WS-96251_96870_CA_IAR_20230503

INITIAL ABATEMENT ACTION REPORT
13’ 6” TRUCK WASH
AST INCIDENT 96870
2500/2502 EAST MARKET STREET
GREENSBORO, GUILFORD COUNTY, NORTH CAROLINA
FACILITY I.D. NO.: N/A
MID-ATLANTIC JOB NO. R4229.01
May 3, 2023
Mid-Atlantic Job No. R4229.01
Prepared For: Prepared By:
VG Greensboro Storage LLC MID-ATLANTIC ASSOCIATES, INC.
Mr. Benjamin Ho
2500 East Market Street
Greensboro, North Carolina 27401
Kevin R. Clay, PG
Project Geologist
Raymond S. Marchant, III P.G.
Principal Geologist
TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................. 1 
1.1 Introduction.................................................................................................................... 1 
1.2 Owner/Operator of the AST ........................................................................................... 2 
1.3 Property Owner ............................................................................................................. 2 
1.4 Facility Information ........................................................................................................ 2 
1.5 Contacts ........................................................................................................................ 2 
1.6 AST Information ............................................................................................................ 3 
1.7 Site Characteristics ....................................................................................................... 3
2.0 INITIAL RESPONSE AND ABATEMENT ACTION .......................................................... 3
2.1 Preliminary Soil and Sediment Assessment .................................................................. 3 
2.2 Site Cleanup and Sediment Removal ........................................................................... 4 
2.3 Soil Excavation .............................................................................................................. 5  
2.4 Backfilling Procedures ................................................................................................... 6 
2.5 Soil/Sediment Disposal ................................................................................................. 6 
2.6 Quality Control Measures .............................................................................................. 6 
2.7 Investigative Results ..................................................................................................... 6
3.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS ............................................ 6 

DRAWINGS

Drawing 1 Topographic Site Map
Drawing 2 Site and Sample Location Map (Preliminary Sampling)
Drawing 3 Site Remediation Activities

TABLE

Table 1 Preliminary Soil Sampling Test Results
Table 2 Summary of Chemical Constituents Detected in Soil (Sediment Cleanup)
Table 3 Summary of Chemical Constituents Detected in Soil (Excavation Near SB-
1)

APPENDICES

Appendix A UST Forms
Appendix B Laboratory Analytical Reports and Chain-of-Custody Records
Appendix C Disposal Documentation
Appendix D Mid-Atlantic Soil Sampling Procedure
1.0 SITE HISTORY AND CHARACTERIZATION

1.1 Introduction

The Subject Property is the property located at 2500/2502 East Market Street in Greensboro,
North Carolina (Drawings 1 and 2). The Subject Property is developed with a four-story brick
and concrete warehouse constructed in 1947 with an areal extent of approximately 40,000 ft2
(main warehouse) with a concrete and steel addition constructed in the 1980’s with an areal
extent of approximately 43,000 ft2 (warehouse addition). The Subject Property is also developed
with an approximately 4,000 ft2 auxiliary building southwest of the main warehouse that formerly
operated as a truck maintenance shop known as 13’ 6” Truck Wash. Maintenance performed by
13’ 6” Truck Wash at the site was focused on large trucks dedicated to freight transportation and
included the use of a waste oil AST and automotive fluid storage. Automotive maintenance has
not taken place at the Subject Property since late 2022.

The April 15, 2022 Phase I Environmental Site Assessment (PESA) by Froehling and
Robertson, Inc. (F&R) identified multiple Recognized Environmental Conditions with respect to
the Subject Property. The RECs included multiple 55-gallon drums and 5-gallon buckets
containing waste oil and waste oil filters with visible spills and staining adjacent to these
containers. The report also notes staining adjacent to a 250-gallon used oil aboveground
storage tank (AST) kept near the auxiliary building.

The PESA recommended additional assessment in connection with staining near the former
truck shop, which was performed and documented in the June 7, 2022 Limited Soil and Soil
Gas Assessment Report (LSA; by F&R). The LSA documents the collection of four shallow soil
samples (SB-1 through SB-4) from underneath the paved area adjacent to the former truck shop
in areas where staining was visible. Of the four samples taken, one (SB-1) exhibited total
petroleum hydrocarbons (TPH) diesel range organics (DRO) above its TPH Action Level (100
milligrams per kilogram; mg/kg) at a reported concentration of 7,000 mg/kg. F&R also collected
a sediment sample from a catch basin located downgradient of the 250-gallon waste oil AST,
which exhibited a TPH DRO concentration above its action level at 492 mg/kg. TPH DRO was
reported in other soil samples (SB-2 through SB-4); however, the reported concentrations were
below the action level.

Based on the outcome of the LSA report, a UST-62 24-Hour Notification of Discharge Form was
submitted to the NC Department of Environmental Quality (NCDEQ) Winston-Salem regional
office (Appendix A). In response, NCDEQ opened AST Incident 96870. From December 2,
2022 to February 3, 2023, Mid-Atlantic performed additional soil assessment and directed cleanup
and excavation activities at the Subject Property to address reported petroleum impacts to soil at
the Subject Property. This report documents the assessment and cleanup activities.

The opinions included herein are based on our experience and the information obtained during the
study. This report is based on limited observations made on the dates noted using the procedures
described herein. If additional information becomes available, we request the opportunity to review
the information, reassess the potential environmental concerns and modify our conclusions and
recommendations, if appropriate.

Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 2
Greensboro, North Carolina

1.2 Owner/Operator of the AST

13’ 6” Truck Wash
2502 East Market Street
Greensboro, North Carolina, 27401

1.3 Property Owner

VG Greensboro Storage LLC
2601 Bayshore Drive, 17th Floor
Miami, Florida, 33133

1.4 Facility Information

2500 East Market Street
Greensboro, North Carolina 27401
Facility ID No: N/A

1.5 Contacts

Primary Contact: Mr. Ben Ho
HHC Storage, L.L.C.
114 East Jones Street
Fuquay-Varina, North Carolina 27526
[phone]

Contractors: Terra Nova Solutions, Inc. (TN)
303 South Maultsby Street
Whiteville, North Carolina 28472
[phone]

A&D Environmental Services (A&D)
2718 Uwharrie Road
Archdale, North Carolina 27263
[phone]

Consultant: Mid-Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610
Kevin Clay, PG
[phone]

Laboratory: Rapid Environmental Diagnostics (RED) Lab
5598 Marvin K. Moss Lane
MARBIONC Building, Suite 2003
Wilmington, North Carolina 28409
[phone]
Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 3
Greensboro, North Carolina

Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
[phone]

1.6 AST Information and Release Source

One 250-gallon AST formerly containing used motor oil was situated on the property beside the
truck maintenance shop. Multiple drums, buckets, and pails were kept beside the AST and
underneath a coal trestle beside the main warehouse structure. The last use date of the tank is
not known. Refer to Drawing 2 for the location of the tank and coal trestle.

1.7 Site Characteristics

The site consists of a 7.28-acre parcel located in Greensboro, North Carolina that is zoned Heavy
Industrial (HI) as reported by the Greensboro NC Planning Department. The property is developed
with two warehouse facilities and a former truck maintenance shop as described in Section 1.1.

The property is owned by VG Greensboro Storage LLC. Based on historical aerial imagery, the first
known developed use of the property was for agriculture until 1946, when the main warehouse was
constructed. The historical use of the main warehouse include a tobacco leaf plant and a general
warehouse. The former truck maintenance shop (auxiliary building) appears to have been built
concurrently with the main warehouse and historically used as a boiler room and for truck
maintenance. Currently, both of these buildings are vacant.

The warehouse addition was constructed in the 1980s and has been used as a warehouse since
its construction. The warehouse addition is occupied by Duffy Boxing and Recycling, Inc. who uses
the space to store and process cardboard, plastic, and metallic items.

Surrounding properties are used for commercial and industrial purposes. The closest property
boundary from the source area is approximately 150-200 feet to the south. The property is
provided municipal water and sewer services.

2.0 INITIAL RESPONSE AND ABATEMENT ACTION

2.1 Preliminary Soil and Sediment Assessment

F&R’s LSA Report identified petroleum impacts to soil at one of four locations sampled. This
sample, SB-1, was collected near a group of drums located under the former coal trestle located
adjacent to the main warehouse and south of the former truck shop.

Prior to remedial activities, Mid-Atlantic performed preliminary sampling to delineate the extent
of petroleum impacts to soil near the drums and surrounding SB-1 on December 2, 2022. A
search of the area did not reveal evidence (hole or concrete patch) of the sample location.
However, data provided in the LSA Report was utilized to place Mid-Atlantic’s boring locations.
Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 4
Greensboro, North Carolina

Using a hammer drill and 1.5-inch masonry bit, Mid-Atlantic penetrated the approximately 1-foot-
thick concrete slab surrounding sample location SB-1 and collected soil samples using a
decontaminated soil recovery probe at 11 locations (SB-101 through SB-111, noted as 1 through
11 on Drawing 2), at depths ranging from 1.5 ft to 2 ft below land surface. Sample locations were
chosen to assess the soils in an area surrounding SB-1. Stained sediment on the land surface was
visible adjacent to the 55-gallon drums under the trestle, and Mid-Atlantic also collected a sediment
sample (SED-101) adjacent to the 55-gallon drums. The 11 soil samples and sediment sample
were submitted to Rapid Environmental Diagnostics Laboratories, LLC (RED Lab) for analysis of
TPH DRO and gasoline range organics (GRO) by ultraviolet fluorescence (UVF).

During sampling activities, Mid-Atlantic personnel also investigated the stormwater catch basin
sampled by F&R as documented in their LSA report. Using a push probe and shovel, Mid-Atlantic
uncovered the bottom of the catch basin and found that the basin is lined with concrete and
constructed as a sealed vault. Therefore, it appears that contaminated sediment was contained
within the vault.

As summarized on Table 1, TPH DRO and GRO were either not detected in the soil samples or
were reported at concentrations below their respective action levels. The sediment sample
collected adjacent to the drums under the trestle exhibited DRO at a concentration (203.2 mg/Kg),
above its TPH Action Level. Laboratory analytical results are provided in Appendix B.

Based on the outcome of soil and sediment sampling surrounding SB-1 and the 55-gallon drums
under the trestle, Mid-Atlantic recommended that the scope of remediation be expanded to include
the disposal of sediment underneath the trestle. The outcome of soil sampling surrounding SB-1
and the 55-gallon drums also indicated that the area of soil contamination in the subsurface
appeared to be limited in areal extent around SB-1.

2.2 Site Cleanup and Sediment Removal

On January 4, 2023, Terra Nova Solutions (Terra Nova), under Mid-Atlantic’s supervision, began
on-site remedial activities. Terra Nova removed and disposed of partially full drums and buckets,
as well as the contents of the aforementioned waste oil AST at the site. The drums and buckets
contained paint, roofing primer, and motor oil. Liquids encountered in buckets found at the site
were disposed into a 55-gallon drum for offsite disposal. Using a vacuum truck, Terra Nova
vacuumed out approximately 20 gallons of oil from the AST and an additional 25 gallons of oil from
a waste oil drum under the coal trestle. Three 55-gallon drums containing used oil filters were also
disposed.

Terra Nova removed the steel grate from the top of the stormwater catchment basin and removed
the sediment within the basin. The sediment was stockpiled on and covered by 6-mil plastic
sheeting pending future disposal. See Section 2.4 (below) for information regarding sediment/soil
disposal.

Terra Nova also hand-excavated and stockpiled an estimated 15 to 18 tons of sediment from
underneath the coal trestle. The soil was placed in the same stockpile as the sediment removed
from the stormwater catchment basin and was covered by plastic sheeting pending future disposal.
Additional sediment exhibiting apparent petroleum impacts (e.g., staining and/or odors) excavated
Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 5
Greensboro, North Carolina

under the trestle were segregated and containerized into eleven 55-gallon drums separate from
stockpiled sediment. An approximately 430 square-foot area (the two western-most of the seven
“bays” of the coal trestle) was not accessible during excavation due to heavy vegetative
overgrowth; however, potential sources (drums, buckets, etc.) and evidence of a release(s) of
petroleum product were not observed in this area.

A total of 15 drums of petroleum impacted sediment, used oil filters, and waste liquids were
disposed offsite. The drums were disposed offsite at the Terra Nova (formerly Zebra Environmental
& Industrial Services, Inc.) facility in High Point, NC. Copies of waste manifests generated for
offsite disposal are included in Appendix C.

To determine the appropriate disposal facility, composite samples of the stockpiled and drummed
soils were collected and submitted to Waypoint Analytical LLC (Waypoint) in Charlotte, North
Carolina. The samples collected were composites packed into pre-labeled laboratory-supplied
glassware, placed into an ice-filled cooler, and delivered under chain-of-custody. Soil samples
were submitted for laboratory analysis of TPH DRO and GRO, volatile organic compounds
(VOCs) by EPA 8260, Semi-VOCs (SVOCs) by EPA 8270, total metals by 6020B, pesticides by
EPA 8081, and polychlorinated biphenyls (PCBs) by EPA 8082. Sample results are summarized
on Table 2 and discussed under Section 2.6.

2.3 Soil Excavation

During site activities performed in support of the property’s status as a Brownfields site, SB-1
was identified adjacent to the coal trestle in an area surrounded by soil borings advanced by
Mid-Atlantic as part of site activities discussed in Section 2.1. During cleanup activities on
January 4, 2023, Mid-Atlantic personnel again searched for the location of SB-1 but it could not be
identified due to heavy precipitation and runoff. However, F&R was contacted regarding the
location of the boring and provided information showing that boring SB-1 was located directly in the
area where Mid-Atlantic personnel collected samples on December 2, 2022. The estimated
location of the F&R soil sample location is shown on Drawing 2.

On February 2 and 3, 2023, A&D Environmental Services (A&D), under Mid-Atlantic’s
supervision, removed a section of the concrete slab surrounding SB-1 and performed a
remedial excavation of soil. A&D created a 5ft x 5ft opening in the concrete slab and excavated
3 ft below land surface. Soils encountered beneath the slab did not exhibit signs of petroleum
contamination including staining and/or odors. Field screening did not indicate elevated
readings on the toxic vapor analyzer (TVA) used by Mid-Atlantic personnel on soil samples
taken from the sidewalls and bottom of the excavation. During excavation, the local water table
was not encountered. Soils encountered during excavation consisted of sandy/clayey silt.

Mid-Atlantic collected a sample from the bottom of the excavation (HA-1) and a stockpile
composite for analysis of TPH DRO and GRO, VOCs, SVOCs, total metals, chromium and lead,
and PCBs to evaluate possible impacts to soil and to determine an appropriate disposal facility
destination. The results are summarized on Table 3 and discussed in Section 2.6.

Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 6
Greensboro, North Carolina

2.4 Backfilling Procedures

After over-excavation activities and collection of confirmation samples, the excavation pit was
backfilled with imported #57 stone and ten inches of aggregate base course to land surface.

2.5 Soil/Sediment Disposal

Excluding the sediment contained in drums and disposed offsite as discussed under Section 2.2, a
total of approximately 19.87 tons of soil and sediment were stockpiled and disposed offsite at the
permitted AES of NC facility in Thomasville, NC. A copy of the transportation manifest is provided
in Appendix C.
2.6 Quality Control Measures

Sample HA-1 and sidewall samples for field screening were retrieved using a decontaminated
hand auger. Samples were collected as discussed in the Mid-Atlantic field procedures included in
Appendix D. New nitrile gloves were worn during the collection and handling of the soils. The
samples collected were placed into pre-labeled, laboratory-supplied glassware, and transported
under chain of custody control by a courier affiliated with Waypoint Analytical to their laboratory in
Charlotte, NC for analysis.

2.7 Investigative Results

As summarized on Table 1, the laboratory results indicate that vadose-zone soils exceeding the
NCDEQ Action Levels for TPH were limited in areal extent and depth to the immediate vicinity of
historical sample location SB-1. As summarized on Tables 2 and 3, the sample collected from
the bottom of the excavation do not exhibit petroleum impacts to soil above applicable Maximum
Soil Contaminant Concentrations (MSCCs). Additionally, stockpiled soil did not exhibit evidence
of petroleum contamination. These results suggest that the release identified as part of F&R’s
LSA has been remediated to concentrations that permit closure of AST Incident 96870.

The laboratory analytical reports and chain-of-custody records for sampling performed as part of
assessment and site cleanup activities are provided in Appendix B.

3.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS

 As documented in F&R’s LSA report, one of four soil boring samples (SB-1) and a
sediment sample collected in a catch basin exhibited petroleum impacts to soil above
NCDEQ’s TPH Action Level for DRO.

 Preliminary assessment activities by Mid-Atlantic included the collection of eleven soil
samples surrounding sample SB-1 and investigation of the catch basin. Mid-Atlantic found
that petroleum impacts to soil were limited in areal extent to the immediate vicinity of SB-1,
and that the catch basin is concrete-lined.

Initial Abatement Action Report May 3, 2023
2500 East Market Street Page 7
Greensboro, North Carolina

 Initial cleanup activities performed in January 2023 included emptying the contents of the
onsite waste oil AST, removing partially full buckets and drums containing waste liquid, and
removing petroleum-impacted sediment from underneath the coal trestle.

 Follow-up remediation was performed in February 2023 by excavation of soils beneath the
pavement in the immediate vicinity of historical sample location SB-1. Field screening and
laboratory testing did not find evidence of petroleum impacts to soil above applicable
MSCCs.

 Waste liquids, drummed and stockpiled sediment/soil, and drummed oil filters collected
from onsite remedial activities were disposed offsite at permitted facilities. Cleanup
generated a total of fifteen 55-gallon drums and 19.87 tons of stockpiled sediment/soil for
offsite disposal.

 Based on field observations and laboratory analytical results from Mid-Atlantic’s preliminary
sampling and oversight of remedial activities performed at the site, the petroleum release
related to AST Incident 96870 has been remediated to levels below existing MSCCs.
Petroleum-impacted sediment has been hand dug and disposed offsite and subsurface
petroleum-impacted soil in the vicinity of SB-1 has been excavated and disposed offsite.
Additionally, the impacted sediment within the catch basin near the waste oil AST has also
been remediated and the basin is a concrete box, thus containing petroleum releases that
migrated towards the basin. In addition, the sources of contamination have been removed
from the site and the waste oil AST is no longer used by the ownership.

 As such, closure of AST Incident 96870 appears to be warranted without land use
restrictions or engineering/institutional controls.

 Mid-Atlantic recommends that a copy of this report is sent to the NCDEQ Winston-Salem
Regional Office, DWM, UST Section for their review.
DRAWINGS
´
TOPOGRAPHIC SITE MAP2500 EAST MARKET STREET GREENSBORO, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO:
REFERENCES:
SCALE:
OCTOBER 2022
R4229.00
3G-R4229.00-11
1. GREENSBORO AND MCLEANSVILLE, NC DIGITAL RASTER GRAPHICS, USGS. SCANNED FROM 1:24,000-SCALE WAKE, NC TOPOGRAPHIC MAPS, PUBLISHED 2019, USGS.2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS, BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
CONTOUR INTERVAL = 10 FEET
0 600 1,200Feet1:12,000
KRC
§¨¦I40§¨¦U29§¨¦U220
§¨¦I85§¨¦GUILFORD
AREA SHOWN WITHIN
3
GUILFORD COUNTY
RSM
RSM
SUBJECTPROPERTY
Approximate Locationof Sample "SB-1"
123
45
10 11
9 6 7 8
Catch Basin
WasteOil AST
Location of Sediment Sample SED-101
Auxiliary Building
Main Warehouse
´
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
SITE AND SAMPLE LOCATION MAP (PRELIMINARY SAMPLING)2500 EAST MARKET STREETGREENSBORO, NORTH CAROLINA
REFERENCE: DATA FROM NC ONEMAP AND NCDOT.
DATE: MARCH 2023
JOB NO.: R4229.01
GIS NO.: 3G-R4229.01-2
FIGURE NO.: 2
KRC
0 50 100 150 20025Feet
1 inch = 25 feet
Legend
Soil Sample Location
Subject Property
RSM
RSM
Catch Basin
WasteOil AST
Auxiliary Building
Main Warehouse
´
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
SITE REMEDIATION ACTIVITIES2500 EAST MARKET STREETGREENSBORO, NORTH CAROLINA
REFERENCE: DATA FROM NC ONEMAP AND NCDOT. MID-ATLANTIC FIELD NOTES
DATE: MARCH 2023
JOB NO.: R4229.01
GIS NO.: 3G-R4229.01-3
FIGURE NO.: 3
KRC
0 50 100 150 20025Feet
1 inch = 25 feet
Legend
Extent of Sediment Removal
Approximate Extent of Excavation
Extent of Sediment Left in Place
Subject Property
RSM
RSM
HA-1 Approximate Locationof Sample "SB-1"
TABLES
TPH GRO UVF<0.58 <0.44 <0.44 <0.41 <0.41 <0.46 <0.43 <0.43 <0.40 <0.45 0.58 <6.650TPH DRO UVF<0.58 <0.44 0.44 <0.41 0.41 <0.46 0.43 31.9 0.40 0.45 <0.22203.2100All samples collected December 2, 2022mg/Kg - Milligrams per KilogramUVF - Ultraviolet FluorescenceBold text indicates exceedance of NCDEQ TPH Action LevelSB-107 SB-108 SB-109 SB-110 SB-111TABLE 1 PRELIMINARY SOIL SAMPLING TEST RESULTS2500 EAST MARKET STREETGREENSBORO, NORTH CAROLINACHEMICAL CONSTITUENTSB-101 SB-102 SB-103Action LevelANALYSIS METHODMID-ATLANTIC JOB NO. R4229.01CONCENTRATION (mg/kg or PPM)SB-104 SB-105SED-101SB-106
Soil‐to‐Water MSCC 
(mg/kg)
Residential Soil Cleanup 
Level (mg/kg)
Industrial/Commercial Soil 
Cleanup Level             
(mg/kg)
Arsenic 3.68 6.43 NE NE NE
Barium 119 119 620 3100 46000
Cadmium 0.856 0.968 NE NE NE
Chromium (Total)* 20.3 25.8 360000 23400 350000
Lead 34.7 40.0 270 400 400
Mercury <0.00931 0.0355 J NE NE NE
Silver 0.251 J <0.223 4.8 78.2 1160
Gasoline Range Organics <4.97 <2.88
Diesel Range Organics 575 326
4,4'‐DDT <0.00211 0.0117M NE NE NE
Endrin <0.00267 0.00446 J NE NE NE
Acetone 0.075 0.062 24 14000 210000
Acrolein 0.022 J 0.006 J NE NE NE
Methyl Ethyl Ketone 0.011 J 0.007 J 16 9380 140000
1,2,3‐Trichlorobenzene 0.001 J <0.0008 2.1 22.8 112
Acenaphthene 0.219 J <0.194 8.3 930 14000
Acenaphthylene 0.165 J <0.175 20 930 14000
Anthracene 0.844 J 0.449 J 640 4600 70000
Benzo(a)anthracene 2.22 0.889 J 0.17 6.6 32
Benzo(a)pyrene 1.71 0.565 J 0.058 66 327
Benzo(b)fluoranthene 2.99 1.75 0.6 6.6 32
Benzo(g,h,i)perylene 1.11 0.491 J 7600 469 7000
Benzo(k)fluoranthene 1.01 0.484 J 5.8 66 327
Chrysene 2.44 1.70 18 663 3270
Dibenzofuran 0.241 J <0.199 5.2 15.6 233
Fluoranthene 4.67 3.13 330 625 9340
Fluorene 0.254 J <0.214 55 625 9340
Ideno(1,2,3‐cd)pyrene 1.27 0.566 J 1.9 6.63 32.7
2‐Methylnaphthalene 0.181 J <0.167 1.5 62.5 934
Naphthalene 0.529 J 0.299 J 0.2 5.5 27
Phenanthrene 2.31 0.913 J 64 469 7000
Pyrene 4.64 2.97 210 469 7000
NOTES:
1. NA =  Not Applicable
2. NE = Not Established
3. All values reported in milligrams per kilogram (mg/kg)
4. VOCs = Volatile Organic Compounds.
5. SVOCs = Semi‐Volatile Organic Compounds.
7. Underlined values exceed the Soil‐to‐Water MSCC
8. * = Chromium was compared to the Cr III PSRG based on known historical uses of the site.
TABLE 2
SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN SOIL (SEDIMENT CLEANUP)
2500 EAST MARKET STREET
GREENSBORO, NORTH CAROLINA
MID‐ATLANTIC JOB NO. R4229.01
NA
6. J = Concentration was detected between the method detection 
DRUM 
COMPOSITE
1/4/2023
STOCKPILE
1/4/2023
Total Petroleum Hydrocarbons by 8015
Pesticides by 8081B
NA
RCRA Metals by Method 6020B/7471A
VOCs by Method 8260D
SVOCs by Method 8270E
PCBs by 8082A
Not Detected
ANALYTE
MAXIMUM SOIL CONTAMINANT CONCENTRATIONS 
(MSCCs)
NA
Soil‐to‐Water MSCC 
(mg/kg)
Residential Soil Cleanup 
Level (mg/kg)
Industrial/Commercial Soil 
Cleanup Level             
(mg/kg)
Chromium (Total)* 27.2 75.6 360000 23400 350000
Lead 0.904 1.24 270 400 400
Acetone 0.007 J 0.006 J 24 14000 210000
NOTES:
1. NA =  Not Applicable
2. NE = Not Established
3. All values reported in milligrams per kilogram (mg/kg)
4. VOCs = Volatile Organic Compounds.
5. SVOCs = Semi‐Volatile Organic Compounds.
7. * = Chromium was compared to the Cr III MSCCs based on known historical uses of the site.
ANALYTE HA‐1
2/3/2023
STOCKPILE
2/3/2023
MAXIMUM SOIL CONTAMINANT CONCENTRATIONS 
(MSCCs)
TABLE 3
SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN SOIL (EXCAVATION NEAR SB‐1)
2500 EAST MARKET STREET
GREENSBORO, NORTH CAROLINA
MID‐ATLANTIC JOB NO. R4229.01
RCRA Metals by Method 6020B/7471A
Total Petroleum Hydrocarbons by 8015
NA
Pesticides by 8081B
PCBs by 8082A
Not Detected
6. J = Concentration was detected between the method detection 
Not Detected NA
Not Detected NA
Not Detected NA
VOCs by Method 8260D
SVOCs by Method 8270E
APPENDIX A

