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HomeMy WebLinkAboutWS-29656_48783_CA_IAR_20230223 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\L4636480000-001.docx February 23, 2023 Mr. James W. Brown Regional Supervisor, Winston-Salem Regional Office UST Section, Division of Waste Management North Carolina Department of Environmental Quality 450 West Hanes Mill Road, Suite 300 Winston-Salem, North Carolina 27105 Subject: Initial Abatement Action Report TForce Holdings USA Facility 4411 Groometown Road, Greensboro, Guilford County, North Carolina Incident Number: 48783 Dear James: Attached please find the Initial Abatement Action Report prepared for the above-referenced facility. Because concentrations of petroleum constituents remain in soil and groundwater at levels above applicable standards, this report is being submitted in lieu of a UST Closure Report. If you have any questions or require additional information regarding the content of this report, please contact me at dszynal@trccompanies.com or 864-420-3976. Sincerely, TRC Engineers, Inc. David Szynal Project Manager Attachment cc: Bill Preece, TForce Rachel Brown, TForce Lisa Clark, TRC \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 1 Initial Abatement Action (Site Check, UST Closure with UST-2 Form, Excavation, Post-Excavation Soil Contamination Assessment) Report A. Site Information 1. Site Identification Date of Report: February 23, 2023 Site Risk: Undetermined Facility I.D.: 00-0-0000009753 UST Incident Number (if known): 48783 Site Name: TForce Freight, Inc. Street Address: 4411 Groometown Road City/Town: Greensboro, NC Zip Code: 27407 County: Guilford Description of Geographical Data Point (e.g., diesel fill port): Site Address Location Method (GPS, topographical map, other): GIS Latitude (decimal degrees): 35.995761 Longitude (decimal degrees): -79.863277 2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city, state, zip code and mailing address, if different) UST/AST Owner: TForce Freight, Inc. Email: enviro@tforcefreight.com Address: 1000 Semmes Ave Richmond VA 23224 804-291-5850 UST/AST Operator: Same as above Email: Address: Tel: Property Owner: Same as above Email: Address: Tel: Property Occupant: Same as above Email: Address: Tel: Consultant/Contractor: TRC Engineers, Inc. Email: dszynal@trccompanies.com Address: 50 International Drive, Suite 150, Greenville, SC 29615 Tel: 864-420-3976 Analytical Laboratory: Eurofins Environmental Testing Savannah State Certification No: 269 Address: 5102 LaRoche Avenue, Savannah, GA 31404 Tel: 912-354-7858 3. Information about the Release Date Discovered: 12/12/2022 (UST Closure Soil Sample Analytical Results) Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release (e.g., Dispenser/Piping/UST): Two 20,000-gallon diesel UST removed in November 2022 Sizes and Contents of Tanks or Other Containment from which the Release Occurred: Two former 20,000-gallon diesel USTs closed by removal in November 2022 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 3 Supplemental Soil Investigation A supplemental soil investigation was conducted in December 2022 to better delineate impacted soil identified on the western side of UST excavation and in the vicinity of the of the fuel dispenser. Direct Push Technology (DPT) was used to collect soil samples from nine locations. TPH-DRO and TPH-GRO were detected in soils collected in the vicinity of the fuel dispenser along with one detection of TPH-GRO southwest of the UST excavation at concentrations above NC DEQ TPH action levels. In addition, three of the soil samples collected in the vicinity of the fuel dispenser had detections of naphthalene, 1- methylnaphthalene, and/or 2-methylnaphthalene at concentrations above applicable NC MSCCs. Monitoring Well Installation/Sampling Two permanent monitoring wells were installed in December 2022. The first permanent monitoring well (MW-02) was installed in center of the former UST excavation. The second permanent well (MW-01) was installed adjacent to the former fuel dispenser. The monitoring well installed in center of the UST excavation area (MW-02) had exceedances of North Carolina Groundwater Quality Standards (i.e., NC 2L Standards) for MA-VPH calculated C9-C22 Aromatics, and Benzene. The concentration of benzene detected did not exceed North Carolina Gross Contamination Levels for Groundwater. Analyzed constituents were not detected above reporting limits in well MW-01. In addition to groundwater sampling at each permanent monitoring well, one soil sample was collected at each location from the interval displaying the highest PID concentration during well installation. Soil samples were submitted to an analytical laboratory for analysis of Massachusetts volatile petroleum hydrocarbon (MA-VPH), Massachusetts extractable petroleum hydrocarbons (MA-EPH), SVOCs, and VOCs. The soil sample collected during installation of MW-01 had exceedances of North Carolina MSCCs for MA-VPH, MA-EPH, along with SVOCs. The soil sample collected during installation of monitoring well MW-02 did not exceed MSCCs. A risk classification has not yet been established for this site. TRC, on behalf of TForce, will submit a Limited Site Assessment (LSA) report to NC DEQ within the established time frame. C. Table of Contents A. Site Information .................................................................................................................................... 1 B. Executive Summary ............................................................................................................................... 2 C. Table of Contents .................................................................................................................................. 3 D. Site History and Characterization.......................................................................................................... 5 E. Site Check Report (if applicable) ........................................................................................................... 7 F. UST Closure Report (following UST-12 Format) and Site Investigation Report for Permanent Closure of Change-in-Service of UST (UST-2 Form)............................................................................................ 7 G. NAPL Investigation and Free Product Recovery Report (if applicable) ................................................. 7 H. Groundwater and Surface Water Investigation .................................................................................... 7 I. Initial Response and Abatement Action ................................................................................................ 8 J. Excavation of Contaminated Soil .......................................................................................................... 8 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 4 K. Conclusions ........................................................................................................................................... 9 L. Figures ................................................................................................................................................. 10 M. Tables .................................................................................................................................................. 19 N. Appendices .......................................................................................................................................... 28 Figures Figure G-1 – Topographic Site Location Map Figure G-2 – Site Map Figure G-3A – UST Closure - Confirmation Soil Analytical Results (November 2022) Figure G-3B – Supplemental Investigation - Soil Investigation Results (December 2022) Figure G-3C – Permanent Groundwater Monitoring Well Soil Results (December 2022) Figure G-4 – Permanent Monitoring Well Groundwater Analytical Results (January 2023) Figure G-5 – Land Use Map Figure G-6 – Private Well Map Tables Table B-1 – Site History: UST/AST System and Other Release Information Table B-2 – Site History: UST/AST Owner/Operator and Other Responsible Party Table B-3 – Summary of Soil Sampling Results Table B-3A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-3B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-3C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Table B-4 – UST Closure – Confirmation Groundwater Analytical Results (January 2023) Table B-5 – Hits Only Summary of Soil Sampling Results Table B-5A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-5B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-5C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Table B-6 – Hits Only UST Closure – Confirmation Groundwater Analytical Results (January 2023) Table B-7 – Summary of Permanent Groundwater Monitoring Well Field Parameters (January 2023) Table B-8 – Summary of UST Closure PID Field Soil Readings (November 2022) Appendices Appendix A – Site Specific Health and Safety Plan (HASP) Appendix B – Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature) Appendix C – Standard procedures (sampling, field equipment decontamination, field screening, etc.) * - included in Appendix F Appendix D – Soil, water, NAPL, and sludge disposal manifests and soil treatment permits Appendix E – Complete chain-of-custody records* - included in Appendix F Appendix F – Copy of all Laboratory Analytical Records Appendix G – Geologic Logs for Borings (related to supplemental investigation only) Appendix H – Monitoring Well Construction Forms (for all wells constructed to date) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 5 D. Site History and Characterization Information regarding the current and former USTs at the facility is summarized on Table B-1 – UST/AST System and Other Release Information. Information regarding known owners/operators of USTs at the site are summarized on Table B-2 – UST/AST Owner/Operator and Other Responsible Party. The Site is an active freight distribution center with a truck maintenance facility. The Site occupies approximately 47.52-acres in a commercial and industrial use area. The site has been improved with an approximately 64,000-square-foot freight terminal building, a 13,000-square foot maintenance and washing building, and a 4,500-square-foot vacant former bunk house. Potable water is provided by an on-site production well. Outdoor surfaces consist of paved parking lots, concrete areas, and truck staging areas surrounding the central buildings. Additional surfaces include vegetated areas, forested land and a storm water pond in the eastern portion, and vacant land along the southern area parking lots. Subsurface soils consist of silty sand to sandy gravel to depths of 1 to 15 feet-below ground surface and silty sand to medium sand from 15 to 27 feet-below ground surface. Groundwater was observed at two permanent monitoring wells (MW-01 and MW-02) prior to groundwater sampling on January 6, 2023 at depths of 16.12 feet-below ground surface at MW-01 and 16.39 feet-below ground surface at MW-02. The Site has a topographic elevation of approximately 840 feet above mean seal level at the northwest corner of the facility and slopes to the east to an elevation of approximately 820 feet MSL. Based on local topography the assumed direction of shallow groundwater flow is eastward. Release(s) were discovered during performance of the UST closure by removal of two 20,000-gallon diesel USTs. Over excavation of non-hazardous petroleum impacted soils was completed during UST closure. A supplemental soil sampling investigation was completed west of the UST excavation and in the vicinity of the fuel dispenser. Site topography is shown on Figure G-1. Site features are shown on Figure G-2. UST Closure On November 14, 2022 the two 20,000-gallon USTs system was permanently closed via removal. The UST closure activities included excavation and removal of the two 20,000-gallon diesel USTs, twenty feet of conveyance line and one fuel dispenser. During the UST closure, a total of sixteen confirmation soil samples were collected; six from the floor underlying the USTs, eight sidewall samples around the USTs, one beneath the conveyance lines and one from underneath the fuel dispenser. UST floor samples were collected approximately eight feet apart (three under each UST) at a depth of nineteen and half feet- below ground surface. UST sidewall samples were collected approximately fifteen feet apart at a depth of fifteen feet-below ground surface. The one conveyance line sample was collected in the middle of the 20- foot segment of excavated conveyance line at a depth of seven and half feet-below ground surface. The fuel dispenser sample was collected under the dispenser at a depth of two feet-below ground surface. Approximately fifty-five feet of conveyance line could not be removed or sampled due to its location beneath the floor of the truck maintenance building. Although fifty-five feet of conveyance line was not removed, the line was pumped dry and capped on both ends. Prior to UST \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 6 closure, TRC received approval via email from NC DEQ regional supervisor James Brown, to leave the remaining conveyance line under the truck maintenance building intact. Total petroleum hydrocarbons (TPH) diesel range organics (TPH-DRO) along with TPH gasoline range organics (TPH-GRO) were detected in soil samples located in the UST excavation area and beneath the Fuel Dispenser at concentrations above their respective NC DEQUST Section TPH action levels. In addition, soil samples from these two locations had detections of naphthalene, 1-methylnaphthalene and 2-methylnaphthalene at concentrations that exceeded soil-to-water and/or residential MSCCs. Analytical results are summarized on Table B-3A and Table B-5A. The confirmation soil sample locations with criteria exceedances are shown on Figure G-3A. Analytical laboratory reports are provided in Appendix F. A total of 747.62 tons of non-hazardous petroleum impacted soil was removed from the site during UST closure activities. Excavated areas were backfilled using self-compacting gravel to ground surface. Surface completion will be restored to match surrounding conditions of asphalt or concrete at a later date. Supplemental Soil Investigation A supplemental soil investigation was conducted in December 2022 to better delineate impacted soil identified on the western side of UST excavation and in the vicinity of the of the fuel dispenser. DPT was used to collect soil samples from nine locations. DPT sample depths varied from 11 to 20 feet- below ground surface. One soil sample was collected at each soil boring location. Soil samples were analyzed by Eurofins Environmental Testing in Savannah Georgia for TPH-DRO, TPH-GRO, and PAHs. TPH-DRO and TPH-GRO were detected in soil samples collected in the vicinity of the fuel dispenser along with one detection of TPH-GRO southwest of the UST excavation at concentrations above NC DEQ TPH action levels. In addition, three of the soil samples collected in the vicinity of the fuel dispenser had detections of naphthalene, 1-methylnaphthalene, and/or 2-methylnaphthalene at concentrations above applicable NC MSCCs. Analytical results are summarized on Table B-3B and Table B-5B. The confirmation soil sample locations with criteria exceedances are shown on Figure G-3B. Analytical laboratory reports are provided in Appendix F. Monitoring Well Installation/Sampling MW-01 Monitoring well MW-01 was installed adjacent to the former fuel dispenser at the location where PID concentrations in soil were found to be the highest during the December 2022 supplemental soil investigation. MW-01 was installed to a depth of 27 feet-below ground surface. One groundwater sample was collected from this well on January 6, 2023 and analyzed for MA-VPH, MA-EPH, SVOCs, and VOCs. Analyzed constituents were not detected above reporting limits in well MW-01. One soil sample was collected from an interval where the highest PID concentration was observed during well installation (i.e., 11 feet-below ground surface). The soil sample collected for laboratory analysis was analyzed for MA-VPH, MA-EPH, SVOCs, and VOCs. The soil sample collected during \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 7 installation of MW-01 had exceedances of North Carolina MSCCs for MA-VPH calculated C9-C22 Aromatics, MA-VPH calculated C9-C18 Aliphatic, 2-Methylnaphthalene, and Naphthalene. MW-02 Monitoring well MW-02 was installed in the center of the former UST excavation. MW-02 was installed to a depth of 26 feet-below ground surface. One groundwater sample was collected from this well on January 6, 2023 and analyzed for MA-VPH, MA-EPH, SVOCs, and VOCs. The groundwater results showed exceedances of North Carolina Groundwater Quality Standards (i.e., NC 2L Standards) for MA-VPH calculated C9-C22 Aromatics, and Benzene. The concentration of benzene detected did not exceed North Carolina Gross Contamination Levels for Groundwater. One soil sample was collected from an interval where the highest PID concentration was observed during well installation (i.e., 20 feet-below ground surface). The soil sample collected for laboratory analysis was analyzed for MA-VPH, MA-EPH, SVOCs, and VOCs. Analytical results from the soil sample did not show exceedances of MSCCs at a sample depth of 20 feet-below ground surface. Analytical results are summarized for soil on Table B-3C and Table B-5C. Analytical results are summarized for groundwater on Table B-4 and Table B-6. The confirmation soil sample locations with criteria exceedances are shown on Figure G-3A. The permanent monitoring well locations with soil criteria exceedances are shown on Figure G-3C. The permanent monitoring well locations with groundwater criteria exceedances are shown on Figure G-4. Analytical laboratory reports are provided in Appendix F. E. Site Check Report (if applicable) Not applicable; soil and groundwater sampling conducted as part of the UST Closure and supplemental soil investigation (described in Section D) have satisfied the requirements of the Site Check. F. UST Closure Report (following UST-12 Format) and Site Investigation Report for Permanent Closure of Change-in-Service of UST (UST-2 Form) Because constituents in soil remain above NC MSCCs and constituents in groundwater remain above NC 2L Standards, this Initial Abatement Action Report is being submitted in lieu of a UST Closure Report. G. NAPL Investigation and Free Product Recovery Report (if applicable) Not applicable. No NAPL identified on facility. H. Groundwater and Surface Water Investigation Following the removal of the two 20,000-gallon diesel USTs system in November 2022, two permanent monitoring wells (MW-01 and MW-02) were installed in December 2022. The first permanent monitoring well (MW-02) was installed in center of the former UST excavation. The second permanent well (MW 01) was installed adjacent to the former fuel dispenser. Analytical results from MW-02 had exceedances of North Carolina Groundwater Quality Standards (i.e., NC 2L Standards) for MA-VPH calculated C9-C22 Aromatics, and Benzene. The concentration of benzene detected did not exceed \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 8 North Carolina Gross Contamination Levels for Groundwater. Analyzed constituents were not detected above reporting limits in well MW-01. No surface water samples have been collected from this site. Analytical results are summarized on Table B-4 and Table B-6. The permanent monitoring well locations with groundwater criteria exceedances are shown on Figure G-4. Site features are shown on Figure G-2. I. Initial Response and Abatement Action The UST system was permanently closed by removal in November 2022 and a closure assessment conducted (see Section F). A total of 747.62 tons of non-hazardous petroleum impacted soil was removed from the site during UST closure activities. Form UST-61, 24-hour Release and UST Leak Reporting Form, was submitted to NC DEQ on December 9, 2022. Based on a conference call with NC DEQ regional supervisor James Brown on December 12, 2022, a 20-Day Report for this site will not be required. Following submittal of this Initial Abatement Action Report, a Limited Site Assessment Report will be prepared and submitted to NC DEQ. J. Excavation of Contaminated Soil During removal of the UST, conveyance line and fuel dispenser, a portable Photoionization Detector (PID) was used to screen excavated soils and segregate potentially impacted soils prior to collection of confirmation soil samples. The PID was field calibrated each day using 100 ppm isobutylene gas prior to screening of soil. Excavated soils were staged on top of plastic sheeting onsite prior to off-site disposal. Over excavation occurred at the UST. The original UST excavation for the two 20,000-gallon diesel UST was estimated to be 32 feet in length, 24 feet in width, and 19.5 feet in depth. During UST removal activities the UST excavation was expanded an additional five feet in each direction (north, south, west and east) all to a depth of 19.5 feet-below ground surface. Excavated soil was described as silty sand to sandy gravel. Approximate boundaries of the excavation are illustrated on Figure G-2. A total of 747.62 tons of non-hazardous petroleum impacted soil was removed from the facility during UST closure activities. Equipment used during UST removal activities included • Walk behind concrete saw (30-inch blade) • 210 excavator with thumb attachment • Vac truck (2,800 gallons) • Vibratory Roller • Skid Steer with hammer attachment (8,000 pound) • Tractor with lowboy • Dump trucks \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 9 • Core Drill • Service truck • Man lift K. Conclusions Soils containing concentrations of TPH and PAHs above North Carolina screening levels remain on site in the vicinity of the two former 20,000-gallon USTs and associated fuel dispenser. Petroleum impacted soils are covered by asphalt or concrete and do not pose a risk to human health if left undisturbed. Groundwater sampled from a monitoring well installed in the vicinity of the former fuel dispenser did not contain concentrations of analyzed constituents above method detection limits. Groundwater sampled from a monitoring well installed within the former UST excavation contained concentrations of C9-C22 aromatics and benzene at levels above North Carolina groundwater quality standards. The concentration of benzene detected did not exceed the gross contamination levels for groundwater. A potable water well is located on site, but a sample collected from this well in June 2021 did not contain detectable levels of analyzed constituents. The potable well is located approximately one- hundred feet east of the two former 20,000-gallon USTs. Other private water supply wells are located within 1,500-feet of the former UST as a municipal water supply is not available in this area. \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 10 L. Figures Figure G-1 – Topographic Site Location Map Figure G-2 – Site Map Figure G-3A – UST Closure - Confirmation Soil Analytical Results (November 2022) Figure G-3B – Supplemental Investigation - Soil Investigation Results (December 2022) Figure G-3C – Permanent Groundwater Monitoring Well Soil Results (December 2022) Figure G-4 – Permanent Monitoring Well Groundwater Analytical Results (January 2023) Figure G-5 – Land Use Map Figure G-6 – Private Well Map \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 11 Figure G-1 – Topographic Site Location Map 463648.0000.0000 Figure G-1 Site Location Map.mxdFIGURE G-1 TOPOGRAPHIC SITE LOCATION MAP DRAWN BY: APPROVED BY: PROJECT NO: FILE NO. DATE: !(1,500' 0 1,000 2,000 FEET 1 " = 2,000 ' 1:24,000 NC VA SC GA WV KY TN OH FEBRUARY 2023 BASE MAP FROM USGS NATIONAL MAP; DATA SOURCES: TRC NORTH CAROLINA OVERVIEW SITE LOCATION TRC - GISTRC - GIS 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030 J. YONTS D. SZYNAL E TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA 1,500 FOOT RADIUS SITE BOUNDARY !(TWO FORMER 20,000-GALLON DIESEL USTs \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 12 Figure G-2 – Site Map DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-2_Site Map.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:3,600 1 " = 300 ' 0 300 600 Feet LEGEND FIGURE G-2 J. YONTS SITE MAP FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. No Public Water Supply Wells Identified within 1500 feet of Former USTs 3. No Well Head Protection Areas within 1500 feet of Former USTs 4. Private Wells within 1500 feet of Former USTs shown on Figure G-6 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com @?Site Potable Well Approximate Property Boundary \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 13 Figure G-3A – UST Closure - Confirmation Soil Analytical Results (November 2022) DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-3A_UST_Soil_Data_Nov2022.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:300 1 " = 25 ' 0 25 50 Feet LEGEND FIGURE G-3A J. YONTS UST CLOSURE - CONFIRMATION SOIL ANALYTICAL RESULTS (NOVEMBER 2022) FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Soil analytical result exceedances above comparison values. 3. Soil sample results expressed in mg/kg 4. NAP = Naphthalene 5. 1-MN = 1-Methylnaphthalene 6. 2-MN = 2-Methylnaphthalene 7. TPH-DRO = Total Petroleum Hydrocarbons - Diesel Range Organics 8. TPH-GRO = Total Petroleum Hydrocarbons - Gasoline Range Organics Approximate location and Extent of Excavation of Former Fuel Dispensers Approximate Extent of Excavation Former Diesel Fuel Pipe and Vent Lines Approximate location of Former 20,000-gallon Diesel Underground Storage Tank 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com Soil Sample Location Site Potable Well@? \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 14 Figure G-3B – Supplemental Investigation - Soil Investigation Results (December 2022) DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-3B_Supplement_Soil_Data_Dec2022.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:300 1 " = 25 ' 0 25 50 Feet LEGEND FIGURE G-3B J. YONTS SUPPLEMENTAL INVESTIGATION - SOIL INVESTIGATION RESULTS (DECEMBER 2022) FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Soil analytical result exceedances above comparison values. 3. Soil sample results expressed in mg/kg 4. NAP = Naphthalene 5. 1-MN = 1-Methylnaphthalene 6. 2-MN = 2-Methylnaphthalene 7. TPH-DRO = Total Petroleum Hydrocarbons - Diesel Range Organics 8. TPH-GRO = Total Petroleum Hydrocarbons - Gasoline Range Organics 9. Fl = Fluoranthene 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com Approximate location and Extent of Excavation of Former Fuel Dispensers Approximate Extent of Excavation Former Diesel Fuel Pipe and Vent Lines Approximate location of Former 20,000-gallon Diesel Underground Storage Tank Soil Sample Location Site Potable Well@? \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 15 Figure G-3C – Permanent Groundwater Monitoring Well Soil Results (December 2022) DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-3C_Permenant_Wells_Soil_Data_Dec2022.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:300 1 " = 25 ' 0 25 50 Feet LEGEND FIGURE G-3C J. YONTS PERMANENT GROUNDWATER MONITORING WELL SOIL RESULTS (DECEMBER 2022) FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Soil analytical result exceedances above comparison values. 3. Soil sample results expressed in mg/kg 4. NAP = Naphthalene 5. 2-MN = 2-Methylnaphthalene Monitoring Well Location@?< 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com Approximate location and Extent of Excavation of Former Fuel Dispensers Approximate Extent of Excavation Former Diesel Fuel Pipe and Vent Lines Approximate location of Former 20,000-gallon Diesel Underground Storage Tank Site Potable Well@? \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 16 Figure G-4 – Permanent Monitoring Well Groundwater Analytical Results (January 2023) DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-4_Permanent_Wells_GW_Data_Jan2023.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:300 1 " = 25 ' 0 25 50 Feet LEGEND FIGURE G-4 J. YONTS PERMANENT MONITORING WELL GROUNDWTER ANALYTICAL RESULTS (JANUARY 2023) FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Groundwater analytical result exceedances above comparison values. 3. Groundwater sample results expressed in µg/L. Approximate location and Extent of Excavation of Former Fuel Dispensers Approximate Extent of Excavation Former Diesel Fuel Pipe and Vent Lines Approximate location of Former 20,000-gallon Diesel Underground Storage Tank Monitoring Well Location@?< 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com Site Potable Well@? \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 17 Figure G-5 – Land Use Map DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-5_Land_Use.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:3,600 1 " = 300 ' 0 150 300 Feet LEGEND FIGURE G-5 J. YONTS LAND USE MAP FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Guilford County North Carolina Government GIS Data Viewer 3. Land Cover Data Obtained from U.S. Geological Survey and NLCD Land Cover Mapping Teams, 2011 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com Open Water Developed Open Space Developed Low Intensity Developed Medium Intensity Developed High Intensity Deciduous Forest Evergreen Forest Mixed Forest Pasture/Hay Woody Wetlands Emergent Herbaceous Wetlands !(Private Wells @?Site Potable Well Site Boundary 1,500 Foot Radius from Former USTs \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 18 Figure G-6 – Private Well Map DATE: APPROVED BY: CHECKED BY: DRAWN BY:PROJ. NO.: FEBRUARY 2023 463648.0000.0000 Figure_G-6_Private_Wells.mxd TFORCE HOLDINGS USA, INC. 4411 GROOMETOWN ROAD GREENSBORO, NORTH CAROLINA D. SZYNAL L. CLARK 1:3,600 1 " = 300 ' 0 300 600 Feet LEGEND FIGURE G-6 J. YONTS PRIVATE WELL MAP FILE NO.: TITLE: PROJECT: NOTES: 1. © 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS 2. Guilford County North Carolina Government GIS Data Viewer !(Private Wells Former Diesel Fuel Pipe and Vent Lines Approximate Extent of Excavation Approximate location of Former 20,000-gallon Diesel Underground Storage Tank Approximate location and Extent of Excavation of Former Fuel Dispensers Site Boundary 1,500 Foot Radius from Former USTs @?Site Potable Well 50 International Drive, Suite 150Patewood Plaza ThreeGreenville, SC 29615Phone: 864.281.0030www.TRCcompanies.com \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 19 M. Tables Table B-1 – Site History: UST/AST System and Other Release Information Table B-2 – Site History: UST/AST Owner/Operator and Other Responsible Party Table B-3 – Summary of Soil Sampling Results Table B-3A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-3B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-3C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Table B-4 – UST Closure – Confirmation Groundwater Analytical Results (January 2023) Table B-5 – Hits Only Summary of Soil Sampling Results Table B-5A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-5B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-5C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Table B-6 – Hits Only UST Closure – Confirmation Groundwater Analytical Results (January 2023) Table B-7 – Summary of Permanent Groundwater Monitoring Well Field Parameters (January 2023) Table B-8 – Summary of UST Closure PID Field Soil Readings (November 2022) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 20 Table B-1 – Site History: UST/AST System and Other Release Information \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-1_Site History (UST-AST System and Other Release Information).docx 1 Table B-1: Site History – UST/AST System and Other Release Information Revision Date: 2/3/2023 Incident Number and Name: 48783 UST ID Number Current / Most-Recent Contents* Previous Contents* Capacity (in gallons) Construction Details** Tank Dimensions Description of Piping and Pumps Date Tank Installed Status of UST*** Release associated with this UST System? 1 Diesel diesel 20,000 Single wall, steel unknown unknown 1980 Permanently closed November 2022 possibly 2 Diesel diesel 20,000 Single wall, steel unknown unknown 1980 Permanently closed November 2022 possibly 3 Gasoline Gasoline 7,500 Single wall, steel unknown unknown 1962 Removed in 1990 possibly 4 Diesel Diesel 7,500 Single wall, steel unknown unknown 1962 Removed in 1989 possibly 5 Diesel Diesel 7,500 Single wall, steel unknown unknown 1962 Removed in 1989 possibly 6 Motor Oil Motor Oil 7,500 Single wall, steel unknown unknown 1962 Removed in 1990 possibly 7 Diesel Diesel 1,000 Single wall, steel unknown unknown 1962 Removed in 1991 Yes 8 Waste Oil Waste Oil 2,000 Single wall, steel unknown unknown 1975 Removed in 1990 possibly 9 Motor Oil Motor Oil 10,000 Single wall, steel unknown unknown 1990 Removed in 1998 Yes Add additional records as necessary \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-1_Site History (UST-AST System and Other Release Information).docx 2 AST ID Number Current / Most-Recent Contents* Previous Contents* Capacity (in gallons) Construction Details** Tank Dimensions Description of Piping and Pumps Date Tank Installed Status of AST*** Release associated with this AST System? 1 Fuel Oil Fuel Oil 500 Single wall, steel unknown unknown unknown On-site No 2 Used Oil Used Oil 500 Single wall, steel unknown unknown unknown On-site No 3 Fuel Oil Fuel Oil 500 Single wall, steel unknown unknown unknown On-site No 4 Motor Oil Motor Oil 500 Single wall, steel unknown unknown unknown On-site No 5 Fuel Oil Fuel Oil 500 Single wall, steel unknown unknown unknown On-site No Add additional records as necessary Incident Number Material Released Date of Release Description of Release 45192 Heating Oil Feb 11, 2018 Heating oil released during removal of UST, soil was excavated, and confirmation soil samples were collected. 