WS-29841_48943_CA_IAR_20230324

INITIAL ABATEMENT ACTION REPORT

Former West End Washette
1602 West English Road
High Point, Guilford County, North Carolina

February 2023

Property Occupant
Vacant

Property Owner / Tank Owner
Guilford Investment Properties
146 Church Avenue
High Point, North Carolina 27262
336-314-3538

UST Operator
Unknown Tank not used in 30 years

Consultant/Contractor

Blue Ridge Geological Services, Inc.
7356 Belmont Drive, Trinity, North Carolina 27370
336-382-6849

Release Information
Date Discovered February 9, 2023
Estimated Quantity - unknown
Cause/Source Holes in 500-gallon Heating Oil UST
Latitude: 35.948 degrees North; Longitude: -80.020 degrees West

Prepared/Reviewed by:
Jeffrey L. Gerlock, L.G.
NC Licensed Geologist #1141

Blue Ridge Geological Services * 7356 Belmont Drive, Trinity, NC 27370 * Phone [phone]

March 24, 2023

Mr. Thomas Jarrell
Guilford Investment Properties, LLC
146 Church Avenue
High Point, North Carolina 27262

Subject: Initial Abatement Action Report
Former West End Washette
1602 West English Road, High Point, North Carolina

Dear Mr. Jarrell:

As authorized by your acceptance of our proposal dated January 20, 2023, Blue Ridge Geological
Services, Inc. (Blue Ridge) personnel performed additional environmental activities at the subject site
and prepared the attached report. This report includes a description of the field activities, the results
obtained, and our conclusions and recommendations. We appreciate the opportunity to provide our
services on this project. Please contact the undersigned if you have any questions concerning this report
or this project.

Sincerely,

Jeffrey L. Gerlock, L.G.
NC Licensed Geologist #1141

Attachment

Blue Ridge Geological Services * 7356 Belmont Drive, Trinity, NC 27370 * Phone [phone]

March 2023

Mr. Gene Mao
Guilford County Department of Public Health
Environmental Health Division
400 West Market Street
Greensboro, North Carolina 27401

Subject: Initial Abatement Action Report
Former West End Washette
1602 West English Road, High Point, North Carolina

Dear Gene:

As authorized by Guilford Investment Properties, Blue Ridge Geological Services, Inc. (Blue Ridge)
personnel and its subcontractor removed a heating oil underground storage tank (UST) from the site.
Blue Ridge personnel supervised and documented the UST removal activities. The field work was
performed and the attached report prepared in general accordance with the North Carolina Department of
Environmental Quality (NCDEQ) Guidelines for Site Checks, Tank Closure, and Initial Response and
Abatement for UST Releases. The report includes a description of the field activities, the results obtained,
and our conclusions and recommendations.

We appreciate your consideration of this report. Please contact the undersigned if you have questions
concerning the report or if you need additional information.

Sincerely,

Jeffrey L. Gerlock, L.G.
NC Licensed Geologist #1141

Attachment

Cc: Mr. Thomas Jarrell

Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

1
A. Site Information
1. Site Identification

Date of Report: March 2023
Facility ID#: Not Assigned UST Incident #: Not Assigned
Site Name: Former West End Washette
Site Location: 1602 West English Road
City/Town: High Point Zip Code: 27262 County: Guilford
Description of Geographical Data Point: UST Location
Location Method: USFWS Website
Latitude: 35.948 degrees North; Longitude: -80.020 degrees West

2. Contacts

UST Owner: Guilford Investment Properties
Address: 146 Church Avenue, High Point, NC 27262 Telephone: [phone]
UST Operator: Tank Not Used for over 30 years
Address: Telephone:
Property Owner: Guilford Investment Properties
Address: 146 Church Avenue, High Point, NC 27262 Telephone: [phone]
Property Occupant: Vacant and not in use
Address: Telephone:
Remediation Contractor: Evo Corporation
Address: 1703 Vargrave Street, Winston-Salem, NC 27107 Telephone: [phone]
Consultant/Contractor: Blue Ridge Geological Services, Inc.
Address: 7356 Belmont Drive, Trinity, NC 27370 Telephone: [phone]
Analytical Laboratory: Pace Analytical Services State Cert No. 37706 / 12
Address: 9600 Kincey Ave, Suite 100, Huntersville, NC 28708 Telephone: [phone]

3. Release Information
Date Discovered: February 9, 2023
Estimated Quantity of Release: Unknown
Cause of Release: Holes in UST
Source of Release: Heating Oil UST
Size and Contents of UST system(s) from which the release occurred: One 500-gallon Heating Oil
UST

4. Certification
I, Jeffrey L. Gerlock, a Licensed Geologist for Blue Ridge Geological Services, Inc. do certify that the
information contained in this report is correct and accurate to the best of my knowledge. Blue Ridge
Geological Services, Inc. is licensed to practice geology in North Carolina. The certification number of
the corporation is C-305.

Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

2

B. Site History and Characterization

The subject site is a 0.07-acre parcel located at 1602 West English Road in High Point, Guilford County,
North Carolina (Figures 1 and 2). The site contains a 1,858 square foot commercial building that was
constructed in 1954. The building is currently vacant; it was occupied by the West End Washette
(laundromat) from the 1950s through 1990s. The subject site is owned by Guilford Investment Properties
who purchased the property in September 2022.

One 500-gallon heating oil underground storage tank (UST) was located outside the northwest side of the
building on the property. The tank was formerly used to supply heating oil to the onsite building. The
installation date of the tank is unknown; it was likely installed by a previous owner when the building was
used as a laundromat in the 1950s / 1960s. The current property owner has never used the tank. The tank
was discovered by Blue Ridge personnel during a limited phase 2 assessment performed at the site in
2022 as part of a real estate transaction.

The tank was not registered with the NCDEQ UST Section; it is a non-regulated heating oil tank used for
heating the premises. No releases were known or reported from the UST. The site history / UST system
information is summarized in Table 1. The UST owner and operator information is summarized in Table 2.
No aboveground storage tanks (ASTs) are located at the site.

The subject site is located in the Town of High Point in Guilford County, North Carolina. The area
around the subject site is commercial and residential (Figures 1 and 2). The subject site is currently
vacant. Commercial buildings are located south, east, and north of the site. A residence is located
adjacent northwest of the site.

No evidence of a water supply well was observed on the subject site or adjacent properties. The nearest
surface water feature is a creek located approximately 2,500 feet north - northeast of the UST / source
area. The creek is located topographically downgradient of the subject site. Table 3 summarizes
information concerning receptors in the area. The receptors are shown on Figure 2.

The subject site is located in the Carolina Slate Geologic Belt. Based on a review of the Geologic Map of
North Carolina, the site is underlain by metamorphosed granitic rock. The soils encountered in this area
are the residual product of in-place chemical weathering of rock presently underlying the site. In this
region, the direction and movement of groundwater through soil is dependent upon soil type and the
Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

3
presence of relict structures and textures of the underlying rock. Fractures, faults, folds, and foliation
planes affect the migration of groundwater in rock. In this geologic setting, groundwater flow is generally
a subdued replica of the surface topography and flows toward drainage features which have eroded deeply
enough to intersect the groundwater level and act as a discharge point.

The site is located in the Piedmont Physiographic Province which generally consists of low rounded hills
and gentle slopes. Topographically, the site is located along the top of a topographic high running along
West English Road. The ground surface elevation at the property is approximately 930 feet above mean
sea level (MSL) and the general surface water and estimated groundwater flow direction at the site is to
the north (Figure 1). The natural groundwater flow direction can be affected by pumping from high-
capacity wells and permanent or temporary dewatering systems.

C. Site Check Report

This section is not applicable.

D. UST Closure Report

On February 9, 2023 Evo Corporation (Evo) personnel mobilized to the site and vacuumed liquids from
the tank using a vacuum truck and flexible hoses. Approximately 349 gallons of liquids were removed
from the tank and transported to Evo s facility in Winston-Salem, North Carolina for disposal / recycling.
A copy of the disposal manifest is included in the Appendix. Next, Evo personnel excavated around the
top and sides of the underground storage tank. The tank was removed and transported to Foss Recycling
in Winston-Salem, North Carolina for recycling. Copies of the weight ticket and tank disposal certificate
are included in the Appendix.

The top of the 500-gallon tank was approximately two feet below the ground surface. The tank was
approximately 3.5 feet in diameter and eight (8) feet long. The single wall steel tank was in poor good
condition; numerous holes were observed in the sides and ends of the tank. Two small diameter copper
product lines ran from the tank into the crawlspace of the onsite building. The product lines were purged
and then crimped at the edge of the tank basin; the lines were not removed. No dispensers or pumps were
attached to the tank. Photographs of the tank removal activities are included in the Appendix.

On February 9, 2023 Evo personnel excavated the soil from around the top, sides, and bottom of the tank
using a backhoe. Soil with a petroleum odor was encountered starting at about 3.5 feet below ground
surface. Therefore, impacted soil was removed from the excavation (see discussion below). The soil in the
excavation was fill material consisting of brown silt, silty clay, and clay. The final excavation was
Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

4
approximately eight (8) feet wide, 11 feet long, and eight to ten feet deep. The approximate limits of the
excavation are shown on Figure 3. Weathered bedrock was encountered in the base / floor of the
excavation. No water or free product was encountered in the excavation.

On February 9, 2023 field personnel collected one grab soil sample from approximately one foot below the
base of the tank (identified as S-1) and five grab samples from the base and four sidewalls of the final soil
excavation (identified as CS-1 through CS-5). These soil samples were grab samples collected from the
excavation using the bucket of the backhoe. The soil sample locations are shown on Figure 3.

The soil samples were screened for organic vapors using a portable meter. Portions of the soil samples
were placed into a baggie, allowed to heat for about 15 minutes, and then the probe of an organic vapor
analyzer (Mini Rae 2000) was used to screen the soil samples for the presence of petroleum vapors. The
meter was zeroed to site background levels prior to measurement of the samples. Organic vapors (153.1
parts per million (ppm)) were detected in sample S-1; no organic vapors (0.0 ppm) were detected in the
five confirmation soil samples. The organic vapor readings are presented in Table 4.

The soil samples were placed into laboratory-prepared containers (some with preservatives), labeled, and
transported to Pace Analytical Services in Huntersville, North Carolina in a cooler containing ice. A chain
of custody form was submitted with the samples. Soil sample S-1 was analyzed for gasoline range
organics (GRO) total petroleum hydrocarbons (TPH) using EPA Method 5030/8015M and diesel range
organics (DRO) TPH using EPA Method 3550/8015M. The base and sidewall confirmation soil samples
(CS-1 to CS-5) were analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi-VOCs
by EPA Method 8270, and volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons
(EPH) by the Massachusetts Department of Environmental Protection (MADEP) Method.

As shown in Table 4, GRO TPH and DRO TPH were detected in soil sample S-1 at concentrations of 117
and 3,930 milligrams per kilogram (mg/kg), respectively. GRO and DRO TPH were detected in soil sample
S-1 collected just below the middle of the tank at concentrations above the North Carolina Department of
Environmental Quality (NCDEQ) Action Levels of 50 and 100 mg/kg, respectively. No VOCs, semi-VOCs,
VPH, or EPH were detected in samples CS-1 through CS-5. Several SVOC tentatively identified
compounds (TICs) were detected in all five of the confirmation soil samples at concentrations ranging from
0.236 to 3.382 mg/kg; there are no MSCCs for the TICs.

The soil analytical results are summarized in Table 4. As shown in the table, no petroleum constituents
were detected in samples CS-1 through CS-5 at concentrations above the NCDEQ Maximum Soil
Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

5
Contaminant Concentrations (MSCCs). The laboratory data and chain of custody documentation are
presented in the Appendix.

On February 9, 2023 field personnel backfilled the excavation with silty sand / sandrock from the nearby
Martin Marietta quarry. Field personnel compacted the soil in the excavation using the bucket of the
backhoe.

Note - Since petroleum contamination was detected in closure samples collected during tank closure,
results were reported in this report (not in a UST Closure Report).

E. Free Product Investigation and Recovery Report

This section is not applicable since no free product was detected in the soil during tank removal and
groundwater or free product were not encountered in the tank excavation.

F. Groundwater and Surface Water Investigation

This section is not applicable since groundwater and surface water were not encountered in the soil
excavation (to a depth of ten feet) and no water samples were collected.

G. Initial Response and Abatement Action

In order to prevent further release and remove the secondary source of petroleum-impacted soil in the tank
area, field personnel pumped the heating oil out of the tank, removed the tank, and excavated and removed
the petroleum-impacted soil from around the top, sides, and bottom of the tank excavation on February 9,
2023. No free product or groundwater was encountered in the tank pit. No hazards due to exposure to
pollutants (i.e., active shallow water supply wells, surface water) were identified in the immediate vicinity of
the former UST. No hazards due to fire, explosion, and vapor hazards were identified in the area on this date.
On February 20, 2023 Blue Ridge personnel submitted a 24-Hour Release and UST Leak Reporting Form to
the Guilford County Department of Public Health (GCDPH) via email informing the County and State of the
petroleum release observed at the site.

Initial Abatement Action Report March 2023
1602 West English Road, High Point, NC Blue Ridge Geological Services

6
H. Excavation of Contaminated Soil

As stated above, field personnel excavated the soil from around the top, sides, and bottom of the tank using
a backhoe on February 9, 2023. Two loads of soil (35.11 tons) were placed into dump trailers and
transported to Evo s facility in Winston-Salem, North Carolina for recycling / remediation. The soil
disposal manifests and certificate of disposal are included in the Appendix. The excavation was advanced
until no soil with a petroleum odor was noted. The excavation was also advanced vertically to the top of
weathered bedrock. The final excavation was approximately eight feet wide, 11 feet long, and eight to ten
feet deep. The approximate limits of the excavation are shown on Figure 3.

I. Conclusions

The 500-gallon heating oil UST was removed from the site in February 2023. The tank was in poor
condition with numerous holes. Soil with a petroleum odor was encountered below the tank starting at
about 3.5 feet below the ground surface. The source of the impacted soil was the holes in the tank.
Approximately 35 tons of petroleum-impacted soil was removed from the tank excavation. No petroleum
constituents were detected in confirmation soil samples CS-1 through CS-5 collected from the sidewalls
and floor of the excavation at concentrations above State standards (MSCCs). Therefore, no additional
assessment or remediation is necessary at the site.

J. FIGURES
T op ograp hic M ap
Mar 2023 Figure 1REF: USGS High Point West NC Quadrangle Map dated 1965 revised 1993
1602 West English Road
High Point, North Carolina
Site Location M ap
Mar 2023 Figure 2REF: High Point NC GIS - 2021 Aerial
1602 West English Road
High Point, North Carolina
Samp le Location Map
Mar 2023 Figure 3
1602 West English Road
High Point, North Carolina
Legend
Former 500-gallon heating oil UST
Soil Sample Location
REF.: Blue Ridge Field Notes
Scale: 1 inch = 10 feet
concrete
slab
Site Building
Adjacent
Building
Concrete retaining wall Gas

l
i
ne
CS-5 CS-1 S-1
CS-4
CS-2
CS-3
excavation
area
former product lines
telephone pole
W W est P o in t A v e

K. TABLES
Revision Date: March 2023 Incident No/Name: Not Assigned - Fomer West End Washette, 1602 West English Rd, High Point
UST ID Number Current/Last
Contents Previous Contents Capacity
(gallons) Construction Details Tank Dimensions
(feet)
Description of Associated Piping and
Pumps
Date Tank
Installed Status of UST Was release associated
with the UST System?
1 Heating Oil /
Heating Oil Heating Oil 500 Steel (single wall)3.6 x 6
Lines leads from tank
underground into crawlspace of
building. No pumps or
dispensers.
Unknown
(Est 1966)Removed 2/9/23 Yes; tank
AST ID Number Current/Last
Contents Previous Contents Capacity
(gallons) Construction Details Tank Dimensions Description of Associated Piping and
Pumps
Date Tank
Installed Status of AST Was release associated
with the AST System?
None
Incident Number Material Released Date of Release
Not Assigned Heating Oil Unknown
Table 1
Site History - UST/AST System and Other Release Information
Description of Release
Leak from holes in tank
Revised Date: March 2023 Incident No. and Name:Not Assigned; Former West End Washette, 1602 W English Rd, High Pt
UST ID Number NA
Name of Property Owner
Street Address
City State Zip
NC 28262
Name of Tank Owner
Street Address
City State Zip
NC 27262
Name of Other Responsible Party
Annie Lee Jarrell 1983 to 1998
Ruth Hoover Prior to 1983
Street Address
City State Zip
Incident Number Not
Assigned
Dates of Release(s)
336-314-3538
146 Church Avenue
Guilford Investment Properties
High Point
Telephone Number
336-314-3538
146 Church Avenue
September 2022 to PresentGuilford Investment Properties
High Point
Table 2
Site History - UST/AST Owner/Operator and Other Responsible Party Information
1 Facility ID Number
Unknown
Kingston Investments 2007 to 2022
Telephone Number
Dates of Ownership
Dates of Operation
Dates of Property/Tank Ownership/Operation
Unknown
Never operated Tank
Telephone Number
Revision Date: March 2023 Incident No/Name: Not Assigned - Fomer West End Washette, 1602 West English Rd, High Point
Public and Private Water Supply Wells
Well #Well Owner/ User (indicate which) Address of Well Phone Number Well Use Well Depth (ft
BGS) Type of Well Well Casing Depth (ft.
BGS)
Well Screen Interval
(x to y ft. BGS)
Distance from source
area of release (ft.) Up or downgradient
No wells observed
Other Receptors
Receptor ID Description Location Contact Phone Number Usage Up or down-
gradient
Distance from source
area of release (ft.)
Creek Creek Downgradient 2,500
See Figure 1 for locations.
Table 3
Public and Private Water Supply Well and Other Receptor Information

Revision Date: March 2023 Incident No/Name: Not Assigned; 1602 West English Road, High Point, NC
Parameter NCDEQ Action Levels
Sample ID S-1 CS-1 CS-2 CS-3 CS-4 CS-5
Sample Depth (ft, bgs)6.0 10.0 7.0 7.0 6.5 7.0 Soil to Industrial/
Field Organic Vapor Measurement (ppm)Analytical 153.1 0 0 0 0 0 Groundwater Residential Commercial
Collection Date Method 2/9/2023 2/9/2023 2/9/2023 2/9/2023 2/9/2023 2/9/2023 TPH MSCC MSCC MSCC
TPH
GRO TPH 5030 117 NA NA NA NA NA 50 NE NE NE
DRO TPH 3550 3930 NA NA NA NA NA 100 NE NE NE
Volatile Organic Compounds - VOCs
Total VOCs 8260 ND ND ND ND ND ND NE NE NE NE
Semi-Volatile Organic Compounds - SVOCs
Total SVOCs 8270 NA ND ND ND ND ND NE NE NE NE
SVOC TICs 8270 NA 0.565 0.236 3.382 0.509 0.515 NE NE NE NE
Volatile Petroleum Hydrocarbons - VPH
C5-C8 Aliphatics VPH NA <18 <15 <16 <16 <10 NE 68 625 9,340
C9-C12 Aliphatics VPH NA <18 <15 <16 <16 <10 NE see below see below see below
C9-C10 Aromatics VPH NA <18 <15 <16 <16 <10 NE see below see below see below
Extractable Petroleum Hydrocarbons - EPH
C9-C18 Aliphatics EPH NA <13.4 <12.3 <13.9 <13.8 <11.9 NE see below see below see below
C19-C36 Aliphatics EPH NA <13.4 <12.3 <13.9 <13.8 <11.9 NE a 31,200 467,000
C11-C22 Aromatics EPH NA <13.4 <12.3 <13.9 <13.8 <11.9 NE see below see below see below
VPH + EPH
C9-C18 Aliphatics VPH + EPH NA ND ND ND ND ND NE 540 1,560 23,300
C9-C22 Aromatics VPH + EPH NA ND ND ND ND ND NE 31 469 7,000
Notes:
All concentrations are in milligrams per kilogram (mg/kg)
ft, bgs - feet below ground surface
ND - Not Detected
NA - Not Analyzed; NM - Not Measured
N/A - Not Applicable; NE - Not Established
Table 4 - Summary of Soil Sampling Results
Laboratory Results

L. APPENDIX

LIQUIDS DISPOSAL MANIFEST
TANK DISPOSAL CERTIFICATE
SOIL DISPOSAL MANIFESTS AND
CERTIFICATE OF DISPOSAL
PHOTOGRAPHS
LABORATORY ANALYTICAL REPORT AND
CHAIN OF CUSTODY RECORD

Photo 1. Tank and product lines near retaining wall. Photo 2. Removing the tank.

