WS-96264_96898_CA_IAR_20230301

March 1, 2023

Guilford County Health Department
Toxic & Health Hazard Division
400 West Market Street, Suite 300
Greensboro, North Carolina 27401

North Carolina Department of Environmental Quality
Winston-Salem Regional Office
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105

ATTN: Mr. Jordan Lerew; Mr. Michael Phelps
Via Email: [e-mail]; [e-mail]

Spill ID Number: 12192022-8
Our File Number: 091-12616
Responsible Party: US1 Logistics, LLC
Driver: Marquise Arrington
Location of Loss: Greensboro, Guilford County, North Carolina
Type of Loss: Diesel Fuel Spill
Date of Loss: Monday, December 19, 2022

INCIDENT CLOSURE REPORT

ENCLOSURES:

1. UST-62
2. Laboratory Analysis
3. Disposal Documentation
4. Photographs

SOURCE & DATE OF ASSIGNMENT:

The Custard Insurance Adjusters, Inc. Environmental Services Division received this
assignment from Rhonda Hyde, with US1 Logistics, on Monday, December 19, 2022.

Address Reply To:

4875 Avalon Ridge Parkway
Peachtree Corners, GA 30071
Direct: 678.287.5447
Fax: [phone]
Page 2
Responsible Party: US1 Logistics, LLC
091-12616

RESPONSIBLE PARTY:

US1 Logistics, LLC
203 Fort Wade Road, Suite # 320
Ponte Vedra, Florida 32081

LOCATION OF LOSS:

35.996868, -79.758845
Interstate 85; Northbound, Exit # 126A
Guilford County
Greensboro, North Carolina

DATE OF LOSS:

Monday, December 19, 2022

DESCRIPTION OF LOSS:

It is our understanding that the US 1 Logistics vehicle was involved in an accident, resulting
in the release of approximately 100 gallons of diesel fuel onto the roadway, paved shoulder,
and into hardpacked roadside gravel and clay.

SITE REMEDIATION:

Upon receipt of this assignment, we contacted Ecoflo Holding, Inc. DBA US Ecology (USE)
to provide site remediation. Fire department personnel were already on scene at the time of
the accident and immediately utilized absorbents to contain most of the spill to the roadway.
A minimal volume of the spilled fuel flowed off the pavement and impacted the hardpacked
gravel area between the roadway and exit ramp. USE personnel applied additional granular
absorbents to the impacted pavement. Hand tools were utilized to work the absorbents into
the pavement and recover the spent absorbents. A vacuum truck and hand tools were
utilized to recover approximately 60 gallons of pooled fuel, spent absorbents, and fuel-
impacted gravel and clay. Background and confirmation soil samples were collected for
laboratory analysis. The laboratory results are attached and indicate that the site was
cleaned to within acceptable standards. All cleanup-generated waste was placed into seven
(7) 55-gallon drums and transported the waste for proper disposal.

WASTE DISPOSAL:

All cleanup-generated waste was transported to the Terranova Solutions facility, located in
High Point, North Carolina, on Manifest Number P215-11455. The waste was received for
disposal on December 19, 2022, by Barry Ward and Blake K. The disposal facility was
chosen by USE and the disposal documentation is attached.

Page 3
Responsible Party: US1 Logistics, LLC
091-12616

REMARKS:

With submittal of this Incident Closure Report, with attachments, we request that this incident
be closed with no further action required.

If you have any questions or need any additional information, please contact us.

Regards,

Custard Insurance Adjusters, Inc.
Angel White
Environmental Specialist
[e-mail]
www.custard.com

