.270<0.270µg/L1,2,3-Trichloropropane
02/16/23 13:360.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/16/23 13:360.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/16/23 13:365.001.00<1.00µg/LVinyl Acetate
02/16/23 13:360.5000.170<0.170µg/LVinyl Chloride
02/16/23 13:360.5000.210<0.210µg/Lo-Xylene
02/16/23 13:361.000.420<0.420µg/Lm,p-Xylene
02/16/23 13:3610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/16/23 13:364-Bromofluorobenzene (S)95.6 70-130
02/16/23 13:36Dibromofluoromethane (S)89.0 70-130
02/16/23 13:361,2-Dichloroethane - d4 (S)89.0 70-130
02/16/23 13:36Toluene-d8 (S)102 70-130
Page 9 of 18Date:02/21/2023 02:25 PM
Page 54 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
LCS-V29876 LCSD-V29876Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.8 57.057.022.840.0µg/LAcetone 40-160 0.0 20.0
19.2 96.097.519.520.0µg/LBenzene 70-130 1.5 20.0
18.4 92.093.018.620.0µg/LBromobenzene 70-130 1.0 20.0
19.1 95.597.519.520.0µg/LBromochloromethane 70-130 2.0 20.0
17.8 89.090.018.020.0µg/LBromodichloromethane 70-130 1.1 20.0
16.9 84.587.017.420.0µg/LBromoform 70-130 2.9 20.0
22.8 11411823.520.0µg/LBromomethane 60-140 3.0 20.0
18.2 91.095.519.120.0µg/Ln-Butylbenzene 70-130 4.8 20.0
18.0 90.095.519.120.0µg/Lsec-Butyl benzene 70-130 5.9 20.0
18.4 92.095.519.120.0µg/Ltert-Butyl benzene 70-130 3.7 20.0
18.7 93.595.519.120.0µg/LCarbon Tetrachloride 70-130 2.1 20.0
18.8 94.097.519.520.0µg/LChlorobenzene 70-130 3.6 20.0
18.7 93.598.019.620.0µg/LChlorodibromomethane 70-130 4.6 20.0
22.2 11111422.720.0µg/LChloroethane 60-140 2.2 20.0
17.9 89.591.518.320.0µg/LChloroform 70-130 2.2 20.0
19.5 97.599.019.820.0µg/LChloromethane 60-140 1.5 20.0
18.2 91.094.518.920.0µg/L2-Chlorotoluene 70-130 3.7 20.0
18.0 90.093.018.620.0µg/L4-Chlorotoluene 70-130 3.2 20.0
19.1 95.595.019.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
19.7 98.510020.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.5 20.0
19.5 97.597.519.520.0µg/L1,2-Dibromoethane 70-130 0.0 20.0
18.8 94.093.018.620.0µg/LDibromomethane 70-130 1.0 20.0
19.0 95.096.019.220.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0
18.9 94.595.519.120.0µg/L1,3-Dichlorobenzene 70-130 1.0 20.0
18.9 94.597.019.420.0µg/L1,4-Dichlorobenzene 70-130 2.6 20.0
18.6 93.093.518.720.0µg/LDichlorodifluoromethane 60-140 0.5 20.0
Page 10 of 18Date:02/21/2023 02:25 PM
Page 55 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
LCS-V29876 LCSD-V29876Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.1 95.596.519.320.0µg/L1,1-Dichloroethane 70-130 1.0 20.0
17.7 88.589.017.820.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
20.4 10210120.120.0µg/L1,1-Dichloroethene 70-130 1.4 20.0
18.4 92.094.518.920.0µg/Lcis-1,2-Dichloroethene 70-130 2.6 20.0
19.2 96.097.019.420.0µg/Ltrans-1,2-Dichloroethene 70-130 1.0 20.0
19.4 97.097.519.520.0µg/L1,2-Dichloropropane 70-130 0.5 20.0
19.4 97.099.519.920.0µg/L1,3-Dichloropropane 70-130 2.5 20.0
19.0 95.097.019.420.0µg/L2,2-Dichloropropane 70-130 2.0 20.0
20.2 10110420.720.0µg/L1,1-Dichloropropene 70-130 2.4 20.0
19.4 97.098.019.620.0µg/Lcis-1,3-Dichloropropene 70-130 1.0 20.0
19.7 98.598.519.720.0µg/Ltrans-1,3-Dichloropropene 70-130 0.0 20.0
433 86.684.6423500µg/LEthanol 60-140 2.3 20.0
18.3 91.594.518.920.0µg/LEthylbenzene 70-130 3.2 20.0
20.5 10310420.720.0µg/LHexachlorobutadiene 70-130 0.9 20.0
16.5 82.580.016.020.0µg/L2-Hexanone 60-140 3.0 20.0
18.4 92.095.019.020.0µg/LIsopropylbenzene 70-130 3.2 20.0
18.8 94.097.019.420.0µg/L4-Isopropyl toluene 70-130 3.1 20.0