Photo 3. One of the numerous holes in the tank. Photo 4. Final limits of the soil excavation.

Photo 5. Loading contaminated soil for off-site disposal. Photo 6. Backfilled area

1602 West English Road March 2023
High Point, North Carolina Blue Ridge Geological Services
#=CL#
March 07, 2023
LIMS USE: FR - JEFF GERLOCK
LIMS OBJECT ID: 92651699
92651699
Project:
Pace Project No.:
RE:
Mr. Jeff Gerlock
Blue Ridge Geological Services
7356 Belmont Drive
Trinity, NC 27370
ENGLISH
Dear Mr. Gerlock:
Enclosed are the analytical results for sample(s) received by the laboratory on February 10, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92651699
ENGLISH
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92651699
ENGLISH
Lab ID Sample ID Matrix Date Collected Date Received
92651699001 S-1 Solid 02/09/23 10:05 02/10/23 05:30
92651699002 CS-1 Solid 02/09/23 10:34 02/10/23 05:30
92651699003 CS-2 Solid 02/09/23 10:25 02/10/23 05:30
92651699004 CS-3 Solid 02/09/23 10:20 02/10/23 05:30
92651699005 CS-4 Solid 02/09/23 10:29 02/10/23 05:30
92651699006 CS-5 Solid 02/09/23 10:40 02/10/23 05:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92651699
ENGLISH
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92651699001 S-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92651699002 CS-1 MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92651699003 CS-2 MADEP EPH 7 PASI-CBAJ
EPA 8270E 74 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92651699004 CS-3 MADEP EPH 7 PASI-CBAJ
EPA 8270E 82 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92651699005 CS-4 MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92651699006 CS-5 MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:S-1 Lab ID:92651699001 Collected:02/09/23 10:05 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3930 mg/kg 02/16/23 15:4402/15/23 15:4867.5 10
Surrogates
n-Pentacosane (S)0 %02/16/23 15:44 629-99-2 S402/15/23 15:4810-130 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)117 mg/kg 02/13/23 16:0702/13/23 11:018.7 1
Surrogates
4-Bromofluorobenzene (S)152 %02/13/23 16:07 460-00-4 S502/13/23 11:0166-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.0 %02/10/23 16:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-1 Lab ID:92651699002 Collected:02/09/23 10:34 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 02/16/23 15:49 N202/16/23 08:5213.4 1
Aliphatic (C19-C36)ND mg/kg 02/16/23 15:49 N202/16/23 08:5213.4 1
Aromatic (C11-C22)ND mg/kg 02/16/23 15:49 N202/16/23 08:5213.4 1
Surrogates
1-Chlorooctadecane (S)68 %02/16/23 15:49 3386-33-202/16/23 08:5240-140 1
o-Terphenyl (S)54 %02/16/23 15:49 84-15-102/16/23 08:5240-140 1
2-Fluorobiphenyl (S)85 %02/16/23 15:49 321-60-802/16/23 08:5240-140 1
2-Bromonaphthalene (S)87 %02/16/23 15:49 580-13-202/16/23 08:5240-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 02/12/23 14:27 83-32-902/10/23 19:274381
Acenaphthylene ND ug/kg 02/12/23 14:27 208-96-802/10/23 19:274381
Aniline ND ug/kg 02/12/23 14:27 62-53-302/10/23 19:274381
Anthracene ND ug/kg 02/12/23 14:27 120-12-702/10/23 19:274381
Benzo(a)anthracene ND ug/kg 02/12/23 14:27 56-55-302/10/23 19:274381
Benzo(a)pyrene ND ug/kg 02/12/23 14:27 50-32-802/10/23 19:274381
Benzo(b)fluoranthene ND ug/kg 02/12/23 14:27 205-99-202/10/23 19:274381
Benzo(g,h,i)perylene ND ug/kg 02/12/23 14:27 191-24-202/10/23 19:274381
Benzo(k)fluoranthene ND ug/kg 02/12/23 14:27 207-08-902/10/23 19:274381
Benzoic Acid ND ug/kg 02/12/23 14:27 65-85-002/10/23 19:2721901
Benzyl alcohol ND ug/kg 02/12/23 14:27 100-51-602/10/23 19:278771
4-Bromophenylphenyl ether ND ug/kg 02/12/23 14:27 101-55-302/10/23 19:274381
Butylbenzylphthalate ND ug/kg 02/12/23 14:27 85-68-702/10/23 19:274381
4-Chloro-3-methylphenol ND ug/kg 02/12/23 14:27 59-50-702/10/23 19:278771
4-Chloroaniline ND ug/kg 02/12/23 14:27 106-47-802/10/23 19:278771
bis(2-Chloroethoxy)methane ND ug/kg 02/12/23 14:27 111-91-102/10/23 19:274381
bis(2-Chloroethyl) ether ND ug/kg 02/12/23 14:27 111-44-402/10/23 19:274381
2-Chloronaphthalene ND ug/kg 02/12/23 14:27 91-58-702/10/23 19:274381
2-Chlorophenol ND ug/kg 02/12/23 14:27 95-57-802/10/23 19:274381
4-Chlorophenylphenyl ether ND ug/kg 02/12/23 14:27 7005-72-302/10/23 19:274381
Chrysene ND ug/kg 02/12/23 14:27 218-01-902/10/23 19:274381
Dibenz(a,h)anthracene ND ug/kg 02/12/23 14:27 53-70-302/10/23 19:274381
Dibenzofuran ND ug/kg 02/12/23 14:27 132-64-902/10/23 19:274381
1,2-Dichlorobenzene ND ug/kg 02/12/23 14:27 95-50-102/10/23 19:274381
1,3-Dichlorobenzene ND ug/kg 02/12/23 14:27 541-73-102/10/23 19:274381
1,4-Dichlorobenzene ND ug/kg 02/12/23 14:27 106-46-702/10/23 19:274381
3,3'-Dichlorobenzidine ND ug/kg 02/12/23 14:27 91-94-102/10/23 19:278771
2,4-Dichlorophenol ND ug/kg 02/12/23 14:27 120-83-202/10/23 19:274381
Diethylphthalate ND ug/kg 02/12/23 14:27 84-66-202/10/23 19:274381
2,4-Dimethylphenol ND ug/kg 02/12/23 14:27 105-67-902/10/23 19:274381
Dimethylphthalate ND ug/kg 02/12/23 14:27 131-11-302/10/23 19:274381
Di-n-butylphthalate ND ug/kg 02/12/23 14:27 84-74-202/10/23 19:274381
4,6-Dinitro-2-methylphenol ND ug/kg 02/12/23 14:27 534-52-102/10/23 19:278771
2,4-Dinitrophenol ND ug/kg 02/12/23 14:27 51-28-5 v102/10/23 19:2721901
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-1 Lab ID:92651699002 Collected:02/09/23 10:34 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 02/12/23 14:27 121-14-202/10/23 19:274381
2,6-Dinitrotoluene ND ug/kg 02/12/23 14:27 606-20-202/10/23 19:274381
Di-n-octylphthalate ND ug/kg 02/12/23 14:27 117-84-002/10/23 19:274381
bis(2-Ethylhexyl)phthalate ND ug/kg 02/12/23 14:27 117-81-702/10/23 19:274381
Fluoranthene ND ug/kg 02/12/23 14:27 206-44-002/10/23 19:274381
Fluorene ND ug/kg 02/12/23 14:27 86-73-702/10/23 19:274381
Hexachloro-1,3-butadiene ND ug/kg 02/12/23 14:27 87-68-302/10/23 19:274381
Hexachlorobenzene ND ug/kg 02/12/23 14:27 118-74-102/10/23 19:274381
Hexachlorocyclopentadiene ND ug/kg 02/12/23 14:27 77-47-402/10/23 19:274381
Hexachloroethane ND ug/kg 02/12/23 14:27 67-72-102/10/23 19:274381
Indeno(1,2,3-cd)pyrene ND ug/kg 02/12/23 14:27 193-39-502/10/23 19:274381
Isophorone ND ug/kg 02/12/23 14:27 78-59-102/10/23 19:274381
1-Methylnaphthalene ND ug/kg 02/12/23 14:27 90-12-002/10/23 19:274381
2-Methylnaphthalene ND ug/kg 02/12/23 14:27 91-57-602/10/23 19:274381
2-Methylphenol(o-Cresol)ND ug/kg 02/12/23 14:27 95-48-702/10/23 19:274381
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/12/23 14:27 15831-10-402/10/23 19:274381
Naphthalene ND ug/kg 02/12/23 14:27 91-20-302/10/23 19:274381
2-Nitroaniline ND ug/kg 02/12/23 14:27 88-74-402/10/23 19:2721901
3-Nitroaniline ND ug/kg 02/12/23 14:27 99-09-202/10/23 19:2721901
4-Nitroaniline ND ug/kg 02/12/23 14:27 100-01-602/10/23 19:278771
Nitrobenzene ND ug/kg 02/12/23 14:27 98-95-302/10/23 19:274381
2-Nitrophenol ND ug/kg 02/12/23 14:27 88-75-502/10/23 19:274381
4-Nitrophenol ND ug/kg 02/12/23 14:27 100-02-702/10/23 19:2721901
N-Nitrosodimethylamine ND ug/kg 02/12/23 14:27 62-75-902/10/23 19:274381
N-Nitroso-di-n-propylamine ND ug/kg 02/12/23 14:27 621-64-702/10/23 19:274381
N-Nitrosodiphenylamine ND ug/kg 02/12/23 14:27 86-30-602/10/23 19:274381
Pentachlorophenol ND ug/kg 02/12/23 14:27 87-86-5 v102/10/23 19:278771
Phenanthrene ND ug/kg 02/12/23 14:27 85-01-802/10/23 19:274381
Phenol ND ug/kg 02/12/23 14:27 108-95-202/10/23 19:274381
Pyrene ND ug/kg 02/12/23 14:27 129-00-002/10/23 19:274381
1,2,4-Trichlorobenzene ND ug/kg 02/12/23 14:27 120-82-102/10/23 19:274381
2,4,5-Trichlorophenol ND ug/kg 02/12/23 14:27 95-95-402/10/23 19:274381
2,4,6-Trichlorophenol ND ug/kg 02/12/23 14:27 88-06-202/10/23 19:274381
Surrogates
Nitrobenzene-d5 (S)58 %02/12/23 14:27 4165-60-002/10/23 19:2710-130 1
2-Fluorobiphenyl (S)60 %02/12/23 14:27 321-60-802/10/23 19:2710-130 1
Terphenyl-d14 (S)65 %02/12/23 14:27 1718-51-002/10/23 19:2710-130 1
Phenol-d6 (S)56 %02/12/23 14:27 13127-88-302/10/23 19:2710-130 1
2-Fluorophenol (S)53 %02/12/23 14:27 367-12-402/10/23 19:2710-130 1
2,4,6-Tribromophenol (S)70 %02/12/23 14:27 118-79-602/10/23 19:2710-131 1
Tentatively Identified Compounds
n-Hexadecanoic acid 262J ug/kg 02/12/23 14:27 57-10-3 N02/10/23 19:271
9-Octadecenamide, (Z)-303J ug/kg 02/12/23 14:27 301-02-0 N02/10/23 19:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-1 Lab ID:92651699002 Collected:02/09/23 10:34 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/14/23 14:42 67-64-102/13/23 19:201611
Benzene ND ug/kg 02/14/23 14:42 71-43-202/13/23 19:208.0 1
Bromobenzene ND ug/kg 02/14/23 14:42 108-86-102/13/23 19:208.0 1
Bromochloromethane ND ug/kg 02/14/23 14:42 74-97-502/13/23 19:208.0 1
Bromodichloromethane ND ug/kg 02/14/23 14:42 75-27-402/13/23 19:208.0 1
Bromoform ND ug/kg 02/14/23 14:42 75-25-202/13/23 19:208.0 1
Bromomethane ND ug/kg 02/14/23 14:42 74-83-902/13/23 19:2032.1 1
2-Butanone (MEK)ND ug/kg 02/14/23 14:42 78-93-302/13/23 19:201611
n-Butylbenzene ND ug/kg 02/14/23 14:42 104-51-802/13/23 19:208.0 1
sec-Butylbenzene ND ug/kg 02/14/23 14:42 135-98-802/13/23 19:208.0 1
tert-Butylbenzene ND ug/kg 02/14/23 14:42 98-06-602/13/23 19:208.0 1
Carbon tetrachloride ND ug/kg 02/14/23 14:42 56-23-502/13/23 19:208.0 1
Chlorobenzene ND ug/kg 02/14/23 14:42 108-90-702/13/23 19:208.0 1
Chloroethane ND ug/kg 02/14/23 14:42 75-00-302/13/23 19:2016.1 1
Chloroform ND ug/kg 02/14/23 14:42 67-66-302/13/23 19:208.0 1
Chloromethane ND ug/kg 02/14/23 14:42 74-87-302/13/23 19:2016.1 1
2-Chlorotoluene ND ug/kg 02/14/23 14:42 95-49-802/13/23 19:208.0 1
4-Chlorotoluene ND ug/kg 02/14/23 14:42 106-43-402/13/23 19:208.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/14/23 14:42 96-12-8 IK02/13/23 19:208.0 1
Dibromochloromethane ND ug/kg 02/14/23 14:42 124-48-102/13/23 19:208.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/14/23 14:42 106-93-402/13/23 19:208.0 1
Dibromomethane ND ug/kg 02/14/23 14:42 74-95-302/13/23 19:208.0 1
1,2-Dichlorobenzene ND ug/kg 02/14/23 14:42 95-50-102/13/23 19:208.0 1
1,3-Dichlorobenzene ND ug/kg 02/14/23 14:42 541-73-102/13/23 19:208.0 1
1,4-Dichlorobenzene ND ug/kg 02/14/23 14:42 106-46-702/13/23 19:208.0 1
Dichlorodifluoromethane ND ug/kg 02/14/23 14:42 75-71-8 IH,v102/13/23 19:2016.1 1
1,1-Dichloroethane ND ug/kg 02/14/23 14:42 75-34-302/13/23 19:208.0 1
1,2-Dichloroethane ND ug/kg 02/14/23 14:42 107-06-202/13/23 19:208.0 1
1,1-Dichloroethene ND ug/kg 02/14/23 14:42 75-35-402/13/23 19:208.0 1
cis-1,2-Dichloroethene ND ug/kg 02/14/23 14:42 156-59-202/13/23 19:208.0 1
trans-1,2-Dichloroethene ND ug/kg 02/14/23 14:42 156-60-502/13/23 19:208.0 1
1,2-Dichloropropane ND ug/kg 02/14/23 14:42 78-87-502/13/23 19:208.0 1
1,3-Dichloropropane ND ug/kg 02/14/23 14:42 142-28-902/13/23 19:208.0 1
2,2-Dichloropropane ND ug/kg 02/14/23 14:42 594-20-7 v202/13/23 19:208.0 1
1,1-Dichloropropene ND ug/kg 02/14/23 14:42 563-58-602/13/23 19:208.0 1
cis-1,3-Dichloropropene ND ug/kg 02/14/23 14:42 10061-01-502/13/23 19:208.0 1
trans-1,3-Dichloropropene ND ug/kg 02/14/23 14:42 10061-02-602/13/23 19:208.0 1
Diisopropyl ether ND ug/kg 02/14/23 14:42 108-20-302/13/23 19:208.0 1
Ethylbenzene ND ug/kg 02/14/23 14:42 100-41-402/13/23 19:208.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/14/23 14:42 87-68-302/13/23 19:2016.1 1
2-Hexanone ND ug/kg 02/14/23 14:42 591-78-602/13/23 19:2080.4 1
Isopropylbenzene (Cumene)ND ug/kg 02/14/23 14:42 98-82-802/13/23 19:208.0 1
p-Isopropyltoluene ND ug/kg 02/14/23 14:42 99-87-602/13/23 19:208.0 1
Methylene Chloride ND ug/kg 02/14/23 14:42 75-09-202/13/23 19:2032.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/14/23 14:42 108-10-102/13/23 19:2080.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-1 Lab ID:92651699002 Collected:02/09/23 10:34 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 02/14/23 14:42 1634-04-402/13/23 19:208.0 1
Naphthalene ND ug/kg 02/14/23 14:42 91-20-3 L102/13/23 19:208.0 1
n-Propylbenzene ND ug/kg 02/14/23 14:42 103-65-102/13/23 19:208.0 1
Styrene ND ug/kg 02/14/23 14:42 100-42-502/13/23 19:208.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/14/23 14:42 630-20-602/13/23 19:208.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/14/23 14:42 79-34-502/13/23 19:208.0 1
Tetrachloroethene ND ug/kg 02/14/23 14:42 127-18-402/13/23 19:208.0 1
Toluene ND ug/kg 02/14/23 14:42 108-88-302/13/23 19:208.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/14/23 14:42 87-61-602/13/23 19:208.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/14/23 14:42 120-82-102/13/23 19:208.0 1
1,1,1-Trichloroethane ND ug/kg 02/14/23 14:42 71-55-602/13/23 19:208.0 1
1,1,2-Trichloroethane ND ug/kg 02/14/23 14:42 79-00-502/13/23 19:208.0 1
Trichloroethene ND ug/kg 02/14/23 14:42 79-01-602/13/23 19:208.0 1
Trichlorofluoromethane ND ug/kg 02/14/23 14:42 75-69-402/13/23 19:208.0 1
1,2,3-Trichloropropane ND ug/kg 02/14/23 14:42 96-18-402/13/23 19:208.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/14/23 14:42 95-63-602/13/23 19:208.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/14/23 14:42 108-67-802/13/23 19:208.0 1
Vinyl acetate ND ug/kg 02/14/23 14:42 108-05-402/13/23 19:2080.4 1
Vinyl chloride ND ug/kg 02/14/23 14:42 75-01-402/13/23 19:2016.1 1
Xylene (Total)ND ug/kg 02/14/23 14:42 1330-20-702/13/23 19:2016.1 1
m&p-Xylene ND ug/kg 02/14/23 14:42 179601-23-102/13/23 19:2016.1 1
o-Xylene ND ug/kg 02/14/23 14:42 95-47-602/13/23 19:208.0 1
Surrogates
Toluene-d8 (S)102 %02/14/23 14:42 2037-26-502/13/23 19:2070-130 1
4-Bromofluorobenzene (S)102 %02/14/23 14:42 460-00-402/13/23 19:2070-130 1
1,2-Dichloroethane-d4 (S)108 %02/14/23 14:42 17060-07-002/13/23 19:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.2 %02/10/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-2 Lab ID:92651699003 Collected:02/09/23 10:25 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 02/16/23 16:14 N202/16/23 08:5212.3 1