23077/6202 Waste Oil Dec 2, 1991 Reported on Dec. 2, 1991 and closed on May 16, 1993. No other info in databases 44974 Diesel Dec 26, 2017 300 gallons of diesel released to concrete pavement due to overpressure. Diesel flowed over soil and into retention pond. Soil was excavated and product removed from pond. Add additional records as necessary * Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non-halogenated or halogenated solvents, etc. ** Fiberglass (single- or double-walled), steel (single- or double-walled), steel with FRP (single- or double-walled), steel with liner, other, unknown. *** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify date) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 21 Table B-2 – Site History: UST/AST Owner/Operator and Other Responsible Party \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-2_Site History.docx 1 Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party Information Revision Date: 2/3/2023 Incident Number and Name: 48783 UST ID Number Facility ID Number 9753 Owner Name (and Contact) Dates of Operation (mm/dd/yy to mm/dd/yy) TForce Freight, Inc. 04/30/21 to present Street Address 1000 Semmes Avenue City State Zip Telephone Number Richmond VA 23224 519-421-3300 #2244 Operator Name (and Contact) Dates of Operation (mm/dd/yy to mm/dd/yy) Same as above Same as above Street Address Same as above City State Zip Telephone Number Other Incidents Onsite or Commingled/In Close Proximity Incident Number Date Incident Occurred Name of Responsible Party for Other Incident Date Incident Reported Date Incident Closed (i/a) Street Address City State Zip Telephone Number \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-2_Site History.docx 2 UST ID Number Facility ID Number 9753 Owner Name (and Contact) Dates of Operation (mm/dd/yy to mm/dd/yy) Overnight Transportation 1962 to 2005 Street Address City State Zip Telephone Number Operator Name (and Contact) Dates of Operation (mm/dd/yy to mm/dd/yy) UPS Freight 2005 to 4/30/2021 Street Address na City State Zip Telephone Number na na na na Other Incidents Onsite or Commingled/In Close Proximity Incident Number Date Incident Occurred Name of Responsible Party for Other Incident Date Incident Reported Date Incident Closed (i/a) Street Address City State Zip Telephone Number \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 22 Table B-3 – Summary of Soil Sampling Results Table B-3A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-3B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-3C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Appendix B Reporting Tables \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-3A_UST Closure Confirmation Soil Analytical Results (November 2022).docx 1 Table B-3A: UST Closure – Confirmation Soil Analytical Results (November 2022) Revision Date: Incident Number and Name: 48783 Facility ID#: Analytical Method (e.g., VOC by EPA 8260)  8015 8015 8270 8270 8270 Contaminant of Concern  Gasoline Range Organics [C6-C10] Diesel Range Organics [C10-C28] 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Sample ID Date Collected (mm/dd/yy) Source Area (e.g., Tank Pit 1) Sample Depth (ft BGS) Incident Phase (IAA, LSA, etc.) SB-FD-1 11/17/2022 2 407 15800 53.6 75.7 18.4 SB-UST-1-2 11/16/2022 19.5 161 1970 0.445 0.395 <0.00819 SB-UST-1-3 11/16/2022 19.5 655 8570 4.95 7.81 <0.0182 SB-UST-2-2 11/16/2022 19.5 830 11800 6.78 11.3 <0.0159 SB-UST-2-3 11/16/2022 19.5 81.7 3300 1.25 1.8 <0.00897 SB-USTSW-3 11/16/2022 15 128 2380 1.19 0.805 <0.00973 SB-USTSW-4 11/16/2022 15 96.1 2010 <0.0210 <0.0210 <0.0210 SB-USTSW-5 11/16/2022 15 <3.38 261 0.0151 <0.00165 <0.00165 Minimum Reporting Limit (mg/kg) 50 100 Soil to Groundwater MSCC (mg/kg) -- -- 0.054 1.5 0.2 Residential MSCC (mg/kg) -- -- 22.8 62.5 5.5 Industrial/Commercial MSCC (mg/kg) -- -- 112 934 27 Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42) Include in the table all of the target analytes listed for the method in Apx. B of the Guidelines for Sampling, current version. MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogram Appendix B Reporting Tables \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-3B_Supplemental Investigation Soil Investigation Locations (December 2022).docx 1 Table B-3B: Supplemental Investigation – Soil Investigation Locations (December 2022) Revision Date: 2/3/2023 Incident Number and Name: 48783 Facility ID#: 9753 Analytical Method (e.g., VOC by EPA 8260)  8015 8015 8270 8270 8270 8270 Contaminant of Concern  Gasoline Range Organics [C6-C10] Diesel Range Organics [C10-C28] Fluoranthene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Sample ID Date Collected (mm/dd/yy) Source Area (e.g., Tank Pit 1) Sample Depth (ft BGS) Incident Phase (IAA, LSA, etc.) SB-02 12/19/2022 15 <2.88 2060 0.125 15.4 26.6 5.27 SB-03 12/19/2022 16 214 5840 0.33 45.6 78.2 17.4 SB-05 12/20/2022 18 <2.51 156 <0.0186 <0.0164 <0.0164 <0.0164 Minimum Reporting Limit (mg/kg) 50 100 Soil to Groundwater MSCC (mg/kg) -- -- 0.19 1.9 1.5 0.2 Residential MSCC (mg/kg) -- -- 0.66 6.63 62.5 5.5 Industrial/Commercial MSCC (mg/kg) -- -- 3.27 32.7 934 27 Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42) Include in the table all of the target analytes listed for the method in Apx. B of the Guidelines for Sampling, current version. MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogram Appendix B Reporting Tables \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-3C_Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022).docx 1 Table B-3C: Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Revision Date: 2/3/2023 Incident Number and Name: 48783 Facility ID#: 9753 Analytical Method (e.g., VOC by EPA 8260)  8015 8015 8270 8270 Contaminant of Concern  C9-C22 Aromatics - Calculated C9-C18 Aliphatic - Calculated 2- Methylnaphthalene Naphthalene Sample ID Date Collected (mm/dd/yy) Source Area (e.g., Tank Pit 1) Sample Depth (ft BGS) Incident Phase (IAA, LSA, etc.) SB-01 12/19/2022 11 1094.47 1720 18.4 4.63 Minimum Reporting Limit (mg/kg) Soil to Groundwater MSCC (mg/kg) 31 540 1.5 0.2 Residential MSCC (mg/kg) 469 1560 62.5 5.5 Industrial/Commercial MSCC (mg/kg) 7000 23300 934 27 Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42) Include in the table all of the target analytes listed for the method in Apx. B of the Guidelines for Sampling, current version. MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogram \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 23 Table B-4 – UST Closure – Confirmation Groundwater Analytical Results (January 2023) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-4_UST Closure Confirmation Groundwater Analytical Results (January 2023).docx 1 Table B-4: UST Closure – Confirmation Groundwater Analytical Results (January 2023) Revision Date: 2/2/2023 Incident Number and Name: 48783 Facility ID#: 9753 Analytical Method (e.g., VOC by SM6000B)  or Field Measurement (FM) Contaminant of Concern/Field Measurement  C9-C22 Aromatics - Calculated Benzene Well or SW ID Date Collected (mm/dd/yy) Sample ID Incident Phase (IAA LSA, etc.) MW-1 01/06/2023 MW-1 No Detections MW-2 01/06/2023 MW-2 1101 96.4 Minimum Reporting Limit (ug/l) 2L Standard (ug/l) GCL (ug/l) 5000 NC 2B Standard or EPA National Criteria (ug/l) 200 1 Field measurement parameters include temperature, pH, dissolved oxygen, specific conductivity, Eh, and alkalinity. Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42) Include in the table all of the target analytes listed for the method in Apx. B of the Guidelines for Sampling, current version. Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 24 Table B-5 – Hits Only Summary of Soil Sampling Results Table B-5A – UST Closure – Confirmation Soil Analytical Results (November 2022) Table B-5B – Supplemental Investigation – Soil Investigation Locations (December 2022) Table B-5C – Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022) Table B-5AUST Closure - Confirmation Soil Analytical ResultsNovember 2022 Greensboro, NC Fuel Dispensers Conveyance Lines 2 ft-bgs 7.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 11/17/2022 11/17/2022 11/15/2022 11/16/2022 11/16/2022 11/15/2022 11/16/2022 11/16/2022 11/15/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/15/2022 Gasoline Range Organics [C6 - C10]NC NC NC 50 407 < 2.81 < 2.81 161 655 < 3.47 830 81.7 < 4.37 28.4 128 96.1 < 3.38 < 3.52 < 3.95 < 4.16Diesel Range Organics [C10-C28]NC NC NC 100 15800 < 2.62 51.4 F1 1970 8570 54.4 11800 3300 61.2 < 2.91 2380 2010 261 10.2 < 3.34 < 3.13 Acenaphthene 8.3 930 14000 NC 7.49 < 0.00141 < 0.00158 < 0.00764 < 0.0170 < 0.00170 < 0.0148 < 0.00837 < 0.00151 < 0.00155 < 0.00908 < 0.0196 < 0.00154 < 0.00159 < 0.00181 < 0.00168Fluoranthene3306259340NC< 0.191 < 0.00171 < 0.00192 < 0.00928 < 0.0207 < 0.00206 < 0.0180 < 0.0102 < 0.00183 < 0.00188 < 0.0110 < 0.0238 0.0193 < 0.00194 < 0.00220 < 0.002031-Methylnaphthalene 0.054 22.8 112 NC 53.6 < 0.00151 < 0.00170 0.445 4.95 0.0152 6.78 1.25 < 0.00161 < 0.00166 1.19 < 0.0210 0.0151 < 0.00171 < 0.00194 < 0.001802-Methylnaphthalene 1.5 62.5 934 NC 75.7 < 0.00151 < 0.00170 0.395 7.81 0.017 11.3 1.8 < 0.00161 < 0.00166 0.805 < 0.0210 < 0.00165 < 0.00171 < 0.00194 < 0.00180Naphthalene0.2 5.5 27 NC 18.4 < 0.00151 < 0.00170 < 0.00819 < 0.0182 0.0103 < 0.0159 < 0.00897 < 0.00161 < 0.00166 < 0.00973 < 0.0210 < 0.00165 < 0.00171 < 0.00194 < 0.00180Phenanthrene644697000NC14.4 < 0.00141 < 0.00158 < 0.00764 0.967 < 0.00170 1.12 < 0.00837 < 0.00151 < 0.00155 0.272 < 0.0196 < 0.00154 < 0.00159 < 0.00181 < 0.00168Pyrene2104697000NC< 0.202 < 0.00181 < 0.00204 0.192 1.01 < 0.00218 1.05 0.281 < 0.00194 < 0.00199 0.299 0.374 0.0596 < 0.00205 < 0.00233 < 0.00215 Notes: Only analytes with one or more detected concentration are reported in this table.mg/Kg: milligrams per kilogram ft-bgs: feet below ground surfaceNC: No Criterion < = Less than the detection limitF1 = MS and/or MSD recovery exceeds control limits Green shaded values indicate concentration exceeded the protection of groundwater MSCC.Blue shaded values indicate concentration exceeded the residential soil MSCC.Orange shaded values indicate concentration exceeded the industrial MSCC.2 Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement (NC DEQ UST Section, May 17, 2021). Total Petroleum Hydrocarbons (mg/Kg) Semivolatiles (mg/Kg) 1North Carolina Department of Environmental Quality UST Section: Tables for STIRA, Sampling Guidelines, Assessment Guidelines and Corrective Action Guidelines, July 2021. Analyte Underground Storage Tank Floor Samples UST-2 Sidewall Samples SB-FD-1 SB-CL-1 SB-UST-1-1 SB-UST-1-2 SB-USTSW-8SB-USTSW-2 SB-USTSW-3 SB-USTSW-4 SB-USTSW-5 Floor Samples UST 1 Soil-to-Water Maximum Contaminant Concentration Residential Soil Cleanup Levels Industrial Commercial Soil Cleanup Levels North Carolina DEQ Maximum Soil Contaminant Concentration Levels (MSCCs)1 North Carolina DEQ UST Section TPH Action Levels (mg/Kg) (2) SB-USTSW-7SB-UST-1-3 SB-UST-2-1 SB-UST-2-2 SB-UST-2-3 SB-USTSW-1 SB-USTSW-6 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-5A_UST Closure Confirmation Soil Analytical Results (November 2022).xlsx 1 Table B-5BSupplemental Investigation - Soil Investigation LocationsDecember 2022 Greensboro, NC 12/19/2022 12/19/2022 12/19/2022 12/20/2022 12/20/2022 12/20/2022 12/20/2022 12/21/2022 12/21/2022 Gasoline Range Organics [C6 - C10]NC NC NC 50 < 2.88 214 < 3.46 < 2.51 < 2.45 < 3.50 < 4.13 < 2.58 < 2.71Diesel Range Organics [C10-C28]NC NC NC 100 2060 5840 < 3.13 156 < 2.91 < 2.92 < 3.04 < 2.95 < 2.85 Acenaphthene 8.3 930 14000 NC 1.27 4.41 < 0.00164 < 0.0153 < 0.00150 < 0.00158 < 0.00161 < 0.00158 < 0.00150Acenaphthylene2093014000NC0.548 < 0.0151 < 0.00164 < 0.0153 < 0.00150 < 0.00158 < 0.00161 < 0.00158 < 0.00150 Benzo[a]anthracene 0.17 6.6 32 NC < 0.0210 < 0.0205 < 0.00222 < 0.0208 0.0266 < 0.00214 < 0.00218 < 0.00215 0.0165Benzo[a]pyrene 0.058 0.66 3.2 NC < 0.0232 < 0.0227 < 0.00246 < 0.0230 0.0209 0.0115 < 0.00241 < 0.00238 0.013 Benzo[b]fluoranthene 0.6 6.6 32 NC < 0.0243 < 0.0238 < 0.00257 < 0.0240 0.038 0.0202 < 0.00252 < 0.00249 0.0223 Benzo[g,h,i]perylene 7600 469 7000 NC < 0.0276 < 0.0270 < 0.00292 < 0.0273 0.0106 < 0.00282 < 0.00287 < 0.00283 < 0.00268Benzo[k]fluoranthene 5.8 66 327 NC < 0.0210 < 0.0205 < 0.00222 < 0.0208 0.0115 < 0.00214 < 0.00218 < 0.00215 0.00748 Chrysene 18 663 3270 NC 0.0948 0.244 < 0.00211 < 0.0197 0.0286 0.0154 < 0.00206 < 0.00204 0.0177Fluoranthene0.19 0.66 3.27 NC 0.125 0.33 < 0.00199 < 0.0186 0.0288 0.0188 < 0.00195 < 0.00192 0.0207Fluorene3306259340NC1.84 5.36 < 0.00140 < 0.0131 < 0.00128 < 0.00135 < 0.00138 < 0.00136 < 0.00129 Indeno[1,2,3-cd]pyrene 55 625 9340 NC < 0.0232 < 0.0227 < 0.00246 < 0.0230 0.013 < 0.00236 < 0.00241 < 0.00238 < 0.002251-Methylnaphthalene 1.9 6.63 32.7 NC 15.4 45.6 < 0.00175 < 0.0164 < 0.00160 < 0.00169 < 0.00172 < 0.00170 < 0.001612-Methylnaphthalene 1.5 62.5 934 NC 26.6 78.2 < 0.00175 < 0.0164 < 0.00160 < 0.00169 0.00824 < 0.00170 < 0.00161 Naphthalene 0.2 5.5 27 NC 5.27 17.4 < 0.00175 < 0.0164 < 0.00160 < 0.00169 < 0.00172 < 0.00170 < 0.00161Phenanthrene644697000NC4.56 12.3 < 0.00164 < 0.0153 < 0.00150 < 0.00158 < 0.00161 < 0.00158 0.00725Pyrene2104697000NC0.406 < 0.0194 < 0.00211 < 0.0197 0.0241 0.0158 < 0.00206 < 0.00204 0.0166 Notes: Only analytes with one or more detected concentration are reported in this table. mg/Kg: milligrams per kilogram ft-bgs: feet below ground surface NC: No Criterion < = Less than the detection limit1North Carolina Department of Green shaded values indicate concentration exceeded the protection of groundwater MSCC. Blue shaded values indicate concentration exceeded the residential soil MSCC. Orange shaded values indicate concentration exceeded the industrial MSCC. 2 Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement (NC DEQ UST Section, May 17, 2021). SB-10 (11') Analyte North Carolina DEQ Maximum Soil Contaminant Concentration Levels (MSCCs)1 North Carolina DEQ UST Section TPH Action Levels (2) SB-02 (15')SB-03 (16')SB-04 (20')Soil-to-Water Maximum Contaminant Concentration Residential Soil Cleanup Levels Industrial Commercial Soil Cleanup Levels SB-05 (18')SB-06 (18')SB-07 (17')SB-08 (17')SB-09 (11') 11-ft bgs Semivolatiles (mg/Kg) Total Petroleum Hydrocarbons (mg/Kg() 15-ft bgs 16-ft bgs 20-ft bgs 18-ft bgs 18-ft bgs 17-ft bgs 17-ft bgs 11-ft bgs \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-5B_Supplemental Investigation Soil Investigation Locations - (December 2022).xlsx 1 Table B-5C Permanent Groundwater Monitoring Well – Soil Analytical ResultsDecember 2022Greensboro, NC-463648.0.0 MW-02 (20')SB-01 (11') 12/20/2022 12/19/2022 C5-C8 Aliphatics Laboratory Concentration 68 625 9340 < 7.48 < 4.14 C9-C22 Aromatics - Calculated C9-C10 Aromatics VPH + C11-C22 Aromatics EPH 31 469 7000 26.4 1094.47C9-C12 Aliphatics --------15.5 < 2.15C9-C10 Aromatics --------26.4 4.47 C9-C18 Aliphatics - Lab --------< 1.93 1720C9-C18 Aliphatics - Calculated C9-C12 Aliphatics VPH + C9-C18 Aliphatics EPH 540 1560 23300 15.5 1720C19-C36 Aliphatics Laboratory Concentration #31200 467000 < 1.93 336C11-C22 Aromatics --------< 3.62 1090 Acenaphthene 8.3 930 14000 < 0.0488 1.22Dibenzofuran5.2 15.6 233 < 0.0393 0.644 Fluorene 55 625 9340 < 0.0429 1.642-Methylnaphthalene 1.5 62.5 934 < 0.0453 18.4Naphthalene0.2 5.5 27 < 0.0357 4.63Phenanthrene644697000< 0.0322 3.51 Notes: Only analytes with one or more detected concentration are reported in this table. mg/kg: milligrams per kilogram ft-bgs: feet below ground surface NC: No Criterion < = Less than the detection limit1NCDEQ Preliminary Soil Remediation Goals (PSRG), January 2021 Green shaded values indicate concentration exceeded the protection of groundwater MSCC. Blue shaded values indicate concentration exceeded the residential soil MSCC. Orange shaded values indicate concentration exceeded the industrial MSCC. MCC = Maximum Contaminant Concentration * Calculations provided in Table 10 of NCDEQ Comprehensive Tables for Corrective Action Guidelines, September 2022 # = Health based level > 100% 11-ft bgs GC Semivolatiles (mg/Kg) Total Petroleum Hydrocarbon - Volatiles (mg/Kg) Semivolatiles (mg/Kg) Analyte Calculating MADEP Soil Sample Results for Medium/High Boiling Point Fuels * 20-ft bgs North Carolina DEQ Maximum Soil Contaminant Concentration Levels (MSCCs)1 Soil-to-Water Maximum Contaminant Concentration Residential Soil Cleanup Levels Industrial Commercial Soil Cleanup Levels \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-5C_Permanent Groundwater Monitoring Well – Soil Analytical Results (December 2022).xlsx 1 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 25 Table B-6 – Hits Only UST Closure – Confirmation Groundwater Analytical Results (January 2023) Table B-6Hits Only UST Closure – Confirmation Groundwater Analytical Results (January 2023) 4411 Groometown RoadGreensboro, NC 01/06/2023 01/06/2023 C5-C8 Aliphatics Laboratory Concentration 400(1)--< 26.0 158 C9-C22 Aromatics - Calculated C9-C10 Aromatics VPH + C11-C22 Aromatics EPH 200(1)--< 303 1101 C9-C12 Aliphatics ----< 11.0 362C9-C10 Aromatics ----< 7.00 538 C9-C18 Aliphatics 700(1)--< 147 < 144 C9-C18 Aliphatics - Calculated C9-C12 Aliphatics VPH + C9-C18 Aliphatics EPH 700(1)--< 147 362 C19-C36 Aliphatics Laboratory Concentration 10000(1)--< 147 < 144 C11-C22 Aromatics ----< 303 563 Benzene 1 5000 < 0.270 96.4 Ethylbenzene 600 80000 < 0.200 3.13 m-Xylene & p-Xylene ----< 0.490 140o-Xylene ----< 0.260 125Toluene600260000< 0.250 4.65Xylenes, Total 500 50000 < 0.230 265 Notes: Only analytes with one or more detected concentration are reported in this table. µg/L: micrograms per liter1 North Carolina Department of Environmental Quality UST Section: Comprehensive Tables for Corrective Action Guidelines, January 2021. Blue shaded values indicate concentration exceeded the Ground Water Quality Standard. Green shaded values indicate concentration exceeded the Gross Contamination Levels for Groundwater Volatiles (ug/L) Analyte MW-1 MW-2Calculating MADEP Groundwater Sample Results for Medium/High Boiling Point Fuels * North Carolina Groundwater Quality Standards Gross Contamination Levels for GroundwaterTotal Petroleum Hydrocarbon - Volatiles (ug/L) Total Petroleum Hydrocarbon - Semivolatiles (ug/L) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-6_Hits Only UST Closure – Confirmation Groundwater Analytical Results (January 2023).xlsx 1 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 26 Table B-7 – Summary of Permanent Groundwater Monitoring Well Field Parameters (January 2023) Table B-7 Summary of Permanent Groundwater Monitoring Well Field Parameters (January 2023)Morrisville, North Carolina Location Sample ID Date Sample Time:Static Water Level (feet below ground surface) Time: Volume Purged (Gallons) Cumulative Volume Purged (gallons)Purge Rate: (mL/min) Depth to Water (feet)pH (SU)Temperature (F) Specific Conductivity (us/cm) Dissolved Oxygen (mg/L)Turbidity (NTU's) Oxygen Reduction Potential (m/v)Color Odor 945 955 0.468 0.468 200 16.18 5.96 12.25 266 3.4 10.8 135 1005 0.468 0.936 200 16.2 6.08 13.42 251 2.5 9.7 150 1010 0.234 1.170 200 16.2 6.05 13.51 246 2.2 12.3 163 1015 0.234 1.404 200 16.2 6.05 13.42 245 1.6 9.8 169 1020 0.234 1.638 200 16.2 6.07 13.36 249 1.4 9.4 173 1025 0.234 1.872 200 16.2 6.08 13.28 247 1.3 9.1 175 1030 0.234 2.106 200 16.2 6.07 13.18 245 1.3 9 178 1035 0.234 2.340 200 16.2 6 13 245 1.3 9 178 Location Sample ID Date Sample Time:Static Water Level (feet below ground surface) Time: Volume Purged (Gallons) Cumulative Volume Purged (gallons) Purge Rate: (mL/min) Depth to Water (feet) pH (SU) Temperature (F) Specific Conductivity (us/cm) Dissolved Oxygen (mg/L) Turbidity (NTU's) Oxygen Reduction Potential (m/v)Color Odor 1100 1120 0.728 0.728 200 16.49 6.09 15.41 0.36 2.62 25.6 183 1130 0.364 1.092 200 16.49 6.11 15.93 0.368 0.3 21 174 1135 0.182 1.274 200 16.49 6.12 16.34 0.364 0.27 19.8 168 1140 0.182 1.456 200 16.49 6.12 16.46 0.362 0 18.7 165 1145 0.182 1.638 200 16.49 6.12 16.64 0.358 0 18.5 165 1150 0.182 1.820 200 16.49 6.1 17 358 0 18.5 165 Analytical Parameters Volatile Organic Compounds (40CFR136A 624.1)Semivolatile Organic Compounds (40CFR136A 625.1)Massachusetts - Volatile Petroleum Hydrocarbons (MA DEP MA-VPH)Massachusetts - Extractable Petroleum Hydrocarbons (MA DEP MA-EPH) Not Observed Field Parameters: FORMER TWO 20,000 GALLON UNDERGROUND STORAGE TANK MW-02 1/6/2023 1150 16.39 Start Purging at rate of 200 mL/min Not Observed Field Parameters: 16.12 VICINITY OF FUEL DISPENSER MW-01 1/6/2023 1035 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-7_Summary of Permanent Groundwater Monitoring Well Field Parameters (January 2023).xlsx 1 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 27 Table B-8 – Summary of UST Closure PID Field Soil Readings (November 2022) Table B-8 Summary of UST Closure PIDField Soil Readings (November 2022) Morrisville, North Carolina Sample ID SB-UST-1-1 SB-UST-1-2 SB-UST-1-3 SB-UST-2-1 SB-UST-2-2 SB-UST-2-3 SB-USTSW-1 SB-USTSW-2 SB-USTSW-3 SB-USTSW-4 SB-USTSW-5 SB-USTSW-6 SB-USTSW-7 SB-USTSW-8 Sample Depth (ft)19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 19.5 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs 15 ft-bgs Date 11/15/2022 11/16/2022 11/16/2022 11/15/2022 11/16/2022 11/16/2022 11/15/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/16/2022 11/15/2022 Time 1430 1205 1535 1145 1140 1320 1325 1005 1515 1525 1410 1330 1025 1540 PID (ppm)2.6 220.0 573.0 2.8 917.0 353.0 1.0 0.0 161.0 163.0 78.4 0.0 0.2 2.0 Location Fuel Dispensers Conveyance Lines Sample ID SB-FD-1 SB-CL-1 Sample Depth (ft)2 ft-bgs 7.5 ft-bgs Date 11/17/2022 11/17/2022 Time 950 1150 PID (ppm)108.3 3.7 Analytical Parameters Semivolatile Organic Compounds (SW846 8270 SIM) Gasoline Range Organics (SW846 8015C) Diesel Range Organics (EPA 8015C) Location Floor Samples UST 1 Floor Samples UST-2 Sidewall Samples Underground Storage Tank \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Table B-8_Summary of UST Closure PID Field Soil Readings (November 2022).xlsx 1 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 28 N. Appendices Appendix A – Site Specific Health and Safety Plan (HASP) Appendix B – Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature) Appendix C – Standard procedures (sampling, field equipment decontamination, field screening, etc.) * - included in Appendix F Appendix D – Soil, water, NAPL, and sludge disposal manifests and soil treatment permits Appendix E – Complete chain-of-custody records* - included in Appendix F Appendix F – Copy of all Laboratory Analytical Records Appendix G – Geologic Logs for Borings (related to supplemental investigation only) Appendix H – Monitoring Well Construction Forms (for all wells constructed to date) \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 29 Appendix A Site Specific Health and Safety Plan (HASP) 1 Site Visit Health & Safety Plan Project Flash Project Details Project Number 416460.0000 —Project Flash Project Manager/Phone No. Mike Ursin / 815.275.6478 (cell) Supervisor/Phone No. Paul Furtick / 615.594.6199 Site Details Site Name: Greensboro UPS Freight Warehouse Address: 4411 Groometown Rd. Greensboro, NC 27407 Date of Visit: 11/10/2020 Brief Description of Site Activities and Potential Hazards: Phase I ESA Client Contact: Name Company Phone No. Email Address Bill Preece TFI International Inc. 519-421-3300#2244 bpreece@TFIintl.com Site Contacts: Name Company Phone No. Email Address Eddie Meadows TForce 336-632-3400 SCMGBO@tforcefreight.com Local Emergency Contacts: Ambulance: 911 Fire Department: 911 Police: 911 Other: In the event of an emergency:  Stop work and notify emergency personnel, as required.  Notify other personnel at the site.  As soon as possible, contact the TRC Safety and Project Manager to inform them of the incident.  Call WorkCare (888-449-7787)  Prepare a summary report of the incident for the client representative as required. Travel and Logistics Details General travel from home to site: car Daily travel hotel to site: N/A Name and address of nearest hospital: Kindred Hospital Greensboro 2401 S Side Blvd. Greensboro, NC 27406 Required site security procedures: None are anticipated. Personal Protective Equipment (verify with site contact): 2 Place a check where applicable. If the site will provide indicate - SITE Required Recommended Place a check where applicable. If the site will provide indicate SITE Required Recommended Steel Toed Shoes X Gloves (specify type) Safety Glasses X Respirator (must be cleared for use) Coveralls Long Sleeves Hearing Protection X Insect Repellent Hard Hat Sun Screen Fire Resistant Clothing (FRC) Hi-Vis Vest X Safety Goggles Other (specify) – Face mask X Pre-Visit Planning TRC Representatives will generally be escorted by facility personnel and adhere to site-specific health and safety rules and procedures. The TRC Representative should seek to understand site-specific control measures and request additional information where potential concerns exist. TRC Representatives should never enter an area if the risks are believed to be unacceptable (e.g., uncontrolled chemical hazards). Site-specific H&S requirements have been reviewed with the site contact. Hazard Analysis Potential Hazard General Control Measures Vehicular Traffic TRC personnel shall follow all applicable state and federal traffic laws while traveling to and from the site, and while working on the site. In particular the following laws should be followed: — speed limits, — parking restrictions, — use of wipers and lights during precipitation events, — no cell phone use, etc. Be aware of traffic patterns associated with local businesses near the work site. Allow traffic to enter and exit the businesses in such a manner to avoid creating traffic hazards, back-ups, delays, or potential accident situations. Practice defensive driving while in route to and from the site. Facility Equipment/Machinery Be aware of active and moving client equipment on site. Insects (ticks, bees, spiders, etc.) Site workers with known allergies to insect bites should carry their own medication. In case of emergencies, inform fellow workers of any severe allergies. Use insect repellant as necessary, and as specifically allowed on site. If possible, wear long-sleeved shirts and pants. If appropriate, check for ticks at the end of each day. Have other appropriate first aid supplies handy for bites. Ladders Ladders should only be used if they are in good condition, conform to OSHA requirements, and if they will be used in an appropriate manner. Be especially cautious of slipping on ladders when the ladder or footwear is wet or dirty. Long Hours/Fatigue Long work hours can lead to fatigue, and fatigue can lead to the physical inability to perform the work in a safe manner, or travel to, or from, a work site in a safe manner. If long work hours are scheduled, or if the scheduled work takes longer than planned, field staff should determine if fatigue is, or will be, an issue. Field staff should evaluate whether they are able to complete the work in a safe manner, or whether they are able to travel in a safe manner. If fatigue is an issue, 3 appropriate breaks should be planned or taken, including overnight stays when necessary. Noise Hearing protection must be worn when noise levels exceed 85 dBA in the work area. If you need to raise your voice to be heard at the work site, then hearing protection should be worn. Overhead Hazards Pay attention to overhead equipment, piping, and structures. A hard hat must be worn at all times when overhead hazards are present on site. On-site Traffic (client, contractors, public, semi-trucks, forklifts, etc.) Obey all posted speed limits. Park in designated areas only. Be aware of traffic patterns on site, and during access to the site. Pedestrians should use designated walkways, stay clear of powered industrial vehicles and avoid walking beneath any elevated work (e.g., crane lifts, overhead work). COVID-19 Refer to CP052.1 Field Guidelines COVID-19 attached for specific actions to be taken as part of TRC’s Pandemic Preparedness Program. Local Hospital: Kindred Hospital Greensboro - 2401 S Side Blvd. Greensboro, NC 27406 Directions to local hospital: 4 TRC HEALTH AND SAFETY MANAGEMENT SYSTEM DOCUMENT TITLE: Pandemic Preparedness Program DOCUMENT NUMBER: CP052 Revision Number: 3 APPROVED BY: Mike Glenn Page 8 of 10 EHS Policy Management System Procedures Compliance Programs Forms, Checklists, Permits, etc. Attachment A CP052.1 Field Guidelines COVID-19 STEPS TO FOLLOW IF YOU DEVELOP SYMPTOMS Symptoms and Warning Signs Take the following steps If you experience the following symptoms, which may appear 2-14 days after exposure. • Fever • Cough • Shortness of breath 1. Notify your field and direct supervisor that you feel ill. 2. Immediately isolate yourself and return to your place of lodging (return home if nearby). 3. Contact your personal healthcare provider asap (consider using the Cigna app) for evaluation and follow their instructions. 4. Update your field and direct supervisor of your health and work status (e.g., when do you expect to return to work). 5. If you’re diagnosed with COVID-19 notify Mike Glenn (949-697-7418) and your HR Business Partner immediately. This communication will be treated as confidential. If you develop any of the following emergency warning signs: • Difficulty breathing or shortness of breath, • Persistent pain or pressure in the chest, • New confusion or inability to arouse, • Bluish lips or face This list is not all inclusive so please consult with your medical provider for further guidance. 1. Get medical attention immediately. 2. If you’re diagnosed with COVID-19, notify Mike Glenn (949-697-7418) and your HR Business Partner immediately. This communication will be treated as confidential. Source: CDC COVID-19 Symptoms https://www.cdc.gov/coronavirus/2019-ncov/about/symptoms.html TRC HEALTH AND SAFETY MANAGEMENT SYSTEM DOCUMENT TITLE: Pandemic Preparedness Program DOCUMENT NUMBER: CP052 Revision Number: 3 APPROVED BY: Mike Glenn Page 9 of 10 EHS Policy Management System Procedures Compliance Programs Forms, Checklists, Permits, etc. PRECAUTIONS 1. Practice Social Distancing Avoid “close contact” which is either 1) a “prolonged period of time” spent “within approximately 6 feet or within the room or care area” of an individual who has been positively diagnosed with the virus or 2) “direct contact with infectious secretions.” Do not share eating or drinking utensils, avoid close conversation, and other direct physical contact like hand shaking. “Close contact” does not include activities such as walking by a person or briefly sitting across an office. 2. Hand Hygiene According to the CDC, washing hands with soap and water is the best way to get rid of germs in most situations. If soap and water are not readily available, you can use an alcohol-based hand sanitizer that contains at least 60% alcohol. You can tell if the sanitizer contains at least 60% alcohol by looking at the product label. 3. Practice good respiratory hygiene – covering mouth and nose when coughing or sneezing, using tissues and disposing of them correctly. 4. Obtain immunizations recommended by healthcare providers to help avoid disease. 5. Early self-isolation of those feeling unwell, feverish and having other symptoms of flu. 6. Avoiding touching your eyes, nose or mouth. 7. Frequently disinfect all areas that are likely to have frequent hand contact (like doorknobs, faucets, handrails). CLIENT MEETINGS/INTERACTIONS Be aware of any restrictions or requirements that clients have in place regarding visiting client facilities or attending meetings. Verify with supervisor/project managers prior to visiting client facilities or meetings in person. BACKGROUND The 2019 novel coronavirus, or COVID-19, is a new respiratory virus first identified in Wuhan, Hubei Province, China. It’s called a “novel” — or new — coronavirus, because it is a coronavirus that has not been previously identified. Both the COVID-19 and influenza (flu) are respiratory illnesses, which have similar symptoms. Both are contagious and both can be mild or severe, even fatal in rare cases. The key difference between the novel coronavirus and influenza is we know what to expect from the flu. TRC HEALTH AND SAFETY MANAGEMENT SYSTEM DOCUMENT TITLE: Pandemic Preparedness Program DOCUMENT NUMBER: CP052 Revision Number: 3 APPROVED BY: Mike Glenn Page 10 of 10 EHS Policy Management System Procedures Compliance Programs Forms, Checklists, Permits, etc. SYMPTOMS OF COVID-19 Initial symptoms of COVID-19 usually include fever greater than 100.4°F (38.0°C), cough, and shortness of breath. However, not all affected individuals will exhibit all symptoms. If you experience these symptoms or have been in recent close contact with someone with these symptoms, notify your doctor and stay home. TRANSMISSION Both COVID-19 and the flu can be spread from person to person through droplets caused by an infected person coughing, sneezing or talking. Flu can be spread by an infected person for several days before their symptoms appear, and COVID-19 is believed to be spread in the same manner, but we don’t yet know for sure. \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 30 Appendix B Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature) PROJECT NAME LOCATION ID DATE PROJECT NUMBER START TIME END TIME SAMPLE ID SAMPLE TIME SITE NAME/NUMBER PAGE OF WELL INTEGRITY WELL DIAMETER (INCHES) 1 X 2 4 6 8 OTHER YES NO N/A CAP X TUBING ID (INCHES) 1/8 X 1/4 3/8 1/2 5/8 OTHER CASING X LOCKED X MEASUREMENT POINT (MP) TOP OF RISER (TOR) X TOP OF CASING (TOC) OTHER COLLAR X INITIAL DTW FINAL DTW PROT. CASING TOC/TOR (BMP)FT (BMP)FT STICKUP (AGS)FT DIFFERENCE FT WELL DEPTH SCREEN PID REFILL TIMER (BMP)FT LENGTH FT AMBIENT AIR PPM SETTING SEC WATER DRAWDOWN PID WELL DISCHARGE COLUMN FT VOLUME GAL MOUTH PPM TIMER SETTING SEC (final DTW - initial DTW X well diam. squared X 0.041) CALCULATED TOTAL VOL. DRAWDOWN/ PRESSURE GAL/VOL GAL PURGED GAL TOTAL PURGED TO PUMP PSI (column X well diameter squared X 0.041) (mL per minute X total minutes X 0.00026 gal/mL) FIELD PARAMETERS WITH PROGRAM STABILIZATION CRITERIA (AS LISTED IN THE QAPP) EQUIPMENT DOCUMENTATION X PERISTALTIC X LIQUINOX X SILICON TUBING S. STEEL PUMP MATERIAL X WL METER SUBMERSIBLE DEIONIZED WATER TEFLON TUBING PVC PUMP MATERIAL PID BLADDER POTABLE WATER TEFLON LINED TUBING GEOPROBE SCREEN X WQ METER NITRIC ACID HDPE TUBING TEFLON BLADDER TURB. METER WATTERA HEXANE X LDPE TUBING OTHER X PUMP OTHER METHANOL OTHER OTHER OTHER OTHER OTHER OTHER OTHER FILTERS NO. TYPE ANALYTICAL PARAMETERS X See Chain of Custody PURGE OBSERVATIONS SKETCH/NOTES PURGE WATER YES NO NUMBER OF GALLONS CONTAINERIZED X X GENERATED NO-PURGE METHOD YES NO UTILIZED X Sampler Signature:Print Name: Cait Serowik Checked By:Date: LOW FLOW GROUNDWATER SAMPLING RECORD 10 Maxwell Drive, Suite 200, Clifton Park, NY 12065 QC COLLECTED SAMPLE BOTTLE ID NUMBERS 2.34 If yes, purged approximately 1 standing volume prior to sampling or __________mL for this sample location. 1/31/2023 PARAMETER METHOD NUMBER FIELD FILTERED PRESERVATION METHOD VOLUME REQUIRED SAMPLE COLLECTED DO: nearest tenth (ex. 3.51 = 3.5) TURB: 3 SF max, nearest tenth (6.19 = 6.2, 101 = 101) ORP: 2 SF (44.1 = 44, 191 = 190) TYPE OF PUMP DECON FLUIDS USED TUBING/PUMP/BLADDER MATERIALS EQUIPMENT USED 13 0.245 6 1.3 9 178 FINAL STABILIZED FIELD PARAMETERS (to appropriate significant figures[SF]) TEMP.: nearest degree (ex. 10.1 = 10) COND.: 3 SF max (ex. 3333 = 3330, 0.696 = 0.696) pH: nearest tenth (ex. 5.53 = 5.5) COMMENTS - 1030 16.20 200 13.18 0.245 1020 16.20 200 13.36 0.249 13.28 6.07 1.31 9 178 26 1.35 9.4 173 26 945 BEGIN PURGING TIME 3-5 Minutes DTW (FT) 0.0-0.33 ft Drawdown PURGE RATE (mL/min) TEMP. (oC) (+/- 3 degrees) SP. CONDUCTANCE (mS/cm) (+/- 3%) pH (units) (+/- 0.1 units) 1005 16.20 200 13.42 0.251 955 16.18 150 26 3.42 10.8 135 26 Sheen on top of purge water5.96200 12.25 0.266 6.08 2.47 9.7 0.01312 2.34 LOW FLOW GROUNDWATER SAMPLING RECORD Greensboro Tforce MW-1 1/6/2023 463648.0000.0000 09:45 10:35 12.02 - 16.12 16.20 - - Greensboro TforceMW-01 1035 1 1 0.005606838 DISS. O2 (mg/L) (+/- 10%) TURBIDITY (ntu) (+/- 10% <10 ntu) REDOX (mv) (+/- 10 mv) PUMP INTAKE DEPTH (ft) 28.14 10 0 1.97128 1015 1025 16.20 16.20 200 200 200 1010 16.20 26 12.3 9.8 9.1 163 16913.42 13.51 0.246 0.245 0.247 6.05 6.05 6.08 2.2 1.55 1.33 175 26 6.07 26 PROJECT NAME LOCATION ID DATE PROJECT NUMBER START TIME END TIME SAMPLE ID SAMPLE TIME SITE NAME/NUMBER PAGE OF WELL INTEGRITY WELL DIAMETER (INCHES) 1 X 2 4 6 8 OTHER YES NO N/A CAP X TUBING ID (INCHES) 1/8 X 1/4 3/8 1/2 5/8 OTHER CASING X LOCKED X MEASUREMENT POINT (MP) TOP OF RISER (TOR) X TOP OF CASING (TOC) OTHER COLLAR X INITIAL DTW FINAL DTW PROT. CASING TOC/TOR (BMP)FT (BMP)FT STICKUP (AGS)FT DIFFERENCE FT WELL DEPTH SCREEN PID REFILL TIMER (BMP)FT LENGTH FT AMBIENT AIR PPM SETTING SEC WATER DRAWDOWN PID WELL DISCHARGE COLUMN FT VOLUME GAL MOUTH PPM TIMER SETTING SEC (final DTW - initial DTW X well diam. squared X 0.041) CALCULATED TOTAL VOL. DRAWDOWN/ PRESSURE GAL/VOL GAL PURGED GAL TOTAL PURGED TO PUMP PSI (column X well diameter squared X 0.041) (mL per minute X total minutes X 0.00026 gal/mL) FIELD PARAMETERS WITH PROGRAM STABILIZATION CRITERIA (AS LISTED IN THE QAPP) EQUIPMENT DOCUMENTATION X PERISTALTIC X LIQUINOX X SILICON TUBING S. STEEL PUMP MATERIAL X WL METER SUBMERSIBLE DEIONIZED WATER TEFLON TUBING PVC PUMP MATERIAL PID BLADDER POTABLE WATER TEFLON LINED TUBING GEOPROBE SCREEN X WQ METER NITRIC ACID HDPE TUBING TEFLON BLADDER TURB. METER WATTERA HEXANE X LDPE TUBING OTHER X PUMP OTHER METHANOL OTHER OTHER OTHER OTHER OTHER OTHER OTHER FILTERS NO. TYPE ANALYTICAL PARAMETERS X See Chain of Custody PURGE OBSERVATIONS SKETCH/NOTES PURGE WATER YES NO NUMBER OF GALLONS CONTAINERIZED X X GENERATED NO-PURGE METHOD YES NO UTILIZED X Sampler Signature:Print Name: Cait Serowik Checked By:Date: LOW FLOW GROUNDWATER SAMPLING RECORD 10 Maxwell Drive, Suite 200, Clifton Park, NY 12065 QC COLLECTED SAMPLE BOTTLE ID NUMBERS 1.82 If yes, purged approximately 1 standing volume prior to sampling or __________mL for this sample location. 