WS-29296_48461_CA_SCH_20230118_SCH-Revised

Initial Abatement Action Report-
Revised
D&M Grocery; Incident No.: 48461
6066 NC 704 Highway East, Sandy
Ridge, North Carolina
S&ME Project No. 22580285
PREPARED FOR:
Huffman Oil Company
P.O. Box 730
Burlington, NC 27216-0730
PREPARED BY:
S&ME, Inc.
8646 W Market St, Ste 105
Greensboro, North Carolina 27409
January 18, 2023

S&ME, Inc. | 8646 W Market St, Ste 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com

January 18, 2023
Huffman Oil Company
P.O. Box 730
Burlington, North Carolina 27216-0730
Attention: Mr. James Barnwell, III
Reference: Initial Abatement Action Report-Revised
D&M Grocery; Incident No.: 48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

Dear Mr. Barnwell:
S&ME Inc. (S&ME) is providing this revised Initial Abatement Action Report to summarize the provided
environmental services related to the underground storage tank (UST) system at D&M Grocery in Sandy Ridge,
North Carolina. S&ME performed services in general accordance with S&ME Proposal number 22580285B, dated
October 27, 2022, and the existing Master Service Agreement between S&ME and Huffman Oil Company
(Huffman Oil) dated July 30, 2015.
If you have any questions, or if we can be of any additional service, please feel free to contact us.
Sincerely,
S&ME, Inc.

Lyndal Butler Wayne Watterson, P.E.
Environmental Scientist Senior Engineer

Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 i

Table of Contents
1.0 Site Identification .................................................................................................. 1
2.0 Executive Summary ............................................................................................... 2
2.1 Source, Discovery Date, Quantity and Type of Contaminant Released ................... 2
2.2 Initial Abatement Actions................................................................................................ 2
2.3 Hydrogeological Results .................................................................................................. 2
2.4 Assessment Results .......................................................................................................... 2
2.5 Risk Classification ............................................................................................................. 3
2.6 Remediation Levels .......................................................................................................... 4
3.0 Site History and Characterization ...................................................................... 4
3.1 General ............................................................................................................................... 4
3.2 UST Owner and System Data ......................................................................................... 4
3.3 Above Ground Storage Tanks......................................................................................... 5
3.4 Release Description .......................................................................................................... 5
4.0 Site Check ............................................................................................................... 6
4.1 Release Reporting ............................................................................................................. 6
4.2 Tank and Line Tightness Testing ................................................................................... 6
4.3 Site Check Procedures ...................................................................................................... 6
4.4 Initial Site Investigation ................................................................................................... 6
4.4.1 Soil Sampling ...................................................................................................................... 6
4.4.2 Water Sampling................................................................................................................... 7
4.5 Free Product ...................................................................................................................... 7
4.6 Groundwater Occurrence and Flow Direction ............................................................. 7
4.7 Analytical Results ............................................................................................................. 8
4.7.1 Soil ....................................................................................................................................... 8
4.7.2 Groundwater ....................................................................................................................... 8
4.8 Assessment Conclusions.................................................................................................. 8
5.0 Preliminary Receptor Information ..................................................................... 9
6.0 Initial Response and Abatement Action ........................................................... 9
7.0 Conclusions and Recommendations ............................................................... 10
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 ii

List of Figures
1 US Topo Map
2 Site Map
3 Site Detail
4 Soil Boring Locations
5 Groundwater Elevation Contour Map (July 26, 2022)
6 Groundwater Elevation Contour Map (November 28, 2022)
7 Soil Analytical Summary
8 Groundwater Analytical Results

List of Additional Tables
1 Summary of Water Supply Well Sampling Results
2 Field Screening Results
3 Summary of Soil Sampling Results
4 Monitor Well Construction and Liquid Level Data
5 Summary of Groundwater Sampling Results

Appendices
Appendix I - Tank Tightness Test Results and UST Inspection Report
Appendix II - Boring Logs, Well Construction Details and Well Construction Records
Appendix III - Groundwater Sampling Forms and Environmental Field Report
Appendix IV - Analytical Reports

Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 2
2.0 Executive Summary
2.1 Source, Discovery Date, Quantity and Type of Contaminant Released
The suspected release source is the underground storage tank (UST) system operating at the D&M Mart
located at 6066 NC 704 Highway East. The release was discovered on May 25, 2022, upon receipt of the
analytical results for a water sample collected from a water supply well located on an adjoining property
at 6080 NC 704 Highway East. Based on the supply well analytical results, the nature of the release is
gasoline. The release quantity is unknown.
2.2 Initial Abatement Actions
Huffman Oil Company temporarily closed the 2,000-gallon premium gasoline UST (UST-1) by removing
product from the tank. UST-1 was last operated on February 20, 2017, and was placed in temporary
closure when it would not siphon. The UST system at D&M Grocery was reported as in compliance during
the most recent inspections performed by North Carolina Department of Environmental Quality (NCDEQ)
during August 2021, and on June 8, 2022. A copy of 00-0-0000009253_UST-10B_20220608 is included in
Appendix I. S&ME is not aware of an equipment failure that may have resulted in a release from the
current UST system.

Tank tightness and line tightness testing performed on May 31, 2022, resulted in passing tests for tanks
and product lines, including UST-1. A copy of the test results is provided as Appendix I.

On July 8, 2022, an alternate water source was provided to the residence located at 6080 NC 704 Highway
East by disconnection from the water supply well located on the property, and connection of the
residence to the water supply well serving 6066 NC 704 Highway East (subject property). The well serving
D&M Mart is located on an adjoining property approximately 525 feet from the UST system.
Free product, or light non-aqueous phase liquids (LNAPL) and water were evacuated from monitoring well
MW-1 by hand bailing approximately 3 to 5 gallons each on August 31, 2022, October 5, 2022, and
January 3, 2023.
2.3 Hydrogeological Results
Groundwater occurrence underlying the UST system ranged from approximately 31 feet to 33.5 feet
below ground surface in monitoring well MW-1 on July 26, 2022, August 31, 2022, October 5, 2022,
November 28, 2022, and January 3, 2023. Groundwater occurs above the top of bedrock. The
approximate groundwater flow direction on July 26 and November 28, 2022, was to the south southwest.
2.4 Assessment Results
Gasoline range organics (GRO) were reported at concentrations greater than the action level for soil
samples collected from soil borings MW-1 and P1. GRO and diesel range organics (DRO) were reported
at concentrations less than the respective action levels in soil samples collected from multiple soil borings.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 3
Multiple volatile organic compounds (VOCs) were reported at concentrations greater than the
corresponding soil-to-groundwater Maximum Soil Contaminant Concentrations (MSCCs) for soil samples
collected from soil borings MW-1, MW-2, MW-3, P-1 and P10, representing the UST basin and dispensers.
VOC concentrations greater than the residential cleanup levels were reported in two soil samples
collected from soil boring MW-1. A VOC concentrations greater than the industrial/commercial cleanup
level was reported in one soil sample collected from soil boring MW-1. VOCs and semivolatile organic
compounds (SVOCs) were reported at concentrations less than the corresponding soil-to-groundwater
MSCCs in soil samples collected from multiple soil borings.
Free product, or light non-aqueous phase liquid, was observed in monitoring well MW-1 on July 20, 2022,
at a thickness of 0.19 feet. Free product was observed in MW-1, at thicknesses ranging from 1.43 feet to
3.59 feet on July 26, 2022, August 31, 2022, October 5, 2022, October 26, 2022, November 28, 2022, and
January 3, 2023 (Table 4).
Analysis of groundwater samples collected from monitoring wells MW-2 and MW-3 on July 20, 2022, each
installed in an apparent downgradient direction relative to the UST system, detected six VOCs and three
carbon-chain fractions at concentrations greater than the corresponding NCAC 2L groundwater quality
standards (2L Standards). No Gross Contamination Level exceedances were reported.
Surface water samples were not collected.
Based on the supply well and monitoring well analytical results, the nature of the release is gasoline.
Based on the analytical results representing the inactive water well located at 6080 NC 704 East, dissolved
phase VOCs impacted this receptor. With the exception of Method 625.1 detection of naphthalene,
dissolved phase SVOCs did not impact the receptor. Naphthalene was also detected in the sample at a
similar concentration by Method 6200B. Naphthalene is typically associated with semivolatile fuels, such
as diesel and kerosene, but naphthalene is also a constituent of gasoline at 0.15% to 0.18% by weight
(https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2922736/).
Dissolved phase VOCs have migrated horizontally to downgradient monitoring well MW-3, and to the
impacted water supply well located at 6080 NC 704 Highway East and approximately 150 feet south of the
dispenser islands. An alternate water source was provided and the impacted water well is inactive. The
extent of dissolved impacts exceeding the 2L groundwater quality standards and the rate of migration is
unknown.
On June 8, 2022, S&ME collected water samples from a water well located approximately 300 feet
southwest of the dispenser island, and at 6100 NC 704 East, and the water well serving the subject
property and located approximately 525 feet west southwest of the dispenser island. Methyl tert-butyl
ether was reported in the sample collected from the 6100 NC 704 East at an estimated concentration of
0.45 micrograms per liter. No target VOCs were reported in the water sample collected from the well
serving 6066 NC 704 East.
2.5 Risk Classification
The NCDEQ classified the incident as High Risk due to the observed presence of water supply wells
proximal to the source area. The incident risk ranking has not been determined.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 4
2.6 Remediation Levels
Remediation levels have not been determined, but the levels will likely be the soil-to-groundwater MSCCs
for soil, the 2L Standards for groundwater, and 0.1 foot thickness for free product.
3.0 Site History and Characterization
3.1 General
D&M Mart is located at 6066 NC 704 Highway East near Sandy Ridge, Stokes County, North Carolina
(Figure 1). The UST system is located on the property as depicted in Figure 2.
3.2 UST Owner and System Data
UST Owner
UST ID
No.
Facility ID
No.
Name of
Owner
Street Address Telephone Dates of
Operation
1 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 4-26-1962 –
2-20-2017
2, 3 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 4-26-1962 –
present
4 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 10-1-1989 –
present
5 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 5-3-1995 –
present

UST Information
Tank No. Last and
Previous
Contents
Capacity Construction
Details
Tank
Dimensions
Date Tank
Installed
1 Gasoline 2,000-gallons Single-wall steel 64” x 12 feet 4-26-1962
2 Gasoline 4,000-gallons Single-wall steel 64” x 24 feet 4-26-1962
3 Gasoline 3,000-gallons Single-wall steel 64” x 18 feet 4-26-1962
4 Kerosene 4,000-gallons Single-wall steel 64” x 24 feet 10-1-1989
5 Gasoline 8,000-gallons Single-wall steel/FRP 96” x 21’4” 5-3-1995
Status of
USTs
Description
of Piping and
Dispensers
Release from
UST System
Material Released Date of
Release
Release
Description
1 Temporarily
closed
Unknown Unknown Unknown Unknown
2, 3, 4, 5 Single-wall
FRP
Unknown Unknown Unknown Unknown

Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 5
The kerosene UST (Tank 4) and associated kerosene dispenser are located beside each other in the
southwest portion of the common UST basin, as shown on Figure 3. The inactive gasoline UST (Tank 1) is
located in the southeast corner of the common UST basin. Three active gasoline USTs (Tanks 2, 3, 5) are
located in the north portion of the common UST basin. Two gasoline dispensers adjoin the northeast
corner of the common UST basin. Product lines are located within the common UST basin, as identified
by the overlying concrete pavement system. The approximate locations of product lines, system control
conduits and vent lines are shown on Figure 3. Huffman Oil informed S&ME that the UST basin was
backfilled with aggregate (pea gravel). S&ME is not aware of prior releases or compliance issues related
to the current UST system.
The UST system at the subject property has been upgraded to meet current NCDEQ regulations. Huffman
Oil Company installed new fiberglass reinforced plastic (FRP) product lines for the UST system and
installed catchment basins at the USTs in May 1995. Containment sumps were added at the two gasoline
dispensers in May 1995.
3.3 Above Ground Storage Tanks
One active diesel above ground storage tank (AST) and associated dispenser, installed in about 2010, are
located approximately 100 feet northwest of the gasoline dispenser island (Figure 2).
One inactive, 500-gallon waste oil AST (installation date unknown) is located approximately 75 feet west
northwest of the gasoline dispenser island (Figure 2).
One inactive 250-gallon heating oil AST (installation date unknown) is located approximately 65 feet west
of the gasoline dispenser island (Figure 2).
3.4 Release Description
Mr. James Barnwell of Huffman Oil Company contacted Wayne Watterson of S&ME on May 23, 2022,
concerning well water with a reported petroleum-like odor on the adjoining Gary Sands property. S&ME
collected a water sample from the well located at 6080 NC 704 East on May 24, 2022. Analysis of the
sample resulted in VOC concentrations greater than the NCAC 2L Standards. A Health Risk Evaluation of
Water Supply (HRE) dated June 1, 2022, was provided by the NCDEQ to Mr. Gray Sands of 6080 NC 704
Highway East, in a letter dated June 2, 2022. The HRE stated that water is not recommended for any
residential use at this time. The residence located at 6080 NC 704 Highway East was disconnected from
the water well on the property, and the residence was connected to the water well serving 6066 NC 704
Highway East (subject property) on July 8, 2022.
S&ME returned to the site on June 8, 2022, to collect water samples from the water well serving 6066 NC
704 Highway East (subject property), and the well serving 6100 NC 704 East. VOCs were not detected in
the 6066 NC 704 East sample. Analysis of the samples resulted in one VOC in the 6100 NC 704 Highway
East sample at a concentration less than the NCAC 2L Standard. The approximate water supply well
locations are shown on Figure 2. Water supply well analytical results are summarized on Table 1.
Based on the water supply well analytical results, the apparent nature of the release is gasoline. S&ME is
not aware of historical releases on the subject property or of off-site releases near the subject property.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 6
4.0 Site Check
4.1 Release Reporting
S&ME submitted a 24-Hour Report, Form UST-61, to the North Carolina Department of Environmental
Quality (NCDEQ) on May 26, 2022. The NCDEQ issued a Notice of Regulatory Requirements dated
May 26, 2022, outlining the requirement to conduct tank tightness and line tightness testing of the UST
system, and to conduct a site check.
4.2 Tank and Line Tightness Testing
Tank and line tightness testing were performed on the operating UST system located at 6066 NC 704
Highway East for Huffman Oil Company by Precision Tank Service on May 31, 2022. The results of the
tank and line tightness testing indicated a passing results for all the tanks and lines. The results of the
tank and line tightness tests were submitted to Karen Hall of the NCDEQ on June 2, 2022, by James
Barnwell. A copy of the test results is provided in Appendix I.
4.3 Site Check Procedures
S&ME proposed to collect subsurface soil and groundwater samples on the subject property at apparent
downgradient locations relative to the operating UST system.
Based on the results of the compliance inspections performed on August 18, 2021 and on June 8, 2022,
and on the results of the tank and line tightness testing, actions for repair, replacement or upgrading of
the current UST system have not been performed. Soil excavation has not been performed.
4.4 Initial Site Investigation
S&ME was on-site with subcontractor Environmental Drilling & Probing Services to perform soil borings
and to install monitoring wells adjacent to the gasoline UST basin and dispenser islands.
4.4.1 Soil Sampling
To assess potential soil impacts from the UST system, four soil probes (MW-1, MW-2, MW-3 and P-1)
were performed at the site on July 18-19, 2022, and 17 additional soil probes (P-2 through P-18) were
performed on November 28-29, 2022. Soil boring locations are shown on Figure 4. Continuous soil
samples were collected to depths ranging from 20 feet to 45 feet below ground surface (bgs) using
direct-push methods. Boring logs for the soil probes are included in Appendix II. The results for
headspace screening for volatile organic vapors performed on grab soil samples collected at intervals of 5
feet with a photo-ionization detector (PID) are summarized on each boring log and on Table 2.
Soil samples from soil probes were selected for laboratory analysis, based on field observations and field
screening results. Selected samples were transferred by hand using Nitrile gloves to laboratory-provided
containers and were placed in a chilled cooler under chain-of-custody procedures. Soil samples collected
on July 18-19, 2022, were shipped to Eurofins analytical laboratory and submitted for analysis for gasoline
range organics (GRO) by Method 8015 and for VOCs by Method 8260D, as summarized on Table 3. Soil
samples collected on November 28-29, 2022, were shipped to Eurofins analytical laboratory and
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 7
submitted for analysis for GRO and DRO by Method 8015, and for VOCs by Method 8260D and SVOCs by
Method 8270D, as summarized on Table 3.
4.4.2 Water Sampling
Surface water samples were not collected.
Soil borings performed by air rotary drilling methods to depths ranging from 40 feet bgs to 41 feet bgs
were converted to 2-inch diameter, PVC, Type II groundwater monitoring wells. The locations of
monitoring wells MW-1, MW-2 and MW-3 are shown on Figure 3. Screened intervals ranging in length
from 15 feet to 20 feet were installed in the lowermost portion of each boring. Each well was secured
with a locked, expandable cap and encased in a cover with bolt-down lid and flush-mount concrete pad.
Well Construction details are summarized on Table 4. Well Construction Details and Well Construction
Records for monitoring wells MW-1, MW-2 and MW-3, are included in Appendix II.
On July 20, 2022, groundwater samples were collected from monitoring wells MW-1, MW-2 and MW-3.
Depth to water measurements ranged from 32.60 feet below top of casing at MW-1, to 33.83 feet below
top of casing in MW-3. Free product, or light non-aqueous phase liquid, was detected in monitoring well
MW-1 at a depth of 31.65 feet below top of casing and at a thickness of 1.43 feet.
A submersible electric pump, using dedicated polyethylene tubing, was used to purge monitoring wells
MW-2 and MW-3 by evacuating greater than three well volumes of water from the well. Groundwater
Sampling Forms are provided in Appendix III. Each groundwater sample was transferred into laboratory-
provided containers using dedicated Nitrile gloves, placed into a cooler with ice, and shipped under
chain-of-custody procedures to Eurofins analytical laboratory. The groundwater samples were submitted
for analysis for volatile petroleum hydrocarbons (VPH) by the MADEP methods, for VOCs by EPA Methods
6200B and 504.1, and for Lead by EPA Method 6010, as summarized on Table 5.
On July 25, 2022, Eurofins informed S&ME that the commercial overnight carrier delivered the sample
container to the laboratory on July 23, 2022, and the sample containers exceeded the acceptable
temperature range (16.6º C).
4.5 Free Product
Free product was observed in monitoring well MW-1 on July 20, 2022, at a thickness of 0.19 feet. Free
product was observed in MW-1, at thicknesses ranging from 1.43 feet to 3.59 feet on July 26, 2022,
August 31, 2022, October 5, 2022, October 26, 2022, November 28, 2022 and January 3, 2023. Liquid level
data are summarized on Table 4.
4.6 Groundwater Occurrence and Flow Direction
S&ME measured the relative top of casing elevations of the monitoring wells. S&ME calculated the
relative water table elevation at each monitoring well location using the top of casing elevations and the
depth of water measurements from the top of casing in monitoring wells MW-2 and MW-3, and the
depth to free product and water measurements in monitoring well MW-1. S&ME calculated the direction
of groundwater flow, based on depth to groundwater elevations in monitoring wells MW-1, MW-2 and
MW-3, to be toward the south southwest from the source area.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 8
Estimated groundwater elevation contours representing liquid level data on July 26, 2022, and November
28, 2022, are shown on Figure 5 and Figure 6, respectively. Estimated hydraulic gradients of 0.059 feet
per foot and 0.055 feet per foot were calculated for July 26, 2022, and November 28, 2022, respectively.
Groundwater occurrence ranged from 0.79 feet to 1.04 feet lower in elevation on November 28, 2022,
relative to July 26, 2022. Liquid level data are summarized on Table 4.
4.7 Analytical Results
4.7.1 Soil
As summarized in Table 3 and shown on Figure 7, 35 soil samples were collected from 21 soil borings
performed on July 18-19 and November 28-29, 2022. The analytical report is provided in Appendix IV.
The analysis for of 35 soil samples collected from 21 soil borings, resulted in the detection of GRO at
concentrations greater than 50 milligrams per Kilogram (mg/Kg) in four soil samples collected from soil
borings MW-1 and P-1. GRO was detected in seven soil samples collected from soil borings MW-2, MW-
3, P-1 and P-17 at concentrations or estimated concentrations less than 50 mg/Kg. GRO was not detected
in 24 soil samples.
DRO was detected in 17 soil samples collected on November 28-29, 2022, at concentrations or estimated
concentrations less than 100 mg/Kg. DRO was not detected in three soil samples.
The analysis resulted in the detection of 13 VOCs at concentrations greater than the corresponding soil-
to-groundwater MSCCs in 11 soil samples collected from soil borings MW-1, MW-2, MW-3, P-1 and P-10.
Residential cleanup levels were exceeded for four VOCs in two soil samples collected from soil boring
MW-1. The industrial/commercial cleanup level was exceeded for naphthalene in soil sample MW-1-30,
collected from a depth of 30 feet in soil boring MW-1.
The analysis resulted in the detection of three SVOCs at estimated concentrations less than the
corresponding soil-to-groundwater MSCCs in three soil samples collected from soil borings P-3 and P-14.
4.7.2 Groundwater
As summarized in Table 5 and shown on Figure 8, multiple volatile organic compounds were reported at
concentrations greater than the corresponding 2L Standards in samples MW-2 and MW-3. One VOC not
typically associated with petroleum products, tetrachloroethene, was reported in sample MW-3 at a
concentration greater than the 2L Standard. Three carbon-chain fractions greater than the corresponding
2L Standards were reported in the groundwater sample collected from monitoring well MW-2.
The analytical report is provided in Appendix IV.
4.8 Assessment Conclusions
• Based on the presence of free product in monitoring well MW-1, the apparent source of the
release is related to UST-2 and product lines, or former product lines, located proximal to MW-1.
USTs and product lines received passing tests in May 2022.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 9
• Based on the soil analytical results, the apparent nature of the release is gasoline, and the source
of the release is related to UST-2 and product lines, or former product lines, located near the
dispensers. USTs and product lines received passing tests in May 2022. The horizontal migration
of soil impacts is indicated by the increased concentrations observed with increasing depths in
soil borings MW-1, MW-2, P-1 and P-10.
• Based on the presence of free product in monitoring well MW-1, the vertical extent of the release
is to the saturated zone. The horizontal extent of free product has not been determined;
however, free product was not detected in MW-2 located approximately 15 feet from MW-1 and
in a cross gradient position relative to MW-1.
• The horizontal and vertical extents of groundwater impacts are unknown.
• The horizontal extent of soil impacts is unknown; however, the concentration of benzene (0.0078
mg/Kg), relative to the soil-to-groundwater MSCC (0.0072 mg/Kg) observed at a depth of 25 feet
in soil boring P-10 is indicative of the horizontal extent of MSCC exceedance. MSCC and
GRO/DRO exceedances were not observed at depths ranging from 10 to 25 feet below ground
surface (ft-bgs) in soil borings P-2 through P-5 representing the gasoline dispensers. MSCC and
GRO/DRO exceedances were not observed at depths ranging from 16-25 ft-bgs in soil borings P-
6 through P-9, each located generally west and north and south, of UST-1, UST-2 and UST-3.
• With the exception of the analytical results for soil samples collected from boring MW-3 at depths
10 and 20 ft-bgs, MSCC exceedances were not reported for soil samples collected from soil
borings performed adjacent to UST-4, UST-5 and the diesel dispenser.
• The depth to consolidated material, or top of bedrock, is greater than 45 feet bgs.
• The depth to the saturated zone, is approximately 33 feet in the source area.
• Initial site check activities included soil and groundwater assessment, due to the presence of
apparent impacts in a water supply well located on an adjoining property.
• Surface water samples were not collected. The nearest surface water body appears to be greater
than 500 feet from the source area.
• Abatement actions required: recover free product from monitoring well MW-1.
• Need for further investigation or remediation: additional soil, free product and groundwater
assessment.
5.0 Preliminary Receptor Information
Water supply wells are located within 1,000 feet of the apparent source area at the D&M Grocery
property. As described in Section 3.4 above, S&ME collected water samples representing three water
supply wells observed within approximately 500 feet of the site, including 6066, 6080 and 6100 NC 704
Highway East (Figure 2). Apparent well structures were not observed at other properties developed near
the D&M site. S&ME is not aware of the availability of municipal water service to the area proximal to the
site; therefore, other properties, if occupied, likely use well water. The preliminary receptor information
indicates a High Risk ranking by NCDEQ.
6.0 Initial Response and Abatement Action
Huffman Oil Company removed product from the 2,000-gallon premium gasoline tank and placed Tank
UST-1 in temporary closure when product would not siphon.
Initial Abatement Action Report- Revised
D&M Grocery; Incident No. 48461
6066 NC 704 Highway East, Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285