14.5 72.570.514.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 2.7 20.0
19.4 97.095.519.120.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.5 20.0
19.4 97.094.518.920.0µg/L4-Methyl-2-Pentanone 60-140 2.6 20.0
18.7 93.595.019.020.0µg/LMethylene Chloride 70-130 1.5 20.0
21.2 10610220.420.0µg/LNaphthalene 70-130 3.8 20.0
18.3 91.595.019.020.0µg/Ln-Propylbenzene 70-130 3.7 20.0
18.0 90.097.019.420.0µg/LStyrene 70-130 7.4 20.0
39.7 99.298.239.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.0 20.0
41.1 10310541.940.0µg/Ltert-Butyl formate (TBF)40-140 1.9 20.0
Page 11 of 18Date:02/21/2023 02:25 PM
Page 56 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29877QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29876
LCS-V29876 LCSD-V29876Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.6 88.090.518.120.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.8 20.0
41.2 10310240.740.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.2 20.0
18.9 94.596.019.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.5 20.0
18.5 92.591.018.220.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.6 20.0
20.2 10110520.920.0µg/LTetrachloroethene 70-130 3.4 20.0
19.4 97.099.019.820.0µg/LToluene 70-130 2.0 20.0
22.8 11411022.020.0µg/L1,2,3-Trichlorobenzene 70-130 3.5 20.0
20.8 10410520.920.0µg/L1,2,4-Trichlorobenzene 70-130 0.4 20.0
18.2 91.092.518.520.0µg/L1,1,1-Trichloroethane 70-130 1.6 20.0
19.9 99.598.019.620.0µg/L1,1,2-Trichloroethane 70-130 1.5 20.0
19.4 97.099.019.820.0µg/LTrichloroethene 70-130 2.0 20.0
20.5 10310521.020.0µg/LTrichlorofluoromethane 60-140 2.4 20.0
19.8 99.097.019.420.0µg/L1,2,3-Trichloropropane 70-130 2.0 20.0
18.1 90.593.018.620.0µg/L1,2,4-Trimethylbenzene 70-130 2.7 20.0
18.2 91.093.018.620.0µg/L1,3,5-Trimethylbenzene 70-130 2.1 20.0
25.1 12613026.020.0µg/LVinyl Acetate 60-140 3.5 20.0
21.4 10711021.920.0µg/LVinyl Chloride 60-140 2.3 20.0
17.8 89.092.018.420.0µg/Lo-Xylene 70-130 3.3 20.0
37.4 93.597.739.140.0µg/Lm,p-Xylene 70-130 4.4 20.0
17.6 88.083.016.620.0µg/L3,3-Dimethyl-1-butanol 70-130 5.8 20.0
95.896.44-Bromofluorobenzene (S)70-130
89.689.2Dibromofluoromethane (S)70-130
90.889.81,2-Dichloroethane - d4 (S)70-130
98.8102Toluene-d8 (S)70-130
Page 12 of 18Date:02/21/2023 02:25 PM
Page 57 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
Associated Lab Samples: 99793
LRB-V29909 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/17/23 14:3710.01.80<1.80µg/LAcetone
02/17/23 14:370.5000.180<0.180µg/LBenzene
02/17/23 14:370.5000.210<0.210µg/LBromobenzene
02/17/23 14:371.000.420<0.420µg/LBromochloromethane
02/17/23 14:370.5000.160<0.160µg/LBromodichloromethane
02/17/23 14:375.001.50<1.50µg/LBromoform
02/17/23 14:371.000.280<0.280µg/LBromomethane
02/17/23 14:370.5000.180<0.180µg/Ln-Butylbenzene
02/17/23 14:370.5000.200<0.200µg/Lsec-Butyl benzene
02/17/23 14:372.000.920<0.920µg/Ltert-Butyl benzene
02/17/23 14:370.5000.180<0.180µg/LCarbon Tetrachloride
02/17/23 14:370.5000.190<0.190µg/LChlorobenzene
02/17/23 14:370.5000.190<0.190µg/LChlorodibromomethane
02/17/23 14:371.000.430<0.430µg/LChloroethane
02/17/23 14:370.5000.220<0.220µg/LChloroform
02/17/23 14:370.5000.220<0.220µg/LChloromethane
02/17/23 14:370.5000.200<0.200µg/L2-Chlorotoluene
02/17/23 14:370.5000.200<0.200µg/L4-Chlorotoluene
02/17/23 14:370.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
02/17/23 14:372.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
02/17/23 14:370.5000.200<0.200µg/L1,2-Dibromoethane