1/31/2023 PARAMETER METHOD NUMBER FIELD FILTERED PRESERVATION METHOD VOLUME REQUIRED SAMPLE COLLECTED DO: nearest tenth (ex. 3.51 = 3.5) TURB: 3 SF max, nearest tenth (6.19 = 6.2, 101 = 101) ORP: 2 SF (44.1 = 44, 191 = 190) TYPE OF PUMP DECON FLUIDS USED TUBING/PUMP/BLADDER MATERIALS EQUIPMENT USED FINAL STABILIZED FIELD PARAMETERS (to appropriate significant figures[SF])TEMP.: nearest degree (ex. 10.1 = 10) COND.: 3 SF max (ex. 3333 = 3330, 0.696 = 0.696) pH: nearest tenth (ex. 5.53 = 5.5) 17 0.358 6.1 0 18.5 165 241145 16.49 200 16.64 0.358 6.12 0 18.5 165 0.27 19.8 168 24 1140 16.49 200 16.46 0.362 6.12 1135 16.49 200 16.34 0.364 6.12 0 18.7 165 24 6.11 0.3 21 174 24 2.62 25.6 183 24 Slight sheen on top of purge water 6.09 1130 16.49 200 15.93 0.368 1120 16.49 200 15.41 0.36 DISS. O2 (mg/L) (+/- 10%) TURBIDITY (ntu) (+/- 10% <10 ntu) REDOX (mv) (+/- 10 mv) PUMP INTAKE DEPTH (ft) COMMENTS 1110 0.009010989 - TIME 3-5 Minutes DTW (FT) 0.0-0.33 ft Drawdown PURGE RATE (mL/min) TEMP. (oC) (+/- 3 degrees) SP. CONDUCTANCE (mS/cm) (+/- 3%) pH (units) (+/- 0.1 units) 1.6154 1.82 26.24 10 0 - 9.85 - 16.39 16.49 - 0.0164 MW-02 11:50 Greensboro Tforce 1 1 LOW FLOW GROUNDWATER SAMPLING RECORD Greensboro Tforce MW-02 1/6/2023 463648.0000.0000 11:10 11:50 Monitoring Well Development Log <0.3 ft ± 3% ± 0.1 su ± 3% ± 10% ± 10 mv ± 10%(3) Time Flow Rate  (ml/min) Depth to  Water (ft) Temp      (°C) pH          (su) Cond  (mS/cm) D.O. (mg/L) ORP         (mv) Turbidity  (NTU) (3) For values greater than 10. Note: Indicator parameters have stabilized when 3 consecutive readings taken every 5 min are within criteria listed above. (1) Use a previously determined total depth. Confirm the total depth of well after developing. WELL NUMBER WELL INFORMATION Date:  Well  Diameter  (inches) Total  Depth(1) (ft) Depth to  Water TOC  (ft) Depth to  Product  TOC (ft) PID      (ppm) Personnel:  Site Name:  PERMIT NUMBER Site Location:  Job Number:  TOC = top of casing PURGING INFORMATION WATER QUALITY METER CALIBRATION READINGS Pump Type Tubing  Type Pump  Intake  Depth(2) (ft) Purge Start  Time Purge Stop  Time Flow Rate  (ml/min) Total Purge  Vol. (US  Gal) Temp: pH: Cond: D.O.: ORP: Turbidity: Rental Meter Name: Rental Meter Serial No.: (2)Below TOC PURGING PARAMETERS (measurements are to be taken approximately every 5 minutes Criteria: Initials Water Conditions/Comments Weather Conditions:  Purge water too turbid to collect parameter measurements Monitoring Well Development Log <0.3 ft ± 3% ± 0.1 su ± 3% ± 10% ± 10 mv ± 10%(3) Time Flow Rate  (ml/min) Depth to  Water (ft) Temp      (°C) pH          (su) Cond  (mS/cm) D.O. (mg/L) ORP         (mv) Turbidity  (NTU) (3) For values greater than 10. Note: Indicator parameters have stabilized when 3 consecutive readings taken every 5 min are within criteria listed above. (1) Use a previously determined total depth. Confirm the total depth of well after developing. WELL NUMBER WELL INFORMATION Date:  Well  Diameter  (inches) Total  Depth(1) (ft) Depth to  Water TOC  (ft) Depth to  Product  TOC (ft) PID      (ppm) Personnel:  Site Name:  PERMIT NUMBER Site Location:  Job Number:  TOC = top of casing PURGING INFORMATION WATER QUALITY METER CALIBRATION READINGS Pump Type Tubing  Type Pump  Intake  Depth(2) (ft) Purge Start  Time Purge Stop  Time Flow Rate  (ml/min) Total Purge  Vol. (US  Gal) Temp: pH: Cond: D.O.: ORP: Turbidity: Rental Meter Name: Rental Meter Serial No.: (2)Below TOC PURGING PARAMETERS (measurements are to be taken approximately every 5 minutes Criteria: Initials Water Conditions/Comments Weather Conditions:  Purge water too turbid to collect parameter measurements \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 31 Appendix C Standard procedures (sampling, field equipment decontamination, field screening, etc.) * - included in Appendix F \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 32 Appendix D Soil, water, NAPL, and sludge disposal manifests and soil treatment permits \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 33 Appendix E Complete chain-of-custody records* - included in Appendix F \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 34 Appendix F Copy of all Laboratory Analytical Records ANALYTICAL REPORT PREPARED FOR Attn: David Szynal TRC Environmental Corporation 50 International Drive Suite 150 Greenville, South Carolina 29615 Generated 1/13/2023 10:15:56 AM JOB DESCRIPTION Greensboro, NC-463648.0.0 JOB NUMBER 680-228273-1 See page two for job notes and contact information. Savannah GA 31404 5102 LaRoche Avenue Eurofins Savannah Page 1 of 32 1 2 3 4 5 6 7 8 9 10 11 12 Eurofins Savannah Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 1/13/2023 10:15:56 AM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Definitions/Glossary Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 3 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Sample Summary Client: TRC Environmental Corporation Job ID: 680-228273-1 Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID Client Sample ID Matrix Collected Received 680-228273-1 SB-01 (11')Solid 12/19/22 15:15 12/22/22 10:45 680-228273-2 MW-02 (20')Solid 12/20/22 10:10 12/22/22 10:45 Eurofins SavannahPage 4 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Case Narrative Client: TRC Environmental Corporation Job ID: 680-228273-1 Project/Site: Greensboro, NC-463648.0.0 Job ID: 680-228273-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-228273-1 Receipt The samples were received on 12/22/2022 10:45 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 3.3°C GC/MS VOA Method 8260D: The following samples were received in pre-weighed containers with a label that was added in the field, which would cause a slight low bias in the final results: All samples. The tare weights were covered on 5 of 6 vials. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-01 (11') (680-228273-1). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-02 (20') (680-228273-2). Elevated reporting limits (RLs) are provided. Method MAVPH: The following sample was diluted because the base dilution for VPH soil analysis is 1:50:SB-01 (11') (680-228273-1). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAEPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-01 (11') (680-228273-1). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins SavannahPage 5 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-1Client Sample ID: SB-01 (11') Matrix: SolidDate Collected: 12/19/22 15:15 Percent Solids: 85.1Date Received: 12/22/22 10:45 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL ND 0.0597 mg/Kg ☼12/28/22 10:10 12/29/22 16:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acetone 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDBenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDBromoform 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDBromomethane 0.0299 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND2-Butanone (MEK) 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDCarbon disulfide 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDCarbon tetrachloride 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDChlorobenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDChlorodibromomethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDChloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDChloroform 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDChloromethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDcis-1,2-Dichloroethene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDcis-1,3-Dichloropropene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDCyclohexane 0.0119 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,2-Dibromo-3-Chloropropane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,2-Dichlorobenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,3-Dichlorobenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,4-Dichlorobenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDDichlorobromomethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1-Dichloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,2-Dichloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1-Dichloroethene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,2-Dichloropropane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDEthylbenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDEthylene Dibromide 0.0299 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND2-Hexanone 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDIsopropylbenzene 0.0299 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDMethyl acetate 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDMethylcyclohexane 0.0119 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDMethylene Chloride 0.0299 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND4-Methyl-2-pentanone (MIBK) 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDMethyl tert-butyl ether 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDStyrene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1,2,2-Tetrachloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDTetrachloroethene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDToluene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDtrans-1,2-Dichloroethene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDtrans-1,3-Dichloropropene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,2,4-Trichlorobenzene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1,1-Trichloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1,2-Trichloroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDTrichloroethene 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDTrichlorofluoromethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane 0.00597 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDVinyl chloride 0.0119 mg/Kg 12/28/22 10:10 12/29/22 16:14 1☼NDXylenes, Total 4-Bromofluorobenzene (Surr)95 65-130 12/28/22 10:10 12/29/22 16:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 6 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-1Client Sample ID: SB-01 (11') Matrix: SolidDate Collected: 12/19/22 15:15 Percent Solids: 85.1Date Received: 12/22/22 10:45 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Dibromofluoromethane (Surr)105 65-130 12/28/22 10:10 12/29/22 16:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 1,2-Dichloroethane-d4 (Surr)100 12/28/22 10:10 12/29/22 16:14 165-130 Toluene-d8 (Surr)105 12/28/22 10:10 12/29/22 16:14 165-130 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 1.22 0.375 mg/Kg ☼12/29/22 18:45 01/04/23 20:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDAcenaphthylene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDAcetophenone 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDAnthracene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDAtrazine 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzaldehyde 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzo[a]anthracene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzo[a]pyrene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzo[b]fluoranthene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzo[g,h,i]perylene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBenzo[k]fluoranthene 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND1,1'-Biphenyl 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBis(2-chloroethoxy)methane 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBis(2-chloroethyl)ether 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDbis (2-chloroisopropyl) ether 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDBis(2-ethylhexyl) phthalate 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Bromophenyl phenyl ether 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDButyl benzyl phthalate 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDCaprolactam 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDCarbazole 0.751 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Chloroaniline 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Chloro-3-methylphenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2-Chloronaphthalene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2-Chlorophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Chlorophenyl phenyl ether 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDChrysene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDDibenz(a,h)anthracene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼0.644Dibenzofuran 0.751 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND3,3'-Dichlorobenzidine 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4-Dichlorophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDDiethyl phthalate 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4-Dimethylphenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDDimethyl phthalate 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDDi-n-butyl phthalate 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4,6-Dinitro-2-methylphenol 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4-Dinitrophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4-Dinitrotoluene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,6-Dinitrotoluene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDDi-n-octyl phthalate 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDFluoranthene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼1.64Fluorene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDHexachlorobenzene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDHexachlorobutadiene Eurofins Savannah Page 7 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-1Client Sample ID: SB-01 (11') Matrix: SolidDate Collected: 12/19/22 15:15 Percent Solids: 85.1Date Received: 12/22/22 10:45 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL ND 0.375 mg/Kg ☼12/29/22 18:45 01/04/23 20:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Hexachlorocyclopentadiene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDHexachloroethane 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDIndeno[1,2,3-cd]pyrene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDIsophorone 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2-Methylphenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND3 & 4 Methylphenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼4.63Naphthalene 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2-Nitroaniline 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND3-Nitroaniline 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Nitroaniline 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDNitrobenzene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2-Nitrophenol 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND4-Nitrophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDN-Nitrosodi-n-propylamine 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDN-Nitrosodiphenylamine 1.93 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDPentachlorophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼3.51Phenanthrene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDPhenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼NDPyrene 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4,5-Trichlorophenol 0.375 mg/Kg 12/29/22 18:45 01/04/23 20:49 1☼ND2,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)68 25-130 12/29/22 18:45 01/04/23 20:49 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)69 12/29/22 18:45 01/04/23 20:49 118-130 Nitrobenzene-d5 (Surr)67 12/29/22 18:45 01/04/23 20:49 119-130 Phenol-d5 (Surr)62 12/29/22 18:45 01/04/23 20:49 121-130 Terphenyl-d14 (Surr)69 12/29/22 18:45 01/04/23 20:49 131-133 2,4,6-Tribromophenol (Surr)87 12/29/22 18:45 01/04/23 20:49 121-132 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - DL RL MDL 18.4 0.751 mg/Kg ☼12/29/22 18:45 01/05/23 22:25 2 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2-Methylnaphthalene Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL ND 4.14 mg/Kg ☼12/28/22 10:00 12/28/22 17:12 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 2.15 mg/Kg 12/28/22 10:00 12/28/22 17:12 50☼NDC9-C12 Aliphatics 1.15 mg/Kg 12/28/22 10:00 12/28/22 17:12 50☼4.47C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 12/28/22 10:00 12/28/22 17:12 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)99 12/28/22 10:00 12/28/22 17:12 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 1720 9.10 mg/Kg ☼12/30/22 14:32 01/04/23 19:12 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 9.10 mg/Kg 12/30/22 14:32 01/04/23 19:12 5☼336C19-C36 Aliphatics 17.1 mg/Kg 12/30/22 14:32 01/04/23 20:19 5☼1090C11-C22 Aromatics Eurofins Savannah Page 8 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-1Client Sample ID: SB-01 (11') Matrix: SolidDate Collected: 12/19/22 15:15 Percent Solids: 85.1Date Received: 12/22/22 10:45 1-Chlorooctadecane 89 40-140 12/30/22 14:32 01/04/23 19:12 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl (Surr)46 12/30/22 14:32 01/04/23 20:19 540-140 2-Fluorobiphenyl (Surr)81 12/30/22 14:32 01/04/23 20:19 540-140 2-Bromonaphthalene 110 12/30/22 14:32 01/04/23 20:19 540-140 Eurofins Savannah Page 9 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-2Client Sample ID: MW-02 (20') Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL ND 0.0526 mg/Kg ☼12/28/22 10:10 12/29/22 16:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acetone 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDBenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDBromoform 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDBromomethane 0.0263 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND2-Butanone (MEK) 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDCarbon disulfide 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDCarbon tetrachloride 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDChlorobenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDChlorodibromomethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDChloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDChloroform 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDChloromethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDcis-1,2-Dichloroethene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDcis-1,3-Dichloropropene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDCyclohexane 0.0105 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,2-Dibromo-3-Chloropropane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,2-Dichlorobenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,3-Dichlorobenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,4-Dichlorobenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDDichlorobromomethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1-Dichloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,2-Dichloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1-Dichloroethene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,2-Dichloropropane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDEthylbenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDEthylene Dibromide 0.0263 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND2-Hexanone 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDIsopropylbenzene 0.0263 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDMethyl acetate 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDMethylcyclohexane 0.0105 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDMethylene Chloride 0.0263 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND4-Methyl-2-pentanone (MIBK) 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDMethyl tert-butyl ether 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDStyrene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1,2,2-Tetrachloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDTetrachloroethene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDToluene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDtrans-1,2-Dichloroethene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDtrans-1,3-Dichloropropene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,2,4-Trichlorobenzene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1,1-Trichloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1,2-Trichloroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDTrichloroethene 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDTrichlorofluoromethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane 0.00526 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDVinyl chloride 0.0105 mg/Kg 12/28/22 10:10 12/29/22 16:37 1☼NDXylenes, Total 4-Bromofluorobenzene (Surr)93 65-130 12/28/22 10:10 12/29/22 16:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 10 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-2Client Sample ID: MW-02 (20') Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) Dibromofluoromethane (Surr)104 65-130 12/28/22 10:10 12/29/22 16:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 1,2-Dichloroethane-d4 (Surr)100 12/28/22 10:10 12/29/22 16:37 165-130 Toluene-d8 (Surr)105 12/28/22 10:10 12/29/22 16:37 165-130 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL ND 0.393 mg/Kg ☼12/29/22 18:45 01/04/23 21:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDAcenaphthylene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDAcetophenone 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDAnthracene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDAtrazine 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzaldehyde 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzo[a]anthracene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzo[a]pyrene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzo[b]fluoranthene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzo[g,h,i]perylene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBenzo[k]fluoranthene 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND1,1'-Biphenyl 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBis(2-chloroethoxy)methane 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBis(2-chloroethyl)ether 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDbis (2-chloroisopropyl) ether 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDBis(2-ethylhexyl) phthalate 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Bromophenyl phenyl ether 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDButyl benzyl phthalate 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDCaprolactam 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDCarbazole 0.786 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Chloroaniline 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Chloro-3-methylphenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Chloronaphthalene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Chlorophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Chlorophenyl phenyl ether 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDChrysene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDibenz(a,h)anthracene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDibenzofuran 0.786 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND3,3'-Dichlorobenzidine 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4-Dichlorophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDiethyl phthalate 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4-Dimethylphenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDimethyl phthalate 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDi-n-butyl phthalate 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4,6-Dinitro-2-methylphenol 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4-Dinitrophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4-Dinitrotoluene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,6-Dinitrotoluene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDDi-n-octyl phthalate 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDFluoranthene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDFluorene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDHexachlorobenzene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDHexachlorobutadiene Eurofins Savannah Page 11 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-2Client Sample ID: MW-02 (20') Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL ND 0.393 mg/Kg ☼12/29/22 18:45 01/04/23 21:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Hexachlorocyclopentadiene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDHexachloroethane 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDIndeno[1,2,3-cd]pyrene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDIsophorone 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Methylnaphthalene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Methylphenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND3 & 4 Methylphenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDNaphthalene 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Nitroaniline 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND3-Nitroaniline 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Nitroaniline 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDNitrobenzene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2-Nitrophenol 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND4-Nitrophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDN-Nitrosodi-n-propylamine 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDN-Nitrosodiphenylamine 2.03 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDPentachlorophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDPhenanthrene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDPhenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼NDPyrene 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4,5-Trichlorophenol 0.393 mg/Kg 12/29/22 18:45 01/04/23 21:14 1☼ND2,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)72 25-130 12/29/22 18:45 01/04/23 21:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)64 12/29/22 18:45 01/04/23 21:14 118-130 Nitrobenzene-d5 (Surr)65 12/29/22 18:45 01/04/23 21:14 119-130 Phenol-d5 (Surr)65 12/29/22 18:45 01/04/23 21:14 121-130 Terphenyl-d14 (Surr)74 12/29/22 18:45 01/04/23 21:14 131-133 2,4,6-Tribromophenol (Surr)95 12/29/22 18:45 01/04/23 21:14 121-132 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL ND 7.48 mg/Kg ☼12/28/22 10:00 12/28/22 18:03 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 3.88 mg/Kg 12/28/22 10:00 12/28/22 18:03 100☼15.5C9-C12 Aliphatics 2.08 mg/Kg 12/28/22 10:00 12/28/22 18:03 100☼26.4C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)101 70-130 12/28/22 10:00 12/28/22 18:03 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)103 12/28/22 10:00 12/28/22 18:03 10070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL ND 1.93 mg/Kg ☼12/30/22 14:32 01/04/23 10:51 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.93 mg/Kg 12/30/22 14:32 01/04/23 10:51 1☼NDC19-C36 Aliphatics 3.62 mg/Kg 12/30/22 14:32 01/04/23 13:58 1☼NDC11-C22 Aromatics 1-Chlorooctadecane 104 40-140 12/30/22 14:32 01/04/23 10:51 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl (Surr)83 12/30/22 14:32 01/04/23 13:58 140-140 2-Fluorobiphenyl (Surr)86 12/30/22 14:32 01/04/23 13:58 140-140 Eurofins Savannah Page 12 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228273-2Client Sample ID: MW-02 (20') Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) 2-Bromonaphthalene 90 40-140 12/30/22 14:32 01/04/23 13:58 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 13 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8260D - Volatile Organic Compounds by GC/MS Client Sample ID: Method BlankLab Sample ID: MB 680-757200/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 RL MDL Acetone ND 0.0500 mg/Kg 12/29/22 14:16 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00500 mg/Kg 12/29/22 14:16 1Benzene ND 0.00500 mg/Kg 12/29/22 14:16 1Bromoform ND 0.00500 mg/Kg 12/29/22 14:16 1Bromomethane ND 0.0250 mg/Kg 12/29/22 14:16 12-Butanone (MEK) ND 0.00500 mg/Kg 12/29/22 14:16 1Carbon disulfide ND 0.00500 mg/Kg 12/29/22 14:16 1Carbon tetrachloride ND 0.00500 mg/Kg 12/29/22 14:16 1Chlorobenzene ND 0.00500 mg/Kg 12/29/22 14:16 1Chlorodibromomethane ND 0.00500 mg/Kg 12/29/22 14:16 1Chloroethane ND 0.00500 mg/Kg 12/29/22 14:16 1Chloroform ND 0.00500 mg/Kg 12/29/22 14:16 1Chloromethane ND 0.00500 mg/Kg 12/29/22 14:16 1cis-1,2-Dichloroethene ND 0.00500 mg/Kg 12/29/22 14:16 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 12/29/22 14:16 1Cyclohexane ND 0.0100 mg/Kg 12/29/22 14:16 11,2-Dibromo-3-Chloropropane 0.005953 0.00500 mg/Kg 12/29/22 14:16 11,2-Dichlorobenzene ND 0.00500 mg/Kg 12/29/22 14:16 11,3-Dichlorobenzene ND 0.00500 mg/Kg 12/29/22 14:16 11,4-Dichlorobenzene ND 0.00500 mg/Kg 12/29/22 14:16 1Dichlorobromomethane ND 0.00500 mg/Kg 12/29/22 14:16 11,1-Dichloroethane ND 0.00500 mg/Kg 12/29/22 14:16 11,2-Dichloroethane ND 0.00500 mg/Kg 12/29/22 14:16 11,1-Dichloroethene ND 0.00500 mg/Kg 12/29/22 14:16 11,2-Dichloropropane ND 0.00500 mg/Kg 12/29/22 14:16 1Ethylbenzene ND 0.00500 mg/Kg 12/29/22 14:16 1Ethylene Dibromide ND 0.0250 mg/Kg 12/29/22 14:16 12-Hexanone ND 0.00500 mg/Kg 12/29/22 14:16 1Isopropylbenzene ND 0.0250 mg/Kg 12/29/22 14:16 1Methyl acetate ND 0.00500 mg/Kg 12/29/22 14:16 1Methylcyclohexane ND 0.0100 mg/Kg 12/29/22 14:16 1Methylene Chloride ND 0.0250 mg/Kg 12/29/22 14:16 14-Methyl-2-pentanone (MIBK) ND 0.00500 mg/Kg 12/29/22 14:16 1Methyl tert-butyl ether ND 0.00500 mg/Kg 12/29/22 14:16 1Styrene ND 0.00500 mg/Kg 12/29/22 14:16 11,1,2,2-Tetrachloroethane ND 0.00500 mg/Kg 12/29/22 14:16 1Tetrachloroethene ND 0.00500 mg/Kg 12/29/22 14:16 1Toluene ND 0.00500 mg/Kg 12/29/22 14:16 1trans-1,2-Dichloroethene ND 0.00500 mg/Kg 12/29/22 14:16 1trans-1,3-Dichloropropene ND 0.00500 mg/Kg 12/29/22 14:16 11,2,4-Trichlorobenzene ND 0.00500 mg/Kg 12/29/22 14:16 11,1,1-Trichloroethane ND 0.00500 mg/Kg 12/29/22 14:16 11,1,2-Trichloroethane ND 0.00500 mg/Kg 12/29/22 14:16 1Trichloroethene ND 0.00500 mg/Kg 12/29/22 14:16 1Trichlorofluoromethane ND 0.00500 mg/Kg 12/29/22 14:16 11,1,2-Trichloro-1,2,2-trifluoroethane ND 0.00500 mg/Kg 12/29/22 14:16 1Vinyl chloride ND 0.0100 mg/Kg 12/29/22 14:16 1Xylenes, Total Eurofins Savannah Page 14 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-757200/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 4-Bromofluorobenzene (Surr)94 65-130 12/29/22 14:16 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 104 12/29/22 14:16 1Dibromofluoromethane (Surr)65-130 94 12/29/22 14:16 11,2-Dichloroethane-d4 (Surr)65-130 106 12/29/22 14:16 1Toluene-d8 (Surr)65-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757200/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 Acetone 0.250 0.2086 mg/Kg 83 10 -150 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Benzene 0.0500 0.05257 mg/Kg 105 70 -130 Bromoform 0.0500 0.05366 mg/Kg 107 68 -130 Bromomethane 0.0500 0.05956 mg/Kg 119 70 -130 2-Butanone (MEK)0.250 0.1977 mg/Kg 79 40 -150 Carbon disulfide 0.0500 0.06472 mg/Kg 129 70 -130 Carbon tetrachloride 0.0500 0.05298 mg/Kg 106 70 -130 Chlorobenzene 0.0500 0.05635 mg/Kg 113 70 -130 Chlorodibromomethane 0.0500 0.05357 mg/Kg 107 64 -133 Chloroethane 0.0500 0.05564 mg/Kg 111 70 -130 Chloroform 0.0500 0.05032 mg/Kg 101 70 -130 Chloromethane 0.0500 0.04001 mg/Kg 80 70 -130 cis-1,2-Dichloroethene 0.0500 0.04933 mg/Kg 99 70 -130 cis-1,3-Dichloropropene 0.0500 0.05007 mg/Kg 100 70 -130 Cyclohexane 0.0500 0.05475 mg/Kg 109 70 -130 1,2-Dibromo-3-Chloropropane 0.0500 0.04302 mg/Kg 86 42 -145 1,2-Dichlorobenzene 0.0500 0.06164 mg/Kg 123 70 -130 1,3-Dichlorobenzene 0.0500 0.05299 mg/Kg 106 70 -130 1,4-Dichlorobenzene 0.0500 0.05393 mg/Kg 108 70 -130 Dichlorobromomethane 0.0500 0.04971 mg/Kg 99 70 -130 1,1-Dichloroethane 0.0500 0.04920 mg/Kg 98 70 -130 1,2-Dichloroethane 0.0500 0.05067 mg/Kg 101 68 -139 1,1-Dichloroethene 0.0500 0.05843 mg/Kg 117 69 -130 1,2-Dichloropropane 0.0500 0.05030 mg/Kg 101 70 -130 Ethylbenzene 0.0500 0.05382 mg/Kg 108 70 -130 Ethylene Dibromide 0.0500 0.05508 mg/Kg 110 48 -150 2-Hexanone 0.250 0.2018 mg/Kg 81 30 -150 Isopropylbenzene 0.0500 0.05567 mg/Kg 111 70 -130 Methyl acetate 0.100 0.09180 mg/Kg 92 22 -150 Methylcyclohexane 0.0500 0.05418 mg/Kg 108 69 -110 Methylene Chloride 0.0500 0.05501 mg/Kg 110 54 -149 4-Methyl-2-pentanone (MIBK)0.250 0.2069 mg/Kg 83 34 -150 Methyl tert-butyl ether 0.0500 0.05075 mg/Kg 102 70 -130 Styrene 0.0500 0.05472 mg/Kg 109 70 -130 1,1,2,2-Tetrachloroethane 0.0500 0.05000 mg/Kg 100 64 -130 Tetrachloroethene 0.0500 0.05988 mg/Kg 120 70 -130 Toluene 0.0500 0.05385 mg/Kg 108 70 -130 trans-1,2-Dichloroethene 0.0500 0.05407 mg/Kg 108 67 -130 Eurofins Savannah Page 15 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757200/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 trans-1,3-Dichloropropene 0.0500 0.05102 mg/Kg 102 54 -150 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2,4-Trichlorobenzene 0.0500 0.05338 mg/Kg 107 70 -130 1,1,1-Trichloroethane 0.0500 0.05150 mg/Kg 103 70 -130 1,1,2-Trichloroethane 0.0500 0.04946 mg/Kg 99 56 -146 Trichloroethene 0.0500 0.05503 mg/Kg 110 70 -130 Trichlorofluoromethane 0.0500 0.06135 mg/Kg 123 70 -130 1,1,2-Trichloro-1,2,2-trifluoroetha ne 0.0500 0.06044 mg/Kg 121 70 -130 Vinyl chloride 0.0500 0.05418 mg/Kg 108 70 -130 Xylenes, Total 0.100 0.1071 mg/Kg 107 70 -130 4-Bromofluorobenzene (Surr)65 -130 Surrogate 95 LCS LCS Qualifier Limits%Recovery 108Dibromofluoromethane (Surr)65 -130 981,2-Dichloroethane-d4 (Surr)65 -130 104Toluene-d8 (Surr)65 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757200/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 Acetone 0.250 0.2048 mg/Kg 82 10 -150 2 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Benzene 0.0500 0.05209 mg/Kg 104 70 -130 1 30 Bromoform 0.0500 0.05363 mg/Kg 107 68 -130 0 30 Bromomethane 0.0500 0.05989 mg/Kg 120 70 -130 1 30 2-Butanone (MEK)0.250 0.1934 mg/Kg 77 40 -150 2 30 Carbon disulfide 0.0500 0.06461 mg/Kg 129 70 -130 0 30 Carbon tetrachloride 0.0500 0.05315 mg/Kg 106 70 -130 0 30 Chlorobenzene 0.0500 0.05633 mg/Kg 113 70 -130 0 30 Chlorodibromomethane 0.0500 0.05290 mg/Kg 106 64 -133 1 30 Chloroethane 0.0500 0.05579 mg/Kg 112 70 -130 0 30 Chloroform 0.0500 0.05024 mg/Kg 100 70 -130 0 30 Chloromethane 0.0500 0.03992 mg/Kg 80 70 -130 0 30 cis-1,2-Dichloroethene 0.0500 0.04867 mg/Kg 97 70 -130 1 30 cis-1,3-Dichloropropene 0.0500 0.04942 mg/Kg 99 70 -130 1 30 Cyclohexane 0.0500 0.05532 mg/Kg 111 70 -130 1 30 1,2-Dibromo-3-Chloropropane 0.0500 0.04209 mg/Kg 84 42 -145 2 30 1,2-Dichlorobenzene 0.0500 0.05949 mg/Kg 119 70 -130 4 30 1,3-Dichlorobenzene 0.0500 0.05257 mg/Kg 105 70 -130 1 30 1,4-Dichlorobenzene 0.0500 0.05366 mg/Kg 107 70 -130 1 30 Dichlorobromomethane 0.0500 0.04883 mg/Kg 98 70 -130 2 30 1,1-Dichloroethane 0.0500 0.04911 mg/Kg 98 70 -130 0 30 1,2-Dichloroethane 0.0500 0.04963 mg/Kg 99 68 -139 2 30 1,1-Dichloroethene 0.0500 0.05853 mg/Kg 117 69 -130 0 50 1,2-Dichloropropane 0.0500 0.04854 mg/Kg 97 70 -130 4 30 Ethylbenzene 0.0500 0.05368 mg/Kg 107 70 -130 0 30 Ethylene Dibromide 0.0500 0.05361 mg/Kg 107 48 -150 3 30 2-Hexanone 0.250 0.1970 mg/Kg 79 30 -150 2 30 Eurofins Savannah Page 16 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757200/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757200 Isopropylbenzene 0.0500 0.05635 mg/Kg 113 70 -130 1 30 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Methyl acetate 0.100 0.08930 mg/Kg 89 22 -150 3 30 Methylcyclohexane 0.0500 0.05334 mg/Kg 107 69 -110 2 30 Methylene Chloride 0.0500 0.05507 mg/Kg 110 54 -149 0 30 4-Methyl-2-pentanone (MIBK)0.250 0.2037 mg/Kg 81 34 -150 2 30 Methyl tert-butyl ether 0.0500 0.05180 mg/Kg 104 70 -130 2 30 Styrene 0.0500 0.05592 mg/Kg 112 70 -130 2 30 1,1,2,2-Tetrachloroethane 0.0500 0.04954 mg/Kg 99 64 -130 1 30 Tetrachloroethene 0.0500 0.05988 mg/Kg 120 70 -130 0 30 Toluene 0.0500 0.05363 mg/Kg 107 70 -130 0 30 trans-1,2-Dichloroethene 0.0500 0.05400 mg/Kg 108 67 -130 0 30 trans-1,3-Dichloropropene 0.0500 0.05012 mg/Kg 100 54 -150 2 30 1,2,4-Trichlorobenzene 0.0500 0.05295 mg/Kg 106 70 -130 1 30 1,1,1-Trichloroethane 0.0500 0.05174 mg/Kg 103 70 -130 0 30 1,1,2-Trichloroethane 0.0500 0.04858 mg/Kg 97 56 -146 2 30 Trichloroethene 0.0500 0.05557 mg/Kg 111 70 -130 1 30 Trichlorofluoromethane 0.0500 0.06124 mg/Kg 122 70 -130 0 30 1,1,2-Trichloro-1,2,2-trifluoroetha ne 0.0500 0.05999 mg/Kg 120 70 -130 1 40 Vinyl chloride 0.0500 0.05422 mg/Kg 108 70 -130 0 30 Xylenes, Total 0.100 0.1073 mg/Kg 107 70 -130 0 30 4-Bromofluorobenzene (Surr)65 -130 Surrogate 94 LCSD LCSD Qualifier Limits%Recovery 106Dibromofluoromethane (Surr)65 -130 961,2-Dichloroethane-d4 (Surr)65 -130 106Toluene-d8 (Surr)65 -130 Method: 8270E - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 680-757327/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757815 Prep Batch: 757327 RL MDL Acenaphthene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Acenaphthylene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Acetophenone ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Anthracene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Atrazine ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzaldehyde ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzo[a]anthracene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzo[a]pyrene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzo[b]fluoranthene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzo[g,h,i]perylene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Benzo[k]fluoranthene ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 