ThisformshouldbecompletedandsubmittedtotheUSTSection’sregionalofficefollowingaknownor suspectedreleaseof
petroleumfromasourceotherthananundergroundstoragetank.Thisformisrequiredtobesubmittedwithin24hoursofdiscoveryofa knownorsuspectedpetroleumrelease
(DWM USEONLY)
Incident#___________Priority Rank(H,I,L,U)_____
Received(time/date)___________________________
Receivedby________________ Region__________
Reportedby (circleone):Phone,FaxorReport
SuspectedContamination?(Y/N)___
ConfirmedGWContamination?(Y/N)___
ConfirmedSoilContamination?(Y/N)___
Samples taken?(Y/N)___Freeproduct?(Y/N)___
IfYes(freeproduct), stategreatestthickness:_____feet
Releasediscovered
(time/date):______________
_______________________
INCIDENTDESCRIPTION
Incident Name:
Address(streetnumber/name):County:
City/Town:Zip Code:RegionalOffice (circleone):Asheville,Mooresville,Fayetteville,Raleigh,Washington,Wilmington,Winston-Salem
Latitude (decimal degrees):Longitude (decimal degrees) :Obtainedby:
Describesuspectedorconfirmedrelease (natureofrelease, time/dateofrelease,quantityofrelease,amountoffree
product):GPS
Electronictopographicmap
GISAddressmatching
Describeinitialresponse/abatement (time/datereleasestopped,cleanupbegun/completed,quantityofproduct
soilremoved,confirmationsampling):
Other
Unknown
Describeimpactedreceptors:Describelocation:
HOW RELEASEWASDISCOVERED (Release Code)
(Checkone)
Observationof ReleaseatOccurrence
VisualorOlfactoryEvidence
SoilContamination
GroundwaterContamination
WaterSupply WellContamination
Surface WaterContamination
Other(specify)_______________
SOURCEOF CONTAMINATION
SourceofRelease
(Checkonetoindicateprimarysource)
CauseofRelease
(Checkonetoindicateprimarycause)
Typeof Release
(Checkone)
ProductType Released
(Checkone toindicateprimarypetroleumproducttypereleased)
AST(tank)
ASTPiping/Dispenser
AST DeliveryProblem
OTRVehicle Tank
OTRBulk TransportTank
RRBulk TransportTank
Transformer
Unknown
Other______________
Definitionspresentedonreverse
Spill(Accidental)
Spill(Intentional)
Corrosion
Physicalor Mechanical
Damage
EquipmentFailure
ASTOverfill
ASTInstallationProblem
Unknown
Other______________
Definitionspresentedonreverse
Petroleum
BothPetroleum
& Non-Petroleum
Location
(Checkone)
Facility
Residence
Highway/Road
Railway
Other
Gasoline/Diesel/
Kerosene
E11–E20
E21–E84
E85–E99
Ethanol100%
Diesel/Veg.Oil
Blend
VegetableOil100%
HeatingOil
WasteOil
MineralOil-no
PCBs
MineralOil-PCBs
OtherPetroleum
Products________
Ownership1. Municipal2.Military3.Unknown4.Private5. Federal6. County7.State
Operation Type
1.PublicService2.Agricultural3.Residential4.Education/Relig.5.Industrial6.Commercial7.Mining
Guidancepresentedonreverse
USTForm62(04/10)Page1of 2
12/19/2022
0700 hrs
N
N
N
N N
US 1 Logistics Diesel Fuel Spill 12192022-8
Guilford County
Greensboro
I-85; Northbound, Exit # 126A
35.996868 -79.758845
Tractor trailer saddle tank ruptured as a result of tractor striking a fire truck at approximately 0630 hours on 12/19/2022. Approximately 100 gallons of diesel fuel and a minimal volume of motor
oil were released.
Fire department personnel were on scene when the incident occured and immediately used granular and pad absorbents to
Paved roadway, paved median, hard packed gravel/clay median
contain the spill to the roadway.US Ecology arrived at 0900 hrs on 12/19/2022, utilized a vac truck to recover 60 gallons of fuel from the roadway, applied additional absorbents, used hand tools to remove impacted gravel where the fuel left the edge of the roadway, recovered and transported 60 gallons of petroleum and six (6) 55-gallon drums of spent absorbents, wreckage debris,
and gravel. No sampling was performed. Cleanup was complete at approximately 1145 hrs on 12/19/2022.
Motor Vehicle Accident
IMPACT ON DRINKINGWATERSUPPLIES
WaterSupplyWellsAffected?1.Yes 2.No 3. Unknown NumberofWaterSupplyWellsAffected______
ListofWaterSupply WellsContaminated: (Include Users Names,AddressesandPhoneNumbers.Attachadditionalsheetifnecessary)
1.
2.
3.
PARTY RESPONSIBLEFOR RELEASE
(ifthesourceof thereleaseisnotanASTsystemorifitisanAST systemandthereisaresponsiblepartyotherthan theASTsystemowner/operator)
NameofPerson/Company Address
City State ZipCode TelephoneNumber
ASTSYSTEMOWNER (ifthesourceofthereleaseisanAST system)
ASTOwner/Company Address
City State ZipCode TelephoneNumber
ASTSYSTEMOPERATOR (ifthesourceof thereleaseisanASTsystem)
USTOperator/Company Address