Aliphatic (C19-C36)ND mg/kg 02/16/23 16:14 N202/16/23 08:5212.3 1
Aromatic (C11-C22)ND mg/kg 02/16/23 16:14 N202/16/23 08:5212.3 1
Surrogates
1-Chlorooctadecane (S)67 %02/16/23 16:14 3386-33-202/16/23 08:5240-140 1
o-Terphenyl (S)58 %02/16/23 16:14 84-15-102/16/23 08:5240-140 1
2-Fluorobiphenyl (S)70 %02/16/23 16:14 321-60-802/16/23 08:5240-140 1
2-Bromonaphthalene (S)75 %02/16/23 16:14 580-13-202/16/23 08:5240-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 02/12/23 15:23 83-32-902/10/23 19:274161
Acenaphthylene ND ug/kg 02/12/23 15:23 208-96-802/10/23 19:274161
Aniline ND ug/kg 02/12/23 15:23 62-53-302/10/23 19:274161
Anthracene ND ug/kg 02/12/23 15:23 120-12-702/10/23 19:274161
Benzo(a)anthracene ND ug/kg 02/12/23 15:23 56-55-302/10/23 19:274161
Benzo(a)pyrene ND ug/kg 02/12/23 15:23 50-32-802/10/23 19:274161
Benzo(b)fluoranthene ND ug/kg 02/12/23 15:23 205-99-202/10/23 19:274161
Benzo(g,h,i)perylene ND ug/kg 02/12/23 15:23 191-24-202/10/23 19:274161
Benzo(k)fluoranthene ND ug/kg 02/12/23 15:23 207-08-902/10/23 19:274161
Benzoic Acid ND ug/kg 02/12/23 15:23 65-85-002/10/23 19:2720801
Benzyl alcohol ND ug/kg 02/12/23 15:23 100-51-602/10/23 19:278321
4-Bromophenylphenyl ether ND ug/kg 02/12/23 15:23 101-55-302/10/23 19:274161
Butylbenzylphthalate ND ug/kg 02/12/23 15:23 85-68-702/10/23 19:274161
4-Chloro-3-methylphenol ND ug/kg 02/12/23 15:23 59-50-702/10/23 19:278321
4-Chloroaniline ND ug/kg 02/12/23 15:23 106-47-802/10/23 19:278321
bis(2-Chloroethoxy)methane ND ug/kg 02/12/23 15:23 111-91-102/10/23 19:274161
bis(2-Chloroethyl) ether ND ug/kg 02/12/23 15:23 111-44-402/10/23 19:274161
2-Chloronaphthalene ND ug/kg 02/12/23 15:23 91-58-702/10/23 19:274161
2-Chlorophenol ND ug/kg 02/12/23 15:23 95-57-802/10/23 19:274161
4-Chlorophenylphenyl ether ND ug/kg 02/12/23 15:23 7005-72-302/10/23 19:274161
Chrysene ND ug/kg 02/12/23 15:23 218-01-902/10/23 19:274161
Dibenz(a,h)anthracene ND ug/kg 02/12/23 15:23 53-70-302/10/23 19:274161
Dibenzofuran ND ug/kg 02/12/23 15:23 132-64-902/10/23 19:274161
1,2-Dichlorobenzene ND ug/kg 02/12/23 15:23 95-50-102/10/23 19:274161
1,3-Dichlorobenzene ND ug/kg 02/12/23 15:23 541-73-102/10/23 19:274161
1,4-Dichlorobenzene ND ug/kg 02/12/23 15:23 106-46-702/10/23 19:274161
3,3'-Dichlorobenzidine ND ug/kg 02/12/23 15:23 91-94-102/10/23 19:278321
2,4-Dichlorophenol ND ug/kg 02/12/23 15:23 120-83-202/10/23 19:274161
Diethylphthalate ND ug/kg 02/12/23 15:23 84-66-202/10/23 19:274161
2,4-Dimethylphenol ND ug/kg 02/12/23 15:23 105-67-902/10/23 19:274161
Dimethylphthalate ND ug/kg 02/12/23 15:23 131-11-302/10/23 19:274161
Di-n-butylphthalate ND ug/kg 02/12/23 15:23 84-74-202/10/23 19:274161
4,6-Dinitro-2-methylphenol ND ug/kg 02/12/23 15:23 534-52-102/10/23 19:278321
2,4-Dinitrophenol ND ug/kg 02/12/23 15:23 51-28-5 v102/10/23 19:2720801
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-2 Lab ID:92651699003 Collected:02/09/23 10:25 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 02/12/23 15:23 121-14-202/10/23 19:274161
2,6-Dinitrotoluene ND ug/kg 02/12/23 15:23 606-20-202/10/23 19:274161
Di-n-octylphthalate ND ug/kg 02/12/23 15:23 117-84-002/10/23 19:274161
bis(2-Ethylhexyl)phthalate ND ug/kg 02/12/23 15:23 117-81-702/10/23 19:274161
Fluoranthene ND ug/kg 02/12/23 15:23 206-44-002/10/23 19:274161
Fluorene ND ug/kg 02/12/23 15:23 86-73-702/10/23 19:274161
Hexachloro-1,3-butadiene ND ug/kg 02/12/23 15:23 87-68-302/10/23 19:274161
Hexachlorobenzene ND ug/kg 02/12/23 15:23 118-74-102/10/23 19:274161
Hexachlorocyclopentadiene ND ug/kg 02/12/23 15:23 77-47-402/10/23 19:274161
Hexachloroethane ND ug/kg 02/12/23 15:23 67-72-102/10/23 19:274161
Indeno(1,2,3-cd)pyrene ND ug/kg 02/12/23 15:23 193-39-502/10/23 19:274161
Isophorone ND ug/kg 02/12/23 15:23 78-59-102/10/23 19:274161
1-Methylnaphthalene ND ug/kg 02/12/23 15:23 90-12-002/10/23 19:274161
2-Methylnaphthalene ND ug/kg 02/12/23 15:23 91-57-602/10/23 19:274161
2-Methylphenol(o-Cresol)ND ug/kg 02/12/23 15:23 95-48-702/10/23 19:274161
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/12/23 15:23 15831-10-402/10/23 19:274161
Naphthalene ND ug/kg 02/12/23 15:23 91-20-302/10/23 19:274161
2-Nitroaniline ND ug/kg 02/12/23 15:23 88-74-402/10/23 19:2720801
3-Nitroaniline ND ug/kg 02/12/23 15:23 99-09-202/10/23 19:2720801
4-Nitroaniline ND ug/kg 02/12/23 15:23 100-01-602/10/23 19:278321
Nitrobenzene ND ug/kg 02/12/23 15:23 98-95-302/10/23 19:274161
2-Nitrophenol ND ug/kg 02/12/23 15:23 88-75-502/10/23 19:274161
4-Nitrophenol ND ug/kg 02/12/23 15:23 100-02-702/10/23 19:2720801
N-Nitrosodimethylamine ND ug/kg 02/12/23 15:23 62-75-902/10/23 19:274161
N-Nitroso-di-n-propylamine ND ug/kg 02/12/23 15:23 621-64-702/10/23 19:274161
N-Nitrosodiphenylamine ND ug/kg 02/12/23 15:23 86-30-602/10/23 19:274161
Pentachlorophenol ND ug/kg 02/12/23 15:23 87-86-5 v102/10/23 19:278321
Phenanthrene ND ug/kg 02/12/23 15:23 85-01-802/10/23 19:274161
Phenol ND ug/kg 02/12/23 15:23 108-95-202/10/23 19:274161
Pyrene ND ug/kg 02/12/23 15:23 129-00-002/10/23 19:274161
1,2,4-Trichlorobenzene ND ug/kg 02/12/23 15:23 120-82-102/10/23 19:274161
2,4,5-Trichlorophenol ND ug/kg 02/12/23 15:23 95-95-402/10/23 19:274161
2,4,6-Trichlorophenol ND ug/kg 02/12/23 15:23 88-06-202/10/23 19:274161
Surrogates
Nitrobenzene-d5 (S)70 %02/12/23 15:23 4165-60-002/10/23 19:2710-130 1
2-Fluorobiphenyl (S)71 %02/12/23 15:23 321-60-802/10/23 19:2710-130 1
Terphenyl-d14 (S)67 %02/12/23 15:23 1718-51-002/10/23 19:2710-130 1
Phenol-d6 (S)69 %02/12/23 15:23 13127-88-302/10/23 19:2710-130 1
2-Fluorophenol (S)67 %02/12/23 15:23 367-12-402/10/23 19:2710-130 1
2,4,6-Tribromophenol (S)74 %02/12/23 15:23 118-79-602/10/23 19:2710-131 1
Tentatively Identified Compounds
Hexadecanoic acid 236J ug/kg 02/12/23 15:23 57-10-3 N02/10/23 19:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-2 Lab ID:92651699003 Collected:02/09/23 10:25 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/14/23 15:00 67-64-102/13/23 19:201411
Benzene ND ug/kg 02/14/23 15:00 71-43-202/13/23 19:207.1 1
Bromobenzene ND ug/kg 02/14/23 15:00 108-86-102/13/23 19:207.1 1
Bromochloromethane ND ug/kg 02/14/23 15:00 74-97-502/13/23 19:207.1 1
Bromodichloromethane ND ug/kg 02/14/23 15:00 75-27-402/13/23 19:207.1 1
Bromoform ND ug/kg 02/14/23 15:00 75-25-202/13/23 19:207.1 1
Bromomethane ND ug/kg 02/14/23 15:00 74-83-902/13/23 19:2028.3 1
2-Butanone (MEK)ND ug/kg 02/14/23 15:00 78-93-302/13/23 19:201411
n-Butylbenzene ND ug/kg 02/14/23 15:00 104-51-802/13/23 19:207.1 1
sec-Butylbenzene ND ug/kg 02/14/23 15:00 135-98-802/13/23 19:207.1 1
tert-Butylbenzene ND ug/kg 02/14/23 15:00 98-06-602/13/23 19:207.1 1
Carbon tetrachloride ND ug/kg 02/14/23 15:00 56-23-502/13/23 19:207.1 1
Chlorobenzene ND ug/kg 02/14/23 15:00 108-90-702/13/23 19:207.1 1
Chloroethane ND ug/kg 02/14/23 15:00 75-00-302/13/23 19:2014.1 1
Chloroform ND ug/kg 02/14/23 15:00 67-66-302/13/23 19:207.1 1
Chloromethane ND ug/kg 02/14/23 15:00 74-87-302/13/23 19:2014.1 1
2-Chlorotoluene ND ug/kg 02/14/23 15:00 95-49-802/13/23 19:207.1 1
4-Chlorotoluene ND ug/kg 02/14/23 15:00 106-43-402/13/23 19:207.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/14/23 15:00 96-12-8 IK02/13/23 19:207.1 1
Dibromochloromethane ND ug/kg 02/14/23 15:00 124-48-102/13/23 19:207.1 1
1,2-Dibromoethane (EDB)ND ug/kg 02/14/23 15:00 106-93-402/13/23 19:207.1 1
Dibromomethane ND ug/kg 02/14/23 15:00 74-95-302/13/23 19:207.1 1
1,2-Dichlorobenzene ND ug/kg 02/14/23 15:00 95-50-102/13/23 19:207.1 1
1,3-Dichlorobenzene ND ug/kg 02/14/23 15:00 541-73-102/13/23 19:207.1 1
1,4-Dichlorobenzene ND ug/kg 02/14/23 15:00 106-46-702/13/23 19:207.1 1
Dichlorodifluoromethane ND ug/kg 02/14/23 15:00 75-71-8 IH,v102/13/23 19:2014.1 1
1,1-Dichloroethane ND ug/kg 02/14/23 15:00 75-34-302/13/23 19:207.1 1
1,2-Dichloroethane ND ug/kg 02/14/23 15:00 107-06-202/13/23 19:207.1 1
1,1-Dichloroethene ND ug/kg 02/14/23 15:00 75-35-402/13/23 19:207.1 1
cis-1,2-Dichloroethene ND ug/kg 02/14/23 15:00 156-59-202/13/23 19:207.1 1
trans-1,2-Dichloroethene ND ug/kg 02/14/23 15:00 156-60-502/13/23 19:207.1 1
1,2-Dichloropropane ND ug/kg 02/14/23 15:00 78-87-502/13/23 19:207.1 1
1,3-Dichloropropane ND ug/kg 02/14/23 15:00 142-28-902/13/23 19:207.1 1
2,2-Dichloropropane ND ug/kg 02/14/23 15:00 594-20-7 v202/13/23 19:207.1 1
1,1-Dichloropropene ND ug/kg 02/14/23 15:00 563-58-602/13/23 19:207.1 1
cis-1,3-Dichloropropene ND ug/kg 02/14/23 15:00 10061-01-502/13/23 19:207.1 1
trans-1,3-Dichloropropene ND ug/kg 02/14/23 15:00 10061-02-602/13/23 19:207.1 1
Diisopropyl ether ND ug/kg 02/14/23 15:00 108-20-302/13/23 19:207.1 1
Ethylbenzene ND ug/kg 02/14/23 15:00 100-41-402/13/23 19:207.1 1
Hexachloro-1,3-butadiene ND ug/kg 02/14/23 15:00 87-68-302/13/23 19:2014.1 1
2-Hexanone ND ug/kg 02/14/23 15:00 591-78-602/13/23 19:2070.7 1
Isopropylbenzene (Cumene)ND ug/kg 02/14/23 15:00 98-82-802/13/23 19:207.1 1
p-Isopropyltoluene ND ug/kg 02/14/23 15:00 99-87-602/13/23 19:207.1 1
Methylene Chloride ND ug/kg 02/14/23 15:00 75-09-202/13/23 19:2028.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/14/23 15:00 108-10-102/13/23 19:2070.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-2 Lab ID:92651699003 Collected:02/09/23 10:25 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 02/14/23 15:00 1634-04-402/13/23 19:207.1 1
Naphthalene ND ug/kg 02/14/23 15:00 91-20-3 L102/13/23 19:207.1 1
n-Propylbenzene ND ug/kg 02/14/23 15:00 103-65-102/13/23 19:207.1 1
Styrene ND ug/kg 02/14/23 15:00 100-42-502/13/23 19:207.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/14/23 15:00 630-20-602/13/23 19:207.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/14/23 15:00 79-34-502/13/23 19:207.1 1
Tetrachloroethene ND ug/kg 02/14/23 15:00 127-18-402/13/23 19:207.1 1
Toluene ND ug/kg 02/14/23 15:00 108-88-302/13/23 19:207.1 1
1,2,3-Trichlorobenzene ND ug/kg 02/14/23 15:00 87-61-602/13/23 19:207.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/14/23 15:00 120-82-102/13/23 19:207.1 1
1,1,1-Trichloroethane ND ug/kg 02/14/23 15:00 71-55-602/13/23 19:207.1 1
1,1,2-Trichloroethane ND ug/kg 02/14/23 15:00 79-00-502/13/23 19:207.1 1
Trichloroethene ND ug/kg 02/14/23 15:00 79-01-602/13/23 19:207.1 1
Trichlorofluoromethane ND ug/kg 02/14/23 15:00 75-69-402/13/23 19:207.1 1
1,2,3-Trichloropropane ND ug/kg 02/14/23 15:00 96-18-402/13/23 19:207.1 1
1,2,4-Trimethylbenzene ND ug/kg 02/14/23 15:00 95-63-602/13/23 19:207.1 1
1,3,5-Trimethylbenzene ND ug/kg 02/14/23 15:00 108-67-802/13/23 19:207.1 1
Vinyl acetate ND ug/kg 02/14/23 15:00 108-05-402/13/23 19:2070.7 1
Vinyl chloride ND ug/kg 02/14/23 15:00 75-01-402/13/23 19:2014.1 1
Xylene (Total)ND ug/kg 02/14/23 15:00 1330-20-702/13/23 19:2014.1 1
m&p-Xylene ND ug/kg 02/14/23 15:00 179601-23-102/13/23 19:2014.1 1
o-Xylene ND ug/kg 02/14/23 15:00 95-47-602/13/23 19:207.1 1
Surrogates
Toluene-d8 (S)105 %02/14/23 15:00 2037-26-502/13/23 19:2070-130 1
4-Bromofluorobenzene (S)96 %02/14/23 15:00 460-00-402/13/23 19:2070-130 1
1,2-Dichloroethane-d4 (S)106 %02/14/23 15:00 17060-07-002/13/23 19:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.3 %02/10/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-3 Lab ID:92651699004 Collected:02/09/23 10:20 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 02/16/23 16:39 N202/16/23 08:5213.9 1
Aliphatic (C19-C36)ND mg/kg 02/16/23 16:39 N202/16/23 08:5213.9 1
Aromatic (C11-C22)ND mg/kg 02/16/23 16:39 N202/16/23 08:5213.9 1
Surrogates
1-Chlorooctadecane (S)55 %02/16/23 16:39 3386-33-202/16/23 08:5240-140 1
o-Terphenyl (S)46 %02/16/23 16:39 84-15-102/16/23 08:5240-140 1
2-Fluorobiphenyl (S)75 %02/16/23 16:39 321-60-802/16/23 08:5240-140 1
2-Bromonaphthalene (S)79 %02/16/23 16:39 580-13-202/16/23 08:5240-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 02/12/23 16:18 83-32-902/10/23 19:274641
Acenaphthylene ND ug/kg 02/12/23 16:18 208-96-802/10/23 19:274641
Aniline ND ug/kg 02/12/23 16:18 62-53-302/10/23 19:274641
Anthracene ND ug/kg 02/12/23 16:18 120-12-702/10/23 19:274641
Benzo(a)anthracene ND ug/kg 02/12/23 16:18 56-55-302/10/23 19:274641
Benzo(a)pyrene ND ug/kg 02/12/23 16:18 50-32-802/10/23 19:274641
Benzo(b)fluoranthene ND ug/kg 02/12/23 16:18 205-99-202/10/23 19:274641
Benzo(g,h,i)perylene ND ug/kg 02/12/23 16:18 191-24-202/10/23 19:274641
Benzo(k)fluoranthene ND ug/kg 02/12/23 16:18 207-08-902/10/23 19:274641
Benzoic Acid ND ug/kg 02/12/23 16:18 65-85-002/10/23 19:2723201
Benzyl alcohol ND ug/kg 02/12/23 16:18 100-51-602/10/23 19:279271
4-Bromophenylphenyl ether ND ug/kg 02/12/23 16:18 101-55-302/10/23 19:274641
Butylbenzylphthalate ND ug/kg 02/12/23 16:18 85-68-702/10/23 19:274641
4-Chloro-3-methylphenol ND ug/kg 02/12/23 16:18 59-50-702/10/23 19:279271
4-Chloroaniline ND ug/kg 02/12/23 16:18 106-47-802/10/23 19:279271
bis(2-Chloroethoxy)methane ND ug/kg 02/12/23 16:18 111-91-102/10/23 19:274641
bis(2-Chloroethyl) ether ND ug/kg 02/12/23 16:18 111-44-402/10/23 19:274641
2-Chloronaphthalene ND ug/kg 02/12/23 16:18 91-58-702/10/23 19:274641
2-Chlorophenol ND ug/kg 02/12/23 16:18 95-57-802/10/23 19:274641
4-Chlorophenylphenyl ether ND ug/kg 02/12/23 16:18 7005-72-302/10/23 19:274641
Chrysene ND ug/kg 02/12/23 16:18 218-01-902/10/23 19:274641
Dibenz(a,h)anthracene ND ug/kg 02/12/23 16:18 53-70-302/10/23 19:274641
Dibenzofuran ND ug/kg 02/12/23 16:18 132-64-902/10/23 19:274641
1,2-Dichlorobenzene ND ug/kg 02/12/23 16:18 95-50-102/10/23 19:274641
1,3-Dichlorobenzene ND ug/kg 02/12/23 16:18 541-73-102/10/23 19:274641
1,4-Dichlorobenzene ND ug/kg 02/12/23 16:18 106-46-702/10/23 19:274641
3,3'-Dichlorobenzidine ND ug/kg 02/12/23 16:18 91-94-102/10/23 19:279271
2,4-Dichlorophenol ND ug/kg 02/12/23 16:18 120-83-202/10/23 19:274641