11,1'-Biphenyl ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Bis(2-chloroethoxy)methane ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Bis(2-chloroethyl)ether Eurofins Savannah Page 17 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-757327/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757815 Prep Batch: 757327 RL MDL bis (2-chloroisopropyl) ether ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Bis(2-ethylhexyl) phthalate ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Bromophenyl phenyl ether ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Butyl benzyl phthalate ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Caprolactam ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Carbazole ND 0.631 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Chloroaniline ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Chloro-3-methylphenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Chloronaphthalene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Chlorophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Chlorophenyl phenyl ether ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Chrysene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Dibenz(a,h)anthracene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Dibenzofuran ND 0.631 mg/Kg 12/29/22 18:45 01/04/23 12:49 13,3'-Dichlorobenzidine ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,4-Dichlorophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Diethyl phthalate ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,4-Dimethylphenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Dimethyl phthalate ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Di-n-butyl phthalate ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 14,6-Dinitro-2-methylphenol ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,4-Dinitrophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,4-Dinitrotoluene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,6-Dinitrotoluene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Di-n-octyl phthalate ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Fluoranthene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Fluorene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Hexachlorobenzene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Hexachlorobutadiene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Hexachlorocyclopentadiene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Hexachloroethane ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Indeno[1,2,3-cd]pyrene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Isophorone ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Methylnaphthalene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Methylphenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 13 & 4 Methylphenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Naphthalene ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Nitroaniline ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 13-Nitroaniline ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Nitroaniline ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Nitrobenzene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12-Nitrophenol ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 14-Nitrophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1N-Nitrosodi-n-propylamine ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1N-Nitrosodiphenylamine ND 1.63 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Pentachlorophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Phenanthrene ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Phenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1Pyrene Eurofins Savannah Page 18 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-757327/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757815 Prep Batch: 757327 RL MDL 2,4,5-Trichlorophenol ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.316 mg/Kg 12/29/22 18:45 01/04/23 12:49 12,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)71 25-130 01/04/23 12:49 1 MB MB Surrogate 12/29/22 18:45 Dil FacPreparedAnalyzedQualifierLimits%Recovery 60 12/29/22 18:45 01/04/23 12:49 12-Fluorophenol (Surr)18-130 65 12/29/22 18:45 01/04/23 12:49 1Nitrobenzene-d5 (Surr)19-130 59 12/29/22 18:45 01/04/23 12:49 1Phenol-d5 (Surr)21-130 79 12/29/22 18:45 01/04/23 12:49 1Terphenyl-d14 (Surr)31-133 84 12/29/22 18:45 01/04/23 12:49 12,4,6-Tribromophenol (Surr)21-132 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757327/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757815 Prep Batch: 757327 Acenaphthene 6.35 4.708 mg/Kg 74 33 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 6.35 4.937 mg/Kg 78 34 -130 Acetophenone 6.35 4.609 mg/Kg 73 28 -130 Anthracene 6.35 5.151 mg/Kg 81 39 -130 Atrazine 6.35 5.254 mg/Kg 83 27 -130 Benzaldehyde 6.35 4.999 mg/Kg 79 10 -130 Benzo[a]anthracene 6.35 5.416 mg/Kg 85 40 -130 Benzo[a]pyrene 6.35 5.360 mg/Kg 84 37 -131 Benzo[b]fluoranthene 6.35 4.912 mg/Kg 77 35 -130 Benzo[g,h,i]perylene 6.35 5.884 mg/Kg 93 39 -130 Benzo[k]fluoranthene 6.35 5.225 mg/Kg 82 35 -130 1,1'-Biphenyl 6.35 4.584 mg/Kg 72 32 -130 Bis(2-chloroethoxy)methane 6.35 4.708 mg/Kg 74 29 -130 Bis(2-chloroethyl)ether 6.35 4.433 mg/Kg 70 18 -130 bis (2-chloroisopropyl) ether 6.35 4.600 mg/Kg 72 12 -130 Bis(2-ethylhexyl) phthalate 6.35 5.016 mg/Kg 79 39 -130 4-Bromophenyl phenyl ether 6.35 5.286 mg/Kg 83 32 -130 Butyl benzyl phthalate 6.35 5.325 mg/Kg 84 38 -130 Caprolactam 6.35 5.998 mg/Kg 95 27 -148 Carbazole 6.35 5.230 mg/Kg 82 43 -130 4-Chloroaniline 6.35 4.138 mg/Kg 65 10 -130 4-Chloro-3-methylphenol 6.35 5.061 mg/Kg 80 31 -130 2-Chloronaphthalene 6.35 4.626 mg/Kg 73 30 -130 2-Chlorophenol 6.35 4.606 mg/Kg 73 28 -130 4-Chlorophenyl phenyl ether 6.35 4.951 mg/Kg 78 32 -130 Chrysene 6.35 5.060 mg/Kg 80 40 -130 Dibenz(a,h)anthracene 6.35 5.617 mg/Kg 89 37 -130 Dibenzofuran 6.35 4.797 mg/Kg 76 34 -130 3,3'-Dichlorobenzidine 6.35 4.934 mg/Kg 78 10 -130 2,4-Dichlorophenol 6.35 5.155 mg/Kg 81 30 -130 Diethyl phthalate 6.35 4.930 mg/Kg 78 36 -130 2,4-Dimethylphenol 6.35 4.899 mg/Kg 77 34 -130 Eurofins Savannah Page 19 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757327/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757815 Prep Batch: 757327 Dimethyl phthalate 6.35 4.803 mg/Kg 76 36 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Di-n-butyl phthalate 6.35 5.320 mg/Kg 84 39 -130 4,6-Dinitro-2-methylphenol 12.7 12.50 mg/Kg 98 22 -130 2,4-Dinitrophenol 12.7 10.51 mg/Kg 83 10 -130 2,4-Dinitrotoluene 6.35 5.253 mg/Kg 83 34 -130 2,6-Dinitrotoluene 6.35 4.983 mg/Kg 79 33 -130 Di-n-octyl phthalate 6.35 5.477 mg/Kg 86 38 -131 Fluoranthene 6.35 5.563 mg/Kg 88 38 -130 Fluorene 6.35 4.753 mg/Kg 75 34 -130 Hexachlorobenzene 6.35 5.395 mg/Kg 85 28 -130 Hexachlorobutadiene 6.35 4.770 mg/Kg 75 22 -130 Hexachlorocyclopentadiene 6.35 5.119 mg/Kg 81 11 -130 Hexachloroethane 6.35 4.140 mg/Kg 65 21 -130 Indeno[1,2,3-cd]pyrene 6.35 6.049 mg/Kg 95 40 -130 Isophorone 6.35 4.655 mg/Kg 73 26 -130 2-Methylnaphthalene 6.35 4.843 mg/Kg 76 28 -130 2-Methylphenol 6.35 4.491 mg/Kg 71 30 -130 3 & 4 Methylphenol 6.35 4.356 mg/Kg 69 31 -130 Naphthalene 6.35 4.512 mg/Kg 71 25 -130 2-Nitroaniline 6.35 5.108 mg/Kg 81 26 -130 3-Nitroaniline 6.35 4.249 mg/Kg 67 10 -130 4-Nitroaniline 6.35 4.948 mg/Kg 78 25 -130 Nitrobenzene 6.35 4.651 mg/Kg 73 25 -130 2-Nitrophenol 6.35 4.950 mg/Kg 78 24 -130 4-Nitrophenol 12.7 11.14 mg/Kg 88 25 -130 N-Nitrosodi-n-propylamine 6.35 4.207 mg/Kg 66 24 -130 N-Nitrosodiphenylamine 6.35 5.047 mg/Kg 80 37 -130 Pentachlorophenol 12.7 12.98 mg/Kg 102 16 -135 Phenanthrene 6.35 5.155 mg/Kg 81 38 -130 Phenol 6.35 4.690 mg/Kg 74 27 -130 Pyrene 6.35 5.165 mg/Kg 81 40 -130 2,4,5-Trichlorophenol 6.35 5.220 mg/Kg 82 33 -130 2,4,6-Trichlorophenol 6.35 5.351 mg/Kg 84 31 -130 2-Fluorobiphenyl (Surr)25 -130 Surrogate 71 LCS LCS Qualifier Limits%Recovery 732-Fluorophenol (Surr)18 -130 73Nitrobenzene-d5 (Surr)19 -130 72Phenol-d5 (Surr)21 -130 81Terphenyl-d14 (Surr)31 -133 942,4,6-Tribromophenol (Surr)21 -132 Eurofins Savannah Page 20 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-606420/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 606419 Prep Batch: 606420 RL MDL C5-C8 Aliphatics ND 2.70 mg/Kg 12/28/22 10:00 12/28/22 16:21 50 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 1.40 mg/Kg 12/28/22 10:00 12/28/22 16:21 50C9-C12 Aliphatics ND 0.750 mg/Kg 12/28/22 10:00 12/28/22 16:21 50C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)97 70-130 12/28/22 16:21 50 MB MB Surrogate 12/28/22 10:00 Dil FacPreparedAnalyzedQualifierLimits%Recovery 97 12/28/22 10:00 12/28/22 16:21 50a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-606420/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 606419 Prep Batch: 606420 C5-C8 Aliphatics 15.0 11.98 mg/Kg 80 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 17.5 14.74 mg/Kg 84 70 -130 C9-C10 Aromatics 2.50 2.412 mg/Kg 96 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 101 LCS LCS Qualifier Limits%Recovery 102a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-606420/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 606419 Prep Batch: 606420 C5-C8 Aliphatics 15.0 14.88 mg/Kg 99 70 -130 22 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 17.5 17.39 mg/Kg 99 70 -130 17 25 C9-C10 Aromatics 2.50 2.916 mg/Kg 117 70 -130 19 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 100 LCSD LCSD Qualifier Limits%Recovery 100a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: SB-01 (11')Lab Sample ID: 680-228273-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 606419 Prep Batch: 606420 C5-C8 Aliphatics ND 23.0 23.30 mg/Kg 101 70 -130☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C9-C12 Aliphatics ND 26.9 25.18 mg/Kg 94 70 -130☼ C9-C10 Aromatics 4.47 3.84 9.081 mg/Kg 120 70 -130☼ a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 100 MS MS Qualifier Limits%Recovery 102a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Savannah Page 21 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: SB-01 (11')Lab Sample ID: 680-228273-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 606419 Prep Batch: 606420 C5-C8 Aliphatics ND 23.0 23.87 mg/Kg 104 70 -130 2 25☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C9-C12 Aliphatics ND 26.9 25.09 mg/Kg 93 70 -130 0 25☼ C9-C10 Aromatics 4.47 3.84 7.318 mg/Kg 74 70 -130 22 25☼ a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 100 MSD MSD Qualifier Limits%Recovery 102a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-606813/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607115 Prep Batch: 606813 RL MDL C9-C18 Aliphatics ND 1.60 mg/Kg 12/30/22 14:32 01/04/23 08:53 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 1.60 mg/Kg 12/30/22 14:32 01/04/23 08:53 1C19-C36 Aliphatics 1-Chlorooctadecane 106 40-140 01/04/23 08:53 1 MB MB Surrogate 12/30/22 14:32 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-606813/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607117 Prep Batch: 606813 RL MDL C11-C22 Aromatics ND 3.00 mg/Kg 12/30/22 14:32 01/04/23 11:41 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl (Surr)73 40-140 01/04/23 11:41 1 MB MB Surrogate 12/30/22 14:32 Dil FacPreparedAnalyzedQualifierLimits%Recovery 80 12/30/22 14:32 01/04/23 11:41 12-Fluorobiphenyl (Surr)40-140 80 12/30/22 14:32 01/04/23 11:41 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-606813/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607115 Prep Batch: 606813 C9-C18 Aliphatics 20.0 13.05 mg/Kg 65 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 27.10 mg/Kg 102 40 -140 1-Chlorooctadecane 40 -140 Surrogate 92 LCS LCS Qualifier Limits%Recovery Eurofins Savannah Page 22 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-606813/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607117 Prep Batch: 606813 C11-C22 Aromatics 56.7 48.88 mg/Kg 86 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl (Surr)40 -140 Surrogate 80 LCS LCS Qualifier Limits%Recovery 882-Fluorobiphenyl (Surr)40 -140 842-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-606813/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607115 Prep Batch: 606813 C9-C18 Aliphatics 20.0 12.70 mg/Kg 63 40 -140 3 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 26.7 22.76 mg/Kg 85 40 -140 17 50 1-Chlorooctadecane 40 -140 Surrogate 91 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-606813/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 607117 Prep Batch: 606813 C11-C22 Aromatics 56.7 46.47 mg/Kg 82 40 -140 5 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl (Surr)40 -140 Surrogate 76 LCSD LCSD Qualifier Limits%Recovery 872-Fluorobiphenyl (Surr)40 -140 832-Bromonaphthalene 40 -140 Eurofins Savannah Page 23 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC/MS VOA Prep Batch: 757043 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035680-228273-1 SB-01 (11')Total/NA Solid 5035680-228273-2 MW-02 (20')Total/NA Analysis Batch: 757200 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 757043680-228273-1 SB-01 (11')Total/NA Solid 8260D 757043680-228273-2 MW-02 (20')Total/NA Solid 8260DMB 680-757200/8 Method Blank Total/NA Solid 8260DLCS 680-757200/5 Lab Control Sample Total/NA Solid 8260DLCSD 680-757200/6 Lab Control Sample Dup Total/NA GC/MS Semi VOA Prep Batch: 757327 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-228273-1 SB-01 (11')Total/NA Solid 3546680-228273-1 - DL SB-01 (11')Total/NA Solid 3546680-228273-2 MW-02 (20')Total/NA Solid 3546MB 680-757327/19-A Method Blank Total/NA Solid 3546LCS 680-757327/20-A Lab Control Sample Total/NA Analysis Batch: 757815 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 757327680-228273-1 SB-01 (11')Total/NA Solid 8270E 757327680-228273-2 MW-02 (20')Total/NA Solid 8270E 757327MB 680-757327/19-A Method Blank Total/NA Solid 8270E 757327LCS 680-757327/20-A Lab Control Sample Total/NA Analysis Batch: 758012 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 757327680-228273-1 - DL SB-01 (11')Total/NA GC VOA Analysis Batch: 606419 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 606420680-228273-1 SB-01 (11')Total/NA Solid MAVPH 606420680-228273-2 MW-02 (20')Total/NA Solid MAVPH 606420MB 400-606420/1-A Method Blank Total/NA Solid MAVPH 606420LCS 400-606420/2-A Lab Control Sample Total/NA Solid MAVPH 606420LCSD 400-606420/3-A Lab Control Sample Dup Total/NA Solid MAVPH 606420680-228273-1 MS SB-01 (11')Total/NA Solid MAVPH 606420680-228273-1 MSD SB-01 (11')Total/NA Prep Batch: 606420 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035680-228273-1 SB-01 (11')Total/NA Solid 5035680-228273-2 MW-02 (20')Total/NA Solid 5035MB 400-606420/1-A Method Blank Total/NA Solid 5035LCS 400-606420/2-A Lab Control Sample Total/NA Solid 5035LCSD 400-606420/3-A Lab Control Sample Dup Total/NA Solid 5035680-228273-1 MS SB-01 (11')Total/NA Eurofins Savannah Page 24 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC VOA (Continued) Prep Batch: 606420 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035680-228273-1 MSD SB-01 (11')Total/NA GC Semi VOA Prep Batch: 606813 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-228273-1 SB-01 (11')Total/NA Solid 3546680-228273-2 MW-02 (20')Total/NA Solid 3546MB 400-606813/1-A Method Blank Total/NA Solid 3546LCS 400-606813/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-606813/3-A Lab Control Sample Dup Total/NA Analysis Batch: 607115 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 606813680-228273-2 MW-02 (20')Total/NA Solid MA-EPH 606813MB 400-606813/1-A Method Blank Total/NA Solid MA-EPH 606813LCS 400-606813/2-A Lab Control Sample Total/NA Solid MA-EPH 606813LCSD 400-606813/3-A Lab Control Sample Dup Total/NA Analysis Batch: 607117 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 606813680-228273-2 MW-02 (20')Total/NA Solid MA-EPH 606813MB 400-606813/1-A Method Blank Total/NA Solid MA-EPH 606813LCS 400-606813/2-A Lab Control Sample Total/NA Solid MA-EPH 606813LCSD 400-606813/3-A Lab Control Sample Dup Total/NA Analysis Batch: 607250 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 606813680-228273-1 SB-01 (11')Total/NA Analysis Batch: 607252 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 606813680-228273-1 SB-01 (11')Total/NA General Chemistry Analysis Batch: 757750 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture680-228273-1 SB-01 (11')Total/NA Solid Moisture680-228273-2 MW-02 (20')Total/NA Eurofins Savannah Page 25 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228273-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-01 (11')Lab Sample ID: 680-228273-1 Matrix: SolidDate Collected: 12/19/22 15:15 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 19:041 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-01 (11')Lab Sample ID: 680-228273-1 Matrix: SolidDate Collected: 12/19/22 15:15 Percent Solids: 85.1Date Received: 12/22/22 10:45 Prep 5035 FES12/28/22 10:10 EET SAV757043 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 4.92 g 5 mL Analysis 8260D 1 757200 12/29/22 16:14 Y1S EET SAVTotal/NA 5 g 5 g CMSP2Instrument ID: Prep 3546 757327 12/29/22 18:45 MJ EET SAVTotal/NA 15.50 g 1 mL Analysis 8270E 1 757815 01/04/23 20:49 T1C EET SAVTotal/NA 1 mL 1 mL CMSGInstrument ID: Prep 3546 DL 757327 12/29/22 18:45 MJ EET SAVTotal/NA 15.50 g 1 mL Analysis 8270E DL 2 758012 01/05/23 22:25 T1C EET SAVTotal/NA 1 mL 1 mL CMSTInstrument ID: Prep 5035 606420 12/28/22 10:00 SAB EET PENTotal/NA 4.324 g 5.0 g Analysis MAVPH 50 606419 12/28/22 17:12 SAB EET PENTotal/NA 5 mL 5 mL CH_TRACYInstrument ID: Prep 3546 606813 12/30/22 14:32 KWS EET PENTotal/NA 15.50 g 2 mL Analysis MA-EPH 5 607250 01/04/23 19:12 RS EET PENTotal/NA EvaInstrument ID: Prep 3546 606813 12/30/22 14:32 KWS EET PENTotal/NA 15.50 g 2 mL Analysis MA-EPH 5 607252 01/04/23 20:19 RS EET PENTotal/NA EvaInstrument ID: Client Sample ID: MW-02 (20')Lab Sample ID: 680-228273-2 Matrix: SolidDate Collected: 12/20/22 10:10 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 19:041 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: MW-02 (20')Lab Sample ID: 680-228273-2 Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Prep 5035 FES12/28/22 10:10 EET SAV757043 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.852 g 5 mL Analysis 8260D 1 757200 12/29/22 16:37 Y1S EET SAVTotal/NA 5 g 5 g CMSP2Instrument ID: Prep 3546 757327 12/29/22 18:45 MJ EET SAVTotal/NA 15.51 g 1 mL Analysis 8270E 1 757815 01/04/23 21:14 T1C EET SAVTotal/NA 1 mL 1 mL CMSGInstrument ID: Eurofins Savannah Page 26 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228273-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: MW-02 (20')Lab Sample ID: 680-228273-2 Matrix: SolidDate Collected: 12/20/22 10:10 Percent Solids: 81.2Date Received: 12/22/22 10:45 Prep 5035 SAB12/28/22 10:00 EET PEN606420 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.342 g 5.0 g Analysis MAVPH 100 606419 12/28/22 18:03 SAB EET PENTotal/NA 5 mL 5 mL CH_TRACYInstrument ID: Prep 3546 606813 12/30/22 14:32 KWS EET PENTotal/NA 15.33 g 2 mL Analysis MA-EPH 1 607115 01/04/23 10:51 RS EET PENTotal/NA EvaInstrument ID: Prep 3546 606813 12/30/22 14:32 KWS EET PENTotal/NA 15.33 g 2 mL Analysis MA-EPH 1 607117 01/04/23 13:58 RS EET PENTotal/NA EvaInstrument ID: Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 27 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Accreditation/Certification Summary Client: TRC Environmental Corporation Job ID: 680-228273-1 Project/Site: Greensboro, NC-463648.0.0 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 269 12-31-23 Laboratory: Eurofins Pensacola The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 Eurofins Savannah Page 28 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Method Summary Job ID: 680-228273-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method Method Description LaboratoryProtocol SW8468260DVolatile Organic Compounds by GC/MS EET SAV SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN EPAMoisturePercent Moisture EET SAV SW8463546Microwave Extraction EET PEN SW8463546Microwave Extraction EET SAV SW8465035Closed System Purge and Trap EET PEN SW8465035Closed System Purge and Trap EET SAV Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 29 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 Page 30 of 32 1/13/2023 1234567 8 9 10 11 12 Page 31 of 32 1/13/2023 1234567 8 9 10 11 12 Login Sample Receipt Checklist Client: TRC Environmental Corporation Job Number: 680-228273-1 Login Number: 228273 Question Answer Comment Creator: Sims, Robert D List Source: Eurofins Savannah List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Savannah Page 32 of 32 1/13/2023 1 2 3 4 5 6 7 8 9 10 11 12 ANALYTICAL REPORT PREPARED FOR Attn: David Szynal TRC Environmental Corporation 50 International Drive Suite 150 Greenville, South Carolina 29615 Generated 1/19/2023 2:03:50 PM JOB DESCRIPTION Greensboro, NC-463648.0.0 JOB NUMBER 680-228821-1 See page two for job notes and contact information. Savannah GA 31404 5102 LaRoche Avenue Eurofins Savannah Page 1 of 28 1 2 3 4 5 6 7 8 9 10 11 12 Eurofins Savannah Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 1/19/2023 2:03:50 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Definitions/Glossary Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Qualifiers GC/MS Semi VOA TICs Qualifier Description J Indicates an Estimated Value for TICs Qualifier N Presumptive evidence of material. T Result is a tentatively identified compound (TIC) and an estimated value. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 3 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Sample Summary Client: TRC Environmental Corporation Job ID: 680-228821-1 Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID Client Sample ID Matrix Collected Received 680-228821-1 MW-1 Water 01/06/23 10:35 01/07/23 10:30 680-228821-2 MW-2 Water 01/06/23 11:50 01/07/23 10:30 680-228821-3 Trip Blank Water 01/06/23 00:00 01/07/23 10:30 Eurofins SavannahPage 4 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Case Narrative Client: TRC Environmental Corporation Job ID: 680-228821-1 Project/Site: Greensboro, NC-463648.0.0 Job ID: 680-228821-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-228821-1 Receipt The samples were received on 1/7/2023 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 9.3°C GC/MS VOA Method 624.1_PREC: One container for the following sample was received empty: MW-1 (680-228821-1). The lab used the other vials received for the analysis. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 625.1_PREC: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-758503 and 680-758780 and analytical batch 680-758900 were outside control limits for one or more analytes, see QC Sample Results for detail. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-2 (680-228821-2). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins SavannahPage 5 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 01/06/23 10:35 Date Received: 01/07/23 10:30 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL ND 1.00 ug/L 01/10/23 19:52 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.00 ug/L 01/10/23 19:52 1ND1,2-Dichlorobenzene 1.00 ug/L 01/10/23 19:52 1ND1,3-Dichlorobenzene 1.00 ug/L 01/10/23 19:52 1ND1,4-Dichlorobenzene 1.00 ug/L 01/10/23 19:52 1NDEthylbenzene 1.00 ug/L 01/10/23 19:52 1NDm-Xylene & p-Xylene 1.00 ug/L 01/10/23 19:52 1NDo-Xylene 1.00 ug/L 01/10/23 19:52 1NDToluene 2.00 ug/L 01/10/23 19:52 1NDXylenes, Total 4-Bromofluorobenzene (Surr)105 60-140 01/10/23 19:52 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)94 01/10/23 19:52 160-140 1,2-Dichloroethane-d4 (Surr)83 01/10/23 19:52 160-140 Toluene-d8 (Surr)112 01/10/23 19:52 160-140 Method: 40CFR136A 625.1 - Semivolatile Organic Compounds (GC/MS) RL MDL ND 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDAcenaphthylene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDAnthracene 81.3 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzidine 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzo[a]anthracene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzo[a]pyrene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzo[b]fluoranthene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzo[g,h,i]perylene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBenzo[k]fluoranthene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBis(2-chloroethoxy)methane 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBis(2-chloroethyl)ether 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDbis (2-chloroisopropyl) ether 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDBis(2-ethylhexyl) phthalate 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND4-Bromophenyl phenyl ether 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDButyl benzyl phthalate 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND4-Chloro-3-methylphenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2-Chloronaphthalene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2-Chlorophenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND4-Chlorophenyl phenyl ether 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDChrysene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDDibenz(a,h)anthracene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND1,2-Dichlorobenzene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND1,3-Dichlorobenzene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND1,4-Dichlorobenzene 61.0 ug/L 01/12/23 08:21 01/12/23 21:05 1ND3,3'-Dichlorobenzidine 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2,4-Dichlorophenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDDiethyl phthalate 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2,4-Dimethylphenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDDimethyl phthalate 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDDi-n-butyl phthalate 50.8 ug/L 01/12/23 08:21 01/12/23 21:05 1ND4,6-Dinitro-2-methylphenol 50.8 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2,4-Dinitrophenol Eurofins Savannah Page 6 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 01/06/23 10:35 Date Received: 01/07/23 10:30 Method: 40CFR136A 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL ND 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2,4-Dinitrotoluene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2,6-Dinitrotoluene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDDi-n-octyl phthalate 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND1,2-Diphenylhydrazine 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDFluoranthene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDFluorene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDHexachlorobenzene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDHexachlorobutadiene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDHexachlorocyclopentadiene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDHexachloroethane 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDIndeno[1,2,3-cd]pyrene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDIsophorone 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDNaphthalene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDNitrobenzene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2-Nitrophenol 50.8 ug/L 01/12/23 08:21 01/12/23 21:05 1ND4-Nitrophenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDN-Nitrosodimethylamine 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDN-Nitrosodi-n-propylamine 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDN-Nitrosodiphenylamine 50.8 ug/L 01/12/23 08:21 01/12/23 21:05 1NDPentachlorophenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDPhenanthrene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDPhenol 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1NDPyrene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND1,2,4-Trichlorobenzene 10.2 ug/L 01/12/23 08:21 01/12/23 21:05 1ND2,4,6-Trichlorophenol Unknown 73.7 T J ug/L 3.11 01/12/23 08:21 01/12/23 21:05 1 Tentatively Identified Compound Dil FacAnalyzedPreparedUnitDQualifierEst. Result CAS No.RT 101/12/23 21:0501/12/23 08:21T J Nn-Hexadecanoic acid 57-10-39.25 ug/L 9.53 101/12/23 21:0501/12/23 08:21T J NHeptadecane 629-78-78.30 ug/L 12.31 101/12/23 21:0501/12/23 08:21T J NHeptacosane 593-49-78.26 ug/L 12.69 2-Fluorobiphenyl (Surr)48 25-130 01/12/23 08:21 01/12/23 21:05 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)21 01/12/23 08:21 01/12/23 21:05 110-130 Nitrobenzene-d5 (Surr)46 01/12/23 08:21 01/12/23 21:05 115-314 Phenol-d5 (Surr)15 01/12/23 08:21 01/12/23 21:05 18-424 Terphenyl-d14 (Surr)76 01/12/23 08:21 01/12/23 21:05 135-131 2,4,6-Tribromophenol (Surr)67 01/12/23 08:21 01/12/23 21:05 130-130 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL ND 26.0 ug/L 01/13/23 13:40 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 11.0 ug/L 01/13/23 13:40 1NDC9-C12 Aliphatics 7.00 ug/L 01/13/23 13:40 1NDC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)87 70-130 01/13/23 13:40 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)88 01/13/23 13:40 170-130 Eurofins Savannah Page 7 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-1Client Sample ID: MW-1 Matrix: WaterDate Collected: 01/06/23 10:35 Date Received: 01/07/23 10:30 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL ND 0.147 mg/L 01/13/23 21:54 01/18/23 21:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 0.147 mg/L 01/13/23 21:54 01/18/23 21:14 1NDC19-C36 Aliphatics 0.303 mg/L 01/13/23 21:54 01/19/23 00:19 1NDC11-C22 Aromatics 1-Chlorooctadecane 93 40-140 01/13/23 21:54 01/18/23 21:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl (Surr)67 01/13/23 21:54 01/19/23 00:19 140-140 2-Fluorobiphenyl (Surr)66 01/13/23 21:54 01/19/23 00:19 140-140 2-Bromonaphthalene 61 01/13/23 21:54 01/19/23 00:19 140-140 Eurofins Savannah Page 8 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 01/06/23 11:50 Date Received: 01/07/23 10:30 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 96.4 1.00 ug/L 01/10/23 20:11 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.00 ug/L 01/10/23 20:11 1ND1,2-Dichlorobenzene 1.00 ug/L 01/10/23 20:11 1ND1,3-Dichlorobenzene 1.00 ug/L 01/10/23 20:11 1ND1,4-Dichlorobenzene 1.00 ug/L 01/10/23 20:11 13.13Ethylbenzene 1.00 ug/L 01/10/23 20:11 1140m-Xylene & p-Xylene 1.00 ug/L 01/10/23 20:11 1125o-Xylene 1.00 ug/L 01/10/23 20:11 14.65Toluene 2.00 ug/L 01/10/23 20:11 1265Xylenes, Total 4-Bromofluorobenzene (Surr)105 60-140 01/10/23 20:11 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)93 01/10/23 20:11 160-140 1,2-Dichloroethane-d4 (Surr)81 01/10/23 20:11 160-140 Toluene-d8 (Surr)109 01/10/23 20:11 160-140 Method: 40CFR136A 625.1 - Semivolatile Organic Compounds (GC/MS) RL MDL ND 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDAcenaphthylene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDAnthracene 84.2 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzidine 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzo[a]anthracene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzo[a]pyrene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzo[b]fluoranthene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzo[g,h,i]perylene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBenzo[k]fluoranthene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBis(2-chloroethoxy)methane 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBis(2-chloroethyl)ether 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDbis (2-chloroisopropyl) ether 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDBis(2-ethylhexyl) phthalate 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND4-Bromophenyl phenyl ether 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDButyl benzyl phthalate 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND4-Chloro-3-methylphenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2-Chloronaphthalene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2-Chlorophenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND4-Chlorophenyl phenyl ether 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDChrysene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDDibenz(a,h)anthracene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND1,2-Dichlorobenzene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND1,3-Dichlorobenzene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND1,4-Dichlorobenzene 63.1 ug/L 01/12/23 08:21 01/12/23 21:30 1ND3,3'-Dichlorobenzidine 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2,4-Dichlorophenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDDiethyl phthalate 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2,4-Dimethylphenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDDimethyl phthalate 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDDi-n-butyl phthalate 52.6 ug/L 01/12/23 08:21 01/12/23 21:30 1ND4,6-Dinitro-2-methylphenol 52.6 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2,4-Dinitrophenol Eurofins Savannah Page 9 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 01/06/23 11:50 Date Received: 01/07/23 10:30 Method: 40CFR136A 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL ND 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2,4-Dinitrotoluene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2,6-Dinitrotoluene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDDi-n-octyl phthalate 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND1,2-Diphenylhydrazine 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDFluoranthene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDFluorene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDHexachlorobenzene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDHexachlorobutadiene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDHexachlorocyclopentadiene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDHexachloroethane 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDIndeno[1,2,3-cd]pyrene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDIsophorone 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDNaphthalene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDNitrobenzene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2-Nitrophenol 52.6 ug/L 01/12/23 08:21 01/12/23 21:30 1ND4-Nitrophenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDN-Nitrosodimethylamine 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDN-Nitrosodi-n-propylamine 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDN-Nitrosodiphenylamine 52.6 ug/L 01/12/23 08:21 01/12/23 21:30 1NDPentachlorophenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDPhenanthrene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDPhenol 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1NDPyrene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND1,2,4-Trichlorobenzene 10.5 ug/L 01/12/23 08:21 01/12/23 21:30 1ND2,4,6-Trichlorophenol 1H-Inden-1-one, 2,3-dihydro-200 T J N ug/L 6.24 83-33-0 01/12/23 08:21 01/12/23 21:30 1 Tentatively Identified Compound Dil FacAnalyzedPreparedUnitDQualifierEst. Result CAS No.RT 101/12/23 21:3001/12/23 08:21T J NBenzeneacetic acid, .alpha.