02/17/23 14:370.5000.230<0.230µg/LDibromomethane
02/17/23 14:370.5000.220<0.220µg/L1,2-Dichlorobenzene
02/17/23 14:370.5000.190<0.190µg/L1,3-Dichlorobenzene
02/17/23 14:370.5000.210<0.210µg/L1,4-Dichlorobenzene
02/17/23 14:375.001.20<1.20µg/LDichlorodifluoromethane
02/17/23 14:370.5000.240<0.240µg/L1,1-Dichloroethane
Page 13 of 18Date:02/21/2023 02:25 PM
Page 58 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
Associated Lab Samples: 99793
LRB-V29909 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/17/23 14:370.5000.150<0.150µg/L1,2-Dichloroethane
02/17/23 14:370.5000.150<0.150µg/L1,1-Dichloroethene
02/17/23 14:370.5000.200<0.200µg/Lcis-1,2-Dichloroethene
02/17/23 14:370.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
02/17/23 14:370.5000.190<0.190µg/L1,2-Dichloropropane
02/17/23 14:370.5000.130<0.130µg/L1,3-Dichloropropane
02/17/23 14:372.000.210<0.210µg/L2,2-Dichloropropane
02/17/23 14:370.5000.200<0.200µg/L1,1-Dichloropropene
02/17/23 14:370.5000.210<0.210µg/Lcis-1,3-Dichloropropene
02/17/23 14:370.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
02/17/23 14:3720042.0<42.0µg/LEthanol
02/17/23 14:370.5000.170<0.170µg/LEthylbenzene
02/17/23 14:373.000.350<0.350µg/LHexachlorobutadiene
02/17/23 14:371.000.380<0.380µg/L2-Hexanone
02/17/23 14:370.5000.180<0.180µg/LIsopropylbenzene
02/17/23 14:370.5000.089<0.089µg/L4-Isopropyl toluene
02/17/23 14:375.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
02/17/23 14:371.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
02/17/23 14:371.000.078<0.078µg/L4-Methyl-2-Pentanone
02/17/23 14:372.000.330<0.330µg/LMethylene Chloride
02/17/23 14:371.000.470<0.470µg/LNaphthalene
02/17/23 14:370.5000.190<0.190µg/Ln-Propylbenzene
02/17/23 14:370.5000.220<0.220µg/LStyrene
02/17/23 14:3710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
02/17/23 14:3710.00.350<0.350µg/Ltert-Butyl formate (TBF)
02/17/23 14:3710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
02/17/23 14:3710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 14 of 18Date:02/21/2023 02:25 PM
Page 59 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
Associated Lab Samples: 99793
LRB-V29909 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/17/23 14:370.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
02/17/23 14:370.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
02/17/23 14:370.5000.220<0.220µg/LTetrachloroethene
02/17/23 14:370.5000.220<0.220µg/LToluene
02/17/23 14:370.5000.380<0.380µg/L1,2,3-Trichlorobenzene
02/17/23 14:370.5000.310<0.310µg/L1,2,4-Trichlorobenzene
02/17/23 14:370.5000.160<0.160µg/L1,1,1-Trichloroethane
02/17/23 14:370.5000.096<0.096µg/L1,1,2-Trichloroethane
02/17/23 14:370.5000.180<0.180µg/LTrichloroethene
02/17/23 14:370.5000.180<0.180µg/LTrichlorofluoromethane
02/17/23 14:370.5000.270<0.270µg/L1,2,3-Trichloropropane
02/17/23 14:370.5000.190<0.190µg/L1,2,4-Trimethylbenzene
02/17/23 14:370.5000.180<0.180µg/L1,3,5-Trimethylbenzene
02/17/23 14:375.001.00<1.00µg/LVinyl Acetate
02/17/23 14:370.5000.170<0.170µg/LVinyl Chloride
02/17/23 14:370.5000.210<0.210µg/Lo-Xylene
02/17/23 14:371.000.420<0.420µg/Lm,p-Xylene
02/17/23 14:3710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
02/17/23 14:374-Bromofluorobenzene (S)101 70-130
02/17/23 14:37Dibromofluoromethane (S)99.8 70-130
02/17/23 14:371,2-Dichloroethane - d4 (S)98.8 70-130
02/17/23 14:37Toluene-d8 (S)99.0 70-130
Page 15 of 18Date:02/21/2023 02:25 PM
Page 60 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