January 18, 2023 10
Tank tightness and line tightness testing of the operating UST system performed on May 31, 2022,
resulted in passing tests for all tanks and product lines (Appendix I).
On July 15, 2022, the residence located at 6080 NC 704 Highway East was disconnected from the water
supply well located on the property, and the residence was connected to the water supply well serving
6066 NC 704 Highway East (subject property).
Limited free product recovery actions have been performed. Soil excavation has not been performed.
7.0 Conclusions and Recommendations
Based on the initial soil and groundwater assessment results, and on the presence of free product in the
subsurface, S&ME recommends performing a Limited Site Assessment. S&ME also recommends
delineating the horizontal extent of free product and performing free product recovery from monitoring
well MW-1.
The results of soil sampling activities to date, and the presence of free product in monitoring well MW-1,
suggest a release may have occurred in the area of product lines located near Tank-2 and Tank-3. A
release may have occurred prior to the replacement of product lines and the installation of tank and
dispenser sumps in 1995. Existing product piping is embedded in pea gravel. Periodic tightness testing
and tank inventory records suggest a release from the current UST system configuration has not occurred.
Although unlikely, a release may have occurred from piping at UST-1 that would have prevented
siphoning from Tank-1. Piping for Tank-1 is near the area of a suspected release, near Tank-2 and Tank-3,
and monitoring well MW-1. Tank-1 was taken out of service in February 2017, is currently empty and in
temporary closure.
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwgN
0 2000 4000
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
1
22580285
DEC. 2022
AS SHOWNUS TOPO MAP
SOURCE: AYERSVILLE, NC QUADRANGLE, 7.5-MINUTE SERIES US TOPO (2019).
SITE
LEGEND
- GROUNDWATER FLOW DIRECTION
OHL
N
0 200 400
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
2
22580285
DEC. 2022
AS SHOWNSITE MAP
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
6080 NC 740 HWY E
SITE
6100 NC 740 HWY E
DIESEL AST
WASTE OIL AST
HEATING OIL AST
SUBJECT PROPERTY WELL
LEGEND
- APPROXIMATE WATER SUPPLY WELL LOCATION
- APPROXIMATE UNDERGROUND STORAGE TANK BASIN LOCATION
- ABOVE GROUND STORAGE TANKAST
P
P PPPPC
C
C
C
C
C CCC C
C
C CCV
V
V
V
V
V
V
V
V
V
V V
V
V
V
V
VVVVVOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHL
N
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
3
22580285
DEC. 2022
AS SHOWNSITE DETAIL
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.
0 20 40
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
LEGEND
- APPROXIMATE DISPENSER LOCATION
- MONITORING WELL LOCATION
- PROPERTY BOUNDARY
- CONDUIT
- VENT LINE
- PRODUCT LINE
- OVERHEAD LINE
- UNDERGROUND STORAGE TANK
- UNDERGROUND STORAGE TANK NUMBER
C C
V V
P P
OHLOHL
1
2
3
1
5
4
MW-3
MW-2
MW-1
PPPPP
P
P
P
P
P
P P P
P
P
PCCCCCC
CCCC
C
C
C
C
C
C CCCCCCCC
C
C
C
C
CVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVV
V
V
POHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLPMW-3MW-2P-1MW-1FIGURE NO.Drawing path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwg
PROJECT NUMBERDATE:SCALE:N01020 (IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALED&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, NORTH CAROLINA4DEC. 2022SOIL BORING LOCATIONSAS SHOWN22580285P-2P-3P-4P-5P-6P-7P-11P-12P-13P-14P-8P-10P-9P-18P-17P-16P-1523154LEGEND- APPROXIMATE DISPENSER LOCATION- SOIL BORING LOCATION- PROPERTY BOUNDARY- CONDUIT- VENT LINE- PRODUCT LINE- OVERHEAD LINE- UNDERGROUND STORAGE TANK- UNDERGROUND STORAGE TANK NUMBERCCVVPPOHLOHL1 BUILDING
CANOPYCONCRETE
ASPHALT CONCRETE ASPHAL
T
GRASSLANDSCAP
ING
NC 704 HWY ENOTE: SAMPLES COLLECTED NOVEMBER 28-29, 2022CONCRETEASPHALT
N
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
5
22580285
JULY 2022
AS SHOWNGROUNDWATER ELEVATION CONTOUR MAP
(JULY 26, 2022)
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\7-22\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·DATE: JULY 26, 2022
·CONTOUR INTERVAL = 1 FOOT
LEGEND
- MONITORING WELL LOCATION
- APPROXIMATE DISPENSER LOCATION
- RELATIVE GROUNDWATER ELEVATION
- GROUNDWATER FLOW DIRECTION
- PROPERTY BOUNDARY
MW-3
MW-2
MW-1
68
67
66
(68.14)
(67.61)
(65.47)
(65.47)
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwgN
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
6
22580285
DEC. 2022
AS SHOWNGROUNDWATER ELEVATION CONTOUR MAP
(NOVEMBER 28, 2022)
SOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·DATE: NOVEMBER 28, 2022
·CONTOUR INTERVAL = 1 FOOT
LEGEND
- MONITORING WELL LOCATION
- APPROXIMATE DISPENSER LOCATION
- RELATIVE GROUNDWATER ELEVATION
- GROUNDWATER FLOW DIRECTION
- PROPERTY BOUNDARY
MW-3
MW-2
MW-1
67
66
65
(67.10)
(66.70)
(64.68)
(64.68)
PPPPP
P
P
P
P
P
P P P
P
P
PCCCCCC
CCCC
C
C
C
C
C
C CCCCCCCC
C
C
C
C
CVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVVV
V
V
POHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLOHLP
FIGURE NO.Drawing path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwg
PROJECT NUMBERDATE:SCALE:N01020 (IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALED&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, NORTH CAROLINA7DEC. 2022SOIL ANALYTICAL SUMMARYAS SHOWN22580285MW-3MW-1P-1MW-2P-2P-3P-4P-5P-6P-7P-11P-12P-13P-14P-8P-10P-9P-18P-17P-16P-1523154LEGEND- APPROXIMATE DISPENSER LOCATION- SOIL BORING LOCATION- PROPERTY BOUNDARY- CONDUIT- VENT LINE- PRODUCT LINE- OVERHEAD LINE- UNDERGROUND STORAGE TANK- UNDERGROUND STORAGE TANK NUMBERCCVVPPOHLOHL1 BUILDING
CANOPYCONCRETE
ASPHALT CONCRETE ASPHAL
T
GRASSLANDSCAPING
NC 704 HWY ENOTES: METHODS = 8260B, 8270D, 8015 - GASOLINE AND DIESEL RANGE ORGANICSEACH SAMPLE RESULT LESS THAN ACTION LEVEL - METHOD 8015NON-DETECT SAMPLES: P-4-25, P-9-16, P-12-20 - METHOD 8015P-2mg/kgP-2-25:All <Soil-to-Groundwater MSCCP-3mg/kgP-3-10:All <Soil-to-Groundwater MSCCP-3-25:All <Soil-to-Groundwater MSCCP-4mg/kgP-4-15:All <Soil-to-Groundwater MSCCP-4-25:All <Soil-to-Groundwater MSCCP-5mg/kgP-5-10:All <Soil-to-Groundwater MSCCP-5-20:All <Soil-to-Groundwater MSCCP-6mg/kgP-6-20:All <Soil-to-Groundwater MSCCP-7mg/kgP-7-25:All <Soil-to-Groundwater MSCCP-8mg/kgP-8-20:All <Soil-to-Groundwater MSCCP-9mg/kgP-9-16:All <Soil-to-Groundwater MSCCP-10mg/kgP-10-25:>Soil-to-Groundwater MSCC(Benzene = 0.00788)P-11mg/kgP-11-25:All <Soil-to-Groundwater MSCCP-2mg/kgP-12-20:All <Soil-to-Groundwater MSCCP-13mg/kgP-13-10:All <Soil-to-Groundwater MSCCP-14mg/kgP-14-5:All <Soil-to-Groundwater MSCCP-15mg/kgP-15-10:All <Soil-to-Groundwater MSCCP-16mg/kgP-16-15:All <Soil-to-Groundwater MSCCP-17mg/kgP-17-5:All <Soil-to-Groundwater MSCCP-18mg/kgP-18-10:All <Soil-to-Groundwater MSCCMW-1mg/kgMW-1-10:<Soil-to-Groundwater MSCCMW-1-20:>Residential MSCCMW-1-30:>Industrial/Commercial MSCCMW-2mg/kgMW-2-10:<Soil-to-Groundwater MSCCMW-2-20:>Soil-to-Groundwater MSCCMW-2-25:>Soil-to-Groundwater MSCCMW-2-30:>Soil-to-Groundwater MSCCP-1mg/kgP-1-10:<Soil-to-Groundwater MSCCP-1-20:>Soil-to-Groundwater MSCCP-1-25:>Soil-to-Groundwater MSCCP-1-30:>Soil-to-Groundwater MSCCMW-3mg/kgMW-3-10:>Soil-to-Groundwater MSCCMW-3-20:>Soil-to-Groundwater MSCCMW-3-25:<Soil-to-Groundwater MSCCMW-3-30:<Soil-to-Groundwater MSCC
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\Greensboro-1580\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\12-22\D&M Grocery-FIGS.dwgN
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
8
22580285
JULY 2022
AS SHOWNGROUNDWATER ANALYTICAL RESULTS
SOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·CONSTITUENT CONCENTRATIONS GREATER THAN 2L STANDARD ARE SHOWN
·FREE PRODUCT THICKNESS IN MW-1 = 1.43 FEET ON JULY 26, 2022
·DATE: JULY 20, 2022; MW-2 & MW-3
·METHODS: 6200B, 504.1, 6010D LEAD; VOLATILE PETROLEUM HYDROCARBONS
·SEE TABLE 5 FOR SUMMARY OF RESULTS
LEGEND
- MONITORING WELL LOCATION
- APPROXIMATE DISPENSER LOCATION
- PROPERTY BOUNDARY
- MICROGRAMS PER LITERug/L
MW-3
MW-2
MW-1
MW-1 ug/L
Not Sampled (Light Non-aqueous Phase Liquid)
MW-2 ug/L
1,2,4-Trimethylbenzene 699
Benzene 995
Ethylbenzene 1,120
Xylenes, Total 7,050
Toluene 12,100
C5-C8 Aliphatics 33,700
C9-C18 Aliphatics 16,700
C9-C22 Aromatics 4,670
MW-3 ug/L
Benzene 14.4
Tetrachloroethene 3.92
Analytical Method 625.1
Location Compounds of
Concern
Sample Date
6080 6080 NC 704 Highway East 05/24/22 5.8 177 27.8 23.1 5.9 0.76 7.8 7.1 176 61.0 3.4 513 227
6100 Well 6100 NC 704 Highway East 06/08/22 NA <0.50 <0.50 <0.50 <0.50 0.45 J <2.0 <0.50 <0.50 <0.50 <0.50 <1.5 <100
6066 Well 6066 NC 704 Highway East 06/08/22 NA <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.5 <100
6 1 70 600 70 20 6 70 600 400 400 500 40
6,000 5,000 70,000 80,000 30,500 20,000 6,000 26,100 260,000 28,500 24,100 50,000 40,000
NOTES:
Analytes that are not shown were not detected
NA = Not Analyzed
Data presented in micrograms per liter
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
J- Detected but less than the reporting limit; result is an estimated concentration.
Value Concentration exceeds the 2L Standard
TABLE 1
S&ME Project No. 22580285
6066 NC 704 Highway East, Sandy Ridge, North Carolina
D&M Grocery
Summary of Water Supply Well Sampling Results
2L Standard
Gross Contamination Level n-PropylbenzeneEthylbenzeneChloroformSample ID
BenzeneIsopropylbenzeneMethyl tert-Butyl Ether (MTBE)NaphthaleneXylenes (Total)NaphthaleneVolatile Organic Compounds by Method 6200B
tert-Amyl Alcohol (TAA)Toluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneFacility ID No.: 00-0-0000009253 Date: 8/1/2022
Facility ID No.: 00-0-0000009253
4-5 9-10 14-15 19-20 24-25 29-30 34-35 39-40 44-45
MW-1 7/18/22 10.0 2.0 223.0 214.0 1,365 988.0 75.0 6.0 2.0
MW-2 7/18/22 7.2 16.3 28.2 90.9 238.0 2,031
MW-3 7/18/22 61 18 7 11.0 <1 1.6
P-1 7/19/22 27.5 38.8 160.9 364.2 654.2 1,212
P-2 11/28/22 <1 2.6 3.0 34.2 152
P-3 11/28/22 19.7 15.7 2.7 6.2 37.8
P-4 11/28/22 2.2 13.4 16.4 10.5 36.1
P-5 11/28/22 2.7 19.1 14.8 61.7 51.0
P-6 11/28/22 2.4 3.4 18.6 140 125
P-7 11/28/22 49.8 2.2 NR 114 137
P-8 11/28/22 1.9 2.6 1.2 7.5
P-9 11/28/22 <1 1.7 1.6 16.2 (Sample depth = 16 feet)
P-10 11/28/22 1.7 1.2 5.6 60.8 185
P-11 11/28/22 1.6 NR 5.0 50.8 154
P-12 11/28/22 2.1 1.7 11.6 15.2
P-13 11/28/22 1.2 10.0 2.0 2.5
P-14 11/29/22 7.5 2.8 1.8 1.7
P-15 11/29/22 2.6 7.6 4.8 6.4
P-16 11/29/22 2.5 5.0 2.2 1.8
P-17 11/29/22 15.5 2.9 4.2 19.0
P-18 11/29/22 <1 7.3 2.2 1.4
Note: Readings collected with photo-ionization detector (PID) in parts per million after allowing headspace equilibration for approximately 5 minutes.
Values shown in bold were selected for laboratory analysis.
NR- No Recovery
Sample
Location Date Depth of PID Reading (feet)
TABLE 2
Field Screening Results
D&M Grocery (Incident No.: 48461)
6066 NC 704 Highway East, Sandy Ridge, North Carolina
S&ME Project No. 22580285
Date: 12/2/2022
1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2-Butanone (MEK)2-Hexanone4-Isopropyltoluene4-Methyl-2-pentanone (MIBK)AcetoneBenzeneEthylbenzeneHexaneIodomethaneIsopropyl etherIsopropylbenzeneMethyl tert-butyl etherNaphthalenen-Butylbenzenen-Heptanen-Propylbenzenesec-ButylbenzeneTolueneXylenes (total)2-MethylnaphthaleneAcetophenoneNaphthaleneGasoline Range OrganicsDiesel Range OrganicsDate
Collected
Sample
Type Sample Depth
(feet)mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
MW-1-10 7/18/22 Grab 10 2.01 0.487 <1.22 <1.22 <0.244 <0.122 <2.44 <0.244 0.944 <2.44 <2.44 <0.488 <2.44 <2.44 0.188 J 0.106 J <2.44 0.319 <2.44 2.56 5.89 NS NS NS 55.1 NS
MW-1-20 7/18/22 Grab 20 222 57.1 <1.52 <1.52 7.36 <1.52 <3.04 1.12 78.4 1.95 <0.304 <0.609 18 <0.304 24.4 8.86 6.82 37.6 2.48 95.8 768 NS NS NS 1,460 NS
MW-1-30 7/18/22 Grab 30 371 129 <33.7 <33.7 5.77 J <33.7 <67.4 25.3 253 32.3 <6.74 <13.5 31.7 <6.74 45.8 29.7 67.4 94.0 <6.74 764 1,360 NS NS NS 19,000 NS
MW-3-10 7/18/22 Grab 10 0.0333 0.0110 <0.0360 <0.0360 <0.00720 <0.0360 0.102 0.0527 0.115 0.00631 J 0.00247 J <0.0144 0.00578 J <0.00720 <0.00720 <0.00720 0.00849 0.0128 <0.00720 1.06 0.548 E NS NS NS 9.57 J NS
MW-3-20 7/18/22 Grab 20 0.0328 0.00967 J <0.0495 <0.0495 <0.00990 <0.0495 0.0351 J 0.0331 0.0845 0.00407 J <0.00990 <0.0198 0.00513 J <0.00990 <0.00990 <0.00990 <0.00990 0.0106 <0.00990 1.68 0.422 NS NS NS 12.1 J NS
MW-3-25 7/19/22 Grab 25 <0.00609 <0.00609 <0.0304 <0.0304 <0.00609 <0.0304 0.0230 J <0.00609 <0.00609 <0.00609 <0.00609 <0.0122 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 0.00383 J 0.00361 J NS NS NS <12.7 1 NS
MW-3-30 7/19/22 Grab 30 <0.00682 <0.00682 <0.0341 <0.0341 <0.00682 <0.0341 0.0153 J <0.00682 <0.00682 <0.00682 <0.00682 <0.0136 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 0.00707 0.0107 J NS NS NS 11.4 NS
MW-2-10 7/19/22 Grab 10 <0.00802 <0.00802 0.0519 <0.0401 <0.00802 <0.0401 0.188 <0.00802 <0.00802 <0.00802 0.00320 J <0.0160 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 0.00433 J <0.0160 NS NS NS <15.7 1 NS
MW-2-20 7/19/22 Grab 20 <0.00894 <0.00894 1.2600 0.1870 <0.00894 0.0639 <3.28 <0.00894 <0.00894 <0.00894 0.00444 J <0.0179 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.0179 NS NS NS 6.96 J NS
MW-2-25 7/19/22 Grab 25 0.00989 <0.00772 0.3960 0.0325 J <0.00772 <0.0386 0.494 0.00775 0.00843 0.00296 J <0.00772 <0.0154 <0.00772 <0.00772 <0.00772 <0.00772 <0.00772 0.00398 J <0.00772 0.0273 0.0533 NS NS NS <15.9 1 NS
MW-2-30 7/19/22 Grab 30 0.0536 0.0245 0.0978 0.0274 J 0.0111 <0.0355 0.306 0.0102 0.0227 0.00793 <0.00710 <0.0142 0.00610 J <0.00710 0.0243 0.016 0.0175 0.0152 0.00406 J 0.0528 0.143 NS NS NS 6.82 J NS
P-1-10 7/19/22 Grab 10 <0.00812 <0.00812 0.0336 J <0.0406 <0.00812 <0.0406 0.299 <0.00812 <0.00812 <0.00812 <0.00812 <0.0162 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 0.00449 J 0.00686 J NS NS NS <15.4 1 NS
P-1-20 7/19/22 Grab 20 0.00662 J <0.00816 0.1090 <0.0408 <0.00816 <0.0408 0.589 0.0122 0.00594 J <0.00816 0.00826 <0.0163 <0.00816 0.0227 <0.00816 <0.00816 <0.00816 <0.00816 <0.00816 0.0334 0.0409 NS NS NS <16.5 1 NS
P-1-25 7/19/22 Grab 25 0.0267 0.0085 0.1890 <0.402 <0.00804 <0.402 0.757 0.0536 0.0381 0.00366 J <0.00804 0.00342 J 0.00402 J 0.0517 <0.00804 <0.00804 0.00707 J 0.00583 J <0.00804 0.244 0.219 NS NS NS 5.48 J NS
P-1-30 7/19/22 Grab 30 32.4 8.02 <1.74 <1.74 1.39 <1.74 <3.47 3.33 19.3 2.67 <0.347 <0.694 1.77 <0.347 3.55 1.87 4.48 5.54 0.497 64.9 105 NS NS NS 828 NS
P2-25 11/28/22 Grab 25 <0.00664 <0.00664 0.632 <0.0332 NS <0.0332 1.3 0.00477 J <0.00664 <0.00664 <0.00664 <0.0133 <0.00664 0.00449 J <0.00664 <0.00664 <0.00664 <0.00664 <0.00664 0.0172 0.0112 J <0.396 <0.396 <0.396 <7.46 4.39 J
P3-10 11/28/22 Grab 10 0.0183 0.00537 J <0.0279 <0.0279 NS <0.0279 0.0512 J <0.00559 0.00736 <0.00559 <0.00559 <0.0112 <0.00559 <0.00559 0.00648 <0.00559 <0.00559 <0.00559 <0.00559 0.0295 0.0454 0.0722 J <0.375 0.0543 J <6.68 30.8
P3-25 11/28/22 Grab 25 0.0171 0.00547 J 0.17 <0.0282 NS <0.0282 0.122 <0.00564 0.00404 J <0.00564 <0.00564 <0.0113 <0.00564 <0.00564 <0.00564 <0.00564 <0.00564 0.00248 J <0.00564 0.0172 0.0412 <0.358 0.0939 J <0.358 <6.21 6.46 J
P4-15 11/28/22 Grab 15 <0.00621 <0.00621 0.0351 <0.0310 NS <0.0310 0.0904 <0.00621 <0.00621 <0.00621 <0.00621 <0.0124 <0.00621 <0.00621 <0.00621 <0.00621 <0.00621 <0.00621 <0.00621 <0.00621 <0.0124 <0.0368 <0.0368 <0.0368 <6.96 9.94
P4-25 11/28/22 Grab 25 <0.00633 <0.00633 0.0158 J <0.0317 NS <0.0317 0.0288 J <0.00633 <0.00633 <0.00633 <0.00633 <0.0127 <0.00633 <0.00633 <0.00633 <0.00633 <0.00633 <0.00633 <0.00633 0.00488 J <0.0127 <0.366 <0.366 <0.366 <6.81 <8.95
P5-10 11/28/22 Grab 10 <0.00610 <0.00610 <0.0305 <0.0305 NS <0.0305 0.0286 J <0.00610 <0.00610 <0.00610 <0.00610 <0.0122 <0.00610 <0.00610 <0.00610 <0.00610 <0.00610 <0.00610 <0.00610 <0.00610 <0.0122 <0.375 <0.375 <0.375 <6.94 7.78 J
P5-20 11/28/22 Grab 20 <0.00605 <0.00605 0.319 <0.00302 NS <0.00302 0.462 <0.00605 <0.00605 <0.00605 <0.00605 <0.0121 <0.00605 <0.00605 <0.00605 <0.00605 <0.00605 <0.00605 <0.00605 0.00426 J <0.0121 <0.389 <0.389 <0.389 <8.06 3.83 J
P6-20 11/28/22 Grab 20 <0.00574 <0.00574 0.358 0.0288 NS <0.0287 0.565 0.00653 <0.00574 <0.00574 <0.00574 <0.0115 <0.00574 0.00817 <0.00574 <0.00574 <0.00574 <0.00574 <0.00574 0.0157 0.00942 J <0.413 <0.413 <0.413 <7.34 5.81 J
P7-25 11/28/22 Grab 25 <0.00672 <0.00672 0.868 0.0595 NS <0.336 0.00323 J <0.00672 <0.00672 0.00233 J <0.0134 <0.00672 0.00331 J <0.00672 <0.00672 <0.00672 <0.00672 <0.00672 0.0147 0.00988 J <0.416 <0.416 <0.416 <8.02 5.90 J
P8-20 11/28/22 Grab 20 <0.00642 <0.00642 0.214 <0.0321 NS <0.0321 0.371 <0.00642 <0.00642 <0.00642 0.00267 J <0.0128 <0.00642 <0.00642 <0.00642 <0.00642 <0.00642 <0.00642 <0.00642 0.00513 J 0.00327 J <0.430 <0.430 <0.430 <7.72 3.60 J
P9-16 11/28/22 Grab 16 <0.00627 <0.00627 0.0341 <0.313 NS <0.313 0.325 <0.00627 <0.00627 <0.00627 <0.00627 <0.0125 <0.00627 <0.00627 <0.00627 <0.00627 <0.00627 <0.00627 <0.00627 <0.00627 <0.0125 <0.389 <0.389 <0.389 <7.17 <9.96
P10-25 11/28/22 Grab 25 <0.00617 <0.00617 0.0398 <0.0308 NS <0.0308 0.0697 0.00788 0.00285 J 0.00544 J <0.00617 <0.0123 <0.00617 <0.00617 <0.00617 <0.00617 <0.00617 <0.00617 <0.00617 0.0337 0.0192 <0.391 <0.391 <0.391 <8.03 5.91 J
P11-25 11/28/22 Grab 25 <0.00648 <0.00648 0.548 0.0584 NS 0.0274 J 1.14 0.00489 J <0.00648 <0.00648 0.00233 J <0.0130 <0.00648 <0.00648 <0.00648 <0.00648 <0.00648 <0.00648 <0.00648 0.0187 0.0145 <0.431 <0.431 <0.431 <7.91 4.38 J
P12-20 11/28/22 Grab 20 <0.00693 <0.00693 0.300 <0.0347 NS <0.0347 0.219 <0.00693 <0.00693 <0.00693 <0.00693 <0.0139 <0.00693 <0.00693 <0.00693 <0.00693 <0.00693 <0.00693 <0.00693 <0.00693 <0.0139 <0.411 <0.411 <0.411 <8.53 <10.1
P13-10 11/29/22 Grab 10 <0.00707 <0.00707 <0.0354 <0.0354 NS <0.0354 0.0580 J <0.00707 <0.00707 <0.00707 <0.00707 <0.0141 <0.00707 <0.00707 <0.00707 <0.00707 <0.00707 <0.00707 <0.00707 <0.00707 <0.0141 <0.438 <0.438 <0.438 <9.00 16.6
P14-5 11/29/22 Grab 5 <0.00669 <0.00669 <0.0335 <0.0335 NS <0.0335 0.0454 J <0.00669 <0.00669 <0.00669 <0.00669 <0.0134 <0.00669 <0.00669 <0.00669 <0.00669 <0.00669 <0.00669 <0.00669 <0.00669 <0.0134 0.0921 J <0.400 <0.400 <6.78 3.72 J
P15-10 11/29/22 Grab 10 <0.00673 <0.00673 <0.0337 <0.0337 NS <0.0337 0.0411 J <0.00673 <0.00673 <0.00673 <0.00673 <0.0135 <0.00673 <0.00673 <0.00673 <0.00673 <0.00673 <0.00673 <0.00673 <0.00673 <0.0135 <0.412 <0.412 <0.412 <8.85 11.1
P16-15 11/29/22 Grab 15 <0.00634 <0.00634 0.0129 J <0.0317 NS <0.0317 0.121 <0.00634 <0.00634 <0.00634 <0.00634 <0.0127 <0.00634 <0.00634 <0.00634 <0.00634 <0.00634 <0.00634 <0.00634 <0.00634 <0.0127 <0.406 <0.406 <0.406 <8.19 3.45 J
P17-5 11/29/22 Grab 5 <0.00489 <0.00489 <0.0245 <0.0245 NS <0.0245 0.0801 <0.00489 <0.00489 <0.00489 <0.00489 <0.00978 <0.00489 <0.00489 <0.00489 <0.00489 <0.00489 <0.00489 <0.00489 <0.00489 <0.00978 <0.412 <0.412 <0.412 6.62 4.62 J
P18-10 11/29/22 Grab 10 <0.00674 <0.00674 0.0199 J <0.0337 NS <0.0337 0.127 <0.00674 <0.00674 <0.00674 <0.00674 <0.0135 <0.00674 <0.00674 <0.00674 <0.00674 <0.00674 <0.00674 <0.00674 <0.00674 <0.0135 <0.435 <0.435 <0.435 <8.88 5.19 J
6.6 6.6 16 0.17 0.12 0.42 24 0.0072 8 NSE NSE 0.32 1.3 0.085 0.2 2.4 NSE 1.4 2.2 5.4 6 1.5 NSE 0.2 NA NA
156 156 9,380 78.2 1,560 1,250 14,000 12 60.3 NSE NSE 156 1,560 156 5.5 782 NSE 1,560 1,560 1,250 3,120 62.5 NSE 5.5 NA NA
2,330 2,330 140,000 1,160 23,300 18,600 210,000 59.4 297 NSE NSE 2,330 23,300 1,810 27 11,600 NSE 23,300 23,300 18,600 46,700 934 NSE 27 NA NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 50 100
Notes:
NS - Not Sampled
NA - Not Applicable
Date: 12/15/2022
mg/kg = milligrams per kilogram
Analytical Method
Sample ID
Constituent
Soil-to-Groundwater MSCCs
Industrial/Commercial Soil Cleanup Levels
Only detected compounds are shown.
Residential Soil Cleanup Levels
Method 8260D
Action Level
J- Detected but concentration is less than the Reporting Limit; result is an approximate value.
Method 8015 Method
8270D
Table 3
Summary of Soil Sampling Results
D&M Grocery (Incident No.: 48461)
6066 NC Highway 704 East, Sandy Ridge, North Carolina
S&ME Project No. 22580285
MSCC = Maximum Soil Contaminant Concentration (September 7, 2022)
Concentration exceeds the Soil-to-Groundwater MSCC
Concentration exceeds the Residential Soil Cleanup Level
Concentration exceeds the Industrial/Commercial Soil Cleanup Level
Facility ID No.: 00-0-0000009253
Facility ID No.: 00-0-0000009253
Well
ID
Date
Installed
Screen
Interval
(ft-BGS)
Well Casing
Depth
(ft-BGS)
Total Depth
(ft-BGS)
Relative Top of
Casing Elevation*
(ft.)
Date of
Measurement
Depth To
Water (ft.
BTOC)
Depth To
Product
(ft. BTOC)
Product
Thickness (ft.)
Relative
Groundwater
Elevation (ft.)
7/26/2022 32.88 31.45 1.43 68.14
34.81 31.50 3.31 69.48
32.96 32.75 0.21 67.19
34.78 31.72 3.06 67.40
32.45 32.43 0.02 67.56
10/26/2022 34.01 32.16 1.85 67.3111/28/2022 34.79 32.14 2.65 67.1035.30 31.71 3.59 67.2632.60 32.50 0.10 67.477/26/2022 32.66 ND ND 67.618/31/2022 33.08 ND ND 67.19
10/5/2022 33.28 ND ND 66.99
11/28/2022 33.57 ND ND 66.70
1/3/2023 33.35 ND ND 66.92
7/26/2022 33.97 ND ND 65.47
8/31/2022 34.30 ND ND 65.14
10/5/2022 34.47 ND ND 64.97
11/28/2022 34.76 ND ND 64.68
1/3/2023 34.52 ND ND 64.92
NOTES:
ft : feet
ft-BGS : feet below ground surface
99.44
ND - Not detected
BTOC: Below top-of-casing
*Reference Point for Elevation Measurements: MW-1, Assigned Elevation: 100.00 ft.
** Product Hand Bailing Performed
MW-3 07/19/22 20 - 40 0.4 - 20 40.0
10/5/2022**
MW-2 07/19/22 20 - 40 0.3 - 20 40.0 100.27
MW-1 07/19/22 25 - 40 0.5 - 25 40.0 100.00
8/31/2022**
1/3/2023**
Date Revised: 1/3/2023
Table 4
Monitor Well Construction and Liquid Level Data
S&ME Project No. 225802856066 NC 704 Highway East, Sandy Ridge, North Carolina
D&M Grocery (Incident No.: 48461)
Page 1 of 1
Facility ID No.: 00-0-0000009253
Method 504.1 6010
Constituent
Sample Date
MW-1 07/20/22
MW-2 07/20/22 <0.0184 <10.0 699 H <250 <250 995 H <250 1,120 H <250 <1,000 7,050 H <500 <250 <250 12,100 H 33,700 16,700 4,670
MW-3 07/20/22 <0.0181 11.6 90.4 29.2 2.41 14.4 0.599 56.5 5.09 5.97 291.2 E 11.0 17.8 3.92 20.0 348 404 533 F1
0.02 15 400 400 25 1 70 600 70 6 500 70 70 0.7 600 400 700 200
50 15,000 28,500 24,100 11,700 5,000 70,000 80,000 30,500 6,000 50,000 5,900 26,100 700 260,000 NSE NSE NSE
NOTES:Concentration exceeds the 2L Standards
Constituents that are not shown were not detected Concentration exceeds the Gross Contamination Levels
Data presented in micrograms per liter or mg/L
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202 (March 7, 2022)
VPH - Volatile Petroleum Hydrocarbons
E - Result exceeded calibration range Toluenen-PropylbenzeneXylenes, TotalTetrachloroetheneNSE - No Gross Contamination Level established
2L Standard
Gross Contamination Level 1,2-Dibromoethane (Ethylene Dibromide)LeadNot Sampled- Free Product (Light Non-aqueous Phase Liquid)EthylbenzeneChloroform4-IsopropyltolueneNaphthalene1,2,4-Trimethylbenzene Date: 8/5/2022
6200B MADEP-VPH
Table 5
Summary of Groundwater Sampling Results
D&M Grocery (Incident No.: 48461)
6066 NC 704 Highway East, Sandy Ridge, North CarolinaS&ME Project No. 22580285
Sample ID
C9-C22 AromaticsC9-C18 AliphaticsC5-C8 Aliphatics1,3,5-Trimethylbenzenen-ButylbenzeneBenzeneIsopropylbenzenePage 1 of 1

Appendices

Appendix I- Tank Tightness Test Results and UST Inspection Report

Page 1 of 12 6/8/2022 11:24 AM
North Carolina
Department of Environmental Quality
Underground Storage Tank
UST-10BPrinted:6/8/2022 11:18 AM
Inspection Result:Passed Inspection Date:6/8/2022
Partial Inspection:No Arrive and Depart Times:9:10 AM-9:45 AM
Facility ID:00-0-0000009253 Inspector Jenny Lilley
Facility Name D &M GROCERY Insp.Type Compliance
Facility Address 6066 NC 704 HWY E
SANDY RIDGE,NC 27046
Stokes County
Located facility,USTs onsite
Reason(s)Routine Compliance,Referral From Incident
Manager
Location 36.471335,-80.100943
Permit Exp.6/30/2022
Facility Phone [phone]
CONTACTS
Contact Type Contact Information
Owner
since 1/1/1998
HUFFMAN OIL COMPANY,INCORPORATED ,PO BOX 730 -1021 QUEEN ANN ST BURLINGTON,NC
27216-0730,Phone:[phone]
Regulatory Operator
since 12/4/2014
MELISSA E YATES ,388 CASE ROAD MADISON ,NC 27025-7658,Phone:(336)
552-3118
Primary Operator
since 2/22/2019
STEVE BARNWELL,1448 N.FAYETTEVILLE ST.ASHEBORO,NC 27203,Phone:[phone],Email:
[e-mail]
Trained:Yes,2/22/2019,Training Type:Online Training
OWNERSHIP CHANGE
New Owner Change Date Basis Transfer of Ownership Form (UST-15)Submitted
No
EMERGENCY RESPONSE
Emergency response placard with emergency response operator contact information is posted in the dispensing areas if the
dispensers are left on without an attendant present?
Yes
OTHER PARTICIPANTS
Name Organization
BILLY PILLAR HUFFMAN OIL
INSPECTOR COMMENTS
Type Date Comment
Tank 6/8/2022 1.BRASWELL/ARNOLD OMEGA INVOICE #440419,DATED 04/20/95 VERIFIES REG TANK
AS 8K GLASTEEL.REGULAR TANK IS FRP/STEEL CLAD BONDED INTO IC SYSTEM.
2.COLLSON-MURRAY COMPANY INVOICE #10791,DATED 08/31/88 VERIFIES STIP-3
UST-10B Facility ID:00-0-0000009253
Page 2 of 12 6/8/2022 11:24 AM
TANK.
3.557 FT FROM FACILITY'S WELL TO REGULAR ATG LID.
4.NO ACCESS AT PREM 2
7.LETTER DATED 06/01/95,SIGNED BY HAROLD KENDRICK OF HUFFMAN OIL VERIFIED
BALL FLOATS FOR ALL USTS EXCEPT KERO AND ALL PIPING IS FRP.
8.LETTER SIGNED BY HAROLD KENDRICK OF HUFFMAN OIL,INSTALLER,DATED
08/29/89 VERIFIED EUROPEAN SUCTION.
9.ALL SPILL BUCKET LINERS DATED 12/2017 EXCEPT FOR REGULAR WHICH IS DATED
09/2016.
Leak Dect.6/6/2022 ALL 5 TANKS PASSED TTT ON 05/31/22.
ADDITIONAL INSPECTOR COMMENTS
TANKS AND PIPING INFORMATION
Tanks Tank #1(1-PREM2)Tank #2(2-MID)Tank #3(3-PREM1)Tank #4(4-KERO)Tank #5(5-REG)
Tank ID 1-PREM2 2-MID 3-PREM1 4-KERO 5-REG
TIMS Tank ID 1 2 3 4 5
Is tank registered?Yes Yes Yes Yes Yes
Date tank installed 4/26/1962 4/26/1962 4/26/1962 10/1/1989 5/3/1995
Capacity of Tank in Gallons 2000 4000 3000 4000 8000
Is tank regulated Yes Yes Yes Yes Yes
Diameter (Inches)64 64 64 64 96
Tank /Product use Motor Fuel Motor Fuel Motor Fuel Motor Fuel Motor Fuel
Product stored in Tank Gasoline,Gas Mix Gasoline,Gas Mix Gasoline,Gas Mix Kerosene,Kero Mix Gasoline,Gas Mix
Product Detail Premium Mid-Grade Premium BLANK Regular
If hazardous substance,CAS#
or description
If other,description
Tank status Temporarily Closed Current Current Current Current
Tank closure report submitted
Date tank last operated 2/20/2017
Inches of product in Tank 0.000000
Compartment tank No No No No No
Other compartment(s)
Base compartment
Manifolded tank No No No No No
Manifolded with tank(s)
Master manifold tank
New Tank System installed in
accordance with NC or MI
Yes Yes
Tank Construction Material
(DW required after 11/1/07)
Single Wall Steel Single Wall Steel Single Wall Steel Single Wall Steel Single Wall
Steel/FRP
If other,description
UST-10B Facility ID:00-0-0000009253
Page 3 of 12 6/8/2022 11:24 AM
Tanks Tank #1(1-PREM2)Tank #2(2-MID)Tank #3(3-PREM1)Tank #4(4-KERO)Tank #5(5-REG)
Tank Manufacturer/Model Unknown Unknown Unknown Unknown Unknown
If other,describe
Tank material verified by UST-7A/B UST-7A/B UST-7A/B Invoice Invoice
Date Pipe Installed 5/3/1995 5/3/1995 5/3/1995 5/3/1995 5/3/1995
Was UST Piping Installed on or
after 11/1/2007?
No No No No No
Piping Construction Material
(DW required after 11/1/07)
None Single Wall FRP Single Wall FRP Single Wall FRP Single Wall FRP
If other,description
Pipe Manufacturer/Model Unknown Unknown Unknown Unknown Unknown
If other,describe
Pipe material verified by Visual Visual Visual Installer Letter Visual
If E-blend >10%or Biodiesel
Blend >20%;Was UST-20
completed and approved?
N/A N/A N/A N/A N/A
CORROSION PROTECTION
Tank Corrosion Protection Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-
REG)
DWM notified of current CP method Yes Yes Yes Yes Yes
Integrity assessment performed after 3/1/06 No No No No No
CP Method 1 Impressed
Current
Impressed
Current
Impressed
Current
Impressed
Current
Steel/FRP
Composite
if other,Description
CP Installation Date 5/30/1995 5/30/1995 5/30/1995 5/30/1995 5/30/1995
CP Method 2 Impressed
Current
if other,Description
CP Installation Date 5/30/1995
Flex Connector ,Piping Extensions,and/or other metal
fittings Present
None Ball Valve,
Elbow
Ball Valve,
Elbow
Ball Valve,
Elbow
Ball Valve,
Elbow
Flex connector isolated from ground No No No No
Source of verification of CP for Flex Connectors,piping
extensions and/or other metal fittings
CP Test
Results
CP Test
Results
CP Test
Results
CP Test
Results
if other,Description
Submersible pump (STP)is isolated from ground N/A Yes Yes N/A Yes
Piping extensions and/or other metal fittings are isolated
from ground
No No No No
Flex connector,STP and/or other metal fittings
protected from corrosion
N/A Yes Yes Yes Yes
Corrosion protection method Impressed
Current
Impressed
Current
Impressed
Current
Impressed
Current
UST-10B Facility ID:00-0-0000009253
Page 4 of 12 6/8/2022 11:24 AM
Tank Corrosion Protection Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-
REG)
Flex connector ,Piping extensions,and/or other metal
fittings CP Installation Date
5/30/1995 5/30/1995 5/30/1995 5/30/1995
Dielectric Coating Installed (If tank installed after
12/22/88
N/A N/A N/A Yes Yes
Pipe Corrosion Protection Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
DWM notified of current CP method Yes Yes Yes Yes Yes
CP method FRP Piping FRP Piping FRP Piping FRP Piping FRP Piping
if other,Description
CP Installation Date 5/30/1995 5/30/1995 5/30/1995 5/30/1995 5/30/1995
Dielectric Coating Installed (If piping installed
after 12/22/88
N/A N/A N/A N/A N/A
Dispenser Corrosion Protection Dispenser #1(1/2)Dispenser #2(3/4)Dispenser
#3(KEROSENE)
Flex Connector ,Piping Extensions,and/or other metal fittings
Present
Flex Connector Flex Connector Flex Connector
Flex connector isolated from ground Yes Yes No
Source of verification of CP for Flex Connectors,piping extensions
and/or other metal fittings
Visual Visual CP Test Results
if other,Description
Piping extensions and/or other metal fittings are isolated from
ground
Yes Yes No
Flex Connectors,Piping extensions and/or other metal fittings
protected from corrosion
N/A N/A Yes
Corrosion protection method Isolated Isolated Impressed Current
Flex connector,Piping extensions,and/or other metal fittings CP
Installation Date
5/30/1995
Source of Information for verification of corrosion protection for
Riser pipe and other metal piping
Visual Visual CP Test Results
if other,Description
CP Conclusions
CP Requirements Met?Yes
Issues
UST-10B Facility ID:00-0-0000009253
Page 5 of 12 6/8/2022 11:24 AM
Impressed Current Systems IC System #1
Applies to Tanks #1(1-PREM2),#2(2-MID),#3(3-PREM1),#4(4-KERO)
Current Voltage (Gauge)64.0000
Current Amperage (Gauge)2.0000
Current Voltage (Multimeter)
Measured Shunt Voltage (mV)
Rectifier Shunt Factor (Amps/mV)
Amps -Calculated
Last three 60-day readings available Yes
System operating properly Yes
If no,select all that apply
If other,describe
Hour meter reading?
Hour meter installed No
CP Tests Test #1
Applies to Tanks #1(1-PREM2),#2(2-MID),#3(3-PREM1),#4(4-
KERO),#5(5-REG)
Portion of System Tested Flex connectors,Tanks
Date of last Corrosion Protection Test 1/25/2022
CP Test Result Pass
Was CP Test done in accordance with National Standard?Yes
CP Tester Name JASON ROGERS
Certificate Number SEE110920.247
Certifying Organization SEE
CP Testing Company Name ENVIRO CONSULTING
CP Testing Company Phone [phone]
As Left Voltage 64
As Left Current 1.8
UST7 form for last CP test submitted to DWM Yes
SPILL PREVENTION
Has DWM been notified of spill methods?Yes
Spill/Overfill Details Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
Is a drop tube present?Yes Yes Yes Yes Yes
Type of Stage I vapor recovery?Dual Point Dual Point Dual Point Not Required Dual Point
UST-10B Facility ID:00-0-0000009253
Page 6 of 12 6/8/2022 11:24 AM
Local Fill Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
Does Tank have a Second Fill?No No No No No
Spill Protection Catchment
Basin
Catchment
Basin
Catchment
Basin
Catchment
Basin
Catchment
Basin
Is spill prevention equipment provided and verified?Yes Yes Yes Yes Yes
Manufacturer/Model Spill bucket with
LINER (SW)
Spill bucket with
LINER (SW)
Spill bucket with
LINER (SW)
Spill bucket with
LINER (SW)
Spill bucket with
LINER (SW)
If other,describe
Spill bucket is double-walled?N/A N/A N/A N/A N/A
Monitoring Type
(UST-6B)
Is spill bucket interstice monitored every 30 days?
(If installed before 11/1/07)
Spill bucket is isolated or made of non-corroding
materials?(If installed after 11/1/07)
N/A N/A N/A N/A N/A
Date spill prevention provided 5/30/1995 5/30/1995 5/30/1995 5/30/1995 5/30/1995
Last 12 monthly spill bucket checks completed and
all deficiencies corrected (UST-27)?
Yes Yes Yes Yes Yes
Is spill prevention operating properly?Yes Yes Yes Yes Yes
If No,select all that apply
If other,describe
O&M walkthrough inspection completed in
accordance with national standard (e.g.PEI RP 900)
(UST-27)?
Yes Yes Yes Yes Yes
3 Year Tightness Test Date
(UST-6D/23A)
5/31/2022 5/31/2022 5/31/2022 5/31/2022 5/31/2022
Primary Tightness Test Result
(UST-6D/23A)
Pass Pass Pass Pass Pass
Secondary Tightness Test Result
(UST-6D/23A)
Tightness Testing done in accordance with a
standard?
Yes Yes Yes Yes Yes
OVERFILL PREVENTION
Has DWM been notified of overfill methods?Yes
Overfill Control Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
Is overfill prevention equipment provided and
verified?
Yes Yes Yes Yes Yes
Date overfill control provided 6/22/2018 6/22/2018 6/22/2018 6/22/2018 6/22/2018
Type of overfill equipment Overfill Alarm Overfill Alarm Overfill Alarm Overfill Alarm Overfill Alarm
UST-10B Facility ID:00-0-0000009253
Page 7 of 12 6/8/2022 11:24 AM
Overfill Control Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
Source of information for overfill control verification Visual
observation
Visual
observation
Visual
observation
Visual
observation
Visual
observation
If other,describe
Manufacturer/Model BLANK BLANK BLANK BLANK BLANK
If other,describe
Is overfill control operating properly?Yes Yes Yes Yes Yes
If No,select all that apply
If other,describe
Overfill check date (UST-22A)5/31/2022 5/31/2022 5/31/2022 5/31/2022 5/31/2022
Overfill check result (UST-22A)Pass Pass Pass Pass Pass
Capacity of Tank in Gallons 2000 4000 3000 4000 8000
Diameter (Inches)64 64 64 64 96
Dispenser Sumps Dispenser #1(1/2)Dispenser #2(3/4)Dispenser
#3(KEROSENE)
Are containment sumps present?Yes Yes No
Installation Date 5/30/1995 5/30/1995
Sump Manufacturer Unknown Unknown
If Other (Specify)
Sump Construction Type Single Walled Single Walled
Sump Construction Material Plastic Plastic
If Other (Specify)
Are containment sumps monitored?No No
Is monitoring required per 2N .0900?No No No
Piping components and/or STP were installed/replaced on or after
11/1/07?
No No No
Are spills or small weeps evident in sumps?No No No
Are single wall piping components located in containment sump?(If
installed after 11/1/07)
UDC Visual Inspection Date
(annually)(UST-22C)
5/31/2022 5/31/2022 5/31/2022
UDC Visual Inspection Results
(UST-22C)
Pass Pass Pass
Annual containment sump check completed in accordance with
national standard (e.g.PEI RP 900)?
Yes Yes Yes
Other Sumps Sump#1(KERO
TT)
Sump#2(MID STP)Sump#3(PREM1
STP)
Sump#4(REG
STP)
Are containment sumps present?No No No No
Installation Date
Sump Manufacturer
UST-10B Facility ID:00-0-0000009253
Page 8 of 12 6/8/2022 11:24 AM
Other Sumps Sump#1(KERO
TT)
Sump#2(MID STP)Sump#3(PREM1
STP)
Sump#4(REG
STP)
If Other (Specify)
Sump Construction Type
Sump Construction Material
If Other (Specify)
Are containment sumps monitored?
Is monitoring required per 2N .0900?No No No No
Piping components and/or STP were installed/replaced on
or after 11/1/07?
No No No No
Are spills or small weeps evident in sumps?No No No No
Are single wall piping components located in containment
sump?(If installed after 11/1/07)
Sump Visual Inspection Date
(annually)(UST-22C)
5/31/2022 5/31/2022 5/31/2022 5/31/2022
Sump Visual Inspection Results
(UST-22C)
Pass Pass Pass Pass
Annual containment sump check completed in accordance
with national standard (e.g.PEI RP 900)?
Yes Yes Yes Yes
SITING AND SECONDARY CONTAINMENT
Siting And Sec.Containment-General Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
UST system upgraded with corrosion protection,
spill and overfill before 1/1/91?
N/A N/A N/A N/A N/A
UST system and/or piping are located within siting
and secondary containment areas?
No No No No No
LEAK DETECTION
General Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
DWM notified of leak detection method?Yes Yes Yes Yes Yes
Piping Type
Piping type Manifold Bar Pressurized
System
Pressurized
System
European
Suction
Pressurized
System
if other,specify
Suction check type Dispenser
Type LLD present.Not Required ELLD ELLD Not Required ELLD
Tank Release Detection
Primary leak detection method Automatic Tank
Gauging
Automatic Tank
Gauging
Automatic Tank
Gauging
Automatic Tank
Gauging
Automatic Tank
Gauging
UST-10B Facility ID:00-0-0000009253
Page 9 of 12 6/8/2022 11:24 AM
General Tank #1(1-
PREM2)
Tank #2(2-MID)Tank #3(3-
PREM1)
Tank #4(4-
KERO)
Tank #5(5-REG)
if other,specify
Primary LD install date 5/30/1995 5/30/1995 5/30/1995 5/30/1995 5/30/1995
Secondary leak detection method
if other,specify
Piping Release Detection
Primary leak detection method Not Required Line Tightness
Testing (LTT)
Line Tightness
Testing (LTT)
Exempt
(European Style)
Line Tightness
Testing (LTT)
if other,specify
Primary LD install date 9/30/2000 9/30/2000 9/30/2000 9/30/2000 9/30/2000
Secondary leak detection method
if other,specify
Equipment Checks
Last 12 monthly RD equipment checks
completed and all deficiencies corrected
(UST-27)?
Yes Yes Yes Yes Yes
if no,select all that apply
Annual RD equipment operability check result
(UST-22B)
Pass Pass Pass Pass Pass
if Fail,select all that apply
Annual RD equipment operability check date
(UST-22B)
5/31/2022 5/31/2022 5/31/2022 5/31/2022 5/31/2022
RD equipment checks completed per national
standard (e.g.PEI RP 900/1200)(UST-22B/27)?
Yes Yes Yes Yes Yes
PIPING LEAK DETECTION
Pressurized Piping Tank #2(2-MID)Tank #3(3-PREM1)Tank #5(5-REG)
Last MLLD/ELLD Test Date 5/31/2022 5/31/2022 5/31/2022
MLLD/ELLD Test Result Pass Pass Pass
Last LTT Test Date 5/31/2022 5/31/2022 5/31/2022
LTT Test Result Pass Pass Pass
Does test result indicate
suspected release?
No No No
Number of MLLD/ELLD Types 1 1 1
MLLD/ELLD Equipment Tank #2(2-MID)LLD #1 Tank #3(3-PREM1)LLD #1 Tank #5(5-REG)LLD #1
MLLD/ELLD Manufacturer/Model V-R/RJ:FX1V (M)V-R:PLLD Series 8484 (E)V-R:PLLD Series 8484 (E)
If other,describe
MLLD/ELLD Third Party Certified?Yes Yes Yes
UST-10B Facility ID:00-0-0000009253
Page 10 of 12 6/8/2022 11:24 AM
MLLD/ELLD Testers MLLD/ELLD Tester #1
MLLD/ELLD Tester Name RICK UMBEL
MLLD/ELLD Testing Company Name PTS
MLLD/ELLD Testing Company Phone Number [phone]
Pressurized Piping LTT LTT #1
LTT Manufacturer/Method AcuRite:Training &Serv
If other,describe
LTT Third Party Certified?Yes
Pressurized Piping LTT Tester LTT Tester #1
LTT Tester Name RICK UMBEL
LTT Testing Company Name PTS
LTT Testing Company Phone Number [phone]
European Suction Tank #4(4-KERO)
Requirements for European suction piping verified?Yes
Source of information for European Suction verification.Installer Certification Letter
If other,specify
AUTOMATIC TANK GAUGE
ATG Systems ATG #1
ATG Manufacturer/Model V-R:TLS-350 CSLD
If other,describe
ATG Third Party Certified?Yes
Is ATG console operational?Yes
Tanks #1(1-PREM2),#2(2-MID),#3(3-PREM1),#4(4-KERO),#5(5-REG)
ATG Monthly LD Tank #1(1-PREM2)Tank #2(2-MID)Tank #3(3-PREM1)Tank #4(4-KERO)Tank #5(5-REG)
2022 Jun Pass Pass Pass Pass Pass
2022 May Pass Pass Pass Pass Pass
2022 Apr Pass Pass Pass Pass Pass
2022 Mar Pass Pass Pass Pass Pass
2022 Feb Pass Pass Pass Pass Pass
2022 Jan Pass Pass Pass Pass Pass
2021 Dec Pass Pass Pass Pass Pass
2021 Nov Pass Pass Pass Pass Pass
2021 Oct Pass Pass Pass Pass Pass
2021 Sep Pass Pass Pass Pass Pass
UST-10B Facility ID:00-0-0000009253
Page 11 of 12 6/8/2022 11:24 AM
ATG Monthly LD Tank #1(1-PREM2)Tank #2(2-MID)Tank #3(3-PREM1)Tank #4(4-KERO)Tank #5(5-REG)
2021 Aug Pass Pass Pass Pass Pass
2021 Jul Pass Pass Pass Pass Pass
ATG Conclusions
Leak Detection Requirements Met?Yes
Do the results indicate a suspected release?
Issues
TEMPORARY CLOSURE
Temporary Closure
Temporary Closure Requirements Met?Yes
Issues
REPAIRS
Repairs
Any Repair Issues?No
Issues
Delivery Information Tank #1(1-PREM2)Tank #2(2-MID)Tank #3(3-PREM1)Tank #4(4-KERO)Tank #5(5-REG)
All deliveries made to permitted tanks Yes Yes Yes Yes Yes
TRANSPORTER/FUEL DELIVERY INFORMATION
Name Address Phone
HUFFMAN OIL
UST-10B Facility ID:00-0-0000009253
Page 12 of 12 6/8/2022 11:24 AM
SITE DIAGRAM 1