City State ZipCode TelephoneNumber
LANDOWNER ATLOCATION OF INCIDENT
Landowner Address
City State ZipCode TelephoneNumber
DrawSketchof AreaorProvideMap (showingincidentsite,locationofrelease,twomajorroadintersections,potential
receptors)
Attachsketchor maptoform.
Give Directionsto IncidentSite Attachdirectionsto formifnecessary.
PersonReportingIncident Company TelephoneNumber
Title Address Date
USTForm62(04/10)Page2of 2
DefinitionsofSources
AST(Tank):meansthetankisusedtostoreproductASTPiping:meansthepipingandconnectorsrunningfromthetanktothedispenserorotherend-useequipment
ASTDispenser:includesthedispenserandtheequipmentusedtoconnectthedispensertothepiping
ASTDeliveryProblem:identifiesreleasesthatoccurredduringproductdeliverytothetank.
OTRVehicleTank:meansthetankisusedtostoreproducttofuelanovertheroadvehicle
OTRBulkTransportTank:meansatankthatisusedtotransportproductinbulkovertheroad(bytruck)
RR:bulkTransportTank:meansatankthatisusedtotransportproductinbulkbytrain
Transformer:meanselectricaltransformerOther:servesastheoptiontousewhenthereleasesourceisknownbutdoesnotfitintooneoftheprecedingcategories
Unknown:identifiesreleasesforwhichthesourcehasnotbeendetermined
DefinitionsofCauses
Spill(Accidental):usethiscausewhenaspilloccursaccidentally(e.g.,whenthedeliveryhoseisdisconnectedfromafillpipe)
Spill(Intentional):usethiscausewhenaspilloccursintentionally(e.g.,intentionaldumpingorbreakage)
Corrosion:usewhenametaltank,piping,orothercomponenthasareleaseduetocorrosion
PhysicalorMechanicalDamage:useforalltypesofphysicalormechanicaldamage,exceptcorrosionEquipmentfailure:usewhenareleaseoccursduetoequipmentfailureotherthancorrosionorphysicalormechanicaldamage
ASTOverfill:usewhenanoverfilloccurs(e.g.,overfillsmayoccurfromthefillpipeatthetankorwhenthenozzlefailstoshutoffatthedispenser)
ASTInstallationProblem:usewhentheproblemisdeterminedtohaveoccurredspecificallybecausetheASTsystemwasnotinstalledproperly
Other:usethisoptionwhenthecauseisknownbutdoesnotfitintooneoftheprecedingcategories
Unknown:usewhenthecausehasnotbeendetermined
Guidance:OwnershipandOperatorTypeOwnershipselectthecategorywhichdescribesowneroftheASTsystem,bulktransporttank,orotherreleasesource
OperatorType selectthecategorywhichdescribestheoperationinwhichownerusestheASTsystem,bulktransporttank,orotherreleasesource
203 Fort Wade Road, Suite # 320
Ponte Vedra Florida 32081 [phone]
Rhonda Hyde for US 1 Logistics, LLC
Department of Transportation
Angel White Custard Insurance Adjusters 706-392-9742
Agent for US 1 Logistics, LLC 12/19/2022
Interstate 85; Northbound on the wedge of land between the interstate and Exit Ramp # 126A
4875 Avalon Ridge Parkway, Peachtree Corners, GA 30071
12192022-8
Hot Zone Sample = Confirmation Sample after Completion of Remediation (41 PPM DRO)
Cold Zone Sample = Sample from outside of spill area (138 PPM DRO)
Legend
Background sample from "Cold Zone" 250 feet away from spill
Confirmation Sample from "Hot Zone" after remediation
70 ft N➤➤NImage Landsat / Copernicus
Image Landsat / Copernicus
Image Landsat / Copernicus
12192022-8
Write a description for your map.
Legend
Accident Site
Impact to Soil
5.44 ft N➤➤N© 2023 Google
© 2023 Google
© 2023 Google
#=CL#
January 30, 2023
LIMS USE: FR - RUSTY WADDELL
LIMS OBJECT ID: 92646290
92646290
Project:
Pace Project No.:
RE:
Rusty Waddell
US ECOLOGY
,
US ECOLOGY
Dear Rusty Waddell:
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Zachary J Tierney
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92646290
US ECOLOGY
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92646290
US ECOLOGY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92646290001 HOT EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 9071B 1 PANABP
92646290002 COLD EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 9071B 1 PANABP
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646290
US ECOLOGY
Sample:HOT Lab ID:92646290001 Collected:01/10/23 00:00 Received:01/10/23 10:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)41.0 mg/kg 01/19/23 11:4001/18/23 16:546.6 1
Surrogates
n-Pentacosane (S)77 %01/19/23 11:40629-99-201/18/23 16:5410-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.2 %01/16/23 16:15 N20.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.2 %01/19/23 11:1901/19/23 10:591
Analytical Method: EPA 9071B Preparation Method: 9071B
Pace National - Mt. Juliet
Wet Chemistry 9071B