LCS-V29909 LCSD-V29909Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.5 98.798.039.240.0µg/LAcetone 40-160 0.7 20.0
20.9 10510220.320.0µg/LBenzene 70-130 2.9 20.0
19.5 97.595.019.020.0µg/LBromobenzene 70-130 2.5 20.0
21.1 10610521.020.0µg/LBromochloromethane 70-130 0.4 20.0
22.7 11411522.920.0µg/LBromodichloromethane 70-130 0.8 20.0
23.1 11611723.320.0µg/LBromoform 70-130 0.8 20.0
24.6 12311923.820.0µg/LBromomethane 60-140 3.3 20.0
18.5 92.591.518.320.0µg/Ln-Butylbenzene 70-130 1.0 20.0
19.0 95.094.018.820.0µg/Lsec-Butyl benzene 70-130 1.0 20.0
19.5 97.598.519.720.0µg/Ltert-Butyl benzene 70-130 1.0 20.0
25.4 12713025.920.0µg/LCarbon Tetrachloride 70-130 1.9 20.0
19.6 98.010220.420.0µg/LChlorobenzene 70-130 4.0 20.0
21.8 10911021.920.0µg/LChlorodibromomethane 70-130 0.4 20.0
23.9 12011422.720.0µg/LChloroethane 60-140 5.1 20.0
20.3 10210220.320.0µg/LChloroform 70-130 0.0 20.0
18.0 90.088.517.720.0µg/LChloromethane 60-140 1.6 20.0
20.6 10393.518.720.0µg/L2-Chlorotoluene 70-130 9.6 20.0
19.6 98.099.519.920.0µg/L4-Chlorotoluene 70-130 1.5 20.0
20.3 10210320.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.9 20.0
21.6 10899.519.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 8.1 20.0
20.5 10310520.920.0µg/L1,2-Dibromoethane 70-130 1.9 20.0
21.0 10510520.920.0µg/LDibromomethane 70-130 0.4 20.0
19.0 95.096.019.220.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0
18.8 94.094.518.920.0µg/L1,3-Dichlorobenzene 70-130 0.5 20.0
19.3 96.595.519.120.0µg/L1,4-Dichlorobenzene 70-130 1.0 20.0
20.2 10110320.520.0µg/LDichlorodifluoromethane 60-140 1.4 20.0
Page 16 of 18Date:02/21/2023 02:25 PM
Page 61 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
LCS-V29909 LCSD-V29909Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10910821.520.0µg/L1,1-Dichloroethane 70-130 0.9 20.0
20.4 10298.019.620.0µg/L1,2-Dichloroethane 70-130 4.0 20.0
23.0 11511122.220.0µg/L1,1-Dichloroethene 70-130 3.5 20.0
20.3 10210120.120.0µg/Lcis-1,2-Dichloroethene 70-130 0.9 20.0
22.5 11310921.720.0µg/Ltrans-1,2-Dichloroethene 70-130 3.6 20.0
21.2 10610521.020.0µg/L1,2-Dichloropropane 70-130 0.9 20.0
20.4 10210320.620.0µg/L1,3-Dichloropropane 70-130 0.9 20.0
21.5 10810821.620.0µg/L2,2-Dichloropropane 70-130 0.4 20.0
23.9 12011923.720.0µg/L1,1-Dichloropropene 70-130 0.8 20.0
20.9 10510120.120.0µg/Lcis-1,3-Dichloropropene 70-130 3.9 20.0
20.9 10510120.120.0µg/Ltrans-1,3-Dichloropropene 70-130 3.9 20.0
504 10199.6498500µg/LEthanol 60-140 1.1 20.0
19.8 99.098.019.620.0µg/LEthylbenzene 70-130 1.0 20.0
15.9 79.579.015.820.0µg/LHexachlorobutadiene 70-130 0.6 20.0
20.3 10298.519.720.0µg/L2-Hexanone 60-140 3.0 20.0
21.3 10710520.920.0µg/LIsopropylbenzene 70-130 1.8 20.0
19.2 96.096.519.320.0µg/L4-Isopropyl toluene 70-130 0.5 20.0
19.0 95.092.018.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.2 20.0
20.3 10210320.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
20.3 10299.019.820.0µg/L4-Methyl-2-Pentanone 60-140 2.4 20.0
20.0 10099.019.820.0µg/LMethylene Chloride 70-130 1.0 20.0
14.7 73.574.514.920.0µg/LNaphthalene 70-130 1.3 20.0
19.7 98.599.019.820.0µg/Ln-Propylbenzene 70-130 0.5 20.0
20.8 10410320.620.0µg/LStyrene 70-130 0.9 20.0
36.7 91.784.733.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 7.9 20.0
31.0 77.576.230.540.0µg/Ltert-Butyl formate (TBF)40-140 1.6 20.0
Page 17 of 18Date:02/21/2023 02:25 PM
Page 62 of 65
Quality Control Data
23-046-0007Report No:
Project Description:
Client ID:Geological Resources, Inc.