Diethylphthalate ND ug/kg 02/12/23 16:18 84-66-202/10/23 19:274641
2,4-Dimethylphenol ND ug/kg 02/12/23 16:18 105-67-902/10/23 19:274641
Dimethylphthalate ND ug/kg 02/12/23 16:18 131-11-302/10/23 19:274641
Di-n-butylphthalate ND ug/kg 02/12/23 16:18 84-74-202/10/23 19:274641
4,6-Dinitro-2-methylphenol ND ug/kg 02/12/23 16:18 534-52-102/10/23 19:279271
2,4-Dinitrophenol ND ug/kg 02/12/23 16:18 51-28-5 v102/10/23 19:2723201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-3 Lab ID:92651699004 Collected:02/09/23 10:20 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 02/12/23 16:18 121-14-202/10/23 19:274641
2,6-Dinitrotoluene ND ug/kg 02/12/23 16:18 606-20-202/10/23 19:274641
Di-n-octylphthalate ND ug/kg 02/12/23 16:18 117-84-002/10/23 19:274641
bis(2-Ethylhexyl)phthalate ND ug/kg 02/12/23 16:18 117-81-702/10/23 19:274641
Fluoranthene ND ug/kg 02/12/23 16:18 206-44-002/10/23 19:274641
Fluorene ND ug/kg 02/12/23 16:18 86-73-702/10/23 19:274641
Hexachloro-1,3-butadiene ND ug/kg 02/12/23 16:18 87-68-302/10/23 19:274641
Hexachlorobenzene ND ug/kg 02/12/23 16:18 118-74-102/10/23 19:274641
Hexachlorocyclopentadiene ND ug/kg 02/12/23 16:18 77-47-402/10/23 19:274641
Hexachloroethane ND ug/kg 02/12/23 16:18 67-72-102/10/23 19:274641
Indeno(1,2,3-cd)pyrene ND ug/kg 02/12/23 16:18 193-39-502/10/23 19:274641
Isophorone ND ug/kg 02/12/23 16:18 78-59-102/10/23 19:274641
1-Methylnaphthalene ND ug/kg 02/12/23 16:18 90-12-002/10/23 19:274641
2-Methylnaphthalene ND ug/kg 02/12/23 16:18 91-57-602/10/23 19:274641
2-Methylphenol(o-Cresol)ND ug/kg 02/12/23 16:18 95-48-702/10/23 19:274641
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/12/23 16:18 15831-10-402/10/23 19:274641
Naphthalene ND ug/kg 02/12/23 16:18 91-20-302/10/23 19:274641
2-Nitroaniline ND ug/kg 02/12/23 16:18 88-74-402/10/23 19:2723201
3-Nitroaniline ND ug/kg 02/12/23 16:18 99-09-202/10/23 19:2723201
4-Nitroaniline ND ug/kg 02/12/23 16:18 100-01-602/10/23 19:279271
Nitrobenzene ND ug/kg 02/12/23 16:18 98-95-302/10/23 19:274641
2-Nitrophenol ND ug/kg 02/12/23 16:18 88-75-502/10/23 19:274641
4-Nitrophenol ND ug/kg 02/12/23 16:18 100-02-702/10/23 19:2723201
N-Nitrosodimethylamine ND ug/kg 02/12/23 16:18 62-75-902/10/23 19:274641
N-Nitroso-di-n-propylamine ND ug/kg 02/12/23 16:18 621-64-702/10/23 19:274641
N-Nitrosodiphenylamine ND ug/kg 02/12/23 16:18 86-30-602/10/23 19:274641
Pentachlorophenol ND ug/kg 02/12/23 16:18 87-86-5 v102/10/23 19:279271
Phenanthrene ND ug/kg 02/12/23 16:18 85-01-802/10/23 19:274641
Phenol ND ug/kg 02/12/23 16:18 108-95-202/10/23 19:274641
Pyrene ND ug/kg 02/12/23 16:18 129-00-002/10/23 19:274641
1,2,4-Trichlorobenzene ND ug/kg 02/12/23 16:18 120-82-102/10/23 19:274641
2,4,5-Trichlorophenol ND ug/kg 02/12/23 16:18 95-95-402/10/23 19:274641
2,4,6-Trichlorophenol ND ug/kg 02/12/23 16:18 88-06-202/10/23 19:274641
Surrogates
Nitrobenzene-d5 (S)69 %02/12/23 16:18 4165-60-002/10/23 19:2710-130 1
2-Fluorobiphenyl (S)69 %02/12/23 16:18 321-60-802/10/23 19:2710-130 1
Terphenyl-d14 (S)67 %02/12/23 16:18 1718-51-002/10/23 19:2710-130 1
Phenol-d6 (S)66 %02/12/23 16:18 13127-88-302/10/23 19:2710-130 1
2-Fluorophenol (S)66 %02/12/23 16:18 367-12-402/10/23 19:2710-130 1
2,4,6-Tribromophenol (S)74 %02/12/23 16:18 118-79-602/10/23 19:2710-131 1
Tentatively Identified Compounds
Tridecane 344J ug/kg 02/12/23 16:18 629-50-5 N02/10/23 19:271
Decane 275J ug/kg 02/12/23 16:18 124-18-5 N02/10/23 19:271
Naphthalene, 1,4-dimethy 349J ug/kg 02/12/23 16:18 571-58-4 N02/10/23 19:271
Pentadecane 346J ug/kg 02/12/23 16:18 629-62-9 N02/10/23 19:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-3 Lab ID:92651699004 Collected:02/09/23 10:20 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Tentatively Identified Compounds
Hexadecane 538J ug/kg 02/12/23 16:18 544-76-3 N02/10/23 19:271
Heptadecane 534J ug/kg 02/12/23 16:18 629-78-7 N02/10/23 19:271
n-Hexadecanoic acid 429J ug/kg 02/12/23 16:18 57-10-3 N02/10/23 19:271
9-Octadecenamide, (Z)-251J ug/kg 02/12/23 16:18 301-02-0 N02/10/23 19:271
Unknown 316J ug/kg 02/12/23 16:1802/10/23 19:271
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/14/23 15:18 67-64-102/13/23 19:201691
Benzene ND ug/kg 02/14/23 15:18 71-43-202/13/23 19:208.5 1
Bromobenzene ND ug/kg 02/14/23 15:18 108-86-102/13/23 19:208.5 1
Bromochloromethane ND ug/kg 02/14/23 15:18 74-97-502/13/23 19:208.5 1
Bromodichloromethane ND ug/kg 02/14/23 15:18 75-27-402/13/23 19:208.5 1
Bromoform ND ug/kg 02/14/23 15:18 75-25-202/13/23 19:208.5 1
Bromomethane ND ug/kg 02/14/23 15:18 74-83-902/13/23 19:2033.8 1
2-Butanone (MEK)ND ug/kg 02/14/23 15:18 78-93-302/13/23 19:201691
n-Butylbenzene ND ug/kg 02/14/23 15:18 104-51-802/13/23 19:208.5 1
sec-Butylbenzene ND ug/kg 02/14/23 15:18 135-98-802/13/23 19:208.5 1
tert-Butylbenzene ND ug/kg 02/14/23 15:18 98-06-602/13/23 19:208.5 1
Carbon tetrachloride ND ug/kg 02/14/23 15:18 56-23-502/13/23 19:208.5 1
Chlorobenzene ND ug/kg 02/14/23 15:18 108-90-702/13/23 19:208.5 1
Chloroethane ND ug/kg 02/14/23 15:18 75-00-302/13/23 19:2016.9 1
Chloroform ND ug/kg 02/14/23 15:18 67-66-302/13/23 19:208.5 1
Chloromethane ND ug/kg 02/14/23 15:18 74-87-302/13/23 19:2016.9 1
2-Chlorotoluene ND ug/kg 02/14/23 15:18 95-49-802/13/23 19:208.5 1
4-Chlorotoluene ND ug/kg 02/14/23 15:18 106-43-402/13/23 19:208.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/14/23 15:18 96-12-8 IK02/13/23 19:208.5 1
Dibromochloromethane ND ug/kg 02/14/23 15:18 124-48-102/13/23 19:208.5 1
1,2-Dibromoethane (EDB)ND ug/kg 02/14/23 15:18 106-93-402/13/23 19:208.5 1
Dibromomethane ND ug/kg 02/14/23 15:18 74-95-302/13/23 19:208.5 1
1,2-Dichlorobenzene ND ug/kg 02/14/23 15:18 95-50-102/13/23 19:208.5 1
1,3-Dichlorobenzene ND ug/kg 02/14/23 15:18 541-73-102/13/23 19:208.5 1
1,4-Dichlorobenzene ND ug/kg 02/14/23 15:18 106-46-702/13/23 19:208.5 1
Dichlorodifluoromethane ND ug/kg 02/14/23 15:18 75-71-8 IH,v102/13/23 19:2016.9 1
1,1-Dichloroethane ND ug/kg 02/14/23 15:18 75-34-302/13/23 19:208.5 1
1,2-Dichloroethane ND ug/kg 02/14/23 15:18 107-06-202/13/23 19:208.5 1
1,1-Dichloroethene ND ug/kg 02/14/23 15:18 75-35-402/13/23 19:208.5 1
cis-1,2-Dichloroethene ND ug/kg 02/14/23 15:18 156-59-202/13/23 19:208.5 1
trans-1,2-Dichloroethene ND ug/kg 02/14/23 15:18 156-60-502/13/23 19:208.5 1
1,2-Dichloropropane ND ug/kg 02/14/23 15:18 78-87-502/13/23 19:208.5 1
1,3-Dichloropropane ND ug/kg 02/14/23 15:18 142-28-902/13/23 19:208.5 1
2,2-Dichloropropane ND ug/kg 02/14/23 15:18 594-20-7 v202/13/23 19:208.5 1
1,1-Dichloropropene ND ug/kg 02/14/23 15:18 563-58-602/13/23 19:208.5 1
cis-1,3-Dichloropropene ND ug/kg 02/14/23 15:18 10061-01-502/13/23 19:208.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-3 Lab ID:92651699004 Collected:02/09/23 10:20 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
trans-1,3-Dichloropropene ND ug/kg 02/14/23 15:18 10061-02-602/13/23 19:208.5 1
Diisopropyl ether ND ug/kg 02/14/23 15:18 108-20-302/13/23 19:208.5 1
Ethylbenzene ND ug/kg 02/14/23 15:18 100-41-402/13/23 19:208.5 1
Hexachloro-1,3-butadiene ND ug/kg 02/14/23 15:18 87-68-302/13/23 19:2016.9 1
2-Hexanone ND ug/kg 02/14/23 15:18 591-78-602/13/23 19:2084.5 1
Isopropylbenzene (Cumene)ND ug/kg 02/14/23 15:18 98-82-802/13/23 19:208.5 1
p-Isopropyltoluene ND ug/kg 02/14/23 15:18 99-87-602/13/23 19:208.5 1
Methylene Chloride ND ug/kg 02/14/23 15:18 75-09-202/13/23 19:2033.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/14/23 15:18 108-10-102/13/23 19:2084.5 1
Methyl-tert-butyl ether ND ug/kg 02/14/23 15:18 1634-04-402/13/23 19:208.5 1
Naphthalene ND ug/kg 02/14/23 15:18 91-20-3 L102/13/23 19:208.5 1
n-Propylbenzene ND ug/kg 02/14/23 15:18 103-65-102/13/23 19:208.5 1
Styrene ND ug/kg 02/14/23 15:18 100-42-502/13/23 19:208.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/14/23 15:18 630-20-602/13/23 19:208.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/14/23 15:18 79-34-502/13/23 19:208.5 1
Tetrachloroethene ND ug/kg 02/14/23 15:18 127-18-402/13/23 19:208.5 1
Toluene ND ug/kg 02/14/23 15:18 108-88-302/13/23 19:208.5 1
1,2,3-Trichlorobenzene ND ug/kg 02/14/23 15:18 87-61-602/13/23 19:208.5 1
1,2,4-Trichlorobenzene ND ug/kg 02/14/23 15:18 120-82-102/13/23 19:208.5 1
1,1,1-Trichloroethane ND ug/kg 02/14/23 15:18 71-55-602/13/23 19:208.5 1
1,1,2-Trichloroethane ND ug/kg 02/14/23 15:18 79-00-502/13/23 19:208.5 1
Trichloroethene ND ug/kg 02/14/23 15:18 79-01-602/13/23 19:208.5 1
Trichlorofluoromethane ND ug/kg 02/14/23 15:18 75-69-402/13/23 19:208.5 1
1,2,3-Trichloropropane ND ug/kg 02/14/23 15:18 96-18-402/13/23 19:208.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/14/23 15:18 95-63-602/13/23 19:208.5 1
1,3,5-Trimethylbenzene ND ug/kg 02/14/23 15:18 108-67-802/13/23 19:208.5 1
Vinyl acetate ND ug/kg 02/14/23 15:18 108-05-402/13/23 19:2084.5 1
Vinyl chloride ND ug/kg 02/14/23 15:18 75-01-402/13/23 19:2016.9 1
Xylene (Total)ND ug/kg 02/14/23 15:18 1330-20-702/13/23 19:2016.9 1
m&p-Xylene ND ug/kg 02/14/23 15:18 179601-23-102/13/23 19:2016.9 1
o-Xylene ND ug/kg 02/14/23 15:18 95-47-602/13/23 19:208.5 1
Surrogates
Toluene-d8 (S)102 %02/14/23 15:18 2037-26-502/13/23 19:2070-130 1
4-Bromofluorobenzene (S)102 %02/14/23 15:18 460-00-402/13/23 19:2070-130 1
1,2-Dichloroethane-d4 (S)103 %02/14/23 15:18 17060-07-002/13/23 19:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.9 %02/10/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-4 Lab ID:92651699005 Collected:02/09/23 10:29 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 02/16/23 17:05 N202/16/23 08:5213.8 1
Aliphatic (C19-C36)ND mg/kg 02/16/23 17:05 N202/16/23 08:5213.8 1
Aromatic (C11-C22)ND mg/kg 02/16/23 17:05 N202/16/23 08:5213.8 1
Surrogates
1-Chlorooctadecane (S)63 %02/16/23 17:05 3386-33-202/16/23 08:5240-140 1
o-Terphenyl (S)40 %02/16/23 17:05 84-15-102/16/23 08:5240-140 1
2-Fluorobiphenyl (S)64 %02/16/23 17:05 321-60-802/16/23 08:5240-140 1
2-Bromonaphthalene (S)69 %02/16/23 17:05 580-13-202/16/23 08:5240-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 02/12/23 16:46 83-32-902/10/23 19:274501
Acenaphthylene ND ug/kg 02/12/23 16:46 208-96-802/10/23 19:274501
Aniline ND ug/kg 02/12/23 16:46 62-53-302/10/23 19:274501
Anthracene ND ug/kg 02/12/23 16:46 120-12-702/10/23 19:274501
Benzo(a)anthracene ND ug/kg 02/12/23 16:46 56-55-302/10/23 19:274501
Benzo(a)pyrene ND ug/kg 02/12/23 16:46 50-32-802/10/23 19:274501
Benzo(b)fluoranthene ND ug/kg 02/12/23 16:46 205-99-202/10/23 19:274501
Benzo(g,h,i)perylene ND ug/kg 02/12/23 16:46 191-24-202/10/23 19:274501
Benzo(k)fluoranthene ND ug/kg 02/12/23 16:46 207-08-902/10/23 19:274501
Benzoic Acid ND ug/kg 02/12/23 16:46 65-85-002/10/23 19:2722501
Benzyl alcohol ND ug/kg 02/12/23 16:46 100-51-602/10/23 19:279011
4-Bromophenylphenyl ether ND ug/kg 02/12/23 16:46 101-55-302/10/23 19:274501
Butylbenzylphthalate ND ug/kg 02/12/23 16:46 85-68-702/10/23 19:274501
4-Chloro-3-methylphenol ND ug/kg 02/12/23 16:46 59-50-702/10/23 19:279011
4-Chloroaniline ND ug/kg 02/12/23 16:46 106-47-802/10/23 19:279011
bis(2-Chloroethoxy)methane ND ug/kg 02/12/23 16:46 111-91-102/10/23 19:274501
bis(2-Chloroethyl) ether ND ug/kg 02/12/23 16:46 111-44-402/10/23 19:274501
2-Chloronaphthalene ND ug/kg 02/12/23 16:46 91-58-702/10/23 19:274501
2-Chlorophenol ND ug/kg 02/12/23 16:46 95-57-802/10/23 19:274501
4-Chlorophenylphenyl ether ND ug/kg 02/12/23 16:46 7005-72-302/10/23 19:274501
Chrysene ND ug/kg 02/12/23 16:46 218-01-902/10/23 19:274501
Dibenz(a,h)anthracene ND ug/kg 02/12/23 16:46 53-70-302/10/23 19:274501
Dibenzofuran ND ug/kg 02/12/23 16:46 132-64-902/10/23 19:274501
1,2-Dichlorobenzene ND ug/kg 02/12/23 16:46 95-50-102/10/23 19:274501
1,3-Dichlorobenzene ND ug/kg 02/12/23 16:46 541-73-102/10/23 19:274501
1,4-Dichlorobenzene ND ug/kg 02/12/23 16:46 106-46-702/10/23 19:274501
3,3'-Dichlorobenzidine ND ug/kg 02/12/23 16:46 91-94-102/10/23 19:279011
2,4-Dichlorophenol ND ug/kg 02/12/23 16:46 120-83-202/10/23 19:274501
Diethylphthalate ND ug/kg 02/12/23 16:46 84-66-202/10/23 19:274501
2,4-Dimethylphenol ND ug/kg 02/12/23 16:46 105-67-902/10/23 19:274501
Dimethylphthalate ND ug/kg 02/12/23 16:46 131-11-302/10/23 19:274501
Di-n-butylphthalate ND ug/kg 02/12/23 16:46 84-74-202/10/23 19:274501
4,6-Dinitro-2-methylphenol ND ug/kg 02/12/23 16:46 534-52-102/10/23 19:279011
2,4-Dinitrophenol ND ug/kg 02/12/23 16:46 51-28-5 v102/10/23 19:2722501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-4 Lab ID:92651699005 Collected:02/09/23 10:29 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 02/12/23 16:46 121-14-202/10/23 19:274501
2,6-Dinitrotoluene ND ug/kg 02/12/23 16:46 606-20-202/10/23 19:274501
Di-n-octylphthalate ND ug/kg 02/12/23 16:46 117-84-002/10/23 19:274501
bis(2-Ethylhexyl)phthalate ND ug/kg 02/12/23 16:46 117-81-702/10/23 19:274501
Fluoranthene ND ug/kg 02/12/23 16:46 206-44-002/10/23 19:274501
Fluorene ND ug/kg 02/12/23 16:46 86-73-702/10/23 19:274501
Hexachloro-1,3-butadiene ND ug/kg 02/12/23 16:46 87-68-302/10/23 19:274501
Hexachlorobenzene ND ug/kg 02/12/23 16:46 118-74-102/10/23 19:274501
Hexachlorocyclopentadiene ND ug/kg 02/12/23 16:46 77-47-402/10/23 19:274501
Hexachloroethane ND ug/kg 02/12/23 16:46 67-72-102/10/23 19:274501
Indeno(1,2,3-cd)pyrene ND ug/kg 02/12/23 16:46 193-39-502/10/23 19:274501
Isophorone ND ug/kg 02/12/23 16:46 78-59-102/10/23 19:274501
1-Methylnaphthalene ND ug/kg 02/12/23 16:46 90-12-002/10/23 19:274501
2-Methylnaphthalene ND ug/kg 02/12/23 16:46 91-57-602/10/23 19:274501
2-Methylphenol(o-Cresol)ND ug/kg 02/12/23 16:46 95-48-702/10/23 19:274501
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/12/23 16:46 15831-10-402/10/23 19:274501
Naphthalene ND ug/kg 02/12/23 16:46 91-20-302/10/23 19:274501
2-Nitroaniline ND ug/kg 02/12/23 16:46 88-74-402/10/23 19:2722501
3-Nitroaniline ND ug/kg 02/12/23 16:46 99-09-202/10/23 19:2722501