UST FORMS
UST-62 24-Hour Notification of Discharge Form
For Non-UST
Releases of
Petroleum in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release of
petroleum from a source other than an underground storage tank. This form is required to be submitted within 24 hours of
discovery of a known or suspected petroleum release
(DWM USE ONLY)
Incident # ___________ Priority Rank (H,I,L,U) _____
Received (time/date) ___________________________
Received by ________________ Region __________
Reported by (circle one): Phone, Fax or Report
Suspected Contamination? (Y/N) ___
Confirmed GW Contamination? (Y/N) ___
Confirmed Soil Contamination ?(Y/N) ___
Samples taken?(Y/N) ___ Free product? (Y/N) ___
If Yes(free product), state greatest thickness: _____feet
Release discovered
(time/date):______________
_______________________
INCIDENT DESCRIPTION
Code:Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) :Obtained by:
Describe suspected or confirmed release (nature of release, time/date of release, quantity of release, amount of free
product):T GPS
soil removed, confirmation sampling):
T Other
T Unknown
Describe impacted receptors: Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
T Observation of Release at Occurrence
T Visual or Olfactory Evidence
T Soil Contamination
T Groundwater Contamination
T Water Supply Well Contamination
T Surface Water Contamination
T Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release
(Check one to indicate primary
source)
Cause of Release
(Check one to indicate primary
cause)
Type of Release
(Check one)
Product Type Released
(Check one to indicate primary petroleum product
type released)
T AST (tank)
T AST Piping/ Dispenser
T AST Delivery Problem
T OTR Vehicle Tank
T OTR Bulk Transport Tank
T RR Bulk Transport Tank
T Transformer
T Unknown
T Other ______________
Definitions presented on reverse
T Spill (Accidental)
T Spill (Intentional)
T Corrosion
T Physical or Mechanical
Damage
T Equipment Failure
T AST Overfill
T AST Installation Problem
T Unknown
T Other ______________
Definitions presented on reverse
T Petroleum
T Both Petroleum
& Non-Petroleum
Location
(Check one)
T Facility
T Residence
T Highway/Road
T Railway
T Other
T Gasoline/ Diesel/
Kerosene
T E11 – E20
T E21 – E84
T E85 – E99
T Ethanol 100%
T Diesel/Veg. Oil
Blend
T Vegetable Oil 100%
T Heating Oil
T Waste Oil
T Mineral Oil-no
PCBs
T Mineral Oil-PCBs
T Other Petroleum
Products ________
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
Guidance presented on reverse
UST Form 62 (04/10) Page 1 of 2
Incident Name:
Address (street number/name):2500 E. Market Street County:
T Electronic topographic map
T GIS Address matching
Describe initial response/abatement (time/date release stopped, cleanup begun/completed, quantity of product
City/Town:Zip Greensboro 27401
2500 E. Market Street Site
Guilford
No initial response required- see attached assesment report
A Phase I ESA and soil assesment conducted as part of a potential property transaction
identified petroleum impacts to soil from an AST & automotive maintenance operations.
None
36.076584 -79.754008
06-07-2022
x Google Earth
X
XX
X vehicle maintenance
X
X
X
X
Y
Y
N
NY
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected ______
List of Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
PARTY RESPONSIBLE FOR RELEASE
(if the source of the release is not an AST system or if it is an AST system and there is a responsible party other than the AST system owner/ operator)
Name of Person/Company Address
City State Zip Code Telephone Number
AST SYSTEM OWNER (if the source of the release is an AST system)
AST Owner/Company Address
City State Zip Code Telephone Number
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF INCIDENT
Draw Sketch of Area or Provide Map (showing incident site, location of release, two major road intersections, potential
receptors)
Attach sketch or map to form.
Give Directions to Incident Site Attach directions to form if necessary.
AST SYSTEM OPERATOR (if the source of the release is an AST system)
AST Operator/Company Address
Landowner Address
City State Zip Code
UST Form 62 (04/10) Page 2 of 2
Definitions of Sources
AST (Tank): means the tank is used to store product
AST Piping: means the piping and connectors running from the tank to the dispenser or other end-use equipment
AST Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping
AST Delivery Problem: identifies releases that occurred during product delivery to the tank.
OTR Vehicle Tank: means the tank is used to store product to fuel an over the road vehicle
OTR Bulk Transport Tank: means a tank that is used to transport product in bulk over the road (by truck)
RR :bulk Transport Tank: means a tank that is used to transport product in bulk by train
Transformer: means electrical transformer
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories
Unknown: identifies releases for which the source has not been determined
Definitions of CausesSpill (Accidental): use this cause when a spill occurs accidentally(e.g., when the delivery hose is disconnected from a fill pipe)
Spill (Intentional): use this cause when a spill occurs intentionally (e.g., intentional dumping or breakage)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion
Equipment failure: use when a release occurs due to equipment failure other than corrosion or physical or mechanical damage
AST Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
AST Installation Problem: use when the problem is determined to have occurred specifically because the AST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories
Unknown: use when the cause has not been determined
Guidance: Ownership and Operator TypeOwnership select the category which describes owner of the AST system, bulk transport tank, or other release source
Operator Type select the category which describes the operation in which owner uses the AST system, bulk transport tank, or other release source
Person Reporting Incident Company
Title Address Date
VG Greensboro Storage LLC 2601 South Bayshore Dr, 17th Floor
FLMiami
N/A
Located on E. Market Street near intersection with Holts Chapel Road. See attached assement report for maps
13'6" Truck Wash
2502 E. Market Street
NCGreensboro 27401
13'6" Truck Wash
Greensboro NC 27401
2502 E. Market Street
11/22/2022
33133
Benjamin Ho HHC Storage, L.L.C.
114 E Jones St. Fuquay-Varina, NC 27526
Telephone Number
Manager / Developer
919-649-2662

APPENDIX B

LABORATORY ANALYTICAL REPORTS
AND CHAIN-OF-CUSTODY RECORDS
Hydrocarbon Analysis Results
Client:MID-ATLANTIC ASSOCIATES Samples taken Friday, December 2, 2022
Address:RALEIGH, NC Samples extracted Friday, December 2, 2022
Samples analysed Tuesday, December 6, 2022
Contact:KEVIN CLAY Operator TORI KELLY
Project:MAA
34 U04049
Matrix Sample ID Dilution used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s SB-101 23.0 <0.58 <0.58 <0.58 <0.58 <0.12 <0.18 <0.023 0 0 0 PHC not detected
s SB-102 17.4 <0.44 <0.44 <0.44 <0.44 <0.09 <0.14 <0.017 0 100 0 Residual HC
s SB-103 17.6 <0.44 <0.44 0.44 0.44 <0.09 <0.14 <0.018 0 68.8 31.2 Deg Fuel 90.3%,(FCM)
s SB-104 16.5 <0.41 <0.41 <0.41 <0.41 <0.08 <0.13 <0.016 0 0 100 Residual HC
s SB-105 16.4 <0.41 <0.41 0.41 0.41 <0.08 <0.13 <0.016 82.3 13.6 4.1 Deg Fuel 75.1%,(FCM)
s SB-106 18.4 <0.46 <0.46 <0.46 <0.46 <0.09 <0.15 <0.018 0 100 0 PHC not detected
s SB-107 17.1 <0.43 <0.43 0.43 0.43 <0.09 <0.14 <0.017 0 42.2 57.8 Deg Fuel 74.6%,(FCM)
s SB-108 17.3 <0.43 <0.43 31.9 31.9 20.4 2.5 0.38 0 60.6 39.4 Pyrogenic HC 75.5%,(FCM)
s SB-109 16.0 <0.4 <0.4 0.4 0.4 0.22 <0.13 <0.016 0 56.3 43.7 Pyrogenic HC 89.5%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 95 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:MID-ATLANTIC ASSOCIATES Samples taken Friday, December 2, 2022
Address:RALEIGH, NC Samples extracted Friday, December 2, 2022
Samples analysed Tuesday, December 6, 2022
Contact:KEVIN CLAY Operator TORI KELLY
Project:MAA
38 U04049
Matrix Sample ID Dilution used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s SB-110 18.1 <0.45 <0.45 0.45 0.45 0.28 <0.14 <0.018 0 48.3 51.7 Pyrogenic HC 75.5%,(FCM)
s SB-111 8.9 <0.22 0.58 <0.22 0.58 <0.04 <0.07 <0.009 94.6 2.8 2.6 Deg.PHC 85.2%,(FCM)
s SED-101 262.0 <6.6 <6.6 203.2 203.2 89.4 4.4 <0.26 0 76.5 23.5 V.Deg.PHC 74.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 102.9 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/20/2023
Mid-Atlantic Associates, Inc. - Raleigh Kevin Clay
409 Rogers View Court Raleigh, NC, 27610
Ref: Analytical Testing
Lab Report Number: 23-006-0013 Client Project Description: 2500 E.Market St.
Dear Kevin Clay:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/6/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 56
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-006-0013
Page 2 of 56
Report Number:
Sample Summary Table
Client Project Description:
23-006-0013
2500 E.Market St.
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
01/04/2023 14:30Solids 96875 Drum Composite 01/06/2023 11:30
01/04/2023 14:30Solids 96875 Drum Composite 01/06/2023 11:30 7471A WP MTN -
01/04/2023 14:30Solids 96875 Drum Composite 01/06/2023 11:30 6010D WP MTN -
01/04/2023 15:45Solids 96876 Stockpile 01/06/2023 11:30
01/04/2023 15:45Solids 96876 Stockpile 01/06/2023 11:30 7471A WP MTN -
01/04/2023 15:45Solids 96876 Stockpile 01/06/2023 11:30 6010D WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 56
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-006-0013
Report Limit
Project:2500 E.Market St.
V 96875Drum Composite
3.68 01/14/2023 01:396010DArsenicmg/Kg - dry 0.333
119 01/14/2023 01:396010DBariummg/Kg - dry 0.180
0.856 01/14/2023 01:396010DCadmiummg/Kg - dry 0.0277
20.3 01/14/2023 01:396010DChromiummg/Kg - dry 0.327
34.7 01/14/2023 01:396010DLeadmg/Kg - dry 0.250
J0.251 01/14/2023 01:396010DSilvermg/Kg - dry 0.222
575 01/18/2023 09:498015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 25.8
0.075 01/11/2023 11:098260DAcetonemg/Kg - dry 0.003
J0.022 01/11/2023 11:098260DAcroleinmg/Kg - dry 0.001
J0.011 01/11/2023 11:098260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
J0.001 01/11/2023 11:098260D1,2,3-Trichlorobenzene mg/Kg - dry 0.0008
J0.219 01/17/2023 04:468270EAcenaphthenemg/Kg - dry 0.161
J0.165 01/17/2023 04:468270EAcenaphthylenemg/Kg - dry 0.145
J0.844 01/17/2023 04:468270EAnthracenemg/Kg - dry 0.198
2.22 01/17/2023 04:468270EBenzo(a)anthracene mg/Kg - dry 0.193
1.71 01/17/2023 04:468270EBenzo(a)pyrene mg/Kg - dry 0.204
2.99 01/17/2023 04:468270EBenzo(b)fluoranthene mg/Kg - dry 0.202
1.11 01/17/2023 04:468270EBenzo(g,h,i)perylene mg/Kg - dry 0.188
1.01 01/17/2023 04:468270EBenzo(k)fluoranthene mg/Kg - dry 0.190
2.44 01/17/2023 04:468270EChrysenemg/Kg - dry 0.197
J0.241 01/17/2023 04:468270EDibenzofuranmg/Kg - dry 0.165
4.67 01/17/2023 04:468270EFluoranthenemg/Kg - dry 0.170
J0.254 01/17/2023 04:468270EFluorenemg/Kg - dry 0.177
1.27 01/17/2023 04:468270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.248
J0.181 01/17/2023 04:468270E2-Methylnaphthalene mg/Kg - dry 0.138
J0.529 01/17/2023 04:468270ENaphthalenemg/Kg - dry 0.200
2.31 01/17/2023 04:468270EPhenanthrenemg/Kg - dry 0.288
4.64 01/17/2023 04:468270EPyrenemg/Kg - dry 0.186
28.0 01/06/2023 17:00SW-DRYWT Moisture %
V 96876Stockpile
6.43 01/14/2023 01:556010DArsenicmg/Kg - dry 0.334
119 01/14/2023 01:556010DBariummg/Kg - dry 0.181
0.968 01/14/2023 01:556010DCadmiummg/Kg - dry 0.0278
25.8 01/14/2023 01:556010DChromiummg/Kg - dry 0.328
40.0 01/14/2023 01:556010DLeadmg/Kg - dry 0.250
J0.0355 01/17/2023 15:107471AMercury (Total)mg/Kg - dry 0.00952
Page 4 of 56
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-006-0013
Report Limit
Project:2500 E.Market St.
V 96876Stockpile
326 01/17/2023 17:068015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 15.6
M11.7 01/18/2023 21:028081B4,4'-DDT µg/Kg - dry 2.12
J4.46 01/18/2023 21:028081BEndrinµg/Kg - dry 2.67
0.062 01/11/2023 11:378260DAcetonemg/Kg - dry 0.003
J0.006 01/11/2023 11:378260DAcroleinmg/Kg - dry 0.001
J0.007 01/11/2023 11:378260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
J0.449 01/17/2023 05:088270EAnthracenemg/Kg - dry 0.239
J0.889 01/17/2023 05:088270EBenzo(a)anthracene mg/Kg - dry 0.232
J0.565 01/17/2023 05:088270EBenzo(a)pyrene mg/Kg - dry 0.246
1.75 01/17/2023 05:088270EBenzo(b)fluoranthene mg/Kg - dry 0.245
J0.491 01/17/2023 05:088270EBenzo(g,h,i)perylene mg/Kg - dry 0.228
J0.484 01/17/2023 05:088270EBenzo(k)fluoranthene mg/Kg - dry 0.229
1.70 01/17/2023 05:088270EChrysenemg/Kg - dry 0.238
3.13 01/17/2023 05:088270EFluoranthenemg/Kg - dry 0.206
J0.566 01/17/2023 05:088270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.299
J0.299 01/17/2023 05:088270ENaphthalenemg/Kg - dry 0.240
J0.913 01/17/2023 05:088270EPhenanthrenemg/Kg - dry 0.348
2.97 01/17/2023 05:088270EPyrenemg/Kg - dry 0.224
28.2 01/06/2023 17:00SW-DRYWT Moisture %
Page 5 of 56

Client: Mid-Atlantic Associates, Inc. - Raleigh CASE NARRATIVE
Project: 2500 E.Market St. Lab Report Number: 23-006-0013
Date: 1/20/2023
Metals Analysis Method 6010D Sample 97039 (Class A) Analyte: Barium
QC Batch No: L658650/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 92675 (UTHVDRUM10123)
Analyte: Mercury QC Batch No: L659074/L658823
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 96875 (Drum Composite)
Analyte: Diesel Range Organics (C10-C28) QC Batch No: V28965/V28949
Sample requires dilution due to high levels of target and/or non-target analytes. Sample 96876 (Stockpile) Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V28965/V28949 Sample requires dilution due to high levels of target and/or non-target analytes.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO Sample 96876 (Stockpile) Analyte: a,a,a-Trifluorotoluene QC Batch No: V28714/V28713 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Organochlorine Pesticides by GC Method 8081B Analyte: 4,4`-DDT QC Batch No: V29029/V28925 ECV result is below range due to sapmle matrix.
Analyte: Methoxychlor QC Batch No: V29029/V28925 ECV result is below range due to sample matrix. Polychlorinated Biphenyls (PCB's) Method 8082A Sample 96875 (Drum Composite)
Page 6 of 56