Roseboro BP
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29909
LCS-V29909 LCSD-V29909Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10912324.620.0µg/Ltert-Amyl Alcohol (TAA)40-140 12.5 20.0
40.8 10210240.640.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.4 20.0
20.4 10210521.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0
21.2 10610621.120.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.4 20.0
20.4 10210120.120.0µg/LTetrachloroethene 70-130 1.4 20.0
20.5 10310120.220.0µg/LToluene 70-130 1.4 20.0
16.4 82.080.516.120.0µg/L1,2,3-Trichlorobenzene 70-130 1.8 20.0
17.4 87.086.517.320.0µg/L1,2,4-Trichlorobenzene 70-130 0.5 20.0
23.0 11511021.920.0µg/L1,1,1-Trichloroethane 70-130 4.8 20.0
19.5 97.510020.020.0µg/L1,1,2-Trichloroethane 70-130 2.5 20.0
20.4 10210320.620.0µg/LTrichloroethene 70-130 0.9 20.0
23.4 11711222.420.0µg/LTrichlorofluoromethane 60-140 4.3 20.0
18.3 91.593.518.720.0µg/L1,2,3-Trichloropropane 70-130 2.1 20.0
19.3 96.597.519.520.0µg/L1,2,4-Trimethylbenzene 70-130 1.0 20.0
20.2 10110220.420.0µg/L1,3,5-Trimethylbenzene 70-130 0.9 20.0
28.2 141*12625.120.0µg/LVinyl Acetate 60-140 11.6 20.0
23.5 11812124.120.0µg/LVinyl Chloride 60-140 2.5 20.0
19.8 99.099.519.920.0µg/Lo-Xylene 70-130 0.5 20.0
41.1 10310441.740.0µg/Lm,p-Xylene 70-130 1.4 20.0
24.9 12512524.920.0µg/L3,3-Dimethyl-1-butanol 70-130 0.0 20.0
99.499.64-Bromofluorobenzene (S)70-130
98.098.2Dibromofluoromethane (S)70-130
98.098.01,2-Dichloroethane - d4 (S)70-130
99.299.6Toluene-d8 (S)70-130
Page 18 of 18* QC Fail Date:02/21/2023 02:25 PM
Page 63 of 65
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-046-0007
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:02/15/2023 11:14:00
Special precautions or instructions included?
Comments:
Page 64 of 65
Page 65 of 65

APPENDIX D
Contaminant Mass Calculations
0.00
5.00
10.00
15.00
20.00
0.00
5,000.00
10,000.00
15,000.00
20,000.00
25,000.00
Average Water Column Height (ft)Contaminant Mass (grams)Time
Total Contaminant Mass vs. Time
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
Contaminant Mass Water Column Height (ft)Linear (Contaminant Mass)
Area ID Well ID
Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-2R
MW-43
MW-44
Area Date Well
Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red. To Date Red.