4-Nitroaniline ND ug/kg 02/12/23 16:46 100-01-602/10/23 19:279011
Nitrobenzene ND ug/kg 02/12/23 16:46 98-95-302/10/23 19:274501
2-Nitrophenol ND ug/kg 02/12/23 16:46 88-75-502/10/23 19:274501
4-Nitrophenol ND ug/kg 02/12/23 16:46 100-02-702/10/23 19:2722501
N-Nitrosodimethylamine ND ug/kg 02/12/23 16:46 62-75-902/10/23 19:274501
N-Nitroso-di-n-propylamine ND ug/kg 02/12/23 16:46 621-64-702/10/23 19:274501
N-Nitrosodiphenylamine ND ug/kg 02/12/23 16:46 86-30-602/10/23 19:274501
Pentachlorophenol ND ug/kg 02/12/23 16:46 87-86-5 v102/10/23 19:279011
Phenanthrene ND ug/kg 02/12/23 16:46 85-01-802/10/23 19:274501
Phenol ND ug/kg 02/12/23 16:46 108-95-202/10/23 19:274501
Pyrene ND ug/kg 02/12/23 16:46 129-00-002/10/23 19:274501
1,2,4-Trichlorobenzene ND ug/kg 02/12/23 16:46 120-82-102/10/23 19:274501
2,4,5-Trichlorophenol ND ug/kg 02/12/23 16:46 95-95-402/10/23 19:274501
2,4,6-Trichlorophenol ND ug/kg 02/12/23 16:46 88-06-202/10/23 19:274501
Surrogates
Nitrobenzene-d5 (S)70 %02/12/23 16:46 4165-60-002/10/23 19:2710-130 1
2-Fluorobiphenyl (S)70 %02/12/23 16:46 321-60-802/10/23 19:2710-130 1
Terphenyl-d14 (S)70 %02/12/23 16:46 1718-51-002/10/23 19:2710-130 1
Phenol-d6 (S)70 %02/12/23 16:46 13127-88-302/10/23 19:2710-130 1
2-Fluorophenol (S)69 %02/12/23 16:46 367-12-402/10/23 19:2710-130 1
2,4,6-Tribromophenol (S)79 %02/12/23 16:46 118-79-602/10/23 19:2710-131 1
Tentatively Identified Compounds
Hexadecanoic acid 233J ug/kg 02/12/23 16:46 57-10-3 N02/10/23 19:271
Unknown 276J ug/kg 02/12/23 16:4602/10/23 19:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-4 Lab ID:92651699005 Collected:02/09/23 10:29 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/14/23 15:35 67-64-102/13/23 19:201721
Benzene ND ug/kg 02/14/23 15:35 71-43-202/13/23 19:208.6 1
Bromobenzene ND ug/kg 02/14/23 15:35 108-86-102/13/23 19:208.6 1
Bromochloromethane ND ug/kg 02/14/23 15:35 74-97-502/13/23 19:208.6 1
Bromodichloromethane ND ug/kg 02/14/23 15:35 75-27-402/13/23 19:208.6 1
Bromoform ND ug/kg 02/14/23 15:35 75-25-202/13/23 19:208.6 1
Bromomethane ND ug/kg 02/14/23 15:35 74-83-902/13/23 19:2034.5 1
2-Butanone (MEK)ND ug/kg 02/14/23 15:35 78-93-302/13/23 19:201721
n-Butylbenzene ND ug/kg 02/14/23 15:35 104-51-802/13/23 19:208.6 1
sec-Butylbenzene ND ug/kg 02/14/23 15:35 135-98-802/13/23 19:208.6 1
tert-Butylbenzene ND ug/kg 02/14/23 15:35 98-06-602/13/23 19:208.6 1
Carbon tetrachloride ND ug/kg 02/14/23 15:35 56-23-502/13/23 19:208.6 1
Chlorobenzene ND ug/kg 02/14/23 15:35 108-90-702/13/23 19:208.6 1
Chloroethane ND ug/kg 02/14/23 15:35 75-00-302/13/23 19:2017.2 1
Chloroform ND ug/kg 02/14/23 15:35 67-66-302/13/23 19:208.6 1
Chloromethane ND ug/kg 02/14/23 15:35 74-87-302/13/23 19:2017.2 1
2-Chlorotoluene ND ug/kg 02/14/23 15:35 95-49-802/13/23 19:208.6 1
4-Chlorotoluene ND ug/kg 02/14/23 15:35 106-43-402/13/23 19:208.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/14/23 15:35 96-12-8 IK02/13/23 19:208.6 1
Dibromochloromethane ND ug/kg 02/14/23 15:35 124-48-102/13/23 19:208.6 1
1,2-Dibromoethane (EDB)ND ug/kg 02/14/23 15:35 106-93-402/13/23 19:208.6 1
Dibromomethane ND ug/kg 02/14/23 15:35 74-95-302/13/23 19:208.6 1
1,2-Dichlorobenzene ND ug/kg 02/14/23 15:35 95-50-102/13/23 19:208.6 1
1,3-Dichlorobenzene ND ug/kg 02/14/23 15:35 541-73-102/13/23 19:208.6 1
1,4-Dichlorobenzene ND ug/kg 02/14/23 15:35 106-46-702/13/23 19:208.6 1
Dichlorodifluoromethane ND ug/kg 02/14/23 15:35 75-71-8 IH,v102/13/23 19:2017.2 1
1,1-Dichloroethane ND ug/kg 02/14/23 15:35 75-34-302/13/23 19:208.6 1
1,2-Dichloroethane ND ug/kg 02/14/23 15:35 107-06-202/13/23 19:208.6 1
1,1-Dichloroethene ND ug/kg 02/14/23 15:35 75-35-402/13/23 19:208.6 1
cis-1,2-Dichloroethene ND ug/kg 02/14/23 15:35 156-59-202/13/23 19:208.6 1
trans-1,2-Dichloroethene ND ug/kg 02/14/23 15:35 156-60-502/13/23 19:208.6 1
1,2-Dichloropropane ND ug/kg 02/14/23 15:35 78-87-502/13/23 19:208.6 1
1,3-Dichloropropane ND ug/kg 02/14/23 15:35 142-28-902/13/23 19:208.6 1
2,2-Dichloropropane ND ug/kg 02/14/23 15:35 594-20-7 v202/13/23 19:208.6 1
1,1-Dichloropropene ND ug/kg 02/14/23 15:35 563-58-602/13/23 19:208.6 1
cis-1,3-Dichloropropene ND ug/kg 02/14/23 15:35 10061-01-502/13/23 19:208.6 1
trans-1,3-Dichloropropene ND ug/kg 02/14/23 15:35 10061-02-602/13/23 19:208.6 1
Diisopropyl ether ND ug/kg 02/14/23 15:35 108-20-302/13/23 19:208.6 1
Ethylbenzene ND ug/kg 02/14/23 15:35 100-41-402/13/23 19:208.6 1
Hexachloro-1,3-butadiene ND ug/kg 02/14/23 15:35 87-68-302/13/23 19:2017.2 1
2-Hexanone ND ug/kg 02/14/23 15:35 591-78-602/13/23 19:2086.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/14/23 15:35 98-82-802/13/23 19:208.6 1
p-Isopropyltoluene ND ug/kg 02/14/23 15:35 99-87-602/13/23 19:208.6 1
Methylene Chloride ND ug/kg 02/14/23 15:35 75-09-202/13/23 19:2034.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/14/23 15:35 108-10-102/13/23 19:2086.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
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Page 20 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-4 Lab ID:92651699005 Collected:02/09/23 10:29 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 02/14/23 15:35 1634-04-402/13/23 19:208.6 1
Naphthalene ND ug/kg 02/14/23 15:35 91-20-3 L102/13/23 19:208.6 1
n-Propylbenzene ND ug/kg 02/14/23 15:35 103-65-102/13/23 19:208.6 1
Styrene ND ug/kg 02/14/23 15:35 100-42-502/13/23 19:208.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/14/23 15:35 630-20-602/13/23 19:208.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/14/23 15:35 79-34-502/13/23 19:208.6 1
Tetrachloroethene ND ug/kg 02/14/23 15:35 127-18-402/13/23 19:208.6 1
Toluene ND ug/kg 02/14/23 15:35 108-88-302/13/23 19:208.6 1
1,2,3-Trichlorobenzene ND ug/kg 02/14/23 15:35 87-61-602/13/23 19:208.6 1
1,2,4-Trichlorobenzene ND ug/kg 02/14/23 15:35 120-82-102/13/23 19:208.6 1
1,1,1-Trichloroethane ND ug/kg 02/14/23 15:35 71-55-602/13/23 19:208.6 1
1,1,2-Trichloroethane ND ug/kg 02/14/23 15:35 79-00-502/13/23 19:208.6 1
Trichloroethene ND ug/kg 02/14/23 15:35 79-01-602/13/23 19:208.6 1
Trichlorofluoromethane ND ug/kg 02/14/23 15:35 75-69-402/13/23 19:208.6 1
1,2,3-Trichloropropane ND ug/kg 02/14/23 15:35 96-18-402/13/23 19:208.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/14/23 15:35 95-63-602/13/23 19:208.6 1
1,3,5-Trimethylbenzene ND ug/kg 02/14/23 15:35 108-67-802/13/23 19:208.6 1
Vinyl acetate ND ug/kg 02/14/23 15:35 108-05-402/13/23 19:2086.2 1
Vinyl chloride ND ug/kg 02/14/23 15:35 75-01-402/13/23 19:2017.2 1
Xylene (Total)ND ug/kg 02/14/23 15:35 1330-20-702/13/23 19:2017.2 1
m&p-Xylene ND ug/kg 02/14/23 15:35 179601-23-102/13/23 19:2017.2 1
o-Xylene ND ug/kg 02/14/23 15:35 95-47-602/13/23 19:208.6 1
Surrogates
Toluene-d8 (S)94 %02/14/23 15:35 2037-26-502/13/23 19:2070-130 1
4-Bromofluorobenzene (S)115 %02/14/23 15:35 460-00-402/13/23 19:2070-130 1
1,2-Dichloroethane-d4 (S)107 %02/14/23 15:35 17060-07-002/13/23 19:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.0 %02/10/23 15:26 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-5 Lab ID:92651699006 Collected:02/09/23 10:40 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 02/20/23 15:18 N202/20/23 09:1611.9 1
Aliphatic (C19-C36)ND mg/kg 02/20/23 15:18 N202/20/23 09:1611.9 1
Aromatic (C11-C22)ND mg/kg 02/20/23 15:18 N202/20/23 09:1611.9 1
Surrogates
1-Chlorooctadecane (S)64 %02/20/23 15:18 3386-33-202/20/23 09:1640-140 1
o-Terphenyl (S)60 %02/20/23 15:18 84-15-102/20/23 09:1640-140 1
2-Fluorobiphenyl (S)79 %02/20/23 15:18 321-60-802/20/23 09:1640-140 1
2-Bromonaphthalene (S)84 %02/20/23 15:18 580-13-202/20/23 09:1640-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 02/12/23 17:14 83-32-902/10/23 19:273841
Acenaphthylene ND ug/kg 02/12/23 17:14 208-96-802/10/23 19:273841
Aniline ND ug/kg 02/12/23 17:14 62-53-302/10/23 19:273841
Anthracene ND ug/kg 02/12/23 17:14 120-12-702/10/23 19:273841
Benzo(a)anthracene ND ug/kg 02/12/23 17:14 56-55-302/10/23 19:273841
Benzo(a)pyrene ND ug/kg 02/12/23 17:14 50-32-802/10/23 19:273841
Benzo(b)fluoranthene ND ug/kg 02/12/23 17:14 205-99-202/10/23 19:273841
Benzo(g,h,i)perylene ND ug/kg 02/12/23 17:14 191-24-202/10/23 19:273841
Benzo(k)fluoranthene ND ug/kg 02/12/23 17:14 207-08-902/10/23 19:273841
Benzoic Acid ND ug/kg 02/12/23 17:14 65-85-002/10/23 19:2719201
Benzyl alcohol ND ug/kg 02/12/23 17:14 100-51-602/10/23 19:277681
4-Bromophenylphenyl ether ND ug/kg 02/12/23 17:14 101-55-302/10/23 19:273841
Butylbenzylphthalate ND ug/kg 02/12/23 17:14 85-68-702/10/23 19:273841
4-Chloro-3-methylphenol ND ug/kg 02/12/23 17:14 59-50-702/10/23 19:277681
4-Chloroaniline ND ug/kg 02/12/23 17:14 106-47-802/10/23 19:277681
bis(2-Chloroethoxy)methane ND ug/kg 02/12/23 17:14 111-91-102/10/23 19:273841
bis(2-Chloroethyl) ether ND ug/kg 02/12/23 17:14 111-44-402/10/23 19:273841
2-Chloronaphthalene ND ug/kg 02/12/23 17:14 91-58-702/10/23 19:273841
2-Chlorophenol ND ug/kg 02/12/23 17:14 95-57-802/10/23 19:273841
4-Chlorophenylphenyl ether ND ug/kg 02/12/23 17:14 7005-72-302/10/23 19:273841
Chrysene ND ug/kg 02/12/23 17:14 218-01-902/10/23 19:273841
Dibenz(a,h)anthracene ND ug/kg 02/12/23 17:14 53-70-302/10/23 19:273841
Dibenzofuran ND ug/kg 02/12/23 17:14 132-64-902/10/23 19:273841
1,2-Dichlorobenzene ND ug/kg 02/12/23 17:14 95-50-102/10/23 19:273841
1,3-Dichlorobenzene ND ug/kg 02/12/23 17:14 541-73-102/10/23 19:273841
1,4-Dichlorobenzene ND ug/kg 02/12/23 17:14 106-46-702/10/23 19:273841
3,3'-Dichlorobenzidine ND ug/kg 02/12/23 17:14 91-94-102/10/23 19:277681
2,4-Dichlorophenol ND ug/kg 02/12/23 17:14 120-83-202/10/23 19:273841
Diethylphthalate ND ug/kg 02/12/23 17:14 84-66-202/10/23 19:273841
2,4-Dimethylphenol ND ug/kg 02/12/23 17:14 105-67-902/10/23 19:273841
Dimethylphthalate ND ug/kg 02/12/23 17:14 131-11-302/10/23 19:273841
Di-n-butylphthalate ND ug/kg 02/12/23 17:14 84-74-202/10/23 19:273841
4,6-Dinitro-2-methylphenol ND ug/kg 02/12/23 17:14 534-52-102/10/23 19:277681
2,4-Dinitrophenol ND ug/kg 02/12/23 17:14 51-28-5 v102/10/23 19:2719201
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-5 Lab ID:92651699006 Collected:02/09/23 10:40 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 02/12/23 17:14 121-14-202/10/23 19:273841
2,6-Dinitrotoluene ND ug/kg 02/12/23 17:14 606-20-202/10/23 19:273841
Di-n-octylphthalate ND ug/kg 02/12/23 17:14 117-84-002/10/23 19:273841
bis(2-Ethylhexyl)phthalate ND ug/kg 02/12/23 17:14 117-81-702/10/23 19:273841
Fluoranthene ND ug/kg 02/12/23 17:14 206-44-002/10/23 19:273841
Fluorene ND ug/kg 02/12/23 17:14 86-73-702/10/23 19:273841
Hexachloro-1,3-butadiene ND ug/kg 02/12/23 17:14 87-68-302/10/23 19:273841
Hexachlorobenzene ND ug/kg 02/12/23 17:14 118-74-102/10/23 19:273841
Hexachlorocyclopentadiene ND ug/kg 02/12/23 17:14 77-47-402/10/23 19:273841
Hexachloroethane ND ug/kg 02/12/23 17:14 67-72-102/10/23 19:273841
Indeno(1,2,3-cd)pyrene ND ug/kg 02/12/23 17:14 193-39-502/10/23 19:273841
Isophorone ND ug/kg 02/12/23 17:14 78-59-102/10/23 19:273841
1-Methylnaphthalene ND ug/kg 02/12/23 17:14 90-12-002/10/23 19:273841
2-Methylnaphthalene ND ug/kg 02/12/23 17:14 91-57-602/10/23 19:273841
2-Methylphenol(o-Cresol)ND ug/kg 02/12/23 17:14 95-48-702/10/23 19:273841
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/12/23 17:14 15831-10-402/10/23 19:273841
Naphthalene ND ug/kg 02/12/23 17:14 91-20-302/10/23 19:273841
2-Nitroaniline ND ug/kg 02/12/23 17:14 88-74-402/10/23 19:2719201
3-Nitroaniline ND ug/kg 02/12/23 17:14 99-09-202/10/23 19:2719201
4-Nitroaniline ND ug/kg 02/12/23 17:14 100-01-602/10/23 19:277681
Nitrobenzene ND ug/kg 02/12/23 17:14 98-95-302/10/23 19:273841
2-Nitrophenol ND ug/kg 02/12/23 17:14 88-75-502/10/23 19:273841
4-Nitrophenol ND ug/kg 02/12/23 17:14 100-02-702/10/23 19:2719201
N-Nitrosodimethylamine ND ug/kg 02/12/23 17:14 62-75-902/10/23 19:273841
N-Nitroso-di-n-propylamine ND ug/kg 02/12/23 17:14 621-64-702/10/23 19:273841
N-Nitrosodiphenylamine ND ug/kg 02/12/23 17:14 86-30-602/10/23 19:273841
Pentachlorophenol ND ug/kg 02/12/23 17:14 87-86-5 v102/10/23 19:277681
Phenanthrene ND ug/kg 02/12/23 17:14 85-01-802/10/23 19:273841
Phenol ND ug/kg 02/12/23 17:14 108-95-202/10/23 19:273841
Pyrene ND ug/kg 02/12/23 17:14 129-00-002/10/23 19:273841
1,2,4-Trichlorobenzene ND ug/kg 02/12/23 17:14 120-82-102/10/23 19:273841
2,4,5-Trichlorophenol ND ug/kg 02/12/23 17:14 95-95-402/10/23 19:273841
2,4,6-Trichlorophenol ND ug/kg 02/12/23 17:14 88-06-202/10/23 19:273841
Surrogates
Nitrobenzene-d5 (S)59 %02/12/23 17:14 4165-60-002/10/23 19:2710-130 1
2-Fluorobiphenyl (S)63 %02/12/23 17:14 321-60-802/10/23 19:2710-130 1
Terphenyl-d14 (S)62 %02/12/23 17:14 1718-51-002/10/23 19:2710-130 1
Phenol-d6 (S)62 %02/12/23 17:14 13127-88-302/10/23 19:2710-130 1
2-Fluorophenol (S)60 %02/12/23 17:14 367-12-402/10/23 19:2710-130 1
2,4,6-Tribromophenol (S)67 %02/12/23 17:14 118-79-602/10/23 19:2710-131 1
Tentatively Identified Compounds
n-Hexadecanoic acid 288J ug/kg 02/12/23 17:14 57-10-3 N02/10/23 19:271
Unknown 227J ug/kg 02/12/23 17:1402/10/23 19:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-5 Lab ID:92651699006 Collected:02/09/23 10:40 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/14/23 15:53 67-64-102/13/23 19:2097.6 1
Benzene ND ug/kg 02/14/23 15:53 71-43-202/13/23 19:204.9 1
Bromobenzene ND ug/kg 02/14/23 15:53 108-86-102/13/23 19:204.9 1
Bromochloromethane ND ug/kg 02/14/23 15:53 74-97-502/13/23 19:204.9 1
Bromodichloromethane ND ug/kg 02/14/23 15:53 75-27-402/13/23 19:204.9 1
Bromoform ND ug/kg 02/14/23 15:53 75-25-202/13/23 19:204.9 1
Bromomethane ND ug/kg 02/14/23 15:53 74-83-902/13/23 19:2019.5 1
2-Butanone (MEK)ND ug/kg 02/14/23 15:53 78-93-302/13/23 19:2097.6 1
n-Butylbenzene ND ug/kg 02/14/23 15:53 104-51-802/13/23 19:204.9 1