QC Batch No: V28867
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 96876 (Stockpile) QC Batch No: V28867
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Volatile Organic Compounds - GC/MS Method 8260D Analyte: Carbon Tetrachloride
QC Batch No: V28798/V28797 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 7 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.0 %Moisture 1 01/06/23 17:00 SW-DRYWTAMB
3.68 mg/Kg - dry 0.333 0.694Arsenic 1 01/14/23 01:39 6010DTJS
119 mg/Kg - dry 0.180 0.694Barium 1 01/14/23 01:39 6010DTJS
0.856 mg/Kg - dry 0.0277 0.139Cadmium 1 01/14/23 01:39 6010DTJS
20.3 mg/Kg - dry 0.327 0.347Chromium 1 01/14/23 01:39 6010DTJS
34.7 mg/Kg - dry 0.250 0.416
Lead 1 01/14/23 01:39 6010DTJS
<0.00931 mg/Kg - dry 0.00931 0.214Mercury (Total)1 01/17/23 15:08 7471AMRE
<0.444 mg/Kg - dry 0.444 0.694Selenium 1 01/14/23 01:39 6010DTJS
0.251 J mg/Kg - dry 0.222 0.347Silver 1 01/14/23 01:39 6010DTJS
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 8 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V28949 01/17/23 10:10
575 mg/Kg - dry 25.8 55.6Diesel Range Organics (C10-C28)4 01/18/23 09:49 V28965AMP
8015C DROSurrogate: OTP Surrogate 74.4 Limits: 31-123%01/18/23 09:494 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V28713 01/09/23 08:00
<4.97 mg/Kg - dry 4.97 12.0Gasoline Range Organics (C6-C10)50 01/09/23 10:41 V28714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 127 Limits: 50-137%01/09/23 10:4150 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V28925 01/16/23 11:55
<2.56 µg/Kg - dry 2.56 6.94
Aldrin 1 01/18/23 20:48 V29029JMV
<1.63 µg/Kg - dry 1.63 6.94alpha-BHC 1 01/18/23 20:48 V29029JMV
<2.76 µg/Kg - dry 2.76 6.94beta-BHC 1 01/18/23 20:48 V29029JMV
<1.74 µg/Kg - dry 1.74 6.94delta-BHC 1 01/18/23 20:48 V29029JMV
<24.4 µg/Kg - dry 24.4 69.4Chlordane 1 01/18/23 20:48 V29029JMV
<2.63 µg/Kg - dry 2.63 6.94alpha-Chlordane 1 01/18/23 20:48 V29029JMV
<2.35 µg/Kg - dry 2.35 6.94gamma-Chlordane 1 01/18/23 20:48 V29029JMV
<2.60 µg/Kg - dry 2.60 6.94
4,4'-DDD 1 01/18/23 20:48 V29029JMV
<2.85 µg/Kg - dry 2.85 6.944,4'-DDE 1 01/18/23 20:48 V29029JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 9 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V28925 01/16/23 11:55
<2.11 µg/Kg - dry 2.11 6.944,4'-DDT 1 01/18/23 20:48 V29029JMV
<2.90 µg/Kg - dry 2.90 6.94Dieldrin 1 01/18/23 20:48 V29029JMV
<2.49 µg/Kg - dry 2.49 6.94Endosulfan I 1 01/18/23 20:48 V29029JMV
<2.43 µg/Kg - dry 2.43 6.94Endosulfan II 1 01/18/23 20:48 V29029JMV
<2.53 µg/Kg - dry 2.53 6.94Endosulfan Sulfate 1 01/18/23 20:48 V29029JMV
<2.67 µg/Kg - dry 2.67 6.94Endrin 1 01/18/23 20:48 V29029JMV
<2.93 µg/Kg - dry 2.93 6.94Endrin Aldehyde 1 01/18/23 20:48 V29029JMV
<2.56 µg/Kg - dry 2.56 6.94Endrin Ketone 1 01/18/23 20:48 V29029JMV
<1.75 µg/Kg - dry 1.75 6.94
gamma-BHC 1 01/18/23 20:48 V29029JMV
<1.89 µg/Kg - dry 1.89 6.94Heptachlor 1 01/18/23 20:48 V29029JMV
<2.49 µg/Kg - dry 2.49 6.94Heptachlor Epoxide 1 01/18/23 20:48 V29029JMV
<3.67 µg/Kg - dry 3.67 6.94Methoxychlor 1 01/18/23 20:48 V29029JMV
<14.2 µg/Kg - dry 14.2 69.4Toxaphene 1 01/18/23 20:48 V29029JMV
Surrogate: Decachlorobiphenyl 127 Limits: 26-204%01/18/23 20:481 JMV V29029
Surrogate: Tetrachloro-m-xylene 48.0 Limits: 40-162%01/18/23 20:481 JMV V29029
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V28827 01/11/23 13:15
<0.247 mg/Kg - dry 0.247 0.694Aroclor 1016 10 01/12/23 17:37 V28867JMV
<0.556 mg/Kg - dry 0.556 1.39Aroclor 1221 10 01/12/23 17:37 V28867JMV
<0.181 mg/Kg - dry 0.181 1.39Aroclor 1232 10 01/12/23 17:37 V28867JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V28827 01/11/23 13:15
<0.185 mg/Kg - dry 0.185 0.694Aroclor 1242 10 01/12/23 17:37 V28867JMV
<0.139 mg/Kg - dry 0.139 0.694Aroclor 1248 10 01/12/23 17:37 V28867JMV
<0.172 mg/Kg - dry 0.172 0.694Aroclor 1254 10 01/12/23 17:37 V28867JMV
<0.207 mg/Kg - dry 0.207 0.694Aroclor 1260 10 01/12/23 17:37 V28867JMV
8082ASurrogate: Decachlorobiphenyl 60.1 Limits: 34-182%01/12/23 17:3710 JMV
8082ASurrogate: Tetrachloro-m-xylene 70.0 Limits: 36-182%01/12/23 17:3710 JMV
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
0.075 mg/Kg - dry 0.003 0.027Acetone 1 01/11/23 11:09 V28798TBL
0.022 J mg/Kg - dry 0.001 0.027Acrolein 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/11/23 11:09 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 01/11/23 11:09 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 11 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 01/11/23 11:09 V28798TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 01/11/23 11:09 V28798TBL
<0.0005 mg/Kg - dry 0.0005 0.006
4-Chlorotoluene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 01/11/23 11:09 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 01/11/23 11:09 V28798TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/11/23 11:09 V28798TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,4-Dichlorobenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/11/23 11:09 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013
Hexachlorobutadiene 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 01/11/23 11:09 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/11/23 11:09 V28798TBL
0.011 J mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 01/11/23 11:09 V28798TBL
<0.020 mg/Kg - dry 0.020 0.027
4-Methyl-2-Pentanone 1 01/11/23 11:09 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/11/23 11:09 V28798TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/11/23 11:09 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 01/11/23 11:09 V28798TBL
0.001 J mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 01/11/23 11:09 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 01/11/23 11:09 V28798TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/11/23 11:09 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2,3-Trichloropropane 1 01/11/23 11:09 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 01/11/23 11:09 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 01/11/23 11:09 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 01/11/23 11:09 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 01/11/23 11:09 V28798
Surrogate: 4-Bromofluorobenzene 112 Limits: 70-130%01/11/23 11:091 TBL V28798
Surrogate: Dibromofluoromethane 103 Limits: 84-123%01/11/23 11:091 TBL V28798
Surrogate: Toluene-d8 102 Limits: 76-129%01/11/23 11:091 TBL V28798
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
0.219 J mg/Kg - dry 0.161 0.916Acenaphthene 1 01/17/23 04:46 V28964JMV
0.165 J mg/Kg - dry 0.145 0.916Acenaphthylene 1 01/17/23 04:46 V28964JMV
<0.211 mg/Kg - dry 0.211 0.916Aniline 1 01/17/23 04:46 V28964JMV
0.844 J mg/Kg - dry 0.198 0.916Anthracene 1 01/17/23 04:46 V28964JMV
2.22 mg/Kg - dry 0.193 0.916Benzo(a)anthracene 1 01/17/23 04:46 V28964JMV
1.71 mg/Kg - dry 0.204 0.916Benzo(a)pyrene 1 01/17/23 04:46 V28964JMV
2.99 mg/Kg - dry 0.202 0.916Benzo(b)fluoranthene 1 01/17/23 04:46 V28964JMV
1.11 mg/Kg - dry 0.188 0.916Benzo(g,h,i)perylene 1 01/17/23 04:46 V28964JMV
1.01 mg/Kg - dry 0.190 0.916
Benzo(k)fluoranthene 1 01/17/23 04:46 V28964JMV
<0.805 mg/Kg - dry 0.805 2.78Benzoic Acid 1 01/17/23 04:46 V28964JMV
<0.145 mg/Kg - dry 0.145 0.916Benzyl alcohol 1 01/17/23 04:46 V28964JMV
<0.163 mg/Kg - dry 0.163 0.916Bis(2-Chloroethoxy)methane 1 01/17/23 04:46 V28964JMV
<0.148 mg/Kg - dry 0.148 0.916Bis(2-Chloroethyl)ether 1 01/17/23 04:46 V28964JMV
<0.188 mg/Kg - dry 0.188 0.458Bis(2-Chloroisopropyl)ether 1 01/17/23 04:46 V28964JMV
<0.166 mg/Kg - dry 0.166 0.916Bis(2-ethylhexyl)phthalate 1 01/17/23 04:46 V28964JMV
<0.151 mg/Kg - dry 0.151 0.916
4-Bromophenyl phenyl ether 1 01/17/23 04:46 V28964JMV
<0.156 mg/Kg - dry 0.156 0.458Butyl benzyl phthalate 1 01/17/23 04:46 V28964JMV
<0.128 mg/Kg - dry 0.128 0.9164-Chloro-3-methylphenol 1 01/17/23 04:46 V28964JMV
<0.155 mg/Kg - dry 0.155 0.4584-Chloroaniline 1 01/17/23 04:46 V28964JMV
<0.161 mg/Kg - dry 0.161 0.9162-Chloronaphthalene 1 01/17/23 04:46 V28964JMV
<0.136 mg/Kg - dry 0.136 0.9162-Chlorophenol 1 01/17/23 04:46 V28964JMV
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 01/17/23 04:46 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
2.44 mg/Kg - dry 0.197 0.916Chrysene 1 01/17/23 04:46 V28964JMV
<0.319 mg/Kg - dry 0.319 0.916Dibenz(a,h)anthracene 1 01/17/23 04:46 V28964JMV
0.241 J mg/Kg - dry 0.165 0.916Dibenzofuran 1 01/17/23 04:46 V28964JMV
<0.131 mg/Kg - dry 0.131 0.9161,2-Dichlorobenzene 1 01/17/23 04:46 V28964JMV
<0.135 mg/Kg - dry 0.135 0.9161,3-Dichlorobenzene 1 01/17/23 04:46 V28964JMV
<0.135 mg/Kg - dry 0.135 0.4581,4-Dichlorobenzene 1 01/17/23 04:46 V28964JMV
<0.204 mg/Kg - dry 0.204 0.9163,3'-Dichlorobenzidine 1 01/17/23 04:46 V28964JMV
<0.133 mg/Kg - dry 0.133 0.9162,4-Dichlorophenol 1 01/17/23 04:46 V28964JMV
<0.250 mg/Kg - dry 0.250 0.916
Diethyl phthalate 1 01/17/23 04:46 V28964JMV
<0.241 mg/Kg - dry 0.241 0.916Dimethyl phthalate 1 01/17/23 04:46 V28964JMV
<0.150 mg/Kg - dry 0.150 0.4582,4-Dimethylphenol 1 01/17/23 04:46 V28964JMV
<0.148 mg/Kg - dry 0.148 0.916Di-n-butyl phthalate 1 01/17/23 04:46 V28964JMV
<0.333 mg/Kg - dry 0.333 2.084,6-Dinitro-2-methylphenol 1 01/17/23 04:46 V28964JMV
<0.722 mg/Kg - dry 0.722 2.082,4-Dinitrophenol 1 01/17/23 04:46 V28964JMV
<0.134 mg/Kg - dry 0.134 0.9162,4-Dinitrotoluene 1 01/17/23 04:46 V28964JMV
<0.150 mg/Kg - dry 0.150 0.916
2,6-Dinitrotoluene 1 01/17/23 04:46 V28964JMV
<0.198 mg/Kg - dry 0.198 0.458Di-n-Octyl Phthalate 1 01/17/23 04:46 V28964JMV
4.67 mg/Kg - dry 0.170 0.916Fluoranthene 1 01/17/23 04:46 V28964JMV
0.254 J mg/Kg - dry 0.177 0.916Fluorene 1 01/17/23 04:46 V28964JMV
<0.147 mg/Kg - dry 0.147 0.916Hexachlorobenzene 1 01/17/23 04:46 V28964JMV
<0.135 mg/Kg - dry 0.135 0.916Hexachlorobutadiene 1 01/17/23 04:46 V28964JMV
<0.218 mg/Kg - dry 0.218 0.916Hexachlorocyclopentadiene 1 01/17/23 04:46 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
<0.110 mg/Kg - dry 0.110 0.916Hexachloroethane 1 01/17/23 04:46 V28964JMV
1.27 mg/Kg - dry 0.248 0.916Indeno(1,2,3-cd)pyrene 1 01/17/23 04:46 V28964JMV
<0.265 mg/Kg - dry 0.265 0.916Isophorone 1 01/17/23 04:46 V28964JMV
<0.147 mg/Kg - dry 0.147 0.9161-Methylnaphthalene 1 01/17/23 04:46 V28964JMV
0.181 J mg/Kg - dry 0.138 0.9162-Methylnaphthalene 1 01/17/23 04:46 V28964JMV
<0.134 mg/Kg - dry 0.134 0.9162-Methylphenol 1 01/17/23 04:46 V28964JMV
<0.117 mg/Kg - dry 0.117 0.9163&4 Methylphenol 1 01/17/23 04:46 V28964JMV
0.529 J mg/Kg - dry 0.200 0.916Naphthalene 1 01/17/23 04:46 V28964JMV
<0.134 mg/Kg - dry 0.134 0.916
2-Nitroaniline 1 01/17/23 04:46 V28964JMV
<0.166 mg/Kg - dry 0.166 0.9163-Nitroaniline 1 01/17/23 04:46 V28964JMV
<0.129 mg/Kg - dry 0.129 0.4584-Nitroaniline 1 01/17/23 04:46 V28964JMV
<0.161 mg/Kg - dry 0.161 0.458Nitrobenzene 1 01/17/23 04:46 V28964JMV
<0.123 mg/Kg - dry 0.123 0.9162-Nitrophenol 1 01/17/23 04:46 V28964JMV
<0.162 mg/Kg - dry 0.162 0.9164-Nitrophenol 1 01/17/23 04:46 V28964JMV
<0.365 mg/Kg - dry 0.365 0.916N-Nitrosodimethylamine 1 01/17/23 04:46 V28964JMV
<0.251 mg/Kg - dry 0.251 0.916
N-Nitrosodiphenylamine 1 01/17/23 04:46 V28964JMV
<0.163 mg/Kg - dry 0.163 0.916N-Nitroso-di-n-propylamine 1 01/17/23 04:46 V28964JMV
<0.481 mg/Kg - dry 0.481 1.39Pentachlorophenol 1 01/17/23 04:46 V28964JMV
2.31 mg/Kg - dry 0.288 0.916Phenanthrene 1 01/17/23 04:46 V28964JMV
<0.155 mg/Kg - dry 0.155 0.916Phenol 1 01/17/23 04:46 V28964JMV
4.64 mg/Kg - dry 0.186 0.916Pyrene 1 01/17/23 04:46 V28964JMV
<0.110 mg/Kg - dry 0.110 0.458Pyridine 1 01/17/23 04:46 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Drum Composite
96875 Matrix:
1/4/2023 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
<0.148 mg/Kg - dry 0.148 0.9161,2,4-Trichlorobenzene 1 01/17/23 04:46 V28964JMV
<0.133 mg/Kg - dry 0.133 0.9162,4,5-Trichlorophenol 1 01/17/23 04:46 V28964JMV
<0.134 mg/Kg - dry 0.134 0.9162,4,6-Trichlorophenol 1 01/17/23 04:46 V28964JMV
8270ESurrogate: Phenol-d5 74.5 Limits: 34-121%01/17/23 04:461 JMV
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%01/17/23 04:461 JMV V28964
Surrogate: 2-Fluorophenol 79.0 Limits: 35-115%01/17/23 04:461 JMV V28964
Surrogate: Nitrobenzene-d5 85.0 Limits: 37-122%01/17/23 04:461 JMV V28964
Surrogate: 4-Terphenyl-d14 97.0 Limits: 54-127%01/17/23 04:461 JMV V28964
Surrogate: 2,4,6-Tribromophenol 82.9 Limits: 39-132%01/17/23 04:461 JMV V28964
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.2 %Moisture 1 01/06/23 17:00 SW-DRYWTAMB
6.43 mg/Kg - dry 0.334 0.696Arsenic 1 01/14/23 01:55 6010DTJS
119 mg/Kg - dry 0.181 0.696Barium 1 01/14/23 01:55 6010DTJS
0.968 mg/Kg - dry 0.0278 0.139Cadmium 1 01/14/23 01:55 6010DTJS
25.8 mg/Kg - dry 0.328 0.348Chromium 1 01/14/23 01:55 6010DTJS
40.0 mg/Kg - dry 0.250 0.417
Lead 1 01/14/23 01:55 6010DTJS
0.0355 J mg/Kg - dry 0.00952 0.219Mercury (Total)1 01/17/23 15:10 7471AMRE
<0.445 mg/Kg - dry 0.445 0.696Selenium 1 01/14/23 01:55 6010DTJS
<0.223 mg/Kg - dry 0.223 0.348Silver 1 01/14/23 01:55 6010DTJS
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V28949 01/17/23 10:10
326 mg/Kg - dry 15.6 33.4Diesel Range Organics (C10-C28)2 01/17/23 17:06 V28965AMP
8015C DROSurrogate: OTP Surrogate 64.4 Limits: 31-123%01/17/23 17:062 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V28713 01/09/23 08:00
<2.88 mg/Kg - dry 2.88 6.96Gasoline Range Organics (C6-C10)50 01/09/23 11:09 V28714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 176 *Limits: 50-137%01/09/23 11:0950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V28925 01/16/23 11:55
<2.56 µg/Kg - dry 2.56 6.96
Aldrin 1 01/18/23 21:02 V29029JMV
<1.63 µg/Kg - dry 1.63 6.96alpha-BHC 1 01/18/23 21:02 V29029JMV
<2.77 µg/Kg - dry 2.77 6.96beta-BHC 1 01/18/23 21:02 V29029JMV
<1.74 µg/Kg - dry 1.74 6.96delta-BHC 1 01/18/23 21:02 V29029JMV
<24.5 µg/Kg - dry 24.5 69.6Chlordane 1 01/18/23 21:02 V29029JMV
<2.63 µg/Kg - dry 2.63 6.96alpha-Chlordane 1 01/18/23 21:02 V29029JMV
<2.35 µg/Kg - dry 2.35 6.96gamma-Chlordane 1 01/18/23 21:02 V29029JMV
<2.60 µg/Kg - dry 2.60 6.96
4,4'-DDD 1 01/18/23 21:02 V29029JMV
<2.86 µg/Kg - dry 2.86 6.964,4'-DDE 1 01/18/23 21:02 V29029JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V28925 01/16/23 11:55
11.7 M µg/Kg - dry 2.12 6.964,4'-DDT 1 01/18/23 21:02 V29029JMV
<2.91 µg/Kg - dry 2.91 6.96Dieldrin 1 01/18/23 21:02 V29029JMV
<2.49 µg/Kg - dry 2.49 6.96Endosulfan I 1 01/18/23 21:02 V29029JMV
<2.44 µg/Kg - dry 2.44 6.96Endosulfan II 1 01/18/23 21:02 V29029JMV
<2.53 µg/Kg - dry 2.53 6.96Endosulfan Sulfate 1 01/18/23 21:02 V29029JMV
4.46 J µg/Kg - dry 2.67 6.96Endrin 1 01/18/23 21:02 V29029JMV
<2.94 µg/Kg - dry 2.94 6.96Endrin Aldehyde 1 01/18/23 21:02 V29029JMV
<2.56 µg/Kg - dry 2.56 6.96Endrin Ketone 1 01/18/23 21:02 V29029JMV
<1.75 µg/Kg - dry 1.75 6.96
gamma-BHC 1 01/18/23 21:02 V29029JMV
<1.89 µg/Kg - dry 1.89 6.96Heptachlor 1 01/18/23 21:02 V29029JMV
<2.49 µg/Kg - dry 2.49 6.96Heptachlor Epoxide 1 01/18/23 21:02 V29029JMV
<3.68 µg/Kg - dry 3.68 6.96Methoxychlor 1 01/18/23 21:02 V29029JMV
<14.2 µg/Kg - dry 14.2 69.6Toxaphene 1 01/18/23 21:02 V29029JMV
Surrogate: Decachlorobiphenyl 173 Limits: 26-204%01/18/23 21:021 JMV V29029
Surrogate: Tetrachloro-m-xylene 82.0 Limits: 40-162%01/18/23 21:021 JMV V29029
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V28827 01/11/23 13:15
<0.298 mg/Kg - dry 0.298 0.836Aroclor 1016 10 01/12/23 17:51 V28867JMV
<0.669 mg/Kg - dry 0.669 1.67Aroclor 1221 10 01/12/23 17:51 V28867JMV
<0.217 mg/Kg - dry 0.217 1.67Aroclor 1232 10 01/12/23 17:51 V28867JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V28827 01/11/23 13:15
<0.223 mg/Kg - dry 0.223 0.836Aroclor 1242 10 01/12/23 17:51 V28867JMV
<0.167 mg/Kg - dry 0.167 0.836Aroclor 1248 10 01/12/23 17:51 V28867JMV
<0.208 mg/Kg - dry 0.208 0.836Aroclor 1254 10 01/12/23 17:51 V28867JMV
<0.249 mg/Kg - dry 0.249 0.836Aroclor 1260 10 01/12/23 17:51 V28867JMV
8082ASurrogate: Decachlorobiphenyl 170 Limits: 34-182%01/12/23 17:5110 JMV
8082ASurrogate: Tetrachloro-m-xylene 90.0 Limits: 36-182%01/12/23 17:5110 JMV
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
0.062 mg/Kg - dry 0.003 0.027Acetone 1 01/11/23 11:37 V28798TBL
0.006 J mg/Kg - dry 0.001 0.027Acrolein 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 01/11/23 11:37 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 01/11/23 11:37 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 01/11/23 11:37 V28798TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 01/11/23 11:37 V28798TBL
<0.0005 mg/Kg - dry 0.0005 0.006
4-Chlorotoluene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 01/11/23 11:37 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 01/11/23 11:37 V28798TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 01/11/23 11:37 V28798TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,4-Dichlorobenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 01/11/23 11:37 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013
Hexachlorobutadiene 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 01/11/23 11:37 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 01/11/23 11:37 V28798TBL
0.007 J mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 01/11/23 11:37 V28798TBL
<0.020 mg/Kg - dry 0.020 0.027
4-Methyl-2-Pentanone 1 01/11/23 11:37 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 01/11/23 11:37 V28798TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 01/11/23 11:37 V28798TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V28797 01/11/23 08:00
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 01/11/23 11:37 V28798TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 01/11/23 11:37 V28798TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 01/11/23 11:37 V28798TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2,3-Trichloropropane 1 01/11/23 11:37 V28798TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 01/11/23 11:37 V28798TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 01/11/23 11:37 V28798TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 01/11/23 11:37 V28798TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 01/11/23 11:37 V28798
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%01/11/23 11:371 TBL V28798
Surrogate: Dibromofluoromethane 106 Limits: 84-123%01/11/23 11:371 TBL V28798
Surrogate: Toluene-d8 102 Limits: 76-129%01/11/23 11:371 TBL V28798
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
<0.194 mg/Kg - dry 0.194 1.11Acenaphthene 1 01/17/23 05:08 V28964JMV
<0.175 mg/Kg - dry 0.175 1.11Acenaphthylene 1 01/17/23 05:08 V28964JMV
<0.254 mg/Kg - dry 0.254 1.11Aniline 1 01/17/23 05:08 V28964JMV
0.449 J mg/Kg - dry 0.239 1.11Anthracene 1 01/17/23 05:08 V28964JMV
0.889 J mg/Kg - dry 0.232 1.11Benzo(a)anthracene 1 01/17/23 05:08 V28964JMV
0.565 J mg/Kg - dry 0.246 1.11Benzo(a)pyrene 1 01/17/23 05:08 V28964JMV
1.75 mg/Kg - dry 0.245 1.11Benzo(b)fluoranthene 1 01/17/23 05:08 V28964JMV
0.491 J mg/Kg - dry 0.228 1.11Benzo(g,h,i)perylene 1 01/17/23 05:08 V28964JMV
0.484 J
mg/Kg - dry 0.229 1.11
Benzo(k)fluoranthene 1 01/17/23 05:08 V28964JMV
<0.969 mg/Kg - dry 0.969 3.34Benzoic Acid 1 01/17/23 05:08 V28964JMV
<0.175 mg/Kg - dry 0.175 1.11Benzyl alcohol 1 01/17/23 05:08 V28964JMV
<0.197 mg/Kg - dry 0.197 1.11Bis(2-Chloroethoxy)methane 1 01/17/23 05:08 V28964JMV
<0.179 mg/Kg - dry 0.179 1.11Bis(2-Chloroethyl)ether 1 01/17/23 05:08 V28964JMV
<0.228 mg/Kg - dry 0.228 0.552Bis(2-Chloroisopropyl)ether 1 01/17/23 05:08 V28964JMV
<0.200 mg/Kg - dry 0.200 1.11Bis(2-ethylhexyl)phthalate 1 01/17/23 05:08 V28964JMV
<0.182 mg/Kg - dry 0.182 1.11
4-Bromophenyl phenyl ether 1 01/17/23 05:08 V28964JMV
<0.189 mg/Kg - dry 0.189 0.552Butyl benzyl phthalate 1 01/17/23 05:08 V28964JMV
<0.154 mg/Kg - dry 0.154 1.114-Chloro-3-methylphenol 1 01/17/23 05:08 V28964JMV
<0.188 mg/Kg - dry 0.188 0.5524-Chloroaniline 1 01/17/23 05:08 V28964JMV
<0.194 mg/Kg - dry 0.194 1.112-Chloronaphthalene 1 01/17/23 05:08 V28964JMV
<0.164 mg/Kg - dry 0.164 1.112-Chlorophenol 1 01/17/23 05:08 V28964JMV
<0.210 mg/Kg - dry 0.210 1.674-Chlorophenyl phenyl ether 1 01/17/23 05:08 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
1.70 mg/Kg - dry 0.238 1.11Chrysene 1 01/17/23 05:08 V28964JMV
<0.385 mg/Kg - dry 0.385 1.11Dibenz(a,h)anthracene 1 01/17/23 05:08 V28964JMV
<0.199 mg/Kg - dry 0.199 1.11Dibenzofuran 1 01/17/23 05:08 V28964JMV
<0.158 mg/Kg - dry 0.158 1.111,2-Dichlorobenzene 1 01/17/23 05:08 V28964JMV
<0.162 mg/Kg - dry 0.162 1.111,3-Dichlorobenzene 1 01/17/23 05:08 V28964JMV
<0.162 mg/Kg - dry 0.162 0.5521,4-Dichlorobenzene 1 01/17/23 05:08 V28964JMV
<0.246 mg/Kg - dry 0.246 1.113,3'-Dichlorobenzidine 1 01/17/23 05:08 V28964JMV
<0.160 mg/Kg - dry 0.160 1.112,4-Dichlorophenol 1 01/17/23 05:08 V28964JMV
<0.302 mg/Kg - dry 0.302 1.11
Diethyl phthalate 1 01/17/23 05:08 V28964JMV
<0.291 mg/Kg - dry 0.291 1.11Dimethyl phthalate 1 01/17/23 05:08 V28964JMV
<0.181 mg/Kg - dry 0.181 0.5522,4-Dimethylphenol 1 01/17/23 05:08 V28964JMV
<0.179 mg/Kg - dry 0.179 1.11Di-n-butyl phthalate 1 01/17/23 05:08 V28964JMV
<0.401 mg/Kg - dry 0.401 2.514,6-Dinitro-2-methylphenol 1 01/17/23 05:08 V28964JMV
<0.869 mg/Kg - dry 0.869 2.512,4-Dinitrophenol 1 01/17/23 05:08 V28964JMV
<0.161 mg/Kg - dry 0.161 1.112,4-Dinitrotoluene 1 01/17/23 05:08 V28964JMV
<0.181 mg/Kg - dry 0.181 1.11
2,6-Dinitrotoluene 1 01/17/23 05:08 V28964JMV
<0.239 mg/Kg - dry 0.239 0.552Di-n-Octyl Phthalate 1 01/17/23 05:08 V28964JMV
3.13 mg/Kg - dry 0.206 1.11Fluoranthene 1 01/17/23 05:08 V28964JMV
<0.214 mg/Kg - dry 0.214 1.11Fluorene 1 01/17/23 05:08 V28964JMV
<0.178 mg/Kg - dry 0.178 1.11Hexachlorobenzene 1 01/17/23 05:08 V28964JMV
<0.162 mg/Kg - dry 0.162 1.11Hexachlorobutadiene 1 01/17/23 05:08 V28964JMV
<0.263 mg/Kg - dry 0.263 1.11Hexachlorocyclopentadiene 1 01/17/23 05:08 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
<0.132 mg/Kg - dry 0.132 1.11Hexachloroethane 1 01/17/23 05:08 V28964JMV
0.566 J mg/Kg - dry 0.299 1.11Indeno(1,2,3-cd)pyrene 1 01/17/23 05:08 V28964JMV
<0.320 mg/Kg - dry 0.320 1.11Isophorone 1 01/17/23 05:08 V28964JMV
<0.178 mg/Kg - dry 0.178 1.111-Methylnaphthalene 1 01/17/23 05:08 V28964JMV
<0.167 mg/Kg - dry 0.167 1.112-Methylnaphthalene 1 01/17/23 05:08 V28964JMV
<0.162 mg/Kg - dry 0.162 1.112-Methylphenol 1 01/17/23 05:08 V28964JMV
<0.142 mg/Kg - dry 0.142 1.113&4 Methylphenol 1 01/17/23 05:08 V28964JMV
0.299 J mg/Kg - dry 0.240 1.11Naphthalene 1 01/17/23 05:08 V28964JMV
<0.161 mg/Kg - dry 0.161 1.11
2-Nitroaniline 1 01/17/23 05:08 V28964JMV
<0.200 mg/Kg - dry 0.200 1.113-Nitroaniline 1 01/17/23 05:08 V28964JMV
<0.155 mg/Kg - dry 0.155 0.5524-Nitroaniline 1 01/17/23 05:08 V28964JMV
<0.194 mg/Kg - dry 0.194 0.552Nitrobenzene 1 01/17/23 05:08 V28964JMV
<0.149 mg/Kg - dry 0.149 1.112-Nitrophenol 1 01/17/23 05:08 V28964JMV
<0.196 mg/Kg - dry 0.196 1.114-Nitrophenol 1 01/17/23 05:08 V28964JMV
<0.440 mg/Kg - dry 0.440 1.11N-Nitrosodimethylamine 1 01/17/23 05:08 V28964JMV
<0.303 mg/Kg - dry 0.303 1.11
N-Nitrosodiphenylamine 1 01/17/23 05:08 V28964JMV
<0.197 mg/Kg - dry 0.197 1.11N-Nitroso-di-n-propylamine 1 01/17/23 05:08 V28964JMV
<0.579 mg/Kg - dry 0.579 1.67Pentachlorophenol 1 01/17/23 05:08 V28964JMV
0.913 J mg/Kg - dry 0.348 1.11Phenanthrene 1 01/17/23 05:08 V28964JMV
<0.188 mg/Kg - dry 0.188 1.11Phenol 1 01/17/23 05:08 V28964JMV
2.97 mg/Kg - dry 0.224 1.11Pyrene 1 01/17/23 05:08 V28964JMV
<0.132 mg/Kg - dry 0.132 0.552Pyridine 1 01/17/23 05:08 V28964JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-006-0013
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 01/06/2023
2500 E.Market St.
Report Date : 01/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
96876 Matrix:
1/4/2023 15:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V28924 01/16/23 11:00
<0.179 mg/Kg - dry 0.179 1.111,2,4-Trichlorobenzene 1 01/17/23 05:08 V28964JMV
<0.161 mg/Kg - dry 0.161 1.112,4,5-Trichlorophenol 1 01/17/23 05:08 V28964JMV
<0.161 mg/Kg - dry 0.161 1.112,4,6-Trichlorophenol 1 01/17/23 05:08 V28964JMV
8270ESurrogate: Phenol-d5 73.8 Limits: 34-121%01/17/23 05:081 JMV
Surrogate: 2-Fluorobiphenyl 95.5 Limits: 44-115%01/17/23 05:081 JMV V28964
Surrogate: 2-Fluorophenol 78.6 Limits: 35-115%01/17/23 05:081 JMV V28964
Surrogate: Nitrobenzene-d5 81.5 Limits: 37-122%01/17/23 05:081 JMV V28964
Surrogate: 4-Terphenyl-d14 98.5 Limits: 54-127%01/17/23 05:081 JMV V28964
Surrogate: 2,4,6-Tribromophenol 83.5 Limits: 39-132%01/17/23 05:081 JMV V28964
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Metals Analysis
6010D
L658650QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L658311
Associated Lab Samples: 96875, 96876
LRB-L658311 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
01/14/23 01:340.5000.240<0.240mg/KgArsenic
01/14/23 01:340.5000.1300.185mg/KgBarium
01/14/23 01:340.1000.0200<0.0200mg/KgCadmium
01/14/23 01:340.2500.236<0.236mg/KgChromium
01/14/23 01:340.3000.180<0.180mg/KgLead
01/14/23 01:340.5000.320<0.320mg/KgSelenium
01/14/23 01:340.2500.160<0.160mg/KgSilver
LCS-L658311Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1105.485.00mg/KgArsenic 80-120
10451.950.0mg/KgBarium 80-120
1075.355.00mg/KgCadmium 80-120
11356.650.0mg/KgChromium 80-120
1055.245.00mg/KgLead 80-120
99.04.935.00mg/KgSelenium 80-120
1035.165.00mg/KgSilver 80-120
V 97039-MS-L658311 V 97039-MSD-L658311Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
7.03 90.06.934.744.662.84mg/KgArsenic 86.0 75-125 1.4 20
149 71.0*14447.446.6116mg/KgBarium 59.0*75-125 3.4 20
4.67 90.04.614.744.660.460mg/KgCadmium 87.0 75-125 1.2 20
57.1 95.055.947.446.612.7mg/KgChromium 91.0 75-125 2.1 20
Page 1 of 25* QC Fail Date:01/20/2023 10:07 AM
Page 30 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Metals Analysis
6010D
L658650QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L658311
V 97039-MS-L658311 V 97039-MSD-L658311Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.8 83.010.54.744.666.94mg/KgLead 75.0 75-125 2.8 20
6.67 95.06.314.744.662.22mg/KgSelenium 86.0 75-125 5.5 20
5.12 89.05.014.744.660.951mg/KgSilver 86.0 75-125 2.1 20
V 97039-PDS-L658311Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
01/14/23 03:1910112.7mg/KgArsenic
01/14/23 03:19101171mg/KgBarium
01/14/23 03:1910211.6mg/KgCadmium
01/14/23 03:19105124mg/KgChromium
01/14/23 03:1910114.7mg/KgLead
01/14/23 03:1910012.3mg/KgSelenium
01/14/23 03:1910211.8mg/KgSilver
Page 2 of 25Date:01/20/2023 10:07 AM
Page 31 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L659074QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L658823
Associated Lab Samples: 96875, 96876
LRB-L658823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
01/17/23 14:530.1600.00697<0.00697mg/KgMercury (Total)
LCS-L658823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
89.00.3550.400mg/KgMercury (Total)80-120
L 92675-MS-L658823 L 92675-MSD-L658823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.288 79.0*0.3400.3660.3630.00718mg/KgMercury (Total)93.0 80-120 16.5 20
L 92675-PDS-L658823Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
01/17/23 15:2485.00.584mg/KgMercury (Total)
Page 3 of 25Date:01/20/2023 10:07 AM
Page 32 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V28965QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28949
Associated Lab Samples: 96875, 96876
LRB-V28949 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/17/23 14:5710.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
01/17/23 14:57OTP Surrogate (S)81.2 31-123
LCS-V28949 LCSD-V28949Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
76.7 11510670.666.7mg/KgDiesel Range Organics (C10-C28)46-126 8.2 20
70.968.5OTP Surrogate (S)31-123
Page 4 of 25Date:01/20/2023 10:07 AM
Page 33 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V28714QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V28713
Associated Lab Samples: 96875, 96876
LRB-V28713 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/09/23 10:135.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
01/09/23 10:13a,a,a-Trifluorotoluene (S)106 50-137
LCS-V28713 LCSD-V28713Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
60.7 12111557.750.0mg/KgGasoline Range Organics (C6-C10)41-138 5.0 20
99.4103a,a,a-Trifluorotoluene (S)50-137
Page 5 of 25Date:01/20/2023 10:07 AM
Page 34 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29029QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28925
Associated Lab Samples: 96875, 96876
LRB-V28925 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/18/23 17:105.001.84<1.84µg/KgAldrin
01/18/23 17:105.001.17<1.17µg/Kgalpha-BHC
01/18/23 17:105.001.99<1.99µg/Kgbeta-BHC
01/18/23 17:105.001.25<1.25µg/Kgdelta-BHC
01/18/23 17:1050.017.6<17.6µg/KgChlordane
01/18/23 17:105.001.89<1.89µg/Kgalpha-Chlordane
01/18/23 17:105.001.69<1.69µg/Kggamma-Chlordane
01/18/23 17:105.001.87<1.87µg/Kg4,4'-DDD
01/18/23 17:105.002.05<2.05µg/Kg4,4'-DDE
01/18/23 17:105.001.52<1.52µg/Kg4,4'-DDT
01/18/23 17:105.002.09<2.09µg/KgDieldrin
01/18/23 17:105.001.79<1.79µg/KgEndosulfan I
01/18/23 17:105.001.75<1.75µg/KgEndosulfan II