-methyl-492-37-5106ug/L 6.48 101/12/23 21:3001/12/23 08:21T J N1(2H)-Naphthalenone, 3,4-dihydro-529-34-0235ug/L 6.74 101/12/23 21:3001/12/23 08:21T J N7-Methylindan-1-one 39627-61-7167ug/L 6.90 101/12/23 21:3001/12/23 08:21T JUnknown83.2 ug/L 6.98 101/12/23 21:3001/12/23 08:21T JUnknown90.3 ug/L 7.12 101/12/23 21:3001/12/23 08:21T JUnknown83.0 ug/L 7.39 101/12/23 21:3001/12/23 08:21T J N1(2H)-Naphthalenone, 3,4-dihydro-5-methyl- 6939-35-171.2 ug/L 7.48 101/12/23 21:3001/12/23 08:21T J NBenzenamine, N,N-dimethyl-4-nitro-100-23-2113ug/L 8.59 101/12/23 21:3001/12/23 08:21T JUnknown85.3 ug/L 8.97 2-Fluorobiphenyl (Surr)53 25-130 01/12/23 08:21 01/12/23 21:30 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)27 01/12/23 08:21 01/12/23 21:30 110-130 Nitrobenzene-d5 (Surr)54 01/12/23 08:21 01/12/23 21:30 115-314 Phenol-d5 (Surr)20 01/12/23 08:21 01/12/23 21:30 18-424 Terphenyl-d14 (Surr)70 01/12/23 08:21 01/12/23 21:30 135-131 2,4,6-Tribromophenol (Surr)89 01/12/23 08:21 01/12/23 21:30 130-130 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 158 130 ug/L 01/13/23 14:45 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics Eurofins Savannah Page 10 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-2Client Sample ID: MW-2 Matrix: WaterDate Collected: 01/06/23 11:50 Date Received: 01/07/23 10:30 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL 362 55.0 ug/L 01/13/23 14:45 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C12 Aliphatics 35.0 ug/L 01/13/23 14:45 5538C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)88 70-130 01/13/23 14:45 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)88 01/13/23 14:45 570-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL ND 0.144 mg/L 01/13/23 21:54 01/18/23 21:31 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 0.144 mg/L 01/13/23 21:54 01/18/23 21:31 1NDC19-C36 Aliphatics 0.296 mg/L 01/13/23 21:54 01/19/23 00:36 10.563C11-C22 Aromatics 1-Chlorooctadecane 94 40-140 01/13/23 21:54 01/18/23 21:31 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl (Surr)63 01/13/23 21:54 01/19/23 00:36 140-140 2-Fluorobiphenyl (Surr)54 01/13/23 21:54 01/19/23 00:36 140-140 2-Bromonaphthalene 53 01/13/23 21:54 01/19/23 00:36 140-140 Eurofins Savannah Page 11 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228821-3Client Sample ID: Trip Blank Matrix: WaterDate Collected: 01/06/23 00:00 Date Received: 01/07/23 10:30 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL ND 1.00 ug/L 01/10/23 13:34 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.00 ug/L 01/10/23 13:34 1ND1,2-Dichlorobenzene 1.00 ug/L 01/10/23 13:34 1ND1,3-Dichlorobenzene 1.00 ug/L 01/10/23 13:34 1ND1,4-Dichlorobenzene 1.00 ug/L 01/10/23 13:34 1NDEthylbenzene 1.00 ug/L 01/10/23 13:34 1NDm-Xylene & p-Xylene 1.00 ug/L 01/10/23 13:34 1NDo-Xylene 1.00 ug/L 01/10/23 13:34 1NDToluene 2.00 ug/L 01/10/23 13:34 1NDXylenes, Total 4-Bromofluorobenzene (Surr)108 60-140 01/10/23 13:34 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)92 01/10/23 13:34 160-140 1,2-Dichloroethane-d4 (Surr)82 01/10/23 13:34 160-140 Toluene-d8 (Surr)109 01/10/23 13:34 160-140 Eurofins Savannah Page 12 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 624.1 - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 680-758485/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 758485 RL MDL Benzene ND 1.00 ug/L 01/10/23 12:31 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 1.00 ug/L 01/10/23 12:31 11,2-Dichlorobenzene ND 1.00 ug/L 01/10/23 12:31 11,3-Dichlorobenzene ND 1.00 ug/L 01/10/23 12:31 11,4-Dichlorobenzene ND 1.00 ug/L 01/10/23 12:31 1Ethylbenzene ND 1.00 ug/L 01/10/23 12:31 1m-Xylene & p-Xylene ND 1.00 ug/L 01/10/23 12:31 1o-Xylene ND 1.00 ug/L 01/10/23 12:31 1Toluene ND 2.00 ug/L 01/10/23 12:31 1Xylenes, Total 4-Bromofluorobenzene (Surr)106 60-140 01/10/23 12:31 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 95 01/10/23 12:31 1Dibromofluoromethane (Surr)60-140 84 01/10/23 12:31 11,2-Dichloroethane-d4 (Surr)60-140 110 01/10/23 12:31 1Toluene-d8 (Surr)60-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-758485/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 758485 Benzene 50.0 50.10 ug/L 100 65 -135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2-Dichlorobenzene 50.0 49.80 ug/L 100 65 -135 1,3-Dichlorobenzene 50.0 50.25 ug/L 100 70 -130 1,4-Dichlorobenzene 50.0 49.49 ug/L 99 65 -135 Ethylbenzene 50.0 49.59 ug/L 99 60 -140 Toluene 50.0 53.25 ug/L 106 70 -130 Xylenes, Total 100 103.8 ug/L 104 82 -121 4-Bromofluorobenzene (Surr)60 -140 Surrogate 101 LCS LCS Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)60 -140 921,2-Dichloroethane-d4 (Surr)60 -140 109Toluene-d8 (Surr)60 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-758485/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 758485 Benzene 50.0 49.62 ug/L 99 65 -135 1 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 1,2-Dichlorobenzene 50.0 49.29 ug/L 99 65 -135 1 57 1,3-Dichlorobenzene 50.0 50.32 ug/L 101 70 -130 0 43 1,4-Dichlorobenzene 50.0 49.34 ug/L 99 65 -135 0 57 Ethylbenzene 50.0 49.77 ug/L 100 60 -140 0 63 Toluene 50.0 53.74 ug/L 107 70 -130 1 41 Xylenes, Total 100 103.2 ug/L 103 82 -121 1 30 Eurofins Savannah Page 13 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-758485/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 758485 4-Bromofluorobenzene (Surr)60 -140 Surrogate 101 LCSD LCSD Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)60 -140 901,2-Dichloroethane-d4 (Surr)60 -140 109Toluene-d8 (Surr)60 -140 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 680-758780/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 758900 Prep Batch: 758780 RL MDL Acenaphthene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Acenaphthylene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Anthracene ND 80.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzidine ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzo[a]anthracene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzo[a]pyrene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzo[b]fluoranthene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzo[g,h,i]perylene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Benzo[k]fluoranthene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Bis(2-chloroethoxy)methane ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Bis(2-chloroethyl)ether ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1bis (2-chloroisopropyl) ether ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Bis(2-ethylhexyl) phthalate ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 14-Bromophenyl phenyl ether ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Butyl benzyl phthalate ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 14-Chloro-3-methylphenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12-Chloronaphthalene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12-Chlorophenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 14-Chlorophenyl phenyl ether ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Chrysene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Dibenz(a,h)anthracene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 11,2-Dichlorobenzene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 11,3-Dichlorobenzene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 11,4-Dichlorobenzene ND 60.0 ug/L 01/12/23 08:21 01/12/23 17:43 13,3'-Dichlorobenzidine ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,4-Dichlorophenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Diethyl phthalate ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,4-Dimethylphenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Dimethyl phthalate ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Di-n-butyl phthalate ND 50.0 ug/L 01/12/23 08:21 01/12/23 17:43 14,6-Dinitro-2-methylphenol ND 50.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,4-Dinitrophenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,4-Dinitrotoluene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,6-Dinitrotoluene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Di-n-octyl phthalate ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 11,2-Diphenylhydrazine ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Fluoranthene Eurofins Savannah Page 14 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-758780/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 758900 Prep Batch: 758780 RL MDL Fluorene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Hexachlorobenzene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Hexachlorobutadiene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Hexachlorocyclopentadiene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Hexachloroethane ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Indeno[1,2,3-cd]pyrene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Isophorone ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Naphthalene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Nitrobenzene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12-Nitrophenol ND 50.0 ug/L 01/12/23 08:21 01/12/23 17:43 14-Nitrophenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1N-Nitrosodimethylamine ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1N-Nitrosodi-n-propylamine ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1N-Nitrosodiphenylamine ND 50.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Pentachlorophenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Phenanthrene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Phenol ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 1Pyrene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 11,2,4-Trichlorobenzene ND 10.0 ug/L 01/12/23 08:21 01/12/23 17:43 12,4,6-Trichlorophenol 4,4'-DDD NC ug/L 72-54-8 01/12/23 08:21 01/12/23 17:43 1 MB MB Tentatively Identified Compound Dil FacPreparedAnalyzedDUnitQualifierEst. Result RT CAS No. 01/12/23 08:21 01/12/23 17:43 1NCug/L 72-55-94,4'-DDE 01/12/23 08:21 01/12/23 17:43 1NCug/L 50-29-34,4'-DDT 01/12/23 08:21 01/12/23 17:43 1NCug/L 92-87-5Benzidine_T 01/12/23 08:21 01/12/23 17:43 1NCug/L 87-86-5Pentachlorophenol_T 01/12/23 08:21 01/12/23 17:43 1Noneug/LTentatively Identified Compound 2-Fluorobiphenyl (Surr)67 25-130 01/12/23 17:43 1 MB MB Surrogate 01/12/23 08:21 Dil FacPreparedAnalyzedQualifierLimits%Recovery 30 01/12/23 08:21 01/12/23 17:43 12-Fluorophenol (Surr)10-130 61 01/12/23 08:21 01/12/23 17:43 1Nitrobenzene-d5 (Surr)15-314 20 01/12/23 08:21 01/12/23 17:43 1Phenol-d5 (Surr)8-424 78 01/12/23 08:21 01/12/23 17:43 1Terphenyl-d14 (Surr)35-131 89 01/12/23 08:21 01/12/23 17:43 12,4,6-Tribromophenol (Surr)30-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-758780/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 758900 Prep Batch: 758780 Acenaphthene 200 154.1 ug/L 77 47 -145 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 200 159.2 ug/L 80 33 -145 Anthracene 200 166.7 ug/L 83 27 -133 Benzidine 200 136.8 ug/L 68 1-122 Benzo[a]anthracene 200 176.4 ug/L 88 33 -143 Benzo[a]pyrene 200 179.6 ug/L 90 17 -163 Eurofins Savannah Page 15 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-758780/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 758900 Prep Batch: 758780 Benzo[b]fluoranthene 200 174.2 ug/L 87 24 -159 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Benzo[g,h,i]perylene 200 183.8 ug/L 92 1-219 Benzo[k]fluoranthene 200 169.9 ug/L 85 11 -162 Bis(2-chloroethoxy)methane 200 149.7 ug/L 75 33 -184 Bis(2-chloroethyl)ether 200 147.1 ug/L 74 12 -158 bis (2-chloroisopropyl) ether 200 156.6 ug/L 78 30 -104 Bis(2-ethylhexyl) phthalate 200 182.4 ug/L 91 8-158 4-Bromophenyl phenyl ether 200 172.1 ug/L 86 53 -127 Butyl benzyl phthalate 200 191.8 ug/L 96 1-152 4-Chloro-3-methylphenol 200 157.6 ug/L 79 22 -147 2-Chloronaphthalene 200 141.0 ug/L 71 60 -120 2-Chlorophenol 200 122.8 ug/L 61 23 -134 4-Chlorophenyl phenyl ether 200 161.4 ug/L 81 25 -158 Chrysene 200 169.7 ug/L 85 17 -168 Dibenz(a,h)anthracene 200 173.3 ug/L 87 1-227 1,2-Dichlorobenzene 200 120.5 ug/L 60 13 -130 1,3-Dichlorobenzene 200 113.9 ug/L 57 12 -130 1,4-Dichlorobenzene 200 115.4 ug/L 58 13 -130 3,3'-Dichlorobenzidine 200 222.5 ug/L 111 1-262 2,4-Dichlorophenol 200 152.1 ug/L 76 39 -135 Diethyl phthalate 200 165.7 ug/L 83 1-120 2,4-Dimethylphenol 200 139.6 ug/L 70 32 -120 Dimethyl phthalate 200 161.8 ug/L 81 1-120 Di-n-butyl phthalate 200 180.4 ug/L 90 1-120 4,6-Dinitro-2-methylphenol 400 425.7 ug/L 106 1-181 2,4-Dinitrophenol 400 398.9 ug/L 100 1-191 2,4-Dinitrotoluene 200 181.9 ug/L 91 39 -139 2,6-Dinitrotoluene 200 165.0 ug/L 83 50 -158 Di-n-octyl phthalate 200 195.9 ug/L 98 4-146 1,2-Diphenylhydrazine 200 162.0 ug/L 81 38 -130 Fluoranthene 200 181.2 ug/L 91 26 -137 Fluorene 200 158.5 ug/L 79 59 -121 Hexachlorobenzene 200 168.1 ug/L 84 1-152 Hexachlorobutadiene 200 129.1 ug/L 65 24 -120 Hexachlorocyclopentadiene 200 146.1 ug/L 73 15 -130 Hexachloroethane 200 106.0 ug/L 53 40 -120 Indeno[1,2,3-cd]pyrene 200 188.3 ug/L 94 1-171 Isophorone 200 157.7 ug/L 79 21 -196 Naphthalene 200 136.8 ug/L 68 21 -133 Nitrobenzene 200 147.4 ug/L 74 35 -180 2-Nitrophenol 200 157.1 ug/L 79 29 -182 4-Nitrophenol 400 146.3 ug/L 37 1-132 N-Nitrosodimethylamine 200 100.9 ug/L 50 15 -130 N-Nitrosodi-n-propylamine 200 150.8 ug/L 75 1-230 N-Nitrosodiphenylamine 200 158.6 ug/L 79 35 -130 Pentachlorophenol 400 409.9 ug/L 102 14 -176 Phenanthrene 200 166.3 ug/L 83 54 -120 Phenol 200 57.76 ug/L 29 5-120 Pyrene 200 179.4 ug/L 90 52 -120 Eurofins Savannah Page 16 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-758780/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 758900 Prep Batch: 758780 1,2,4-Trichlorobenzene 200 132.4 ug/L 66 44 -142 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 2,4,6-Trichlorophenol 200 167.3 ug/L 84 37 -144 2-Fluorobiphenyl (Surr)25 -130 Surrogate 68 LCS LCS Qualifier Limits%Recovery 362-Fluorophenol (Surr)10 -130 70Nitrobenzene-d5 (Surr)15 -314 25Phenol-d5 (Surr)8 -424 88Terphenyl-d14 (Surr)35 -131 952,4,6-Tribromophenol (Surr)30 -130 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-608344/2 Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 RL MDL C5-C8 Aliphatics ND 26.0 ug/L 01/13/23 12:36 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 11.0 ug/L 01/13/23 12:36 1C9-C12 Aliphatics ND 7.00 ug/L 01/13/23 12:36 1C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)87 70-130 01/13/23 12:36 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 88 01/13/23 12:36 1a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-608344/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 C5-C8 Aliphatics 300 240.0 ug/L 80 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 350 297.7 ug/L 85 70 -130 C9-C10 Aromatics 50.0 41.55 ug/L 83 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 87 LCS LCS Qualifier Limits%Recovery 86a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-608344/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 C5-C8 Aliphatics 300 252.9 ug/L 84 70 -130 5 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 350 309.2 ug/L 88 70 -130 4 25 C9-C10 Aromatics 50.0 43.50 ug/L 87 70 -130 5 25 Eurofins Savannah Page 17 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-608344/6 Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 87 LCSD LCSD Qualifier Limits%Recovery 87a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: MW-1Lab Sample ID: 680-228821-1 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 C5-C8 Aliphatics ND 300 256.3 ug/L 85 70 -130 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C9-C12 Aliphatics ND 350 300.8 ug/L 86 70 -130 C9-C10 Aromatics ND 50.0 53.43 ug/L 107 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 87 MS MS Qualifier Limits%Recovery 86a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: MW-1Lab Sample ID: 680-228821-1 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 608344 C5-C8 Aliphatics ND 300 260.6 ug/L 87 70 -130 2 25 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C9-C12 Aliphatics ND 350 296.1 ug/L 85 70 -130 2 25 C9-C10 Aromatics ND 50.0 45.71 ug/L 91 70 -130 16 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 86 MSD MSD Qualifier Limits%Recovery 86a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-608463/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 608980 Prep Batch: 608463 RL MDL C9-C18 Aliphatics ND 0.150 mg/L 01/13/23 21:54 01/18/23 20:23 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.150 mg/L 01/13/23 21:54 01/18/23 20:23 1C19-C36 Aliphatics 1-Chlorooctadecane 90 40-140 01/18/23 20:23 1 MB MB Surrogate 01/13/23 21:54 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-608463/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 609004 Prep Batch: 608463 RL MDL C11-C22 Aromatics ND 0.309 mg/L 01/13/23 21:54 01/18/23 23:12 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Eurofins Savannah Page 18 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) o-Terphenyl (Surr)67 40-140 01/18/23 23:12 1 MB MB Surrogate 01/13/23 21:54 Dil FacPreparedAnalyzedQualifierLimits%Recovery 68 01/13/23 21:54 01/18/23 23:12 12-Fluorobiphenyl (Surr)40-140 64 01/13/23 21:54 01/18/23 23:12 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-608463/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 608980 Prep Batch: 608463 C9-C18 Aliphatics 1.36 1.366 mg/L 100 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 1.82 2.036 mg/L 112 40 -140 1-Chlorooctadecane 40 -140 Surrogate 107 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-608463/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 609004 Prep Batch: 608463 C11-C22 Aromatics 3.86 3.893 mg/L 101 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl (Surr)40 -140 Surrogate 83 LCS LCS Qualifier Limits%Recovery 752-Fluorobiphenyl (Surr)40 -140 552-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-608463/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 608980 Prep Batch: 608463 C9-C18 Aliphatics 1.36 1.499 mg/L 110 40 -140 9 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 1.82 1.973 mg/L 109 40 -140 3 50 1-Chlorooctadecane 40 -140 Surrogate 95 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-608463/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 609004 Prep Batch: 608463 C11-C22 Aromatics 3.86 4.105 mg/L 106 40 -140 5 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl (Surr)40 -140 Surrogate 88 LCSD LCSD Qualifier Limits%Recovery 772-Fluorobiphenyl (Surr)40 -140 582-Bromonaphthalene 40 -140 Eurofins Savannah Page 19 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC/MS VOA Analysis Batch: 758485 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1680-228821-1 MW-1 Total/NA Water 624.1680-228821-2 MW-2 Total/NA Water 624.1680-228821-3 Trip Blank Total/NA Water 624.1MB 680-758485/8 Method Blank Total/NA Water 624.1LCS 680-758485/5 Lab Control Sample Total/NA Water 624.1LCSD 680-758485/6 Lab Control Sample Dup Total/NA GC/MS Semi VOA Prep Batch: 758780 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water CWA_Prep680-228821-1 MW-1 Total/NA Water CWA_Prep680-228821-2 MW-2 Total/NA Water CWA_PrepMB 680-758780/1-A Method Blank Total/NA Water CWA_PrepLCS 680-758780/2-A Lab Control Sample Total/NA Analysis Batch: 758900 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625.1 758780680-228821-1 MW-1 Total/NA Water 625.1 758780680-228821-2 MW-2 Total/NA Water 625.1 758780MB 680-758780/1-A Method Blank Total/NA Water 625.1 758780LCS 680-758780/2-A Lab Control Sample Total/NA GC VOA Analysis Batch: 608344 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MAVPH680-228821-1 MW-1 Total/NA Water MAVPH680-228821-2 MW-2 Total/NA Water MAVPHMB 400-608344/2 Method Blank Total/NA Water MAVPHLCS 400-608344/5 Lab Control Sample Total/NA Water MAVPHLCSD 400-608344/6 Lab Control Sample Dup Total/NA Water MAVPH680-228821-1 MS MW-1 Total/NA Water MAVPH680-228821-1 MSD MW-1 Total/NA GC Semi VOA Prep Batch: 608463 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3511680-228821-1 MW-1 Total/NA Water 3511680-228821-2 MW-2 Total/NA Water 3511MB 400-608463/1-A Method Blank Total/NA Water 3511LCS 400-608463/2-A Lab Control Sample Total/NA Water 3511LCSD 400-608463/3-A Lab Control Sample Dup Total/NA Analysis Batch: 608980 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 608463680-228821-1 MW-1 Total/NA Water MA-EPH 608463680-228821-2 MW-2 Total/NA Water MA-EPH 608463MB 400-608463/1-A Method Blank Total/NA Water MA-EPH 608463LCS 400-608463/2-A Lab Control Sample Total/NA Water MA-EPH 608463LCSD 400-608463/3-A Lab Control Sample Dup Total/NA Eurofins Savannah Page 20 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC Semi VOA Analysis Batch: 609004 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 608463680-228821-1 MW-1 Total/NA Water MA-EPH 608463680-228821-2 MW-2 Total/NA Water MA-EPH 608463MB 400-608463/1-A Method Blank Total/NA Water MA-EPH 608463LCS 400-608463/2-A Lab Control Sample Total/NA Water MA-EPH 608463LCSD 400-608463/3-A Lab Control Sample Dup Total/NA Eurofins Savannah Page 21 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228821-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: MW-1 Lab Sample ID: 680-228821-1 Matrix: WaterDate Collected: 01/06/23 10:35 Date Received: 01/07/23 10:30 Analysis 624.1 Y1S01/10/23 19:521 EET SAV758485 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Instrument ID:CMSC Prep CWA_Prep 758780 01/12/23 08:21 LA EET SAVTotal/NA 492 mL 1 mL Analysis 625.1 1 758900 01/12/23 21:05 T1C EET SAVTotal/NA 1 mL 1 mL CMSGInstrument ID: Analysis MAVPH 1 608344 01/13/23 13:40 SAB EET PENTotal/NA 5 mL 5 mL CH_CAROLInstrument ID: Prep 3511 608463 01/13/23 21:54 JTC EET PENTotal/NA 56 mL 2 mL Analysis MA-EPH 1 608980 01/18/23 21:14 JAW EET PENTotal/NA EvaInstrument ID: Prep 3511 608463 01/13/23 21:54 JTC EET PENTotal/NA 56 mL 2 mL Analysis MA-EPH 1 609004 01/19/23 00:19 JAW EET PENTotal/NA EvaInstrument ID: Client Sample ID: MW-2 Lab Sample ID: 680-228821-2 Matrix: WaterDate Collected: 01/06/23 11:50 Date Received: 01/07/23 10:30 Analysis 624.1 Y1S01/10/23 20:111 EET SAV758485 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Instrument ID:CMSC Prep CWA_Prep 758780 01/12/23 08:21 LA EET SAVTotal/NA 475.2 mL 1 mL Analysis 625.1 1 758900 01/12/23 21:30 T1C EET SAVTotal/NA 1 mL 1 mL CMSGInstrument ID: Analysis MAVPH 5 608344 01/13/23 14:45 SAB EET PENTotal/NA 5 mL 5 mL CH_CAROLInstrument ID: Prep 3511 608463 01/13/23 21:54 JTC EET PENTotal/NA 57.4 mL 2 mL Analysis MA-EPH 1 608980 01/18/23 21:31 JAW EET PENTotal/NA EvaInstrument ID: Prep 3511 608463 01/13/23 21:54 JTC EET PENTotal/NA 57.4 mL 2 mL Analysis MA-EPH 1 609004 01/19/23 00:36 JAW EET PENTotal/NA EvaInstrument ID: Client Sample ID: Trip Blank Lab Sample ID: 680-228821-3 Matrix: WaterDate Collected: 01/06/23 00:00 Date Received: 01/07/23 10:30 Analysis 624.1 Y1S01/10/23 13:341 EET SAV758485 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Instrument ID:CMSC Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 22 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Accreditation/Certification Summary Client: TRC Environmental Corporation Job ID: 680-228821-1 Project/Site: Greensboro, NC-463648.0.0 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 269 12-31-23 Laboratory: Eurofins Pensacola The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 Eurofins Savannah Page 23 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Method Summary Job ID: 680-228821-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method Method Description LaboratoryProtocol EPA624.1 Volatile Organic Compounds (GC/MS)EET SAV 40CFR136A625.1 Semivolatile Organic Compounds (GC/MS)EET SAV MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8463511Microextraction of Organic Compounds EET PEN SW8465030BPurge and Trap EET PEN 40CFR136ACWA_Prep Liquid-Liquid Extraction (Separatory Funnel)EET SAV Protocol References: 40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and subsequent revisions. EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 24 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Page 25 of 28 1/19/2023 1234567 8 9 10 11 12 Page 26 of 28 1/19/2023 1234567 8 9 10 11 12 Login Sample Receipt Checklist Client: TRC Environmental Corporation Job Number: 680-228821-1 Login Number: 228821 Question Answer Comment Creator: Givens, Keshia List Source: Eurofins Savannah List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. N/AIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Savannah Page 27 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 Login Sample Receipt Checklist Client: TRC Environmental Corporation Job Number: 680-228821-1 Login Number: 228821 Question Answer Comment Creator: Peckinpaugh, Marshall List Source: Eurofins Pensacola List Creation: 01/12/23 05:27 PMList Number: 2 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.3.9°C IR8 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Savannah Page 28 of 28 1/19/2023 1 2 3 4 5 6 7 8 9 10 11 12 ANALYTICAL REPORT PREPARED FOR Attn: David Szynal TRC Environmental Corporation 50 International Drive Suite 150 Greenville, South Carolina 29615 Generated 1/12/2023 5:09:42 PM JOB DESCRIPTION Greensboro, NC-463648.0.0 JOB NUMBER 680-228269-1 See page two for job notes and contact information. Savannah GA 31404 5102 LaRoche Avenue Eurofins Savannah Page 1 of 29 1 2 3 4 5 6 7 8 9 10 11 12 Eurofins Savannah Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 1/12/2023 5:09:42 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Definitions/Glossary Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Qualifiers GC/MS Semi VOA Qualifier Description D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. Qualifier GC VOA Qualifier Description S1-Surrogate recovery exceeds control limits, low biased. Qualifier GC Semi VOA Qualifier Description D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. Qualifier H Sample was prepped or analyzed beyond the specified holding time S1-Surrogate recovery exceeds control limits, low biased. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 3 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Sample Summary Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID Client Sample ID Matrix Collected Received 680-228269-1 SB-02 (15')Solid 12/19/22 15:05 12/22/22 10:45 680-228269-2 SB-03 (16')Solid 12/19/22 14:20 12/22/22 10:45 680-228269-3 SB-04 (20')Solid 12/19/22 12:00 12/22/22 10:45 680-228269-4 SB-05 (18')Solid 12/20/22 14:30 12/22/22 10:45 680-228269-5 SB-06 (18')Solid 12/20/22 15:05 12/22/22 10:45 680-228269-6 SB-07 (17')Solid 12/20/22 15:40 12/22/22 10:45 680-228269-7 SB-08 (17')Solid 12/20/22 16:15 12/22/22 10:45 680-228269-8 SB-09 (11')Solid 12/21/22 08:45 12/22/22 10:45 680-228269-9 SB-10 (11')Solid 12/21/22 09:05 12/22/22 10:45 Eurofins SavannahPage 4 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Case Narrative Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Job ID: 680-228269-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-228269-1 Receipt The samples were received on 12/22/2022 10:45 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 3.3°C GC/MS Semi VOA Method 8270E_SIM: The following samples were diluted due to the nature of the sample matrix : SB-02 (15') (680-228269-1) and SB-03 (16') (680-228269-2). As such, surrogate recoveries are below the calibration range or are not reported, and elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following sample was diluted due to the nature of the sample matrix : SB-05 (18') (680-228269-4). As such, surrogate recoveries are below the calibration range or are not reported, and elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-02 (15') (680-228269-1). Elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-03 (16') (680-228269-2). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Gasoline Range Organics Method 8015C_GRO: The following MeOH terra core vials contain very little preservative: -6C and -7C.SB-07 (17') (680-228269-6) and SB-08 (17') (680-228269-7) Method 8015C_GRO: Surrogate recovery for the following sample was outside control limits: SB-03 (16') (680-228269-2). Re-analysis was performed and surrogate recovery was outside control limits. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Diesel Range Organics Method 8015C_DRO: The following samples required a dilution due to the nature of the sample matrix: SB-02 (15') (680-228269-1), SB-03 (16') (680-228269-2) and SB-05 (18') (680-228269-4). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information. Method 8015C_DRO: Surrogate recovery for the following sample was outside control limits: SB-04 (20') (680-228269-3). Re-extraction re-analysis was performed outside of holding time with acceptable results. Both sets of results are included in the report. The re-extracted results confirmed the original DRO results. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins SavannahPage 5 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-1Client Sample ID: SB-02 (15') Matrix: SolidDate Collected: 12/19/22 15:05 Percent Solids: 89.6Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 1.27 0.0740 mg/Kg ☼12/29/22 12:30 01/01/23 22:51 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼0.548Acenaphthylene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDAnthracene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDBenzo[a]anthracene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDBenzo[a]pyrene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDBenzo[b]fluoranthene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDBenzo[g,h,i]perylene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDBenzo[k]fluoranthene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼0.0948Chrysene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDDibenz(a,h)anthracene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼0.125Fluoranthene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼1.84Fluorene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼NDIndeno[1,2,3-cd]pyrene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼5.27Naphthalene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼4.56Phenanthrene 0.0740 mg/Kg 12/29/22 12:30 01/01/23 22:51 10☼0.406Pyrene 2-Fluorobiphenyl (Surr)0 D 30-130 12/29/22 12:30 01/01/23 22:51 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 12/29/22 12:30 01/01/23 22:51 1030-130 Terphenyl-d14 (Surr)0 D 12/29/22 12:30 01/01/23 22:51 1030-130 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) - DL RL MDL 15.4 0.740 mg/Kg ☼12/29/22 12:30 01/04/23 14:31 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 0.740 mg/Kg 12/29/22 12:30 01/04/23 14:31 100☼26.62-Methylnaphthalene Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 11.5 mg/Kg ☼12/28/22 09:29 01/02/23 13:45 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 12/28/22 09:29 01/02/23 13:45 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 2060 174 mg/Kg ☼12/28/22 20:15 12/30/22 15:51 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 12/28/22 20:15 12/30/22 15:51 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 6 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-2Client Sample ID: SB-03 (16') Matrix: SolidDate Collected: 12/19/22 14:20 Percent Solids: 89.6Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 4.41 0.0724 mg/Kg ☼12/29/22 12:30 01/01/23 23:14 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDAcenaphthylene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDAnthracene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDBenzo[a]anthracene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDBenzo[a]pyrene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDBenzo[b]fluoranthene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDBenzo[g,h,i]perylene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDBenzo[k]fluoranthene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼0.244Chrysene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDDibenz(a,h)anthracene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼0.330Fluoranthene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼5.36Fluorene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDIndeno[1,2,3-cd]pyrene 0.0724 mg/Kg 12/29/22 12:30 01/01/23 23:14 10☼NDPyrene 2-Fluorobiphenyl (Surr)0 D 30-130 12/29/22 12:30 01/01/23 23:14 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 12/29/22 12:30 01/01/23 23:14 1030-130 Terphenyl-d14 (Surr)0 D 12/29/22 12:30 01/01/23 23:14 1030-130 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) - DL RL MDL 45.6 1.45 mg/Kg ☼12/29/22 12:30 01/05/23 12:47 200 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 1.45 mg/Kg 12/29/22 12:30 01/05/23 12:47 200☼78.22-Methylnaphthalene 1.45 mg/Kg 12/29/22 12:30 01/05/23 12:47 200☼17.4Naphthalene 1.45 mg/Kg 12/29/22 12:30 01/05/23 12:47 200☼12.3Phenanthrene Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 214 108 mg/Kg ☼12/28/22 09:29 01/02/23 18:49 1000 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 40 S1-70-131 12/28/22 09:29 01/02/23 18:49 1000 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 5840 441 mg/Kg ☼12/28/22 20:15 12/30/22 16:06 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 12/28/22 20:15 12/30/22 16:06 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 7 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-3Client Sample ID: SB-04 (20') Matrix: SolidDate Collected: 12/19/22 12:00 Percent Solids: 81.9Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00784 mg/Kg ☼12/29/22 12:30 01/01/23 02:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDAcenaphthylene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDAnthracene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDBenzo[a]anthracene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDBenzo[a]pyrene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDBenzo[b]fluoranthene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDBenzo[g,h,i]perylene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDBenzo[k]fluoranthene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDChrysene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDDibenz(a,h)anthracene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDFluoranthene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDFluorene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDIndeno[1,2,3-cd]pyrene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼ND1-Methylnaphthalene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼ND2-Methylnaphthalene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDNaphthalene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDPhenanthrene 0.00784 mg/Kg 12/29/22 12:30 01/01/23 02:14 1☼NDPyrene 2-Fluorobiphenyl (Surr)75 30-130 12/29/22 12:30 01/01/23 02:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)70 12/29/22 12:30 01/01/23 02:14 130-130 Terphenyl-d14 (Surr)77 12/29/22 12:30 01/01/23 02:14 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 13.8 mg/Kg ☼12/28/22 09:29 01/02/23 14:07 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 12/28/22 09:29 01/02/23 14:07 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 9.63 mg/Kg ☼12/28/22 20:15 12/29/22 23:28 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)3 S1-15-139 12/28/22 20:15 12/29/22 23:28 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) - RE RL MDL ND H 9.67 mg/Kg ☼01/05/23 20:15 01/09/23 20:37 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)52 15-139 01/05/23 20:15 01/09/23 20:37 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 8 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-4Client Sample ID: SB-05 (18') Matrix: SolidDate Collected: 12/20/22 14:30 Percent Solids: 90.8Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0732 mg/Kg ☼12/29/22 12:30 01/01/23 02:36 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDAcenaphthylene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDAnthracene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDBenzo[a]anthracene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDBenzo[a]pyrene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDBenzo[b]fluoranthene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDBenzo[g,h,i]perylene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDBenzo[k]fluoranthene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDChrysene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDDibenz(a,h)anthracene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDFluoranthene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDFluorene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDIndeno[1,2,3-cd]pyrene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼ND1-Methylnaphthalene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼ND2-Methylnaphthalene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDNaphthalene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDPhenanthrene 0.0732 mg/Kg 12/29/22 12:30 01/01/23 02:36 10☼NDPyrene 2-Fluorobiphenyl (Surr)0 D 30-130 12/29/22 12:30 01/01/23 02:36 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 12/29/22 12:30 01/01/23 02:36 1030-130 Terphenyl-d14 (Surr)0 D 12/29/22 12:30 01/01/23 02:36 1030-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 10.1 mg/Kg ☼12/28/22 09:29 01/02/23 14:29 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 12/28/22 09:29 01/02/23 14:29 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 156 43.2 mg/Kg ☼12/28/22 20:15 12/30/22 16:37 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 12/28/22 20:15 12/30/22 16:37 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 9 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-5Client Sample ID: SB-06 (18') Matrix: SolidDate Collected: 12/20/22 15:05 Percent Solids: 88.6Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00716 mg/Kg ☼12/29/22 12:30 01/01/23 02:59 