sec-Butylbenzene ND ug/kg 02/14/23 15:53 135-98-802/13/23 19:204.9 1
tert-Butylbenzene ND ug/kg 02/14/23 15:53 98-06-602/13/23 19:204.9 1
Carbon tetrachloride ND ug/kg 02/14/23 15:53 56-23-502/13/23 19:204.9 1
Chlorobenzene ND ug/kg 02/14/23 15:53 108-90-702/13/23 19:204.9 1
Chloroethane ND ug/kg 02/14/23 15:53 75-00-302/13/23 19:209.8 1
Chloroform ND ug/kg 02/14/23 15:53 67-66-302/13/23 19:204.9 1
Chloromethane ND ug/kg 02/14/23 15:53 74-87-302/13/23 19:209.8 1
2-Chlorotoluene ND ug/kg 02/14/23 15:53 95-49-802/13/23 19:204.9 1
4-Chlorotoluene ND ug/kg 02/14/23 15:53 106-43-402/13/23 19:204.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/14/23 15:53 96-12-8 IK02/13/23 19:204.9 1
Dibromochloromethane ND ug/kg 02/14/23 15:53 124-48-102/13/23 19:204.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/14/23 15:53 106-93-402/13/23 19:204.9 1
Dibromomethane ND ug/kg 02/14/23 15:53 74-95-302/13/23 19:204.9 1
1,2-Dichlorobenzene ND ug/kg 02/14/23 15:53 95-50-102/13/23 19:204.9 1
1,3-Dichlorobenzene ND ug/kg 02/14/23 15:53 541-73-102/13/23 19:204.9 1
1,4-Dichlorobenzene ND ug/kg 02/14/23 15:53 106-46-702/13/23 19:204.9 1
Dichlorodifluoromethane ND ug/kg 02/14/23 15:53 75-71-8 IH,v102/13/23 19:209.8 1
1,1-Dichloroethane ND ug/kg 02/14/23 15:53 75-34-302/13/23 19:204.9 1
1,2-Dichloroethane ND ug/kg 02/14/23 15:53 107-06-202/13/23 19:204.9 1
1,1-Dichloroethene ND ug/kg 02/14/23 15:53 75-35-402/13/23 19:204.9 1
cis-1,2-Dichloroethene ND ug/kg 02/14/23 15:53 156-59-202/13/23 19:204.9 1
trans-1,2-Dichloroethene ND ug/kg 02/14/23 15:53 156-60-502/13/23 19:204.9 1
1,2-Dichloropropane ND ug/kg 02/14/23 15:53 78-87-502/13/23 19:204.9 1
1,3-Dichloropropane ND ug/kg 02/14/23 15:53 142-28-902/13/23 19:204.9 1
2,2-Dichloropropane ND ug/kg 02/14/23 15:53 594-20-7 v202/13/23 19:204.9 1
1,1-Dichloropropene ND ug/kg 02/14/23 15:53 563-58-602/13/23 19:204.9 1
cis-1,3-Dichloropropene ND ug/kg 02/14/23 15:53 10061-01-502/13/23 19:204.9 1
trans-1,3-Dichloropropene ND ug/kg 02/14/23 15:53 10061-02-602/13/23 19:204.9 1
Diisopropyl ether ND ug/kg 02/14/23 15:53 108-20-302/13/23 19:204.9 1
Ethylbenzene ND ug/kg 02/14/23 15:53 100-41-402/13/23 19:204.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/14/23 15:53 87-68-302/13/23 19:209.8 1
2-Hexanone ND ug/kg 02/14/23 15:53 591-78-602/13/23 19:2048.8 1
Isopropylbenzene (Cumene)ND ug/kg 02/14/23 15:53 98-82-802/13/23 19:204.9 1
p-Isopropyltoluene ND ug/kg 02/14/23 15:53 99-87-602/13/23 19:204.9 1
Methylene Chloride ND ug/kg 02/14/23 15:53 75-09-202/13/23 19:2019.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/14/23 15:53 108-10-102/13/23 19:2048.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92651699
ENGLISH
Sample:CS-5 Lab ID:92651699006 Collected:02/09/23 10:40 Received:02/10/23 05:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 02/14/23 15:53 1634-04-402/13/23 19:204.9 1
Naphthalene ND ug/kg 02/14/23 15:53 91-20-3 L102/13/23 19:204.9 1
n-Propylbenzene ND ug/kg 02/14/23 15:53 103-65-102/13/23 19:204.9 1
Styrene ND ug/kg 02/14/23 15:53 100-42-502/13/23 19:204.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/14/23 15:53 630-20-602/13/23 19:204.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/14/23 15:53 79-34-502/13/23 19:204.9 1
Tetrachloroethene ND ug/kg 02/14/23 15:53 127-18-402/13/23 19:204.9 1
Toluene ND ug/kg 02/14/23 15:53 108-88-302/13/23 19:204.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/14/23 15:53 87-61-602/13/23 19:204.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/14/23 15:53 120-82-102/13/23 19:204.9 1
1,1,1-Trichloroethane ND ug/kg 02/14/23 15:53 71-55-602/13/23 19:204.9 1
1,1,2-Trichloroethane ND ug/kg 02/14/23 15:53 79-00-502/13/23 19:204.9 1
Trichloroethene ND ug/kg 02/14/23 15:53 79-01-602/13/23 19:204.9 1
Trichlorofluoromethane ND ug/kg 02/14/23 15:53 75-69-402/13/23 19:204.9 1
1,2,3-Trichloropropane ND ug/kg 02/14/23 15:53 96-18-402/13/23 19:204.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/14/23 15:53 95-63-602/13/23 19:204.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/14/23 15:53 108-67-802/13/23 19:204.9 1
Vinyl acetate ND ug/kg 02/14/23 15:53 108-05-402/13/23 19:2048.8 1
Vinyl chloride ND ug/kg 02/14/23 15:53 75-01-402/13/23 19:209.8 1
Xylene (Total)ND ug/kg 02/14/23 15:53 1330-20-702/13/23 19:209.8 1
m&p-Xylene ND ug/kg 02/14/23 15:53 179601-23-102/13/23 19:209.8 1
o-Xylene ND ug/kg 02/14/23 15:53 95-47-602/13/23 19:204.9 1
Surrogates
Toluene-d8 (S)101 %02/14/23 15:53 2037-26-502/13/23 19:2070-130 1
4-Bromofluorobenzene (S)102 %02/14/23 15:53 460-00-402/13/23 19:2070-130 1
1,2-Dichloroethane-d4 (S)105 %02/14/23 15:53 17060-07-002/13/23 19:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.4 %02/10/23 15:27 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755472
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3925076
Associated Lab Samples:92651699001
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 02/13/23 13:32
4-Bromofluorobenzene (S)%90 66-130 02/13/23 13:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3925077LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 48.649.9 97 70-130
4-Bromofluorobenzene (S)%91 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3925079MATRIX SPIKE SAMPLE:
MSSpike
Result
92651501002
Gas Range Organics (C6-C10)mg/kg 73.363.6 114 65-146ND
4-Bromofluorobenzene (S)%91 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651501001
3925078SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755604
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3925913
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 02/14/23 12:22
1,1,1-Trichloroethane ug/kg ND 5.0 02/14/23 12:22
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 02/14/23 12:22
1,1,2-Trichloroethane ug/kg ND 5.0 02/14/23 12:22
1,1-Dichloroethane ug/kg ND 5.0 02/14/23 12:22
1,1-Dichloroethene ug/kg ND 5.0 02/14/23 12:22
1,1-Dichloropropene ug/kg ND 5.0 02/14/23 12:22
1,2,3-Trichlorobenzene ug/kg ND 5.0 02/14/23 12:22
1,2,3-Trichloropropane ug/kg ND 5.0 02/14/23 12:22
1,2,4-Trichlorobenzene ug/kg ND 5.0 02/14/23 12:22
1,2,4-Trimethylbenzene ug/kg ND 5.0 02/14/23 12:22
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 IK02/14/23 12:22
1,2-Dibromoethane (EDB)ug/kg ND 5.0 02/14/23 12:22
1,2-Dichlorobenzene ug/kg ND 5.0 02/14/23 12:22
1,2-Dichloroethane ug/kg ND 5.0 02/14/23 12:22
1,2-Dichloropropane ug/kg ND 5.0 02/14/23 12:22
1,3,5-Trimethylbenzene ug/kg ND 5.0 02/14/23 12:22
1,3-Dichlorobenzene ug/kg ND 5.0 02/14/23 12:22
1,3-Dichloropropane ug/kg ND 5.0 02/14/23 12:22
1,4-Dichlorobenzene ug/kg ND 5.0 02/14/23 12:22
2,2-Dichloropropane ug/kg ND 5.0 v202/14/23 12:22
2-Butanone (MEK)ug/kg ND 100 02/14/23 12:22
2-Chlorotoluene ug/kg ND 5.0 02/14/23 12:22
2-Hexanone ug/kg ND 50.0 02/14/23 12:22
4-Chlorotoluene ug/kg ND 5.0 02/14/23 12:22
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 02/14/23 12:22
Acetone ug/kg ND 100 02/14/23 12:22
Benzene ug/kg ND 5.0 02/14/23 12:22
Bromobenzene ug/kg ND 5.0 02/14/23 12:22
Bromochloromethane ug/kg ND 5.0 02/14/23 12:22
Bromodichloromethane ug/kg ND 5.0 02/14/23 12:22
Bromoform ug/kg ND 5.0 02/14/23 12:22
Bromomethane ug/kg ND 20.0 02/14/23 12:22
Carbon tetrachloride ug/kg ND 5.0 02/14/23 12:22
Chlorobenzene ug/kg ND 5.0 02/14/23 12:22
Chloroethane ug/kg ND 10.0 02/14/23 12:22
Chloroform ug/kg ND 5.0 02/14/23 12:22
Chloromethane ug/kg ND 10.0 02/14/23 12:22
cis-1,2-Dichloroethene ug/kg ND 5.0 02/14/23 12:22
cis-1,3-Dichloropropene ug/kg ND 5.0 02/14/23 12:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3925913
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 02/14/23 12:22
Dibromomethane ug/kg ND 5.0 02/14/23 12:22
Dichlorodifluoromethane ug/kg ND 10.0 IH,v102/14/23 12:22
Diisopropyl ether ug/kg ND 5.0 02/14/23 12:22
Ethylbenzene ug/kg ND 5.0 02/14/23 12:22
Hexachloro-1,3-butadiene ug/kg ND 10.0 02/14/23 12:22
Isopropylbenzene (Cumene)ug/kg ND 5.0 02/14/23 12:22
m&p-Xylene ug/kg ND 10.0 02/14/23 12:22
Methyl-tert-butyl ether ug/kg ND 5.0 02/14/23 12:22
Methylene Chloride ug/kg ND 20.0 02/14/23 12:22
n-Butylbenzene ug/kg ND 5.0 02/14/23 12:22
n-Propylbenzene ug/kg ND 5.0 02/14/23 12:22
Naphthalene ug/kg ND 5.0 02/14/23 12:22
o-Xylene ug/kg ND 5.0 02/14/23 12:22
p-Isopropyltoluene ug/kg ND 5.0 02/14/23 12:22
sec-Butylbenzene ug/kg ND 5.0 02/14/23 12:22
Styrene ug/kg ND 5.0 02/14/23 12:22
tert-Butylbenzene ug/kg ND 5.0 02/14/23 12:22
Tetrachloroethene ug/kg ND 5.0 02/14/23 12:22
Toluene ug/kg ND 5.0 02/14/23 12:22
trans-1,2-Dichloroethene ug/kg ND 5.0 02/14/23 12:22
trans-1,3-Dichloropropene ug/kg ND 5.0 02/14/23 12:22
Trichloroethene ug/kg ND 5.0 02/14/23 12:22
Trichlorofluoromethane ug/kg ND 5.0 02/14/23 12:22
Vinyl acetate ug/kg ND 50.0 02/14/23 12:22
Vinyl chloride ug/kg ND 10.0 02/14/23 12:22
Xylene (Total)ug/kg ND 10.0 02/14/23 12:22
1,2-Dichloroethane-d4 (S)%106 70-130 02/14/23 12:22
4-Bromofluorobenzene (S)%113 70-130 02/14/23 12:22
Toluene-d8 (S)%102 70-130 02/14/23 12:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3925914LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 476500 95 70-130
1,1,1-Trichloroethane ug/kg 473500 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 481500 96 70-130
1,1,2-Trichloroethane ug/kg 485500 97 70-130
1,1-Dichloroethane ug/kg 458500 92 70-130
1,1-Dichloroethene ug/kg 501500 100 70-130
1,1-Dichloropropene ug/kg 468500 94 70-130
1,2,3-Trichlorobenzene ug/kg 640500 128 70-130
1,2,3-Trichloropropane ug/kg 455500 91 70-130
1,2,4-Trichlorobenzene ug/kg 513500 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3925914LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 517500 103 70-130
1,2-Dibromo-3-chloropropane ug/kg 485 IK5009767-130
1,2-Dibromoethane (EDB)ug/kg 480500 96 70-130
1,2-Dichlorobenzene ug/kg 470500 94 70-130
1,2-Dichloroethane ug/kg 476500 95 70-130
1,2-Dichloropropane ug/kg 482500 96 70-130
1,3,5-Trimethylbenzene ug/kg 515500 103 70-130
1,3-Dichlorobenzene ug/kg 468500 94 70-130
1,3-Dichloropropane ug/kg 456500 91 70-130
1,4-Dichlorobenzene ug/kg 464500 93 70-130
2,2-Dichloropropane ug/kg 371 v35007467-130
2-Butanone (MEK)ug/kg 9611000 96 66-130
2-Chlorotoluene ug/kg 503500 101 70-130
2-Hexanone ug/kg 10201000 102 70-130
4-Chlorotoluene ug/kg 490500 98 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9911000 99 70-130
Acetone ug/kg 10101000 101 67-130
Benzene ug/kg 472500 94 70-130
Bromobenzene ug/kg 494500 99 70-130
Bromochloromethane ug/kg 503500 101 70-130
Bromodichloromethane ug/kg 457500 91 70-130
Bromoform ug/kg 467500 93 70-130
Bromomethane ug/kg 452500 90 53-175
Carbon tetrachloride ug/kg 487500 97 70-130
Chlorobenzene ug/kg 455500 91 70-130
Chloroethane ug/kg 464500 93 70-135
Chloroform ug/kg 447500 89 70-130
Chloromethane ug/kg 531500 106 64-130
cis-1,2-Dichloroethene ug/kg 477500 95 70-130
cis-1,3-Dichloropropene ug/kg 470500 94 70-130
Dibromochloromethane ug/kg 490500 98 70-130
Dibromomethane ug/kg 490500 98 70-130
Dichlorodifluoromethane ug/kg 574 IH,v150011563-145
Diisopropyl ether ug/kg 441500 88 68-130
Ethylbenzene ug/kg 438500 88 70-130
Hexachloro-1,3-butadiene ug/kg 477500 95 70-130
Isopropylbenzene (Cumene)ug/kg 495500 99 70-130
m&p-Xylene ug/kg 9461000 95 70-130
Methyl-tert-butyl ether ug/kg 428500 86 70-130
Methylene Chloride ug/kg 510500 102 67-130
n-Butylbenzene ug/kg 441500 88 70-130
n-Propylbenzene ug/kg 482500 96 70-130
Naphthalene ug/kg 660 L150013270-130
o-Xylene ug/kg 458500 92 70-130
p-Isopropyltoluene ug/kg 466500 93 70-130
sec-Butylbenzene ug/kg 482500 96 70-130
Styrene ug/kg 484500 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3925914LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 494500 99 64-130
Tetrachloroethene ug/kg 481500 96 70-130
Toluene ug/kg 460500 92 70-130
trans-1,2-Dichloroethene ug/kg 473500 95 70-130
trans-1,3-Dichloropropene ug/kg 461500 92 70-130
Trichloroethene ug/kg 462500 92 70-130
Trichlorofluoromethane ug/kg 415500 83 70-130
Vinyl acetate ug/kg 9681000 97 70-134
Vinyl chloride ug/kg 415500 83 68-130
Xylene (Total)ug/kg 14001500 94 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3925915MATRIX SPIKE SAMPLE:
MSSpike
Result
92651857001
1,1,1,2-Tetrachloroethane ug/kg 812773 105 58-140ND
1,1,1-Trichloroethane ug/kg 957773 124 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 788773 102 52-139ND
1,1,2-Trichloroethane ug/kg 886773 115 56-140ND
1,1-Dichloroethane ug/kg 907773 117 58-145ND
1,1-Dichloroethene ug/kg 1090773 140 57-158ND
1,1-Dichloropropene ug/kg 957773 124 58-151ND
1,2,3-Trichlorobenzene ug/kg 847773 110 48-149ND
1,2,3-Trichloropropane ug/kg 704773 91 54-132ND
1,2,4-Trichlorobenzene ug/kg 743773 96 51-151ND
1,2,4-Trimethylbenzene ug/kg 823773 106 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 573 IK7737444-134ND
1,2-Dibromoethane (EDB)ug/kg 757773 98 60-138ND
1,2-Dichlorobenzene ug/kg 850773 110 59-147ND
1,2-Dichloroethane ug/kg 819773 106 57-139ND
1,2-Dichloropropane ug/kg 896773 116 62-145ND
1,3,5-Trimethylbenzene ug/kg 839773 109 47-159ND
1,3-Dichlorobenzene ug/kg 840773 109 58-144ND
1,3-Dichloropropane ug/kg 751773 97 60-142ND
1,4-Dichlorobenzene ug/kg 768773 99 57-143ND
2,2-Dichloropropane ug/kg 706 v37739137-144ND
2-Butanone (MEK)ug/kg 14801540 96 28-146ND
2-Chlorotoluene ug/kg 802773 104 55-158ND
2-Hexanone ug/kg 12501540 81 44-141ND
4-Chlorotoluene ug/kg 794773 103 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 15101540 97 50-138ND
Acetone ug/kg 13801540 89 20-136ND
Benzene ug/kg 946773 122 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3925915MATRIX SPIKE SAMPLE:
MSSpike
Result
92651857001
Bromobenzene ug/kg 756773 98 59-145ND
Bromochloromethane ug/kg 942773 122 57-143ND
Bromodichloromethane ug/kg 817773 106 53-133ND
Bromoform ug/kg 708773 92 48-133ND
Bromomethane ug/kg 488773 63 10-167ND