Oil and Grease 1710 mg/kg 01/21/23 17:5301/20/23 10:331201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646290
US ECOLOGY
Sample:COLD Lab ID:92646290002 Collected:01/10/23 00:00 Received:01/10/23 10:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)138 mg/kg 01/19/23 11:5601/18/23 16:545.7 1
Surrogates
n-Pentacosane (S)58 %01/19/23 11:56629-99-201/18/23 16:5410-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.3 %01/16/23 16:15 N20.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 89.0 %01/19/23 11:1901/19/23 10:591
Analytical Method: EPA 9071B Preparation Method: 9071B
Pace National - Mt. Juliet
Wet Chemistry 9071B
Oil and Grease 2740 mg/kg 01/21/23 17:5301/20/23 10:331121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646290
US ECOLOGY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
750190
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92646290001, 92646290002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3899364
Associated Lab Samples:92646290001, 92646290002
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.101/19/23 10:27
n-Pentacosane (S)%68 10-13001/19/23 10:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3899365LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 40.866.2 62 44-130
n-Pentacosane (S)%69 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3899366MATRIX SPIKE SAMPLE:
MSSpike
Result
92647173001
Diesel Range Organics(C10-C28)mg/kg 4910 M178.4 1180 10-1303990
n-Pentacosane (S)%S019910-130
Parameter Units
Dup
Result QualifiersRPDResult
92647173002
3899367SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 3050 63250
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646290
US ECOLOGY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
749633
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92646290001, 92646290002
Parameter Units
Dup
Result QualifiersRPDResult
92646290001
3897017SAMPLE DUPLICATE:
Percent Moisture %22.3 N2423.2
Parameter Units
Dup
Result QualifiersRPDResult
92646930004
3897018SAMPLE DUPLICATE:
Percent Moisture %13.4 N21215.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646290
US ECOLOGY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1990711
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92646290001, 92646290002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3882786-1
Associated Lab Samples:92646290001, 92646290002
Matrix:Solid
Analyzed
Total Solids %0.00100 01/19/23 11:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3882786-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result QualifiersRPDResult
92646290002
R3882786-3SAMPLE DUPLICATE:
Total Solids %88.1 0.92589.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646290
US ECOLOGY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1991707
9071B
EPA 9071B
Wet Chemistry 9071B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92646290001, 92646290002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3883169-1
Associated Lab Samples:92646290001, 92646290002
Matrix:Solid
Analyzed
Oil and Grease mg/kg ND 10001/21/23 17:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3883169-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3883169-3
Oil and Grease mg/kg 35904000 89.8 80.0-12099.83990 10.6 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3883169-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1577452-01
R3883169-6
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Oil and Grease mg/kg ML400074.2 80.0-12075.1 1.14400018831503190
Parameter Units
Dup
Result QualifiersRPDResult
L1577452-01
R3883169-4SAMPLE DUPLICATE:
Oil and Grease mg/kg ND D862.1188
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92646290
US ECOLOGY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not be
statistically valid.D8
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. Acomplete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92646290
US ECOLOGY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92646290001 750190 750408HOTEPA 3546 EPA 8015C
92646290002 750190 750408COLDEPA 3546 EPA 8015C
92646290001 749633HOTSW-846
92646290002 749633COLDSW-846
92646290001 1990711 1990711HOTSM 2540 G SM 2540G
92646290002 1990711 1990711COLDSM 2540 G SM 2540G
92646290001 1991707 1991707HOT9071BEPA 9071B
92646290002 1991707 1991707COLD9071BEPA 9071B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/30/2023 06:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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