01/18/23 17:105.001.82<1.82µg/KgEndosulfan Sulfate
01/18/23 17:105.001.92<1.92µg/KgEndrin
01/18/23 17:105.002.11<2.11µg/KgEndrin Aldehyde
01/18/23 17:105.001.84<1.84µg/KgEndrin Ketone
01/18/23 17:105.001.26<1.26µg/Kggamma-BHC
01/18/23 17:105.001.36<1.36µg/KgHeptachlor
01/18/23 17:105.001.79<1.79µg/KgHeptachlor Epoxide
01/18/23 17:105.002.64<2.64µg/KgMethoxychlor
01/18/23 17:1050.010.2<10.2µg/KgToxaphene
01/18/23 17:10Decachlorobiphenyl (S)111 26-204
01/18/23 17:10Tetrachloro-m-xylene (S)105 40-162
Page 6 of 25Date:01/20/2023 10:07 AM
Page 35 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29029QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28925
LCS-V28925Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11137.033.3µg/KgAldrin 45-136
11337.733.3µg/Kgalpha-BHC 45-137
10334.333.3µg/Kgbeta-BHC 50-136
83.127.733.3µg/Kgdelta-BHC 47-139
120399333µg/KgChlordane 43-149
10936.333.3µg/Kgalpha-Chlordane 54-133
11036.733.3µg/Kggamma-Chlordane 53-135
11638.733.3µg/Kg4,4'-DDD 56-139
11939.733.3µg/Kg4,4'-DDE 56-134
12742.333.3µg/Kg4,4'-DDT 50-145
11538.333.3µg/KgDieldrin 56-136
11237.333.3µg/KgEndosulfan I 53-132
11739.033.3µg/KgEndosulfan II 53-134
11036.733.3µg/KgEndosulfan Sulfate 55-136
12040.033.3µg/KgEndrin 57-140
10434.733.3µg/KgEndrin Aldehyde 35-137
11638.733.3µg/KgEndrin Ketone 55-136
11137.033.3µg/Kggamma-BHC 49-135
11137.033.3µg/KgHeptachlor 47-136
10936.333.3µg/KgHeptachlor Epoxide 52-136
11739.033.3µg/KgMethoxychlor 52-143
107355333µg/KgToxaphene 33-141
114Decachlorobiphenyl (S)26-204
112Tetrachloro-m-xylene (S)40-162
Page 7 of 25Date:01/20/2023 10:07 AM
Page 36 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29029QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28925
V 97126-MS-V28925 V 97126-MSD-V28925Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
35.3 10633.033.333.3< 1.84µg/KgAldrin 99.0 45-136 6.7 29.0
36.3 10934.733.333.3< 1.17µg/Kgalpha-BHC 104 45-137 4.5 24.0
33.0 99.031.033.333.3< 1.99µg/Kgbeta-BHC 93.0 50-136 6.2 17.0
26.6 79.825.733.333.3< 1.25µg/Kgdelta-BHC 77.1 47-139 3.4 18.0
34.0 10232.033.333.3< 1.89µg/Kgalpha-Chlordane 96.0 54-133 6.0 25.0
29.6 88.828.733.333.3< 1.69µg/Kggamma-Chlordane 86.1 53-135 3.0 27.0
37.0 11135.733.333.3< 1.87µg/Kg4,4'-DDD 107 56-139 3.5 29.0
37.0 11134.733.333.3< 2.05µg/Kg4,4'-DDE 104 56-134 6.4 36.0
38.3 11535.733.333.3< 1.52µg/Kg4,4'-DDT 107 50-145 7.0 38.0
36.0 10834.333.333.3< 2.09µg/KgDieldrin 103 56-136 4.8 30.0
34.6 10433.033.333.3< 1.79µg/KgEndosulfan I 99.0 53-132 4.7 32.0
34.0 10232.033.333.3< 1.75µg/KgEndosulfan II 96.0 53-134 6.0 20.0
31.0 93.031.333.333.3< 1.82µg/KgEndosulfan Sulfate 93.9 55-136 0.9 24.0
38.6 11638.333.333.3< 1.92µg/KgEndrin 115 57-140 0.7 21.0
21.3 63.921.033.333.3< 2.11µg/KgEndrin Aldehyde 63.0 35-137 1.4 35.0
33.0 99.033.033.333.3< 1.84µg/KgEndrin Ketone 99.0 55-136 0.0 18.0
35.6 10734.033.333.3< 1.26µg/Kggamma-BHC 102 49-135 4.5 22.0
35.3 10632.333.333.3< 1.36µg/KgHeptachlor 96.9 47-136 8.8 27.0
31.0 93.028.733.333.3< 1.79µg/KgHeptachlor Epoxide 86.1 52-136 7.7 18.0
35.6 10736.733.333.3< 2.64µg/KgMethoxychlor 110 52-143 3.0 30.0
99.0Decachlorobiphenyl (S)90.9 26-204
110Tetrachloro-m-xylene (S)104 40-162
Page 8 of 25Date:01/20/2023 10:07 AM
Page 37 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Polychlorinated Biphenyls (PCB's)
8082A
V28867QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28827
Associated Lab Samples: 96875, 96876
LRB-V28827 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/12/23 15:340.05000.0178<0.0178mg/KgAroclor 1016
01/12/23 15:340.1000.0400<0.0400mg/KgAroclor 1221
01/12/23 15:340.1000.0130<0.0130mg/KgAroclor 1232
01/12/23 15:340.05000.0133<0.0133mg/KgAroclor 1242
01/12/23 15:340.05000.0100<0.0100mg/KgAroclor 1248
01/12/23 15:340.05000.0124<0.0124mg/KgAroclor 1254
01/12/23 15:340.05000.0149<0.0149mg/KgAroclor 1260
01/12/23 15:34Decachlorobiphenyl (S)96.0 34-182
01/12/23 15:34Tetrachloro-m-xylene (S)81.0 36-182
LCS-V28827 LCSD-V28827Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.273 81.997.20.3240.333mg/KgAroclor 1016 64-151 17.0 50
0.294 88.21030.3440.333mg/KgAroclor 1260 45-166 15.6 50
95.199.0Decachlorobiphenyl (S)34-182
81.971.1Tetrachloro-m-xylene (S)36-182
Page 9 of 25Date:01/20/2023 10:07 AM
Page 38 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
Associated Lab Samples: 96875, 96876
LRB-V28797 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/11/23 10:410.0200.002<0.002mg/KgAcetone
01/11/23 10:410.0200.001<0.001mg/KgAcrolein
01/11/23 10:410.0200.0008<0.0008mg/KgAcrylonitrile
01/11/23 10:410.0050.0006<0.0006mg/KgBenzene
01/11/23 10:410.0050.0005<0.0005mg/KgBromobenzene
01/11/23 10:410.0050.0008<0.0008mg/KgBromochloromethane
01/11/23 10:410.0050.001<0.001mg/KgBromodichloromethane
01/11/23 10:410.0050.001<0.001mg/KgBromoform
01/11/23 10:410.0100.001<0.001mg/KgBromomethane
01/11/23 10:410.0050.0005<0.0005mg/Kgn-Butylbenzene
01/11/23 10:410.0050.0006<0.0006mg/Kgsec-Butyl benzene
01/11/23 10:410.0050.0005<0.0005mg/Kgtert-Butyl benzene
01/11/23 10:410.0050.0006<0.0006mg/KgCarbon Disulfide
01/11/23 10:410.0050.001<0.001mg/KgCarbon Tetrachloride
01/11/23 10:410.0050.0007<0.0007mg/KgChlorobenzene
01/11/23 10:410.0050.0009<0.0009mg/KgChlorodibromomethane
01/11/23 10:410.0100.0009<0.0009mg/KgChloroethane
01/11/23 10:410.0050.001<0.001mg/KgChloroform
01/11/23 10:410.0100.0006<0.0006mg/KgChloromethane
01/11/23 10:410.0050.0005<0.0005mg/Kg2-Chlorotoluene
01/11/23 10:410.0050.0004<0.0004mg/Kg4-Chlorotoluene
01/11/23 10:410.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
01/11/23 10:410.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
01/11/23 10:410.0050.0006<0.0006mg/Kg1,2-Dibromoethane
01/11/23 10:410.0050.0006<0.0006mg/KgDibromomethane
01/11/23 10:410.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
01/11/23 10:410.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 25Date:01/20/2023 10:07 AM
Page 39 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
Associated Lab Samples: 96875, 96876
LRB-V28797 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/11/23 10:410.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
01/11/23 10:410.0100.001<0.001mg/KgDichlorodifluoromethane
01/11/23 10:410.0050.0008<0.0008mg/Kg1,1-Dichloroethane
01/11/23 10:410.0050.001<0.001mg/Kg1,2-Dichloroethane
01/11/23 10:410.0050.0007<0.0007mg/Kg1,1-Dichloroethene
01/11/23 10:410.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
01/11/23 10:410.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
01/11/23 10:410.0050.0004<0.0004mg/Kg1,2-Dichloropropane
01/11/23 10:410.0050.0006<0.0006mg/Kg1,3-Dichloropropane
01/11/23 10:410.0050.001<0.001mg/Kg2,2-Dichloropropane
01/11/23 10:410.0050.0008<0.0008mg/Kg1,1-Dichloropropene
01/11/23 10:410.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
01/11/23 10:410.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
01/11/23 10:410.0050.0006<0.0006mg/KgEthylbenzene
01/11/23 10:410.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
01/11/23 10:410.0100.0008<0.0008mg/KgHexachlorobutadiene
01/11/23 10:410.0100.0007<0.0007mg/Kgn-Hexane
01/11/23 10:410.0200.0006<0.0006mg/Kg2-Hexanone
01/11/23 10:410.0050.0005<0.0005mg/KgIsopropylbenzene
01/11/23 10:410.0050.001<0.001mg/Kg4-Isopropyl toluene
01/11/23 10:410.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
01/11/23 10:410.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
01/11/23 10:410.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
01/11/23 10:410.0100.001<0.001mg/KgMethylene Chloride
01/11/23 10:410.0100.0010<0.0010mg/KgNaphthalene
01/11/23 10:410.0050.0005<0.0005mg/Kgn-Propylbenzene
01/11/23 10:410.0050.001<0.001mg/KgStyrene
Page 11 of 25Date:01/20/2023 10:07 AM
Page 40 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
Associated Lab Samples: 96875, 96876
LRB-V28797 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/11/23 10:410.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
01/11/23 10:410.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
01/11/23 10:410.0050.0009<0.0009mg/KgTetrachloroethene
01/11/23 10:410.0050.0007<0.0007mg/KgToluene
01/11/23 10:410.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
01/11/23 10:410.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
01/11/23 10:410.0050.001<0.001mg/Kg1,1,1-Trichloroethane
01/11/23 10:410.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
01/11/23 10:410.0050.0009<0.0009mg/KgTrichloroethene
01/11/23 10:410.0100.002<0.002mg/KgTrichlorofluoromethane
01/11/23 10:410.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
01/11/23 10:410.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
01/11/23 10:410.0100.0005<0.0005mg/KgVinyl Acetate
01/11/23 10:410.0100.0005<0.0005mg/KgVinyl Chloride
01/11/23 10:410.0050.0005<0.0005mg/Kgo-Xylene
01/11/23 10:410.0100.001<0.001mg/Kgm,p-Xylene
01/11/23 10:414-Bromofluorobenzene (S)105 70-130
01/11/23 10:41Dibromofluoromethane (S)103 84-123
01/11/23 10:41Toluene-d8 (S)101 76-129
LCS-V28797 LCSD-V28797Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.092 92.51010.1010.100mg/KgAcetone 29-198 8.7 20
0.081 81.785.00.0850.100mg/KgAcrolein 70-130 3.9 20
0.108 1081060.1060.100mg/KgAcrylonitrile 65-134 1.8 20
Page 12 of 25Date:01/20/2023 10:07 AM
Page 41 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
LCS-V28797 LCSD-V28797Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.695.80.0470.050mg/KgBenzene 74-127 4.4 20
0.046 92.895.20.0470.050mg/KgBromobenzene 73-125 2.5 20
0.049 99.495.60.0470.050mg/KgBromochloromethane 72-134 3.8 20
0.045 91.894.40.0470.050mg/KgBromodichloromethane 75-122 2.7 20
0.049 98.21000.0500.050mg/KgBromoform 66-135 2.0 20
0.045 90.694.20.0470.050mg/KgBromomethane 20-180 3.8 20
0.048 97.01030.0510.050mg/Kgn-Butylbenzene 65-135 6.0 20
0.045 91.699.40.0490.050mg/Kgsec-Butyl benzene 66-131 8.1 20
0.046 93.898.40.0490.050mg/Kgtert-Butyl benzene 67-132 4.7 20
0.043 87.293.20.0460.050mg/KgCarbon Disulfide 61-129 6.6 20
0.039 78.697.20.0480.050mg/KgCarbon Tetrachloride 64-143 21.1*20
0.044 89.896.60.0480.050mg/KgChlorobenzene 74-118 7.2 20
0.047 95.495.00.0470.050mg/KgChlorodibromomethane 73-122 0.4 20
0.044 88.089.40.0440.050mg/KgChloroethane 33-149 1.5 20
0.044 88.494.40.0470.050mg/KgChloroform 73-127 6.5 20
0.045 90.898.00.0490.050mg/KgChloromethane 45-143 7.6 20
0.046 93.496.00.0480.050mg/Kg2-Chlorotoluene 67-124 2.7 20
0.046 93.496.00.0480.050mg/Kg4-Chlorotoluene 71-126 2.7 20
0.045 91.492.20.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.8 20
0.055 1101130.0560.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.3 20
0.047 94.094.40.0470.050mg/Kg1,2-Dibromoethane 70-132 0.4 20
0.044 88.489.40.0440.050mg/KgDibromomethane 74-133 1.1 20
0.049 98.699.00.0490.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.046 92.096.80.0480.050mg/Kg1,3-Dichlorobenzene 71-120 5.0 20
0.046 93.696.80.0480.050mg/Kg1,4-Dichlorobenzene 71-123 3.3 20
0.040 81.087.20.0430.050mg/KgDichlorodifluoromethane 26-146 7.3 20
Page 13 of 25* QC Fail Date:01/20/2023 10:07 AM
Page 42 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
LCS-V28797 LCSD-V28797Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.095.60.0470.050mg/Kg1,1-Dichloroethane 74-127 7.1 20
0.045 91.690.00.0450.050mg/Kg1,2-Dichloroethane 68-128 1.7 20
0.043 87.890.20.0450.050mg/Kg1,1-Dichloroethene 67-149 2.6 20
0.044 89.896.60.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 7.2 20
0.043 87.294.80.0470.050mg/Kgtrans-1,2-Dichloroethene 73-132 8.3 20
0.045 90.493.20.0460.050mg/Kg1,2-Dichloropropane 73-130 3.0 20
0.047 94.299.40.0490.050mg/Kg1,3-Dichloropropane 75-124 5.3 20
0.043 86.293.60.0460.050mg/Kg2,2-Dichloropropane 50-142 8.2 20
0.044 88.696.00.0480.050mg/Kg1,1-Dichloropropene 71-130 8.0 20
0.047 94.295.00.0470.050mg/Kgcis-1,3-Dichloropropene 71-125 0.8 20
0.050 1001000.0500.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
0.043 87.494.80.0470.050mg/KgEthylbenzene 74-128 8.1 20
0.090 90.093.10.0930.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 3.3 20
0.043 86.699.20.0490.050mg/KgHexachlorobutadiene 64-125 13.5 20
0.046 92.092.60.0460.050mg/Kgn-Hexane 70-130 0.6 20
0.047 95.21020.0510.050mg/Kg2-Hexanone 61-157 7.0 20
0.045 90.697.00.0480.050mg/KgIsopropylbenzene 68-126 6.8 20
0.045 91.299.20.0490.050mg/Kg4-Isopropyl toluene 68-129 8.4 20
0.050 1011020.0510.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.1 20
0.044 88.492.60.0460.050mg/KgMethyl tert-butyl ether (MTBE)70-130 4.6 20
0.049 99.61070.0530.050mg/Kg4-Methyl-2-Pentanone 57-162 6.7 20
0.041 83.687.00.0430.050mg/KgMethylene Chloride 74-129 3.9 20
0.048 97.21010.0500.050mg/KgNaphthalene 57-157 4.2 20
0.045 91.897.20.0480.050mg/Kgn-Propylbenzene 67-130 5.7 20
0.047 95.01020.0500.050mg/KgStyrene 77-121 6.7 20
0.046 92.693.60.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
Page 14 of 25Date:01/20/2023 10:07 AM
Page 43 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V28798QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V28797
LCS-V28797 LCSD-V28797Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 95.293.40.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.9 20
0.045 91.495.40.0470.050mg/KgTetrachloroethene 68-130 4.2 20
0.044 89.092.60.0460.050mg/KgToluene 71-129 3.9 20
0.048 96.699.80.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.2 20
0.047 95.01020.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 7.1 20
0.043 87.492.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.9 20
0.046 92.21010.0500.050mg/Kg1,1,2-Trichloroethane 70-133 8.7 20
0.043 87.692.60.0460.050mg/KgTrichloroethene 75-133 5.5 20
0.043 87.895.80.0470.050mg/KgTrichlorofluoromethane 44-146 8.7 20
0.052 1041040.0510.050mg/Kg1,2,3-Trichloropropane 60-137 0.3 20
0.045 91.699.80.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.5 20
0.043 86.684.20.0420.050mg/KgVinyl Acetate 60-140 2.8 20
0.041 82.691.20.0450.050mg/KgVinyl Chloride 48-147 9.8 20
0.044 88.697.00.0480.050mg/Kgo-Xylene 74-126 9.0 20
0.092 92.296.70.0960.100mg/Kgm,p-Xylene 75-124 4.7 20
1031044-Bromofluorobenzene (S)70-130
100102Dibromofluoromethane (S)84-123
101103Toluene-d8 (S)76-129
Page 15 of 25Date:01/20/2023 10:07 AM
Page 44 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
Associated Lab Samples: 96875, 96876
LRB-V28924 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/16/23 17:070.6600.116<0.116mg/KgAcenaphthene
01/16/23 17:070.6600.105<0.105mg/KgAcenaphthylene
01/16/23 17:070.6600.152<0.152mg/KgAniline
01/16/23 17:070.6600.143<0.143mg/KgAnthracene
01/16/23 17:070.6600.139<0.139mg/KgBenzo(a)anthracene
01/16/23 17:070.6600.147<0.147mg/KgBenzo(a)pyrene
01/16/23 17:070.6600.146<0.146mg/KgBenzo(b)fluoranthene
01/16/23 17:070.6600.136<0.136mg/KgBenzo(g,h,i)perylene
01/16/23 17:070.6600.137<0.137mg/KgBenzo(k)fluoranthene
01/16/23 17:072.000.580<0.580mg/KgBenzoic Acid
01/16/23 17:070.6600.105<0.105mg/KgBenzyl alcohol
01/16/23 17:070.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
01/16/23 17:070.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
01/16/23 17:070.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
01/16/23 17:070.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
01/16/23 17:070.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
01/16/23 17:070.3300.113<0.113mg/KgButyl benzyl phthalate
01/16/23 17:070.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
01/16/23 17:070.3300.112<0.112mg/Kg4-Chloroaniline
01/16/23 17:070.6600.116<0.116mg/Kg2-Chloronaphthalene
01/16/23 17:070.6600.098<0.098mg/Kg2-Chlorophenol
01/16/23 17:071.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
01/16/23 17:070.6600.142<0.142mg/KgChrysene
01/16/23 17:070.6600.230<0.230mg/KgDibenz(a,h)anthracene
01/16/23 17:070.6600.119<0.119mg/KgDibenzofuran
01/16/23 17:070.6600.094<0.094mg/Kg1,2-Dichlorobenzene
01/16/23 17:070.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 16 of 25Date:01/20/2023 10:07 AM
Page 45 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
Associated Lab Samples: 96875, 96876
LRB-V28924 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/16/23 17:070.3300.097<0.097mg/Kg1,4-Dichlorobenzene
01/16/23 17:070.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
01/16/23 17:070.6600.095<0.095mg/Kg2,4-Dichlorophenol
01/16/23 17:070.6600.180<0.180mg/KgDiethyl phthalate
01/16/23 17:070.6600.174<0.174mg/KgDimethyl phthalate
01/16/23 17:070.3300.108<0.108mg/Kg2,4-Dimethylphenol
01/16/23 17:070.6600.107<0.107mg/KgDi-n-butyl phthalate
01/16/23 17:071.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
01/16/23 17:071.500.520<0.520mg/Kg2,4-Dinitrophenol
01/16/23 17:070.6600.096<0.096mg/Kg2,4-Dinitrotoluene
01/16/23 17:070.6600.108<0.108mg/Kg2,6-Dinitrotoluene
01/16/23 17:070.3300.143<0.143mg/KgDi-n-Octyl Phthalate
01/16/23 17:070.6600.123<0.123mg/KgFluoranthene
01/16/23 17:070.6600.128<0.128mg/KgFluorene
01/16/23 17:070.6600.106<0.106mg/KgHexachlorobenzene
01/16/23 17:070.6600.097<0.097mg/KgHexachlorobutadiene
01/16/23 17:070.6600.157<0.157mg/KgHexachlorocyclopentadiene
01/16/23 17:070.6600.079<0.079mg/KgHexachloroethane
01/16/23 17:070.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
01/16/23 17:070.6600.191<0.191mg/KgIsophorone
01/16/23 17:070.6600.106<0.106mg/Kg1-Methylnaphthalene
01/16/23 17:070.6600.100<0.100mg/Kg2-Methylnaphthalene
01/16/23 17:070.6600.097<0.097mg/Kg2-Methylphenol
01/16/23 17:070.6600.084<0.084mg/Kg3&4 Methylphenol
01/16/23 17:070.6600.144<0.144mg/KgNaphthalene
01/16/23 17:070.6600.096<0.096mg/Kg2-Nitroaniline
01/16/23 17:070.6600.120<0.120mg/Kg3-Nitroaniline
Page 17 of 25Date:01/20/2023 10:07 AM
Page 46 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
Associated Lab Samples: 96875, 96876
LRB-V28924 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/16/23 17:070.3300.093<0.093mg/Kg4-Nitroaniline
01/16/23 17:070.3300.116<0.116mg/KgNitrobenzene
01/16/23 17:070.6600.088<0.088mg/Kg2-Nitrophenol
01/16/23 17:070.6600.117<0.117mg/Kg4-Nitrophenol
01/16/23 17:070.6600.263<0.263mg/KgN-Nitrosodimethylamine
01/16/23 17:070.6600.181<0.181mg/KgN-Nitrosodiphenylamine
01/16/23 17:070.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
01/16/23 17:071.000.347<0.347mg/KgPentachlorophenol
01/16/23 17:070.6600.208<0.208mg/KgPhenanthrene
01/16/23 17:070.6600.112<0.112mg/KgPhenol
01/16/23 17:070.6600.134<0.134mg/KgPyrene
01/16/23 17:070.3300.079<0.079mg/KgPyridine
01/16/23 17:070.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
01/16/23 17:070.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
01/16/23 17:070.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
01/16/23 17:072-Fluorobiphenyl (S)95.8 44-115
01/16/23 17:072-Fluorophenol (S)81.6 35-115
01/16/23 17:07Nitrobenzene-d5 (S)83.8 37-122
01/16/23 17:074-Terphenyl-d14 (S)104 54-127
01/16/23 17:072,4,6-Tribromophenol (S)87.6 39-132
01/16/23 17:07Phenol-d5 (S)79.8 34-121
LCS-V28924Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.81.551.67mg/KgAcenaphthene 40-123
89.21.491.67mg/KgAcenaphthylene 32-132
Page 18 of 25Date:01/20/2023 10:07 AM
Page 47 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
LCS-V28924Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1322.201.67mg/KgAniline 12-197
94.01.571.67mg/KgAnthracene 47-123
92.21.541.67mg/KgBenzo(a)anthracene 49-126
83.81.401.67mg/KgBenzo(a)pyrene 45-129
83.21.391.67mg/KgBenzo(b)fluoranthene 45-132
76.01.271.67mg/KgBenzo(g,h,i)perylene 43-134
77.81.301.67mg/KgBenzo(k)fluoranthene 47-132
51.50.8611.67mg/KgBenzoic Acid 10-83
94.61.581.67mg/KgBenzyl alcohol 29-122
81.41.361.67mg/KgBis(2-Chloroethoxy)methane 36-121
84.41.411.67mg/KgBis(2-Chloroethyl)ether 31-120
90.41.511.67mg/KgBis(2-Chloroisopropyl)ether 33-131
96.41.611.67mg/KgBis(2-ethylhexyl)phthalate 51-133
97.01.621.67mg/Kg4-Bromophenyl phenyl ether 46-124
96.41.611.67mg/KgButyl benzyl phthalate 48-132
79.61.331.67mg/Kg4-Chloro-3-methylphenol 45-122
67.61.131.67mg/Kg4-Chloroaniline 17-106
91.61.531.67mg/Kg2-Chloronaphthalene 41-114
91.61.531.67mg/Kg2-Chlorophenol 34-121
95.81.601.67mg/Kg4-Chlorophenyl phenyl ether 45-121
92.21.541.67mg/KgChrysene 50-124
78.41.311.67mg/KgDibenz(a,h)anthracene 45-134
90.41.511.67mg/KgDibenzofuran 44-120
86.21.441.67mg/Kg1,2-Dichlorobenzene 33-117
82.61.381.67mg/Kg1,3-Dichlorobenzene 30-115
81.41.361.67mg/Kg1,4-Dichlorobenzene 31-115
61.61.031.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 19 of 25Date:01/20/2023 10:07 AM
Page 48 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
LCS-V28924Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.21.391.67mg/Kg2,4-Dichlorophenol 40-122
94.61.581.67mg/KgDiethyl phthalate 50-124
95.21.591.67mg/KgDimethyl phthalate 48-124
1041.731.67mg/Kg2,4-Dimethylphenol 30-127
98.21.641.67mg/KgDi-n-butyl phthalate 51-128
1071.791.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1031.721.67mg/Kg2,4-Dinitrophenol 27-129
94.61.581.67mg/Kg2,4-Dinitrotoluene 48-126
94.61.581.67mg/Kg2,6-Dinitrotoluene 46-124
80.81.351.67mg/KgDi-n-Octyl Phthalate 45-140
85.61.431.67mg/KgFluoranthene 50-127
93.41.561.67mg/KgFluorene 43-125
95.81.601.67mg/KgHexachlorobenzene 45-122
76.61.281.67mg/KgHexachlorobutadiene 32-123
73.61.231.67mg/KgHexachlorocyclopentadiene 32-117
80.21.341.67mg/KgHexachloroethane 28-117
77.21.291.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
51.90.8681.67mg/KgIsophorone 30-122
74.81.251.67mg/Kg1-Methylnaphthalene 40-119
74.81.251.67mg/Kg2-Methylnaphthalene 38-122
91.61.531.67mg/Kg2-Methylphenol 32-122
84.41.411.67mg/Kg3&4 Methylphenol 34-119
73.01.221.67mg/KgNaphthalene 35-123
96.41.611.67mg/Kg2-Nitroaniline 44-127
79.01.321.67mg/Kg3-Nitroaniline 33-119
89.81.501.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 20 of 25Date:01/20/2023 10:07 AM
Page 49 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
LCS-V28924Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2-Nitrophenol 36-123
92.21.541.67mg/Kg4-Nitrophenol 30-132
76.01.271.67mg/KgN-Nitrosodimethylamine 10-146
1141.901.67mg/KgN-Nitrosodiphenylamine 38-127
84.41.411.67mg/KgN-Nitroso-di-n-propylamine 36-120
1141.901.67mg/KgPentachlorophenol 25-133
94.01.571.67mg/KgPhenanthrene 50-121
85.01.421.67mg/KgPhenol 34-121
95.21.591.67mg/KgPyrene 47-127
46.20.7731.67mg/KgPyridine 10-80
74.81.251.67mg/Kg1,2,4-Trichlorobenzene 34-118
88.61.481.67mg/Kg2,4,5-Trichlorophenol 41-124
92.81.551.67mg/Kg2,4,6-Trichlorophenol 39-126
98.82-Fluorobiphenyl (S)44-115
85.82-Fluorophenol (S)35-115
76.0Nitrobenzene-d5 (S)37-122
1064-Terphenyl-d14 (S)54-127
93.92,4,6-Tribromophenol (S)39-132
82.2Phenol-d5 (S)34-121
V 97092-MS-V28924 V 97092-MSD-V28924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.44 86.21.481.671.67<0.116mg/KgAcenaphthene 88.6 40-123 2.7 20
1.43 85.61.541.671.67<0.105mg/KgAcenaphthylene 92.2 32-132 7.4 20
1.23 73.61.461.671.67<0.152mg/KgAniline 87.4 12-197 17.1 20
Page 21 of 25Date:01/20/2023 10:07 AM
Page 50 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
V 97092-MS-V28924 V 97092-MSD-V28924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.49 89.21.581.671.67<0.143mg/KgAnthracene 94.6 47-123 5.8 20
1.43 85.61.531.671.67<0.139mg/KgBenzo(a)anthracene 91.6 49-126 6.7 20
1.32 79.01.411.671.67<0.147mg/KgBenzo(a)pyrene 84.4 45-129 6.5 20
1.29 77.21.381.671.67<0.146mg/KgBenzo(b)fluoranthene 82.6 45-132 6.7 20
1.20 71.81.261.671.67<0.136mg/KgBenzo(g,h,i)perylene 75.4 43-134 4.8 20
1.23 73.61.311.671.67<0.137mg/KgBenzo(k)fluoranthene 78.4 47-132 6.2 20
1.37 82.01.431.671.67<0.580mg/KgBenzoic Acid 85.6 10-83 4.2 20
1.50 89.81.601.671.67<0.105mg/KgBenzyl alcohol 95.8 29-122 6.4 20
1.28 76.61.401.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 83.8 36-121 8.9 20
1.45 86.81.551.671.67<0.107mg/KgBis(2-Chloroethyl)ether 92.8 31-120 6.6 20
1.40 83.81.521.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 91.0 33-131 8.2 20
1.57 94.01.691.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 101 51-133 7.3 20
1.54 92.21.631.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 97.6 46-124 5.6 20
1.56 93.41.681.671.67<0.113mg/KgButyl benzyl phthalate 101 48-132 7.4 20
1.22 73.01.311.671.67<0.092mg/Kg4-Chloro-3-methylphenol 78.4 45-122 7.1 20
0.922 55.21.051.671.67<0.112mg/Kg4-Chloroaniline 62.8 17-106 12.9 20
1.46 87.41.611.671.67<0.116mg/Kg2-Chloronaphthalene 96.4 41-114 9.7 20
1.48 88.61.561.671.67<0.098mg/Kg2-Chlorophenol 93.4 34-121 5.2 20
1.49 89.21.581.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 94.6 45-121 5.8 20
1.44 86.21.551.671.67<0.142mg/KgChrysene 92.8 50-124 7.3 20
1.22 73.01.291.671.67<0.230mg/KgDibenz(a,h)anthracene 77.2 45-134 5.5 20
1.42 85.01.541.671.67<0.119mg/KgDibenzofuran 92.2 44-120 8.1 20
1.35 80.81.471.671.67<0.094mg/Kg1,2-Dichlorobenzene 88.0 33-117 8.5 20
1.28 76.61.431.671.67<0.097mg/Kg1,3-Dichlorobenzene 85.6 30-115 11.0 20
1.28 76.61.411.671.67<0.097mg/Kg1,4-Dichlorobenzene 84.4 31-115 9.6 20
0.631 37.70.7681.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 45.9 22-121 19.5 20
Page 22 of 25Date:01/20/2023 10:07 AM
Page 51 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
V 97092-MS-V28924 V 97092-MSD-V28924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.30 77.81.401.671.67<0.095mg/Kg2,4-Dichlorophenol 83.8 40-122 7.4 20
1.45 86.81.571.671.67<0.180mg/KgDiethyl phthalate 94.0 50-124 7.9 20
1.46 87.41.581.671.67<0.174mg/KgDimethyl phthalate 94.6 48-124 7.8 30
1.61 96.41.751.671.67<0.108mg/Kg2,4-Dimethylphenol 105 30-127 8.3 20
1.55 92.81.641.671.67<0.107mg/KgDi-n-butyl phthalate 98.2 51-128 5.6 20
1.73 1041.791.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 107 29-132 3.4 20
1.77 1061.911.671.67<0.520mg/Kg2,4-Dinitrophenol 114 27-129 7.6 20
1.48 88.61.591.671.67<0.096mg/Kg2,4-Dinitrotoluene 95.2 48-126 7.1 20
1.51 90.41.571.671.67<0.108mg/Kg2,6-Dinitrotoluene 94.0 46-124 3.8 20
1.32 79.01.421.671.67<0.143mg/KgDi-n-Octyl Phthalate 85.0 45-140 7.2 20
1.36 81.41.421.671.67<0.123mg/KgFluoranthene 85.0 50-127 4.3 20
1.44 86.21.571.671.67<0.128mg/KgFluorene 94.0 43-125 8.6 20
1.54 92.21.621.671.67<0.106mg/KgHexachlorobenzene 97.0 45-122 5.0 20
1.26 75.41.381.671.67<0.097mg/KgHexachlorobutadiene 82.6 32-123 9.0 20
0.894 53.50.9271.671.67<0.157mg/KgHexachlorocyclopentadiene 55.5 32-117 3.6 20
1.24 74.21.381.671.67<0.079mg/KgHexachloroethane 82.6 28-117 10.6 20
1.22 73.01.291.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 77.2 45-133 5.5 20
0.817 48.90.8741.671.67<0.191mg/KgIsophorone 52.3 30-122 6.7 20
1.20 71.81.291.671.67<0.106mg/Kg1-Methylnaphthalene 77.2 40-119 7.2 20
1.18 70.61.301.671.67<0.100mg/Kg2-Methylnaphthalene 77.8 38-122 9.6 20
1.44 86.21.531.671.67<0.097mg/Kg2-Methylphenol 91.6 32-122 6.0 20
1.27 76.01.361.671.67<0.084mg/Kg3&4 Methylphenol 81.4 34-119 6.8 20
1.19 71.21.311.671.67<0.144mg/KgNaphthalene 78.4 35-123 9.6 20
1.49 89.21.601.671.67<0.096mg/Kg2-Nitroaniline 95.8 44-127 7.1 20
1.25 74.81.401.671.67<0.120mg/Kg3-Nitroaniline 83.8 33-119 11.3 20
1.28 76.61.451.671.67<0.093mg/Kg4-Nitroaniline 86.8 63-147 12.4 20
Page 23 of 25Date:01/20/2023 10:07 AM
Page 52 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V28964QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V28924
V 97092-MS-V28924 V 97092-MSD-V28924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.14 68.21.261.671.67<0.116mg/KgNitrobenzene 75.4 34-122 10.0 20
1.25 74.81.351.671.67<0.088mg/Kg2-Nitrophenol 80.8 32-123 7.6 20
1.42 85.01.551.671.67<0.117mg/Kg4-Nitrophenol 92.8 30-132 8.7 20
0.654 39.10.7471.671.67<0.263mg/KgN-Nitrosodimethylamine 44.7 10-146 13.2 30
1.79 1071.861.671.67<0.181mg/KgN-Nitrosodiphenylamine 111 38-127 3.8 20
1.33 79.61.441.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 86.2 36-120 7.9 20
1.89 1131.971.671.67<0.347mg/KgPentachlorophenol 118 25-133 4.1 20
1.50 89.81.591.671.67<0.208mg/KgPhenanthrene 95.2 50-121 5.8 20
1.31 78.41.411.671.67<0.112mg/KgPhenol 84.4 34-121 7.3 20
1.51 90.41.611.671.67<0.134mg/KgPyrene 96.4 47-127 6.4 20
0.456 27.30.4561.671.67<0.079mg/KgPyridine 27.3 10-80 0.0 20
1.22 73.01.341.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 80.2 34-118 9.3 20
1.47 88.01.531.671.67<0.096mg/Kg2,4,5-Trichlorophenol 91.6 41-124 4.0 20
1.45 86.81.581.671.67<0.096mg/Kg2,4,6-Trichlorophenol 94.6 39-126 8.5 20
95.22-Fluorobiphenyl (S)101 44-115
81.32-Fluorophenol (S)87.0 35-115
74.8Nitrobenzene-d5 (S)79.6 37-122
1044-Terphenyl-d14 (S)110 54-127
86.72,4,6-Tribromophenol (S)91.5 39-132
77.4Phenol-d5 (S)79.8 34-121
Page 24 of 25Date:01/20/2023 10:07 AM
Page 53 of 56
Quality Control Data
23-006-0013Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E.Market St.
Dry Weight Determination
SW-DRYWT
V28684QC Analytical Batch:
Analysis Method:
Analysis Description:
V 96875-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 01/06/23 17:005.229.528.0%Moisture
Page 25 of 25Date:01/20/2023 10:07 AM
Page 54 of 56
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-006-0013
Mid-Atlantic Associates, Inc. - Raleigh
01139
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:01/06/2023 12:54:01
Special precautions or instructions included?
Comments:
Page 55 of 56
Page 56 of 56