Carbon tetrachloride ug/kg 845773 109 57-147ND
Chlorobenzene ug/kg 812773 105 61-144ND
Chloroethane ug/kg 458773 59 10-153ND
Chloroform ug/kg 885773 115 58-141ND
Chloromethane ug/kg 1060773 137 54-165ND
cis-1,2-Dichloroethene ug/kg 933773 121 59-144ND
cis-1,3-Dichloropropene ug/kg 872773 113 56-137ND
Dibromochloromethane ug/kg 734773 95 53-139ND
Dibromomethane ug/kg 822773 106 60-136ND
Dichlorodifluoromethane ug/kg 1500 IH,M1,v177319449-177ND
Diisopropyl ether ug/kg 862773 112 53-136ND
Ethylbenzene ug/kg 847773 100 53-1500.075 mg/kg
Hexachloro-1,3-butadiene ug/kg 1110773 143 42-186ND
Isopropylbenzene (Cumene)ug/kg 902773 116 62-1540.0065J mg/kg
m&p-Xylene ug/kg 20001540 107 49-1560.35 mg/kg
Methyl-tert-butyl ether ug/kg 801773 104 54-133ND
Methylene Chloride ug/kg 991773 128 50-153ND
n-Butylbenzene ug/kg 899773 116 44-174ND
n-Propylbenzene ug/kg 812773 104 52-1570.010 mg/kg
Naphthalene ug/kg 709773 79 37-1500.10 mg/kg
o-Xylene ug/kg 922773 104 54-1500.12 mg/kg
p-Isopropyltoluene ug/kg 942773 110 50-1640.092 mg/kg
sec-Butylbenzene ug/kg 897773 115 58-1610.0077J mg/kg
Styrene ug/kg 857773 110 60-1480.0054J mg/kg
tert-Butylbenzene ug/kg 860773 111 44-151ND
Tetrachloroethene ug/kg 686773 89 53-151ND
Toluene ug/kg 895773 115 52-148ND
trans-1,2-Dichloroethene ug/kg 934773 121 60-148ND
trans-1,3-Dichloropropene ug/kg 833773 108 55-133ND
Trichloroethene ug/kg 845773 109 60-148ND
Trichlorofluoromethane ug/kg 637773 83 10-154ND
Vinyl acetate ug/kg 9681540 63 50-149ND
Vinyl chloride ug/kg 893773 116 57-157ND
Xylene (Total)ug/kg 29202320 106 52-1530.47 mg/kg
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651857002
3925916SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND IK30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND v230ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH,v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651857002
3925916SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 300.0051Jmg/kg
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%107105
4-Bromofluorobenzene (S)%95100
Toluene-d8 (S)%102100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755987
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3927632
Associated Lab Samples:92651699001
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 4.9 02/16/23 10:01
n-Pentacosane (S)%82 10-130 02/16/23 10:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3927633LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 60.565.6 92 44-130
n-Pentacosane (S)%88 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3928147MATRIX SPIKE SAMPLE:
MSSpike
Result
92651523006
Diesel Range Organics(C10-C28)mg/kg 94.0104 80 10-13010.2
n-Pentacosane (S)%63 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651523004
3927635SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 43.0 D6188301410
n-Pentacosane (S)%73710
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755294
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3924483
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 325 02/12/23 10:45
1,2-Dichlorobenzene ug/kg ND 325 02/12/23 10:45
1,3-Dichlorobenzene ug/kg ND 325 02/12/23 10:45
1,4-Dichlorobenzene ug/kg ND 325 02/12/23 10:45
1-Methylnaphthalene ug/kg ND 325 02/12/23 10:45
2,4,5-Trichlorophenol ug/kg ND 325 02/12/23 10:45
2,4,6-Trichlorophenol ug/kg ND 325 02/12/23 10:45
2,4-Dichlorophenol ug/kg ND 325 02/12/23 10:45
2,4-Dimethylphenol ug/kg ND 325 02/12/23 10:45
2,4-Dinitrophenol ug/kg ND 1620 v102/12/23 10:45
2,4-Dinitrotoluene ug/kg ND 325 02/12/23 10:45
2,6-Dinitrotoluene ug/kg ND 325 02/12/23 10:45
2-Chloronaphthalene ug/kg ND 325 02/12/23 10:45
2-Chlorophenol ug/kg ND 325 02/12/23 10:45
2-Methylnaphthalene ug/kg ND 325 02/12/23 10:45
2-Methylphenol(o-Cresol)ug/kg ND 325 02/12/23 10:45
2-Nitroaniline ug/kg ND 1620 02/12/23 10:45
2-Nitrophenol ug/kg ND 325 02/12/23 10:45
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 02/12/23 10:45
3,3'-Dichlorobenzidine ug/kg ND 649 02/12/23 10:45
3-Nitroaniline ug/kg ND 1620 02/12/23 10:45
4,6-Dinitro-2-methylphenol ug/kg ND 649 02/12/23 10:45
4-Bromophenylphenyl ether ug/kg ND 325 02/12/23 10:45
4-Chloro-3-methylphenol ug/kg ND 649 02/12/23 10:45
4-Chloroaniline ug/kg ND 649 02/12/23 10:45
4-Chlorophenylphenyl ether ug/kg ND 325 02/12/23 10:45
4-Nitroaniline ug/kg ND 649 02/12/23 10:45
4-Nitrophenol ug/kg ND 1620 02/12/23 10:45
Acenaphthene ug/kg ND 325 02/12/23 10:45
Acenaphthylene ug/kg ND 325 02/12/23 10:45
Aniline ug/kg ND 325 02/12/23 10:45
Anthracene ug/kg ND 325 02/12/23 10:45
Benzo(a)anthracene ug/kg ND 325 02/12/23 10:45
Benzo(a)pyrene ug/kg ND 325 02/12/23 10:45
Benzo(b)fluoranthene ug/kg ND 325 02/12/23 10:45
Benzo(g,h,i)perylene ug/kg ND 325 02/12/23 10:45
Benzo(k)fluoranthene ug/kg ND 325 02/12/23 10:45
Benzoic Acid ug/kg ND 1620 02/12/23 10:45
Benzyl alcohol ug/kg ND 649 02/12/23 10:45
bis(2-Chloroethoxy)methane ug/kg ND 325 02/12/23 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3924483
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 325 02/12/23 10:45
bis(2-Ethylhexyl)phthalate ug/kg ND 325 02/12/23 10:45
Butylbenzylphthalate ug/kg ND 325 02/12/23 10:45
Chrysene ug/kg ND 325 02/12/23 10:45
Di-n-butylphthalate ug/kg ND 325 02/12/23 10:45
Di-n-octylphthalate ug/kg ND 325 02/12/23 10:45
Dibenz(a,h)anthracene ug/kg ND 325 02/12/23 10:45
Dibenzofuran ug/kg ND 325 02/12/23 10:45
Diethylphthalate ug/kg ND 325 02/12/23 10:45
Dimethylphthalate ug/kg ND 325 02/12/23 10:45
Fluoranthene ug/kg ND 325 02/12/23 10:45
Fluorene ug/kg ND 325 02/12/23 10:45
Hexachloro-1,3-butadiene ug/kg ND 325 02/12/23 10:45
Hexachlorobenzene ug/kg ND 325 02/12/23 10:45
Hexachlorocyclopentadiene ug/kg ND 325 02/12/23 10:45
Hexachloroethane ug/kg ND 325 02/12/23 10:45
Indeno(1,2,3-cd)pyrene ug/kg ND 325 02/12/23 10:45
Isophorone ug/kg ND 325 02/12/23 10:45
N-Nitroso-di-n-propylamine ug/kg ND 325 02/12/23 10:45
N-Nitrosodimethylamine ug/kg ND 325 02/12/23 10:45
N-Nitrosodiphenylamine ug/kg ND 325 02/12/23 10:45
Naphthalene ug/kg ND 325 02/12/23 10:45
Nitrobenzene ug/kg ND 325 02/12/23 10:45
Pentachlorophenol ug/kg ND 649 v102/12/23 10:45
Phenanthrene ug/kg ND 325 02/12/23 10:45
Phenol ug/kg ND 325 02/12/23 10:45
Pyrene ug/kg ND 325 02/12/23 10:45
2,4,6-Tribromophenol (S)%68 10-131 02/12/23 10:45
2-Fluorobiphenyl (S)%67 10-130 02/12/23 10:45
2-Fluorophenol (S)%66 10-130 02/12/23 10:45
Nitrobenzene-d5 (S)%68 10-130 02/12/23 10:45
Phenol-d6 (S)%68 10-130 02/12/23 10:45
Terphenyl-d14 (S)%59 10-130 02/12/23 10:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3924484LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11101680 66 43-130
1,2-Dichlorobenzene ug/kg 11101680 66 43-130
1,3-Dichlorobenzene ug/kg 10901680 65 43-130
1,4-Dichlorobenzene ug/kg 10901680 65 44-130
1-Methylnaphthalene ug/kg 12701680 75 47-130
2,4,5-Trichlorophenol ug/kg 12501680 74 47-130
2,4,6-Trichlorophenol ug/kg 12601680 75 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3924484LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 12001680 72 45-130
2,4-Dimethylphenol ug/kg 16501680 98 45-130
2,4-Dinitrophenol ug/kg 7160 v183908527-140
2,4-Dinitrotoluene ug/kg 12101680 72 46-130
2,6-Dinitrotoluene ug/kg 12101680 72 48-130
2-Chloronaphthalene ug/kg 11801680 70 46-130
2-Chlorophenol ug/kg 11301680 68 43-130
2-Methylnaphthalene ug/kg 12101680 72 47-130
2-Methylphenol(o-Cresol)ug/kg 12001680 72 42-130
2-Nitroaniline ug/kg 26603360 79 41-130
2-Nitrophenol ug/kg 12301680 73 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 12501680 74 39-130
3,3'-Dichlorobenzidine ug/kg 21403360 64 41-130
3-Nitroaniline ug/kg 22303360 66 37-130
4,6-Dinitro-2-methylphenol ug/kg 29103360 87 38-141
4-Bromophenylphenyl ether ug/kg 12701680 76 47-130
4-Chloro-3-methylphenol ug/kg 25403360 76 44-130
4-Chloroaniline ug/kg 23303360 70 41-130
4-Chlorophenylphenyl ether ug/kg 12501680 74 45-130
4-Nitroaniline ug/kg 25603360 76 42-130
4-Nitrophenol ug/kg 63308390 75 39-131
Acenaphthene ug/kg 12701680 76 49-130
Acenaphthylene ug/kg 12501680 74 50-130
Aniline ug/kg 10701680 64 38-130
Anthracene ug/kg 12201680 73 49-130
Benzo(a)anthracene ug/kg 12601680 75 51-130
Benzo(a)pyrene ug/kg 12401680 74 51-130
Benzo(b)fluoranthene ug/kg 12601680 75 49-130
Benzo(g,h,i)perylene ug/kg 12701680 76 48-140
Benzo(k)fluoranthene ug/kg 13001680 78 51-130
Benzoic Acid ug/kg 68508390 82 22-130
Benzyl alcohol ug/kg 23403360 70 43-130
bis(2-Chloroethoxy)methane ug/kg 12101680 72 43-130
bis(2-Chloroethyl) ether ug/kg 11601680 69 42-130
bis(2-Ethylhexyl)phthalate ug/kg 13101680 78 43-130
Butylbenzylphthalate ug/kg 13001680 78 44-131
Chrysene ug/kg 12801680 76 51-130
Di-n-butylphthalate ug/kg 13001680 77 46-130
Di-n-octylphthalate ug/kg 12701680 76 45-130
Dibenz(a,h)anthracene ug/kg 13101680 78 48-130
Dibenzofuran ug/kg 11901680 71 10-130
Diethylphthalate ug/kg 12901680 77 48-130
Dimethylphthalate ug/kg 12501680 75 48-130
Fluoranthene ug/kg 13001680 77 48-130
Fluorene ug/kg 12401680 74 48-130
Hexachloro-1,3-butadiene ug/kg 11601680 69 39-130
Hexachlorobenzene ug/kg 12801680 77 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3924484LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorocyclopentadiene ug/kg 12301680 73 17-130
Hexachloroethane ug/kg 11001680 66 40-130
Indeno(1,2,3-cd)pyrene ug/kg 12801680 76 50-130
Isophorone ug/kg 12601680 75 41-130
N-Nitroso-di-n-propylamine ug/kg 12401680 74 36-130
N-Nitrosodimethylamine ug/kg 11901680 71 34-130
N-Nitrosodiphenylamine ug/kg 12901680 77 48-130
Naphthalene ug/kg 12001680 71 46-130
Nitrobenzene ug/kg 11601680 69 39-130
Pentachlorophenol ug/kg 2750 v133608242-130
Phenanthrene ug/kg 13201680 79 50-130
Phenol ug/kg 11801680 71 42-130
Pyrene ug/kg 12901680 77 50-130
2,4,6-Tribromophenol (S)%74 10-131
2-Fluorobiphenyl (S)%67 10-130
2-Fluorophenol (S)%69 10-130
Nitrobenzene-d5 (S)%69 10-130
Phenol-d6 (S)%68 10-130
Terphenyl-d14 (S)%72 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3924485MATRIX SPIKE SAMPLE:
MSSpike
Result
92651699002
1,2,4-Trichlorobenzene ug/kg 13402190 61 16-130ND
1,2-Dichlorobenzene ug/kg 13002190 59 19-130ND
1,3-Dichlorobenzene ug/kg 12902190 59 19-130ND
1,4-Dichlorobenzene ug/kg 12902190 59 20-130ND
1-Methylnaphthalene ug/kg 16402190 75 19-130ND
2,4,5-Trichlorophenol ug/kg 16902190 77 19-130ND
2,4,6-Trichlorophenol ug/kg 16702190 76 18-130ND
2,4-Dichlorophenol ug/kg 15802190 72 16-130ND
2,4-Dimethylphenol ug/kg 21302190 97 10-130ND
2,4-Dinitrophenol ug/kg 10100 v1110009210-143ND
2,4-Dinitrotoluene ug/kg 16702190 76 19-130ND
2,6-Dinitrotoluene ug/kg 16802190 76 22-130ND
2-Chloronaphthalene ug/kg 15202190 69 18-130ND
2-Chlorophenol ug/kg 14302190 65 20-130ND
2-Methylnaphthalene ug/kg 15802190 72 18-130ND
2-Methylphenol(o-Cresol)ug/kg 16002190 73 13-130ND
2-Nitroaniline ug/kg 35704400 81 18-130ND
2-Nitrophenol ug/kg 15102190 69 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 16302190 74 13-130ND
3,3'-Dichlorobenzidine ug/kg 30904400 70 10-130ND
3-Nitroaniline ug/kg 32104400 73 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 38604400 88 10-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3924485MATRIX SPIKE SAMPLE:
MSSpike
Result
92651699002
4-Bromophenylphenyl ether ug/kg 16802190 76 18-130ND
4-Chloro-3-methylphenol ug/kg 34804400 79 16-130ND
4-Chloroaniline ug/kg 31504400 72 17-130ND
4-Chlorophenylphenyl ether ug/kg 16802190 77 17-130ND
4-Nitroaniline ug/kg 36904400 84 21-130ND
4-Nitrophenol ug/kg 898011000 82 13-131ND
Acenaphthene ug/kg 16502190 75 20-130ND
Acenaphthylene ug/kg 16802190 76 21-130ND
Aniline ug/kg 13602190 62 10-130ND
Anthracene ug/kg 15902190 72 19-130ND
Benzo(a)anthracene ug/kg 16602190 75 17-130ND
Benzo(a)pyrene ug/kg 16302190 74 14-130ND
Benzo(b)fluoranthene ug/kg 16502190 75 11-134ND
Benzo(g,h,i)perylene ug/kg 14702190 67 12-130ND
Benzo(k)fluoranthene ug/kg 16802190 76 15-130ND
Benzoic Acid ug/kg 843011000 77 10-130ND
Benzyl alcohol ug/kg 31004400 70 20-130ND
bis(2-Chloroethoxy)methane ug/kg 15502190 71 16-130ND
bis(2-Chloroethyl) ether ug/kg 14102190 64 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 17402190 79 11-130ND
Butylbenzylphthalate ug/kg 17702190 80 10-130ND
Chrysene ug/kg 17202190 78 17-130ND
Di-n-butylphthalate ug/kg 18102190 82 16-130ND
Di-n-octylphthalate ug/kg 18802190 85 16-130ND
Dibenz(a,h)anthracene ug/kg 15402190 70 13-130ND
Dibenzofuran ug/kg 15902190 72 19-130ND
Diethylphthalate ug/kg 18102190 82 22-130ND
Dimethylphthalate ug/kg 17702190 80 23-130ND
Fluoranthene ug/kg 17802190 81 14-130ND
Fluorene ug/kg 17002190 77 19-130ND
Hexachloro-1,3-butadiene ug/kg 13602190 62 12-130ND
Hexachlorobenzene ug/kg 16502190 75 17-130ND
Hexachlorocyclopentadiene ug/kg 14802190 67 10-130ND
Hexachloroethane ug/kg 13102190 60 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15702190 71 13-130ND
Isophorone ug/kg 16902190 77 17-130ND
N-Nitroso-di-n-propylamine ug/kg 16702190 76 10-130ND
N-Nitrosodimethylamine ug/kg 14802190 67 16-130ND
N-Nitrosodiphenylamine ug/kg 16602190 76 19-130ND
Naphthalene ug/kg 14802190 67 18-130ND
Nitrobenzene ug/kg 14102190 64 15-130ND
Pentachlorophenol ug/kg 3770 v144008610-130ND
Phenanthrene ug/kg 17102190 78 17-130ND
Phenol ug/kg 15102190 68 15-130ND
Pyrene ug/kg 15802190 72 31-130ND
2,4,6-Tribromophenol (S)%76 10-131
2-Fluorobiphenyl (S)%68 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3924485MATRIX SPIKE SAMPLE:
MSSpike
Result
92651699002
2-Fluorophenol (S)%63 10-130
Nitrobenzene-d5 (S)%66 10-130
Phenol-d6 (S)%66 10-130
Terphenyl-d14 (S)%70 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651699003
3924486SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND v130ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651699003
3924486SAMPLE DUPLICATE:
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND v130ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6674