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDAcenaphthylene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDAnthracene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0266Benzo[a]anthracene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0209Benzo[a]pyrene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0380Benzo[b]fluoranthene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0106Benzo[g,h,i]perylene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0115Benzo[k]fluoranthene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0286Chrysene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDDibenz(a,h)anthracene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0288Fluoranthene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDFluorene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0130Indeno[1,2,3-cd]pyrene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼ND1-Methylnaphthalene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼ND2-Methylnaphthalene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDNaphthalene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼NDPhenanthrene 0.00716 mg/Kg 12/29/22 12:30 01/01/23 02:59 1☼0.0241Pyrene 2-Fluorobiphenyl (Surr)82 30-130 12/29/22 12:30 01/01/23 02:59 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)79 12/29/22 12:30 01/01/23 02:59 130-130 Terphenyl-d14 (Surr)103 12/29/22 12:30 01/01/23 02:59 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 9.79 mg/Kg ☼01/02/23 11:19 01/02/23 15:55 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 75 70-131 01/02/23 11:19 01/02/23 15:55 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 8.95 mg/Kg ☼12/28/22 20:15 12/29/22 23:58 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)61 15-139 12/28/22 20:15 12/29/22 23:58 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 10 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-6Client Sample ID: SB-07 (17') Matrix: SolidDate Collected: 12/20/22 15:40 Percent Solids: 87.2Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00754 mg/Kg ☼12/29/22 12:30 01/01/23 03:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDAcenaphthylene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDAnthracene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDBenzo[a]anthracene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼0.0115Benzo[a]pyrene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼0.0202Benzo[b]fluoranthene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDBenzo[g,h,i]perylene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDBenzo[k]fluoranthene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼0.0154Chrysene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDDibenz(a,h)anthracene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼0.0188Fluoranthene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDFluorene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDIndeno[1,2,3-cd]pyrene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼ND1-Methylnaphthalene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼ND2-Methylnaphthalene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDNaphthalene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼NDPhenanthrene 0.00754 mg/Kg 12/29/22 12:30 01/01/23 03:22 1☼0.0158Pyrene 2-Fluorobiphenyl (Surr)69 30-130 12/29/22 12:30 01/01/23 03:22 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)69 12/29/22 12:30 01/01/23 03:22 130-130 Terphenyl-d14 (Surr)87 12/29/22 12:30 01/01/23 03:22 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 14.0 mg/Kg ☼12/28/22 09:29 01/02/23 14:50 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 75 70-131 12/28/22 09:29 01/02/23 14:50 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 8.98 mg/Kg ☼12/28/22 20:15 12/30/22 00:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)55 15-139 12/28/22 20:15 12/30/22 00:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 11 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-7Client Sample ID: SB-08 (17') Matrix: SolidDate Collected: 12/20/22 16:15 Percent Solids: 84.1Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00769 mg/Kg ☼12/29/22 12:30 01/01/23 03:44 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDAcenaphthylene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDAnthracene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDBenzo[a]anthracene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDBenzo[a]pyrene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDBenzo[b]fluoranthene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDBenzo[g,h,i]perylene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDBenzo[k]fluoranthene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDChrysene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDDibenz(a,h)anthracene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDFluoranthene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDFluorene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDIndeno[1,2,3-cd]pyrene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼ND1-Methylnaphthalene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼0.008242-Methylnaphthalene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDNaphthalene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDPhenanthrene 0.00769 mg/Kg 12/29/22 12:30 01/01/23 03:44 1☼NDPyrene 2-Fluorobiphenyl (Surr)70 30-130 12/29/22 12:30 01/01/23 03:44 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)69 12/29/22 12:30 01/01/23 03:44 130-130 Terphenyl-d14 (Surr)95 12/29/22 12:30 01/01/23 03:44 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 16.5 mg/Kg ☼12/28/22 09:29 01/02/23 15:12 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 77 70-131 12/28/22 09:29 01/02/23 15:12 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 9.35 mg/Kg ☼12/28/22 20:15 12/30/22 00:29 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)57 15-139 12/28/22 20:15 12/30/22 00:29 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 12 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-8Client Sample ID: SB-09 (11') Matrix: SolidDate Collected: 12/21/22 08:45 Percent Solids: 86.2Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00758 mg/Kg ☼12/29/22 12:30 01/01/23 04:07 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDAcenaphthylene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDAnthracene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDBenzo[a]anthracene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDBenzo[a]pyrene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDBenzo[b]fluoranthene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDBenzo[g,h,i]perylene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDBenzo[k]fluoranthene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDChrysene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDDibenz(a,h)anthracene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDFluoranthene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDFluorene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDIndeno[1,2,3-cd]pyrene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼ND1-Methylnaphthalene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼ND2-Methylnaphthalene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDNaphthalene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDPhenanthrene 0.00758 mg/Kg 12/29/22 12:30 01/01/23 04:07 1☼NDPyrene 2-Fluorobiphenyl (Surr)70 30-130 12/29/22 12:30 01/01/23 04:07 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)68 12/29/22 12:30 01/01/23 04:07 130-130 Terphenyl-d14 (Surr)91 12/29/22 12:30 01/01/23 04:07 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 10.3 mg/Kg ☼01/02/23 11:19 01/02/23 16:16 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 01/02/23 11:19 01/02/23 16:16 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 9.08 mg/Kg ☼12/28/22 20:15 12/30/22 00:44 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)47 15-139 12/28/22 20:15 12/30/22 00:44 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 13 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Lab Sample ID: 680-228269-9Client Sample ID: SB-10 (11') Matrix: SolidDate Collected: 12/21/22 09:05 Percent Solids: 88.7Date Received: 12/22/22 10:45 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00719 mg/Kg ☼12/29/22 12:30 01/01/23 04:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDAcenaphthylene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDAnthracene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0165Benzo[a]anthracene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0130Benzo[a]pyrene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0223Benzo[b]fluoranthene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDBenzo[g,h,i]perylene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.00748Benzo[k]fluoranthene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0177Chrysene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDDibenz(a,h)anthracene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0207Fluoranthene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDFluorene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDIndeno[1,2,3-cd]pyrene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼ND1-Methylnaphthalene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼ND2-Methylnaphthalene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼NDNaphthalene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.00725Phenanthrene 0.00719 mg/Kg 12/29/22 12:30 01/01/23 04:30 1☼0.0166Pyrene 2-Fluorobiphenyl (Surr)82 30-130 12/29/22 12:30 01/01/23 04:30 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)80 12/29/22 12:30 01/01/23 04:30 130-130 Terphenyl-d14 (Surr)94 12/29/22 12:30 01/01/23 04:30 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 10.9 mg/Kg ☼12/28/22 09:29 01/02/23 15:33 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 12/28/22 09:29 01/02/23 15:33 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 8.75 mg/Kg ☼12/28/22 20:15 12/30/22 01:00 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)45 15-139 12/28/22 20:15 12/30/22 01:00 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 14 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) Client Sample ID: Method BlankLab Sample ID: MB 680-757209/17-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757533 Prep Batch: 757209 RL MDL Acenaphthene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Acenaphthylene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Anthracene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Benzo[a]anthracene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Benzo[a]pyrene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Benzo[b]fluoranthene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Benzo[g,h,i]perylene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Benzo[k]fluoranthene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Chrysene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Dibenz(a,h)anthracene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Fluoranthene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Fluorene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Indeno[1,2,3-cd]pyrene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 11-Methylnaphthalene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 12-Methylnaphthalene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Naphthalene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Phenanthrene ND 0.00657 mg/Kg 12/29/22 12:30 12/31/22 17:09 1Pyrene 2-Fluorobiphenyl (Surr)85 30-130 12/31/22 17:09 1 MB MB Surrogate 12/29/22 12:30 Dil FacPreparedAnalyzedQualifierLimits%Recovery 83 12/29/22 12:30 12/31/22 17:09 1Nitrobenzene-d5 (Surr)30-130 100 12/29/22 12:30 12/31/22 17:09 1Terphenyl-d14 (Surr)30-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757209/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757533 Prep Batch: 757209 Acenaphthene 0.165 0.1376 mg/Kg 84 30 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 0.165 0.1390 mg/Kg 84 30 -130 Anthracene 0.165 0.1487 mg/Kg 90 30 -130 Benzo[a]anthracene 0.165 0.1678 mg/Kg 102 30 -130 Benzo[a]pyrene 0.165 0.1763 mg/Kg 107 30 -130 Benzo[b]fluoranthene 0.165 0.1858 mg/Kg 113 30 -130 Benzo[g,h,i]perylene 0.165 0.1794 mg/Kg 109 30 -130 Benzo[k]fluoranthene 0.165 0.1773 mg/Kg 108 30 -130 Chrysene 0.165 0.1717 mg/Kg 104 30 -130 Dibenz(a,h)anthracene 0.165 0.1853 mg/Kg 113 30 -130 Fluoranthene 0.165 0.1623 mg/Kg 99 30 -130 Fluorene 0.165 0.1439 mg/Kg 87 30 -130 Indeno[1,2,3-cd]pyrene 0.165 0.1859 mg/Kg 113 30 -130 1-Methylnaphthalene 0.165 0.1342 mg/Kg 82 30 -130 2-Methylnaphthalene 0.165 0.1371 mg/Kg 83 30 -130 Naphthalene 0.165 0.1333 mg/Kg 81 30 -130 Phenanthrene 0.165 0.1507 mg/Kg 92 30 -130 Pyrene 0.165 0.1618 mg/Kg 98 30 -130 Eurofins Savannah Page 15 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757209/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757533 Prep Batch: 757209 2-Fluorobiphenyl (Surr)30 -130 Surrogate 83 LCS LCS Qualifier Limits%Recovery 80Nitrobenzene-d5 (Surr)30 -130 105Terphenyl-d14 (Surr)30 -130 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) Client Sample ID: Method BlankLab Sample ID: MB 680-757583/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757583 RL MDL Gasoline Range Organics [C6 - C10]ND 10.0 mg/Kg 01/02/23 13:23 100 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier a,a,a-Trifluorotoluene 79 70-131 01/02/23 13:23 100 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757583/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757583 Gasoline Range Organics [C6 - C10] 50.0 59.49 mg/Kg 119 64 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits a,a,a-Trifluorotoluene 70 -131 Surrogate 110 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-757583/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 757583 Gasoline Range Organics [C6 - C10] 50.0 59.52 mg/Kg 119 64 -133 0 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD a,a,a-Trifluorotoluene 70 -131 Surrogate 109 LCSD LCSD Qualifier Limits%Recovery Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Client Sample ID: Method BlankLab Sample ID: MB 680-757155/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757321 Prep Batch: 757155 RL MDL Diesel Range Organics [C10-C28]ND 7.89 mg/Kg 12/28/22 20:15 12/29/22 18:14 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Eurofins Savannah Page 16 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-757155/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757321 Prep Batch: 757155 o-Terphenyl (Surr)68 15-139 12/29/22 18:14 1 MB MB Surrogate 12/28/22 20:15 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757155/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 757321 Prep Batch: 757155 Diesel Range Organics [C10-C28] 32.5 27.82 mg/Kg 86 26 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl (Surr)15 -139 Surrogate 96 LCS LCS Qualifier Limits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 680-758065/11-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 758421 Prep Batch: 758065 RL MDL Diesel Range Organics [C10-C28]ND 7.88 mg/Kg 01/05/23 20:15 01/09/23 20:06 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl (Surr)79 15-139 01/09/23 20:06 1 MB MB Surrogate 01/05/23 20:15 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-758065/12-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 758421 Prep Batch: 758065 Diesel Range Organics [C10-C28] 32.9 25.40 mg/Kg 77 26 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl (Surr)15 -139 Surrogate 86 LCS LCS Qualifier Limits%Recovery Eurofins Savannah Page 17 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC/MS Semi VOA Prep Batch: 757209 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-228269-1 SB-02 (15')Total/NA Solid 3546680-228269-1 - DL SB-02 (15')Total/NA Solid 3546680-228269-2 - DL SB-03 (16')Total/NA Solid 3546680-228269-2 SB-03 (16')Total/NA Solid 3546680-228269-3 SB-04 (20')Total/NA Solid 3546680-228269-4 SB-05 (18')Total/NA Solid 3546680-228269-5 SB-06 (18')Total/NA Solid 3546680-228269-6 SB-07 (17')Total/NA Solid 3546680-228269-7 SB-08 (17')Total/NA Solid 3546680-228269-8 SB-09 (11')Total/NA Solid 3546680-228269-9 SB-10 (11')Total/NA Solid 3546MB 680-757209/17-A Method Blank Total/NA Solid 3546LCS 680-757209/18-A Lab Control Sample Total/NA Analysis Batch: 757533 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 757209680-228269-3 SB-04 (20')Total/NA Solid 8270E SIM 757209680-228269-4 SB-05 (18')Total/NA Solid 8270E SIM 757209680-228269-5 SB-06 (18')Total/NA Solid 8270E SIM 757209680-228269-6 SB-07 (17')Total/NA Solid 8270E SIM 757209680-228269-7 SB-08 (17')Total/NA Solid 8270E SIM 757209680-228269-8 SB-09 (11')Total/NA Solid 8270E SIM 757209680-228269-9 SB-10 (11')Total/NA Solid 8270E SIM 757209MB 680-757209/17-A Method Blank Total/NA Solid 8270E SIM 757209LCS 680-757209/18-A Lab Control Sample Total/NA Analysis Batch: 757571 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 757209680-228269-1 SB-02 (15')Total/NA Solid 8270E SIM 757209680-228269-2 SB-03 (16')Total/NA Analysis Batch: 757712 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 757209680-228269-1 - DL SB-02 (15')Total/NA Analysis Batch: 757963 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 757209680-228269-2 - DL SB-03 (16')Total/NA GC VOA Prep Batch: 757037 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035A680-228269-1 SB-02 (15')Total/NA Solid 5035A680-228269-2 SB-03 (16')Total/NA Solid 5035A680-228269-3 SB-04 (20')Total/NA Solid 5035A680-228269-4 SB-05 (18')Total/NA Solid 5035A680-228269-6 SB-07 (17')Total/NA Solid 5035A680-228269-7 SB-08 (17')Total/NA Solid 5035A680-228269-9 SB-10 (11')Total/NA Eurofins Savannah Page 18 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC VOA Analysis Batch: 757583 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 757037680-228269-1 SB-02 (15')Total/NA Solid 8015C 757037680-228269-2 SB-03 (16')Total/NA Solid 8015C 757037680-228269-3 SB-04 (20')Total/NA Solid 8015C 757037680-228269-4 SB-05 (18')Total/NA Solid 8015C 757584680-228269-5 SB-06 (18')Total/NA Solid 8015C 757037680-228269-6 SB-07 (17')Total/NA Solid 8015C 757037680-228269-7 SB-08 (17')Total/NA Solid 8015C 757584680-228269-8 SB-09 (11')Total/NA Solid 8015C 757037680-228269-9 SB-10 (11')Total/NA Solid 8015CMB 680-757583/7 Method Blank Total/NA Solid 8015CLCS 680-757583/5 Lab Control Sample Total/NA Solid 8015CLCSD 680-757583/6 Lab Control Sample Dup Total/NA Prep Batch: 757584 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5030B680-228269-5 SB-06 (18')Total/NA Solid 5030B680-228269-8 SB-09 (11')Total/NA GC Semi VOA Prep Batch: 757155 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-228269-1 SB-02 (15')Total/NA Solid 3546680-228269-2 SB-03 (16')Total/NA Solid 3546680-228269-3 SB-04 (20')Total/NA Solid 3546680-228269-4 SB-05 (18')Total/NA Solid 3546680-228269-5 SB-06 (18')Total/NA Solid 3546680-228269-6 SB-07 (17')Total/NA Solid 3546680-228269-7 SB-08 (17')Total/NA Solid 3546680-228269-8 SB-09 (11')Total/NA Solid 3546680-228269-9 SB-10 (11')Total/NA Solid 3546MB 680-757155/19-A Method Blank Total/NA Solid 3546LCS 680-757155/20-A Lab Control Sample Total/NA Analysis Batch: 757321 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 757155680-228269-3 SB-04 (20')Total/NA Solid 8015C 757155680-228269-5 SB-06 (18')Total/NA Solid 8015C 757155680-228269-6 SB-07 (17')Total/NA Solid 8015C 757155680-228269-7 SB-08 (17')Total/NA Solid 8015C 757155680-228269-8 SB-09 (11')Total/NA Solid 8015C 757155680-228269-9 SB-10 (11')Total/NA Solid 8015C 757155MB 680-757155/19-A Method Blank Total/NA Solid 8015C 757155LCS 680-757155/20-A Lab Control Sample Total/NA Analysis Batch: 757446 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 757155680-228269-1 SB-02 (15')Total/NA Solid 8015C 757155680-228269-2 SB-03 (16')Total/NA Solid 8015C 757155680-228269-4 SB-05 (18')Total/NA Eurofins Savannah Page 19 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 GC Semi VOA Prep Batch: 758065 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-228269-3 - RE SB-04 (20')Total/NA Solid 3546MB 680-758065/11-A Method Blank Total/NA Solid 3546LCS 680-758065/12-A Lab Control Sample Total/NA Analysis Batch: 758421 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 758065680-228269-3 - RE SB-04 (20')Total/NA Solid 8015C 758065MB 680-758065/11-A Method Blank Total/NA Solid 8015C 758065LCS 680-758065/12-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 757750 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture680-228269-1 SB-02 (15')Total/NA Solid Moisture680-228269-2 SB-03 (16')Total/NA Solid Moisture680-228269-3 SB-04 (20')Total/NA Solid Moisture680-228269-4 SB-05 (18')Total/NA Solid Moisture680-228269-5 SB-06 (18')Total/NA Solid Moisture680-228269-6 SB-07 (17')Total/NA Solid Moisture680-228269-7 SB-08 (17')Total/NA Solid Moisture680-228269-8 SB-09 (11')Total/NA Solid Moisture680-228269-9 SB-10 (11')Total/NA Eurofins Savannah Page 20 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-02 (15')Lab Sample ID: 680-228269-1 Matrix: SolidDate Collected: 12/19/22 15:05 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-02 (15')Lab Sample ID: 680-228269-1 Matrix: SolidDate Collected: 12/19/22 15:05 Percent Solids: 89.6Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.17 g 1 mL Analysis 8270E SIM 10 757571 01/01/23 22:51 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 3546 DL 757209 12/29/22 12:30 MEW EET SAVTotal/NA 15.17 g 1 mL Analysis 8270E SIM DL 100 757712 01/04/23 14:31 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 5.386 g 5 mL Analysis 8015C 100 757583 01/02/23 13:45 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.80 g 1 mL Analysis 8015C 20 757446 12/30/22 15:51 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-03 (16')Lab Sample ID: 680-228269-2 Matrix: SolidDate Collected: 12/19/22 14:20 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-03 (16')Lab Sample ID: 680-228269-2 Matrix: SolidDate Collected: 12/19/22 14:20 Percent Solids: 89.6Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.50 g 1 mL Analysis 8270E SIM 10 757571 01/01/23 23:14 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 3546 DL 757209 12/29/22 12:30 MEW EET SAVTotal/NA 15.50 g 1 mL Analysis 8270E SIM DL 200 757963 01/05/23 12:47 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 5.802 g 5 mL Analysis 8015C 1000 757583 01/02/23 18:49 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.36 g 1 mL Analysis 8015C 50 757446 12/30/22 16:06 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 21 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-04 (20')Lab Sample ID: 680-228269-3 Matrix: SolidDate Collected: 12/19/22 12:00 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-04 (20')Lab Sample ID: 680-228269-3 Matrix: SolidDate Collected: 12/19/22 12:00 Percent Solids: 81.9Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.65 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 02:14 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 10.498 g 10 mL Analysis 8015C 100 757583 01/02/23 14:07 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.42 g 1 mL Analysis 8015C 1 757321 12/29/22 23:28 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Prep 3546 RE 758065 01/05/23 20:15 MJ EET SAVTotal/NA 30.28 g 1 mL Analysis 8015C RE 1 758421 01/09/23 20:37 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-05 (18')Lab Sample ID: 680-228269-4 Matrix: SolidDate Collected: 12/20/22 14:30 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-05 (18')Lab Sample ID: 680-228269-4 Matrix: SolidDate Collected: 12/20/22 14:30 Percent Solids: 90.8Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.11 g 1 mL Analysis 8270E SIM 10 757533 01/01/23 02:36 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 6.09 g 5 mL Analysis 8015C 100 757583 01/02/23 14:29 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.56 g 1 mL Analysis 8015C 5 757446 12/30/22 16:37 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 22 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-06 (18')Lab Sample ID: 680-228269-5 Matrix: SolidDate Collected: 12/20/22 15:05 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-06 (18')Lab Sample ID: 680-228269-5 Matrix: SolidDate Collected: 12/20/22 15:05 Percent Solids: 88.6Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.84 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 02:59 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5030B 757584 01/02/23 11:19 DBM EET SAVTotal/NA 5.76 g 5 mL Analysis 8015C 100 757583 01/02/23 15:55 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.26 g 1 mL Analysis 8015C 1 757321 12/29/22 23:58 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-07 (17')Lab Sample ID: 680-228269-6 Matrix: SolidDate Collected: 12/20/22 15:40 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-07 (17')Lab Sample ID: 680-228269-6 Matrix: SolidDate Collected: 12/20/22 15:40 Percent Solids: 87.2Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.28 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 03:22 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 4.584 g 5 mL Analysis 8015C 100 757583 01/02/23 14:50 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.67 g 1 mL Analysis 8015C 1 757321 12/30/22 00:14 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 23 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-08 (17')Lab Sample ID: 680-228269-7 Matrix: SolidDate Collected: 12/20/22 16:15 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-08 (17')Lab Sample ID: 680-228269-7 Matrix: SolidDate Collected: 12/20/22 16:15 Percent Solids: 84.1Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.55 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 03:44 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 4.068 g 5 mL Analysis 8015C 100 757583 01/02/23 15:12 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.53 g 1 mL Analysis 8015C 1 757321 12/30/22 00:29 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-09 (11')Lab Sample ID: 680-228269-8 Matrix: SolidDate Collected: 12/21/22 08:45 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-09 (11')Lab Sample ID: 680-228269-8 Matrix: SolidDate Collected: 12/21/22 08:45 Percent Solids: 86.2Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.37 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 04:07 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5030B 757584 01/02/23 11:19 DBM EET SAVTotal/NA 5.62 g 5 mL Analysis 8015C 100 757583 01/02/23 16:16 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.65 g 1 mL Analysis 8015C 1 757321 12/30/22 00:44 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 24 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Client Sample ID: SB-10 (11')Lab Sample ID: 680-228269-9 Matrix: SolidDate Collected: 12/21/22 09:05 Date Received: 12/22/22 10:45 Analysis Moisture WRB01/03/23 18:091 EET SAV757750 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-10 (11')Lab Sample ID: 680-228269-9 Matrix: SolidDate Collected: 12/21/22 09:05 Percent Solids: 88.7Date Received: 12/22/22 10:45 Prep 3546 MEW12/29/22 12:30 EET SAV757209 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.76 g 1 mL Analysis 8270E SIM 1 757533 01/01/23 04:30 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 757037 12/28/22 09:29 FES EET SAVTotal/NA 5.883 g 5 mL Analysis 8015C 100 757583 01/02/23 15:33 JCK EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 757155 12/28/22 20:15 MJ EET SAVTotal/NA 30.90 g 1 mL Analysis 8015C 1 757321 12/30/22 01:00 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 25 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Accreditation/Certification Summary Client: TRC Environmental Corporation Job ID: 680-228269-1 Project/Site: Greensboro, NC-463648.0.0 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 269 12-31-23 Eurofins Savannah Page 26 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Method Summary Job ID: 680-228269-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC-463648.0.0 Method Method Description LaboratoryProtocol SW8468270E SIM Semivolatile Organic Compounds (GC/MS SIM)EET SAV SW8468015CNonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)EET SAV SW8468015CNonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)EET SAV EPAMoisturePercent Moisture EET SAV SW8463546Microwave Extraction EET SAV SW8465030BPurge and Trap EET SAV SW8465035AClosed System Purge & Trap/Field Methanol EET SAV Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 27 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 Page 28 of 29 1/12/2023 1234567 8 9 10 11 12 Login Sample Receipt Checklist Client: TRC Environmental Corporation Job Number: 680-228269-1 Login Number: 228269 Question Answer Comment Creator: Sims, Robert D List Source: Eurofins Savannah List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Savannah Page 29 of 29 1/12/2023 1 2 3 4 5 6 7 8 9 10 11 12 ANALYTICAL REPORT PREPARED FOR Attn: David Szynal TRC Environmental Corporation 50 International Drive Suite 150 Greenville, South Carolina 29615 Generated 12/5/2022 6:06:18 PM JOB DESCRIPTION Greensboro, NC - Nov 2022 JOB NUMBER 680-225959-1 See page two for job notes and contact information. Savannah GA 31404 5102 LaRoche Avenue Eurofins Savannah Page 1 of 44 1 2 3 4 5 6 7 8 9 10 11 12 Eurofins Savannah Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 12/5/2022 6:06:18 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Definitions/Glossary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Qualifiers GC/MS Semi VOA Qualifier Description *-LCS and/or LCSD is outside acceptance limits, low biased. Qualifier D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. F1 MS and/or MSD recovery exceeds control limits. S1-Surrogate recovery exceeds control limits, low biased. GC VOA Qualifier Description S1-Surrogate recovery exceeds control limits, low biased. Qualifier GC Semi VOA Qualifier Description D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. Qualifier F1 MS and/or MSD recovery exceeds control limits. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 3 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Sample Summary Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID Client Sample ID Matrix Collected Received 680-225959-1 SB-UST-1-1 Solid 11/15/22 14:30 11/19/22 06:00 680-225959-2 SB-UST-1-2 Solid 11/16/22 12:05 11/19/22 06:00 680-225959-3 SB-UST-1-3 Solid 11/16/22 15:35 11/19/22 06:00 680-225959-4 SB-UST-2-1 Solid 11/15/22 11:45 11/19/22 06:00 680-225959-5 SB-UST-2-2 Solid 11/16/22 11:40 11/19/22 06:00 680-225959-6 SB-UST-2-3 Solid 11/16/22 13:20 11/19/22 06:00 680-225959-7 SB-CL-1 Solid 11/17/22 11:50 11/19/22 06:00 680-225959-8 SB-FD-1 Solid 11/17/22 09:50 11/19/22 06:00 680-225959-9 SB-USTSW-1 Solid 11/15/22 13:25 11/19/22 06:00 680-225959-10 SB-USTSW-2 Solid 11/16/22 10:05 11/19/22 06:00 680-225959-11 SB-USTSW-3 Solid 11/16/22 15:15 11/19/22 06:00 680-225959-12 SB-USTSW-4 Solid 11/16/22 15:25 11/19/22 06:00 680-225959-13 SB-USTSW-5 Solid 11/16/22 14:10 11/19/22 06:00 680-225959-14 SB-USTSW-6 Solid 11/16/22 13:30 11/19/22 06:00 680-225959-15 SB-USTSW-7 Solid 11/16/22 10:25 11/19/22 06:00 680-225959-16 SB-USTSW-8 Solid 11/15/22 15:40 11/19/22 06:00 Eurofins SavannahPage 4 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Case Narrative Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Job ID: 680-225959-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-225959-1 Receipt The samples were received on 11/19/2022 6:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 2.7°C and 2.8°C GC/MS Semi VOA Method 8270E_SIM: The following analyte recovered outside control limits for the LCS associated with preparation batch 680-752003 and analytical batch 680-752727: Fluorene. This is not indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported. Method 8270E_SIM: The laboratory control sample (LCS) associated with preparation batch 680-752003 and analytical batch 680-752727 was outside acceptance criteria for Fluorene. The batch matrix spike/matrix spike duplicate (MS/MSD) was within acceptance limits and may be used to evaluate matrix performance. Method 8270E_SIM: Surrogate recovery for the following samples were outside control limits: SB-UST-1-2 (680-225959-2), SB-UST-2-3 (680-225959-6) and SB-USTSW-3 (680-225959-11). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. Method 8270E_SIM: The following samples were diluted due to the nature of the sample matrix: SB-UST-1-2 (680-225959-2), SB-UST-2-3 (680-225959-6) and SB-USTSW-3 (680-225959-11). Elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following samples were diluted due to the nature of the sample matrix : SB-UST-1-3 (680-225959-3), SB-UST-2-2 (680-225959-5) and SB-USTSW-4 (680-225959-12). As such, surrogate recoveries are below the calibration range or are not reported, and elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-UST-2-2 (680-225959-5). Elevated reporting limits (RLs) are provided. Method 8270E_SIM: The following sample was diluted due to the nature of the sample matrix : SB-FD-1 (680-225959-8). As such, surrogate recoveries are below the calibration range or are not reported, and elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Gasoline Range Organics Method 8015C_GRO: Surrogate recovery for the following sample was outside control limits: SB-UST-1-3 (680-225959-3). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Diesel Range Organics Method 8015C_DRO: The following sample required a dilution due to the nature of the sample matrix: SB-UST-1-2 (680-225959-2), SB-UST-2-2 (680-225959-5), SB-UST-2-3 (680-225959-6), SB-FD-1 (680-225959-8), SB-USTSW-3 (680-225959-11) and SB-USTSW-4 (680-225959-12). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information. Method 8015C_DRO: The following sample required a dilution due to the nature of the sample matrix: SB-UST-1-3 (680-225959-3). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins SavannahPage 5 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Case Narrative Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Job ID: 680-225959-1 (Continued) Laboratory: Eurofins Savannah (Continued) General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins SavannahPage 6 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-1Client Sample ID: SB-UST-1-1 Matrix: SolidDate Collected: 11/15/22 14:30 Percent Solids: 85.3Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00758 mg/Kg ☼11/22/22 18:00 11/28/22 17:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDAcenaphthylene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDAnthracene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDBenzo[a]anthracene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDBenzo[a]pyrene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDBenzo[b]fluoranthene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼ND F1Benzo[g,h,i]perylene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDBenzo[k]fluoranthene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDChrysene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDDibenz(a,h)anthracene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDFluoranthene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼ND *-Fluorene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼ND F1Indeno[1,2,3-cd]pyrene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼ND1-Methylnaphthalene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼ND2-Methylnaphthalene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDNaphthalene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDPhenanthrene 0.00758 mg/Kg 11/22/22 18:00 11/28/22 17:04 1☼NDPyrene 2-Fluorobiphenyl (Surr)53 30-130 11/22/22 18:00 11/28/22 17:04 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)53 11/22/22 18:00 11/28/22 17:04 130-130 Terphenyl-d14 (Surr)75 11/22/22 18:00 11/28/22 17:04 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 11.2 mg/Kg ☼11/22/22 09:57 11/27/22 17:27 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 70 70-131 11/22/22 09:57 11/27/22 17:27 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 51.4 F1 9.25 mg/Kg ☼11/23/22 18:30 11/28/22 23:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)56 15-139 11/23/22 18:30 11/28/22 23:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 7 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-2Client Sample ID: SB-UST-1-2 Matrix: SolidDate Collected: 11/16/22 12:05 Percent Solids: 90.0Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0366 mg/Kg ☼11/22/22 18:00 11/30/22 00:59 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDAcenaphthylene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDAnthracene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDBenzo[a]anthracene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDBenzo[a]pyrene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDBenzo[b]fluoranthene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDBenzo[g,h,i]perylene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDBenzo[k]fluoranthene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDChrysene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDDibenz(a,h)anthracene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDFluoranthene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼ND *-Fluorene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDIndeno[1,2,3-cd]pyrene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼0.4451-Methylnaphthalene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼0.3952-Methylnaphthalene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDNaphthalene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼NDPhenanthrene 0.0366 mg/Kg 11/22/22 18:00 11/30/22 00:59 5☼0.192Pyrene 2-Fluorobiphenyl (Surr)68 30-130 11/22/22 18:00 11/30/22 00:59 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 S1-11/22/22 18:00 11/30/22 00:59 530-130 Terphenyl-d14 (Surr)71 11/22/22 18:00 11/30/22 00:59 530-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 161 21.8 mg/Kg ☼11/22/22 09:57 11/29/22 15:11 200 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 99 70-131 11/22/22 09:57 11/29/22 15:11 200 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 1970 176 mg/Kg ☼11/23/22 18:30 11/29/22 14:33 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 14:33 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 8 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-3Client Sample ID: SB-UST-1-3 Matrix: SolidDate Collected: 11/16/22 15:35 Percent Solids: 80.7Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0815 mg/Kg ☼11/22/22 18:00 11/30/22 01:22 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDAcenaphthylene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDAnthracene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDBenzo[a]anthracene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDBenzo[a]pyrene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDBenzo[b]fluoranthene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDBenzo[g,h,i]perylene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDBenzo[k]fluoranthene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDChrysene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDDibenz(a,h)anthracene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDFluoranthene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼ND *-Fluorene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDIndeno[1,2,3-cd]pyrene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼4.951-Methylnaphthalene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼7.812-Methylnaphthalene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼NDNaphthalene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼0.967Phenanthrene 0.0815 mg/Kg 11/22/22 18:00 11/30/22 01:22 10☼1.01Pyrene 2-Fluorobiphenyl (Surr)0 D 30-130 11/22/22 18:00 11/30/22 01:22 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 11/22/22 18:00 11/30/22 01:22 1030-130 Terphenyl-d14 (Surr)0 D 11/22/22 18:00 11/30/22 01:22 1030-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 655 139 mg/Kg ☼11/22/22 09:57 11/29/22 15:54 1000 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 61 S1-70-131 11/22/22 09:57 11/29/22 15:54 1000 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 8570 490 mg/Kg ☼11/23/22 18:30 11/29/22 21:29 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 21:29 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 9 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-4Client Sample ID: SB-UST-2-1 Matrix: SolidDate Collected: 11/15/22 11:45 Percent Solids: 80.0Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00813 mg/Kg ☼11/22/22 18:00 11/28/22 18:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDAcenaphthylene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDAnthracene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDBenzo[a]anthracene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDBenzo[a]pyrene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDBenzo[b]fluoranthene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDBenzo[g,h,i]perylene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDBenzo[k]fluoranthene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDChrysene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDDibenz(a,h)anthracene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDFluoranthene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼ND *-Fluorene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDIndeno[1,2,3-cd]pyrene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼0.01521-Methylnaphthalene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼0.01702-Methylnaphthalene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼0.0103Naphthalene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDPhenanthrene 0.00813 mg/Kg 11/22/22 18:00 11/28/22 18:12 1☼NDPyrene 2-Fluorobiphenyl (Surr)43 30-130 11/22/22 18:00 11/28/22 18:12 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)44 11/22/22 18:00 11/28/22 18:12 130-130 Terphenyl-d14 (Surr)62 11/22/22 18:00 11/28/22 18:12 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 13.9 mg/Kg ☼11/22/22 09:57 11/29/22 13:02 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 78 70-131 11/22/22 09:57 11/29/22 13:02 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 54.4 9.74 mg/Kg ☼11/23/22 18:30 11/28/22 23:54 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)52 15-139 11/23/22 18:30 11/28/22 23:54 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 10 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-5Client Sample ID: SB-UST-2-2 Matrix: SolidDate Collected: 11/16/22 11:40 Percent Solids: 90.0Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0710 mg/Kg ☼11/22/22 18:00 11/30/22 01:44 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDAcenaphthylene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDAnthracene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDBenzo[a]anthracene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDBenzo[a]pyrene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDBenzo[b]fluoranthene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDBenzo[g,h,i]perylene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDBenzo[k]fluoranthene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDChrysene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDDibenz(a,h)anthracene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDFluoranthene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼ND *-Fluorene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDIndeno[1,2,3-cd]pyrene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼6.781-Methylnaphthalene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼NDNaphthalene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼1.12Phenanthrene 0.0710 mg/Kg 11/22/22 18:00 11/30/22 01:44 10☼1.05Pyrene 2-Fluorobiphenyl (Surr)0 D 30-130 11/22/22 18:00 11/30/22 01:44 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 11/22/22 18:00 11/30/22 01:44 1030-130 Terphenyl-d14 (Surr)0 D 11/22/22 18:00 11/30/22 01:44 1030-130 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) - DL RL MDL 11.3 0.355 mg/Kg ☼11/22/22 18:00 11/30/22 07:58 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2-Methylnaphthalene Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 830 119 mg/Kg ☼11/22/22 09:57 11/29/22 16:15 1000 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 73 70-131 11/22/22 09:57 11/29/22 16:15 1000 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 11800 433 mg/Kg ☼11/23/22 18:30 11/29/22 15:04 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 15:04 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 11 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-6Client Sample ID: SB-UST-2-3 Matrix: SolidDate Collected: 11/16/22 13:20 Percent Solids: 81.8Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0400 mg/Kg ☼11/22/22 18:00 11/30/22 02:07 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDAcenaphthylene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDAnthracene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDBenzo[a]anthracene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDBenzo[a]pyrene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDBenzo[b]fluoranthene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDBenzo[g,h,i]perylene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDBenzo[k]fluoranthene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDChrysene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDDibenz(a,h)anthracene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDFluoranthene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼ND *-Fluorene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDIndeno[1,2,3-cd]pyrene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼1.251-Methylnaphthalene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼1.802-Methylnaphthalene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDNaphthalene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼NDPhenanthrene 0.0400 mg/Kg 11/22/22 18:00 11/30/22 02:07 5☼0.281Pyrene 2-Fluorobiphenyl (Surr)72 30-130 11/22/22 18:00 11/30/22 02:07 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 S1-11/22/22 18:00 11/30/22 02:07 530-130 Terphenyl-d14 (Surr)71 11/22/22 18:00 11/30/22 02:07 530-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 81.7 16.5 mg/Kg ☼11/22/22 09:57 11/29/22 14:06 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 11/22/22 09:57 11/29/22 14:06 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 3300 193 mg/Kg ☼11/23/22 18:30 11/29/22 15:20 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 15:20 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 12 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-7Client Sample ID: SB-CL-1 Matrix: SolidDate Collected: 11/17/22 11:50 Percent Solids: 97.0Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00673 mg/Kg ☼11/22/22 18:00 11/28/22 19:20 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDAcenaphthylene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDAnthracene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDBenzo[a]anthracene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDBenzo[a]pyrene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDBenzo[b]fluoranthene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDBenzo[g,h,i]perylene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDBenzo[k]fluoranthene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDChrysene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDDibenz(a,h)anthracene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDFluoranthene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼ND *-Fluorene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDIndeno[1,2,3-cd]pyrene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼ND1-Methylnaphthalene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼ND2-Methylnaphthalene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDNaphthalene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDPhenanthrene 0.00673 mg/Kg 11/22/22 18:00 11/28/22 19:20 1☼NDPyrene 2-Fluorobiphenyl (Surr)61 30-130 11/22/22 18:00 11/28/22 19:20 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)61 11/22/22 18:00 11/28/22 19:20 130-130 Terphenyl-d14 (Surr)86 11/22/22 18:00 11/28/22 19:20 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 11.2 mg/Kg ☼11/22/22 09:57 11/29/22 13:45 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 79 70-131 11/22/22 09:57 11/29/22 13:45 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 8.06 mg/Kg ☼11/23/22 18:30 11/29/22 00:40 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)64 15-139 11/23/22 18:30 11/29/22 00:40 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 13 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-8Client Sample ID: SB-FD-1 Matrix: SolidDate Collected: 11/17/22 09:50 Percent Solids: 87.4Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 7.49 0.752 mg/Kg ☼11/22/22 18:00 11/30/22 08:23 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDAcenaphthylene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDAnthracene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDBenzo[a]anthracene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDBenzo[a]pyrene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDBenzo[b]fluoranthene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDBenzo[g,h,i]perylene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDBenzo[k]fluoranthene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDChrysene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDDibenz(a,h)anthracene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDFluoranthene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼ND *-Fluorene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDIndeno[1,2,3-cd]pyrene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼53.61-Methylnaphthalene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼18.4Naphthalene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼14.4Phenanthrene 0.752 mg/Kg 11/22/22 18:00 11/30/22 08:23 100☼NDPyrene 2-Fluorobiphenyl (Surr)0 D 30-130 11/22/22 18:00 11/30/22 08:23 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 11/22/22 18:00 11/30/22 08:23 10030-130 Terphenyl-d14 (Surr)0 D 11/22/22 18:00 11/30/22 08:23 10030-130 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) - DL2 RL MDL 75.7 1.50 mg/Kg ☼11/22/22 18:00 12/01/22 17:57 200 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2-Methylnaphthalene Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 407 61.5 mg/Kg ☼11/22/22 09:57 11/29/22 15:32 500 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 70 70-131 11/22/22 09:57 11/29/22 15:32 500 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 15800 447 mg/Kg ☼11/23/22 18:30 11/29/22 15:35 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 15:35 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 14 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-9Client Sample ID: SB-USTSW-1 Matrix: SolidDate Collected: 11/15/22 13:25 Percent Solids: 89.5Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00721 mg/Kg ☼11/22/22 18:00 11/28/22 20:06 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDAcenaphthylene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDAnthracene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDBenzo[a]anthracene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDBenzo[a]pyrene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDBenzo[b]fluoranthene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDBenzo[g,h,i]perylene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDBenzo[k]fluoranthene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDChrysene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDDibenz(a,h)anthracene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDFluoranthene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼ND *-Fluorene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDIndeno[1,2,3-cd]pyrene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼ND1-Methylnaphthalene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼ND2-Methylnaphthalene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDNaphthalene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDPhenanthrene 0.00721 mg/Kg 11/22/22 18:00 11/28/22 20:06 1☼NDPyrene 2-Fluorobiphenyl (Surr)51 30-130 11/22/22 18:00 11/28/22 20:06 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)51 11/22/22 18:00 11/28/22 20:06 130-130 Terphenyl-d14 (Surr)75 11/22/22 18:00 11/28/22 20:06 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 17.5 mg/Kg ☼11/22/22 09:57 11/29/22 13:24 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 80 70-131 11/22/22 09:57 11/29/22 13:24 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 61.2 8.85 mg/Kg ☼11/23/22 18:30 11/29/22 01:10 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)68 15-139 11/23/22 18:30 11/29/22 01:10 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 15 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-10Client Sample ID: SB-USTSW-2 Matrix: SolidDate Collected: 11/16/22 10:05 Percent Solids: 88.5Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00742 mg/Kg ☼11/22/22 18:00 11/28/22 20:28 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDAcenaphthylene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDAnthracene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDBenzo[a]anthracene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDBenzo[a]pyrene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDBenzo[b]fluoranthene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDBenzo[g,h,i]perylene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDBenzo[k]fluoranthene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDChrysene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDDibenz(a,h)anthracene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDFluoranthene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼ND *-Fluorene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDIndeno[1,2,3-cd]pyrene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼ND1-Methylnaphthalene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼ND2-Methylnaphthalene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDNaphthalene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDPhenanthrene 0.00742 mg/Kg 11/22/22 18:00 11/28/22 20:28 1☼NDPyrene 2-Fluorobiphenyl (Surr)59 30-130 11/22/22 18:00 11/28/22 20:28 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)62 11/22/22 18:00 11/28/22 20:28 130-130 Terphenyl-d14 (Surr)77 11/22/22 18:00 11/28/22 20:28 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 28.4 13.2 mg/Kg ☼11/22/22 09:57 11/29/22 14:28 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 74 70-131 11/22/22 09:57 11/29/22 14:28 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 8.95 mg/Kg ☼11/23/22 18:30 11/29/22 01:26 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)58 15-139 11/23/22 18:30 11/29/22 01:26 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 16 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-11Client Sample ID: SB-USTSW-3 Matrix: SolidDate Collected: 11/16/22 15:15 Percent Solids: 75.4Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0435 mg/Kg ☼11/22/22 18:00 11/30/22 02:52 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDAcenaphthylene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDAnthracene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDBenzo[a]anthracene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDBenzo[a]pyrene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDBenzo[b]fluoranthene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDBenzo[g,h,i]perylene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDBenzo[k]fluoranthene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDChrysene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDDibenz(a,h)anthracene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDFluoranthene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼ND *-Fluorene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDIndeno[1,2,3-cd]pyrene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼1.191-Methylnaphthalene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼0.8052-Methylnaphthalene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼NDNaphthalene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼0.272Phenanthrene 0.0435 mg/Kg 11/22/22 18:00 11/30/22 02:52 5☼0.299Pyrene 2-Fluorobiphenyl (Surr)82 30-130 11/22/22 18:00 11/30/22 02:52 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 S1-11/22/22 18:00 11/30/22 02:52 530-130 Terphenyl-d14 (Surr)83 11/22/22 18:00 11/30/22 02:52 530-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 128 16.4 mg/Kg ☼11/22/22 09:57 11/27/22 21:02 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 102 70-131 11/22/22 09:57 11/27/22 21:02 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 2380 209 mg/Kg ☼11/23/22 18:30 11/29/22 15:51 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 15:51 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 17 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-12Client Sample ID: SB-USTSW-4 Matrix: SolidDate Collected: 11/16/22 15:25 Percent Solids: 69.0Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.0939 mg/Kg ☼11/22/22 18:00 11/30/22 03:15 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDAcenaphthylene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDAnthracene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDBenzo[a]anthracene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDBenzo[a]pyrene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDBenzo[b]fluoranthene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDBenzo[g,h,i]perylene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDBenzo[k]fluoranthene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDChrysene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDDibenz(a,h)anthracene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDFluoranthene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼ND *-Fluorene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDIndeno[1,2,3-cd]pyrene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼ND1-Methylnaphthalene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼ND2-Methylnaphthalene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDNaphthalene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼NDPhenanthrene 0.0939 mg/Kg 11/22/22 18:00 11/30/22 03:15 10☼0.374Pyrene 2-Fluorobiphenyl (Surr)0 D 30-130 11/22/22 18:00 11/30/22 03:15 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)0 D 11/22/22 18:00 11/30/22 03:15 1030-130 Terphenyl-d14 (Surr)0 D 11/22/22 18:00 11/30/22 03:15 1030-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL 96.1 17.9 mg/Kg ☼11/22/22 09:57 11/27/22 21:24 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 79 70-131 11/22/22 09:57 11/27/22 21:24 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 2010 230 mg/Kg ☼11/23/22 18:30 11/29/22 16:06 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)0 D 15-139 11/23/22 18:30 11/29/22 16:06 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 18 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-13Client Sample ID: SB-USTSW-5 Matrix: SolidDate Collected: 11/16/22 14:10 Percent Solids: 87.1Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00739 mg/Kg ☼11/22/22 18:00 11/30/22 03:38 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDAcenaphthylene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDAnthracene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDBenzo[a]anthracene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDBenzo[a]pyrene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDBenzo[b]fluoranthene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDBenzo[g,h,i]perylene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDBenzo[k]fluoranthene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDChrysene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDDibenz(a,h)anthracene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼0.0193Fluoranthene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼ND *-Fluorene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDIndeno[1,2,3-cd]pyrene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼0.01511-Methylnaphthalene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼ND2-Methylnaphthalene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDNaphthalene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼NDPhenanthrene 0.00739 mg/Kg 11/22/22 18:00 11/30/22 03:38 1☼0.0596Pyrene 2-Fluorobiphenyl (Surr)56 30-130 11/22/22 18:00 11/30/22 03:38 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)54 11/22/22 18:00 11/30/22 03:38 130-130 Terphenyl-d14 (Surr)72 11/22/22 18:00 11/30/22 03:38 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 13.5 mg/Kg ☼11/22/22 09:57 11/29/22 14:49 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 71 70-131 11/22/22 09:57 11/29/22 14:49 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 261 9.10 mg/Kg ☼11/23/22 18:30 11/29/22 02:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)74 15-139 11/23/22 18:30 11/29/22 02:12 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 19 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-14Client Sample ID: SB-USTSW-6 Matrix: SolidDate Collected: 11/16/22 13:30 Percent Solids: 86.5Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00763 mg/Kg ☼11/22/22 18:00 11/30/22 04:00 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDAcenaphthylene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDAnthracene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDBenzo[a]anthracene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDBenzo[a]pyrene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDBenzo[b]fluoranthene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDBenzo[g,h,i]perylene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDBenzo[k]fluoranthene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDChrysene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDDibenz(a,h)anthracene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDFluoranthene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼ND *-Fluorene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDIndeno[1,2,3-cd]pyrene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼ND1-Methylnaphthalene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼ND2-Methylnaphthalene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDNaphthalene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDPhenanthrene 0.00763 mg/Kg 11/22/22 18:00 11/30/22 04:00 1☼NDPyrene 2-Fluorobiphenyl (Surr)50 30-130 11/22/22 18:00 11/30/22 04:00 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)53 11/22/22 18:00 11/30/22 04:00 130-130 Terphenyl-d14 (Surr)72 11/22/22 18:00 11/30/22 04:00 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 14.1 mg/Kg ☼11/22/22 09:57 11/27/22 22:06 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 74 70-131 11/22/22 09:57 11/27/22 22:06 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL 10.2 9.19 mg/Kg ☼11/23/22 18:30 11/29/22 02:27 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)66 15-139 11/23/22 18:30 11/29/22 02:27 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 20 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-15Client Sample ID: SB-USTSW-7 Matrix: SolidDate Collected: 11/16/22 10:25 Percent Solids: 75.9Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00867 mg/Kg ☼11/22/22 18:00 11/30/22 04:23 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDAcenaphthylene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDAnthracene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDBenzo[a]anthracene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDBenzo[a]pyrene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDBenzo[b]fluoranthene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDBenzo[g,h,i]perylene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDBenzo[k]fluoranthene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDChrysene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDDibenz(a,h)anthracene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDFluoranthene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼ND *-Fluorene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDIndeno[1,2,3-cd]pyrene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼ND1-Methylnaphthalene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼ND2-Methylnaphthalene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDNaphthalene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDPhenanthrene 0.00867 mg/Kg 11/22/22 18:00 11/30/22 04:23 1☼NDPyrene 2-Fluorobiphenyl (Surr)65 30-130 11/22/22 18:00 11/30/22 04:23 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)70 11/22/22 18:00 11/30/22 04:23 130-130 Terphenyl-d14 (Surr)80 11/22/22 18:00 11/30/22 04:23 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 15.8 mg/Kg ☼11/22/22 09:57 11/27/22 22:28 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 76 70-131 11/22/22 09:57 11/27/22 22:28 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 10.3 mg/Kg ☼11/23/22 18:30 11/29/22 02:42 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)53 15-139 11/23/22 18:30 11/29/22 02:42 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 21 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Client Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Lab Sample ID: 680-225959-16Client Sample ID: SB-USTSW-8 Matrix: SolidDate Collected: 11/15/22 15:40 Percent Solids: 81.8Date Received: 11/19/22 06:00 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL ND 0.00802 mg/Kg ☼11/22/22 18:00 11/30/22 04:46 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDAcenaphthylene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDAnthracene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDBenzo[a]anthracene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDBenzo[a]pyrene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDBenzo[b]fluoranthene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDBenzo[g,h,i]perylene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDBenzo[k]fluoranthene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDChrysene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDDibenz(a,h)anthracene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDFluoranthene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼ND *-Fluorene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDIndeno[1,2,3-cd]pyrene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼ND1-Methylnaphthalene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼ND2-Methylnaphthalene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDNaphthalene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDPhenanthrene 0.00802 mg/Kg 11/22/22 18:00 11/30/22 04:46 1☼NDPyrene 2-Fluorobiphenyl (Surr)52 30-130 11/22/22 18:00 11/30/22 04:46 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 (Surr)58 11/22/22 18:00 11/30/22 04:46 130-130 Terphenyl-d14 (Surr)74 11/22/22 18:00 11/30/22 04:46 130-130 Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL ND 16.6 mg/Kg ☼11/22/22 09:57 11/27/22 22:49 100 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Gasoline Range Organics [C6 - C10] a,a,a-Trifluorotoluene 78 70-131 11/22/22 09:57 11/27/22 22:49 100 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: SW846 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL ND 9.62 mg/Kg ☼11/23/22 18:30 11/29/22 02:58 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Diesel Range Organics [C10-C28] o-Terphenyl (Surr)61 15-139 11/23/22 18:30 11/29/22 02:58 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Eurofins Savannah Page 22 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) Client Sample ID: Method BlankLab Sample ID: MB 680-752003/17-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752485 Prep Batch: 752003 RL MDL Acenaphthene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Acenaphthylene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Anthracene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Benzo[a]anthracene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Benzo[a]pyrene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Benzo[b]fluoranthene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Benzo[g,h,i]perylene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Benzo[k]fluoranthene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Chrysene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Dibenz(a,h)anthracene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Fluoranthene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Fluorene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Indeno[1,2,3-cd]pyrene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 11-Methylnaphthalene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 12-Methylnaphthalene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Naphthalene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Phenanthrene ND 0.00636 mg/Kg 11/22/22 18:00 11/28/22 15:34 1Pyrene 2-Fluorobiphenyl (Surr)62 30-130 11/28/22 15:34 1 MB MB Surrogate 11/22/22 18:00 Dil FacPreparedAnalyzedQualifierLimits%Recovery 62 11/22/22 18:00 11/28/22 15:34 1Nitrobenzene-d5 (Surr)30-130 85 11/22/22 18:00 11/28/22 15:34 1Terphenyl-d14 (Surr)30-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752003/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752727 Prep Batch: 752003 Acenaphthene 0.163 0.1317 mg/Kg 81 30 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 0.163 0.1285 mg/Kg 79 30 -130 Anthracene 0.163 0.1349 mg/Kg 83 30 -130 Benzo[a]anthracene 0.163 0.1345 mg/Kg 83 30 -130 Benzo[a]pyrene 0.163 0.1424 mg/Kg 87 30 -130 Benzo[b]fluoranthene 0.163 0.1460 mg/Kg 90 30 -130 Benzo[g,h,i]perylene 0.163 0.1385 mg/Kg 85 30 -130 Benzo[k]fluoranthene 0.163 0.1448 mg/Kg 89 30 -130 Chrysene 0.163 0.1402 mg/Kg 86 30 -130 Dibenz(a,h)anthracene 0.163 0.1429 mg/Kg 88 30 -130 Fluoranthene 0.163 0.1480 mg/Kg 91 30 -130 Fluorene 0.163 0.02020 *-mg/Kg 12 30 -130 Indeno[1,2,3-cd]pyrene 0.163 0.1415 mg/Kg 87 30 -130 1-Methylnaphthalene 0.163 0.1203 mg/Kg 74 30 -130 2-Methylnaphthalene 0.163 0.1215 mg/Kg 75 30 -130 Naphthalene 0.163 0.1195 mg/Kg 73 30 -130 Phenanthrene 0.163 0.1365 mg/Kg 84 30 -130 Pyrene 0.163 0.1480 mg/Kg 91 30 -130 Eurofins Savannah Page 23 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752003/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752727 Prep Batch: 752003 2-Fluorobiphenyl (Surr)30 -130 Surrogate 69 LCS LCS Qualifier Limits%Recovery 76Nitrobenzene-d5 (Surr)30 -130 82Terphenyl-d14 (Surr)30 -130 Client Sample ID: SB-UST-1-1Lab Sample ID: 680-225959-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 752485 Prep Batch: 752003 Acenaphthene ND 0.186 0.1096 mg/Kg 59 30 -130☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Acenaphthylene ND 0.186 0.1061 mg/Kg 57 30 -130☼ Anthracene ND 0.186 0.1236 mg/Kg 66 30 -130☼ Benzo[a]anthracene ND 0.186 0.1262 mg/Kg 68 30 -130☼ Benzo[a]pyrene ND 0.186 0.09427 mg/Kg 51 30 -130☼ Benzo[b]fluoranthene ND 0.186 0.1070 mg/Kg 57 30 -130☼ Benzo[g,h,i]perylene ND F1 0.186 0.04469 F1 mg/Kg 24 30 -130☼ Benzo[k]fluoranthene ND 0.186 0.1072 mg/Kg 58 30 -130☼ Chrysene ND 0.186 0.1304 mg/Kg 70 30 -130☼ Dibenz(a,h)anthracene ND 0.186 0.05815 mg/Kg 31 30 -130☼ Fluoranthene ND 0.186 0.1425 mg/Kg 77 30 -130☼ Fluorene ND *-0.186 0.1209 mg/Kg 65 30 -130☼ Indeno[1,2,3-cd]pyrene ND F1 0.186 0.05158 F1 mg/Kg 28 30 -130☼ 1-Methylnaphthalene ND 0.186 0.1022 mg/Kg 51 30 -130☼ 2-Methylnaphthalene ND 0.186 0.1018 mg/Kg 52 30 -130☼ Naphthalene ND 0.186 0.09703 mg/Kg 52 30 -130☼ Phenanthrene ND 0.186 0.1249 mg/Kg 67 30 -130☼ Pyrene ND 0.186 0.1498 mg/Kg 78 30 -130☼ 2-Fluorobiphenyl (Surr)30 -130 Surrogate 48 MS MS Qualifier Limits%Recovery 50Nitrobenzene-d5 (Surr)30 -130 68Terphenyl-d14 (Surr)30 -130 Client Sample ID: SB-UST-1-1Lab Sample ID: 680-225959-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 752485 Prep Batch: 752003 Acenaphthene ND 0.191 0.1290 mg/Kg 67 30 -130 16 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Acenaphthylene ND 0.191 0.1230 mg/Kg 64 30 -130 15 30☼ Anthracene ND 0.191 0.1442 mg/Kg 75 30 -130 15 30☼ Benzo[a]anthracene ND 0.191 0.1558 mg/Kg 81 30 -130 21 30☼ Benzo[a]pyrene ND 0.191 0.1177 mg/Kg 62 30 -130 22 30☼ Benzo[b]fluoranthene ND 0.191 0.1350 mg/Kg 71 30 -130 23 30☼ Benzo[g,h,i]perylene ND F1 0.191 0.05309 F1 mg/Kg 28 30 -130 17 30☼ Benzo[k]fluoranthene ND 0.191 0.1345 mg/Kg 70 30 -130 23 30☼ Chrysene ND 0.191 0.1606 mg/Kg 84 30 -130 21 30☼ Dibenz(a,h)anthracene ND 0.191 0.07233 mg/Kg 38 30 -130 22 30☼ Eurofins Savannah Page 24 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Client Sample ID: SB-UST-1-1Lab Sample ID: 680-225959-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 752485 Prep Batch: 752003 Fluoranthene ND 0.191 0.1716 mg/Kg 90 30 -130 19 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Fluorene ND *-0.191 0.1417 mg/Kg 74 30 -130 16 30☼ Indeno[1,2,3-cd]pyrene ND F1 0.191 0.06178 mg/Kg 32 30 -130 18 30☼ 1-Methylnaphthalene ND 0.191 0.1177 mg/Kg 58 30 -130 14 30☼ 2-Methylnaphthalene ND 0.191 0.1166 mg/Kg 58 30 -130 13 30☼ Naphthalene ND 0.191 0.1106 mg/Kg 58 30 -130 13 30☼ Phenanthrene ND 0.191 0.1451 mg/Kg 76 30 -130 15 30☼ Pyrene ND 0.191 0.1806 mg/Kg 92 30 -130 19 30☼ 2-Fluorobiphenyl (Surr)30 -130 Surrogate 56 MSD MSD Qualifier Limits%Recovery 56Nitrobenzene-d5 (Surr)30 -130 82Terphenyl-d14 (Surr)30 -130 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) Client