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/20/2023
Mid-Atlantic Associates, Inc. - Raleigh Kevin Clay
409 Rogers View Court Raleigh, NC, 27610
Ref: Analytical Testing
Lab Report Number: 23-038-0021 Client Project Description: 2500 E. Market St.
Dear Kevin Clay:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/7/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 53
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-038-0021
Page 2 of 53
Report Number:
Sample Summary Table
Client Project Description:
23-038-0021
2500 E. Market St.
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
02/03/2023 10:40Solids 99112 HA-1 02/07/2023 13:00
02/03/2023 10:40Solids 99112 HA-1 02/07/2023 13:00 6010D WP MTN -
02/03/2023 12:10Solids 99117 Stockpile 02/07/2023 13:00
02/03/2023 12:10Solids 99117 Stockpile 02/07/2023 13:00 6010D WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 53
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-038-0021
Report Limit
Project:2500 E. Market St.
V 99112HA-1
27.2 02/11/2023 00:506010DChromiummg/Kg - dry 0.345
0.904 02/11/2023 00:506010DLeadmg/Kg - dry 0.263
J0.007 02/08/2023 12:038260DAcetonemg/Kg - dry 0.003
31.7 02/08/2023 17:05SW-DRYWT Moisture %
V 99117Stockpile
75.6 02/11/2023 01:066010DChromiummg/Kg - dry 0.359
1.24 02/11/2023 01:066010DLeadmg/Kg - dry 0.274
J0.006 02/08/2023 12:308260DAcetonemg/Kg - dry 0.003
34.4 02/08/2023 17:05SW-DRYWT Moisture %
Page 4 of 53