2-Fluorobiphenyl (S)%6271
2-Fluorophenol (S)%6167
Nitrobenzene-d5 (S)%6370
Phenol-d6 (S)%6269
Terphenyl-d14 (S)%5967
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
756199
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3928818
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.1 N202/16/23 13:42
Aliphatic (C19-C36)mg/kg ND 10.1 N202/16/23 13:42
Aromatic (C11-C22)mg/kg ND 10.1 N202/16/23 13:42
1-Chlorooctadecane (S)%76 40-140 02/16/23 13:42
2-Bromonaphthalene (S)%70 40-140 02/16/23 13:42
2-Fluorobiphenyl (S)%69 40-140 02/16/23 13:42
o-Terphenyl (S)%69 40-140 02/16/23 13:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3928819LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3928820
Aliphatic (C09-C18)mg/kg ND N29.8 51 40-14053ND 50
Aliphatic (C19-C36)mg/kg ND N213.1 73 40-14072ND 50
Aromatic (C11-C22)mg/kg 18.0 N227.9 65 40-1406819.6 8 50
1-Chlorooctadecane (S)%68 40-14069
2-Bromonaphthalene (S)%72 40-14072
2-Fluorobiphenyl (S)%71 40-14070
o-Terphenyl (S)%64 40-14068
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
756862
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3932096
Associated Lab Samples:92651699006
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10 N202/20/23 14:03
Aliphatic (C19-C36)mg/kg ND 10 N202/20/23 14:03
Aromatic (C11-C22)mg/kg ND 10 N202/20/23 14:03
1-Chlorooctadecane (S)%83 40-140 02/20/23 14:03
2-Bromonaphthalene (S)%76 40-140 02/20/23 14:03
2-Fluorobiphenyl (S)%72 40-140 02/20/23 14:03
o-Terphenyl (S)%79 40-140 02/20/23 14:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3932097LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3932098
Aliphatic (C09-C18)mg/kg ND N2105940-14056ND 50
Aliphatic (C19-C36)mg/kg 11.0 N213.3 83 40-1408310.9 1 50
Aromatic (C11-C22)mg/kg 19.5 N228.2 69 40-1406919.3 1 50
1-Chlorooctadecane (S)%94 40-14091
2-Bromonaphthalene (S)%78 40-14080
2-Fluorobiphenyl (S)%74 40-14076
o-Terphenyl (S)%82 40-14076
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755274
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699002, 92651699003, 92651699004, 92651699005, 92651699006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651703001
3924251SAMPLE DUPLICATE:
Percent Moisture %20.0 N212519.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651699006
3924252SAMPLE DUPLICATE:
Percent Moisture %16.0 N232515.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92651699
ENGLISH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
755280
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92651699001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651724001
3924310SAMPLE DUPLICATE:
Percent Moisture %21.0 N2192517.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92651743002
3924420SAMPLE DUPLICATE:
Percent Moisture %13.9 N252514.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92651699
ENGLISH
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92651699
ENGLISH
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92651699001 755987 756216S-1 EPA 3546 EPA 8015C
92651699002 756199 756403CS-1 MADEP EPH MADEP EPH
92651699003 756199 756403CS-2 MADEP EPH MADEP EPH
92651699004 756199 756403CS-3 MADEP EPH MADEP EPH
92651699005 756199 756403CS-4 MADEP EPH MADEP EPH
92651699006 756862 756976CS-5 MADEP EPH MADEP EPH
92651699001 755472 755499S-1 EPA 5030B EPA 8015C
92651699002 755294 755383CS-1 EPA 3546 EPA 8270E
92651699003 755294 755383CS-2 EPA 3546 EPA 8270E
92651699004 755294 755383CS-3 EPA 3546 EPA 8270E
92651699005 755294 755383CS-4 EPA 3546 EPA 8270E
92651699006 755294 755383CS-5 EPA 3546 EPA 8270E
92651699002 755604 755697CS-1 EPA 5035A/5030B EPA 8260D
92651699003 755604 755697CS-2 EPA 5035A/5030B EPA 8260D
92651699004 755604 755697CS-3 EPA 5035A/5030B EPA 8260D
92651699005 755604 755697CS-4 EPA 5035A/5030B EPA 8260D
92651699006 755604 755697CS-5 EPA 5035A/5030B EPA 8260D
92651699001 755280S-1 SW-846
92651699002 755274CS-1 SW-846
92651699003 755274CS-2 SW-846
92651699004 755274CS-3 SW-846
92651699005 755274CS-4 SW-846
92651699006 755274CS-5 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:26 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 49
Page 48 of 49
Page 49 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
February 22, 2023
Johnathan Biddix
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: English
Client Job Number:
Project Number: 92651699
Laboratory Work Order Number: 23B1472
Enclosed are results of analyses for samples as received by the laboratory on February 14, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 22
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23B1472-01 5
23B1472-02 7
23B1472-03 9
23B1472-04 11
23B1472-05 13
Sample Preparation Information 15
QC Data 16
Petroleum Hydrocarbons Analyses - VPH 16
B331583 16
Flag/Qualifier Summary 18
Certifications 19
Chain of Custody/Sample Receipt 20
Page 2 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
2/22/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Johnathan Biddix
92651699
23B1472
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
English
CS-1 23B1472-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
CS-2 23B1472-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
CS-3 23B1472-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
CS-4 23B1472-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
CS-5 23B1472-05 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 3 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with
less than the method-specified amount.
Analyte & Samples(s) Qualified:
O-01
23B1472-05[CS-5]
Average of 3 markers passes
Analyte & Samples(s) Qualified:
Z-01
2-Methylpentane
B331583-BS1, B331583-BSD1
Pentane
B331583-BS1, S083375-CCV1
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 4 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-01
Field Sample #: CS-1
Sample Matrix: Soil
Sampled: 2/9/2023 10:34
[TOC_2]23B1472-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.92
Petroleum Hydrocarbons Analyses - VPH
ND 18 2/15/23 16:38 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 18 2/15/23 16:38 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 18 2/15/23 16:38 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 18 2/15/23 16:38 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 18 2/15/23 16:38 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)110 2/15/23 16:3870-130
2,5-Dibromotoluene (PID)108 2/15/23 16:3870-130
[TOC_1]Sample Results[TOC]
Page 5 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-01
Field Sample #: CS-1
Sample Matrix: Soil
Sampled: 2/9/2023 10:34
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
75.2 2/16/23 7:09 WDC% Wt 2/16/23SM 2540G1% Solids
Page 6 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-02
Field Sample #: CS-2
Sample Matrix: Soil
Sampled: 2/9/2023 10:25
[TOC_2]23B1472-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.08
Petroleum Hydrocarbons Analyses - VPH
ND 15 2/15/23 17:08 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 15 2/15/23 17:08 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 15 2/15/23 17:08 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 15 2/15/23 17:08 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 15 2/15/23 17:08 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)119 2/15/23 17:0870-130
2,5-Dibromotoluene (PID)113 2/15/23 17:0870-130
Page 7 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-02
Field Sample #: CS-2
Sample Matrix: Soil
Sampled: 2/9/2023 10:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.7 2/16/23 7:09 WDC% Wt 2/16/23SM 2540G1% Solids
Page 8 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-03
Field Sample #: CS-3
Sample Matrix: Soil
Sampled: 2/9/2023 10:20
[TOC_2]23B1472-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.14
Petroleum Hydrocarbons Analyses - VPH
ND 16 2/15/23 17:37 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 2/15/23 17:37 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 2/15/23 17:37 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 2/15/23 17:37 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 2/15/23 17:37 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)128 2/15/23 17:3770-130
2,5-Dibromotoluene (PID)120 2/15/23 17:3770-130
Page 9 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-03
Field Sample #: CS-3
Sample Matrix: Soil
Sampled: 2/9/2023 10:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
72.9 2/16/23 7:09 WDC% Wt 2/16/23SM 2540G1% Solids
Page 10 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-04
Field Sample #: CS-4
Sample Matrix: Soil
Sampled: 2/9/2023 10:29
[TOC_2]23B1472-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.10
Petroleum Hydrocarbons Analyses - VPH
ND 16 2/15/23 18:07 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 2/15/23 18:07 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 2/15/23 18:07 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 2/15/23 18:07 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 2/15/23 18:07 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 2/15/23 18:0770-130
2,5-Dibromotoluene (PID)104 2/15/23 18:0770-130
Page 11 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-04
Field Sample #: CS-4
Sample Matrix: Soil
Sampled: 2/9/2023 10:29
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.7 2/16/23 7:09 WDC% Wt 2/16/23SM 2540G1% Solids
Page 12 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-05
Field Sample #: CS-5
Sample Matrix: Soil
Sampled: 2/9/2023 10:40
[TOC_2]23B1472-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.40
Petroleum Hydrocarbons Analyses - VPH
ND 10 2/15/23 18:36 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 10 2/15/23 18:36 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 10 2/15/23 18:36 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 10 2/15/23 18:36 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 10 2/15/23 18:36 EEHmg/Kg dry 2/15/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)115 2/15/23 18:3670-130
2,5-Dibromotoluene (PID)113 2/15/23 18:3670-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/14/2023
Work Order: 23B1472Sample Description:Project Location: English
Sample ID: 23B1472-05
Field Sample #: CS-5
Sample Matrix: Soil
Sampled: 2/9/2023 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.2 2/16/23 7:09 WDC% Wt 2/16/23SM 2540G1% Solids
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B331583 02/15/239.20 12.323B1472-01 [CS-1]
B331583 02/15/2310.8 12.423B1472-02 [CS-2]
B331583 02/15/2311.4 13.123B1472-03 [CS-3]
B331583 02/15/2311.0 12.823B1472-04 [CS-4]
B331583 02/15/2314.0 12.123B1472-05 [CS-5]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B331724 02/16/2323B1472-01 [CS-1]
B331724 02/16/2323B1472-02 [CS-2]
B331724 02/16/2323B1472-03 [CS-3]
B331724 02/16/2323B1472-04 [CS-4]
B331724 02/16/2323B1472-05 [CS-5]
[TOC_1]Sample Preparation Information[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B331583 - MA VPH
[TOC_3]B331583[TOC]
Blank (B331583-BLK1) Prepared & Analyzed: 02/15/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)74.429.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)73.029.2
LCS (B331583-BS1) Prepared & Analyzed: 02/15/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301309.72
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301128.39
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301182.94
Benzene mg/Kg wet0.050 2.50 70-1301283.20
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301192.98
Decane mg/Kg wet0.050 2.50 70-13095.52.39
Ethylbenzene mg/Kg wet0.050 2.50 70-1301223.05
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301202.99
2-Methylpentane mg/Kg wet0.050 2.50 Z-0170-130134*3.35
Naphthalene mg/Kg wet0.50 2.50 70-13091.62.29
Nonane mg/Kg wet0.050 2.50 30-1301213.02
Pentane mg/Kg wet0.050 2.50 Z-0170-130133*3.33
Toluene mg/Kg wet0.050 2.50 70-1301233.08
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301182.94
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-1301223.04
m+p Xylene mg/Kg wet0.10 5.00 70-1301206.02
o-Xylene mg/Kg wet0.050 2.50 70-1301203.00
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11245.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11044.1
[TOC_1]QC Data[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B331583 - MA VPH
LCS Dup (B331583-BSD1) Prepared & Analyzed: 02/15/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130128 0.9559.63
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130113 1.288.50
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130120 2.283.01
Benzene mg/Kg wet0.050 2.50 2570-130127 0.5573.18
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130121 1.613.03
Decane mg/Kg wet0.050 2.50 2570-13096.8 1.292.42
Ethylbenzene mg/Kg wet0.050 2.50 2570-130123 1.033.08
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130120 0.04013.00
2-Methylpentane mg/Kg wet0.050 2.50 25 Z-0170-130135 0.600*3.37
Naphthalene mg/Kg wet0.50 2.50 2570-13098.1 6.822.45
Nonane mg/Kg wet0.050 2.50 2530-130122 0.9463.04
Pentane mg/Kg wet0.050 2.50 2570-130128 4.003.20
Toluene mg/Kg wet0.050 2.50 2570-130123 0.03083.08
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130120 2.283.01
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-130122 0.6023.06
m+p Xylene mg/Kg wet0.10 5.00 2570-130122 1.766.12
o-Xylene mg/Kg wet0.050 2.50 2570-130122 1.623.05
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)11646.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11746.7
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered
with methanol, but with less than the method-specified amount.
O-01
Average of 3 markers passesZ-01
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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