MW-2R 517.00 61.30 1,620.00 3,070.00 73.00 1,240.00 6,581.30 11.16
MW-43 1,090.00 4,460.00 1,170.00 5,670.00 73.60 263.00 12,726.60 11.07
MW-44 1,180.00 129.00 1,000.00 2,430.00 611.00 380.00 5,730.00 10.02
Avg.929.00 1,550.10 1,263.33 3,723.33 252.53 627.67 8,345.97 10.75
MW-2R 250.00 13.10 650.00 269.00 34.60 1330.00 2546.70 11.50
MW-43 2110.00 5880.00 798.00 3970.00 0.00 180.00 12938.00 11.37
MW-44 603.00 44.30 330.00 939.00 290.00 138.00 2344.30 10.40
Avg.987.67 1979.13 592.67 1726.00 108.20 549.33 5943.00 11.09
MW-2R 647.00 74.70 1480.00 3400.00 55.80 1140.00 6797.50 11.76
MW-43 8020.00 15500.00 1560.00 6950.00 198.00 290.00 32518.00 12.26
MW-44 269.00 16.70 54.30 282.00 80.10 34.30 736.40 11.19
Avg.2978.67 5197.13 1031.43 3544.00 111.30 488.10 13350.63 11.74
MW-2R 461.00 15.90 1190.00 99.20 42.70 1200.00 3008.80 12.68
MW-43 8940.00 20500.00 1990.00 8340.00 396.00 812.00 40978.00 12.39
MW-44 232.00 6.50 24.10 98.60 71.00 30.10 462.30 11.39
Avg.3211.00 6840.80 1068.03 2845.93 169.90 680.70 14816.37 12.15
MW-2R 170.00 14.50 613.00 97.50 0.00 684.00 1579.00 12.58
MW-43 3480.00 7690.00 945.00 4570.00 74.10 146.00 16905.10 12.37
MW-44 584.00 42.50 392.00 1030.00 169.00 142.00 2359.50 11.37
Avg.1411.33 2582.33 650.00 1899.17 81.03 324.00 6947.87 12.11
MW-2R 163.00 6.80 403.00 27.10 19.50 798.00 1417.40 13.23
MW-43 5540.00 13800.00 1440.00 6880.00 92.00 354.00 28106.00 12.88
MW-44 480.00 16.10 189.00 678.00 107.00 68.40 1538.50 11.81
Avg.2061.00 4607.63 677.33 2528.37 72.83 406.80 10353.97 12.64
MW-2R 26.70 0.97 27.90 9.70 11.20 226.00 302.47 11.62
MW-43 2880.00 7610.00 964.00 4690.00 0.00 136.00 16280.00 11.43
MW-44 252.00 8.20 132.00 471.00 71.10 83.20 1017.50 10.42
Avg.1052.90 2539.72 374.63 1723.57 27.43 148.40 5866.66 11.16
MW-2R 58.30 0.00 28.50 0.00 20.10 291.00 397.90 11.84
MW-43 1710.00 3640.00 659.00 3160.00 0.00 152.00 9321.00 13.18
MW-44 600.00 25.70 370.00 1180.00 121.00 156.00 2452.70 12.16
Avg.789.43 1221.90 352.50 1446.67 47.03 199.67 4057.20 12.39
MW-2R NS NS NS NS NS NS NM NM
MW-43 1640.00 2740.00 597.00 2730.00 0.00 0.00 7707.00 14.11
MW-44 219.00 7.61 62.80 167.00 30.00 46.00 532.41 13.02
Avg.929.50 1373.81 329.90 1448.50 15.00 23.00 4119.71 13.57
Date
Average Water
Column Height
(ft.)12/15/15 14.25
06/08/16 13.91
02/20/17 13.26
05/16/18 12.85
11/13/18 12.89
11/07/19 12.36
11/04/20 13.84
01/04/22 12.61
02/14/23 11.44
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 6
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
36.5% 31.7%
22,369.09 -7.5% -60.0%
-7.6%
9,715.14 30.5% 30.5%
13.26 20,809.93 -114.2% -48.9%
60%
------
30%30%
25%
57.0%
13,976.80 --- ---
11/13/18 12.89 10,527.68 52.9% 24.7%
14.25
12.61
06/08/16
02/20/17
6,010.95 37.0%
05/16/18
APPENDIX D
CONTAMINANT MASS CALCULATIONS
FORMER ROSEBORO BP STATION (INCIDENT NO. 6601)
Baseline Event
1 20,751.1 25 10.78 14.22 295,081 8,355,756 0.20 1,671,151
Area 1
02/14/23 11.44 5,536.28 7.9%
12/15/15
01/04/22
11/07/19
11/04/20
13.91
12.85
13.84
12.36 15,039.78 -42.9%
9,544.37
60.4%
13,976.80
9,715.14
5,536.28
20,809.93 -114%-49%
22,369.09 -7%-60%
10,527.68 53%
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
43%
6,010.95 37%57%
15,039.78 -43%-8%
9,544.37 37%32%