Client: Mid-Atlantic Associates, Inc. - Raleigh CASE NARRATIVE
Project: 2500 E. Market St. Lab Report Number: 23-038-0021
Date: 2/20/2023
Metals Analysis Method 6010D Sample 83951 QC Batch No: L663515/L663017
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 83951
Analyte: Lead QC Batch No: L663862/L663017
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Total Petroleum Hydrocarbons - Volatile Method 8015C GRO Sample 99117 (Stockpile)
Analyte: a,a,a-Trifluorotoluene QC Batch No: V29612/V29611
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits. Polychlorinated Biphenyls (PCB's) Method 8082A QC Batch No: V29840
CCV result for aroclor 1260 is above range, due to one 1260 congener being above range. Samples show no aroclor patterns. No further action taken.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Benzoic Acid QC Batch No: V29677/V29651 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.

Page 5 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
31.7 %Moisture 1 02/08/23 17:05 SW-DRYWTAMB
27.2 mg/Kg - dry 0.345 0.366Chromium 1 02/11/23 00:50 6010DTJS
0.904 mg/Kg - dry 0.263 0.439Lead 1 02/11/23 00:50 6010DTJS
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 6 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29704 02/13/23 09:45
<6.81 mg/Kg - dry 6.81 14.6Diesel Range Organics (C10-C28)1 02/13/23 19:13 V29729AMP
8015C DROSurrogate: OTP Surrogate 74.0 Limits: 31-123%02/13/23 19:131 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29611 02/08/23 08:00
<3.03 mg/Kg - dry 3.03 7.32Gasoline Range Organics (C6-C10)50 02/08/23 12:50 V29612TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 121 Limits: 50-137%02/08/23 12:5050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V29735 02/13/23 15:40
<0.0026 mg/Kg - dry 0.0026 0.0073
Aldrin 1 02/17/23 18:09 V29928JMV
<0.0017 mg/Kg - dry 0.0017 0.0073alpha-BHC 1 02/17/23 18:09 V29928JMV
<0.0029 mg/Kg - dry 0.0029 0.0073beta-BHC 1 02/17/23 18:09 V29928JMV
<0.0018 mg/Kg - dry 0.0018 0.0073delta-BHC 1 02/17/23 18:09 V29928JMV
<0.0257 mg/Kg - dry 0.0257 0.0732Chlordane 1 02/17/23 18:09 V29928JMV
<0.0027 mg/Kg - dry 0.0027 0.0073alpha-Chlordane 1 02/17/23 18:09 V29928JMV
<0.0024 mg/Kg - dry 0.0024 0.0073gamma-Chlordane 1 02/17/23 18:09 V29928JMV
<0.0027 mg/Kg - dry 0.0027 0.0073
4,4'-DDD 1 02/17/23 18:09 V29928JMV
<0.0030 mg/Kg - dry 0.0030 0.00734,4'-DDE 1 02/17/23 18:09 V29928JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 7 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V29735 02/13/23 15:40
<0.0022 mg/Kg - dry 0.0022 0.00734,4'-DDT 1 02/17/23 18:09 V29928JMV
<0.0030 mg/Kg - dry 0.0030 0.0073Dieldrin 1 02/17/23 18:09 V29928JMV
<0.0026 mg/Kg - dry 0.0026 0.0073Endosulfan I 1 02/17/23 18:09 V29928JMV
<0.0025 mg/Kg - dry 0.0025 0.0073Endosulfan II 1 02/17/23 18:09 V29928JMV
<0.0026 mg/Kg - dry 0.0026 0.0073Endosulfan Sulfate 1 02/17/23 18:09 V29928JMV
<0.0028 mg/Kg - dry 0.0028 0.0073Endrin 1 02/17/23 18:09 V29928JMV
<0.0030 mg/Kg - dry 0.0030 0.0073Endrin Aldehyde 1 02/17/23 18:09 V29928JMV
<0.0026 mg/Kg - dry 0.0026 0.0073Endrin Ketone 1 02/17/23 18:09 V29928JMV
<0.0018 mg/Kg - dry 0.0018 0.0073
gamma-BHC 1 02/17/23 18:09 V29928JMV
<0.0019 mg/Kg - dry 0.0019 0.0073Heptachlor 1 02/17/23 18:09 V29928JMV
<0.0026 mg/Kg - dry 0.0026 0.0073Heptachlor Epoxide 1 02/17/23 18:09 V29928JMV
<0.0038 mg/Kg - dry 0.0038 0.0073Methoxychlor 1 02/17/23 18:09 V29928JMV
<0.0149 mg/Kg - dry 0.0149 0.0732Toxaphene 1 02/17/23 18:09 V29928JMV
Surrogate: Decachlorobiphenyl 76.0 Limits: 26-204%02/17/23 18:091 JMV V29928
Surrogate: Tetrachloro-m-xylene 83.8 Limits: 40-162%02/17/23 18:091 JMV V29928
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V29736 02/13/23 15:40
<0.0260 mg/Kg - dry 0.0260 0.0733Aroclor 1016 1 02/15/23 15:21 V29840JMV
<0.0585 mg/Kg - dry 0.0585 0.146Aroclor 1221 1 02/15/23 15:21 V29840JMV
<0.0190 mg/Kg - dry 0.0190 0.146Aroclor 1232 1 02/15/23 15:21 V29840JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 8 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V29736 02/13/23 15:40
<0.0194 mg/Kg - dry 0.0194 0.0733Aroclor 1242 1 02/15/23 15:21 V29840JMV
<0.0146 mg/Kg - dry 0.0146 0.0733Aroclor 1248 1 02/15/23 15:21 V29840JMV
<0.0181 mg/Kg - dry 0.0181 0.0733Aroclor 1254 1 02/15/23 15:21 V29840JMV
<0.0218 mg/Kg - dry 0.0218 0.0733Aroclor 1260 1 02/15/23 15:21 V29840JMV
8082ASurrogate: Decachlorobiphenyl 103 Limits: 34-182%02/15/23 15:211 JMV
8082ASurrogate: Tetrachloro-m-xylene 150 Limits: 36-182%02/15/23 15:211 JMV
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
0.007 J mg/Kg - dry 0.003 0.029Acetone 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.029Acrolein 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007
Bromochloromethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.014Bromomethane 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 02/08/23 12:03 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 9 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 02/08/23 12:03 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 02/08/23 12:03 V29616TBL
<0.0006 mg/Kg - dry 0.0006 0.007
4-Chlorotoluene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 02/08/23 12:03 V29616TBL
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 02/08/23 12:03 V29616TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 02/08/23 12:03 V29616TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007
1,4-Dichlorobenzene 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.0071,2-Dichloroethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 02/08/23 12:03 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 10 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.073Ethyl Tertiary Butyl Ether (ETBE)1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.014
Hexachlorobutadiene 1 02/08/23 12:03 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.014n-Hexane 1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.0292-Hexanone 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 02/08/23 12:03 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.029Methyl Ethyl Ketone (MEK)1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 02/08/23 12:03 V29616TBL
<0.021 mg/Kg - dry 0.021 0.029
4-Methyl-2-Pentanone 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 02/08/23 12:03 V29616TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 02/08/23 12:03 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 11 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 02/08/23 12:03 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 02/08/23 12:03 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 02/08/23 12:03 V29616TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 02/08/23 12:03 V29616TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2,3-Trichloropropane 1 02/08/23 12:03 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 02/08/23 12:03 V29616TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 02/08/23 12:03 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 02/08/23 12:03 V29616
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%02/08/23 12:031 TBL V29616
Surrogate: Dibromofluoromethane 105 Limits: 84-123%02/08/23 12:031 TBL V29616
Surrogate: Toluene-d8 93.0 Limits: 76-129%02/08/23 12:031 TBL V29616
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.169 mg/Kg - dry 0.169 0.966Acenaphthene 1 02/10/23 13:52 V29677JMV
<0.153 mg/Kg - dry 0.153 0.966Acenaphthylene 1 02/10/23 13:52 V29677JMV
<0.222 mg/Kg - dry 0.222 0.966Aniline 1 02/10/23 13:52 V29677JMV
<0.209 mg/Kg - dry 0.209 0.966Anthracene 1 02/10/23 13:52 V29677JMV
<0.203 mg/Kg - dry 0.203 0.966Benzo(a)anthracene 1 02/10/23 13:52 V29677JMV
<0.215 mg/Kg - dry 0.215 0.966Benzo(a)pyrene 1 02/10/23 13:52 V29677JMV
<0.213 mg/Kg - dry 0.213 0.966Benzo(b)fluoranthene 1 02/10/23 13:52 V29677JMV
<0.199 mg/Kg - dry 0.199 0.966Benzo(g,h,i)perylene 1 02/10/23 13:52 V29677JMV
<0.200 mg/Kg - dry 0.200 0.966
Benzo(k)fluoranthene 1 02/10/23 13:52 V29677JMV
<0.849 M mg/Kg - dry 0.849 2.93Benzoic Acid 1 02/10/23 13:52 V29677JMV
<0.153 mg/Kg - dry 0.153 0.966Benzyl alcohol 1 02/10/23 13:52 V29677JMV
<0.172 mg/Kg - dry 0.172 0.966Bis(2-Chloroethoxy)methane 1 02/10/23 13:52 V29677JMV
<0.156 mg/Kg - dry 0.156 0.966Bis(2-Chloroethyl)ether 1 02/10/23 13:52 V29677JMV
<0.199 mg/Kg - dry 0.199 0.483Bis(2-Chloroisopropyl)ether 1 02/10/23 13:52 V29677JMV
<0.175 mg/Kg - dry 0.175 0.966Bis(2-ethylhexyl)phthalate 1 02/10/23 13:52 V29677JMV
<0.159 mg/Kg - dry 0.159 0.966
4-Bromophenyl phenyl ether 1 02/10/23 13:52 V29677JMV
<0.165 mg/Kg - dry 0.165 0.483Butyl benzyl phthalate 1 02/10/23 13:52 V29677JMV
<0.135 mg/Kg - dry 0.135 0.9664-Chloro-3-methylphenol 1 02/10/23 13:52 V29677JMV
<0.163 mg/Kg - dry 0.163 0.4834-Chloroaniline 1 02/10/23 13:52 V29677JMV
<0.169 mg/Kg - dry 0.169 0.9662-Chloronaphthalene 1 02/10/23 13:52 V29677JMV
<0.143 mg/Kg - dry 0.143 0.9662-Chlorophenol 1 02/10/23 13:52 V29677JMV
<0.184 mg/Kg - dry 0.184 1.464-Chlorophenyl phenyl ether 1 02/10/23 13:52 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.207 mg/Kg - dry 0.207 0.966Chrysene 1 02/10/23 13:52 V29677JMV
<0.336 mg/Kg - dry 0.336 0.966Dibenz(a,h)anthracene 1 02/10/23 13:52 V29677JMV
<0.174 mg/Kg - dry 0.174 0.966Dibenzofuran 1 02/10/23 13:52 V29677JMV
<0.138 mg/Kg - dry 0.138 0.9661,2-Dichlorobenzene 1 02/10/23 13:52 V29677JMV
<0.142 mg/Kg - dry 0.142 0.9661,3-Dichlorobenzene 1 02/10/23 13:52 V29677JMV
<0.142 mg/Kg - dry 0.142 0.4831,4-Dichlorobenzene 1 02/10/23 13:52 V29677JMV
<0.215 mg/Kg - dry 0.215 0.9663,3'-Dichlorobenzidine 1 02/10/23 13:52 V29677JMV
<0.140 mg/Kg - dry 0.140 0.9662,4-Dichlorophenol 1 02/10/23 13:52 V29677JMV
<0.263 mg/Kg - dry 0.263 0.966
Diethyl phthalate 1 02/10/23 13:52 V29677JMV
<0.254 mg/Kg - dry 0.254 0.966Dimethyl phthalate 1 02/10/23 13:52 V29677JMV
<0.158 mg/Kg - dry 0.158 0.4832,4-Dimethylphenol 1 02/10/23 13:52 V29677JMV
<0.156 mg/Kg - dry 0.156 0.966Di-n-butyl phthalate 1 02/10/23 13:52 V29677JMV
<0.351 mg/Kg - dry 0.351 2.204,6-Dinitro-2-methylphenol 1 02/10/23 13:52 V29677JMV
<0.761 mg/Kg - dry 0.761 2.202,4-Dinitrophenol 1 02/10/23 13:52 V29677JMV
<0.141 mg/Kg - dry 0.141 0.9662,4-Dinitrotoluene 1 02/10/23 13:52 V29677JMV
<0.158 mg/Kg - dry 0.158 0.966
2,6-Dinitrotoluene 1 02/10/23 13:52 V29677JMV
<0.209 mg/Kg - dry 0.209 0.483Di-n-Octyl Phthalate 1 02/10/23 13:52 V29677JMV
<0.180 mg/Kg - dry 0.180 0.966Fluoranthene 1 02/10/23 13:52 V29677JMV
<0.187 mg/Kg - dry 0.187 0.966Fluorene 1 02/10/23 13:52 V29677JMV
<0.155 mg/Kg - dry 0.155 0.966Hexachlorobenzene 1 02/10/23 13:52 V29677JMV
<0.142 mg/Kg - dry 0.142 0.966Hexachlorobutadiene 1 02/10/23 13:52 V29677JMV
<0.229 mg/Kg - dry 0.229 0.966Hexachlorocyclopentadiene 1 02/10/23 13:52 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.115 mg/Kg - dry 0.115 0.966Hexachloroethane 1 02/10/23 13:52 V29677JMV
<0.262 mg/Kg - dry 0.262 0.966Indeno(1,2,3-cd)pyrene 1 02/10/23 13:52 V29677JMV
<0.279 mg/Kg - dry 0.279 0.966Isophorone 1 02/10/23 13:52 V29677JMV
<0.155 mg/Kg - dry 0.155 0.9661-Methylnaphthalene 1 02/10/23 13:52 V29677JMV
<0.146 mg/Kg - dry 0.146 0.9662-Methylnaphthalene 1 02/10/23 13:52 V29677JMV
<0.142 mg/Kg - dry 0.142 0.9662-Methylphenol 1 02/10/23 13:52 V29677JMV
<0.124 mg/Kg - dry 0.124 0.9663&4 Methylphenol 1 02/10/23 13:52 V29677JMV
<0.210 mg/Kg - dry 0.210 0.966Naphthalene 1 02/10/23 13:52 V29677JMV
<0.141 mg/Kg - dry 0.141 0.966
2-Nitroaniline 1 02/10/23 13:52 V29677JMV
<0.175 mg/Kg - dry 0.175 0.9663-Nitroaniline 1 02/10/23 13:52 V29677JMV
<0.136 mg/Kg - dry 0.136 0.4834-Nitroaniline 1 02/10/23 13:52 V29677JMV
<0.169 mg/Kg - dry 0.169 0.483Nitrobenzene 1 02/10/23 13:52 V29677JMV
<0.130 mg/Kg - dry 0.130 0.9662-Nitrophenol 1 02/10/23 13:52 V29677JMV
<0.171 mg/Kg - dry 0.171 0.9664-Nitrophenol 1 02/10/23 13:52 V29677JMV
<0.385 mg/Kg - dry 0.385 0.966N-Nitrosodimethylamine 1 02/10/23 13:52 V29677JMV
<0.265 mg/Kg - dry 0.265 0.966
N-Nitrosodiphenylamine 1 02/10/23 13:52 V29677JMV
<0.172 mg/Kg - dry 0.172 0.966N-Nitroso-di-n-propylamine 1 02/10/23 13:52 V29677JMV
<0.508 mg/Kg - dry 0.508 1.46Pentachlorophenol 1 02/10/23 13:52 V29677JMV
<0.304 mg/Kg - dry 0.304 0.966Phenanthrene 1 02/10/23 13:52 V29677JMV
<0.163 mg/Kg - dry 0.163 0.966Phenol 1 02/10/23 13:52 V29677JMV
<0.196 mg/Kg - dry 0.196 0.966Pyrene 1 02/10/23 13:52 V29677JMV
<0.115 mg/Kg - dry 0.115 0.483Pyridine 1 02/10/23 13:52 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.156 mg/Kg - dry 0.156 0.9661,2,4-Trichlorobenzene 1 02/10/23 13:52 V29677JMV
<0.140 mg/Kg - dry 0.140 0.9662,4,5-Trichlorophenol 1 02/10/23 13:52 V29677JMV
<0.141 mg/Kg - dry 0.141 0.9662,4,6-Trichlorophenol 1 02/10/23 13:52 V29677JMV
8270ESurrogate: Phenol-d5 71.5 Limits: 34-121%02/10/23 13:521 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%02/10/23 13:521 JMV V29677
Surrogate: 2-Fluorophenol 74.5 Limits: 35-115%02/10/23 13:521 JMV V29677
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%02/10/23 13:521 JMV V29677
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%02/10/23 13:521 JMV V29677
Surrogate: 2,4,6-Tribromophenol 85.9 Limits: 39-132%02/10/23 13:521 JMV V29677
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:HA-1
99112 Matrix:
2/3/2023 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V29676 02/10/23 10:45
<13.5 mg/Kg - dry 13.5 73.2Aliphatic C9-C18 1 02/13/23 13:31 V29727AMP
<17.9 mg/Kg - dry 17.9 73.2Aliphatic C19-C36 1 02/13/23 13:31 V29727AMP
<20.8 mg/Kg - dry 20.8 73.2Aromatic C11-C22 1 02/13/23 13:31 V29727AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 111 Limits: 40-140%02/13/23 13:311 AMP
MADEP-EPHSurrogate: Chlorooctadecane 96.0 Limits: 40-140%02/13/23 13:311 AMP
MADEP-EPHSurrogate: OTP Surrogate 90.5 Limits: 40-140%02/13/23 13:311 AMP
Surrogate: 2-Fluorobiphenyl 112 Limits: 40-140%02/13/23 13:311 AMP V29727
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V29596 02/08/23 08:00
<1790 µg/Kg - dry 1790 11700
Aliphatic C5-C8 100 02/08/23 15:07 V29597TBL
<6680 µg/Kg - dry 6680 11700Aliphatic C9-C12 100 02/08/23 15:07 V29597TBL
<914 µg/Kg - dry 914 11700Aromatic C9-C10 100 02/08/23 15:07 V29597TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)98.2 Limits: 70-130%02/08/23 15:07100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)87.1 Limits: 70-130%02/08/23 15:07100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
34.4 %Moisture 1 02/08/23 17:05 SW-DRYWTAMB
75.6 mg/Kg - dry 0.359 0.381Chromium 1 02/11/23 01:06 6010DTJS
1.24 mg/Kg - dry 0.274 0.457Lead 1 02/11/23 01:06 6010DTJS
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V29704 02/13/23 09:45
<7.09 mg/Kg - dry 7.09 15.2Diesel Range Organics (C10-C28)1 02/13/23 19:34 V29729AMP
8015C DROSurrogate: OTP Surrogate 77.4 Limits: 31-123%02/13/23 19:341 AMP
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V29611 02/08/23 08:00
<3.16 mg/Kg - dry 3.16 7.62Gasoline Range Organics (C6-C10)50 02/08/23 13:18 V29612TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 142 *Limits: 50-137%02/08/23 13:1850 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V29735 02/13/23 15:40
<0.0028 mg/Kg - dry 0.0028 0.0076
Aldrin 1 02/17/23 18:22 V29928JMV
<0.0017 mg/Kg - dry 0.0017 0.0076alpha-BHC 1 02/17/23 18:22 V29928JMV
<0.0030 mg/Kg - dry 0.0030 0.0076beta-BHC 1 02/17/23 18:22 V29928JMV
<0.0019 mg/Kg - dry 0.0019 0.0076delta-BHC 1 02/17/23 18:22 V29928JMV
<0.0268 mg/Kg - dry 0.0268 0.0762Chlordane 1 02/17/23 18:22 V29928JMV
<0.0028 mg/Kg - dry 0.0028 0.0076alpha-Chlordane 1 02/17/23 18:22 V29928JMV
<0.0025 mg/Kg - dry 0.0025 0.0076gamma-Chlordane 1 02/17/23 18:22 V29928JMV
<0.0028 mg/Kg - dry 0.0028 0.0076
4,4'-DDD 1 02/17/23 18:22 V29928JMV
<0.0031 mg/Kg - dry 0.0031 0.00764,4'-DDE 1 02/17/23 18:22 V29928JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8081B Prep Batch(es):V29735 02/13/23 15:40
<0.0023 mg/Kg - dry 0.0023 0.00764,4'-DDT 1 02/17/23 18:22 V29928JMV
<0.0031 mg/Kg - dry 0.0031 0.0076Dieldrin 1 02/17/23 18:22 V29928JMV
<0.0027 mg/Kg - dry 0.0027 0.0076Endosulfan I 1 02/17/23 18:22 V29928JMV
<0.0026 mg/Kg - dry 0.0026 0.0076Endosulfan II 1 02/17/23 18:22 V29928JMV
<0.0027 mg/Kg - dry 0.0027 0.0076Endosulfan Sulfate 1 02/17/23 18:22 V29928JMV
<0.0029 mg/Kg - dry 0.0029 0.0076Endrin 1 02/17/23 18:22 V29928JMV
<0.0032 mg/Kg - dry 0.0032 0.0076Endrin Aldehyde 1 02/17/23 18:22 V29928JMV
<0.0028 mg/Kg - dry 0.0028 0.0076Endrin Ketone 1 02/17/23 18:22 V29928JMV
<0.0019 mg/Kg - dry 0.0019 0.0076
gamma-BHC 1 02/17/23 18:22 V29928JMV
<0.0020 mg/Kg - dry 0.0020 0.0076Heptachlor 1 02/17/23 18:22 V29928JMV
<0.0027 mg/Kg - dry 0.0027 0.0076Heptachlor Epoxide 1 02/17/23 18:22 V29928JMV
<0.0040 mg/Kg - dry 0.0040 0.0076Methoxychlor 1 02/17/23 18:22 V29928JMV
<0.0155 mg/Kg - dry 0.0155 0.0762Toxaphene 1 02/17/23 18:22 V29928JMV
Surrogate: Decachlorobiphenyl 76.9 Limits: 26-204%02/17/23 18:221 JMV V29928
Surrogate: Tetrachloro-m-xylene 83.8 Limits: 40-162%02/17/23 18:221 JMV V29928
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V29736 02/13/23 15:40
<0.0271 mg/Kg - dry 0.0271 0.0763Aroclor 1016 1 02/15/23 15:34 V29840JMV
<0.0609 mg/Kg - dry 0.0609 0.152Aroclor 1221 1 02/15/23 15:34 V29840JMV
<0.0198 mg/Kg - dry 0.0198 0.152Aroclor 1232 1 02/15/23 15:34 V29840JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8082A Prep Batch(es):V29736 02/13/23 15:40
<0.0202 mg/Kg - dry 0.0202 0.0763Aroclor 1242 1 02/15/23 15:34 V29840JMV
<0.0152 mg/Kg - dry 0.0152 0.0763Aroclor 1248 1 02/15/23 15:34 V29840JMV
<0.0189 mg/Kg - dry 0.0189 0.0763Aroclor 1254 1 02/15/23 15:34 V29840JMV
<0.0227 mg/Kg - dry 0.0227 0.0763Aroclor 1260 1 02/15/23 15:34 V29840JMV
8082ASurrogate: Decachlorobiphenyl 102 Limits: 34-182%02/15/23 15:341 JMV
8082ASurrogate: Tetrachloro-m-xylene 155 Limits: 36-182%02/15/23 15:341 JMV
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
0.006 J mg/Kg - dry 0.003 0.030Acetone 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.030Acrolein 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.030Acrylonitrile 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007Benzene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007Bromobenzene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007
Bromochloromethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.015Bromomethane 1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007sec-Butyl benzene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007tert-Butyl benzene 1 02/08/23 12:30 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.0010 mg/Kg - dry 0.0010 0.007Carbon Disulfide 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorobenzene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.015Chloroethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 02/08/23 12:30 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.015Chloromethane 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0072-Chlorotoluene 1 02/08/23 12:30 V29616TBL
<0.0006 mg/Kg - dry 0.0006 0.007
4-Chlorotoluene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.0151,2-Dibromo-3-Chloropropane 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007Dibromomethane 1 02/08/23 12:30 V29616TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 02/08/23 12:30 V29616TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007
1,4-Dichlorobenzene 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.015Dichlorodifluoromethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.0071,2-Dichloroethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 02/08/23 12:30 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2-Dichloropropane 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007Ethylbenzene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.076Ethyl Tertiary Butyl Ether (ETBE)1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.015
Hexachlorobutadiene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.015n-Hexane 1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.0302-Hexanone 1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 02/08/23 12:30 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.030Methyl Ethyl Ketone (MEK)1 02/08/23 12:30 V29616TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 02/08/23 12:30 V29616TBL
<0.022 mg/Kg - dry 0.022 0.030
4-Methyl-2-Pentanone 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.015Methylene Chloride 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.015Naphthalene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 02/08/23 12:30 V29616TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 02/08/23 12:30 V29616TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29615 02/08/23 08:00
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Toluene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0151,2,3-Trichlorobenzene 1 02/08/23 12:30 V29616TBL
<0.0010 mg/Kg - dry 0.0010 0.0151,2,4-Trichlorobenzene 1 02/08/23 12:30 V29616TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 02/08/23 12:30 V29616TBL
<0.003 mg/Kg - dry 0.003 0.015Trichlorofluoromethane 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2,3-Trichloropropane 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.015Vinyl Acetate 1 02/08/23 12:30 V29616TBL
<0.0007 mg/Kg - dry 0.0007 0.015Vinyl Chloride 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007o-Xylene 1 02/08/23 12:30 V29616TBL
<0.001 mg/Kg - dry 0.001 0.015m,p-Xylene 1 02/08/23 12:30 V29616TBL
<0.0008 mg/Kg - dry 0.0008 0.007Xylene (Total)1 02/08/23 12:30 V29616
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/08/23 12:301 TBL V29616
Surrogate: Dibromofluoromethane 104 Limits: 84-123%02/08/23 12:301 TBL V29616
Surrogate: Toluene-d8 91.2 Limits: 76-129%02/08/23 12:301 TBL V29616
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.176 mg/Kg - dry 0.176 1.01Acenaphthene 1 02/10/23 14:14 V29677JMV
<0.160 mg/Kg - dry 0.160 1.01Acenaphthylene 1 02/10/23 14:14 V29677JMV
<0.231 mg/Kg - dry 0.231 1.01Aniline 1 02/10/23 14:14 V29677JMV
<0.217 mg/Kg - dry 0.217 1.01Anthracene 1 02/10/23 14:14 V29677JMV
<0.211 mg/Kg - dry 0.211 1.01Benzo(a)anthracene 1 02/10/23 14:14 V29677JMV
<0.224 mg/Kg - dry 0.224 1.01Benzo(a)pyrene 1 02/10/23 14:14 V29677JMV
<0.222 mg/Kg - dry 0.222 1.01Benzo(b)fluoranthene 1 02/10/23 14:14 V29677JMV
<0.207 mg/Kg - dry 0.207 1.01Benzo(g,h,i)perylene 1 02/10/23 14:14 V29677JMV
<0.208 mg/Kg - dry 0.208 1.01
Benzo(k)fluoranthene 1 02/10/23 14:14 V29677JMV
<0.884 M mg/Kg - dry 0.884 3.05Benzoic Acid 1 02/10/23 14:14 V29677JMV
<0.160 mg/Kg - dry 0.160 1.01Benzyl alcohol 1 02/10/23 14:14 V29677JMV
<0.179 mg/Kg - dry 0.179 1.01Bis(2-Chloroethoxy)methane 1 02/10/23 14:14 V29677JMV
<0.163 mg/Kg - dry 0.163 1.01Bis(2-Chloroethyl)ether 1 02/10/23 14:14 V29677JMV
<0.207 mg/Kg - dry 0.207 0.503Bis(2-Chloroisopropyl)ether 1 02/10/23 14:14 V29677JMV
<0.182 mg/Kg - dry 0.182 1.01Bis(2-ethylhexyl)phthalate 1 02/10/23 14:14 V29677JMV
<0.166 mg/Kg - dry 0.166 1.01
4-Bromophenyl phenyl ether 1 02/10/23 14:14 V29677JMV
<0.172 mg/Kg - dry 0.172 0.503Butyl benzyl phthalate 1 02/10/23 14:14 V29677JMV
<0.140 mg/Kg - dry 0.140 1.014-Chloro-3-methylphenol 1 02/10/23 14:14 V29677JMV
<0.170 mg/Kg - dry 0.170 0.5034-Chloroaniline 1 02/10/23 14:14 V29677JMV
<0.176 mg/Kg - dry 0.176 1.012-Chloronaphthalene 1 02/10/23 14:14 V29677JMV
<0.149 mg/Kg - dry 0.149 1.012-Chlorophenol 1 02/10/23 14:14 V29677JMV
<0.192 mg/Kg - dry 0.192 1.524-Chlorophenyl phenyl ether 1 02/10/23 14:14 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.216 mg/Kg - dry 0.216 1.01Chrysene 1 02/10/23 14:14 V29677JMV
<0.350 mg/Kg - dry 0.350 1.01Dibenz(a,h)anthracene 1 02/10/23 14:14 V29677JMV
<0.181 mg/Kg - dry 0.181 1.01Dibenzofuran 1 02/10/23 14:14 V29677JMV
<0.143 mg/Kg - dry 0.143 1.011,2-Dichlorobenzene 1 02/10/23 14:14 V29677JMV
<0.148 mg/Kg - dry 0.148 1.011,3-Dichlorobenzene 1 02/10/23 14:14 V29677JMV
<0.148 mg/Kg - dry 0.148 0.5031,4-Dichlorobenzene 1 02/10/23 14:14 V29677JMV
<0.224 mg/Kg - dry 0.224 1.013,3'-Dichlorobenzidine 1 02/10/23 14:14 V29677JMV
<0.146 mg/Kg - dry 0.146 1.012,4-Dichlorophenol 1 02/10/23 14:14 V29677JMV
<0.274 mg/Kg - dry 0.274 1.01
Diethyl phthalate 1 02/10/23 14:14 V29677JMV
<0.265 mg/Kg - dry 0.265 1.01Dimethyl phthalate 1 02/10/23 14:14 V29677JMV
<0.164 mg/Kg - dry 0.164 0.5032,4-Dimethylphenol 1 02/10/23 14:14 V29677JMV
<0.163 mg/Kg - dry 0.163 1.01Di-n-butyl phthalate 1 02/10/23 14:14 V29677JMV
<0.365 mg/Kg - dry 0.365 2.294,6-Dinitro-2-methylphenol 1 02/10/23 14:14 V29677JMV
<0.792 mg/Kg - dry 0.792 2.292,4-Dinitrophenol 1 02/10/23 14:14 V29677JMV
<0.147 mg/Kg - dry 0.147 1.012,4-Dinitrotoluene 1 02/10/23 14:14 V29677JMV
<0.164 mg/Kg - dry 0.164 1.01
2,6-Dinitrotoluene 1 02/10/23 14:14 V29677JMV
<0.217 mg/Kg - dry 0.217 0.503Di-n-Octyl Phthalate 1 02/10/23 14:14 V29677JMV
<0.187 mg/Kg - dry 0.187 1.01Fluoranthene 1 02/10/23 14:14 V29677JMV
<0.195 mg/Kg - dry 0.195 1.01Fluorene 1 02/10/23 14:14 V29677JMV
<0.161 mg/Kg - dry 0.161 1.01Hexachlorobenzene 1 02/10/23 14:14 V29677JMV
<0.148 mg/Kg - dry 0.148 1.01Hexachlorobutadiene 1 02/10/23 14:14 V29677JMV
<0.239 mg/Kg - dry 0.239 1.01Hexachlorocyclopentadiene 1 02/10/23 14:14 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.120 mg/Kg - dry 0.120 1.01Hexachloroethane 1 02/10/23 14:14 V29677JMV
<0.272 mg/Kg - dry 0.272 1.01Indeno(1,2,3-cd)pyrene 1 02/10/23 14:14 V29677JMV
<0.291 mg/Kg - dry 0.291 1.01Isophorone 1 02/10/23 14:14 V29677JMV
<0.161 mg/Kg - dry 0.161 1.011-Methylnaphthalene 1 02/10/23 14:14 V29677JMV
<0.152 mg/Kg - dry 0.152 1.012-Methylnaphthalene 1 02/10/23 14:14 V29677JMV
<0.147 mg/Kg - dry 0.147 1.012-Methylphenol 1 02/10/23 14:14 V29677JMV
<0.129 mg/Kg - dry 0.129 1.013&4 Methylphenol 1 02/10/23 14:14 V29677JMV
<0.219 mg/Kg - dry 0.219 1.01Naphthalene 1 02/10/23 14:14 V29677JMV
<0.147 mg/Kg - dry 0.147 1.01
2-Nitroaniline 1 02/10/23 14:14 V29677JMV
<0.182 mg/Kg - dry 0.182 1.013-Nitroaniline 1 02/10/23 14:14 V29677JMV
<0.142 mg/Kg - dry 0.142 0.5034-Nitroaniline 1 02/10/23 14:14 V29677JMV
<0.176 mg/Kg - dry 0.176 0.503Nitrobenzene 1 02/10/23 14:14 V29677JMV
<0.135 mg/Kg - dry 0.135 1.012-Nitrophenol 1 02/10/23 14:14 V29677JMV
<0.178 mg/Kg - dry 0.178 1.014-Nitrophenol 1 02/10/23 14:14 V29677JMV
<0.400 mg/Kg - dry 0.400 1.01N-Nitrosodimethylamine 1 02/10/23 14:14 V29677JMV
<0.275 mg/Kg - dry 0.275 1.01
N-Nitrosodiphenylamine 1 02/10/23 14:14 V29677JMV
<0.179 mg/Kg - dry 0.179 1.01N-Nitroso-di-n-propylamine 1 02/10/23 14:14 V29677JMV
<0.528 mg/Kg - dry 0.528 1.52Pentachlorophenol 1 02/10/23 14:14 V29677JMV
<0.317 mg/Kg - dry 0.317 1.01Phenanthrene 1 02/10/23 14:14 V29677JMV
<0.170 mg/Kg - dry 0.170 1.01Phenol 1 02/10/23 14:14 V29677JMV
<0.204 mg/Kg - dry 0.204 1.01Pyrene 1 02/10/23 14:14 V29677JMV
<0.120 mg/Kg - dry 0.120 0.503Pyridine 1 02/10/23 14:14 V29677JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V29651 02/10/23 11:00
<0.163 mg/Kg - dry 0.163 1.011,2,4-Trichlorobenzene 1 02/10/23 14:14 V29677JMV
<0.146 mg/Kg - dry 0.146 1.012,4,5-Trichlorophenol 1 02/10/23 14:14 V29677JMV
<0.147 mg/Kg - dry 0.147 1.012,4,6-Trichlorophenol 1 02/10/23 14:14 V29677JMV
8270ESurrogate: Phenol-d5 73.9 Limits: 34-121%02/10/23 14:141 JMV
Surrogate: 2-Fluorobiphenyl 90.4 Limits: 44-115%02/10/23 14:141 JMV V29677
Surrogate: 2-Fluorophenol 76.9 Limits: 35-115%02/10/23 14:141 JMV V29677
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%02/10/23 14:141 JMV V29677
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%02/10/23 14:141 JMV V29677
Surrogate: 2,4,6-Tribromophenol 85.6 Limits: 39-132%02/10/23 14:141 JMV V29677
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27610
23-038-0021
01139
Mid-Atlantic Associates, Inc. - Raleigh
409 Rogers View Court
Kevin Clay
Raleigh
Received : 02/07/2023
2500 E. Market St.
Report Date : 02/20/2023
Sample ID :
Lab No :
Sampled:Stockpile
99117 Matrix:
2/3/2023 12:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V29676 02/10/23 10:45
<14.1 mg/Kg - dry 14.1 76.4Aliphatic C9-C18 1 02/13/23 14:07 V29727AMP
<18.6 mg/Kg - dry 18.6 76.4Aliphatic C19-C36 1 02/13/23 14:07 V29727AMP
<21.6 mg/Kg - dry 21.6 76.4Aromatic C11-C22 1 02/13/23 14:07 V29727AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 97.5 Limits: 40-140%02/13/23 14:071 AMP
MADEP-EPHSurrogate: Chlorooctadecane 92.5 Limits: 40-140%02/13/23 14:071 AMP
MADEP-EPHSurrogate: OTP Surrogate 83.5 Limits: 40-140%02/13/23 14:071 AMP
Surrogate: 2-Fluorobiphenyl 101 Limits: 40-140%02/13/23 14:071 AMP V29727
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V29596 02/08/23 08:00
<1860 µg/Kg - dry 1860 12200
Aliphatic C5-C8 100 02/08/23 15:31 V29597TBL
<6950 µg/Kg - dry 6950 12200Aliphatic C9-C12 100 02/08/23 15:31 V29597TBL
<951 µg/Kg - dry 951 12200Aromatic C9-C10 100 02/08/23 15:31 V29597TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.4 Limits: 70-130%02/08/23 15:31100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)81.7 Limits: 70-130%02/08/23 15:31100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Metals Analysis