Appendix II - Boring Logs, Well Construction Details and Well
Construction Records

S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.0
223.0
1365
988.0 Yes
30
No
25
Yes
20 Sandy Silt , Brown, Micaceous Wet- 38 feet
No
15
Yes
10
Sandy Silt, Red, Brown, Micaceous
5 DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESClayey Silt, Red
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable W. Watterson
DATE DRILLED:Monday, July 18, 2022 45
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-16066 NC 704 Highway East, Sandy Ridge, NC
10.0
214.0
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE75.0
6.0
2.0
60
55
50
No
45 Boring Terminated at 45 Ft-BGS
Yes
40
35
No
DRILLING METHOD: DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESHAMMER TYPE: Not Applicable W. Watterson
SAMPLING METHOD: Macro-Core Sampler
DRILL RIG: Geoprobe 7822 DT
DRILLER: Environmental Drilling and Probing Services, LLC
PROJECT:D&M Grocery
BORING LOG: MW-16066 NC 704 Highway East, Sandy Ridge, NC
DATE DRILLED:Monday, July 18, 2022 45
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE7.2
16.3
28.2
238.0
2031
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-26066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course, .,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable C. McMechen
No
5
Fill, Clayey Silt, Orange, Dry,
Yes
10
Residuum, Silt, Brown, Dry, Moist at 25 feet, Strong Petroleum Odors at 20 feet
No
15
Yes
20
Yes
25
Yes
30
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE61.0
18.0
7.0
0.5
1.6 Yes
30
Yes
25
Yes
20
No
15
Yes
10
Residuum, Silt, Brown, Tan, Mica, Dry
No
5
Fill, Clayey Silt, Orange, Dry DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable W. Watterson
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-36066 NC 704 Highway East, Sandy Ridge, NC
11
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE27.5
38.8
160.9
654.2
1212
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-16066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course, .,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable C. McMechen
No
5
Fill, Clayey Silt, Orange, Dry,
Yes
10
Residuum, Silt, Brown, Stained soil at 10 feet, Dry, Moist at 25 feet, wet at 30 feet, Strong Petroleum
No
15
Yes
20
Yes
25
Yes
30
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.4
2.6
3.0
152.0
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-26066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5 Residuum, Silt, Tan, Brown, Trace Fine Sand and Mica Dry,
Residuum, Silt, Orange, Brown, Dry,
No
10
Residuum, Sandy Silt, Brown, Fine, Mica Dry,
No
15
No
20 Saprolite, Silt, Brown, Gold, Trace Small Gravel; Very Micaceous, Dry, Unidentified Odor at 24 ft.
Yes
25 Boring Terminated at 25 Ft-BGS
30
34.2
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE19.7
15.7
2.7
37.8
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-36066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
Residuum, Silt, Tan, Brown, Trace Fine Sand and Mica Dry, No
5
Residuum, Clayey Silt, Orange, Brown, Moist,
Yes
10
Residuum, Sandy Silt, Brown, Fine, Mica Dry,
No
15
No
20 Saprolite, Silt, Brown, Gold, Trace Small Gravel; Very Micaceous, Dry, Slight Petroleum Odors
Yes
25 Boring Terminated at 25 Ft-BGS
30
6.2
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.2
13.4
16.4
36.1
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-46066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
Residuum, Silt, Tan, Brown, Trace Fine Sand and Mica Dry, No
5
Residuum, Silt, Orange, Brown, Dry,
No
10
Residuum, Sandy Silt, Brown, Fine, Mica with Quartz Veins Dry,
Yes
15
No
20 Saprolite, Silt, Brown, Gold, Trace Small Gravel; Very Micaceous, Dry, Unidentified Odor
Yes
25 Boring Terminated at 25 Ft-BGS
30
10.5
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.7
19.1
14.8
51.0
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-56066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
Residuum, Silt, Tan, Brown, Trace Fine Sand and Mica Dry,
No
5
Residuum, Silt, Orange, Brown, Dry,
Residuum, Sandy Silt, Brown, Fine, Mica Dry,
No
10
No
15
Saprolite, Silt, Brown, Gold, Trace Small Gravel; Very Micaceous, Dry, Slight Petroleum Odors Yes
20
No
25 Boring Terminated at 25 Ft-BGS
30
61.7
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.4
3.4
18.6
125.1
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-66066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5 Saprolite, Sandy Silt, Brown, Fine, Seam Quartz Veins, Dry,
Fill, Silt, Brown, Slight Mica Moist,
Residuum, Silt, Orange, Brown, Moist,
No
10
Saprolite, Silt, Brown, Gold, Trace Small Quartz Gravel, Dry, Petroleum Odor at 19-25 ft. No
15
Yes
20
No
25 Boring Terminated at 25 Ft-BGS
30
140
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE49.8
2.2
114.4
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-76066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5
Fill, Silt, Tan, Brown, Trace Fine Sand, Slight Mica Moist, No Recovery 10-15 ft.
No
10
15 Residuum, Sandy Silt, Brown, Fine, Moist, Petroleum Odors
No
20
Yes
25 Boring Terminated at 25 Ft-BGS
30
137
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE1.9
2.6
1.2
DATE DRILLED:Monday, November 28, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-86066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
Residuum, Silt, Tan, Brown, Trace Fine Sand, Slight Mica Moist, No
5
Residuum, Clayey Silt, Orange, Brown, Moist,
Saprolite, Silt, Brown, Gold, Trace Small Gravel, Very Micaceous Moist, No
10
No
15
Yes
20 Boring Terminated at 20 Ft-BGS
25
30
7.5
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.6
1.7
1.6
16.2
DATE DRILLED:Monday, November 28, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-96066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5
Fill, Sand, Tan, Coarse, Fine, Moist,
Residuum, Silt, Tan, Brown, Trace Fine Sand, Slight Mica Moist, Slight Petroleum Odor at 15-16 ft.
No
10
No
15 Yes
Saprolite, Silt, Brown, Gold, Very Micaceous, Moist,
No
20 Boring Terminated at 20 Ft-BGS
Residuum, Sandy Silt, Brown, Fine, Mica, Moist,
25
30
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.0
1.2
5.6
185.0
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-106066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5
Fill, Sand, Tan, Coarse, Fine, Moist,
No
10
Residuum, Silt, Tan, Brown, Trace Fine Sand, Slight Mica Moist,
No
15
Saprolite, Silt, Brown, Gold, Very Micaceous, Moist, No
20
Yes
25 Boring Terminated at 25 Ft-BGS
30
60.8
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.1
5.0
154.0
DATE DRILLED:Monday, November 28, 2022 25
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-116066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5
Fill, Sand, Tan, Coarse, Fine, No Recovery to 5-10 ft., Moist,
10
No
15 Residuum, Sandy Silt, Brown, Fine, Mica, Dry,
Residuum, Silt, Tan, Brown, Trace Fine Sand, Slight Mica Moist,
No
20
Saprolite, Silt, Brown, Gold, Moist, Slight Petroleum Odor, Strong Odor at 24 ft.
Yes
25 Boring Terminated at 25 Ft-BGS
30
50.8
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.1
1.7
11.6
DATE DRILLED:Monday, November 28, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-126066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
No
5
Fill, Silt, Tan, Brown, Poor Recovery to 5 ft., Dry,
Residuum, Sandy Silt, Tan, Brown, Mica, Dry,
No
10
Saprolite, Silt, Brown, Gold, Very Micaceous, Moist, Slight Petroleum Odors
No
15
Yes
20 Boring Terminated at 20 Ft-BGS
25
30
15.2
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE1.2
10.0
2.0
DATE DRILLED:Monday, November 28, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-136066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: L. Butler
Residuum, Silt, Tan, Brown, Trace Fine Sand, Moist,
No
5
Residuum, Clay Silt, Orange , Brown, Dry,
Saprolite, Sandy Silt, Brown, Fine, Moist, No
10
Saprolite, Silt, Gold, Brown, Trace Small Gravel, Very Micaceous, Dry,
Yes
15
No
20 Boring Terminated at 20 Ft-BGS
25
30
2.5
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE7.5
2.8
1.8
DATE DRILLED:Tuesday, November 29, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-146066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Cody McMechen
No
5
Residuum, Silt, Tan, Brown, Dry,
Fill, Clay Silt, Orange , Brown, Dry,
Residuum, Sandy Silt, Brown, Fine, Dry, No
10
Residuum, Silt, Gold, Brown, Dry, Yes
15
No
20 Boring Terminated at 20 Ft-BGS
25
30
1.7
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.6
7.6
4.8
30
25
No
20 Boring Terminated at 20 Ft-BGS
Residuum, Silt, Gold, Brown, Dry,
No
15
Residuum, Sandy Silt, Brown, Fine, Dry,
Yes
10
No
5
Residuum, Silt, Tan, Brown, Dry,
Fill, Clay Silt, Orange , Brown, Dry, DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Cody McMechen
DATE DRILLED:Tuesday, November 29, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-156066 NC 704 Highway East, Sandy Ridge, NC
6.4
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.5
5.0
2.2
30
25
No
20 Boring Terminated at 20 Ft-BGS
Residuum, Silt, Gold, Brown, Dry, Yes
15
No
10
No
5
Residuum, Silt, Tan, Brown, Dry, DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESResiduum, Sandy Silt, Brown, Fine, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Cody McMechen
DATE DRILLED:Tuesday, November 29, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-166066 NC 704 Highway East, Sandy Ridge, NC
1.8
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE15.5
2.9
4.2
30
25
No
20 Boring Terminated at 20 Ft-BGS
Residuum, Sandy Silt, Brown, Fine, Dry, No
15
No
10
Residuum, Silt, Tan, Brown, Dry,
Fill, Clay Silt, Orange , Brown, Dry, Yes
5
Fill, Sandy Clay, Brown, Orange, Fine, Dry, DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Cody McMechen
DATE DRILLED:Tuesday, November 29, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-176066 NC 704 Highway East, Sandy Ridge, NC
19.0
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.9
7.3
2.1
30
25
No
20 Boring Terminated at 20 Ft-BGS
Residuum, Silt, Gold, Brown, Dry,
No
15
Residuum, Sandy Silt, Brown, Fine, Dry,
Yes
10
Residuum, Silt, Tan, Brown, Dry,
No
5
Fill, Clay Silt, Orange , Brown, Dry, DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESConcrete, Concrete/Gravel,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (3-in. OD)
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Cody McMechen
DATE DRILLED:Tuesday, November 29, 2022 20
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-186066 NC 704 Highway East, Sandy Ridge, NC
1.4
Well ID
MW-1
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.1 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.5 ft
0.5 to 25.0
25.0 to 40.0
Top of Seal - 21.0 0.1 ft-bgs
Top of Filter Pack - 23.0 0.1 ft-bgs
0.5 to 21.0
Top of Screen - 25.0 0.1 ft-bgs
21.0 to 23.0
Screened Interval -15.0 0.1 ft-bgs
23.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 40.5 0.1 ft-bgs
Form Revision Date:
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable
40.0
35.0
Northing (0.1 ft)Date/Time
7/19/22 12:20
Total Well Depth (0.1 ft-bgs)
31.45 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
9/1/17 2:10 PM
TBD - To Be Determined
Notes: Free product detected; lowermost screened interval length = 5 feet
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
No
For lithologic information
see attached boring log
BTOC - Below Top of Casing
Well ID
MW-2
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.1 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.3 ft
0.3 to 20.0
20.0 to 40.0
Top of Seal - 15.0 0.1 ft-bgs
Top of Filter Pack - 18.0 0.1 ft-bgs
0.3 to 15.0
Top of Screen - 20.0 0.1 ft-bgs
15.0 to 18.0
Screened Interval -20.0 0.1 ft-bgs
18.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 41.0 0.1 ft-bgs
Form Revision Date:9/1/17 2:10 PM
TBD - To Be Determined
Notes:
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
For lithologic information
see attached boring log
15
BTOC - Below Top of Casing
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
40.0
37.0
Northing (0.1 ft)Date/Time
7/19/22 13:15
Total Well Depth (0.1 ft-bgs)
32.66 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable
Well ID
MW-3
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.01 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.4 ft
0.4 to 20.0
20.0 to 40.0
Top of Seal - 16.0 0.1 ft-bgs
Top of Filter Pack - 18.0 0.1 ft-bgs
0.4 to 16.0
Top of Screen - 20.0 0.1 ft-bgs
16.0 to 18.0
Screened Interval -20.0 0.1 ft-bgs
18.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 40.0 0.1 ft-bgs
Form Revision Date:9/1/17 2:10 PM
TBD - To Be Determined
Notes:
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
For lithologic information
see attached boring log
10
BTOC - Below Top of Casing
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
40.0
Dry
Northing (0.1 ft)Date/Time
7/19/22 0:00
Total Well Depth (0.1 ft-bgs)
33.97 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable

Appendix III- Groundwater Sampling Forms and Environmental
Field Reports

° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
31.84 ft-TOC inch
40.85 ft-TOC gal
9.01 feet gal
15 ft-GRD gal
ft-GRD
End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
Qty Container Pres.Qty Pres.
(1)
Notes:
Form Revision Date:
Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:
Project Location:
Project Number:
Source Well:
D&M Grocery
6066 NC-704, Sandy Ridge, NC 27046
22580285
MW-1
Purge Date: July 20, 2022
Analytical Data
Method Method
Did not develop/ purge or sample due to presence of free product from 31.65 ft below ToC to 31.84 ft below ToC.
9/13/17 8:00 AM
Name Signature
Cody McMechen
Date
8/3/2022
Container
Sample Method:Sample Time:
Total Volume Purged:Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
(Gal)
Stickup Height:
Well Purging Information
Purge Method:Purge Start Time:
Total Well Depth:Well Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
1.5
4.4
7.4
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter
Conductivity 1,413 1,413
7.0
µS/cm
2
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
pH 4.00, 7.00, 10.00
Air Temp:
July 20, 2022
90
Sample Time:
Sample Date:
Weather:
Locked?:
Sampled By:
Yes
Cody McMechen
Sunny
° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
32.60 ft-TOC inch
40.22 ft-TOC gal
7.62 feet gal
20 ft-GRD gal
ft-GRD
12:35 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
14:40 5.4 19.4 375
14:40
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
1 250mL P HNO3
2 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Cody McMechen 8/3/2022
Developed/ purged well until turbidity was lowered to an acceptable level.
9/13/17 8:00 AM
EDB 504.1
Name Signature Date
Metals 6010 (Total)
VPH MADEP
Analytical Data
Method Method Container
VOCs 6200
Sample Method:Bailer Sample Time:
(Gal)
15.0
Total Volume Purged:15.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 6.2
Stickup Height:
Well Purging Information
Purge Method:Submersible Pump Purge Start Time:13:30
Total Well Depth:Well Volume 1.2
Height of Water Column:3 * Well Volume 3.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather: Sunny Air Temp: 90
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?: Yes Sample Date: July 20, 2022
Sampled By: Cody McMechen Sample Time: 14:40
Project Number: 22580285 Purge Date: July 20, 2022
Source Well:MW-2 Purge Time (Min.): 55
GROUNDWATER SAMPLING FORM
Project Name: D&M Grocery
Project Location: 6066 NC-704, Sandy Ridge, NC 27046
° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
33.83 ft-TOC inch
40.21 ft-TOC gal
6.38 feet gal
20 ft-GRD gal
ft-GRD
10:55 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
14:15 4.7 18.2 203
14:15
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
1 250mL P HNO3
2 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Cody McMechen 8/3/2022
Developed/ purged well until turbidity was lowered to an acceptable level.
9/13/17 8:00 AM
EDB 504.1
Name Signature Date
Metals 6010 (Total)
VPH MADEP
Analytical Data
Method Method Container
VOCs 6200
Sample Method:Bailer Sample Time:
(Gal)
10.3 No Odors
Total Volume Purged:10.3 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 5.2
Stickup Height:
Well Purging Information
Purge Method:Submersible Pump Purge Start Time:11:45
Total Well Depth:Well Volume 1.0
Height of Water Column:3 * Well Volume 3.1
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather: Sunny Air Temp: 85
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?: Yes Sample Date: July 20, 2022
Sampled By: Cody McMechen Sample Time: 14:15
Project Number: 22580285 Purge Date: July 20, 2022
Source Well:MW-3 Purge Time (Min.): 50
GROUNDWATER SAMPLING FORM
Project Name: D&M Grocery
Project Location: 6066 NC-704, Sandy Ridge, NC 27046

Hours Mileage Signature of S&ME Personnel
2 70 Wayne Watterson

S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
7/26/2022
Job Number:
22580285
Project Name:
D&M Grocery
Weather/Temperature:
Clear, hot
Project Location:
Sandy Ridge, NC
Notes By:
☒
Present at the Site:
Wayne Watterson
☐

Arrived at the property at approximately 1250.
The pads for monitoring wells MW-1, 2, and 3, installed last week, were in good condition. I asked the
store employee if there were or if there appeared to be any changes to the UST equipment since S&ME
completed the soil probes and monitoring well installations last week. He said there was no change to
the system.
I opened monitoring wells and checked depth to water/product in the monitoring wells. Information is
provided below
well Depth to water (ft) Depth to product (ft) Notes
MW-1 32.88 31.45 Used oil/water interface
for measurements
MW-2 32.66 No product Used oil/water interface
for measurements
MW-3 33.97 No product Used water level probe.
No odors or observed
product or sheen on
probe.

After taking depth to water/product measurements, I closed the wells and bolted down the well covers.

I left the site at approximately 1320.

Attachments:

Equipment Used

Appendix IV- Analytical Reports

ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-218771-1
Client Project/Site: D&M Grocery
For:
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, North Carolina 27409
Attn: Wayne Watterson
Authorized for release by:
8/4/2022 5:25:53 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
Definitions/Glossary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
E Result exceeded calibration range.
H Sample was prepped or analyzed beyond the specified holding time
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1-Surrogate recovery exceeds control limits, low biased.
GC Semi VOA
Qualifier Description
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Qualifier
S1+Surrogate recovery exceeds control limits, high biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 96 8/4/2022
1
2
3
4
5
6
7
8
9
10
11
12
Sample Summary
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Lab Sample ID Client Sample ID Matrix Collected Received
680-218771-1 MW-1-10 Soil 07/18/22 10:45 07/23/22 09:30
680-218771-2 MW-1-20 Soil 07/18/22 10:50 07/23/22 09:30
680-218771-3 MW-1-30 Soil 07/18/22 10:55 07/23/22 09:30
680-218771-4 MW-3-10 Soil 07/18/22 11:35 07/23/22 09:30
680-218771-5 MW-3-20 Soil 07/18/22 11:45 07/23/22 09:30
680-218771-6 MW-3-25 Soil 07/19/22 16:10 07/23/22 09:30
680-218771-7 MW-3-30 Soil 07/19/22 16:15 07/23/22 09:30
680-218771-8 MW-2-10 Soil 07/19/22 16:20 07/23/22 09:30
680-218771-9 MW-2-20 Soil 07/19/22 16:26 07/23/22 09:30
680-218771-10 MW-2-25 Soil 07/19/22 16:30 07/23/22 09:30
680-218771-11 MW-2-30 Soil 07/19/22 16:35 07/23/22 09:30
680-218771-12 P-1-10 Soil 07/19/22 16:44 07/23/22 09:30
680-218771-13 P-1-20 Soil 07/19/22 16:48 07/23/22 09:30
680-218771-14 P-1-25 Soil 07/19/22 16:50 07/23/22 09:30
680-218771-15 P-1-30 Soil 07/19/22 16:55 07/23/22 09:30
680-218771-16 MW-3 Ground Water 07/20/22 14:15 07/23/22 09:30
680-218771-17 MW-2 Ground Water 07/20/22 14:40 07/23/22 09:30
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Case Narrative
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Job ID: 680-218771-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-218771-1
Receipt
The samples were received on 7/23/2022 9:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 16.6°C
Receipt Exceptions
Received warm with very little water in cooler. Cooler was in transit for 3 days. Client was contacted and the lab received permission
to proceed with the analyses.
GC/MS VOA
Method SM6200_B: Reanalysis of the following sample(s) was performed outside of the analytical holding time due to dilutions. The
samples are one day out of hold: MW-2 (680-218771-17).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Gasoline Range Organics
Method 8015D_GRO: Surrogate recovery for the following sample was outside control limits: MW-1-20 (680-218771-2). Re-analysis was
performed and surrogate recovery was outside control limits. Sample matrix interference is suspected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method 504.1: Sample was moved to an empty vial because of sediment in the following sample: MW-3 (680-218771-16) and MW-2
(680-218771-17)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-1Client Sample ID: MW-1-10
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.244 0.0634 mg/Kg ☼07/26/22 10:32 07/27/22 18:29 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,1-Trichloroethane ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2,2-Tetrachloroethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.244 0.0732 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2-Trichloroethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloroethane ND
0.244 0.176 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloroethene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloropropene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,3-Trichlorobenzene ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,3-Trichloropropane ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,4-Trichlorobenzene ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,4-Trimethylbenzene 2.01
0.488 0.0780 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dibromo-3-Chloropropane ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichlorobenzene ND
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichloroethane ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichloropropane ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3,5-Trimethylbenzene 0.487
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3-Dichlorobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3-Dichloropropane ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,4-Dichlorobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2,2-Dichloropropane ND
1.22 0.449 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Butanone (MEK)ND
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Chlorotoluene ND
1.22 0.927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Hexanone ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Chlorotoluene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Isopropyltoluene ND
1.22 0.878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Methyl-2-pentanone (MIBK)ND
2.44 0.537 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Acetone ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Benzene ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromoform ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromomethane ND *+
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Carbon disulfide ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Carbon tetrachloride ND
0.244 0.0683 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorobenzene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorobromomethane ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorodibromomethane ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloroethane ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloroform ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloromethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼cis-1,2-Dichloroethene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼cis-1,3-Dichloropropene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Dibromomethane ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Dichlorobromomethane ND
0.488 0.488 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethyl acetate ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethylbenzene 0.944
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethylene Dibromide ND
0.244 0.200 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Hexachlorobutadiene ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-1Client Sample ID: MW-1-10
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.244 0.0829 mg/Kg ☼07/26/22 10:32 07/27/22 18:29 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.488 0.0732 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Isopropyl ether ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Isopropylbenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Methyl tert-butyl ether ND *+
0.488 0.390 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Methylene Chloride ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼m-Xylene & p-Xylene 3.97
0.244 0.151 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Naphthalene 0.188 J
0.244 0.0927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼n-Butylbenzene 0.106 J
0.244 0.210 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼n-Heptane ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼N-Propylbenzene 0.319
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼o-Xylene 1.92
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼sec-Butylbenzene ND
0.244 0.0927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Styrene ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼tert-Butylbenzene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Tetrachloroethene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Toluene 2.56
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,2-Dichloroethene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,3-Dichloropropene ND
0.488 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,4-Dichloro-2-butene ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Trichloroethene ND
0.244 0.151 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Trichlorofluoromethane ND
0.488 0.268 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Vinyl acetate ND
0.244 0.137 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Vinyl chloride ND
0.488 0.176 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Xylenes, Total 5.89
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 18:29 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 07/26/22 10:32 07/27/22 18:29 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 18:29 4065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 18:29 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
55.1 14.1 3.52 mg/Kg ☼07/26/22 10:32 07/28/22 15:36 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 15:36 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.304 0.0791 mg/Kg ☼07/26/22 10:32 07/26/22 20:13 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,1-Trichloroethane ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2,2-Tetrachloroethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.304 0.0913 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2-Trichloroethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloroethane ND
0.304 0.219 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloroethene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloropropene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,3-Trichlorobenzene ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,3-Trichloropropane ND
0.304 0.152 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,4-Trichlorobenzene ND
0.609 0.0974 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dibromo-3-Chloropropane ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichlorobenzene ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichloroethane ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichloropropane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,3-Dichlorobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,3-Dichloropropane ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,4-Dichlorobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2,2-Dichloropropane ND
1.52 0.560 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Butanone (MEK)ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Chlorotoluene ND
1.52 1.16 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Hexanone ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Chlorotoluene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Isopropyltoluene 7.36
1.52 1.10 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Methyl-2-pentanone (MIBK)ND
3.04 0.670 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Acetone ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Benzene 1.12
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromoform ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromomethane ND *+
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Carbon disulfide ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Carbon tetrachloride ND
0.304 0.0852 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorobenzene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorobromomethane ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorodibromomethane ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloroethane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloroform ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloromethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼cis-1,2-Dichloroethene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼cis-1,3-Dichloropropene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Dibromomethane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Dichlorobromomethane ND
0.609 0.609 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Ethyl acetate ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Ethylene Dibromide ND
0.304 0.250 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Hexachlorobutadiene ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Hexane 1.95
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Iodomethane ND
0.609 0.0913 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Isopropyl ether ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Methyl tert-butyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride ND 0.609 0.487 mg/Kg ☼07/26/22 10:32 07/26/22 20:13 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.304 0.116 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼n-Butylbenzene 8.86
0.304 0.262 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼n-Heptane 6.82
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼sec-Butylbenzene 2.48
0.304 0.116 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Styrene ND
0.304 0.152 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼tert-Butylbenzene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Tetrachloroethene ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,2-Dichloroethene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,3-Dichloropropene ND
0.609 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,4-Dichloro-2-butene ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Trichloroethene ND
0.304 0.189 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Trichlorofluoromethane ND
0.609 0.335 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Vinyl acetate ND
0.304 0.170 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)90 65-130 07/26/22 10:32 07/26/22 20:13 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)113 07/26/22 10:32 07/26/22 20:13 4065-130
Dibromofluoromethane (Surr)90 07/26/22 10:32 07/26/22 20:13 4065-130
Toluene-d8 (Surr)92 07/26/22 10:32 07/26/22 20:13 4065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 222 7.61 3.80 mg/Kg ☼07/26/22 10:32 07/27/22 16:28 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.61 3.65 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼1,3,5-Trimethylbenzene 57.1
7.61 3.20 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Ethylbenzene 78.4
7.61 3.35 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Isopropylbenzene 18.0
7.61 4.72 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Naphthalene 24.4
7.61 3.35 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼N-Propylbenzene 37.6
7.61 3.50 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼o-Xylene 147
7.61 3.96 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Toluene 95.8
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 16:28 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 16:28 100065-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 16:28 100065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 16:28 100065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL2
RL MDL
m-Xylene & p-Xylene 521 38.0 16.7 mg/Kg ☼07/26/22 10:32 08/01/22 17:33 5000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
76.1 27.4 mg/Kg 07/26/22 10:32 08/01/22 17:33 5000☼Xylenes, Total 768
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 08/01/22 17:33 5000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 07/26/22 10:32 08/01/22 17:33 500065-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 08/01/22 17:33 500065-130
Toluene-d8 (Surr)97 07/26/22 10:32 08/01/22 17:33 500065-130
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
1460 157 39.3 mg/Kg ☼07/26/22 10:32 07/29/22 19:45 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 68 S1-70-131 07/26/22 10:32 07/29/22 19:45 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-3Client Sample ID: MW-1-30
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 6.74 1.75 mg/Kg ☼07/26/22 10:32 07/27/22 16:52 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,1-Trichloroethane ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2,2-Tetrachloroethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
6.74 2.02 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2-Trichloroethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloroethane ND
6.74 4.85 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloroethene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloropropene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,3-Trichlorobenzene ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,3-Trichloropropane ND
6.74 3.37 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,4-Trichlorobenzene ND
13.5 2.16 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dibromo-3-Chloropropane ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichlorobenzene ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichloroethane ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichloropropane ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3,5-Trimethylbenzene 129
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3-Dichlorobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3-Dichloropropane ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,4-Dichlorobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2,2-Dichloropropane ND
33.7 12.4 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Butanone (MEK)ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Chlorotoluene ND
33.7 25.6 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Hexanone ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Chlorotoluene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Isopropyltoluene 5.77 J
33.7 24.3 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Methyl-2-pentanone (MIBK)ND
67.4 14.8 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Acetone ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Benzene 25.3
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromoform ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromomethane ND *+
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Carbon disulfide ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Carbon tetrachloride ND
6.74 1.89 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorobenzene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorobromomethane ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorodibromomethane ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloroethane ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloroform ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloromethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼cis-1,2-Dichloroethene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼cis-1,3-Dichloropropene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Dibromomethane ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Dichlorobromomethane ND
13.5 13.5 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Ethyl acetate ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Ethylene Dibromide ND
6.74 5.53 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Hexachlorobutadiene ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Hexane 32.3
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Iodomethane ND
13.5 2.02 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Isopropyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-3Client Sample ID: MW-1-30
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropylbenzene 31.7 6.74 2.97 mg/Kg ☼07/26/22 10:32 07/27/22 16:52 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Methyl tert-butyl ether ND *+
13.5 10.8 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Methylene Chloride ND
6.74 4.18 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Naphthalene 45.8
6.74 2.56 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼n-Butylbenzene 29.7
6.74 5.80 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼n-Heptane 67.4
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼N-Propylbenzene 94.0
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼sec-Butylbenzene ND
6.74 2.56 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Styrene ND
6.74 3.37 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼tert-Butylbenzene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Tetrachloroethene ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,2-Dichloroethene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,3-Dichloropropene ND
13.5 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,4-Dichloro-2-butene ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Trichloroethene ND
6.74 4.18 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Trichlorofluoromethane ND
13.5 7.42 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Vinyl acetate ND
6.74 3.77 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 16:52 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 16:52 100065-130
Dibromofluoromethane (Surr)99 07/26/22 10:32 07/27/22 16:52 100065-130
Toluene-d8 (Surr)99 07/26/22 10:32 07/27/22 16:52 100065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 371 33.7 16.9 mg/Kg ☼07/26/22 10:32 07/28/22 21:33 5000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
33.7 14.2 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Ethylbenzene 253
33.7 14.8 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼m-Xylene & p-Xylene 951
33.7 15.5 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼o-Xylene 411
33.7 17.5 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Toluene 764
67.4 24.3 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Xylenes, Total 1360
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/28/22 21:33 5000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 07/26/22 10:32 07/28/22 21:33 500065-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/28/22 21:33 500065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/28/22 21:33 500065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
19000 2730 683 mg/Kg ☼07/26/22 10:32 08/01/22 16:14 20000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 80 70-131 07/26/22 10:32 08/01/22 16:14 20000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-4Client Sample ID: MW-3-10
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00720 0.00187 mg/Kg ☼07/26/22 10:32 07/26/22 15:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,1-Trichloroethane ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2,2-Tetrachloroethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00720 0.00216 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2-Trichloroethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloroethane ND
0.00720 0.00519 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloroethene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloropropene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,3-Trichlorobenzene ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,3-Trichloropropane ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,4-Trichlorobenzene ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,4-Trimethylbenzene 0.0333
0.0144 0.00230 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dibromo-3-Chloropropane ND
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichlorobenzene ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichloroethane ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichloropropane ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3,5-Trimethylbenzene 0.0110
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3-Dichlorobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3-Dichloropropane ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,4-Dichlorobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2,2-Dichloropropane ND
0.0360 0.0133 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Butanone (MEK)ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Chlorotoluene ND
0.0360 0.0274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Hexanone ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Chlorotoluene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Isopropyltoluene ND
0.0360 0.0259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Methyl-2-pentanone (MIBK)ND
0.0720 0.0158 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Acetone 0.102
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Benzene 0.0527
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromoform ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromomethane ND *+
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Carbon disulfide ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Carbon tetrachloride ND
0.00720 0.00202 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorobenzene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorobromomethane ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorodibromomethane ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloroethane ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloroform ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloromethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼cis-1,2-Dichloroethene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼cis-1,3-Dichloropropene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Dibromomethane ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Dichlorobromomethane ND
0.0144 0.0144 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethyl acetate ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethylbenzene 0.115
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethylene Dibromide ND
0.00720 0.00591 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Hexachlorobutadiene ND
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Hexane 0.00631 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-4Client Sample ID: MW-3-10
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00247 J 0.00720 0.00245 mg/Kg ☼07/26/22 10:32 07/26/22 15:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0144 0.00216 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Isopropyl ether ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Isopropylbenzene 0.00578 J
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Methyl tert-butyl ether ND *+
0.0144 0.0115 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Methylene Chloride ND
0.00720 0.00447 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Naphthalene ND
0.00720 0.00274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼n-Butylbenzene ND
0.00720 0.00619 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼n-Heptane 0.00849
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼N-Propylbenzene 0.0128
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼o-Xylene 0.161
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼sec-Butylbenzene ND
0.00720 0.00274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Styrene ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼tert-Butylbenzene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Tetrachloroethene ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,2-Dichloroethene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,3-Dichloropropene ND
0.0144 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,4-Dichloro-2-butene ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Trichloroethene ND
0.00720 0.00447 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Trichlorofluoromethane ND
0.0144 0.00792 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Vinyl acetate ND
0.00720 0.00403 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Vinyl chloride ND
0.0144 0.00519 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Xylenes, Total 0.548 E
1,2-Dichloroethane-d4 (Surr)105 65-130 07/26/22 10:32 07/26/22 15:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/26/22 15:23 165-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 07/26/22 15:23 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/26/22 15:23 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
m-Xylene & p-Xylene 0.715 0.281 0.124 mg/Kg ☼07/26/22 10:32 07/27/22 18:53 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.281 0.146 mg/Kg 07/26/22 10:32 07/27/22 18:53 40☼Toluene 1.06
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/27/22 18:53 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 18:53 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 18:53 4065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 18:53 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
9.57 J 14.1 3.53 mg/Kg ☼07/26/22 10:32 08/01/22 14:25 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 08/01/22 14:25 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-5Client Sample ID: MW-3-20
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00990 0.00257 mg/Kg ☼07/26/22 10:32 07/26/22 15:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,1-Trichloroethane ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2,2-Tetrachloroethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00990 0.00297 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2-Trichloroethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloroethane ND
0.00990 0.00713 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloroethene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloropropene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,3-Trichlorobenzene ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,3-Trichloropropane ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,4-Trichlorobenzene ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,4-Trimethylbenzene 0.0328
0.0198 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dibromo-3-Chloropropane ND
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichlorobenzene ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichloroethane ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichloropropane ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3,5-Trimethylbenzene 0.00967 J
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3-Dichlorobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3-Dichloropropane ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,4-Dichlorobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2,2-Dichloropropane ND
0.0495 0.0182 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Butanone (MEK)ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Chlorotoluene ND
0.0495 0.0376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Hexanone ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Chlorotoluene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Isopropyltoluene ND
0.0495 0.0356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Methyl-2-pentanone (MIBK)ND
0.0990 0.0218 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Acetone 0.0351 J
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Benzene 0.0331
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromoform ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromomethane ND *+
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Carbon disulfide ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Carbon tetrachloride ND
0.00990 0.00277 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorobenzene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorobromomethane ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorodibromomethane ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloroethane ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloroform ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloromethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼cis-1,2-Dichloroethene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼cis-1,3-Dichloropropene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Dibromomethane ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Dichlorobromomethane ND
0.0198 0.0198 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethyl acetate ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethylbenzene 0.0845
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethylene Dibromide ND
0.00990 0.00812 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Hexachlorobutadiene ND
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Hexane 0.00407 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-5Client Sample ID: MW-3-20
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00990 0.00337 mg/Kg ☼07/26/22 10:32 07/26/22 15:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0198 0.00297 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Isopropyl ether ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Isopropylbenzene 0.00513 J
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Methyl tert-butyl ether ND *+
0.0198 0.0158 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Methylene Chloride ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼m-Xylene & p-Xylene 0.286
0.00990 0.00614 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Naphthalene ND
0.00990 0.00376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼n-Butylbenzene ND
0.00990 0.00851 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼n-Heptane ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼N-Propylbenzene 0.0106
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼o-Xylene 0.136
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼sec-Butylbenzene ND
0.00990 0.00376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Styrene ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼tert-Butylbenzene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Tetrachloroethene ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,2-Dichloroethene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,3-Dichloropropene ND
0.0198 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,4-Dichloro-2-butene ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Trichloroethene ND
0.00990 0.00614 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Trichlorofluoromethane ND
0.0198 0.0109 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Vinyl acetate ND
0.00990 0.00554 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Vinyl chloride ND
0.0198 0.00713 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Xylenes, Total 0.422
1,2-Dichloroethane-d4 (Surr)108 65-130 07/26/22 10:32 07/26/22 15:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)111 07/26/22 10:32 07/26/22 15:47 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 15:47 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 15:47 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Toluene 1.68 0.394 0.205 mg/Kg ☼07/26/22 10:32 07/27/22 19:17 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)100 65-130 07/26/22 10:32 07/27/22 19:17 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 19:17 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 19:17 4065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 19:17 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
12.1 J 21.2 5.30 mg/Kg ☼07/26/22 10:32 07/29/22 17:57 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 77 70-131 07/26/22 10:32 07/29/22 17:57 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-6Client Sample ID: MW-3-25
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00609 0.00158 mg/Kg ☼07/26/22 10:32 07/26/22 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,1-Trichloroethane ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2,2-Tetrachloroethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00609 0.00183 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2-Trichloroethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloroethane ND
0.00609 0.00438 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloroethene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloropropene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,3-Trichlorobenzene ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,3-Trichloropropane ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,4-Trichlorobenzene ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,4-Trimethylbenzene ND
0.0122 0.00195 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dibromo-3-Chloropropane ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichlorobenzene ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichloroethane ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichloropropane ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3,5-Trimethylbenzene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3-Dichlorobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3-Dichloropropane ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,4-Dichlorobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2,2-Dichloropropane ND
0.0304 0.0112 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Butanone (MEK)ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Chlorotoluene ND
0.0304 0.0231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Hexanone ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Chlorotoluene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Isopropyltoluene ND
0.0304 0.0219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Methyl-2-pentanone (MIBK)ND
0.0609 0.0134 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Acetone 0.0230 J
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Benzene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromoform ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromomethane ND *+
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Carbon disulfide ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Carbon tetrachloride ND
0.00609 0.00170 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorobenzene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorobromomethane ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorodibromomethane ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloroethane ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloroform ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloromethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼cis-1,2-Dichloroethene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼cis-1,3-Dichloropropene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Dibromomethane ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Dichlorobromomethane ND
0.0122 0.0122 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethyl acetate ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethylbenzene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethylene Dibromide ND
0.00609 0.00499 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Hexachlorobutadiene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-6Client Sample ID: MW-3-25
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00609 0.00207 mg/Kg ☼07/26/22 10:32 07/26/22 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0122 0.00183 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Isopropyl ether ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Isopropylbenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Methyl tert-butyl ether ND *+
0.0122 0.00974 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Methylene Chloride ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼m-Xylene & p-Xylene 0.00361 J
0.00609 0.00377 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Naphthalene ND
0.00609 0.00231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼n-Butylbenzene ND
0.00609 0.00524 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼n-Heptane ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼N-Propylbenzene ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼o-Xylene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼sec-Butylbenzene ND
0.00609 0.00231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Styrene ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼tert-Butylbenzene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Tetrachloroethene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Toluene 0.00383 J
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,2-Dichloroethene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,3-Dichloropropene ND
0.0122 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,4-Dichloro-2-butene ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Trichloroethene ND
0.00609 0.00377 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Trichlorofluoromethane ND
0.0122 0.00670 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Vinyl acetate ND
0.00609 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Vinyl chloride ND
0.0122 0.00438 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 07/26/22 16:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 16:11 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 16:11 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 16:11 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 12.7 3.19 mg/Kg ☼07/26/22 10:32 07/29/22 18:19 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 81 70-131 07/26/22 10:32 07/29/22 18:19 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-7Client Sample ID: MW-3-30