Sample ID: Method BlankLab Sample ID: MB 680-752410/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752410 RL MDL Gasoline Range Organics [C6 - C10]ND 10.0 mg/Kg 11/27/22 15:17 100 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier a,a,a-Trifluorotoluene 79 70-131 11/27/22 15:17 100 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752410/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752410 Gasoline Range Organics [C6 - C10] 50.0 52.25 mg/Kg 105 64 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits a,a,a-Trifluorotoluene 70 -131 Surrogate 105 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-752410/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752410 Gasoline Range Organics [C6 - C10] 50.0 52.41 mg/Kg 105 64 -133 0 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD a,a,a-Trifluorotoluene 70 -131 Surrogate 104 LCSD LCSD Qualifier Limits%Recovery Eurofins Savannah Page 25 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 680-752712/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752712 RL MDL Gasoline Range Organics [C6 - C10]ND 10.0 mg/Kg 11/29/22 12:40 100 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier a,a,a-Trifluorotoluene 80 70-131 11/29/22 12:40 100 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752712/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752712 Gasoline Range Organics [C6 - C10] 50.0 49.53 mg/Kg 99 64 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits a,a,a-Trifluorotoluene 70 -131 Surrogate 104 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-752712/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 752712 Gasoline Range Organics [C6 - C10] 50.0 49.52 mg/Kg 99 64 -133 0 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD a,a,a-Trifluorotoluene 70 -131 Surrogate 105 LCSD LCSD Qualifier Limits%Recovery Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Client Sample ID: Method BlankLab Sample ID: MB 680-752235/17-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752554 Prep Batch: 752235 RL MDL Diesel Range Organics [C10-C28]ND 7.90 mg/Kg 11/23/22 18:30 11/28/22 22:37 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl (Surr)57 15-139 11/28/22 22:37 1 MB MB Surrogate 11/23/22 18:30 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752235/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752554 Prep Batch: 752235 Diesel Range Organics [C10-C28] 32.4 21.71 mg/Kg 67 26 -133 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Eurofins Savannah Page 26 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Sample Results Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-752235/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 752554 Prep Batch: 752235 o-Terphenyl (Surr)15 -139 Surrogate 67 LCS LCS Qualifier Limits%Recovery Client Sample ID: SB-UST-1-1Lab Sample ID: 680-225959-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 752554 Prep Batch: 752235 Diesel Range Organics [C10-C28] 51.4 F1 38.6 56.18 F1 mg/Kg 12 26 -133☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits o-Terphenyl (Surr)15 -139 Surrogate 66 MS MS Qualifier Limits%Recovery Client Sample ID: SB-UST-1-1Lab Sample ID: 680-225959-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 752554 Prep Batch: 752235 Diesel Range Organics [C10-C28] 51.4 F1 38.4 68.96 mg/Kg 46 26 -133 20 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD o-Terphenyl (Surr)15 -139 Surrogate 77 MSD MSD Qualifier Limits%Recovery Eurofins Savannah Page 27 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 GC/MS Semi VOA Prep Batch: 752003 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-225959-1 SB-UST-1-1 Total/NA Solid 3546680-225959-2 SB-UST-1-2 Total/NA Solid 3546680-225959-3 SB-UST-1-3 Total/NA Solid 3546680-225959-4 SB-UST-2-1 Total/NA Solid 3546680-225959-5 - DL SB-UST-2-2 Total/NA Solid 3546680-225959-5 SB-UST-2-2 Total/NA Solid 3546680-225959-6 SB-UST-2-3 Total/NA Solid 3546680-225959-7 SB-CL-1 Total/NA Solid 3546680-225959-8 SB-FD-1 Total/NA Solid 3546680-225959-8 - DL2 SB-FD-1 Total/NA Solid 3546680-225959-9 SB-USTSW-1 Total/NA Solid 3546680-225959-10 SB-USTSW-2 Total/NA Solid 3546680-225959-11 SB-USTSW-3 Total/NA Solid 3546680-225959-12 SB-USTSW-4 Total/NA Solid 3546680-225959-13 SB-USTSW-5 Total/NA Solid 3546680-225959-14 SB-USTSW-6 Total/NA Solid 3546680-225959-15 SB-USTSW-7 Total/NA Solid 3546680-225959-16 SB-USTSW-8 Total/NA Solid 3546MB 680-752003/17-A Method Blank Total/NA Solid 3546LCS 680-752003/18-A Lab Control Sample Total/NA Solid 3546680-225959-1 MS SB-UST-1-1 Total/NA Solid 3546680-225959-1 MSD SB-UST-1-1 Total/NA Analysis Batch: 752485 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 752003680-225959-1 SB-UST-1-1 Total/NA Solid 8270E SIM 752003680-225959-4 SB-UST-2-1 Total/NA Solid 8270E SIM 752003680-225959-7 SB-CL-1 Total/NA Solid 8270E SIM 752003680-225959-9 SB-USTSW-1 Total/NA Solid 8270E SIM 752003680-225959-10 SB-USTSW-2 Total/NA Solid 8270E SIM 752003MB 680-752003/17-A Method Blank Total/NA Solid 8270E SIM 752003680-225959-1 MS SB-UST-1-1 Total/NA Solid 8270E SIM 752003680-225959-1 MSD SB-UST-1-1 Total/NA Analysis Batch: 752727 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 752003680-225959-2 SB-UST-1-2 Total/NA Solid 8270E SIM 752003680-225959-3 SB-UST-1-3 Total/NA Solid 8270E SIM 752003680-225959-5 SB-UST-2-2 Total/NA Solid 8270E SIM 752003680-225959-6 SB-UST-2-3 Total/NA Solid 8270E SIM 752003680-225959-11 SB-USTSW-3 Total/NA Solid 8270E SIM 752003680-225959-12 SB-USTSW-4 Total/NA Solid 8270E SIM 752003680-225959-13 SB-USTSW-5 Total/NA Solid 8270E SIM 752003680-225959-14 SB-USTSW-6 Total/NA Solid 8270E SIM 752003680-225959-15 SB-USTSW-7 Total/NA Solid 8270E SIM 752003680-225959-16 SB-USTSW-8 Total/NA Solid 8270E SIM 752003LCS 680-752003/18-A Lab Control Sample Total/NA Analysis Batch: 752826 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 752003680-225959-5 - DL SB-UST-2-2 Total/NA Eurofins Savannah Page 28 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 GC/MS Semi VOA (Continued) Analysis Batch: 752826 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 752003680-225959-8 SB-FD-1 Total/NA Analysis Batch: 753207 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 752003680-225959-8 - DL2 SB-FD-1 Total/NA GC VOA Prep Batch: 751888 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035A680-225959-1 SB-UST-1-1 Total/NA Solid 5035A680-225959-2 SB-UST-1-2 Total/NA Solid 5035A680-225959-3 SB-UST-1-3 Total/NA Solid 5035A680-225959-4 SB-UST-2-1 Total/NA Solid 5035A680-225959-5 SB-UST-2-2 Total/NA Solid 5035A680-225959-6 SB-UST-2-3 Total/NA Solid 5035A680-225959-7 SB-CL-1 Total/NA Solid 5035A680-225959-8 SB-FD-1 Total/NA Solid 5035A680-225959-9 SB-USTSW-1 Total/NA Solid 5035A680-225959-10 SB-USTSW-2 Total/NA Solid 5035A680-225959-11 SB-USTSW-3 Total/NA Solid 5035A680-225959-12 SB-USTSW-4 Total/NA Solid 5035A680-225959-13 SB-USTSW-5 Total/NA Solid 5035A680-225959-14 SB-USTSW-6 Total/NA Solid 5035A680-225959-15 SB-USTSW-7 Total/NA Solid 5035A680-225959-16 SB-USTSW-8 Total/NA Analysis Batch: 752410 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 751888680-225959-1 SB-UST-1-1 Total/NA Solid 8015C 751888680-225959-11 SB-USTSW-3 Total/NA Solid 8015C 751888680-225959-12 SB-USTSW-4 Total/NA Solid 8015C 751888680-225959-14 SB-USTSW-6 Total/NA Solid 8015C 751888680-225959-15 SB-USTSW-7 Total/NA Solid 8015C 751888680-225959-16 SB-USTSW-8 Total/NA Solid 8015CMB 680-752410/7 Method Blank Total/NA Solid 8015CLCS 680-752410/5 Lab Control Sample Total/NA Solid 8015CLCSD 680-752410/6 Lab Control Sample Dup Total/NA Analysis Batch: 752712 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 751888680-225959-2 SB-UST-1-2 Total/NA Solid 8015C 751888680-225959-3 SB-UST-1-3 Total/NA Solid 8015C 751888680-225959-4 SB-UST-2-1 Total/NA Solid 8015C 751888680-225959-5 SB-UST-2-2 Total/NA Solid 8015C 751888680-225959-6 SB-UST-2-3 Total/NA Solid 8015C 751888680-225959-7 SB-CL-1 Total/NA Solid 8015C 751888680-225959-8 SB-FD-1 Total/NA Solid 8015C 751888680-225959-9 SB-USTSW-1 Total/NA Solid 8015C 751888680-225959-10 SB-USTSW-2 Total/NA Solid 8015C 751888680-225959-13 SB-USTSW-5 Total/NA Eurofins Savannah Page 29 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 GC VOA (Continued) Analysis Batch: 752712 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015CMB 680-752712/8 Method Blank Total/NA Solid 8015CLCS 680-752712/6 Lab Control Sample Total/NA Solid 8015CLCSD 680-752712/7 Lab Control Sample Dup Total/NA GC Semi VOA Prep Batch: 752235 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546680-225959-1 SB-UST-1-1 Total/NA Solid 3546680-225959-2 SB-UST-1-2 Total/NA Solid 3546680-225959-3 SB-UST-1-3 Total/NA Solid 3546680-225959-4 SB-UST-2-1 Total/NA Solid 3546680-225959-5 SB-UST-2-2 Total/NA Solid 3546680-225959-6 SB-UST-2-3 Total/NA Solid 3546680-225959-7 SB-CL-1 Total/NA Solid 3546680-225959-8 SB-FD-1 Total/NA Solid 3546680-225959-9 SB-USTSW-1 Total/NA Solid 3546680-225959-10 SB-USTSW-2 Total/NA Solid 3546680-225959-11 SB-USTSW-3 Total/NA Solid 3546680-225959-12 SB-USTSW-4 Total/NA Solid 3546680-225959-13 SB-USTSW-5 Total/NA Solid 3546680-225959-14 SB-USTSW-6 Total/NA Solid 3546680-225959-15 SB-USTSW-7 Total/NA Solid 3546680-225959-16 SB-USTSW-8 Total/NA Solid 3546MB 680-752235/17-A Method Blank Total/NA Solid 3546LCS 680-752235/18-A Lab Control Sample Total/NA Solid 3546680-225959-1 MS SB-UST-1-1 Total/NA Solid 3546680-225959-1 MSD SB-UST-1-1 Total/NA Analysis Batch: 752554 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 752235680-225959-1 SB-UST-1-1 Total/NA Solid 8015C 752235680-225959-4 SB-UST-2-1 Total/NA Solid 8015C 752235680-225959-7 SB-CL-1 Total/NA Solid 8015C 752235680-225959-9 SB-USTSW-1 Total/NA Solid 8015C 752235680-225959-10 SB-USTSW-2 Total/NA Solid 8015C 752235680-225959-13 SB-USTSW-5 Total/NA Solid 8015C 752235680-225959-14 SB-USTSW-6 Total/NA Solid 8015C 752235680-225959-15 SB-USTSW-7 Total/NA Solid 8015C 752235680-225959-16 SB-USTSW-8 Total/NA Solid 8015C 752235MB 680-752235/17-A Method Blank Total/NA Solid 8015C 752235LCS 680-752235/18-A Lab Control Sample Total/NA Solid 8015C 752235680-225959-1 MS SB-UST-1-1 Total/NA Solid 8015C 752235680-225959-1 MSD SB-UST-1-1 Total/NA Analysis Batch: 752741 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 752235680-225959-2 SB-UST-1-2 Total/NA Solid 8015C 752235680-225959-3 SB-UST-1-3 Total/NA Solid 8015C 752235680-225959-5 SB-UST-2-2 Total/NA Solid 8015C 752235680-225959-6 SB-UST-2-3 Total/NA Eurofins Savannah Page 30 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 QC Association Summary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 GC Semi VOA (Continued) Analysis Batch: 752741 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 752235680-225959-8 SB-FD-1 Total/NA Solid 8015C 752235680-225959-11 SB-USTSW-3 Total/NA Solid 8015C 752235680-225959-12 SB-USTSW-4 Total/NA General Chemistry Analysis Batch: 752222 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture680-225959-1 SB-UST-1-1 Total/NA Solid Moisture680-225959-2 SB-UST-1-2 Total/NA Solid Moisture680-225959-3 SB-UST-1-3 Total/NA Solid Moisture680-225959-4 SB-UST-2-1 Total/NA Solid Moisture680-225959-5 SB-UST-2-2 Total/NA Solid Moisture680-225959-6 SB-UST-2-3 Total/NA Solid Moisture680-225959-7 SB-CL-1 Total/NA Solid Moisture680-225959-8 SB-FD-1 Total/NA Solid Moisture680-225959-9 SB-USTSW-1 Total/NA Solid Moisture680-225959-10 SB-USTSW-2 Total/NA Solid Moisture680-225959-11 SB-USTSW-3 Total/NA Solid Moisture680-225959-12 SB-USTSW-4 Total/NA Solid Moisture680-225959-13 SB-USTSW-5 Total/NA Solid Moisture680-225959-14 SB-USTSW-6 Total/NA Solid Moisture680-225959-15 SB-USTSW-7 Total/NA Solid Moisture680-225959-16 SB-USTSW-8 Total/NA Eurofins Savannah Page 31 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-UST-1-1 Lab Sample ID: 680-225959-1 Matrix: SolidDate Collected: 11/15/22 14:30 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-1-1 Lab Sample ID: 680-225959-1 Matrix: SolidDate Collected: 11/15/22 14:30 Percent Solids: 85.3Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.55 g 1 mL Analysis 8270E SIM 1 752485 11/28/22 17:04 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 6.162 g 5 mL Analysis 8015C 100 752410 11/27/22 17:27 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.43 g 1 mL Analysis 8015C 1 752554 11/28/22 23:08 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-UST-1-2 Lab Sample ID: 680-225959-2 Matrix: SolidDate Collected: 11/16/22 12:05 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-1-2 Lab Sample ID: 680-225959-2 Matrix: SolidDate Collected: 11/16/22 12:05 Percent Solids: 90.0Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.27 g 1 mL Analysis 8270E SIM 5 752727 11/30/22 00:59 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.668 g 5 mL Analysis 8015C 200 752712 11/29/22 15:11 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.30 g 1 mL Analysis 8015C 20 752741 11/29/22 14:33 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 32 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-UST-1-3 Lab Sample ID: 680-225959-3 Matrix: SolidDate Collected: 11/16/22 15:35 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-1-3 Lab Sample ID: 680-225959-3 Matrix: SolidDate Collected: 11/16/22 15:35 Percent Solids: 80.7Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.28 g 1 mL Analysis 8270E SIM 10 752727 11/30/22 01:22 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.37 g 5 mL Analysis 8015C 1000 752712 11/29/22 15:54 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.35 g 1 mL Analysis 8015C 50 752741 11/29/22 21:29 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-UST-2-1 Lab Sample ID: 680-225959-4 Matrix: SolidDate Collected: 11/15/22 11:45 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-2-1 Lab Sample ID: 680-225959-4 Matrix: SolidDate Collected: 11/15/22 11:45 Percent Solids: 80.0Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.45 g 1 mL Analysis 8270E SIM 1 752485 11/28/22 18:12 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.483 g 5 mL Analysis 8015C 100 752712 11/29/22 13:02 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.81 g 1 mL Analysis 8015C 1 752554 11/28/22 23:54 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 33 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-UST-2-2 Lab Sample ID: 680-225959-5 Matrix: SolidDate Collected: 11/16/22 11:40 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-2-2 Lab Sample ID: 680-225959-5 Matrix: SolidDate Collected: 11/16/22 11:40 Percent Solids: 90.0Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00DL EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.74 g 1 mL Analysis 8270E SIM DL 50 752826 11/30/22 07:58 NED EET SAVTotal/NA 1 mL 1 mL CMSXInstrument ID: Prep 3546 752003 11/22/22 18:00 MJ EET SAVTotal/NA 15.74 g 1 mL Analysis 8270E SIM 10 752727 11/30/22 01:44 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.158 g 5 mL Analysis 8015C 1000 752712 11/29/22 16:15 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.83 g 1 mL Analysis 8015C 50 752741 11/29/22 15:04 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-UST-2-3 Lab Sample ID: 680-225959-6 Matrix: SolidDate Collected: 11/16/22 13:20 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-UST-2-3 Lab Sample ID: 680-225959-6 Matrix: SolidDate Collected: 11/16/22 13:20 Percent Solids: 81.8Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.34 g 1 mL Analysis 8270E SIM 5 752727 11/30/22 02:07 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.275 g 5 mL Analysis 8015C 100 752712 11/29/22 14:06 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.34 g 1 mL Analysis 8015C 20 752741 11/29/22 15:20 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 34 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-CL-1 Lab Sample ID: 680-225959-7 Matrix: SolidDate Collected: 11/17/22 11:50 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-CL-1 Lab Sample ID: 680-225959-7 Matrix: SolidDate Collected: 11/17/22 11:50 Percent Solids: 97.0Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.39 g 1 mL Analysis 8270E SIM 1 752485 11/28/22 19:20 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.726 g 5 mL Analysis 8015C 100 752712 11/29/22 13:45 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.71 g 1 mL Analysis 8015C 1 752554 11/29/22 00:40 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-FD-1 Lab Sample ID: 680-225959-8 Matrix: SolidDate Collected: 11/17/22 09:50 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-FD-1 Lab Sample ID: 680-225959-8 Matrix: SolidDate Collected: 11/17/22 09:50 Percent Solids: 87.4Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.28 g 1 mL Analysis 8270E SIM 100 752826 11/30/22 08:23 NED EET SAVTotal/NA 1 mL 1 mL CMSXInstrument ID: Prep 3546 DL2 752003 11/22/22 18:00 MJ EET SAVTotal/NA 15.28 g 1 mL Analysis 8270E SIM DL2 200 753207 12/01/22 17:57 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.267 g 5 mL Analysis 8015C 500 752712 11/29/22 15:32 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.69 g 1 mL Analysis 8015C 50 752741 11/29/22 15:35 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 35 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-USTSW-1 Lab Sample ID: 680-225959-9 Matrix: SolidDate Collected: 11/15/22 13:25 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-1 Lab Sample ID: 680-225959-9 Matrix: SolidDate Collected: 11/15/22 13:25 Percent Solids: 89.5Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.59 g 1 mL Analysis 8270E SIM 1 752485 11/28/22 20:06 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 3.429 g 5 mL Analysis 8015C 100 752712 11/29/22 13:24 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.30 g 1 mL Analysis 8015C 1 752554 11/29/22 01:10 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-USTSW-2 Lab Sample ID: 680-225959-10 Matrix: SolidDate Collected: 11/16/22 10:05 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-2 Lab Sample ID: 680-225959-10 Matrix: SolidDate Collected: 11/16/22 10:05 Percent Solids: 88.5Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.31 g 1 mL Analysis 8270E SIM 1 752485 11/28/22 20:28 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.751 g 5 mL Analysis 8015C 100 752712 11/29/22 14:28 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.31 g 1 mL Analysis 8015C 1 752554 11/29/22 01:26 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 36 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-USTSW-3 Lab Sample ID: 680-225959-11 Matrix: SolidDate Collected: 11/16/22 15:15 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-3 Lab Sample ID: 680-225959-11 Matrix: SolidDate Collected: 11/16/22 15:15 Percent Solids: 75.4Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.33 g 1 mL Analysis 8270E SIM 5 752727 11/30/22 02:52 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.042 g 5 mL Analysis 8015C 100 752410 11/27/22 21:02 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.49 g 1 mL Analysis 8015C 20 752741 11/29/22 15:51 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-USTSW-4 Lab Sample ID: 680-225959-12 Matrix: SolidDate Collected: 11/16/22 15:25 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-4 Lab Sample ID: 680-225959-12 Matrix: SolidDate Collected: 11/16/22 15:25 Percent Solids: 69.0Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.51 g 1 mL Analysis 8270E SIM 10 752727 11/30/22 03:15 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.429 g 5 mL Analysis 8015C 100 752410 11/27/22 21:24 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.31 g 1 mL Analysis 8015C 20 752741 11/29/22 16:06 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 37 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-USTSW-5 Lab Sample ID: 680-225959-13 Matrix: SolidDate Collected: 11/16/22 14:10 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-5 Lab Sample ID: 680-225959-13 Matrix: SolidDate Collected: 11/16/22 14:10 Percent Solids: 87.1Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.62 g 1 mL Analysis 8270E SIM 1 752727 11/30/22 03:38 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.765 g 5 mL Analysis 8015C 100 752712 11/29/22 14:49 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.29 g 1 mL Analysis 8015C 1 752554 11/29/22 02:12 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-USTSW-6 Lab Sample ID: 680-225959-14 Matrix: SolidDate Collected: 11/16/22 13:30 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-6 Lab Sample ID: 680-225959-14 Matrix: SolidDate Collected: 11/16/22 13:30 Percent Solids: 86.5Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.23 g 1 mL Analysis 8270E SIM 1 752727 11/30/22 04:00 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.615 g 5 mL Analysis 8015C 100 752410 11/27/22 22:06 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.20 g 1 mL Analysis 8015C 1 752554 11/29/22 02:27 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Eurofins Savannah Page 38 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Lab Chronicle Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Client Sample ID: SB-USTSW-7 Lab Sample ID: 680-225959-15 Matrix: SolidDate Collected: 11/16/22 10:25 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-7 Lab Sample ID: 680-225959-15 Matrix: SolidDate Collected: 11/16/22 10:25 Percent Solids: 75.9Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.27 g 1 mL Analysis 8270E SIM 1 752727 11/30/22 04:23 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 5.212 g 5 mL Analysis 8015C 100 752410 11/27/22 22:28 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.79 g 1 mL Analysis 8015C 1 752554 11/29/22 02:42 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Client Sample ID: SB-USTSW-8 Lab Sample ID: 680-225959-16 Matrix: SolidDate Collected: 11/15/22 15:40 Date Received: 11/19/22 06:00 Analysis Moisture TD11/23/22 17:381 EET SAV752222 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Instrument ID:NOEQUIP Client Sample ID: SB-USTSW-8 Lab Sample ID: 680-225959-16 Matrix: SolidDate Collected: 11/15/22 15:40 Percent Solids: 81.8Date Received: 11/19/22 06:00 Prep 3546 MJ11/22/22 18:00 EET SAV752003 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.32 g 1 mL Analysis 8270E SIM 1 752727 11/30/22 04:46 NED EET SAVTotal/NA 1 mL 1 mL CMSYInstrument ID: Prep 5035A 751888 11/22/22 09:57 FES EET SAVTotal/NA 4.239 g 5 mL Analysis 8015C 100 752410 11/27/22 22:49 DBM EET SAVTotal/NA 5 mL 5 mL CVGWFID1Instrument ID: Prep 3546 752235 11/23/22 18:30 MJ EET SAVTotal/NA 30.51 g 1 mL Analysis 8015C 1 752554 11/29/22 02:58 JCK EET SAVTotal/NA 1 mL 1 mL CSGAB1Instrument ID: Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 39 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Accreditation/Certification Summary Client: TRC Environmental Corporation Job ID: 680-225959-1 Project/Site: Greensboro, NC - Nov 2022 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 269 12-31-22 Eurofins Savannah Page 40 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Method Summary Job ID: 680-225959-1Client: TRC Environmental Corporation Project/Site: Greensboro, NC - Nov 2022 Method Method Description LaboratoryProtocol SW8468270E SIM Semivolatile Organic Compounds (GC/MS SIM)EET SAV SW8468015CNonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)EET SAV SW8468015CNonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)EET SAV EPAMoisturePercent Moisture EET SAV SW8463546Microwave Extraction EET SAV SW8465035AClosed System Purge & Trap/Field Methanol EET SAV Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 41 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 Page 42 of 44 12/5/2022 1234567 8 9 10 11 12 Page 43 of 44 12/5/2022 1234567 8 9 10 11 12 Login Sample Receipt Checklist Client: TRC Environmental Corporation Job Number: 680-225959-1 Login Number: 225959 Question Answer Comment Creator: Givens, Keshia List Source: Eurofins Savannah List Number: 1 Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time (excluding tests with immediate HTs) Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. Eurofins Savannah Page 44 of 44 12/5/2022 1 2 3 4 5 6 7 8 9 10 11 12 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 35 Appendix G Geologic Logs for Borings (related to supplemental investigation only) MC MC MC MC MC MC 50 100 100 100 100 75 SW-SM SP-SM SW SP 3.0 8.0 10.0 11.0 25.0 0 '- 3 ' Asphalt and gravel. 8 '- 10 ' (SP-SM) Grey and brown, SILTY UNSORTED SAND (SP-SM), dry, petroleum odor. 10 '- 11 ' (SW) Tan, FINE SAND (SW), dry, petroleum odor. petroleum odor. Refusal at 27.0 feet.Bottom of borehole at 27.0 feet. Top of casing Grout 2" Sch. 40PVC Bentonite Seal Morrie #2 Silica Sand0.01- Slot 2"Sch. 40 PVC End Screen,End Boring PID = 66 PID = 13 PID = 53 PID = 105 PID = 145 PID = 89 PID = 312 PID = 280 PID = 183 PID = 253 PID = 178 PID = 255 PID = 103 PID = 85 NOTES Analytical sample collected from 11 to 12 ft. bgs. Refusal at 27' GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Hollow Stem Auger HOLE SIZE 4 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/19/21 COMPLETED 12/19/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING 16.50 ft DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 WELL NUMBER MW-01/SB-01 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGWELL DIAGRAM EnvironmentalData3 '- 8 ' (SW-SM) Tan, SILTY FINE SAND (SW-SM), dry, petroleum odor. PID = 136 PROJECT NUMBER 463648.0000.0000 11 '- 25 ' (SP) Light brown, tan, and gray, UNSORTED SAND (SP), dry, MC MC MC MC MC MC 30 20 20 0 80 250 GP SP SW SP CL 1.0 15.0 20.0 25.0 27.0 29.0 30.0 0 '- 1 ' Asphalt. 1 '- 15 ' (GP) Grey, SANDY GRAVEL (GP), dry, no odor. 15 '- 20 ' No Recovery. 20 '- 25 ' (SP) Tan and white, UNSORTED SAND (SP), dry, no odor. 25 '- 27 ' (SW) Dark brown, MEDIUM SAND (SW), dry, no odor. 27 '- 29 ' (SP) Tan and white, UNSORTED SAND (SP), moist, no odor. 29 '- 30 ' (CL) Medium brown, CLAY (CL), moist, no odor. Bottom of borehole at 30.0 feet. Top of casing Grout 2" Sch. 40 PVC Bentonite Seal Morrie #2Silica Sand 0.01- Slot 2"Sch. 40 PVC End Screen,End Boring PID = 0.3 PID = 0.3 PID = 0 PID = 10.4 PID = 9.5 PID = 45 PID = 80 PID = 10.6 NOTES Analytical sample collected from 20 to 21 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Hollow Stem Auger HOLE SIZE 4 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING 16.92 ft DEPTH(ft)0 5 10 15 20 25 30 SAMPLE TYPENUMBERPAGE 1 OF 1 WELL NUMBER MW-02 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGWELL DIAGRAM EnvironmentalDataPID = 280 PROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 60 80 80 100 100 SP SW-SM 1.0 20.0 25.0 0 '- 1 ' Concrete. 20 '- 25 ' (SW-SM) Light tan and white, MEDIUM SAND WITH SILT (SW-SM), dry, petroleum odor. Bottom of borehole at 25.0 feet. PID = 0 PID = 10 PID = 57 PID = 48 PID = 48 PID = 22 PID = 16 PID = 74 PID = 55 PID = 20 PID = 15.5 PID = 4.5 PID = 0 NOTES Analytical sample collected from 15 to 16 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/19/21 COMPLETED 12/19/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-02 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 2 '- 20 ' (SP) Light tan and white, UNSORTED SAND (SP) with some gravel, dry, petroleum odor. MC MC MC MC MC MC 100 80 100 100 80 100 SP SP SW- SM 10.0 23.0 26.0 0 '- 10 ' (SP) Tan and white, UNSORTED SAND (SP), dry, petroleum odor. 10 '- 23 ' (SP) Tan and white, UNSORTED SAND (SP) with some fine gravel, dry until moist at 20', petroleum odor. 23 '- 26 ' (SW-SM) Medium brown, FINE SAND WITH SILT (SW-SM), moist, petroleum. Refusal at 26.0 feet. Bottom of borehole at 26.0 feet. PID = 26.8 PID = 30 PID = 77 PID = 133 PID = 145 PID = 145 PID = 207 PID = 195 PID = 170 PID = 133 PID = 153 NOTES Analytical sample collected from 16 to 17 ft. bgs. Refusal at 26' GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/19/21 COMPLETED 12/19/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-03 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 60 100 100 100 100 SP-SM SW-SM 1.0 8.0 25.0 0 '- 1 ' Concrete. 1 '- 8 ' (SP-SM) Tan to light brown, FINE TO MEDIUM SAND WITH SILT (SP-SM), dry, no odor. 8 '- 25 ' (SW-SM) Light tan, UNSORTED SAND, dry until moist at 21', no odor. Bottom of borehole at 25.0 feet. PID = 9.3 PID = 1.5 PID = 0 PID = 1.5 NOTES Analytical sample collected from 20 ro 21 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/19/21 COMPLETED 12/19/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-04 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 80 80 100 30 50 SP SP 1.0 10.0 25.0 0 '- 1 ' Asphalt. 1 '- 10 ' (SP) Tan and white, UNSORTED SAND (SP) with gravel, dry, no odor. 10 '- 25 ' (SP) Brown, UNSORTED SAND (SP), dry until moist at 19', no odor. Bottom of borehole at 25.0 feet. PID = 0 PID = 0 PID = 0 PID = 1.5 NOTES Analytical sample collected from 18 to 19 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-05 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 80 50 80 100 100 SW-SM SP SW-SM SP 1.0 3.0 8.0 12.0 25.0 0 '- 1 ' Asphalt and fill. 1 '- 3 ' (SW-SM) Tan, SILTY FINE SAND (SW-SM), damp, no odor. 3 '- 8 ' (SP) Tan and white, UNSORTED SAND (SP) with gravel, dry, no odor. 8 '- 12 ' (SW-SM) Tan, SILTY FINE SAND (SW-SM), damp, no odor. 12 '- 25 ' (SP) Tan and white, UNSORTED SAND (SP), damp until saturation at 18.5', no odor. Bottom of borehole at 25.0 feet. PID = 0 PID = 0 PID = 0 PID = 0 NOTES Analytical sample collected from 18 to 19 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-06 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 50 50 40 100 60 SP SP SP 1.0 10.0 13.0 25.0 0 '- 1 ' Asphalt and fill. 1 '- 10 ' (SP) Tan and white, UNSORTED SAND (SP) with some gravel, moist, no odor. 10 '- 13 ' (SP) Tan and white, FINE TO MEDIUM SAND (SP), moist, no odor. 13 '- 25 ' (SP) Tan and white, UNSORTED SAND (SP) with some gravel, moist, no odor. Bottom of borehole at 25.0 feet. PID = 0 PID = 0 PID = 0 PID = 0 NOTES Analytical sample collected from 17 to 18 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-07 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC MC MC 40 50 60 60 100 SP SP 1.0 8.0 25.0 0 '- 1 ' Asphalt and gravel. 1 '- 8 ' (SP) Light brown, FINE SAND (SW), moist, no odor. 8 '- 25 ' (SP) Tan and white, UNSORTED SAND (SP), moist until saturation at 18', no odor. Bottom of borehole at 25.0 feet. PID = 0 PID = 0 PID = 0 PID = 0 NOTES Analytical sample collected from 17 to 18 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-08 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC 40 80 100 SP 1.0 15.0 0 '- 1 ' Concrete. 1 '- 15 ' (SP) Tan and white, UNSORTED SAND (SP), dry, no odor. Bottom of borehole at 15.0 feet. PID = 10.3 PID = 3.4 PID = 3.5 PID = 3.5 PID = 0.6 PID = 0.1 PID = 0.2 PID = 0.2 NOTES Analytical sample collected from 11 to 12 ft bgs. GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/21/21 COMPLETED 12/21/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0.0 2.5 5.0 7.5 10.0 12.5 15.0 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-09 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 MC MC MC 40 80 80 SP SP SW 7.0 12.0 15.0 0 '- 7 ' (SP) Tan, SILTY SAND (SP-SM), dry, petroleum odor. 7 '- 12 ' (SP) Tan, UNSORTED SAND (SP), dry, no odor. 12 '- 15 ' (SW) Tan, FINE SAND WITH SILT, moist, no odor. Bottom of borehole at 15.0 feet. PID = 50.5 PID = 53.3 PID = 5.5 PID = 4 PID = 0.5 PID = 0.9 NOTES Analytical sample collected from 11 to 12 ft bgs. GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Direct Push HOLE SIZE 2 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/21/21 COMPLETED 12/21/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING ---DEPTH(ft)0.0 2.5 5.0 7.5 10.0 12.5 15.0 SAMPLE TYPENUMBERPAGE 1 OF 1 BORING NUMBER SB-10 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE LOGS_REV01.GPJRECOVERY %U.S.C.S.MATERIAL DESCRIPTION GRAPHICLOGEnvironmentalDataPROJECT NUMBER 463648.0000.0000 \\greenville-fp1\WPGVL\PJT2\463648\0000\000003\IAA\Initial Abatement Action Report - Greensboro.docx 36 Appendix H Monitoring Well Construction Forms (for all wells constructed to date) Top of casing Grout 2" Sch. 40PVC Bentonite Seal Morrie #2 Silica Sand0.01- Slot 2"Sch. 40 PVC End Screen,End Boring NOTES Analytical sample collected from 11 to 12 ft. bgs. Refusal at 27' GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Hollow Stem Auger HOLE SIZE 4 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/19/21 COMPLETED 12/19/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING 16.50 ft DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 WELL NUMBER MW-01 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE MW LOGS.GPJMATERIAL DESCRIPTION GRAPHICLOGWELL DIAGRAM PROJECT NUMBER 463648.0000.0000 Top of casing Grout 2" Sch. 40PVC Bentonite Seal Morrie #2 Silica Sand 0.01- Slot 2" Sch. 40 PVC End Screen, End Boring NOTES Analytical sample collected from 20 to 21 ft. bgs GROUND ELEVATION LOGGED BY Caitlin Serowik DRILLING METHOD Hollow Stem Auger HOLE SIZE 4 inch DRILLING CONTRACTOR Parratt-Wolff GROUND WATER LEVELS: CHECKED BY David Syznal DATE STARTED 12/20/21 COMPLETED 12/20/21 AT TIME OF DRILLING --- AT END OF DRILLING --- AFTER DRILLING 16.92 ft DEPTH(ft)0 5 10 15 20 25 SAMPLE TYPENUMBERPAGE 1 OF 1 WELL NUMBER MW-02 PROJECT NAME TForce-Greensboro PROJECT LOCATION Greensboro, NC CLIENT TForce GENERAL BH / TP / WELL - TRC_WINDSOR_STD.GDT - 1/31/23C:\USERS\CSEROWIK\ONEDRIVE - TRC\DESKTOP\GREENSBORO TFORCE MW LOGS.GPJMATERIAL DESCRIPTION GRAPHICLOGWELL DIAGRAM PROJECT NUMBER 463648.0000.0000 WELL CONSTRUCTION RECORD Guilford County Division of Environmental Health 1. Site Name: ______________________________________________________ Well #: ___________ 2. Well Location: ___________________________________________________________________ 3. GPS Location latitude (decimal degrees):_______________ longitude (decimal degrees): ______________ 4. Type of Well: monitoring ___ air injection ___ air sparging ___ groundwater recovery ___ SVE ___ 5. Depth of Well: ____ feet 6. Diameter of Well: ___ inches 7. Depth of Water Table below Top of Casing: _____ feet 8. Well Casing: Depth Material Depth Drilling Log from ____to ____ft _________________ From To Formation Description __________ ________________ from ____to ____ft _________________ __________ ________________ 9. Screen Interval: from ____ to ____ ft __________ ________________ 10. Grout: depth material __________ ________________ from ____to ____ft _________________ __________ ________________ from ____to ____ft _________________ __________ ________________ 11. Gravel or sand pack interval: from ___ to ___ ft __________ ________________ 12. How is the well secured? ___________________________ 13. Well Construction Date: beginning: _____________ completion: ____________ 14. Remarks: ___________________________________________________________________________ I do hereby certify that this well was constructed in accordance with the Guilford County Well Rules and a copy of this record has been provided to the well owner. ______________________________________________________ Signature of Contractor or Agent Date 01.10.2023 WELL CONSTRUCTION RECORD Guilford County Division of Environmental Health 1. Site Name: ______________________________________________________ Well #: ___________ 2. Well Location: ___________________________________________________________________ 3. GPS Location latitude (decimal degrees):_______________ longitude (decimal degrees): ______________ 4. Type of Well: monitoring ___ air injection ___air sparging ___ groundwater recovery ___ SVE ___ 5. Depth of Well: ____ feet 6. Diameter of Well: ___ inches 7. Depth of Water Table below Top of Casing: _____ feet 8. Well Casing:Depth Material Depth Drilling Log from ____to ____ft _________________ From To Formation Description __________ ________________ from ____to ____ft _________________ __________ ________________ 9. Screen Interval: from ____ to ____ ft __________ ________________ 10. Grout:depth material __________ ________________ from ____to ____ft _________________ __________ ________________ from ____to ____ft _________________ __________ ________________ 11. Gravel or sand pack interval: from ___ to ___ ft __________ ________________ 12. How is the well secured? ___________________________ 13. Well Construction Date: beginning: _____________ completion: ____________ 14. Remarks: ___________________________________________________________________________ I do hereby certify that this well was constructed in accordance with the Guilford County Well Rules and a copy of this record has been provided to the well owner. ______________________________________________________ Signature of Contractor or Agent Date 01.10.2023