6010D
L663515,L663862QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L663017
Associated Lab Samples: 99112, 99117
LRB-L663017 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/10/23 23:420.2500.236<0.236mg/KgChromium
02/10/23 23:420.3000.180<0.180mg/KgLead
LCS-L663017Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10653.250.0mg/KgChromium 80-120
1015.075.00mg/KgLead 80-120
L 83951-MS-L663017 L 83951-MSD-L663017Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
62.6 98.067.947.145.318.3mg/KgChromium 105 75-125 8.1 20
25.1 10227.14.714.5320.5mg/KgLead 140*75-125 7.6 20
L 83951-PDS-L663017Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/13/23 22:04100106mg/KgChromium
02/13/23 22:0496.012.0mg/KgLead
Page 1 of 22* QC Fail Date:02/20/2023 03:23 PM
Page 30 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V29729QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29704
Associated Lab Samples: 99112, 99117
LRB-V29704 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/13/23 13:3310.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
02/13/23 13:33OTP Surrogate (S)79.6 31-123
LCS-V29704Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10771.366.7mg/KgDiesel Range Organics (C10-C28)46-126
78.1OTP Surrogate (S)31-123
V 99034-MS-V29704 V 99034-MSD-V29704Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
71.6 10771.966.666.8<4.65mg/KgDiesel Range Organics (C10-C28)108 50-117 0.4 24
76.1OTP Surrogate (S)74.0 31-123
Page 2 of 22Date:02/20/2023 03:23 PM
Page 31 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V29612QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V29611
Associated Lab Samples: 99112, 99117
LRB-V29611 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/23 12:215.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
02/08/23 12:21a,a,a-Trifluorotoluene (S)118 50-137
LCS-V29611Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
13567.350.0mg/KgGasoline Range Organics (C6-C10)41-138
110a,a,a-Trifluorotoluene (S)50-137
V 99112-MS-V29611 V 99112-MSD-V29611Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
54.3 10946.950.050.0<2.07mg/KgGasoline Range Organics (C6-C10)93.8 41-138 14.6 34
134a,a,a-Trifluorotoluene (S)113 50-137
Page 3 of 22Date:02/20/2023 03:23 PM
Page 32 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29928QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29735
Associated Lab Samples: 99112, 99117
LRB-V29735 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/17/23 17:010.00500.0018<0.0018mg/KgAldrin
02/17/23 17:010.00500.0011<0.0011mg/Kgalpha-BHC
02/17/23 17:010.00500.0019<0.0019mg/Kgbeta-BHC
02/17/23 17:010.00500.0012<0.0012mg/Kgdelta-BHC
02/17/23 17:010.05000.0176<0.0176mg/KgChlordane
02/17/23 17:010.00500.0018<0.0018mg/Kgalpha-Chlordane
02/17/23 17:010.00500.0016<0.0016mg/Kggamma-Chlordane
02/17/23 17:010.00500.0018<0.0018mg/Kg4,4'-DDD
02/17/23 17:010.00500.0020<0.0020mg/Kg4,4'-DDE
02/17/23 17:010.00500.0015<0.0015mg/Kg4,4'-DDT
02/17/23 17:010.00500.0020<0.0020mg/KgDieldrin
02/17/23 17:010.00500.0017<0.0017mg/KgEndosulfan I
02/17/23 17:010.00500.0017<0.0017mg/KgEndosulfan II
02/17/23 17:010.00500.0018<0.0018mg/KgEndosulfan Sulfate
02/17/23 17:010.00500.0019<0.0019mg/KgEndrin
02/17/23 17:010.00500.0021<0.0021mg/KgEndrin Aldehyde
02/17/23 17:010.00500.0018<0.0018mg/KgEndrin Ketone
02/17/23 17:010.00500.0012<0.0012mg/Kggamma-BHC
02/17/23 17:010.00500.0013<0.0013mg/KgHeptachlor
02/17/23 17:010.00500.0017<0.0017mg/KgHeptachlor Epoxide
02/17/23 17:010.00500.0026<0.0026mg/KgMethoxychlor
02/17/23 17:010.05000.0102<0.0102mg/KgToxaphene
02/17/23 17:01Decachlorobiphenyl (S)84.0 26-204
02/17/23 17:01Tetrachloro-m-xylene (S)87.9 40-162
Page 4 of 22Date:02/20/2023 03:23 PM
Page 33 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29928QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29735
LCS-V29735Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.20.2940.333mg/KgChlordane 43-149
93.30.3110.333mg/KgToxaphene 33-141
LCS-V29735 LCSD-V29735Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.0303 90.984.00.02800.0333mg/KgAldrin 45-136 7.8 20
0.0297 89.183.10.02770.0333mg/Kgalpha-BHC 45-137 6.9 20
0.0300 90.084.90.02830.0333mg/Kgbeta-BHC 50-136 5.8 20
0.0243 72.966.90.02230.0333mg/Kgdelta-BHC 47-139 8.5 20
0.0297 89.183.10.02770.0333mg/Kgalpha-Chlordane 54-133 6.9 20
0.0247 74.172.00.02400.0333mg/Kggamma-Chlordane 53-135 2.8 20
0.0300 90.084.00.02800.0333mg/Kg4,4'-DDD 56-139 6.8 20
0.0310 93.087.00.02900.0333mg/Kg4,4'-DDE 56-134 6.6 20
0.0333 10093.00.03100.0333mg/Kg4,4'-DDT 50-145 7.1 20
0.0313 93.987.90.02930.0333mg/KgDieldrin 56-136 6.6 20
0.0310 93.087.00.02900.0333mg/KgEndosulfan I 53-132 6.6 20
0.0313 93.987.00.02900.0333mg/KgEndosulfan II 53-134 7.6 20
0.0287 86.180.10.02670.0333mg/KgEndosulfan Sulfate 55-136 7.2 20
0.0317 95.187.00.02900.0333mg/KgEndrin 57-140 8.8 20
0.0283 84.978.90.02630.0333mg/KgEndrin Aldehyde 35-137 7.3 20
0.0303 90.986.10.02870.0333mg/KgEndrin Ketone 55-136 5.4 20
0.0310 93.086.10.02870.0333mg/Kggamma-BHC 49-135 7.7 20
0.0310 93.087.00.02900.0333mg/KgHeptachlor 47-136 6.6 20
0.0307 92.186.10.02870.0333mg/KgHeptachlor Epoxide 52-136 6.7 20
0.0287 86.181.90.02730.0333mg/KgMethoxychlor 52-143 5.0 20
Page 5 of 22Date:02/20/2023 03:23 PM
Page 34 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Organochlorine Pesticides by GC
8081B
V29928QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29735
LCS-V29735 LCSD-V29735Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
81.078.0Decachlorobiphenyl (S)26-204
87.983.1Tetrachloro-m-xylene (S)40-162
Page 6 of 22Date:02/20/2023 03:23 PM
Page 35 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Polychlorinated Biphenyls (PCB's)
8082A
V29840QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29736
Associated Lab Samples: 99112, 99117
LRB-V29736 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/15/23 11:410.05000.0178<0.0178mg/KgAroclor 1016
02/15/23 11:410.1000.0400<0.0400mg/KgAroclor 1221
02/15/23 11:410.1000.0130<0.0130mg/KgAroclor 1232
02/15/23 11:410.05000.0133<0.0133mg/KgAroclor 1242
02/15/23 11:410.05000.0100<0.0100mg/KgAroclor 1248
02/15/23 11:410.05000.0124<0.0124mg/KgAroclor 1254
02/15/23 11:410.05000.0149<0.0149mg/KgAroclor 1260
02/15/23 11:41Decachlorobiphenyl (S)111 34-182
02/15/23 11:41Tetrachloro-m-xylene (S)145 36-182
LCS-V29736 LCSD-V29736Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.487 1461480.4920.333mg/KgAroclor 1016 64-151 1.0 50
0.397 1191200.3990.333mg/KgAroclor 1260 45-166 0.5 50
109104Decachlorobiphenyl (S)34-182
154148Tetrachloro-m-xylene (S)36-182
Page 7 of 22Date:02/20/2023 03:23 PM
Page 36 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
Associated Lab Samples: 99112, 99117
LRB-V29615 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/23 11:360.0200.002<0.002mg/KgAcetone
02/08/23 11:360.0200.001<0.001mg/KgAcrolein
02/08/23 11:360.0200.0008<0.0008mg/KgAcrylonitrile
02/08/23 11:360.0050.0006<0.0006mg/KgBenzene
02/08/23 11:360.0050.0005<0.0005mg/KgBromobenzene
02/08/23 11:360.0050.0008<0.0008mg/KgBromochloromethane
02/08/23 11:360.0050.001<0.001mg/KgBromodichloromethane
02/08/23 11:360.0050.001<0.001mg/KgBromoform
02/08/23 11:360.0100.001<0.001mg/KgBromomethane
02/08/23 11:360.0050.0005<0.0005mg/Kgn-Butylbenzene
02/08/23 11:360.0050.0006<0.0006mg/Kgsec-Butyl benzene
02/08/23 11:360.0050.0005<0.0005mg/Kgtert-Butyl benzene
02/08/23 11:360.0050.0006<0.0006mg/KgCarbon Disulfide
02/08/23 11:360.0050.001<0.001mg/KgCarbon Tetrachloride
02/08/23 11:360.0050.0007<0.0007mg/KgChlorobenzene
02/08/23 11:360.0050.0009<0.0009mg/KgChlorodibromomethane
02/08/23 11:360.0100.0009<0.0009mg/KgChloroethane
02/08/23 11:360.0050.001<0.001mg/KgChloroform
02/08/23 11:360.0100.0006<0.0006mg/KgChloromethane
02/08/23 11:360.0050.0005<0.0005mg/Kg2-Chlorotoluene
02/08/23 11:360.0050.0004<0.0004mg/Kg4-Chlorotoluene
02/08/23 11:360.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
02/08/23 11:360.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
02/08/23 11:360.0050.0006<0.0006mg/Kg1,2-Dibromoethane
02/08/23 11:360.0050.0006<0.0006mg/KgDibromomethane
02/08/23 11:360.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
02/08/23 11:360.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 8 of 22Date:02/20/2023 03:23 PM
Page 37 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
Associated Lab Samples: 99112, 99117
LRB-V29615 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/23 11:360.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
02/08/23 11:360.0100.001<0.001mg/KgDichlorodifluoromethane
02/08/23 11:360.0050.0008<0.0008mg/Kg1,1-Dichloroethane
02/08/23 11:360.0050.001<0.001mg/Kg1,2-Dichloroethane
02/08/23 11:360.0050.0007<0.0007mg/Kg1,1-Dichloroethene
02/08/23 11:360.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
02/08/23 11:360.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
02/08/23 11:360.0050.0004<0.0004mg/Kg1,2-Dichloropropane
02/08/23 11:360.0050.0006<0.0006mg/Kg1,3-Dichloropropane
02/08/23 11:360.0050.001<0.001mg/Kg2,2-Dichloropropane
02/08/23 11:360.0050.0008<0.0008mg/Kg1,1-Dichloropropene
02/08/23 11:360.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
02/08/23 11:360.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
02/08/23 11:360.0050.0006<0.0006mg/KgEthylbenzene
02/08/23 11:360.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
02/08/23 11:360.0100.0008<0.0008mg/KgHexachlorobutadiene
02/08/23 11:360.0100.0007<0.0007mg/Kgn-Hexane
02/08/23 11:360.0200.0006<0.0006mg/Kg2-Hexanone
02/08/23 11:360.0050.0005<0.0005mg/KgIsopropylbenzene
02/08/23 11:360.0050.001<0.001mg/Kg4-Isopropyl toluene
02/08/23 11:360.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
02/08/23 11:360.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
02/08/23 11:360.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
02/08/23 11:360.0100.001<0.001mg/KgMethylene Chloride
02/08/23 11:360.0100.0010<0.0010mg/KgNaphthalene
02/08/23 11:360.0050.0005<0.0005mg/Kgn-Propylbenzene
02/08/23 11:360.0050.001<0.001mg/KgStyrene
Page 9 of 22Date:02/20/2023 03:23 PM
Page 38 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
Associated Lab Samples: 99112, 99117
LRB-V29615 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/23 11:360.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
02/08/23 11:360.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
02/08/23 11:360.0050.0009<0.0009mg/KgTetrachloroethene
02/08/23 11:360.0050.0007<0.0007mg/KgToluene
02/08/23 11:360.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
02/08/23 11:360.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
02/08/23 11:360.0050.001<0.001mg/Kg1,1,1-Trichloroethane
02/08/23 11:360.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
02/08/23 11:360.0050.0009<0.0009mg/KgTrichloroethene
02/08/23 11:360.0100.002<0.002mg/KgTrichlorofluoromethane
02/08/23 11:360.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
02/08/23 11:360.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
02/08/23 11:360.0100.0005<0.0005mg/KgVinyl Acetate
02/08/23 11:360.0100.0005<0.0005mg/KgVinyl Chloride
02/08/23 11:360.0050.0005<0.0005mg/Kgo-Xylene
02/08/23 11:360.0100.001<0.001mg/Kgm,p-Xylene
02/08/23 11:364-Bromofluorobenzene (S)101 70-130
02/08/23 11:36Dibromofluoromethane (S)99.2 84-123
02/08/23 11:36Toluene-d8 (S)93.6 76-129
LCS-V29615 LCSD-V29615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101070.1070.100mg/KgAcetone 29-198 2.7 20
0.085 85.496.00.0960.100mg/KgAcrolein 70-130 11.6 20
0.110 1101110.1110.100mg/KgAcrylonitrile 65-134 0.9 20
Page 10 of 22Date:02/20/2023 03:23 PM
Page 39 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
LCS-V29615 LCSD-V29615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1051050.0520.050mg/KgBenzene 74-127 0.5 20
0.042 85.885.20.0420.050mg/KgBromobenzene 73-125 0.7 20
0.055 1111070.0530.050mg/KgBromochloromethane 72-134 2.9 20
0.054 1091050.0520.050mg/KgBromodichloromethane 75-122 3.5 20
0.049 98.61020.0500.050mg/KgBromoform 66-135 2.9 20
0.055 1121090.0540.050mg/KgBromomethane 20-180 2.5 20
0.044 88.292.60.0460.050mg/Kgn-Butylbenzene 65-135 4.8 20
0.041 83.287.20.0430.050mg/Kgsec-Butyl benzene 66-131 4.6 20
0.042 84.890.40.0450.050mg/Kgtert-Butyl benzene 67-132 6.3 20
0.050 1001020.0510.050mg/KgCarbon Disulfide 61-129 1.7 20
0.051 1041110.0550.050mg/KgCarbon Tetrachloride 64-143 6.3 20
0.048 96.494.80.0470.050mg/KgChlorobenzene 74-118 1.6 20
0.048 96.097.80.0480.050mg/KgChlorodibromomethane 73-122 1.8 20
0.047 94.893.40.0460.050mg/KgChloroethane 33-149 1.4 20
0.049 99.699.00.0490.050mg/KgChloroform 73-127 0.6 20
0.055 1111040.0510.050mg/KgChloromethane 45-143 7.0 20
0.041 83.286.60.0430.050mg/Kg2-Chlorotoluene 67-124 4.0 20
0.041 83.286.80.0430.050mg/Kg4-Chlorotoluene 71-126 4.2 20
0.051 1031000.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.1 20
0.048 97.094.60.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.5 20
0.047 94.497.40.0480.050mg/Kg1,2-Dibromoethane 70-132 3.1 20
0.050 1011030.0510.050mg/KgDibromomethane 74-133 1.9 20
0.045 91.890.20.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.7 20
0.043 87.290.80.0450.050mg/Kg1,3-Dichlorobenzene 71-120 4.0 20
0.043 86.285.60.0420.050mg/Kg1,4-Dichlorobenzene 71-123 0.6 20
0.044 88.693.00.0460.050mg/KgDichlorodifluoromethane 26-146 4.8 20
Page 11 of 22Date:02/20/2023 03:23 PM
Page 40 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
LCS-V29615 LCSD-V29615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.499.40.0490.050mg/Kg1,1-Dichloroethane 74-127 0.0 20
0.050 1011020.0500.050mg/Kg1,2-Dichloroethane 68-128 0.9 20
0.049 99.41020.0510.050mg/Kg1,1-Dichloroethene 67-149 2.7 20
0.050 10097.00.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 3.2 20
0.050 1001010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 0.5 20
0.052 1041020.0510.050mg/Kg1,2-Dichloropropane 73-130 1.9 20
0.050 10099.20.0490.050mg/Kg1,3-Dichloropropane 75-124 1.0 20
0.049 98.61010.0500.050mg/Kg2,2-Dichloropropane 50-142 2.2 20
0.050 1001070.0530.050mg/Kg1,1-Dichloropropene 71-130 6.9 20
0.053 1081040.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 3.7 20
0.056 1131090.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.4 20
0.043 87.892.00.0460.050mg/KgEthylbenzene 74-128 4.6 20
0.102 1021010.1010.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.041 83.689.20.0440.050mg/KgHexachlorobutadiene 64-125 6.4 20
0.054 1101090.0540.050mg/Kgn-Hexane 70-130 0.1 20
0.045 90.098.60.0490.050mg/Kg2-Hexanone 61-157 9.1 20
0.042 84.888.40.0440.050mg/KgIsopropylbenzene 68-126 4.1 20
0.042 85.689.80.0440.050mg/Kg4-Isopropyl toluene 68-129 4.7 20
0.052 1051130.0560.050mg/KgMethyl Ethyl Ketone (MEK)63-149 7.1 20
0.052 1051040.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.9 20
0.053 1061060.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 0.3 20
0.047 95.096.00.0480.050mg/KgMethylene Chloride 74-129 1.0 20
0.042 85.285.00.0420.050mg/KgNaphthalene 57-157 0.2 20
0.041 83.488.80.0440.050mg/Kgn-Propylbenzene 67-130 6.2 20
0.048 96.696.20.0480.050mg/KgStyrene 77-121 0.4 20
0.044 89.891.60.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.9 20
Page 12 of 22Date:02/20/2023 03:23 PM
Page 41 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29616QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29615
LCS-V29615 LCSD-V29615Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.083.80.0410.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.4 20
0.048 97.41020.0510.050mg/KgTetrachloroethene 68-130 5.0 20
0.050 1011000.0500.050mg/KgToluene 71-129 1.1 20
0.043 87.685.40.0420.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.5 20
0.046 93.690.60.0450.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.2 20
0.047 95.61010.0500.050mg/Kg1,1,1-Trichloroethane 67-131 5.0 20
0.049 98.094.20.0470.050mg/Kg1,1,2-Trichloroethane 70-133 3.9 20
0.048 97.81020.0510.050mg/KgTrichloroethene 75-133 4.5 20
0.043 87.692.80.0460.050mg/KgTrichlorofluoromethane 44-146 5.7 20
0.044 88.689.40.0440.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.043 87.888.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.4 20
0.047 94.887.20.0430.050mg/KgVinyl Acetate 60-140 8.3 20
0.046 92.896.80.0480.050mg/KgVinyl Chloride 48-147 4.2 20
0.046 92.092.40.0460.050mg/Kgo-Xylene 74-126 0.4 20
0.091 91.393.30.0930.100mg/Kgm,p-Xylene 75-124 2.1 20
99.41014-Bromofluorobenzene (S)70-130
108104Dibromofluoromethane (S)84-123
96.093.4Toluene-d8 (S)76-129
Page 13 of 22Date:02/20/2023 03:23 PM
Page 42 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
Associated Lab Samples: 99112, 99117
LRB-V29651 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/23 10:290.6600.116<0.116mg/KgAcenaphthene
02/10/23 10:290.6600.105<0.105mg/KgAcenaphthylene
02/10/23 10:290.6600.152<0.152mg/KgAniline
02/10/23 10:290.6600.143<0.143mg/KgAnthracene
02/10/23 10:290.6600.139<0.139mg/KgBenzo(a)anthracene
02/10/23 10:290.6600.147<0.147mg/KgBenzo(a)pyrene
02/10/23 10:290.6600.146<0.146mg/KgBenzo(b)fluoranthene
02/10/23 10:290.6600.136<0.136mg/KgBenzo(g,h,i)perylene
02/10/23 10:290.6600.137<0.137mg/KgBenzo(k)fluoranthene
02/10/23 10:292.000.580<0.580mg/KgBenzoic Acid
02/10/23 10:290.6600.105<0.105mg/KgBenzyl alcohol
02/10/23 10:290.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
02/10/23 10:290.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
02/10/23 10:290.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
02/10/23 10:290.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
02/10/23 10:290.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
02/10/23 10:290.3300.113<0.113mg/KgButyl benzyl phthalate
02/10/23 10:290.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
02/10/23 10:290.3300.112<0.112mg/Kg4-Chloroaniline
02/10/23 10:290.6600.116<0.116mg/Kg2-Chloronaphthalene
02/10/23 10:290.6600.098<0.098mg/Kg2-Chlorophenol
02/10/23 10:291.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
02/10/23 10:290.6600.142<0.142mg/KgChrysene
02/10/23 10:290.6600.230<0.230mg/KgDibenz(a,h)anthracene
02/10/23 10:290.6600.119<0.119mg/KgDibenzofuran
02/10/23 10:290.6600.094<0.094mg/Kg1,2-Dichlorobenzene
02/10/23 10:290.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 14 of 22Date:02/20/2023 03:23 PM
Page 43 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
Associated Lab Samples: 99112, 99117
LRB-V29651 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/23 10:290.3300.097<0.097mg/Kg1,4-Dichlorobenzene
02/10/23 10:290.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
02/10/23 10:290.6600.095<0.095mg/Kg2,4-Dichlorophenol
02/10/23 10:290.6600.180<0.180mg/KgDiethyl phthalate
02/10/23 10:290.6600.174<0.174mg/KgDimethyl phthalate
02/10/23 10:290.3300.108<0.108mg/Kg2,4-Dimethylphenol
02/10/23 10:290.6600.107<0.107mg/KgDi-n-butyl phthalate
02/10/23 10:291.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
02/10/23 10:291.500.520<0.520mg/Kg2,4-Dinitrophenol
02/10/23 10:290.6600.096<0.096mg/Kg2,4-Dinitrotoluene
02/10/23 10:290.6600.108<0.108mg/Kg2,6-Dinitrotoluene
02/10/23 10:290.3300.143<0.143mg/KgDi-n-Octyl Phthalate
02/10/23 10:290.6600.123<0.123mg/KgFluoranthene
02/10/23 10:290.6600.128<0.128mg/KgFluorene
02/10/23 10:290.6600.106<0.106mg/KgHexachlorobenzene
02/10/23 10:290.6600.097<0.097mg/KgHexachlorobutadiene
02/10/23 10:290.6600.157<0.157mg/KgHexachlorocyclopentadiene
02/10/23 10:290.6600.079<0.079mg/KgHexachloroethane
02/10/23 10:290.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
02/10/23 10:290.6600.191<0.191mg/KgIsophorone
02/10/23 10:290.6600.106<0.106mg/Kg1-Methylnaphthalene
02/10/23 10:290.6600.100<0.100mg/Kg2-Methylnaphthalene
02/10/23 10:290.6600.097<0.097mg/Kg2-Methylphenol
02/10/23 10:290.6600.084<0.084mg/Kg3&4 Methylphenol
02/10/23 10:290.6600.144<0.144mg/KgNaphthalene
02/10/23 10:290.6600.096<0.096mg/Kg2-Nitroaniline
02/10/23 10:290.6600.120<0.120mg/Kg3-Nitroaniline
Page 15 of 22Date:02/20/2023 03:23 PM
Page 44 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
Associated Lab Samples: 99112, 99117
LRB-V29651 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/10/23 10:290.3300.093<0.093mg/Kg4-Nitroaniline
02/10/23 10:290.3300.116<0.116mg/KgNitrobenzene
02/10/23 10:290.6600.088<0.088mg/Kg2-Nitrophenol
02/10/23 10:290.6600.117<0.117mg/Kg4-Nitrophenol
02/10/23 10:290.6600.263<0.263mg/KgN-Nitrosodimethylamine
02/10/23 10:290.6600.181<0.181mg/KgN-Nitrosodiphenylamine
02/10/23 10:290.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
02/10/23 10:291.000.347<0.347mg/KgPentachlorophenol
02/10/23 10:290.6600.208<0.208mg/KgPhenanthrene
02/10/23 10:290.6600.112<0.112mg/KgPhenol
02/10/23 10:290.6600.134<0.134mg/KgPyrene
02/10/23 10:290.3300.079<0.079mg/KgPyridine
02/10/23 10:290.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
02/10/23 10:290.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
02/10/23 10:290.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
02/10/23 10:292-Fluorobiphenyl (S)91.0 44-115
02/10/23 10:292-Fluorophenol (S)82.2 35-115
02/10/23 10:29Nitrobenzene-d5 (S)80.8 37-122
02/10/23 10:294-Terphenyl-d14 (S)103 54-127
02/10/23 10:292,4,6-Tribromophenol (S)83.4 39-132
02/10/23 10:29Phenol-d5 (S)78.0 34-121
LCS-V29651 LCSD-V29651Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.38 82.684.41.411.67mg/KgAcenaphthene 40-123 2.1 20
Page 16 of 22Date:02/20/2023 03:23 PM
Page 45 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
LCS-V29651 LCSD-V29651Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.39 83.283.81.401.67mg/KgAcenaphthylene 32-132 0.7 20
2.37 1421412.351.67mg/KgAniline 12-197 0.8 20
1.54 92.290.41.511.67mg/KgAnthracene 47-123 1.9 20
1.54 92.291.01.521.67mg/KgBenzo(a)anthracene 49-126 1.3 20
1.44 86.285.61.431.67mg/KgBenzo(a)pyrene 45-129 0.6 20
1.37 82.082.01.371.67mg/KgBenzo(b)fluoranthene 45-132 0.0 20
1.26 75.476.01.271.67mg/KgBenzo(g,h,i)perylene 43-134 0.7 20
1.33 79.677.81.301.67mg/KgBenzo(k)fluoranthene 47-132 2.2 20
0.610 36.50.0*<0.5801.67mg/KgBenzoic Acid 10-83 5.0 20
1.49 89.285.61.431.67mg/KgBenzyl alcohol 29-122 4.1 20
1.26 75.474.81.251.67mg/KgBis(2-Chloroethoxy)methane 36-121 0.7 20
1.34 80.277.81.301.67mg/KgBis(2-Chloroethyl)ether 31-120 3.0 20
1.34 80.279.01.321.67mg/KgBis(2-Chloroisopropyl)ether 33-131 1.5 20
1.71 1021011.681.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.7 20
1.53 91.692.21.541.67mg/Kg4-Bromophenyl phenyl ether 46-124 0.6 20
1.64 98.295.21.591.67mg/KgButyl benzyl phthalate 48-132 3.0 20
1.32 79.080.21.341.67mg/Kg4-Chloro-3-methylphenol 45-122 1.5 20
1.38 82.682.01.371.67mg/Kg4-Chloroaniline 17-106 0.7 20
1.37 82.084.41.411.67mg/Kg2-Chloronaphthalene 41-114 2.8 20
1.43 85.683.81.401.67mg/Kg2-Chlorophenol 34-121 2.1 20
1.54 92.293.41.561.67mg/Kg4-Chlorophenyl phenyl ether 45-121 1.2 20
1.51 90.490.41.511.67mg/KgChrysene 50-124 0.0 20
1.27 76.076.61.281.67mg/KgDibenz(a,h)anthracene 45-134 0.7 20
1.39 83.285.61.431.67mg/KgDibenzofuran 44-120 2.8 20
1.27 76.074.81.251.67mg/Kg1,2-Dichlorobenzene 33-117 1.5 20
1.22 73.072.41.211.67mg/Kg1,3-Dichlorobenzene 30-115 0.8 20
Page 17 of 22* QC Fail Date:02/20/2023 03:23 PM
Page 46 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
LCS-V29651 LCSD-V29651Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.24 74.272.41.211.67mg/Kg1,4-Dichlorobenzene 31-115 2.4 20
1.48 88.688.01.471.67mg/Kg3,3'-Dichlorobenzidine 22-121 0.6 20
1.36 81.480.81.351.67mg/Kg2,4-Dichlorophenol 40-122 0.7 20
1.53 91.692.81.551.67mg/KgDiethyl phthalate 50-124 1.2 20
1.51 90.491.61.531.67mg/KgDimethyl phthalate 48-124 1.3 20
1.72 1031021.711.67mg/Kg2,4-Dimethylphenol 30-127 0.5 20
1.66 99.499.41.661.67mg/KgDi-n-butyl phthalate 51-128 0.0 20
1.28 76.682.61.381.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 7.5 20
1.07 64.076.01.271.67mg/Kg2,4-Dinitrophenol 27-129 17.0 20
1.51 90.489.81.501.67mg/Kg2,4-Dinitrotoluene 48-126 0.6 20
1.44 86.289.21.491.67mg/Kg2,6-Dinitrotoluene 46-124 3.4 20
1.47 88.088.01.471.67mg/KgDi-n-Octyl Phthalate 45-140 0.0 20
1.43 85.686.21.441.67mg/KgFluoranthene 50-127 0.6 20
1.47 88.089.21.491.67mg/KgFluorene 43-125 1.3 20
1.50 89.889.21.491.67mg/KgHexachlorobenzene 45-122 0.6 20
1.24 74.273.01.221.67mg/KgHexachlorobutadiene 32-123 1.6 20
1.19 71.270.01.171.67mg/KgHexachlorocyclopentadiene 32-117 1.6 20
1.23 73.670.61.181.67mg/KgHexachloroethane 28-117 4.1 20
1.30 77.877.81.301.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 0.0 20
1.08 64.664.01.071.67mg/KgIsophorone 30-122 0.9 20
1.21 72.471.21.191.67mg/Kg1-Methylnaphthalene 40-119 1.6 20
1.20 71.870.01.171.67mg/Kg2-Methylnaphthalene 38-122 2.5 20
1.45 86.886.81.451.67mg/Kg2-Methylphenol 32-122 0.0 20
1.30 77.876.01.271.67mg/Kg3&4 Methylphenol 34-119 2.3 20
1.17 70.067.61.131.67mg/KgNaphthalene 35-123 3.4 20
1.49 89.291.61.531.67mg/Kg2-Nitroaniline 44-127 2.6 20
Page 18 of 22Date:02/20/2023 03:23 PM
Page 47 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V29677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V29651
LCS-V29651 LCSD-V29651Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.49 89.290.41.511.67mg/Kg3-Nitroaniline 33-119 1.3 20
1.55 92.893.41.561.67mg/Kg4-Nitroaniline 63-147 0.6 20
1.12 67.065.81.101.67mg/KgNitrobenzene 34-122 1.8 20
1.24 74.273.61.231.67mg/Kg2-Nitrophenol 36-123 0.8 20
1.56 93.497.61.631.67mg/Kg4-Nitrophenol 30-132 4.3 20
0.806 48.250.40.8421.67mg/KgN-Nitrosodimethylamine 10-146 4.3 20
1.79 1071071.791.67mg/KgN-Nitrosodiphenylamine 38-127 0.0 20
1.34 80.282.01.371.67mg/KgN-Nitroso-di-n-propylamine 36-120 2.2 20
1.73 1041041.731.67mg/KgPentachlorophenol 25-133 0.0 20
1.47 88.088.61.481.67mg/KgPhenanthrene 50-121 0.6 20
1.39 83.283.21.391.67mg/KgPhenol 34-121 0.0 20
1.54 92.292.21.541.67mg/KgPyrene 47-127 0.0 20
0.828 49.547.40.7931.67mg/KgPyridine 10-80 4.3 20
1.18 70.668.81.151.67mg/Kg1,2,4-Trichlorobenzene 34-118 2.5 20
1.48 88.694.61.581.67mg/Kg2,4,5-Trichlorophenol 41-124 6.5 20
1.39 83.286.21.441.67mg/Kg2,4,6-Trichlorophenol 39-126 3.5 20
85.690.42-Fluorobiphenyl (S)44-115
78.678.32-Fluorophenol (S)35-115
70.671.2Nitrobenzene-d5 (S)37-122
1011024-Terphenyl-d14 (S)54-127
81.684.92,4,6-Tribromophenol (S)39-132
73.274.4Phenol-d5 (S)34-121
Page 19 of 22Date:02/20/2023 03:23 PM
Page 48 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V29727QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V29676
Associated Lab Samples: 99112, 99117
LRB-V29676 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/13/23 11:4250.09.20<9.20mg/KgAliphatic C9-C18
02/13/23 11:4250.012.2<12.2mg/KgAliphatic C19-C36
02/13/23 11:4250.014.2<14.2mg/KgAromatic C11-C22
02/13/23 11:422-Fluorobiphenyl (S)97.5 40-140
02/13/23 11:422-Bromonaphthalene (S)96.2 40-140
02/13/23 11:42Chlorooctadecane (S)84.5 40-140
02/13/23 11:42OTP Surrogate (S)83.5 40-140
LCS-V29676 LCSD-V29676Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
41.4 69.064.838.960.0mg/KgAliphatic C9-C18 40-140 6.2 50
78.9 98.688.370.780.0mg/KgAliphatic C19-C36 40-140 10.9 50
176 10491.7156170mg/KgAromatic C11-C22 40-140 12.0 50
10397.02-Fluorobiphenyl (S)40-140
10397.02-Bromonaphthalene (S)40-140
10797.0Chlorooctadecane (S)40-140
88.582.5OTP Surrogate (S)40-140
Page 20 of 22Date:02/20/2023 03:23 PM
Page 49 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V29597QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V29596
Associated Lab Samples: 99112, 99117
LRB-V29596 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/08/23 14:4380001220<1220µg/KgAliphatic C5-C8
02/08/23 14:4380004560<4560µg/KgAliphatic C9-C12
02/08/23 14:438000624<624µg/KgAromatic C9-C10
02/08/23 14:432,5-Dibromotoluene (FID) (S)102 70-130
02/08/23 14:432,5-Dibromotoluene (PID) (S)96.2 70-130
LCS-V29596 LCSD-V29596Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37000 1161113560032000µg/KgAliphatic C5-C8 70-130 3.8 50.0
38500 1201183760032000µg/KgAliphatic C9-C12 70-130 2.3 50.0
11200 1051061130010700µg/KgAromatic C9-C10 70-130 0.8 50.0
99.096.22,5-Dibromotoluene (FID) (S)70-130
85.390.22,5-Dibromotoluene (PID) (S)70-130
Page 21 of 22Date:02/20/2023 03:23 PM
Page 50 of 53
Quality Control Data
23-038-0021Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Raleigh
2500 E. Market St.
Dry Weight Determination
SW-DRYWT
V29608QC Analytical Batch:
Analysis Method:
Analysis Description:
V 99060-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/08/23 17:051.282.081.0%Moisture
V 99122-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/08/23 17:051.631.031.5%Moisture
Page 22 of 22Date:02/20/2023 03:23 PM
Page 51 of 53
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-038-0021
Mid-Atlantic Associates, Inc. - Raleigh
01139
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:02/07/2023 14:05:16
Special precautions or instructions included?
Comments:
Page 52 of 53
Page 53 of 53
APPENDIX C