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00682 0.00177 mg/Kg ☼07/26/22 10:32 07/26/22 16:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,1-Trichloroethane ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2,2-Tetrachloroethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00682 0.00205 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2-Trichloroethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloroethane ND
0.00682 0.00491 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloroethene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloropropene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,3-Trichlorobenzene ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,3-Trichloropropane ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,4-Trichlorobenzene ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,4-Trimethylbenzene ND
0.0136 0.00218 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dibromo-3-Chloropropane ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichlorobenzene ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichloroethane ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichloropropane ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3,5-Trimethylbenzene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3-Dichlorobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3-Dichloropropane ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,4-Dichlorobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2,2-Dichloropropane ND
0.0341 0.0125 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Butanone (MEK)ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Chlorotoluene ND
0.0341 0.0259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Hexanone ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Chlorotoluene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Isopropyltoluene ND
0.0341 0.0245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Methyl-2-pentanone (MIBK)ND
0.0682 0.0150 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Acetone 0.0153 J
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Benzene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromoform ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromomethane ND *+
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Carbon disulfide ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Carbon tetrachloride ND
0.00682 0.00191 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorobenzene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorobromomethane ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorodibromomethane ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloroethane ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloroform ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloromethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼cis-1,2-Dichloroethene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼cis-1,3-Dichloropropene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Dibromomethane ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Dichlorobromomethane ND
0.0136 0.0136 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethyl acetate ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethylbenzene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethylene Dibromide ND
0.00682 0.00559 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Hexachlorobutadiene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-7Client Sample ID: MW-3-30
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00682 0.00232 mg/Kg ☼07/26/22 10:32 07/26/22 16:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0136 0.00205 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Isopropyl ether ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Isopropylbenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Methyl tert-butyl ether ND *+
0.0136 0.0109 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Methylene Chloride ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼m-Xylene & p-Xylene 0.00657 J
0.00682 0.00423 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Naphthalene ND
0.00682 0.00259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼n-Butylbenzene ND
0.00682 0.00586 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼n-Heptane ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼N-Propylbenzene ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼o-Xylene 0.00409 J
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼sec-Butylbenzene ND
0.00682 0.00259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Styrene ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼tert-Butylbenzene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Tetrachloroethene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Toluene 0.00707
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,2-Dichloroethene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,3-Dichloropropene ND
0.0136 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,4-Dichloro-2-butene ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Trichloroethene ND
0.00682 0.00423 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Trichlorofluoromethane ND
0.0136 0.00750 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Vinyl acetate ND
0.00682 0.00382 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Vinyl chloride ND
0.0136 0.00491 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Xylenes, Total 0.0107 J
1,2-Dichloroethane-d4 (Surr)107 65-130 07/26/22 10:32 07/26/22 16:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 16:35 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/26/22 16:35 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 16:35 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
11.4 J 15.1 3.78 mg/Kg ☼07/26/22 10:32 07/28/22 17:46 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/28/22 17:46 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-8Client Sample ID: MW-2-10
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00802 0.00208 mg/Kg ☼07/26/22 10:32 07/26/22 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,1-Trichloroethane ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2,2-Tetrachloroethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00802 0.00241 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2-Trichloroethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloroethane ND
0.00802 0.00577 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloroethene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloropropene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,3-Trichlorobenzene ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,3-Trichloropropane ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,4-Trichlorobenzene ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,4-Trimethylbenzene ND
0.0160 0.00257 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dibromo-3-Chloropropane ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichlorobenzene ND
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichloroethane ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichloropropane ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3,5-Trimethylbenzene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3-Dichlorobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3-Dichloropropane ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,4-Dichlorobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2,2-Dichloropropane ND
0.0401 0.0148 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Butanone (MEK)0.0519
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Chlorotoluene ND
0.0401 0.0305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Hexanone ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Chlorotoluene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Isopropyltoluene ND
0.0401 0.0289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Methyl-2-pentanone (MIBK)ND
0.0802 0.0176 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Acetone 0.188
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Benzene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromoform ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromomethane ND *+
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Carbon disulfide ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Carbon tetrachloride ND
0.00802 0.00224 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorobenzene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorobromomethane ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorodibromomethane ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloroethane ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloroform ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloromethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼cis-1,2-Dichloroethene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼cis-1,3-Dichloropropene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Dibromomethane ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Dichlorobromomethane ND
0.0160 0.0160 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethyl acetate ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethylbenzene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethylene Dibromide ND
0.00802 0.00657 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Hexachlorobutadiene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-8Client Sample ID: MW-2-10
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00320 J 0.00802 0.00273 mg/Kg ☼07/26/22 10:32 07/26/22 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0160 0.00241 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Isopropyl ether ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Isopropylbenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Methyl tert-butyl ether ND *+
0.0160 0.0128 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Methylene Chloride ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼m-Xylene & p-Xylene ND
0.00802 0.00497 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Naphthalene ND
0.00802 0.00305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼n-Butylbenzene ND
0.00802 0.00690 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼n-Heptane ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼N-Propylbenzene ND
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼o-Xylene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼sec-Butylbenzene ND
0.00802 0.00305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Styrene ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼tert-Butylbenzene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Tetrachloroethene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Toluene 0.00433 J
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,2-Dichloroethene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,3-Dichloropropene ND
0.0160 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,4-Dichloro-2-butene ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Trichloroethene ND
0.00802 0.00497 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Trichlorofluoromethane ND
0.0160 0.00882 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Vinyl acetate ND
0.00802 0.00449 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Vinyl chloride ND
0.0160 0.00577 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)104 65-130 07/26/22 10:32 07/26/22 17:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 17:00 165-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/26/22 17:00 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 17:00 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.7 3.93 mg/Kg ☼07/26/22 10:32 07/28/22 18:08 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/28/22 18:08 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-9Client Sample ID: MW-2-20
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00894 0.00233 mg/Kg ☼07/26/22 10:32 07/26/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,1-Trichloroethane ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2,2-Tetrachloroethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00894 0.00268 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2-Trichloroethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloroethane ND
0.00894 0.00644 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloroethene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloropropene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,3-Trichlorobenzene ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,3-Trichloropropane ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,4-Trichlorobenzene ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,4-Trimethylbenzene ND
0.0179 0.00286 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dibromo-3-Chloropropane ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichlorobenzene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichloroethane ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichloropropane ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3,5-Trimethylbenzene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3-Dichlorobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3-Dichloropropane ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,4-Dichlorobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2,2-Dichloropropane ND
0.0447 0.0165 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Butanone (MEK)1.26
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Chlorotoluene ND
0.0447 0.0340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Hexanone 0.187
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Chlorotoluene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Isopropyltoluene ND
0.0447 0.0322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Methyl-2-pentanone (MIBK)0.0639
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Benzene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromoform ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromomethane ND *+
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Carbon disulfide ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Carbon tetrachloride ND
0.00894 0.00250 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorobenzene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorobromomethane ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorodibromomethane ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloroethane ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloroform ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloromethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼cis-1,2-Dichloroethene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼cis-1,3-Dichloropropene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Dibromomethane ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Dichlorobromomethane ND
0.0179 0.0179 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethyl acetate ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethylbenzene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethylene Dibromide ND
0.00894 0.00733 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Hexachlorobutadiene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Hexane ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Iodomethane 0.00444 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-9Client Sample ID: MW-2-20
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropyl ether ND 0.0179 0.00268 mg/Kg ☼07/26/22 10:32 07/26/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Isopropylbenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Methyl tert-butyl ether ND *+
0.0179 0.0143 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Methylene Chloride ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼m-Xylene & p-Xylene ND
0.00894 0.00554 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Naphthalene ND
0.00894 0.00340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼n-Butylbenzene ND
0.00894 0.00769 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼n-Heptane ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼N-Propylbenzene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼o-Xylene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼sec-Butylbenzene ND
0.00894 0.00340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Styrene ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼tert-Butylbenzene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Tetrachloroethene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Toluene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,2-Dichloroethene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,3-Dichloropropene ND
0.0179 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,4-Dichloro-2-butene ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Trichloroethene ND
0.00894 0.00554 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Trichlorofluoromethane ND
0.0179 0.00984 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Vinyl acetate ND
0.00894 0.00501 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Vinyl chloride ND
0.0179 0.00644 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)104 65-130 07/26/22 10:32 07/26/22 17:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 07/26/22 10:32 07/26/22 17:24 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/26/22 17:24 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 17:24 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Acetone ND 3.28 0.721 mg/Kg ☼07/26/22 10:32 08/01/22 17:55 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)109 65-130 07/26/22 10:32 08/01/22 17:55 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 07/26/22 10:32 08/01/22 17:55 4065-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 08/01/22 17:55 4065-130
Toluene-d8 (Surr)93 07/26/22 10:32 08/01/22 17:55 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
6.96 J 13.6 3.40 mg/Kg ☼07/26/22 10:32 07/28/22 18:30 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 84 70-131 07/26/22 10:32 07/28/22 18:30 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-10Client Sample ID: MW-2-25
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00772 0.00201 mg/Kg ☼07/26/22 10:32 07/27/22 13:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,1-Trichloroethane ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2,2-Tetrachloroethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00772 0.00232 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2-Trichloroethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloroethane ND
0.00772 0.00556 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloroethene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloropropene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,3-Trichlorobenzene ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,3-Trichloropropane ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,4-Trichlorobenzene ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,4-Trimethylbenzene 0.00989
0.0154 0.00247 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dibromo-3-Chloropropane ND
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichlorobenzene ND
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichloroethane ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichloropropane ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3,5-Trimethylbenzene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3-Dichlorobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3-Dichloropropane ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,4-Dichlorobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2,2-Dichloropropane ND
0.0386 0.0142 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Butanone (MEK)0.396
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Chlorotoluene ND
0.0386 0.0294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Hexanone 0.0325 J
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Chlorotoluene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Isopropyltoluene ND
0.0386 0.0278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Methyl-2-pentanone (MIBK)ND
0.0772 0.0170 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Acetone 0.494
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Benzene 0.00775
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromoform ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromomethane ND *+
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Carbon disulfide ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Carbon tetrachloride ND
0.00772 0.00216 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorobenzene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorobromomethane ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorodibromomethane ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloroethane ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloroform ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloromethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼cis-1,2-Dichloroethene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼cis-1,3-Dichloropropene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Dibromomethane ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Dichlorobromomethane ND
0.0154 0.0154 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethyl acetate ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethylbenzene 0.00843
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethylene Dibromide ND
0.00772 0.00633 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Hexachlorobutadiene ND
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Hexane 0.00296 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-10Client Sample ID: MW-2-25
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00772 0.00263 mg/Kg ☼07/26/22 10:32 07/27/22 13:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0154 0.00232 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Isopropyl ether ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Isopropylbenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Methyl tert-butyl ether ND *+
0.0154 0.0124 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Methylene Chloride ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼m-Xylene & p-Xylene 0.0355
0.00772 0.00479 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Naphthalene ND
0.00772 0.00294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼n-Butylbenzene ND
0.00772 0.00664 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼n-Heptane ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼N-Propylbenzene 0.00398 J
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼o-Xylene 0.0178
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼sec-Butylbenzene ND
0.00772 0.00294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Styrene ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼tert-Butylbenzene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Tetrachloroethene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Toluene 0.0273
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,2-Dichloroethene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,3-Dichloropropene ND
0.0154 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,4-Dichloro-2-butene ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Trichloroethene ND
0.00772 0.00479 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Trichlorofluoromethane ND
0.0154 0.00850 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Vinyl acetate ND
0.00772 0.00433 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Vinyl chloride ND
0.0154 0.00556 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Xylenes, Total 0.0533
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 07/27/22 13:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 13:16 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 13:16 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 13:16 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.9 3.97 mg/Kg ☼07/26/22 10:32 07/28/22 18:51 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 18:51 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-11Client Sample ID: MW-2-30
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00710 0.00185 mg/Kg ☼07/26/22 10:32 07/26/22 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,1-Trichloroethane ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2,2-Tetrachloroethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00710 0.00213 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2-Trichloroethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloroethane ND
0.00710 0.00511 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloroethene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloropropene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,3-Trichlorobenzene ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,3-Trichloropropane ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,4-Trichlorobenzene ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,4-Trimethylbenzene 0.0536
0.0142 0.00227 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dibromo-3-Chloropropane ND
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichlorobenzene ND
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichloroethane ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichloropropane ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3,5-Trimethylbenzene 0.0245
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3-Dichlorobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3-Dichloropropane ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,4-Dichlorobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2,2-Dichloropropane ND
0.0355 0.0131 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Butanone (MEK)0.0978
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Chlorotoluene ND
0.0355 0.0270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Hexanone 0.0274 J
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Chlorotoluene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Isopropyltoluene 0.0111
0.0355 0.0256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Methyl-2-pentanone (MIBK)ND
0.0710 0.0156 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Acetone 0.306
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Benzene 0.0102
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromoform ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromomethane ND *+
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Carbon disulfide ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Carbon tetrachloride ND
0.00710 0.00199 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorobenzene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorobromomethane ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorodibromomethane ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloroethane ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloroform ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloromethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼cis-1,2-Dichloroethene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼cis-1,3-Dichloropropene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Dibromomethane ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Dichlorobromomethane ND
0.0142 0.0142 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethyl acetate ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethylbenzene 0.0227
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethylene Dibromide ND
0.00710 0.00582 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Hexachlorobutadiene ND
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Hexane 0.00793
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-11Client Sample ID: MW-2-30
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00710 0.00241 mg/Kg ☼07/26/22 10:32 07/26/22 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0142 0.00213 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Isopropyl ether ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Isopropylbenzene 0.00610 J
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Methyl tert-butyl ether ND *+
0.0142 0.0114 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Methylene Chloride ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼m-Xylene & p-Xylene 0.0830
0.00710 0.00440 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Naphthalene 0.0243
0.00710 0.00270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼n-Butylbenzene 0.0160
0.00710 0.00611 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼n-Heptane 0.0175
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼N-Propylbenzene 0.0152
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼o-Xylene 0.0603
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼sec-Butylbenzene 0.00406 J
0.00710 0.00270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Styrene ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼tert-Butylbenzene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Tetrachloroethene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Toluene 0.0528
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,2-Dichloroethene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,3-Dichloropropene ND
0.0142 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,4-Dichloro-2-butene ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Trichloroethene ND
0.00710 0.00440 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Trichlorofluoromethane ND
0.0142 0.00781 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Vinyl acetate ND
0.00710 0.00398 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Vinyl chloride ND
0.0142 0.00511 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Xylenes, Total 0.143
1,2-Dichloroethane-d4 (Surr)103 65-130 07/26/22 10:32 07/26/22 18:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 07/26/22 10:32 07/26/22 18:12 165-130
Dibromofluoromethane (Surr)103 07/26/22 10:32 07/26/22 18:12 165-130
Toluene-d8 (Surr)103 07/26/22 10:32 07/26/22 18:12 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
6.82 J 14.1 3.51 mg/Kg ☼07/26/22 10:32 07/28/22 19:13 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:13 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-12Client Sample ID: P-1-10
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00812 0.00211 mg/Kg ☼07/26/22 10:32 07/27/22 13:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,1-Trichloroethane ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2,2-Tetrachloroethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00812 0.00244 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2-Trichloroethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloroethane ND
0.00812 0.00585 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloroethene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloropropene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,3-Trichlorobenzene ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,3-Trichloropropane ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,4-Trichlorobenzene ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,4-Trimethylbenzene ND
0.0162 0.00260 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dibromo-3-Chloropropane ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichlorobenzene ND
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichloroethane ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichloropropane ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3,5-Trimethylbenzene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3-Dichlorobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3-Dichloropropane ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,4-Dichlorobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2,2-Dichloropropane ND
0.0406 0.0149 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Butanone (MEK)0.0336 J
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Chlorotoluene ND
0.0406 0.0309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Hexanone ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Chlorotoluene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Isopropyltoluene ND
0.0406 0.0292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Methyl-2-pentanone (MIBK)ND
0.0812 0.0179 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Acetone 0.299
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Benzene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromoform ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromomethane ND *+
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Carbon disulfide ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Carbon tetrachloride ND
0.00812 0.00227 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorobenzene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorobromomethane ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorodibromomethane ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloroethane ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloroform ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloromethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼cis-1,2-Dichloroethene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼cis-1,3-Dichloropropene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Dibromomethane ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Dichlorobromomethane ND
0.0162 0.0162 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethyl acetate ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethylbenzene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethylene Dibromide ND
0.00812 0.00666 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Hexachlorobutadiene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-12Client Sample ID: P-1-10
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00812 0.00276 mg/Kg ☼07/26/22 10:32 07/27/22 13:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0162 0.00244 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Isopropyl ether ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Isopropylbenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Methyl tert-butyl ether ND *+
0.0162 0.0130 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Methylene Chloride ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼m-Xylene & p-Xylene 0.00686 J
0.00812 0.00503 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Naphthalene ND
0.00812 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼n-Butylbenzene ND
0.00812 0.00698 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼n-Heptane ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼N-Propylbenzene ND
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼o-Xylene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼sec-Butylbenzene ND
0.00812 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Styrene ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼tert-Butylbenzene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Tetrachloroethene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Toluene 0.00449 J
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,2-Dichloroethene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,3-Dichloropropene ND
0.0162 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,4-Dichloro-2-butene ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Trichloroethene ND
0.00812 0.00503 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Trichlorofluoromethane ND
0.0162 0.00893 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Vinyl acetate ND
0.00812 0.00455 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Vinyl chloride ND
0.0162 0.00585 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Xylenes, Total 0.00686 J
1,2-Dichloroethane-d4 (Surr)107 65-130 07/26/22 10:32 07/27/22 13:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 13:40 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 13:40 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 13:40 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.4 3.84 mg/Kg ☼07/26/22 10:32 07/28/22 19:35 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:35 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-13Client Sample ID: P-1-20
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00816 0.00212 mg/Kg ☼07/26/22 10:32 07/26/22 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,1-Trichloroethane ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2,2-Tetrachloroethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00816 0.00245 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2-Trichloroethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloroethane ND
0.00816 0.00587 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloroethene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloropropene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,3-Trichlorobenzene ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,3-Trichloropropane ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,4-Trichlorobenzene ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,4-Trimethylbenzene 0.00662 J
0.0163 0.00261 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dibromo-3-Chloropropane ND
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichlorobenzene ND
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichloroethane ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichloropropane ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3,5-Trimethylbenzene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3-Dichlorobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3-Dichloropropane ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,4-Dichlorobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2,2-Dichloropropane ND
0.0408 0.0150 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Butanone (MEK)0.109
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Chlorotoluene ND
0.0408 0.0310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Hexanone ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Chlorotoluene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Isopropyltoluene ND
0.0408 0.0294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Methyl-2-pentanone (MIBK)ND
0.0816 0.0179 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Acetone 0.589
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Benzene 0.0122
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromoform ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromomethane ND *+
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Carbon disulfide ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Carbon tetrachloride ND
0.00816 0.00228 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorobenzene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorobromomethane ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorodibromomethane ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloroethane ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloroform ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloromethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼cis-1,2-Dichloroethene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼cis-1,3-Dichloropropene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Dibromomethane ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Dichlorobromomethane ND
0.0163 0.0163 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethyl acetate ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethylbenzene 0.00594 J
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethylene Dibromide ND
0.00816 0.00669 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Hexachlorobutadiene ND
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-13Client Sample ID: P-1-20
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00826 0.00816 0.00277 mg/Kg ☼07/26/22 10:32 07/26/22 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0163 0.00245 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Isopropyl ether ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Isopropylbenzene ND
0.00806 0.00355 mg/Kg 07/26/22 10:32 08/01/22 16:26 1☼Methyl tert-butyl ether 0.0227
0.0163 0.0130 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Methylene Chloride ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼m-Xylene & p-Xylene 0.0226
0.00816 0.00506 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Naphthalene ND
0.00816 0.00310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼n-Butylbenzene ND
0.00816 0.00701 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼n-Heptane ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼N-Propylbenzene ND
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼o-Xylene 0.0183
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼sec-Butylbenzene ND
0.00816 0.00310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Styrene ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼tert-Butylbenzene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Tetrachloroethene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Toluene 0.0334
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,2-Dichloroethene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,3-Dichloropropene ND
0.0163 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,4-Dichloro-2-butene ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Trichloroethene ND
0.00816 0.00506 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Trichlorofluoromethane ND
0.0163 0.00897 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Vinyl acetate ND
0.00816 0.00457 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Vinyl chloride ND
0.0163 0.00587 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Xylenes, Total 0.0409
1,2-Dichloroethane-d4 (Surr)102 65-130 07/26/22 10:32 07/26/22 19:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)112 07/26/22 10:32 08/01/22 16:26 165-130
4-Bromofluorobenzene (Surr)106 07/26/22 10:32 07/26/22 19:00 165-130
4-Bromofluorobenzene (Surr)98 07/26/22 10:32 08/01/22 16:26 165-130
Dibromofluoromethane (Surr)99 07/26/22 10:32 07/26/22 19:00 165-130
Dibromofluoromethane (Surr)103 07/26/22 10:32 08/01/22 16:26 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 19:00 165-130
Toluene-d8 (Surr)100 07/26/22 10:32 08/01/22 16:26 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 16.5 4.13 mg/Kg ☼07/26/22 10:32 07/28/22 19:57 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:57 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-14Client Sample ID: P-1-25
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00804 0.00209 mg/Kg ☼07/26/22 10:32 07/26/22 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,1-Trichloroethane ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2,2-Tetrachloroethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00804 0.00241 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2-Trichloroethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloroethane ND
0.00804 0.00579 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloroethene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloropropene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,3-Trichlorobenzene ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,3-Trichloropropane ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,4-Trichlorobenzene ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,4-Trimethylbenzene 0.0267
0.0161 0.00257 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dibromo-3-Chloropropane ND
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichlorobenzene ND
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichloroethane ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichloropropane ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3,5-Trimethylbenzene 0.00848
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3-Dichlorobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3-Dichloropropane ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,4-Dichlorobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2,2-Dichloropropane ND
0.0402 0.0148 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Butanone (MEK)0.189
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Chlorotoluene ND
0.0402 0.0306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Hexanone ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Chlorotoluene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Isopropyltoluene ND
0.0402 0.0289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Methyl-2-pentanone (MIBK)ND
0.0804 0.0177 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Acetone 0.757
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Benzene 0.0536
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromoform ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromomethane ND *+
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Carbon disulfide ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Carbon tetrachloride ND
0.00804 0.00225 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorobenzene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorobromomethane ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorodibromomethane ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloroethane ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloroform ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloromethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼cis-1,2-Dichloroethene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼cis-1,3-Dichloropropene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Dibromomethane ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Dichlorobromomethane ND
0.0161 0.0161 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethyl acetate ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethylbenzene 0.0381
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethylene Dibromide ND
0.00804 0.00659 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Hexachlorobutadiene ND
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Hexane 0.00366 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-14Client Sample ID: P-1-25
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00804 0.00273 mg/Kg ☼07/26/22 10:32 07/26/22 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0161 0.00241 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Isopropyl ether 0.00342 J
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Isopropylbenzene 0.00402 J
0.00828 0.00364 mg/Kg 07/26/22 10:32 08/01/22 16:47 1☼Methyl tert-butyl ether 0.0517
0.0161 0.0129 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Methylene Chloride ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼m-Xylene & p-Xylene 0.131
0.00804 0.00499 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Naphthalene ND
0.00804 0.00306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼n-Butylbenzene ND
0.00804 0.00692 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼n-Heptane 0.00707 J
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼N-Propylbenzene 0.00583 J
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼o-Xylene 0.0883
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼sec-Butylbenzene ND
0.00804 0.00306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Styrene ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼tert-Butylbenzene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Tetrachloroethene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Toluene 0.244
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,2-Dichloroethene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,3-Dichloropropene ND
0.0161 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,4-Dichloro-2-butene ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Trichloroethene ND
0.00804 0.00499 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Trichlorofluoromethane ND
0.0161 0.00885 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Vinyl acetate ND
0.00804 0.00450 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Vinyl chloride ND
0.0161 0.00579 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Xylenes, Total 0.219
1,2-Dichloroethane-d4 (Surr)103 65-130 07/26/22 10:32 07/26/22 19:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)113 07/26/22 10:32 08/01/22 16:47 165-130
4-Bromofluorobenzene (Surr)105 07/26/22 10:32 07/26/22 19:25 165-130
4-Bromofluorobenzene (Surr)95 07/26/22 10:32 08/01/22 16:47 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 19:25 165-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 08/01/22 16:47 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/26/22 19:25 165-130
Toluene-d8 (Surr)98 07/26/22 10:32 08/01/22 16:47 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
5.48 J 16.3 4.07 mg/Kg ☼07/26/22 10:32 07/28/22 20:18 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 77 70-131 07/26/22 10:32 07/28/22 20:18 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-15Client Sample ID: P-1-30
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.347 0.0902 mg/Kg ☼07/26/22 10:32 07/26/22 21:02 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,1-Trichloroethane ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2,2-Tetrachloroethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.347 0.104 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2-Trichloroethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloroethane ND
0.347 0.250 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloroethene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloropropene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,3-Trichlorobenzene ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,3-Trichloropropane ND
0.347 0.174 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,4-Trichlorobenzene ND
0.694 0.111 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dibromo-3-Chloropropane ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichlorobenzene ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichloroethane ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichloropropane ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3,5-Trimethylbenzene 8.02
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3-Dichlorobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3-Dichloropropane ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,4-Dichlorobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2,2-Dichloropropane ND
1.74 0.639 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Butanone (MEK)ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Chlorotoluene ND
1.74 1.32 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Hexanone ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Chlorotoluene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Isopropyltoluene 1.39
1.74 1.25 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Methyl-2-pentanone (MIBK)ND
3.47 0.764 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Acetone ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Benzene 3.33
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromoform ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromomethane ND *+
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Carbon disulfide ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Carbon tetrachloride ND
0.347 0.0972 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorobenzene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorobromomethane ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorodibromomethane ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloroethane ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloroform ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloromethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼cis-1,2-Dichloroethene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼cis-1,3-Dichloropropene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Dibromomethane ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Dichlorobromomethane ND
0.694 0.694 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Ethyl acetate ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Ethylene Dibromide ND
0.347 0.285 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Hexachlorobutadiene ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Hexane 2.67
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Iodomethane ND
0.694 0.104 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Isopropyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-15Client Sample ID: P-1-30
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropylbenzene 1.77 0.347 0.153 mg/Kg ☼07/26/22 10:32 07/26/22 21:02 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Methyl tert-butyl ether ND
0.694 0.555 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Methylene Chloride ND
0.347 0.215 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Naphthalene 3.55
0.347 0.132 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼n-Butylbenzene 1.87
0.347 0.298 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼n-Heptane 4.48
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼N-Propylbenzene 5.54
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼sec-Butylbenzene 0.497
0.347 0.132 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Styrene ND
0.347 0.174 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼tert-Butylbenzene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Tetrachloroethene ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,2-Dichloroethene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,3-Dichloropropene ND
0.694 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,4-Dichloro-2-butene ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Trichloroethene ND
0.347 0.215 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Trichlorofluoromethane ND
0.694 0.382 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Vinyl acetate ND
0.347 0.194 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)92 65-130 07/26/22 10:32 07/26/22 21:02 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 07/26/22 10:32 07/26/22 21:02 4065-130
Dibromofluoromethane (Surr)95 07/26/22 10:32 07/26/22 21:02 4065-130
Toluene-d8 (Surr)99 07/26/22 10:32 07/26/22 21:02 4065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 32.4 4.34 2.17 mg/Kg ☼07/26/22 10:32 07/27/22 17:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.34 1.82 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Ethylbenzene 19.3
4.34 1.91 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼m-Xylene & p-Xylene 75.2
4.34 2.00 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼o-Xylene 31.1
4.34 2.26 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Toluene 64.9
8.68 3.12 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Xylenes, Total 106
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/27/22 17:16 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 17:16 50065-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/27/22 17:16 50065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 17:16 50065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
828 169 42.3 mg/Kg ☼07/26/22 10:32 07/29/22 21:12 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/29/22 21:12 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/03/22 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.190 ug/L 08/03/22 18:06 11,1,1-Trichloroethane ND
0.500 0.100 ug/L 08/03/22 18:06 11,1,2,2-Tetrachloroethane ND
0.500 0.140 ug/L 08/03/22 18:06 11,1,2-Trichloroethane ND
0.500 0.180 ug/L 08/03/22 18:06 11,1-Dichloroethane ND
0.500 0.180 ug/L 08/03/22 18:06 11,1-Dichloroethene ND
0.500 0.200 ug/L 08/03/22 18:06 11,1-Dichloropropene ND
1.00 0.770 ug/L 08/03/22 18:06 11,2,3-Trichlorobenzene ND
0.500 0.120 ug/L 08/03/22 18:06 11,2,3-Trichloropropane ND
0.500 0.350 ug/L 08/03/22 18:06 11,2,4-Trichlorobenzene ND
0.500 0.140 ug/L 08/03/22 18:06 11,2,4-Trimethylbenzene 90.4
0.500 0.120 ug/L 08/03/22 18:06 11,2-Dichlorobenzene ND
0.500 0.160 ug/L 08/03/22 18:06 11,2-Dichloroethane ND
0.500 0.230 ug/L 08/03/22 18:06 11,2-Dichloroethene, Total ND
0.500 0.160 ug/L 08/03/22 18:06 11,2-Dichloropropane ND
0.500 0.160 ug/L 08/03/22 18:06 11,3,5-Trimethylbenzene 29.2
0.500 0.160 ug/L 08/03/22 18:06 11,3-Dichlorobenzene ND
0.500 0.140 ug/L 08/03/22 18:06 11,3-Dichloropropane ND
0.500 0.220 ug/L 08/03/22 18:06 11,3-Dichloropropene, Total ND
0.500 0.120 ug/L 08/03/22 18:06 11,4-Dichlorobenzene ND
0.500 0.180 ug/L 08/03/22 18:06 12,2-Dichloropropane ND
10.0 5.20 ug/L 08/03/22 18:06 12-Butanone (MEK)ND
0.500 0.160 ug/L 08/03/22 18:06 12-Chlorotoluene ND
10.0 5.00 ug/L 08/03/22 18:06 12-Hexanone ND
20.0 9.10 ug/L 08/03/22 18:06 13,3-Dimethyl-1-butanol ND
0.500 0.160 ug/L 08/03/22 18:06 14-Chlorotoluene ND
0.500 0.180 ug/L 08/03/22 18:06 14-Isopropyltoluene 2.41
10.0 5.20 ug/L 08/03/22 18:06 14-Methyl-2-pentanone (MIBK)ND
20.0 5.60 ug/L 08/03/22 18:06 1AcetoneND
0.500 0.180 ug/L 08/03/22 18:06 1Benzene14.4
0.500 0.140 ug/L 08/03/22 18:06 1BromobenzeneND
0.500 0.180 ug/L 08/03/22 18:06 1BromoformND
5.00 2.30 ug/L 08/03/22 18:06 1BromomethaneND
0.500 0.220 ug/L 08/03/22 18:06 1Carbon tetrachloride ND
0.500 0.160 ug/L 08/03/22 18:06 1ChlorobenzeneND
0.500 0.130 ug/L 08/03/22 18:06 1ChlorobromomethaneND
1.00 0.460 ug/L 08/03/22 18:06 1ChlorodibromomethaneND
10.0 4.10 ug/L 08/03/22 18:06 1ChloroethaneND
0.500 0.380 ug/L 08/03/22 18:06 1Chloroform0.599
0.500 0.100 ug/L 08/03/22 18:06 1ChloromethaneND
0.500 0.0640 ug/L 08/03/22 18:06 1cis-1,2-Dichloroethene ND
0.500 0.110 ug/L 08/03/22 18:06 1cis-1,3-Dichloropropene ND
0.500 0.170 ug/L 08/03/22 18:06 1DibromomethaneND
1.00 0.410 ug/L 08/03/22 18:06 1DichlorobromomethaneND
0.500 0.0910 ug/L 08/03/22 18:06 1DichlorodifluoromethaneND
0.500 0.140 ug/L 08/03/22 18:06 1DichlorofluoromethaneND
200 140 ug/L 08/03/22 18:06 1EthanolND
0.500 0.0920 ug/L 08/03/22 18:06 1Ethyl ether ND
0.500 0.170 ug/L 08/03/22 18:06 1Ethylbenzene56.5
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Ethylene Dibromide ND 0.500 0.170 ug/L 08/03/22 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.0580 ug/L 08/03/22 18:06 1Isopropyl ether ND
0.500 0.180 ug/L 08/03/22 18:06 1Isopropylbenzene5.09
0.500 0.110 ug/L 08/03/22 18:06 1Methyl tert-butyl ether ND
0.500 0.150 ug/L 08/03/22 18:06 1Methylene Chloride ND
0.500 0.180 ug/L 08/03/22 18:06 1m-Xylene & p-Xylene 209 E
2.00 1.20 ug/L 08/03/22 18:06 1Naphthalene5.97
1.00 0.160 ug/L 08/03/22 18:06 1n-Butylbenzene 11.0
0.500 0.180 ug/L 08/03/22 18:06 1N-Propylbenzene 17.8
0.500 0.150 ug/L 08/03/22 18:06 1o-Xylene 82.2
1.00 0.170 ug/L 08/03/22 18:06 1sec-Butylbenzene ND
0.500 0.170 ug/L 08/03/22 18:06 1StyreneND
5.00 1.90 ug/L 08/03/22 18:06 1t-Amyl alcohol ND
0.500 0.0790 ug/L 08/03/22 18:06 1Tert-amyl methyl ether ND
0.500 0.0580 ug/L 08/03/22 18:06 1Tert-butyl ethyl ether ND
5.00 1.76 ug/L 08/03/22 18:06 1tert-Butyl Formate ND
0.500 0.180 ug/L 08/03/22 18:06 1tert-Butylbenzene ND
0.500 0.220 ug/L 08/03/22 18:06 1Tetrachloroethene3.92
0.500 0.200 ug/L 08/03/22 18:06 1Toluene20.0
0.500 0.170 ug/L 08/03/22 18:06 1trans-1,2-Dichloroethene ND
0.500 0.120 ug/L 08/03/22 18:06 1trans-1,3-Dichloropropene ND
0.500 0.200 ug/L 08/03/22 18:06 1TrichloroetheneND
0.500 0.140 ug/L 08/03/22 18:06 1TrichlorofluoromethaneND
1.00 0.640 ug/L 08/03/22 18:06 1Vinyl acetate ND
0.500 0.120 ug/L 08/03/22 18:06 1Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)95 70-130 08/03/22 18:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 08/03/22 18:06 170-130
Dibromofluoromethane (Surr)98 08/03/22 18:06 170-130
Toluene-d8 (Surr)102 08/03/22 18:06 170-130
Method: SM6200-B - Volatile Organic Compounds - DL
RL MDL
m-Xylene & p-Xylene 169 H 2.50 0.900 ug/L 08/04/22 13:42 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)93 70-130 08/04/22 13:42 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 08/04/22 13:42 570-130
Dibromofluoromethane (Surr)99 08/04/22 13:42 570-130
Toluene-d8 (Surr)105 08/04/22 13:42 570-130
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 348 130 130 ug/L 08/02/22 10:10 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
35.0 35.0 ug/L 08/02/22 10:10 5C9-C10 Aromatics 533 F1
55.0 55.0 ug/L 08/02/22 10:10 5C9-C12 Aliphatics 404
a,a,a-Trifluorotoluene (fid)101 70-130 08/02/22 10:10 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)101 08/02/22 10:10 570-130
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
1,2-Dibromoethane (EDB)ND 0.0181 0.00503 ug/L 07/25/22 11:15 07/25/22 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane 89 p 70-130 07/25/22 11:15 07/25/22 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP) - Total Recoverable
RL MDL
Lead, Total 11.6 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1,2-Tetrachloroethane ND H 250 75.0 ug/L 08/04/22 13:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
250 95.0 ug/L 08/04/22 13:16 5001,1,1-Trichloroethane ND H
250 50.0 ug/L 08/04/22 13:16 5001,1,2,2-Tetrachloroethane ND H
250 70.0 ug/L 08/04/22 13:16 5001,1,2-Trichloroethane ND H
250 90.0 ug/L 08/04/22 13:16 5001,1-Dichloroethane ND H
250 90.0 ug/L 08/04/22 13:16 5001,1-Dichloroethene ND H
250 100 ug/L 08/04/22 13:16 5001,1-Dichloropropene ND H
500 385 ug/L 08/04/22 13:16 5001,2,3-Trichlorobenzene ND H
250 60.0 ug/L 08/04/22 13:16 5001,2,3-Trichloropropane ND H
250 175 ug/L 08/04/22 13:16 5001,2,4-Trichlorobenzene ND H
250 70.0 ug/L 08/04/22 13:16 5001,2,4-Trimethylbenzene 699 H
250 60.0 ug/L 08/04/22 13:16 5001,2-Dichlorobenzene ND H
250 80.0 ug/L 08/04/22 13:16 5001,2-Dichloroethane ND H
250 115 ug/L 08/04/22 13:16 5001,2-Dichloroethene, Total ND H
250 80.0 ug/L 08/04/22 13:16 5001,2-Dichloropropane ND H
250 80.0 ug/L 08/04/22 13:16 5001,3,5-Trimethylbenzene ND H
250 80.0 ug/L 08/04/22 13:16 5001,3-Dichlorobenzene ND H
250 70.0 ug/L 08/04/22 13:16 5001,3-Dichloropropane ND H
250 110 ug/L 08/04/22 13:16 5001,3-Dichloropropene, Total ND H
250 60.0 ug/L 08/04/22 13:16 5001,4-Dichlorobenzene ND H
250 90.0 ug/L 08/04/22 13:16 5002,2-Dichloropropane ND H
5000 2600 ug/L 08/04/22 13:16 5002-Butanone (MEK)ND H
250 80.0 ug/L 08/04/22 13:16 5002-Chlorotoluene ND H
5000 2500 ug/L 08/04/22 13:16 5002-Hexanone ND H
10000 4550 ug/L 08/04/22 13:16 5003,3-Dimethyl-1-butanol ND H
250 80.0 ug/L 08/04/22 13:16 5004-Chlorotoluene ND H
250 90.0 ug/L 08/04/22 13:16 5004-Isopropyltoluene ND H
5000 2600 ug/L 08/04/22 13:16 5004-Methyl-2-pentanone (MIBK)ND H
10000 2800 ug/L 08/04/22 13:16 500AcetoneNDH
250 90.0 ug/L 08/04/22 13:16 500Benzene995H
250 70.0 ug/L 08/04/22 13:16 500BromobenzeneNDH
250 90.0 ug/L 08/04/22 13:16 500BromoformNDH
2500 1150 ug/L 08/04/22 13:16 500BromomethaneNDH
250 110 ug/L 08/04/22 13:16 500Carbon tetrachloride ND H
250 80.0 ug/L 08/04/22 13:16 500ChlorobenzeneNDH
250 65.0 ug/L 08/04/22 13:16 500ChlorobromomethaneNDH
500 230 ug/L 08/04/22 13:16 500ChlorodibromomethaneNDH
5000 2050 ug/L 08/04/22 13:16 500ChloroethaneNDH
250 190 ug/L 08/04/22 13:16 500ChloroformNDH
250 50.0 ug/L 08/04/22 13:16 500ChloromethaneNDH
250 32.0 ug/L 08/04/22 13:16 500cis-1,2-Dichloroethene ND H
250 55.0 ug/L 08/04/22 13:16 500cis-1,3-Dichloropropene ND H
250 85.0 ug/L 08/04/22 13:16 500DibromomethaneNDH
500 205 ug/L 08/04/22 13:16 500DichlorobromomethaneNDH
250 45.5 ug/L 08/04/22 13:16 500DichlorodifluoromethaneNDH
250 70.0 ug/L 08/04/22 13:16 500DichlorofluoromethaneNDH
100000 70000 ug/L 08/04/22 13:16 500EthanolNDH
250 46.0 ug/L 08/04/22 13:16 500Ethyl ether ND H
250 85.0 ug/L 08/04/22 13:16 500Ethylbenzene1120H
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Ethylene Dibromide ND H 250 85.0 ug/L 08/04/22 13:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
250 29.0 ug/L 08/04/22 13:16 500Isopropyl ether ND H
250 90.0 ug/L 08/04/22 13:16 500IsopropylbenzeneNDH
250 55.0 ug/L 08/04/22 13:16 500Methyl tert-butyl ether ND H
250 75.0 ug/L 08/04/22 13:16 500Methylene Chloride ND H
250 90.0 ug/L 08/04/22 13:16 500m-Xylene & p-Xylene 4640 H
1000 600 ug/L 08/04/22 13:16 500NaphthaleneNDH
500 80.0 ug/L 08/04/22 13:16 500n-Butylbenzene ND H
250 90.0 ug/L 08/04/22 13:16 500N-Propylbenzene ND H
250 75.0 ug/L 08/04/22 13:16 500o-Xylene 2410 H
500 85.0 ug/L 08/04/22 13:16 500sec-Butylbenzene ND H
250 85.0 ug/L 08/04/22 13:16 500StyreneNDH
2500 950 ug/L 08/04/22 13:16 500t-Amyl alcohol ND H
250 39.5 ug/L 08/04/22 13:16 500Tert-amyl methyl ether ND H
250 29.0 ug/L 08/04/22 13:16 500Tert-butyl ethyl ether ND H
2500 880 ug/L 08/04/22 13:16 500tert-Butyl Formate ND H
250 90.0 ug/L 08/04/22 13:16 500tert-Butylbenzene ND H
250 110 ug/L 08/04/22 13:16 500TetrachloroetheneNDH
250 100 ug/L 08/04/22 13:16 500Toluene12100H
250 85.0 ug/L 08/04/22 13:16 500trans-1,2-Dichloroethene ND H
250 60.0 ug/L 08/04/22 13:16 500trans-1,3-Dichloropropene ND H
250 100 ug/L 08/04/22 13:16 500TrichloroetheneNDH
250 70.0 ug/L 08/04/22 13:16 500TrichlorofluoromethaneNDH
500 320 ug/L 08/04/22 13:16 500Vinyl acetate ND H
250 60.0 ug/L 08/04/22 13:16 500Vinyl chloride ND H
1,2-Dichloroethane-d4 (Surr)93 70-130 08/04/22 13:16 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 08/04/22 13:16 50070-130
Dibromofluoromethane (Surr)98 08/04/22 13:16 50070-130
Toluene-d8 (Surr)105 08/04/22 13:16 50070-130
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 33700 2600 2600 ug/L 08/02/22 15:32 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
700 700 ug/L 08/02/22 15:32 100C9-C10 Aromatics 4670
1100 1100 ug/L 08/02/22 15:32 100C9-C12 Aliphatics 16700
a,a,a-Trifluorotoluene (fid)95 70-130 08/02/22 15:32 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 08/02/22 15:32 10070-130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
1,2-Dibromoethane (EDB)ND 0.0184 0.00510 ug/L 07/25/22 11:15 07/25/22 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane 160 p S1+70-130 07/25/22 11:15 07/25/22 19:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: 6010D - Metals (ICP) - Total Recoverable
RL MDL
Lead, Total ND 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-732600/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/26/22 13:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/26/22 13:22 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/26/22 13:22 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/26/22 13:22 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/26/22 13:22 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/26/22 13:22 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/26/22 13:22 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/26/22 13:22 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/26/22 13:22 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/26/22 13:22 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/26/22 13:22 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/26/22 13:22 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/26/22 13:22 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/26/22 13:22 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/26/22 13:22 12-Hexanone
ND 0.002100.00500 mg/Kg 07/26/22 13:22 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/26/22 13:22 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/26/22 13:22 1Acetone
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Benzene
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Bromoform
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Bromomethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/26/22 13:22 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Chloroethane
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Chloroform
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Chloromethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/26/22 13:22 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/26/22 13:22 1Hexachlorobutadiene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732600/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
RL MDL
Hexane ND 0.00500 0.00170 mg/Kg 07/26/22 13:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Iodomethane
ND 0.001500.0100 mg/Kg 07/26/22 13:22 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/26/22 13:22 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/26/22 13:22 1Naphthalene
ND 0.001900.00500 mg/Kg 07/26/22 13:22 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/26/22 13:22 1n-Heptane
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 1o-Xylene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/26/22 13:22 1Styrene
ND 0.002500.00500 mg/Kg 07/26/22 13:22 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1Toluene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/26/22 13:22 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/26/22 13:22 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/26/22 13:22 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/26/22 13:22 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/26/22 13:22 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/26/22 13:22 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)100 65-130 07/26/22 13:22 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
110 07/26/22 13:22 14-Bromofluorobenzene (Surr)65-130
101 07/26/22 13:22 1Dibromofluoromethane (Surr)65-130
107 07/26/22 13:22 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,1,1,2-Tetrachloroethane 0.0500 0.04761 mg/Kg 95 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04518 mg/Kg 90 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04978 mg/Kg 100 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04578 mg/Kg 92 70 -130
1,1,2-Trichloroethane 0.0500 0.05066 mg/Kg 101 56 -146
1,1-Dichloroethane 0.0500 0.05049 mg/Kg 101 70 -130
1,1-Dichloroethene 0.0500 0.04679 mg/Kg 94 69 -130
1,1-Dichloropropene 0.0500 0.04601 mg/Kg 92 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05303 mg/Kg 106 70 -130
1,2,3-Trichloropropane 0.0500 0.04879 mg/Kg 98 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05239 mg/Kg 105 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,2,4-Trimethylbenzene 0.0500 0.04663 mg/Kg 93 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.05142 mg/Kg 103 42 -145
1,2-Dichlorobenzene 0.0500 0.05122 mg/Kg 102 70 -130
1,2-Dichloroethane 0.0500 0.05022 mg/Kg 100 68 -139
1,2-Dichloropropane 0.0500 0.05098 mg/Kg 102 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04560 mg/Kg 91 70 -130
1,3-Dichlorobenzene 0.0500 0.05126 mg/Kg 103 70 -130
1,3-Dichloropropane 0.0500 0.04915 mg/Kg 98 54 -150
1,4-Dichlorobenzene 0.0500 0.05119 mg/Kg 102 70 -130
2,2-Dichloropropane 0.0500 0.04697 mg/Kg 94 70 -130
2-Butanone (MEK)0.250 0.2582 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.04914 mg/Kg 98 70 -130
2-Hexanone 0.250 0.2647 mg/Kg 106 30 -150
4-Chlorotoluene 0.0500 0.04498 mg/Kg 90 70 -130
4-Isopropyltoluene 0.0500 0.04858 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2613 mg/Kg 105 34 -150
Acetone 0.250 0.2717 mg/Kg 109 10 -150
Benzene 0.0500 0.04846 mg/Kg 97 70 -130
Bromobenzene 0.0500 0.04763 mg/Kg 95 70 -130
Bromoform 0.0500 0.04638 mg/Kg 93 68 -130
Bromomethane 0.0500 0.06967 *+mg/Kg 139 70 -130
Carbon disulfide 0.0500 0.04775 mg/Kg 95 70 -130
Carbon tetrachloride 0.0500 0.04337 mg/Kg 87 70 -130
Chlorobenzene 0.0500 0.04938 mg/Kg 99 70 -130
Chlorobromomethane 0.0500 0.04663 mg/Kg 93 66 -130
Chlorodibromomethane 0.0500 0.04814 mg/Kg 96 64 -133
Chloroethane 0.0500 0.05507 mg/Kg 110 70 -130
Chloroform 0.0500 0.05162 mg/Kg 103 70 -130
Chloromethane 0.0500 0.04756 mg/Kg 95 70 -130
cis-1,2-Dichloroethene 0.0500 0.05072 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.04996 mg/Kg 100 70 -130
Dibromomethane 0.0500 0.04917 mg/Kg 98 59 -142
Dichlorobromomethane 0.0500 0.04986 mg/Kg 100 70 -130
Ethyl acetate 0.100 0.1022 mg/Kg 102 70 -130
Ethylbenzene 0.0500 0.04970 mg/Kg 99 70 -130
Ethylene Dibromide 0.0500 0.04811 mg/Kg 96 48 -150
Hexachlorobutadiene 0.0500 0.04597 mg/Kg 92 70 -130
Hexane 0.0500 0.04668 mg/Kg 93 70 -130
Iodomethane 0.0500 0.05034 mg/Kg 101 65 -138
Isopropyl ether 0.0500 0.05026 mg/Kg 101 50 -150
Isopropylbenzene 0.0500 0.04674 mg/Kg 93 70 -130
Methyl tert-butyl ether 0.0500 0.07066 *+mg/Kg 141 70 -130
Methylene Chloride 0.0500 0.04632 mg/Kg 93 54 -149
m-Xylene & p-Xylene 0.0500 0.04992 mg/Kg 100 70 -130
Naphthalene 0.0500 0.05408 mg/Kg 108 46 -150
n-Butylbenzene 0.0500 0.04951 mg/Kg 99 70 -130
n-Heptane 0.0500 0.04421 mg/Kg 88 70 -130
N-Propylbenzene 0.0500 0.04685 mg/Kg 94 70 -130
o-Xylene 0.0500 0.05081 mg/Kg 102 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
sec-Butylbenzene 0.0500 0.04525 mg/Kg 91 69 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Styrene 0.0500 0.04852 mg/Kg 97 70 -130
tert-Butylbenzene 0.0500 0.04460 mg/Kg 89 67 -145
Tetrachloroethene 0.0500 0.05467 mg/Kg 109 70 -130
Toluene 0.0500 0.04736 mg/Kg 95 70 -130
trans-1,2-Dichloroethene 0.0500 0.04918 mg/Kg 98 67 -130
trans-1,3-Dichloropropene 0.0500 0.04796 mg/Kg 96 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04931 mg/Kg 99 54 -150
Trichloroethene 0.0500 0.04649 mg/Kg 93 70 -130
Trichlorofluoromethane 0.0500 0.04860 mg/Kg 97 70 -130
Vinyl acetate 0.100 0.1044 mg/Kg 104 53 -150
Vinyl chloride 0.0500 0.05217 mg/Kg 104 70 -130
Xylenes, Total 0.100 0.1007 mg/Kg 101 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
1124-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,1,1,2-Tetrachloroethane 0.0500 0.04760 mg/Kg 95 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04525 mg/Kg 91 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05103 mg/Kg 102 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04554 mg/Kg 91 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.05138 mg/Kg 103 56 -146 1 30
1,1-Dichloroethane 0.0500 0.05114 mg/Kg 102 70 -130 1 30
1,1-Dichloroethene 0.0500 0.04661 mg/Kg 93 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04535 mg/Kg 91 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05342 mg/Kg 107 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.05003 mg/Kg 100 64 -130 3 30
1,2,4-Trichlorobenzene 0.0500 0.05181 mg/Kg 104 70 -130 1 30
1,2,4-Trimethylbenzene 0.0500 0.04424 mg/Kg 88 70 -130 5 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05391 mg/Kg 108 42 -145 5 30
1,2-Dichlorobenzene 0.0500 0.05222 mg/Kg 104 70 -130 2 30
1,2-Dichloroethane 0.0500 0.05101 mg/Kg 102 68 -139 2 30
1,2-Dichloropropane 0.0500 0.05227 mg/Kg 105 70 -130 2 30
1,3,5-Trimethylbenzene 0.0500 0.04363 mg/Kg 87 70 -130 4 30
1,3-Dichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130 0 30
1,3-Dichloropropane 0.0500 0.05113 mg/Kg 102 54 -150 4 30
1,4-Dichlorobenzene 0.0500 0.05175 mg/Kg 104 70 -130 1 30
2,2-Dichloropropane 0.0500 0.04695 mg/Kg 94 70 -130 0 30
2-Butanone (MEK)0.250 0.2661 mg/Kg 106 40 -150 3 30
2-Chlorotoluene 0.0500 0.04722 mg/Kg 94 70 -130 4 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
2-Hexanone 0.250 0.2742 mg/Kg 110 30 -150 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 0.0500 0.04395 mg/Kg 88 70 -130 2 30
4-Isopropyltoluene 0.0500 0.04605 mg/Kg 92 70 -130 5 30
4-Methyl-2-pentanone (MIBK)0.250 0.2691 mg/Kg 108 34 -150 3 30
Acetone 0.250 0.2746 mg/Kg 110 10 -150 1 50
Benzene 0.0500 0.04910 mg/Kg 98 70 -130 1 30
Bromobenzene 0.0500 0.04700 mg/Kg 94 70 -130 1 30
Bromoform 0.0500 0.04783 mg/Kg 96 68 -130 3 30
Bromomethane 0.0500 0.07191 *+mg/Kg 144 70 -130 3 30
Carbon disulfide 0.0500 0.04790 mg/Kg 96 70 -130 0 30
Carbon tetrachloride 0.0500 0.04381 mg/Kg 88 70 -130 1 30
Chlorobenzene 0.0500 0.04884 mg/Kg 98 70 -130 1 30
Chlorobromomethane 0.0500 0.04851 mg/Kg 97 66 -130 4 30
Chlorodibromomethane 0.0500 0.04874 mg/Kg 97 64 -133 1 30
Chloroethane 0.0500 0.05595 mg/Kg 112 70 -130 2 30
Chloroform 0.0500 0.05259 mg/Kg 105 70 -130 2 30
Chloromethane 0.0500 0.04787 mg/Kg 96 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.05159 mg/Kg 103 70 -130 2 30
cis-1,3-Dichloropropene 0.0500 0.05093 mg/Kg 102 70 -130 2 30
Dibromomethane 0.0500 0.05003 mg/Kg 100 59 -142 2 30
Dichlorobromomethane 0.0500 0.05047 mg/Kg 101 70 -130 1 30
Ethyl acetate 0.100 0.1053 mg/Kg 105 70 -130 3 30
Ethylbenzene 0.0500 0.04805 mg/Kg 96 70 -130 3 30
Ethylene Dibromide 0.0500 0.04917 mg/Kg 98 48 -150 2 30
Hexachlorobutadiene 0.0500 0.04058 mg/Kg 81 70 -130 12 30
Hexane 0.0500 0.04618 mg/Kg 92 70 -130 1 30
Iodomethane 0.0500 0.05191 mg/Kg 104 65 -138 3 30
Isopropyl ether 0.0500 0.05093 mg/Kg 102 50 -150 1 30
Isopropylbenzene 0.0500 0.04478 mg/Kg 90 70 -130 4 30
Methyl tert-butyl ether 0.0500 0.07311 *+mg/Kg 146 70 -130 3 30
Methylene Chloride 0.0500 0.04780 mg/Kg 96 54 -149 3 30
m-Xylene & p-Xylene 0.0500 0.04844 mg/Kg 97 70 -130 3 30
Naphthalene 0.0500 0.05626 mg/Kg 113 46 -150 4 30
n-Butylbenzene 0.0500 0.04566 mg/Kg 91 70 -130 8 30
n-Heptane 0.0500 0.04334 mg/Kg 87 70 -130 2 30
N-Propylbenzene 0.0500 0.04394 mg/Kg 88 70 -130 6 30
o-Xylene 0.0500 0.04945 mg/Kg 99 70 -130 3 30
sec-Butylbenzene 0.0500 0.04148 mg/Kg 83 69 -142 9 30
Styrene 0.0500 0.04795 mg/Kg 96 70 -130 1 30
tert-Butylbenzene 0.0500 0.04247 mg/Kg 85 67 -145 5 30
Tetrachloroethene 0.0500 0.05345 mg/Kg 107 70 -130 2 30
Toluene 0.0500 0.04790 mg/Kg 96 70 -130 1 30
trans-1,2-Dichloroethene 0.0500 0.04960 mg/Kg 99 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04924 mg/Kg 98 54 -150 3 30
trans-1,4-Dichloro-2-butene 0.0500 0.04916 mg/Kg 98 54 -150 0 30
Trichloroethene 0.0500 0.04621 mg/Kg 92 70 -130 1 30
Trichlorofluoromethane 0.0500 0.04853 mg/Kg 97 70 -130 0 30
Vinyl acetate 0.100 0.1066 mg/Kg 107 53 -150 2 30
Vinyl chloride 0.0500 0.05310 mg/Kg 106 70 -130 2 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
Xylenes, Total 0.100 0.09789 mg/Kg 98 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
1144-Bromofluorobenzene (Surr)65 -130
100Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-732793/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/27/22 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/27/22 12:15 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/27/22 12:15 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/27/22 12:15 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/27/22 12:15 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/27/22 12:15 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/27/22 12:15 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/27/22 12:15 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/27/22 12:15 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/27/22 12:15 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/27/22 12:15 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/27/22 12:15 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/27/22 12:15 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/27/22 12:15 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/27/22 12:15 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/27/22 12:15 12-Hexanone
ND 0.002100.00500 mg/Kg 07/27/22 12:15 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/27/22 12:15 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/27/22 12:15 1Acetone
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Benzene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Bromoform
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Bromomethane
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/27/22 12:15 1Chlorobenzene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732793/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
RL MDL
Chlorobromomethane ND 0.00500 0.00200 mg/Kg 07/27/22 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Chloroethane
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Chloroform
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Chloromethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/27/22 12:15 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/27/22 12:15 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Hexane
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Iodomethane
ND 0.001500.0100 mg/Kg 07/27/22 12:15 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/27/22 12:15 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/27/22 12:15 1Naphthalene
ND 0.001900.00500 mg/Kg 07/27/22 12:15 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/27/22 12:15 1n-Heptane
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 1o-Xylene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/27/22 12:15 1Styrene
ND 0.002500.00500 mg/Kg 07/27/22 12:15 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1Toluene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/27/22 12:15 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/27/22 12:15 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/27/22 12:15 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/27/22 12:15 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/27/22 12:15 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/27/22 12:15 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)98 65-130 07/27/22 12:15 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
109 07/27/22 12:15 14-Bromofluorobenzene (Surr)65-130
99 07/27/22 12:15 1Dibromofluoromethane (Surr)65-130
106 07/27/22 12:15 1Toluene-d8 (Surr)65-130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732793/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,1,1,2-Tetrachloroethane 0.0500 0.04642 mg/Kg 93 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04392 mg/Kg 88 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04747 mg/Kg 95 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04462 mg/Kg 89 70 -130