DISPOSAL DOCUMENTATIONP
APPENDIX D

MID-ATLANTIC SOIL SAMPLING PROCEDURE
Soil Sampling Procedures

I. Sample Collection

Direct Push Technology (DPT, or “Geoprobe”)

DPT uses a truck-mounted hydraulic rig to push a steel sampling probe into the
subsurface to collect soil and/or groundwater samples. The sampling device used to
collect the soil samples during this investigation was the “macrocore” sampler. This
sampler consists of a four-foot long, two-inch diameter stainless steel spoon containing a
clear, acetate liner. When the macrocore sampler is driven into the subsurface, the soil is
collected into the acetate liner and then retrieved to the land surface. The liner is then cut
open and the soil lithology is characterized and soil samples are collected.

Split Spoon Sampling

This method of soil sampling is typically used during advancement of hollowstem augers
for the construction of monitoring wells. Soil samples are obtained from the borings by
driving a prewashed, 1-3/8-inch inner-diameter split-spoon sampler at five foot intervals to
termination in general accordance with ASTM D-1586 (Standard Penetration Test)
specifications. Blow counts for each six inches of split-spoon penetration are recorded
during advancement of the spoon. Samples are then retrieved to the land surface, the
split-spoon is opened, and the soil lithology is characterized and soil samples are
collected.

Hand Augering

This method is typically used for shallow sampling in areas where access is limited or
underground obstacles such as utilities may be present. A pre-washed, three-inch
diameter steel auger bucket is attached to extension rods and manually turned to
penetrate the subsurface to the desired sampling depth. Samples are then retrieved to the
land surface and the soil lithology is characterized and soil samples are collected directly
from the hand auger bucket.

Excavator Bucket Sampling

This method is typically used during UST excavation and soil excavation projects. The soil
samples are collected from the excavator bucket when it is not safe to collect the samples
by other means. Care is taken when collecting samples from the bucket to avoid soil that
has come in contact with the bucket itself to avoid cross contamination.

II. Headspace Field Screening

A portion of each sample is removed from the sampling device and placed in a pre-
labeled, plastic "ziploc" bag. After several minutes, the gas contained in the "headspace"
or void area within the bag is tested with a photoionization detection (PID) and/or Flame
Ionization Detector (FID). These are useful as scanning devices to detect the presence of
volatile organic compounds (VOCs) but are not relied upon to determine specific levels of
contamination. Typically, the samples exhibiting the highest headspace readings will be
submitted to the laboratory for analysis.

III. Preparation for Laboratory Analysis

The sample collector dons new nitrile sampling gloves prior to handling each sample. The
samples are placed into laboratory-prepared, pre-labeled, sampling containers, packed in
ice, and shipped to a certified laboratory under chain-of-custody control. Laboratory
analyses to be performed on the samples, along with other sampling information, are
specified on the chain-of-custody, which is placed in the cooler with the samples.