1,1,2-Trichloroethane 0.0500 0.04911 mg/Kg 98 56 -146
1,1-Dichloroethane 0.0500 0.04951 mg/Kg 99 70 -130
1,1-Dichloroethene 0.0500 0.04672 mg/Kg 93 69 -130
1,1-Dichloropropene 0.0500 0.04532 mg/Kg 91 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05149 mg/Kg 103 70 -130
1,2,3-Trichloropropane 0.0500 0.04632 mg/Kg 93 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05154 mg/Kg 103 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04682 mg/Kg 94 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04723 mg/Kg 94 42 -145
1,2-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,2-Dichloroethane 0.0500 0.04879 mg/Kg 98 68 -139
1,2-Dichloropropane 0.0500 0.05029 mg/Kg 101 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04588 mg/Kg 92 70 -130
1,3-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,3-Dichloropropane 0.0500 0.04830 mg/Kg 97 54 -150
1,4-Dichlorobenzene 0.0500 0.05079 mg/Kg 102 70 -130
2,2-Dichloropropane 0.0500 0.04591 mg/Kg 92 70 -130
2-Butanone (MEK)0.250 0.2413 mg/Kg 97 40 -150
2-Chlorotoluene 0.0500 0.04859 mg/Kg 97 70 -130
2-Hexanone 0.250 0.2463 mg/Kg 99 30 -150
4-Chlorotoluene 0.0500 0.04517 mg/Kg 90 70 -130
4-Isopropyltoluene 0.0500 0.04855 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2428 mg/Kg 97 34 -150
Acetone 0.250 0.2500 mg/Kg 100 10 -150
Benzene 0.0500 0.04809 mg/Kg 96 70 -130
Bromobenzene 0.0500 0.04705 mg/Kg 94 70 -130
Bromoform 0.0500 0.04431 mg/Kg 89 68 -130
Bromomethane 0.0500 0.06823 *+mg/Kg 136 70 -130
Carbon disulfide 0.0500 0.04677 mg/Kg 94 70 -130
Carbon tetrachloride 0.0500 0.04244 mg/Kg 85 70 -130
Chlorobenzene 0.0500 0.04831 mg/Kg 97 70 -130
Chlorobromomethane 0.0500 0.04656 mg/Kg 93 66 -130
Chlorodibromomethane 0.0500 0.04649 mg/Kg 93 64 -133
Chloroethane 0.0500 0.05435 mg/Kg 109 70 -130
Chloroform 0.0500 0.04889 mg/Kg 98 70 -130
Chloromethane 0.0500 0.04525 mg/Kg 90 70 -130
cis-1,2-Dichloroethene 0.0500 0.04945 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04942 mg/Kg 99 70 -130
Dibromomethane 0.0500 0.04822 mg/Kg 96 59 -142
Dichlorobromomethane 0.0500 0.04864 mg/Kg 97 70 -130
Ethyl acetate 0.100 0.09684 mg/Kg 97 70 -130
Ethylbenzene 0.0500 0.04837 mg/Kg 97 70 -130
Ethylene Dibromide 0.0500 0.04673 mg/Kg 93 48 -150
Hexachlorobutadiene 0.0500 0.04628 mg/Kg 93 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732793/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
Hexane 0.0500 0.04551 mg/Kg 91 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Iodomethane 0.0500 0.04788 mg/Kg 96 65 -138
Isopropyl ether 0.0500 0.04969 mg/Kg 99 50 -150
Isopropylbenzene 0.0500 0.04617 mg/Kg 92 70 -130
Methyl tert-butyl ether 0.0500 0.06987 *+mg/Kg 140 70 -130
Methylene Chloride 0.0500 0.04593 mg/Kg 92 54 -149
m-Xylene & p-Xylene 0.0500 0.04818 mg/Kg 96 70 -130
Naphthalene 0.0500 0.05146 mg/Kg 103 46 -150
n-Butylbenzene 0.0500 0.05008 mg/Kg 100 70 -130
n-Heptane 0.0500 0.04286 mg/Kg 86 70 -130
N-Propylbenzene 0.0500 0.04676 mg/Kg 94 70 -130
o-Xylene 0.0500 0.04934 mg/Kg 99 70 -130
sec-Butylbenzene 0.0500 0.04477 mg/Kg 90 69 -142
Styrene 0.0500 0.04736 mg/Kg 95 70 -130
tert-Butylbenzene 0.0500 0.04401 mg/Kg 88 67 -145
Tetrachloroethene 0.0500 0.05026 mg/Kg 101 70 -130
Toluene 0.0500 0.04748 mg/Kg 95 70 -130
trans-1,2-Dichloroethene 0.0500 0.04762 mg/Kg 95 67 -130
trans-1,3-Dichloropropene 0.0500 0.04693 mg/Kg 94 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04659 mg/Kg 93 54 -150
Trichloroethene 0.0500 0.04612 mg/Kg 92 70 -130
Trichlorofluoromethane 0.0500 0.04561 mg/Kg 91 70 -130
Vinyl acetate 0.100 0.1030 mg/Kg 103 53 -150
Vinyl chloride 0.0500 0.04981 mg/Kg 100 70 -130
Xylenes, Total 0.100 0.09752 mg/Kg 98 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)65 -130
98Dibromofluoromethane (Surr)65 -130
101Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,1,1,2-Tetrachloroethane 0.0500 0.04682 mg/Kg 94 70 -130 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04419 mg/Kg 88 70 -130 1 30
1,1,2,2-Tetrachloroethane 0.0500 0.04744 mg/Kg 95 64 -130 0 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04432 mg/Kg 89 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.04842 mg/Kg 97 56 -146 1 30
1,1-Dichloroethane 0.0500 0.04985 mg/Kg 100 70 -130 1 30
1,1-Dichloroethene 0.0500 0.04682 mg/Kg 94 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04490 mg/Kg 90 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05099 mg/Kg 102 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.04638 mg/Kg 93 64 -130 0 30
1,2,4-Trichlorobenzene 0.0500 0.05143 mg/Kg 103 70 -130 0 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,2,4-Trimethylbenzene 0.0500 0.04561 mg/Kg 91 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dibromo-3-Chloropropane 0.0500 0.04823 mg/Kg 96 42 -145 2 30
1,2-Dichlorobenzene 0.0500 0.05044 mg/Kg 101 70 -130 1 30
1,2-Dichloroethane 0.0500 0.04860 mg/Kg 97 68 -139 0 30
1,2-Dichloropropane 0.0500 0.04997 mg/Kg 100 70 -130 1 30
1,3,5-Trimethylbenzene 0.0500 0.04449 mg/Kg 89 70 -130 3 30
1,3-Dichlorobenzene 0.0500 0.04994 mg/Kg 100 70 -130 0 30
1,3-Dichloropropane 0.0500 0.04848 mg/Kg 97 54 -150 0 30
1,4-Dichlorobenzene 0.0500 0.05048 mg/Kg 101 70 -130 1 30
2,2-Dichloropropane 0.0500 0.04616 mg/Kg 92 70 -130 1 30
2-Butanone (MEK)0.250 0.2410 mg/Kg 96 40 -150 0 30
2-Chlorotoluene 0.0500 0.04816 mg/Kg 96 70 -130 1 30
2-Hexanone 0.250 0.2498 mg/Kg 100 30 -150 1 30
4-Chlorotoluene 0.0500 0.04464 mg/Kg 89 70 -130 1 30
4-Isopropyltoluene 0.0500 0.04716 mg/Kg 94 70 -130 3 30
4-Methyl-2-pentanone (MIBK)0.250 0.2428 mg/Kg 97 34 -150 0 30
Acetone 0.250 0.2494 mg/Kg 100 10 -150 0 50
Benzene 0.0500 0.04806 mg/Kg 96 70 -130 0 30
Bromobenzene 0.0500 0.04619 mg/Kg 92 70 -130 2 30
Bromoform 0.0500 0.04440 mg/Kg 89 68 -130 0 30
Bromomethane 0.0500 0.06516 mg/Kg 130 70 -130 5 30
Carbon disulfide 0.0500 0.04706 mg/Kg 94 70 -130 1 30
Carbon tetrachloride 0.0500 0.04240 mg/Kg 85 70 -130 0 30
Chlorobenzene 0.0500 0.04799 mg/Kg 96 70 -130 1 30
Chlorobromomethane 0.0500 0.04681 mg/Kg 94 66 -130 1 30
Chlorodibromomethane 0.0500 0.04644 mg/Kg 93 64 -133 0 30
Chloroethane 0.0500 0.05225 mg/Kg 104 70 -130 4 30
Chloroform 0.0500 0.04914 mg/Kg 98 70 -130 0 30
Chloromethane 0.0500 0.04381 mg/Kg 88 70 -130 3 30
cis-1,2-Dichloroethene 0.0500 0.04970 mg/Kg 99 70 -130 0 30
cis-1,3-Dichloropropene 0.0500 0.04920 mg/Kg 98 70 -130 0 30
Dibromomethane 0.0500 0.04790 mg/Kg 96 59 -142 1 30
Dichlorobromomethane 0.0500 0.04851 mg/Kg 97 70 -130 0 30
Ethyl acetate 0.100 0.09674 mg/Kg 97 70 -130 0 30
Ethylbenzene 0.0500 0.04818 mg/Kg 96 70 -130 0 30
Ethylene Dibromide 0.0500 0.04619 mg/Kg 92 48 -150 1 30
Hexachlorobutadiene 0.0500 0.04418 mg/Kg 88 70 -130 5 30
Hexane 0.0500 0.04500 mg/Kg 90 70 -130 1 30
Iodomethane 0.0500 0.04861 mg/Kg 97 65 -138 2 30
Isopropyl ether 0.0500 0.04964 mg/Kg 99 50 -150 0 30
Isopropylbenzene 0.0500 0.04498 mg/Kg 90 70 -130 3 30
Methyl tert-butyl ether 0.0500 0.06982 *+mg/Kg 140 70 -130 0 30
Methylene Chloride 0.0500 0.04600 mg/Kg 92 54 -149 0 30
m-Xylene & p-Xylene 0.0500 0.04823 mg/Kg 96 70 -130 0 30
Naphthalene 0.0500 0.05328 mg/Kg 107 46 -150 3 30
n-Butylbenzene 0.0500 0.04810 mg/Kg 96 70 -130 4 30
n-Heptane 0.0500 0.04225 mg/Kg 84 70 -130 1 30
N-Propylbenzene 0.0500 0.04494 mg/Kg 90 70 -130 4 30
o-Xylene 0.0500 0.04948 mg/Kg 99 70 -130 0 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
sec-Butylbenzene 0.0500 0.04312 mg/Kg 86 69 -142 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Styrene 0.0500 0.04720 mg/Kg 94 70 -130 0 30
tert-Butylbenzene 0.0500 0.04339 mg/Kg 87 67 -145 1 30
Tetrachloroethene 0.0500 0.05004 mg/Kg 100 70 -130 0 30
Toluene 0.0500 0.04754 mg/Kg 95 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.04737 mg/Kg 95 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04719 mg/Kg 94 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04692 mg/Kg 94 54 -150 1 30
Trichloroethene 0.0500 0.04505 mg/Kg 90 70 -130 2 30
Trichlorofluoromethane 0.0500 0.04547 mg/Kg 91 70 -130 0 30
Vinyl acetate 0.100 0.1026 mg/Kg 103 53 -150 0 30
Vinyl chloride 0.0500 0.04923 mg/Kg 98 70 -130 1 30
Xylenes, Total 0.100 0.09771 mg/Kg 98 70 -130 0 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)65 -130
98Dibromofluoromethane (Surr)65 -130
102Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/28/22 13:55 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/28/22 13:55 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/28/22 13:55 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/28/22 13:55 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/28/22 13:55 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/28/22 13:55 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/28/22 13:55 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/28/22 13:55 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/28/22 13:55 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/28/22 13:55 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/28/22 13:55 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/28/22 13:55 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/28/22 13:55 12-Chlorotoluene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
2-Hexanone ND 0.0250 0.0190 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002100.00500 mg/Kg 07/28/22 13:55 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/28/22 13:55 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/28/22 13:55 1Acetone
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Benzene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Bromoform
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Bromomethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/28/22 13:55 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Chloroethane
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Chloroform
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Chloromethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/28/22 13:55 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/28/22 13:55 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Hexane
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Iodomethane
ND 0.001500.0100 mg/Kg 07/28/22 13:55 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/28/22 13:55 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/28/22 13:55 1Naphthalene
ND 0.001900.00500 mg/Kg 07/28/22 13:55 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/28/22 13:55 1n-Heptane
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 1o-Xylene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/28/22 13:55 1Styrene
ND 0.002500.00500 mg/Kg 07/28/22 13:55 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1Toluene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/28/22 13:55 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/28/22 13:55 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/28/22 13:55 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/28/22 13:55 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/28/22 13:55 1Vinyl chloride
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
Xylenes, Total ND 0.0100 0.00360 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1,2-Dichloroethane-d4 (Surr)98 65-130 07/28/22 13:55 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 07/28/22 13:55 14-Bromofluorobenzene (Surr)65-130
99 07/28/22 13:55 1Dibromofluoromethane (Surr)65-130
106 07/28/22 13:55 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732966/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
1,1,1,2-Tetrachloroethane 0.0500 0.04602 mg/Kg 92 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04414 mg/Kg 88 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04782 mg/Kg 96 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04404 mg/Kg 88 70 -130
1,1,2-Trichloroethane 0.0500 0.04855 mg/Kg 97 56 -146
1,1-Dichloroethane 0.0500 0.04920 mg/Kg 98 70 -130
1,1-Dichloroethene 0.0500 0.04531 mg/Kg 91 69 -130
1,1-Dichloropropene 0.0500 0.04497 mg/Kg 90 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130
1,2,3-Trichloropropane 0.0500 0.04576 mg/Kg 92 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04586 mg/Kg 92 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04722 mg/Kg 94 42 -145
1,2-Dichlorobenzene 0.0500 0.04960 mg/Kg 99 70 -130
1,2-Dichloroethane 0.0500 0.04844 mg/Kg 97 68 -139
1,2-Dichloropropane 0.0500 0.05025 mg/Kg 101 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04547 mg/Kg 91 70 -130
1,3-Dichlorobenzene 0.0500 0.05006 mg/Kg 100 70 -130
1,3-Dichloropropane 0.0500 0.04829 mg/Kg 97 54 -150
1,4-Dichlorobenzene 0.0500 0.05047 mg/Kg 101 70 -130
2,2-Dichloropropane 0.0500 0.04591 mg/Kg 92 70 -130
2-Butanone (MEK)0.250 0.2460 mg/Kg 98 40 -150
2-Chlorotoluene 0.0500 0.04848 mg/Kg 97 70 -130
2-Hexanone 0.250 0.2512 mg/Kg 100 30 -150
4-Chlorotoluene 0.0500 0.04472 mg/Kg 89 70 -130
4-Isopropyltoluene 0.0500 0.04862 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2495 mg/Kg 100 34 -150
Acetone 0.250 0.2536 mg/Kg 101 10 -150
Benzene 0.0500 0.04766 mg/Kg 95 70 -130
Bromobenzene 0.0500 0.04606 mg/Kg 92 70 -130
Bromoform 0.0500 0.04420 mg/Kg 88 68 -130
Bromomethane 0.0500 0.06740 *+mg/Kg 135 70 -130
Carbon disulfide 0.0500 0.04560 mg/Kg 91 70 -130
Carbon tetrachloride 0.0500 0.04292 mg/Kg 86 70 -130
Chlorobenzene 0.0500 0.04770 mg/Kg 95 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732966/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
Chlorobromomethane 0.0500 0.04570 mg/Kg 91 66 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chlorodibromomethane 0.0500 0.04655 mg/Kg 93 64 -133
Chloroethane 0.0500 0.05657 mg/Kg 113 70 -130
Chloroform 0.0500 0.04848 mg/Kg 97 70 -130
Chloromethane 0.0500 0.04513 mg/Kg 90 70 -130
cis-1,2-Dichloroethene 0.0500 0.04940 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04867 mg/Kg 97 70 -130
Dibromomethane 0.0500 0.04657 mg/Kg 93 59 -142
Dichlorobromomethane 0.0500 0.04862 mg/Kg 97 70 -130
Ethyl acetate 0.100 0.09874 mg/Kg 99 70 -130
Ethylbenzene 0.0500 0.04767 mg/Kg 95 70 -130
Ethylene Dibromide 0.0500 0.04640 mg/Kg 93 48 -150
Hexachlorobutadiene 0.0500 0.04671 mg/Kg 93 70 -130
Hexane 0.0500 0.04471 mg/Kg 89 70 -130
Iodomethane 0.0500 0.04759 mg/Kg 95 65 -138
Isopropyl ether 0.0500 0.04844 mg/Kg 97 50 -150
Isopropylbenzene 0.0500 0.04602 mg/Kg 92 70 -130
Methyl tert-butyl ether 0.0500 0.06904 *+mg/Kg 138 70 -130
Methylene Chloride 0.0500 0.04516 mg/Kg 90 54 -149
m-Xylene & p-Xylene 0.0500 0.04770 mg/Kg 95 70 -130
Naphthalene 0.0500 0.05151 mg/Kg 103 46 -150
n-Butylbenzene 0.0500 0.05015 mg/Kg 100 70 -130
n-Heptane 0.0500 0.04295 mg/Kg 86 70 -130
N-Propylbenzene 0.0500 0.04647 mg/Kg 93 70 -130
o-Xylene 0.0500 0.04857 mg/Kg 97 70 -130
sec-Butylbenzene 0.0500 0.04488 mg/Kg 90 69 -142
Styrene 0.0500 0.04657 mg/Kg 93 70 -130
tert-Butylbenzene 0.0500 0.04419 mg/Kg 88 67 -145
Tetrachloroethene 0.0500 0.04660 mg/Kg 93 70 -130
Toluene 0.0500 0.04691 mg/Kg 94 70 -130
trans-1,2-Dichloroethene 0.0500 0.04766 mg/Kg 95 67 -130
trans-1,3-Dichloropropene 0.0500 0.04690 mg/Kg 94 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04708 mg/Kg 94 54 -150
Trichloroethene 0.0500 0.04544 mg/Kg 91 70 -130
Trichlorofluoromethane 0.0500 0.04633 mg/Kg 93 70 -130
Vinyl acetate 0.100 0.1043 mg/Kg 104 53 -150
Vinyl chloride 0.0500 0.04784 mg/Kg 96 70 -130
Xylenes, Total 0.100 0.09627 mg/Kg 96 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
1074-Bromofluorobenzene (Surr)65 -130
97Dibromofluoromethane (Surr)65 -130
100Toluene-d8 (Surr)65 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732966/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
1,1,1,2-Tetrachloroethane 0.0500 0.04672 mg/Kg 93 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04502 mg/Kg 90 70 -130 2 30
1,1,2,2-Tetrachloroethane 0.0500 0.04886 mg/Kg 98 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04540 mg/Kg 91 70 -130 3 40
1,1,2-Trichloroethane 0.0500 0.04976 mg/Kg 100 56 -146 2 30
1,1-Dichloroethane 0.0500 0.05097 mg/Kg 102 70 -130 4 30
1,1-Dichloroethene 0.0500 0.04669 mg/Kg 93 69 -130 3 50
1,1-Dichloropropene 0.0500 0.04649 mg/Kg 93 70 -130 3 30
1,2,3-Trichlorobenzene 0.0500 0.05173 mg/Kg 103 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.04830 mg/Kg 97 64 -130 5 30
1,2,4-Trichlorobenzene 0.0500 0.05184 mg/Kg 104 70 -130 1 30
1,2,4-Trimethylbenzene 0.0500 0.04605 mg/Kg 92 70 -130 0 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05080 mg/Kg 102 42 -145 7 30
1,2-Dichlorobenzene 0.0500 0.05094 mg/Kg 102 70 -130 3 30
1,2-Dichloroethane 0.0500 0.04975 mg/Kg 100 68 -139 3 30
1,2-Dichloropropane 0.0500 0.05104 mg/Kg 102 70 -130 2 30
1,3,5-Trimethylbenzene 0.0500 0.04545 mg/Kg 91 70 -130 0 30
1,3-Dichlorobenzene 0.0500 0.05141 mg/Kg 103 70 -130 3 30
1,3-Dichloropropane 0.0500 0.04907 mg/Kg 98 54 -150 2 30
1,4-Dichlorobenzene 0.0500 0.05155 mg/Kg 103 70 -130 2 30
2,2-Dichloropropane 0.0500 0.04709 mg/Kg 94 70 -130 3 30
2-Butanone (MEK)0.250 0.2545 mg/Kg 102 40 -150 3 30
2-Chlorotoluene 0.0500 0.04882 mg/Kg 98 70 -130 1 30
2-Hexanone 0.250 0.2618 mg/Kg 105 30 -150 4 30
4-Chlorotoluene 0.0500 0.04549 mg/Kg 91 70 -130 2 30
4-Isopropyltoluene 0.0500 0.04820 mg/Kg 96 70 -130 1 30
4-Methyl-2-pentanone (MIBK)0.250 0.2566 mg/Kg 103 34 -150 3 30
Acetone 0.250 0.2660 mg/Kg 106 10 -150 5 50
Benzene 0.0500 0.04857 mg/Kg 97 70 -130 2 30
Bromobenzene 0.0500 0.04722 mg/Kg 94 70 -130 2 30
Bromoform 0.0500 0.04492 mg/Kg 90 68 -130 2 30
Bromomethane 0.0500 0.06936 *+mg/Kg 139 70 -130 3 30
Carbon disulfide 0.0500 0.04745 mg/Kg 95 70 -130 4 30
Carbon tetrachloride 0.0500 0.04393 mg/Kg 88 70 -130 2 30
Chlorobenzene 0.0500 0.04882 mg/Kg 98 70 -130 2 30
Chlorobromomethane 0.0500 0.04711 mg/Kg 94 66 -130 3 30
Chlorodibromomethane 0.0500 0.04696 mg/Kg 94 64 -133 1 30
Chloroethane 0.0500 0.05826 mg/Kg 117 70 -130 3 30
Chloroform 0.0500 0.04956 mg/Kg 99 70 -130 2 30
Chloromethane 0.0500 0.04590 mg/Kg 92 70 -130 2 30
cis-1,2-Dichloroethene 0.0500 0.05114 mg/Kg 102 70 -130 3 30
cis-1,3-Dichloropropene 0.0500 0.04986 mg/Kg 100 70 -130 2 30
Dibromomethane 0.0500 0.04943 mg/Kg 99 59 -142 6 30
Dichlorobromomethane 0.0500 0.04964 mg/Kg 99 70 -130 2 30
Ethyl acetate 0.100 0.1021 mg/Kg 102 70 -130 3 30
Ethylbenzene 0.0500 0.04913 mg/Kg 98 70 -130 3 30
Ethylene Dibromide 0.0500 0.04744 mg/Kg 95 48 -150 2 30
Hexachlorobutadiene 0.0500 0.04615 mg/Kg 92 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732966/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
Hexane 0.0500 0.04479 mg/Kg 90 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Iodomethane 0.0500 0.05036 mg/Kg 101 65 -138 6 30
Isopropyl ether 0.0500 0.04821 mg/Kg 96 50 -150 0 30
Isopropylbenzene 0.0500 0.04614 mg/Kg 92 70 -130 0 30
Methyl tert-butyl ether 0.0500 0.07013 *+mg/Kg 140 70 -130 2 30
Methylene Chloride 0.0500 0.04644 mg/Kg 93 54 -149 3 30
m-Xylene & p-Xylene 0.0500 0.04920 mg/Kg 98 70 -130 3 30
Naphthalene 0.0500 0.05275 mg/Kg 106 46 -150 2 30
n-Butylbenzene 0.0500 0.05013 mg/Kg 100 70 -130 0 30
n-Heptane 0.0500 0.04350 mg/Kg 87 70 -130 1 30
N-Propylbenzene 0.0500 0.04626 mg/Kg 93 70 -130 0 30
o-Xylene 0.0500 0.04959 mg/Kg 99 70 -130 2 30
sec-Butylbenzene 0.0500 0.04466 mg/Kg 89 69 -142 0 30
Styrene 0.0500 0.04770 mg/Kg 95 70 -130 2 30
tert-Butylbenzene 0.0500 0.04438 mg/Kg 89 67 -145 0 30
Tetrachloroethene 0.0500 0.05099 mg/Kg 102 70 -130 9 30
Toluene 0.0500 0.04786 mg/Kg 96 70 -130 2 30
trans-1,2-Dichloroethene 0.0500 0.04967 mg/Kg 99 67 -130 4 30
trans-1,3-Dichloropropene 0.0500 0.04738 mg/Kg 95 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04930 mg/Kg 99 54 -150 5 30
Trichloroethene 0.0500 0.04651 mg/Kg 93 70 -130 2 30
Trichlorofluoromethane 0.0500 0.04689 mg/Kg 94 70 -130 1 30
Vinyl acetate 0.100 0.1035 mg/Kg 103 53 -150 1 30
Vinyl chloride 0.0500 0.04889 mg/Kg 98 70 -130 2 30
Xylenes, Total 0.100 0.09879 mg/Kg 99 70 -130 3 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
1114-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 08/01/22 16:03 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 08/01/22 16:03 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 08/01/22 16:03 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 08/01/22 16:03 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 08/01/22 16:03 11,2,4-Trichlorobenzene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
1,2,4-Trimethylbenzene ND 0.00500 0.00250 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001600.0100 mg/Kg 08/01/22 16:03 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 08/01/22 16:03 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 08/01/22 16:03 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 08/01/22 16:03 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 08/01/22 16:03 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 08/01/22 16:03 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 08/01/22 16:03 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 08/01/22 16:03 12-Hexanone
ND 0.002100.00500 mg/Kg 08/01/22 16:03 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 08/01/22 16:03 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 08/01/22 16:03 1Acetone
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Benzene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Bromobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Bromoform
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Bromomethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Carbon disulfide
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 08/01/22 16:03 1Chlorobenzene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Chloroethane
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Chloroform
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Chloromethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Dibromomethane
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 08/01/22 16:03 1Ethyl acetate
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Ethylbenzene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 08/01/22 16:03 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Hexane
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Iodomethane
ND 0.001500.0100 mg/Kg 08/01/22 16:03 1Isopropyl ether
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 08/01/22 16:03 1Methylene Chloride
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 08/01/22 16:03 1Naphthalene
ND 0.001900.00500 mg/Kg 08/01/22 16:03 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 08/01/22 16:03 1n-Heptane
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 1o-Xylene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
sec-Butylbenzene ND 0.00500 0.00200 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001900.00500 mg/Kg 08/01/22 16:03 1Styrene
ND 0.002500.00500 mg/Kg 08/01/22 16:03 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1Toluene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 08/01/22 16:03 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 08/01/22 16:03 1Trichloroethene
ND 0.003100.00500 mg/Kg 08/01/22 16:03 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 08/01/22 16:03 1Vinyl acetate
ND 0.002800.00500 mg/Kg 08/01/22 16:03 1Vinyl chloride
ND 0.003600.0100 mg/Kg 08/01/22 16:03 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)107 65-130 08/01/22 16:03 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 08/01/22 16:03 14-Bromofluorobenzene (Surr)65-130
104 08/01/22 16:03 1Dibromofluoromethane (Surr)65-130
100 08/01/22 16:03 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,1,1,2-Tetrachloroethane 0.0500 0.05364 mg/Kg 107 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04891 mg/Kg 98 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05396 mg/Kg 108 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04828 mg/Kg 97 70 -130
1,1,2-Trichloroethane 0.0500 0.04954 mg/Kg 99 56 -146
1,1-Dichloroethane 0.0500 0.05002 mg/Kg 100 70 -130
1,1-Dichloroethene 0.0500 0.05195 mg/Kg 104 69 -130
1,1-Dichloropropene 0.0500 0.04947 mg/Kg 99 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05339 mg/Kg 107 70 -130
1,2,3-Trichloropropane 0.0500 0.05563 mg/Kg 111 64 -130
1,2,4-Trichlorobenzene 0.0500 0.04933 mg/Kg 99 70 -130
1,2,4-Trimethylbenzene 0.0500 0.05678 mg/Kg 114 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.05425 mg/Kg 108 42 -145
1,2-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,2-Dichloroethane 0.0500 0.05031 mg/Kg 101 68 -139
1,2-Dichloropropane 0.0500 0.05287 mg/Kg 106 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05632 mg/Kg 113 70 -130
1,3-Dichlorobenzene 0.0500 0.04927 mg/Kg 99 70 -130
1,3-Dichloropropane 0.0500 0.05070 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.04842 mg/Kg 97 70 -130
2,2-Dichloropropane 0.0500 0.05024 mg/Kg 100 70 -130
2-Butanone (MEK)0.250 0.2579 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.05567 mg/Kg 111 70 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
2-Hexanone 0.250 0.2323 mg/Kg 93 30 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
4-Chlorotoluene 0.0500 0.05476 mg/Kg 110 70 -130
4-Isopropyltoluene 0.0500 0.04969 mg/Kg 99 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2506 mg/Kg 100 34 -150
Acetone 0.250 0.2474 mg/Kg 99 10 -150
Benzene 0.0500 0.05006 mg/Kg 100 70 -130
Bromobenzene 0.0500 0.05549 mg/Kg 111 70 -130
Bromoform 0.0500 0.05532 mg/Kg 111 68 -130
Bromomethane 0.0500 0.05517 mg/Kg 110 70 -130
Carbon disulfide 0.0500 0.05260 mg/Kg 105 70 -130
Carbon tetrachloride 0.0500 0.04800 mg/Kg 96 70 -130
Chlorobenzene 0.0500 0.05045 mg/Kg 101 70 -130
Chlorobromomethane 0.0500 0.05102 mg/Kg 102 66 -130
Chlorodibromomethane 0.0500 0.05252 mg/Kg 105 64 -133
Chloroethane 0.0500 0.04867 mg/Kg 97 70 -130
Chloroform 0.0500 0.04878 mg/Kg 98 70 -130
Chloromethane 0.0500 0.05148 mg/Kg 103 70 -130
cis-1,2-Dichloroethene 0.0500 0.05026 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.05236 mg/Kg 105 70 -130
Dibromomethane 0.0500 0.05195 mg/Kg 104 59 -142
Dichlorobromomethane 0.0500 0.05096 mg/Kg 102 70 -130
Ethylbenzene 0.0500 0.04886 mg/Kg 98 70 -130
Ethylene Dibromide 0.0500 0.04980 mg/Kg 100 48 -150
Hexachlorobutadiene 0.0500 0.04698 mg/Kg 94 70 -130
Hexane 0.0500 0.04527 mg/Kg 91 70 -130
Iodomethane 0.0500 0.05813 mg/Kg 116 65 -138
Isopropylbenzene 0.0500 0.05148 mg/Kg 103 70 -130
Methyl tert-butyl ether 0.0500 0.05181 mg/Kg 104 70 -130
Methylene Chloride 0.0500 0.05051 mg/Kg 101 54 -149
m-Xylene & p-Xylene 0.0500 0.04874 mg/Kg 97 70 -130
Naphthalene 0.0500 0.05456 mg/Kg 109 46 -150
n-Butylbenzene 0.0500 0.04887 mg/Kg 98 70 -130
n-Heptane 0.0500 0.04806 mg/Kg 96 70 -130
N-Propylbenzene 0.0500 0.05337 mg/Kg 107 70 -130
o-Xylene 0.0500 0.04868 mg/Kg 97 70 -130
sec-Butylbenzene 0.0500 0.05572 mg/Kg 111 69 -142
Styrene 0.0500 0.04754 mg/Kg 95 70 -130
tert-Butylbenzene 0.0500 0.05513 mg/Kg 110 67 -145
Tetrachloroethene 0.0500 0.05030 mg/Kg 101 70 -130
Toluene 0.0500 0.04913 mg/Kg 98 70 -130
trans-1,2-Dichloroethene 0.0500 0.05019 mg/Kg 100 67 -130
trans-1,3-Dichloropropene 0.0500 0.05309 mg/Kg 106 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.05589 mg/Kg 112 54 -150
Trichloroethene 0.0500 0.04892 mg/Kg 98 70 -130
Trichlorofluoromethane 0.0500 0.05250 mg/Kg 105 70 -130
Vinyl acetate 0.100 0.1517 *+mg/Kg 152 53 -150
Vinyl chloride 0.0500 0.05026 mg/Kg 101 70 -130
Xylenes, Total 0.100 0.09742 mg/Kg 97 70 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)65 -130
102Dibromofluoromethane (Surr)65 -130
112Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733530/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,1,1,2-Tetrachloroethane 0.0500 0.05256 mg/Kg 105 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04881 mg/Kg 98 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05128 mg/Kg 103 64 -130 5 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04933 mg/Kg 99 70 -130 2 40
1,1,2-Trichloroethane 0.0500 0.04936 mg/Kg 99 56 -146 0 30
1,1-Dichloroethane 0.0500 0.05000 mg/Kg 100 70 -130 0 30
1,1-Dichloroethene 0.0500 0.05186 mg/Kg 104 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04971 mg/Kg 99 70 -130 0 30
1,2,3-Trichlorobenzene 0.0500 0.05796 mg/Kg 116 70 -130 8 30
1,2,3-Trichloropropane 0.0500 0.05149 mg/Kg 103 64 -130 8 30
1,2,4-Trichlorobenzene 0.0500 0.05063 mg/Kg 101 70 -130 3 30
1,2,4-Trimethylbenzene 0.0500 0.05062 mg/Kg 101 70 -130 11 30
1,2-Dibromo-3-Chloropropane 0.0500 0.06249 mg/Kg 125 42 -145 14 30
1,2-Dichlorobenzene 0.0500 0.05143 mg/Kg 103 70 -130 2 30
1,2-Dichloroethane 0.0500 0.04978 mg/Kg 100 68 -139 1 30
1,2-Dichloropropane 0.0500 0.04694 mg/Kg 94 70 -130 12 30
1,3,5-Trimethylbenzene 0.0500 0.04973 mg/Kg 99 70 -130 12 30
1,3-Dichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130 4 30
1,3-Dichloropropane 0.0500 0.05008 mg/Kg 100 54 -150 1 30
1,4-Dichlorobenzene 0.0500 0.05018 mg/Kg 100 70 -130 4 30
2,2-Dichloropropane 0.0500 0.05007 mg/Kg 100 70 -130 0 30
2-Butanone (MEK)0.250 0.2591 mg/Kg 104 40 -150 0 30
2-Chlorotoluene 0.0500 0.05079 mg/Kg 102 70 -130 9 30
2-Hexanone 0.250 0.2409 mg/Kg 96 30 -150 4 30
4-Chlorotoluene 0.0500 0.04929 mg/Kg 99 70 -130 10 30
4-Isopropyltoluene 0.0500 0.05106 mg/Kg 102 70 -130 3 30
4-Methyl-2-pentanone (MIBK)0.250 0.2527 mg/Kg 101 34 -150 1 30
Acetone 0.250 0.2457 mg/Kg 98 10 -150 1 50
Benzene 0.0500 0.05027 mg/Kg 101 70 -130 0 30
Bromobenzene 0.0500 0.05144 mg/Kg 103 70 -130 8 30
Bromoform 0.0500 0.05109 mg/Kg 102 68 -130 8 30
Bromomethane 0.0500 0.05582 mg/Kg 112 70 -130 1 30
Carbon disulfide 0.0500 0.05263 mg/Kg 105 70 -130 0 30
Carbon tetrachloride 0.0500 0.04842 mg/Kg 97 70 -130 1 30
Chlorobenzene 0.0500 0.05072 mg/Kg 101 70 -130 1 30
Chlorobromomethane 0.0500 0.05139 mg/Kg 103 66 -130 1 30
Chlorodibromomethane 0.0500 0.05280 mg/Kg 106 64 -133 1 30
Chloroethane 0.0500 0.04629 mg/Kg 93 70 -130 5 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733530/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
Chloroform 0.0500 0.04968 mg/Kg 99 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 0.0500 0.05074 mg/Kg 101 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.04990 mg/Kg 100 70 -130 1 30
cis-1,3-Dichloropropene 0.0500 0.04839 mg/Kg 97 70 -130 8 30
Dibromomethane 0.0500 0.04707 mg/Kg 94 59 -142 10 30
Dichlorobromomethane 0.0500 0.04786 mg/Kg 96 70 -130 6 30
Ethylbenzene 0.0500 0.05128 mg/Kg 103 70 -130 5 30
Ethylene Dibromide 0.0500 0.05028 mg/Kg 101 48 -150 1 30
Hexachlorobutadiene 0.0500 0.05258 mg/Kg 105 70 -130 11 30
Hexane 0.0500 0.04551 mg/Kg 91 70 -130 1 30
Iodomethane 0.0500 0.05928 mg/Kg 119 65 -138 2 30
Isopropylbenzene 0.0500 0.05059 mg/Kg 101 70 -130 2 30
Methyl tert-butyl ether 0.0500 0.05209 mg/Kg 104 70 -130 1 30
Methylene Chloride 0.0500 0.05073 mg/Kg 101 54 -149 0 30
m-Xylene & p-Xylene 0.0500 0.04939 mg/Kg 99 70 -130 1 30
Naphthalene 0.0500 0.05501 mg/Kg 110 46 -150 1 30
n-Butylbenzene 0.0500 0.04969 mg/Kg 99 70 -130 2 30
n-Heptane 0.0500 0.05038 mg/Kg 101 70 -130 5 30
N-Propylbenzene 0.0500 0.04992 mg/Kg 100 70 -130 7 30
o-Xylene 0.0500 0.04977 mg/Kg 100 70 -130 2 30
sec-Butylbenzene 0.0500 0.05184 mg/Kg 104 69 -142 7 30
Styrene 0.0500 0.04862 mg/Kg 97 70 -130 2 30
tert-Butylbenzene 0.0500 0.05145 mg/Kg 103 67 -145 7 30
Tetrachloroethene 0.0500 0.05258 mg/Kg 105 70 -130 4 30
Toluene 0.0500 0.04899 mg/Kg 98 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.05101 mg/Kg 102 67 -130 2 30
trans-1,3-Dichloropropene 0.0500 0.05242 mg/Kg 105 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04913 mg/Kg 98 54 -150 13 30
Trichloroethene 0.0500 0.04895 mg/Kg 98 70 -130 0 30
Trichlorofluoromethane 0.0500 0.05228 mg/Kg 105 70 -130 0 30
Vinyl acetate 0.100 0.1490 mg/Kg 149 53 -150 2 30
Vinyl chloride 0.0500 0.04991 mg/Kg 100 70 -130 1 30
Xylenes, Total 0.100 0.09916 mg/Kg 99 70 -130 2 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)65 -130
103Dibromofluoromethane (Surr)65 -130
97Toluene-d8 (Surr)65 -130
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1900.500 ug/L 08/03/22 17:40 11,1,1-Trichloroethane
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
1,1,2,2-Tetrachloroethane ND 0.500 0.100 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1400.500 ug/L 08/03/22 17:40 11,1,2-Trichloroethane
ND 0.1800.500 ug/L 08/03/22 17:40 11,1-Dichloroethane
ND 0.1800.500 ug/L 08/03/22 17:40 11,1-Dichloroethene
ND 0.2000.500 ug/L 08/03/22 17:40 11,1-Dichloropropene
ND 0.7701.00 ug/L 08/03/22 17:40 11,2,3-Trichlorobenzene
ND 0.1200.500 ug/L 08/03/22 17:40 11,2,3-Trichloropropane
ND 0.3500.500 ug/L 08/03/22 17:40 11,2,4-Trichlorobenzene
ND 0.1400.500 ug/L 08/03/22 17:40 11,2,4-Trimethylbenzene
ND 0.1200.500 ug/L 08/03/22 17:40 11,2-Dichlorobenzene
ND 0.1600.500 ug/L 08/03/22 17:40 11,2-Dichloroethane
ND 0.2300.500 ug/L 08/03/22 17:40 11,2-Dichloroethene, Total
ND 0.1600.500 ug/L 08/03/22 17:40 11,2-Dichloropropane
ND 0.1600.500 ug/L 08/03/22 17:40 11,3,5-Trimethylbenzene
ND 0.1600.500 ug/L 08/03/22 17:40 11,3-Dichlorobenzene
ND 0.1400.500 ug/L 08/03/22 17:40 11,3-Dichloropropane
ND 0.2200.500 ug/L 08/03/22 17:40 11,3-Dichloropropene, Total
ND 0.1200.500 ug/L 08/03/22 17:40 11,4-Dichlorobenzene
ND 0.1800.500 ug/L 08/03/22 17:40 12,2-Dichloropropane
ND 5.2010.0 ug/L 08/03/22 17:40 12-Butanone (MEK)
ND 0.1600.500 ug/L 08/03/22 17:40 12-Chlorotoluene
ND 5.0010.0 ug/L 08/03/22 17:40 12-Hexanone
ND 9.1020.0 ug/L 08/03/22 17:40 13,3-Dimethyl-1-butanol
ND 0.1600.500 ug/L 08/03/22 17:40 14-Chlorotoluene
ND 0.1800.500 ug/L 08/03/22 17:40 14-Isopropyltoluene
ND 5.2010.0 ug/L 08/03/22 17:40 14-Methyl-2-pentanone (MIBK)
ND 5.6020.0 ug/L 08/03/22 17:40 1Acetone
ND 0.1800.500 ug/L 08/03/22 17:40 1Benzene
ND 0.1400.500 ug/L 08/03/22 17:40 1Bromobenzene
ND 0.1800.500 ug/L 08/03/22 17:40 1Bromoform
ND 2.305.00 ug/L 08/03/22 17:40 1Bromomethane
ND 0.2200.500 ug/L 08/03/22 17:40 1Carbon tetrachloride
ND 0.1600.500 ug/L 08/03/22 17:40 1Chlorobenzene
ND 0.1300.500 ug/L 08/03/22 17:40 1Chlorobromomethane
ND 0.4601.00 ug/L 08/03/22 17:40 1Chlorodibromomethane
ND 4.1010.0 ug/L 08/03/22 17:40 1Chloroethane
ND 0.3800.500 ug/L 08/03/22 17:40 1Chloroform
ND 0.1000.500 ug/L 08/03/22 17:40 1Chloromethane
ND 0.06400.500 ug/L 08/03/22 17:40 1cis-1,2-Dichloroethene
ND 0.1100.500 ug/L 08/03/22 17:40 1cis-1,3-Dichloropropene
ND 0.1700.500 ug/L 08/03/22 17:40 1Dibromomethane
ND 0.4101.00 ug/L 08/03/22 17:40 1Dichlorobromomethane
ND 0.09100.500 ug/L 08/03/22 17:40 1Dichlorodifluoromethane
ND 0.1400.500 ug/L 08/03/22 17:40 1Dichlorofluoromethane
ND 140200 ug/L 08/03/22 17:40 1Ethanol
ND 0.09200.500 ug/L 08/03/22 17:40 1Ethyl ether
ND 0.1700.500 ug/L 08/03/22 17:40 1Ethylbenzene
ND 0.1700.500 ug/L 08/03/22 17:40 1Ethylene Dibromide
ND 0.05800.500 ug/L 08/03/22 17:40 1Isopropyl ether
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
Isopropylbenzene ND 0.500 0.180 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1100.500 ug/L 08/03/22 17:40 1Methyl tert-butyl ether
ND 0.1500.500 ug/L 08/03/22 17:40 1Methylene Chloride
ND 0.1800.500 ug/L 08/03/22 17:40 1m-Xylene & p-Xylene
ND 1.202.00 ug/L 08/03/22 17:40 1Naphthalene
ND 0.1601.00 ug/L 08/03/22 17:40 1n-Butylbenzene
ND 0.1800.500 ug/L 08/03/22 17:40 1N-Propylbenzene
ND 0.1500.500 ug/L 08/03/22 17:40 1o-Xylene
ND 0.1701.00 ug/L 08/03/22 17:40 1sec-Butylbenzene
ND 0.1700.500 ug/L 08/03/22 17:40 1Styrene
ND 1.905.00 ug/L 08/03/22 17:40 1t-Amyl alcohol
ND 0.07900.500 ug/L 08/03/22 17:40 1Tert-amyl methyl ether
ND 0.05800.500 ug/L 08/03/22 17:40 1Tert-butyl ethyl ether
ND 1.765.00 ug/L 08/03/22 17:40 1tert-Butyl Formate
ND 0.1800.500 ug/L 08/03/22 17:40 1tert-Butylbenzene
ND 0.2200.500 ug/L 08/03/22 17:40 1Tetrachloroethene
ND 0.2000.500 ug/L 08/03/22 17:40 1Toluene
ND 0.1700.500 ug/L 08/03/22 17:40 1trans-1,2-Dichloroethene
ND 0.1200.500 ug/L 08/03/22 17:40 1trans-1,3-Dichloropropene
ND 0.2000.500 ug/L 08/03/22 17:40 1Trichloroethene
ND 0.1400.500 ug/L 08/03/22 17:40 1Trichlorofluoromethane
ND 0.6401.00 ug/L 08/03/22 17:40 1Vinyl acetate
ND 0.1200.500 ug/L 08/03/22 17:40 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr)97 70-130 08/03/22 17:40 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 08/03/22 17:40 14-Bromofluorobenzene (Surr)70-130
99 08/03/22 17:40 1Dibromofluoromethane (Surr)70-130
106 08/03/22 17:40 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,1,1,2-Tetrachloroethane 25.0 26.90 ug/L 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 25.0 25.17 ug/L 101 70 -130
1,1,2,2-Tetrachloroethane 25.0 25.43 ug/L 102 70 -130
1,1,2-Trichloroethane 25.0 23.62 ug/L 94 70 -130
1,1-Dichloroethane 25.0 23.66 ug/L 95 70 -130
1,1-Dichloroethene 25.0 24.97 ug/L 100 70 -130
1,1-Dichloropropene 25.0 24.02 ug/L 96 70 -130
1,2,3-Trichlorobenzene 25.0 25.19 ug/L 101 70 -130
1,2,3-Trichloropropane 25.0 25.16 ug/L 101 70 -130
1,2,4-Trichlorobenzene 25.0 24.93 ug/L 100 70 -130
1,2,4-Trimethylbenzene 25.0 25.79 ug/L 103 70 -130
1,2-Dichlorobenzene 25.0 24.90 ug/L 100 70 -130
1,2-Dichloroethane 25.0 23.26 ug/L 93 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,2-Dichloroethene, Total 50.0 48.31 ug/L 97 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloropropane 25.0 23.55 ug/L 94 70 -130
1,3,5-Trimethylbenzene 25.0 25.96 ug/L 104 70 -130
1,3-Dichlorobenzene 25.0 25.48 ug/L 102 70 -130
1,3-Dichloropropane 25.0 23.65 ug/L 95 70 -130
1,3-Dichloropropene, Total 50.0 52.38 ug/L 105 70 -130
1,4-Dichlorobenzene 25.0 24.93 ug/L 100 70 -130
2,2-Dichloropropane 25.0 26.04 ug/L 104 70 -130
2-Butanone (MEK)125 117.6 ug/L 94 70 -130
2-Chlorotoluene 25.0 25.51 ug/L 102 70 -130
2-Hexanone 125 122.8 ug/L 98 70 -130
3,3-Dimethyl-1-butanol 100 104.7 ug/L 105 70 -130
4-Chlorotoluene 25.0 25.27 ug/L 101 70 -130
4-Isopropyltoluene 25.0 26.64 ug/L 107 70 -130
4-Methyl-2-pentanone (MIBK)125 121.7 ug/L 97 70 -130
Acetone 125 123.8 ug/L 99 70 -130
Benzene 25.0 23.49 ug/L 94 70 -130
Bromobenzene 25.0 25.57 ug/L 102 70 -130
Bromoform 25.0 29.65 ug/L 119 70 -130
Bromomethane 25.0 29.14 ug/L 117 70 -130
Carbon tetrachloride 25.0 25.63 ug/L 103 70 -130
Chlorobenzene 25.0 24.44 ug/L 98 70 -130
Chlorobromomethane 25.0 24.42 ug/L 98 70 -130
Chlorodibromomethane 25.0 26.79 ug/L 107 70 -130
Chloroethane 25.0 25.13 ug/L 101 70 -130
Chloroform 25.0 24.24 ug/L 97 70 -130
Chloromethane 25.0 23.42 ug/L 94 70 -130
cis-1,2-Dichloroethene 25.0 23.84 ug/L 95 70 -130
cis-1,3-Dichloropropene 25.0 26.05 ug/L 104 70 -130
Dibromomethane 25.0 24.62 ug/L 98 70 -130
Dichlorobromomethane 25.0 25.80 ug/L 103 70 -130
Dichlorodifluoromethane 25.0 23.10 ug/L 92 70 -130
Dichlorofluoromethane 25.0 24.12 ug/L 96 70 -130
Ethanol 1000 929.0 ug/L 93 70 -130
Ethyl ether 25.0 23.87 ug/L 95 70 -130
Ethylbenzene 25.0 25.76 ug/L 103 70 -130
Ethylene Dibromide 25.0 24.74 ug/L 99 70 -130
Isopropyl ether 25.0 23.37 ug/L 93 70 -130
Isopropylbenzene 25.0 26.64 ug/L 107 70 -130
Methyl tert-butyl ether 25.0 24.24 ug/L 97 70 -130
Methylene Chloride 25.0 24.67 ug/L 99 70 -130
m-Xylene & p-Xylene 25.0 25.64 ug/L 103 70 -130
Naphthalene 25.0 26.46 ug/L 106 70 -130
n-Butylbenzene 25.0 25.62 ug/L 102 70 -130
N-Propylbenzene 25.0 25.91 ug/L 104 70 -130
o-Xylene 25.0 25.80 ug/L 103 70 -130
sec-Butylbenzene 25.0 26.67 ug/L 107 70 -130
Styrene 25.0 26.73 ug/L 107 70 -130
t-Amyl alcohol 250 234.3 ug/L 94 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
Tert-amyl methyl ether 25.0 24.56 ug/L 98 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tert-butyl ethyl ether 25.0 24.47 ug/L 98 70 -130
tert-Butyl Formate 100 107.5 ug/L 107 70 -130
tert-Butylbenzene 25.0 26.34 ug/L 105 70 -130
Tetrachloroethene 25.0 24.19 ug/L 97 70 -130
Toluene 25.0 23.94 ug/L 96 70 -130
trans-1,2-Dichloroethene 25.0 24.47 ug/L 98 70 -130
trans-1,3-Dichloropropene 25.0 26.33 ug/L 105 70 -130
Trichloroethene 25.0 24.54 ug/L 98 70 -130
Trichlorofluoromethane 25.0 25.84 ug/L 103 70 -130
Vinyl acetate 50.0 51.35 ug/L 103 70 -130
Vinyl chloride 25.0 22.84 ug/L 91 70 -130
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,1,1,2-Tetrachloroethane 25.0 26.45 ug/L 106 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 25.0 24.30 ug/L 97 70 -130 3 30
1,1,2,2-Tetrachloroethane 25.0 24.94 ug/L 100 70 -130 2 30
1,1,2-Trichloroethane 25.0 23.41 ug/L 94 70 -130 1 30
1,1-Dichloroethane 25.0 23.04 ug/L 92 70 -130 3 30
1,1-Dichloroethene 25.0 24.25 ug/L 97 70 -130 3 30
1,1-Dichloropropene 25.0 22.95 ug/L 92 70 -130 5 30
1,2,3-Trichlorobenzene 25.0 25.47 ug/L 102 70 -130 1 30
1,2,3-Trichloropropane 25.0 24.92 ug/L 100 70 -130 1 30
1,2,4-Trichlorobenzene 25.0 24.77 ug/L 99 70 -130 1 30
1,2,4-Trimethylbenzene 25.0 25.73 ug/L 103 70 -130 0 50
1,2-Dichlorobenzene 25.0 24.50 ug/L 98 70 -130 2 30
1,2-Dichloroethane 25.0 23.19 ug/L 93 70 -130 0 30
1,2-Dichloroethene, Total 50.0 46.76 ug/L 94 70 -130 3 30
1,2-Dichloropropane 25.0 23.01 ug/L 92 70 -130 2 30
1,3,5-Trimethylbenzene 25.0 25.65 ug/L 103 70 -130 1 50
1,3-Dichlorobenzene 25.0 24.82 ug/L 99 70 -130 3 30
1,3-Dichloropropane 25.0 23.45 ug/L 94 70 -130 1 30
1,3-Dichloropropene, Total 50.0 51.38 ug/L 103 70 -130 2 50
1,4-Dichlorobenzene 25.0 24.48 ug/L 98 70 -130 2 30
2,2-Dichloropropane 25.0 24.94 ug/L 100 70 -130 4 30
2-Butanone (MEK)125 116.6 ug/L 93 70 -130 1 30
2-Chlorotoluene 25.0 24.76 ug/L 99 70 -130 3 30
2-Hexanone 125 123.6 ug/L 99 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
3,3-Dimethyl-1-butanol 100 107.4 ug/L 107 70 -130 3
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 25.0 24.91 ug/L 100 70 -130 1 30
4-Isopropyltoluene 25.0 25.69 ug/L 103 70 -130 4 50
4-Methyl-2-pentanone (MIBK)125 121.2 ug/L 97 70 -130 0 30
Acetone 125 123.1 ug/L 98 70 -130 1 50
Benzene 25.0 22.81 ug/L 91 70 -130 3 30
Bromobenzene 25.0 25.16 ug/L 101 70 -130 2 30
Bromoform 25.0 29.61 ug/L 118 70 -130 0 30
Bromomethane 25.0 27.65 ug/L 111 70 -130 5 50
Carbon tetrachloride 25.0 24.53 ug/L 98 70 -130 4 30
Chlorobenzene 25.0 23.69 ug/L 95 70 -130 3 30
Chlorobromomethane 25.0 23.56 ug/L 94 70 -130 4 30
Chlorodibromomethane 25.0 26.51 ug/L 106 70 -130 1 50
Chloroethane 25.0 23.65 ug/L 95 70 -130 6 40
Chloroform 25.0 23.39 ug/L 94 70 -130 4 30
Chloromethane 25.0 22.86 ug/L 91 70 -130 2 30
cis-1,2-Dichloroethene 25.0 22.96 ug/L 92 70 -130 4 30
cis-1,3-Dichloropropene 25.0 25.56 ug/L 102 70 -130 2 30
Dibromomethane 25.0 24.14 ug/L 97 70 -130 2 30
Dichlorobromomethane 25.0 25.46 ug/L 102 70 -130 1 30
Dichlorodifluoromethane 25.0 22.45 ug/L 90 70 -130 3 50
Dichlorofluoromethane 25.0 23.20 ug/L 93 70 -130 4 50
Ethanol 1000 936.3 ug/L 94 70 -130 1 50
Ethyl ether 25.0 23.59 ug/L 94 70 -130 1 50
Ethylbenzene 25.0 24.83 ug/L 99 70 -130 4 30
Ethylene Dibromide 25.0 24.37 ug/L 97 70 -130 2 30
Isopropyl ether 25.0 23.06 ug/L 92 70 -130 1 50
Isopropylbenzene 25.0 25.52 ug/L 102 70 -130 4 30
Methyl tert-butyl ether 25.0 24.30 ug/L 97 70 -130 0 30
Methylene Chloride 25.0 24.06 ug/L 96 70 -130 3 30
m-Xylene & p-Xylene 25.0 24.97 ug/L 100 70 -130 3 30
Naphthalene 25.0 27.18 ug/L 109 70 -130 3 30
n-Butylbenzene 25.0 24.86 ug/L 99 70 -130 3 30
N-Propylbenzene 25.0 25.07 ug/L 100 70 -130 3 30
o-Xylene 25.0 25.25 ug/L 101 70 -130 2 30
sec-Butylbenzene 25.0 25.91 ug/L 104 70 -130 3 30
Styrene 25.0 26.10 ug/L 104 70 -130 2 30
t-Amyl alcohol 250 234.8 ug/L 94 70 -130 0 30
Tert-amyl methyl ether 25.0 24.52 ug/L 98 70 -130 0 30
Tert-butyl ethyl ether 25.0 24.23 ug/L 97 70 -130 1 30
tert-Butyl Formate 100 105.0 ug/L 105 70 -130 2
tert-Butylbenzene 25.0 25.61 ug/L 102 70 -130 3 30
Tetrachloroethene 25.0 23.24 ug/L 93 70 -130 4 30
Toluene 25.0 23.17 ug/L 93 70 -130 3 30
trans-1,2-Dichloroethene 25.0 23.81 ug/L 95 70 -130 3 30
trans-1,3-Dichloropropene 25.0 25.82 ug/L 103 70 -130 2 50
Trichloroethene 25.0 23.77 ug/L 95 70 -130 3 30
Trichlorofluoromethane 25.0 24.75 ug/L 99 70 -130 4 30
Vinyl acetate 50.0 48.06 ug/L 96 70 -130 7 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
Vinyl chloride 25.0 22.21 ug/L 89 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-734030/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/04/22 11:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1900.500 ug/L 08/04/22 11:08 11,1,1-Trichloroethane
ND 0.1000.500 ug/L 08/04/22 11:08 11,1,2,2-Tetrachloroethane
ND 0.1400.500 ug/L 08/04/22 11:08 11,1,2-Trichloroethane
ND 0.1800.500 ug/L 08/04/22 11:08 11,1-Dichloroethane
ND 0.1800.500 ug/L 08/04/22 11:08 11,1-Dichloroethene
ND 0.2000.500 ug/L 08/04/22 11:08 11,1-Dichloropropene
ND 0.7701.00 ug/L 08/04/22 11:08 11,2,3-Trichlorobenzene
ND 0.1200.500 ug/L 08/04/22 11:08 11,2,3-Trichloropropane
ND 0.3500.500 ug/L 08/04/22 11:08 11,2,4-Trichlorobenzene
ND 0.1400.500 ug/L 08/04/22 11:08 11,2,4-Trimethylbenzene
ND 0.1200.500 ug/L 08/04/22 11:08 11,2-Dichlorobenzene
ND 0.1600.500 ug/L 08/04/22 11:08 11,2-Dichloroethane
ND 0.2300.500 ug/L 08/04/22 11:08 11,2-Dichloroethene, Total
ND 0.1600.500 ug/L 08/04/22 11:08 11,2-Dichloropropane
ND 0.1600.500 ug/L 08/04/22 11:08 11,3,5-Trimethylbenzene
ND 0.1600.500 ug/L 08/04/22 11:08 11,3-Dichlorobenzene
ND 0.1400.500 ug/L 08/04/22 11:08 11,3-Dichloropropane
ND 0.2200.500 ug/L 08/04/22 11:08 11,3-Dichloropropene, Total
ND 0.1200.500 ug/L 08/04/22 11:08 11,4-Dichlorobenzene
ND 0.1800.500 ug/L 08/04/22 11:08 12,2-Dichloropropane
ND 5.2010.0 ug/L 08/04/22 11:08 12-Butanone (MEK)
ND 0.1600.500 ug/L 08/04/22 11:08 12-Chlorotoluene
ND 5.0010.0 ug/L 08/04/22 11:08 12-Hexanone
ND 9.1020.0 ug/L 08/04/22 11:08 13,3-Dimethyl-1-butanol
ND 0.1600.500 ug/L 08/04/22 11:08 14-Chlorotoluene
ND 0.1800.500 ug/L 08/04/22 11:08 14-Isopropyltoluene
ND 5.2010.0 ug/L 08/04/22 11:08 14-Methyl-2-pentanone (MIBK)
ND 5.6020.0 ug/L 08/04/22 11:08 1Acetone
ND 0.1800.500 ug/L 08/04/22 11:08 1Benzene
ND 0.1400.500 ug/L 08/04/22 11:08 1Bromobenzene
ND 0.1800.500 ug/L 08/04/22 11:08 1Bromoform
ND 2.305.00 ug/L 08/04/22 11:08 1Bromomethane
ND 0.2200.500 ug/L 08/04/22 11:08 1Carbon tetrachloride
ND 0.1600.500 ug/L 08/04/22 11:08 1Chlorobenzene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-734030/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
RL MDL
Chlorobromomethane ND 0.500 0.130 ug/L 08/04/22 11:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.4601.00 ug/L 08/04/22 11:08 1Chlorodibromomethane
ND 4.1010.0 ug/L 08/04/22 11:08 1Chloroethane
ND 0.3800.500 ug/L 08/04/22 11:08 1Chloroform
ND 0.1000.500 ug/L 08/04/22 11:08 1Chloromethane
ND 0.06400.500 ug/L 08/04/22 11:08 1cis-1,2-Dichloroethene
ND 0.1100.500 ug/L 08/04/22 11:08 1cis-1,3-Dichloropropene
ND 0.1700.500 ug/L 08/04/22 11:08 1Dibromomethane
ND 0.4101.00 ug/L 08/04/22 11:08 1Dichlorobromomethane
ND 0.09100.500 ug/L 08/04/22 11:08 1Dichlorodifluoromethane
ND 0.1400.500 ug/L 08/04/22 11:08 1Dichlorofluoromethane
ND 140200 ug/L 08/04/22 11:08 1Ethanol
ND 0.09200.500 ug/L 08/04/22 11:08 1Ethyl ether
ND 0.1700.500 ug/L 08/04/22 11:08 1Ethylbenzene
ND 0.1700.500 ug/L 08/04/22 11:08 1Ethylene Dibromide
ND 0.05800.500 ug/L 08/04/22 11:08 1Isopropyl ether
ND 0.1800.500 ug/L 08/04/22 11:08 1Isopropylbenzene
ND 0.1100.500 ug/L 08/04/22 11:08 1Methyl tert-butyl ether
ND 0.1500.500 ug/L 08/04/22 11:08 1Methylene Chloride
ND 0.1800.500 ug/L 08/04/22 11:08 1m-Xylene & p-Xylene
ND 1.202.00 ug/L 08/04/22 11:08 1Naphthalene
ND 0.1601.00 ug/L 08/04/22 11:08 1n-Butylbenzene
ND 0.1800.500 ug/L 08/04/22 11:08 1N-Propylbenzene
ND 0.1500.500 ug/L 08/04/22 11:08 1o-Xylene
ND 0.1701.00 ug/L 08/04/22 11:08 1sec-Butylbenzene
ND 0.1700.500 ug/L 08/04/22 11:08 1Styrene
ND 1.905.00 ug/L 08/04/22 11:08 1t-Amyl alcohol
ND 0.07900.500 ug/L 08/04/22 11:08 1Tert-amyl methyl ether
ND 0.05800.500 ug/L 08/04/22 11:08 1Tert-butyl ethyl ether
ND 1.765.00 ug/L 08/04/22 11:08 1tert-Butyl Formate
ND 0.1800.500 ug/L 08/04/22 11:08 1tert-Butylbenzene
ND 0.2200.500 ug/L 08/04/22 11:08 1Tetrachloroethene
ND 0.2000.500 ug/L 08/04/22 11:08 1Toluene
ND 0.1700.500 ug/L 08/04/22 11:08 1trans-1,2-Dichloroethene
ND 0.1200.500 ug/L 08/04/22 11:08 1trans-1,3-Dichloropropene
ND 0.2000.500 ug/L 08/04/22 11:08 1Trichloroethene
ND 0.1400.500 ug/L 08/04/22 11:08 1Trichlorofluoromethane
ND 0.6401.00 ug/L 08/04/22 11:08 1Vinyl acetate
ND 0.1200.500 ug/L 08/04/22 11:08 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr)94 70-130 08/04/22 11:08 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
102 08/04/22 11:08 14-Bromofluorobenzene (Surr)70-130
98 08/04/22 11:08 1Dibromofluoromethane (Surr)70-130
106 08/04/22 11:08 1Toluene-d8 (Surr)70-130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-734030/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,1,1,2-Tetrachloroethane 25.0 26.89 ug/L 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 25.0 23.56 ug/L 94 70 -130
1,1,2,2-Tetrachloroethane 25.0 23.19 ug/L 93 70 -130
1,1,2-Trichloroethane 25.0 22.28 ug/L 89 70 -130
1,1-Dichloroethane 25.0 21.87 ug/L 87 70 -130
1,1-Dichloroethene 25.0 23.75 ug/L 95 70 -130
1,1-Dichloropropene 25.0 22.53 ug/L 90 70 -130
1,2,3-Trichlorobenzene 25.0 21.87 ug/L 87 70 -130
1,2,3-Trichloropropane 25.0 23.11 ug/L 92 70 -130
1,2,4-Trichlorobenzene 25.0 23.28 ug/L 93 70 -130
1,2,4-Trimethylbenzene 25.0 24.52 ug/L 98 70 -130
1,2-Dichlorobenzene 25.0 25.04 ug/L 100 70 -130
1,2-Dichloroethane 25.0 21.41 ug/L 86 70 -130
1,2-Dichloroethene, Total 50.0 45.18 ug/L 90 70 -130
1,2-Dichloropropane 25.0 21.89 ug/L 88 70 -130
1,3,5-Trimethylbenzene 25.0 24.59 ug/L 98 70 -130
1,3-Dichlorobenzene 25.0 25.44 ug/L 102 70 -130
1,3-Dichloropropane 25.0 22.12 ug/L 88 70 -130
1,3-Dichloropropene, Total 50.0 49.69 ug/L 99 70 -130
1,4-Dichlorobenzene 25.0 25.00 ug/L 100 70 -130
2,2-Dichloropropane 25.0 25.11 ug/L 100 70 -130
2-Butanone (MEK)125 98.91 ug/L 79 70 -130
2-Chlorotoluene 25.0 24.36 ug/L 97 70 -130
2-Hexanone 125 106.0 ug/L 85 70 -130
3,3-Dimethyl-1-butanol 100 91.11 ug/L 91 70 -130
4-Chlorotoluene 25.0 24.34 ug/L 97 70 -130
4-Isopropyltoluene 25.0 26.37 ug/L 105 70 -130
4-Methyl-2-pentanone (MIBK)125 107.1 ug/L 86 70 -130
Acetone 125 110.7 ug/L 89 70 -130
Benzene 25.0 22.29 ug/L 89 70 -130
Bromobenzene 25.0 25.13 ug/L 101 70 -130
Bromoform 25.0 28.52 ug/L 114 70 -130
Bromomethane 25.0 25.35 ug/L 101 70 -130
Carbon tetrachloride 25.0 24.25 ug/L 97 70 -130
Chlorobenzene 25.0 23.93 ug/L 96 70 -130
Chlorobromomethane 25.0 22.95 ug/L 92 70 -130
Chlorodibromomethane 25.0 25.58 ug/L 102 70 -130
Chloroethane 25.0 22.26 ug/L 89 70 -130
Chloroform 25.0 22.38 ug/L 90 70 -130
Chloromethane 25.0 21.95 ug/L 88 70 -130
cis-1,2-Dichloroethene 25.0 22.11 ug/L 88 70 -130
cis-1,3-Dichloropropene 25.0 24.81 ug/L 99 70 -130
Dibromomethane 25.0 22.72 ug/L 91 70 -130
Dichlorobromomethane 25.0 24.28 ug/L 97 70 -130
Dichlorodifluoromethane 25.0 21.58 ug/L 86 70 -130
Dichlorofluoromethane 25.0 23.65 ug/L 95 70 -130
Ethanol 1000 869.2 ug/L 87 70 -130
Ethyl ether 25.0 21.71 ug/L 87 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-734030/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
Ethylbenzene 25.0 24.98 ug/L 100 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Ethylene Dibromide 25.0 23.14 ug/L 93 70 -130
Isopropyl ether 25.0 21.80 ug/L 87 70 -130
Isopropylbenzene 25.0 25.68 ug/L 103 70 -130
Methyl tert-butyl ether 25.0 22.01 ug/L 88 70 -130
Methylene Chloride 25.0 23.50 ug/L 94 70 -130
m-Xylene & p-Xylene 25.0 24.88 ug/L 100 70 -130
Naphthalene 25.0 23.26 ug/L 93 70 -130
n-Butylbenzene 25.0 25.51 ug/L 102 70 -130
N-Propylbenzene 25.0 24.83 ug/L 99 70 -130
o-Xylene 25.0 25.07 ug/L 100 70 -130
sec-Butylbenzene 25.0 25.47 ug/L 102 70 -130
Styrene 25.0 25.71 ug/L 103 70 -130
t-Amyl alcohol 250 209.7 ug/L 84 70 -130
Tert-amyl methyl ether 25.0 22.75 ug/L 91 70 -130
Tert-butyl ethyl ether 25.0 22.63 ug/L 91 70 -130
tert-Butyl Formate 100 101.6 ug/L 102 70 -130
tert-Butylbenzene 25.0 25.30 ug/L 101 70 -130
Tetrachloroethene 25.0 23.70 ug/L 95 70 -130
Toluene 25.0 22.70 ug/L 91 70 -130
trans-1,2-Dichloroethene 25.0 23.07 ug/L 92 70 -130
trans-1,3-Dichloropropene 25.0 24.88 ug/L 100 70 -130
Trichloroethene 25.0 23.48 ug/L 94 70 -130
Trichlorofluoromethane 25.0 25.18 ug/L 101 70 -130
Vinyl acetate 50.0 49.11 ug/L 98 70 -130
Vinyl chloride 25.0 22.01 ug/L 88 70 -130
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)70 -130
97Dibromofluoromethane (Surr)70 -130
105Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,1,1,2-Tetrachloroethane 25.0 26.26 ug/L 105 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 25.0 22.96 ug/L 92 70 -130 3 30
1,1,2,2-Tetrachloroethane 25.0 23.63 ug/L 95 70 -130 2 30
1,1,2-Trichloroethane 25.0 22.43 ug/L 90 70 -130 1 30
1,1-Dichloroethane 25.0 21.45 ug/L 86 70 -130 2 30
1,1-Dichloroethene 25.0 22.96 ug/L 92 70 -130 3 30
1,1-Dichloropropene 25.0 21.83 ug/L 87 70 -130 3 30
1,2,3-Trichlorobenzene 25.0 21.83 ug/L 87 70 -130 0 30
1,2,3-Trichloropropane 25.0 23.72 ug/L 95 70 -130 3 30
1,2,4-Trichlorobenzene 25.0 23.02 ug/L 92 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,2,4-Trimethylbenzene 25.0 23.73 ug/L 95 70 -130 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichlorobenzene 25.0 24.26 ug/L 97 70 -130 3 30
1,2-Dichloroethane 25.0 21.46 ug/L 86 70 -130 0 30
1,2-Dichloroethene, Total 50.0 44.03 ug/L 88 70 -130 3 30
1,2-Dichloropropane 25.0 21.63 ug/L 87 70 -130 1 30
1,3,5-Trimethylbenzene 25.0 23.94 ug/L 96 70 -130 3 50
1,3-Dichlorobenzene 25.0 24.72 ug/L 99 70 -130 3 30
1,3-Dichloropropane 25.0 22.17 ug/L 89 70 -130 0 30
1,3-Dichloropropene, Total 50.0 49.28 ug/L 99 70 -130 1 50
1,4-Dichlorobenzene 25.0 24.25 ug/L 97 70 -130 3 30
2,2-Dichloropropane 25.0 23.95 ug/L 96 70 -130 5 30
2-Butanone (MEK)125 102.6 ug/L 82 70 -130 4 30
2-Chlorotoluene 25.0 23.75 ug/L 95 70 -130 3 30
2-Hexanone 125 110.5 ug/L 88 70 -130 4 30
3,3-Dimethyl-1-butanol 100 94.43 ug/L 94 70 -130 4
4-Chlorotoluene 25.0 23.51 ug/L 94 70 -130 3 30
4-Isopropyltoluene 25.0 25.37 ug/L 101 70 -130 4 50
4-Methyl-2-pentanone (MIBK)125 110.3 ug/L 88 70 -130 3 30
Acetone 125 111.6 ug/L 89 70 -130 1 50
Benzene 25.0 21.68 ug/L 87 70 -130 3 30
Bromobenzene 25.0 24.63 ug/L 99 70 -130 2 30
Bromoform 25.0 29.30 ug/L 117 70 -130 3 30
Bromomethane 25.0 24.05 ug/L 96 70 -130 5 50
Carbon tetrachloride 25.0 23.38 ug/L 94 70 -130 4 30
Chlorobenzene 25.0 23.53 ug/L 94 70 -130 2 30
Chlorobromomethane 25.0 22.94 ug/L 92 70 -130 0 30
Chlorodibromomethane 25.0 25.46 ug/L 102 70 -130 0 50
Chloroethane 25.0 20.96 ug/L 84 70 -130 6 40
Chloroform 25.0 22.01 ug/L 88 70 -130 2 30
Chloromethane 25.0 21.25 ug/L 85 70 -130 3 30
cis-1,2-Dichloroethene 25.0 21.73 ug/L 87 70 -130 2 30
cis-1,3-Dichloropropene 25.0 24.45 ug/L 98 70 -130 1 30
Dibromomethane 25.0 22.73 ug/L 91 70 -130 0 30
Dichlorobromomethane 25.0 24.06 ug/L 96 70 -130 1 30
Dichlorodifluoromethane 25.0 20.51 ug/L 82 70 -130 5 50
Dichlorofluoromethane 25.0 22.31 ug/L 89 70 -130 6 50
Ethanol 1000 873.2 ug/L 87 70 -130 0 50
Ethyl ether 25.0 21.49 ug/L 86 70 -130 1 50
Ethylbenzene 25.0 24.22 ug/L 97 70 -130 3 30
Ethylene Dibromide 25.0 23.33 ug/L 93 70 -130 1 30
Isopropyl ether 25.0 21.66 ug/L 87 70 -130 1 50
Isopropylbenzene 25.0 25.06 ug/L 100 70 -130 2 30
Methyl tert-butyl ether 25.0 22.24 ug/L 89 70 -130 1 30
Methylene Chloride 25.0 23.01 ug/L 92 70 -130 2 30
m-Xylene & p-Xylene 25.0 24.31 ug/L 97 70 -130 2 30
Naphthalene 25.0 23.50 ug/L 94 70 -130 1 30
n-Butylbenzene 25.0 24.51 ug/L 98 70 -130 4 30
N-Propylbenzene 25.0 24.09 ug/L 96 70 -130 3 30
o-Xylene 25.0 24.46 ug/L 98 70 -130 2 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
sec-Butylbenzene 25.0 24.55 ug/L 98 70 -130 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Styrene 25.0 25.21 ug/L 101 70 -130 2 30
t-Amyl alcohol 250 218.7 ug/L 87 70 -130 4 30
Tert-amyl methyl ether 25.0 22.92 ug/L 92 70 -130 1 30
Tert-butyl ethyl ether 25.0 22.66 ug/L 91 70 -130 0 30
tert-Butyl Formate 100 102.4 ug/L 102 70 -130 1
tert-Butylbenzene 25.0 24.64 ug/L 99 70 -130 3 30
Tetrachloroethene 25.0 23.12 ug/L 92 70 -130 2 30
Toluene 25.0 22.27 ug/L 89 70 -130 2 30
trans-1,2-Dichloroethene 25.0 22.31 ug/L 89 70 -130 3 30
trans-1,3-Dichloropropene 25.0 24.83 ug/L 99 70 -130 0 50
Trichloroethene 25.0 22.67 ug/L 91 70 -130 4 30
Trichlorofluoromethane 25.0 24.06 ug/L 96 70 -130 5 30
Vinyl acetate 50.0 48.64 ug/L 97 70 -130 1 30
Vinyl chloride 25.0 21.20 ug/L 85 70 -130 4 30
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)70 -130
97Dibromofluoromethane (Surr)70 -130
104Toluene-d8 (Surr)70 -130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-733048/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 07/28/22 15:12 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 72 70-131 07/28/22 15:12 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733048/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
Gasoline Range Organics [C6 -
C10]
40.0 40.19 mg/Kg 100 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8015D - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733048/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
Gasoline Range Organics [C6 -
C10]
40.0 38.07 mg/Kg 95 64 -133 5 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-733231/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 07/29/22 14:51 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/29/22 14:51 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733231/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
Gasoline Range Organics [C6 -
C10]
50.0 54.75 mg/Kg 110 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733231/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
Gasoline Range Organics [C6 -
C10]
50.0 50.23 mg/Kg 100 64 -133 9 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-733517/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 08/01/22 12:51 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 81 70-131 08/01/22 12:51 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8015D - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733517/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
Gasoline Range Organics [C6 -
C10]
50.0 47.58 mg/Kg 95 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733517/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
Gasoline Range Organics [C6 -
C10]
50.0 49.29 mg/Kg 99 64 -133 4 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
106
LCSD LCSD
Qualifier Limits%Recovery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-587039/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
RL MDL
C5-C8 Aliphatics ND 26.0 26.0 ug/L 08/01/22 17:42 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 7.007.00 ug/L 08/01/22 17:42 1C9-C10 Aromatics
ND 11.011.0 ug/L 08/01/22 17:42 1C9-C12 Aliphatics
a,a,a-Trifluorotoluene (fid)94 70-130 08/01/22 17:42 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 08/01/22 17:42 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-587039/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 300 309.8 ug/L 103 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.0 53.47 ug/L 107 70 -130
C9-C12 Aliphatics 350 349.0 ug/L 100 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
94a,a,a-Trifluorotoluene (pid)70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-587039/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 300 298.8 ug/L 100 70 -130 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.0 50.83 ug/L 102 70 -130 5 25
C9-C12 Aliphatics 350 327.2 ug/L 93 70 -130 6 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
94a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-3Lab Sample ID: 680-218771-16 MS
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 348 1500 1828 ug/L 99 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C9-C10 Aromatics 533 F1 250 742.9 ug/L 84 70 -130
C9-C12 Aliphatics 404 1750 2120 ug/L 98 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
MS MS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-3Lab Sample ID: 680-218771-16 MSD
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 348 1500 1770 ug/L 95 70 -130 3 25
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 533 F1 250 701.4 F1 ug/L 67 70 -130 6 25
C9-C12 Aliphatics 404 1750 1903 ug/L 86 70 -130 11 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-732468/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
RL MDL
1,2-Dibromoethane (EDB)ND 0.0180 0.00500 ug/L 07/25/22 11:15 07/25/22 16:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Pentachloroethane 111 70-130 07/25/22 16:49 1
MB MB
Surrogate
07/25/22 11:15
Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732468/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
1,2-Dibromoethane (EDB)0.100 0.08743 ug/L 87 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Pentachloroethane 70 -130
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732468/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
1,2-Dibromoethane (EDB)0.100 0.08092 ug/L 81 70 -130 8 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pentachloroethane 70 -130
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 680-732357/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 732619 Prep Batch: 732357
RL MDL
Lead, Total ND 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732357/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 732619 Prep Batch: 732357
Lead, Total 505 443.4 ug/L 88 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC/MS VOA
Analysis Batch: 732600
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-2 MW-1-20 Total/NA
Soil 8260D 732626680-218771-4 MW-3-10 Total/NA
Soil 8260D 732626680-218771-5 MW-3-20 Total/NA
Soil 8260D 732626680-218771-6 MW-3-25 Total/NA
Soil 8260D 732626680-218771-7 MW-3-30 Total/NA
Soil 8260D 732626680-218771-8 MW-2-10 Total/NA
Soil 8260D 732626680-218771-9 MW-2-20 Total/NA
Soil 8260D 732626680-218771-11 MW-2-30 Total/NA
Soil 8260D 732626680-218771-13 P-1-20 Total/NA
Soil 8260D 732626680-218771-14 P-1-25 Total/NA
Soil 8260D 732626680-218771-15 P-1-30 Total/NA
Solid 8260DMB 680-732600/8 Method Blank Total/NA
Solid 8260DLCS 680-732600/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732600/5 Lab Control Sample Dup Total/NA
Prep Batch: 732626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-218771-1 MW-1-10 Total/NA
Soil 5035A680-218771-2 - DL2 MW-1-20 Total/NA
Soil 5035A680-218771-2 - DL MW-1-20 Total/NA
Soil 5035A680-218771-2 MW-1-20 Total/NA
Soil 5035A680-218771-3 MW-1-30 Total/NA
Soil 5035A680-218771-3 - DL MW-1-30 Total/NA
Soil 5035A680-218771-4 MW-3-10 Total/NA
Soil 5035A680-218771-4 - DL MW-3-10 Total/NA
Soil 5035A680-218771-5 MW-3-20 Total/NA
Soil 5035A680-218771-5 - DL MW-3-20 Total/NA
Soil 5035A680-218771-6 MW-3-25 Total/NA
Soil 5035A680-218771-7 MW-3-30 Total/NA
Soil 5035A680-218771-8 MW-2-10 Total/NA
Soil 5035A680-218771-9 - DL MW-2-20 Total/NA
Soil 5035A680-218771-9 MW-2-20 Total/NA
Soil 5035A680-218771-10 MW-2-25 Total/NA
Soil 5035A680-218771-11 MW-2-30 Total/NA
Soil 5035A680-218771-12 P-1-10 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-15 P-1-30 Total/NA
Soil 5035A680-218771-15 - DL P-1-30 Total/NA
Analysis Batch: 732793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-1 MW-1-10 Total/NA
Soil 8260D 732626680-218771-2 - DL MW-1-20 Total/NA
Soil 8260D 732626680-218771-3 MW-1-30 Total/NA
Soil 8260D 732626680-218771-4 - DL MW-3-10 Total/NA
Soil 8260D 732626680-218771-5 - DL MW-3-20 Total/NA
Soil 8260D 732626680-218771-10 MW-2-25 Total/NA
Soil 8260D 732626680-218771-12 P-1-10 Total/NA
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC/MS VOA (Continued)
Analysis Batch: 732793 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-15 - DL P-1-30 Total/NA
Solid 8260DMB 680-732793/8 Method Blank Total/NA
Solid 8260DLCS 680-732793/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732793/5 Lab Control Sample Dup Total/NA
Analysis Batch: 732966
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-3 - DL MW-1-30 Total/NA
Solid 8260DMB 680-732966/8 Method Blank Total/NA
Solid 8260DLCS 680-732966/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732966/5 Lab Control Sample Dup Total/NA
Analysis Batch: 733530
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-2 - DL2 MW-1-20 Total/NA
Soil 8260D 732626680-218771-9 - DL MW-2-20 Total/NA
Soil 8260D 732626680-218771-13 P-1-20 Total/NA
Soil 8260D 732626680-218771-14 P-1-25 Total/NA
Solid 8260DMB 680-733530/8 Method Blank Total/NA
Solid 8260DLCS 680-733530/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-733530/5 Lab Control Sample Dup Total/NA
Analysis Batch: 733831
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water SM6200-B680-218771-16 MW-3 Total/NA
Water SM6200-BMB 680-733831/19 Method Blank Total/NA
Water SM6200-BLCS 680-733831/1015 Lab Control Sample Total/NA
Water SM6200-BLCSD 680-733831/16 Lab Control Sample Dup Total/NA
Analysis Batch: 734030
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water SM6200-B680-218771-16 - DL MW-3 Total/NA
Ground Water SM6200-B680-218771-17 MW-2 Total/NA
Water SM6200-BMB 680-734030/7 Method Blank Total/NA
Water SM6200-BLCS 680-734030/3 Lab Control Sample Total/NA
Water SM6200-BLCSD 680-734030/4 Lab Control Sample Dup Total/NA
GC VOA
Analysis Batch: 587039
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MAVPH680-218771-16 MW-3 Total/NA
Ground Water MAVPH680-218771-17 MW-2 Total/NA
Water MAVPHMB 400-587039/2 Method Blank Total/NA
Water MAVPHLCS 400-587039/3 Lab Control Sample Total/NA
Water MAVPHLCSD 400-587039/4 Lab Control Sample Dup Total/NA
Ground Water MAVPH680-218771-16 MS MW-3 Total/NA
Ground Water MAVPH680-218771-16 MSD MW-3 Total/NA
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC VOA
Prep Batch: 732626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-218771-1 MW-1-10 Total/NA
Soil 5035A680-218771-2 MW-1-20 Total/NA
Soil 5035A680-218771-3 MW-1-30 Total/NA
Soil 5035A680-218771-4 MW-3-10 Total/NA
Soil 5035A680-218771-5 MW-3-20 Total/NA
Soil 5035A680-218771-6 MW-3-25 Total/NA
Soil 5035A680-218771-7 MW-3-30 Total/NA
Soil 5035A680-218771-8 MW-2-10 Total/NA
Soil 5035A680-218771-9 MW-2-20 Total/NA
Soil 5035A680-218771-10 MW-2-25 Total/NA
Soil 5035A680-218771-11 MW-2-30 Total/NA
Soil 5035A680-218771-12 P-1-10 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-15 P-1-30 Total/NA
Analysis Batch: 733048
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-1 MW-1-10 Total/NA
Soil 8015D 732626680-218771-7 MW-3-30 Total/NA
Soil 8015D 732626680-218771-8 MW-2-10 Total/NA
Soil 8015D 732626680-218771-9 MW-2-20 Total/NA
Soil 8015D 732626680-218771-10 MW-2-25 Total/NA
Soil 8015D 732626680-218771-11 MW-2-30 Total/NA
Soil 8015D 732626680-218771-12 P-1-10 Total/NA
Soil 8015D 732626680-218771-13 P-1-20 Total/NA
Soil 8015D 732626680-218771-14 P-1-25 Total/NA
Solid 8015DMB 680-733048/7 Method Blank Total/NA
Solid 8015DLCS 680-733048/5 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733048/6 Lab Control Sample Dup Total/NA
Analysis Batch: 733231
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-2 MW-1-20 Total/NA
Soil 8015D 732626680-218771-5 MW-3-20 Total/NA
Soil 8015D 732626680-218771-6 MW-3-25 Total/NA
Soil 8015D 732626680-218771-15 P-1-30 Total/NA
Solid 8015DMB 680-733231/7 Method Blank Total/NA
Solid 8015DLCS 680-733231/9 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733231/10 Lab Control Sample Dup Total/NA
Analysis Batch: 733517
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-3 MW-1-30 Total/NA
Soil 8015D 732626680-218771-4 MW-3-10 Total/NA
Solid 8015DMB 680-733517/7 Method Blank Total/NA
Solid 8015DLCS 680-733517/5 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733517/6 Lab Control Sample Dup Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC Semi VOA
Prep Batch: 732468
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1680-218771-16 MW-3 Total/NA
Ground Water 504.1680-218771-17 MW-2 Total/NA
Water 504.1MB 680-732468/3-A Method Blank Total/NA
Water 504.1LCS 680-732468/4-A Lab Control Sample Total/NA
Water 504.1LCSD 680-732468/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 732532
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1 732468680-218771-16 MW-3 Total/NA
Ground Water 504.1 732468680-218771-17 MW-2 Total/NA
Water 504.1 732468MB 680-732468/3-A Method Blank Total/NA
Water 504.1 732468LCS 680-732468/4-A Lab Control Sample Total/NA
Water 504.1 732468LCSD 680-732468/5-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 732357
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 3005A680-218771-16 MW-3 Total Recoverable
Ground Water 3005A680-218771-17 MW-2 Total Recoverable
Water 3005AMB 680-732357/1-A Method Blank Total Recoverable
Water 3005ALCS 680-732357/2-A Lab Control Sample Total Recoverable
Analysis Batch: 732619
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 6010D 732357680-218771-16 MW-3 Total Recoverable
Ground Water 6010D 732357680-218771-17 MW-2 Total Recoverable
Water 6010D 732357MB 680-732357/1-A Method Blank Total Recoverable
Water 6010D 732357LCS 680-732357/2-A Lab Control Sample Total Recoverable
General Chemistry
Analysis Batch: 733216
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture680-218771-1 MW-1-10 Total/NA
Soil Moisture680-218771-2 MW-1-20 Total/NA
Soil Moisture680-218771-3 MW-1-30 Total/NA
Soil Moisture680-218771-4 MW-3-10 Total/NA
Soil Moisture680-218771-5 MW-3-20 Total/NA
Soil Moisture680-218771-6 MW-3-25 Total/NA
Soil Moisture680-218771-7 MW-3-30 Total/NA
Soil Moisture680-218771-8 MW-2-10 Total/NA
Soil Moisture680-218771-9 MW-2-20 Total/NA
Soil Moisture680-218771-10 MW-2-25 Total/NA
Soil Moisture680-218771-11 MW-2-30 Total/NA
Soil Moisture680-218771-12 P-1-10 Total/NA
Soil Moisture680-218771-13 P-1-20 Total/NA
Soil Moisture680-218771-14 P-1-25 Total/NA
Soil Moisture680-218771-15 P-1-30 Total/NA
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-1-10 Lab Sample ID: 680-218771-1
Matrix: SoilDate Collected: 07/18/22 10:45
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-10 Lab Sample ID: 680-218771-1
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.014 g 5 mL
Analysis 8260D 40 732793 07/27/22 18:29 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.071 g 5 mL
Analysis 8015D 100 733048 07/28/22 15:36 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-1-20 Lab Sample ID: 680-218771-2
Matrix: SoilDate Collected: 07/18/22 10:50
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-20 Lab Sample ID: 680-218771-2
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32DL2 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.928 g 5 mL
Analysis 8260D DL2 5000 733530 08/01/22 17:33 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.928 g 5 mL
Analysis 8260D 40 732600 07/26/22 20:13 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.928 g 5 mL
Analysis 8260D DL 1000 732793 07/27/22 16:28 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.68 g 5 mL
Analysis 8015D 1000 733231 07/29/22 19:45 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-1-30 Lab Sample ID: 680-218771-3
Matrix: SoilDate Collected: 07/18/22 10:55
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-30 Lab Sample ID: 680-218771-3
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.519 g 5 mL
Analysis 8260D 1000 732793 07/27/22 16:52 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 6.519 g 5 mL
Analysis 8260D DL 5000 732966 07/28/22 21:33 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 6.401 g 5 mL
Analysis 8015D 20000 733517 08/01/22 16:14 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-10 Lab Sample ID: 680-218771-4
Matrix: SoilDate Collected: 07/18/22 11:35
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-10 Lab Sample ID: 680-218771-4
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.739 g 5 mL
Analysis 8260D 1 732600 07/26/22 15:23 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.917 g 5 mL
Analysis 8260D DL 40 732793 07/27/22 18:53 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.892 g 5 mL
Analysis 8015D 100 733517 08/01/22 14:25 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3-20 Lab Sample ID: 680-218771-5
Matrix: SoilDate Collected: 07/18/22 11:45
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-20 Lab Sample ID: 680-218771-5
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.64 g 5 mL
Analysis 8260D 1 732600 07/26/22 15:47 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.69 g 5 mL
Analysis 8260D DL 40 732793 07/27/22 19:17 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.128 g 5 mL
Analysis 8015D 100 733231 07/29/22 17:57 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-25 Lab Sample ID: 680-218771-6
Matrix: SoilDate Collected: 07/19/22 16:10
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-25 Lab Sample ID: 680-218771-6
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.396 g 5 mL
Analysis 8260D 1 732600 07/26/22 16:11 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.125 g 5 mL
Analysis 8015D 100 733231 07/29/22 18:19 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-30 Lab Sample ID: 680-218771-7
Matrix: SoilDate Collected: 07/19/22 16:15
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3-30 Lab Sample ID: 680-218771-7
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.699 g 5 mL
Analysis 8260D 1 732600 07/26/22 16:35 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.018 g 5 mL
Analysis 8015D 100 733048 07/28/22 17:46 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-10 Lab Sample ID: 680-218771-8
Matrix: SoilDate Collected: 07/19/22 16:20
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-10 Lab Sample ID: 680-218771-8
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.875 g 5 mL
Analysis 8260D 1 732600 07/26/22 17:00 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.997 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:08 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32DL TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.661 g 5 mL
Analysis 8260D DL 40 733530 08/01/22 17:55 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.05 g 5 mL
Analysis 8260D 1 732600 07/26/22 17:24 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.156 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:30 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-25 Lab Sample ID: 680-218771-10
Matrix: SoilDate Collected: 07/19/22 16:30
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-25 Lab Sample ID: 680-218771-10
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.323 g 5 mL
Analysis 8260D 1 732793 07/27/22 13:16 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.149 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:51 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-30 Lab Sample ID: 680-218771-11
Matrix: SoilDate Collected: 07/19/22 16:35
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-30 Lab Sample ID: 680-218771-11
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.948 g 5 mL
Analysis 8260D 1 732600 07/26/22 18:12 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.008 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:13 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: P-1-10 Lab Sample ID: 680-218771-12
Matrix: SoilDate Collected: 07/19/22 16:44
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-10 Lab Sample ID: 680-218771-12
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.87 g 5 mL
Analysis 8260D 1 732793 07/27/22 13:40 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.217 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:35 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-20 Lab Sample ID: 680-218771-13
Matrix: SoilDate Collected: 07/19/22 16:48
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-20 Lab Sample ID: 680-218771-13
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.014 g 5 mL
Analysis 8260D 1 733530 08/01/22 16:26 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.941 g 5 mL
Analysis 8260D 1 732600 07/26/22 19:00 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.868 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:57 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-25 Lab Sample ID: 680-218771-14
Matrix: SoilDate Collected: 07/19/22 16:50
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: P-1-25 Lab Sample ID: 680-218771-14
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.955 g 5 mL
Analysis 8260D 1 733530 08/01/22 16:47 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.141 g 5 mL
Analysis 8260D 1 732600 07/26/22 19:25 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.071 g 5 mL
Analysis 8015D 100 733048 07/28/22 20:18 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-30 Lab Sample ID: 680-218771-15
Matrix: SoilDate Collected: 07/19/22 16:55
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-30 Lab Sample ID: 680-218771-15
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.679 g 5 mL
Analysis 8260D 40 732600 07/26/22 21:02 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.679 g 5 mL
Analysis 8260D DL 500 732793 07/27/22 17:16 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.884 g 5 mL
Analysis 8015D 1000 733231 07/29/22 21:12 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3 Lab Sample ID: 680-218771-16
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Analysis SM6200-B SMP08/03/22 18:061 TAL SAV733831
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSO2
Analysis SM6200-B DL 5 734030 08/04/22 13:42 SMP TAL SAVTotal/NA 5 mL 5 mL
CMSO2Instrument ID:
Analysis MAVPH 5 587039 08/02/22 10:10 SAB EETSE PENTotal/NA 5 mL 5 mL
CH_CAROLInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3 Lab Sample ID: 680-218771-16
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Prep 504.1 IB07/25/22 11:15 TAL SAV732468
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 34.8 mL 2 mL
Analysis 504.1 1 732532 07/25/22 18:58 JCK TAL SAVTotal/NA
CSGXInstrument ID:
Prep 3005A 732357 07/25/22 06:08 RR TAL SAVTotal Recoverable 50 mL 50 mL
Analysis 6010D 1 732619 07/25/22 20:30 BCB TAL SAVTotal Recoverable
ICPHInstrument ID:
Client Sample ID: MW-2 Lab Sample ID: 680-218771-17
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Analysis SM6200-B SMP08/04/22 13:16500 TAL SAV734030
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSO2
Analysis MAVPH 100 587039 08/02/22 15:32 SAB EETSE PENTotal/NA 5 mL 5 mL
CH_CAROLInstrument ID:
Prep 504.1 732468 07/25/22 11:15 IB TAL SAVTotal/NA 34.3 mL 2 mL
Analysis 504.1 1 732532 07/25/22 19:07 JCK TAL SAVTotal/NA
CSGXInstrument ID:
Prep 3005A 732357 07/25/22 06:08 RR TAL SAVTotal Recoverable 50 mL 50 mL
Analysis 6010D 1 732619 07/25/22 20:33 BCB TAL SAVTotal Recoverable
ICPHInstrument ID:
Laboratory References:
EETSE PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Alabama State 40150 06-30-23
ANAB ISO/IEC 17025 L2471 02-23-23
Arkansas DEQ State 88-0689 09-01-22
California State 2510 06-30-23
Florida NELAP E81010 06-30-23
Georgia State E81010(FL)06-30-23
Illinois NELAP 200041 10-09-22
Kansas NELAP E-10253 10-31-22
Kentucky (UST)State 53 06-30-23
Kentucky (WW)State KY98030 12-31-22
Louisiana (All)NELAP 30976 06-30-23
Louisiana (DW)State LA017 12-31-22
Maryland State 233 09-30-22
Michigan State 9912 06-30-23
North Carolina (WW/SW)State 314 12-31-22
Oklahoma NELAP 9810 08-31-22
Pennsylvania NELAP 68-00467 01-31-23
South Carolina State 96026 06-30-23
Tennessee State TN02907 06-30-23
Texas NELAP T104704286 09-30-22
US Fish & Wildlife US Federal Programs A22340 06-30-23
USDA US Federal Programs P330-21-00056 05-17-24
Virginia NELAP 460166 06-14-23
West Virginia DEP State 136 03-31-23
Eurofins Savannah
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Method Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL SAV
SMSM6200-B Volatile Organic Compounds TAL SAV
SW8468015DGasoline Range Organics (GRO) (GC)TAL SAV
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EETSE PEN
EPA-DW504.1 EDB, DBCP and 1,2,3-TCP (GC)TAL SAV
SW8466010DMetals (ICP)TAL SAV
EPAMoisturePercent Moisture TAL SAV
SW8463005APreparation, Total Recoverable or Dissolved Metals TAL SAV
SW8465030BPurge and Trap EETSE PEN
SW8465035AClosed System Purge & Trap TAL SAV
SW8465035AClosed System Purge & Trap/Field Methanol TAL SAV
EPA-DW504.1 Microextraction TAL SAV
SMSM6200-B Purge and Trap TAL SAV
Protocol References:
EPA = US Environmental Protection Agency
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
MA DEP = Massachusetts Department Of Environmental Protection
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EETSE PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-218771-1
Login Number: 218771
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
FalseCooler Temperature is acceptable.Cooler temperature outside required temperature
criteria.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-218771-1
Login Number: 218771
Question Answer Comment
Creator: Roberts, Alexis J
List Source: Eurofins Pensacola
List Creation: 07/27/22 02:36 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.7°C IR8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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ANALYTICAL REPORT
PREPARED FOR
Attn: Wayne Watterson
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, North Carolina 27409
Generated 12/14/2022 7:19:51 PM
JOB DESCRIPTION
D&M Market
JOB NUMBER
680-226646-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
12/14/2022 7:19:51 PM
Authorized for release by
Chad Bechtold, Project Manager
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Sample Summary
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Lab Sample ID Client Sample ID Matrix Collected Received
680-226646-1 P3-10 Solid 11/28/22 11:00 12/01/22 06:30
680-226646-2 P3-25 Solid 11/28/22 11:10 12/01/22 06:30
680-226646-3 P2-25 Solid 11/28/22 11:35 12/01/22 06:30
680-226646-4 P4-15 Solid 11/28/22 12:03 12/01/22 06:30
680-226646-5 P4-25 Solid 11/28/22 12:05 12/01/22 06:30
680-226646-6 P5-10 Solid 11/28/22 12:20 12/01/22 06:30
680-226646-7 P5-20 Solid 11/28/22 12:25 12/01/22 06:30
680-226646-8 P6-20 Solid 11/28/22 13:52 12/01/22 06:30
680-226646-9 P7-25 Solid 11/28/22 14:20 12/01/22 06:30
680-226646-10 P11-25 Solid 11/28/22 14:40 12/01/22 06:30
680-226646-11 P9-16 Solid 11/28/22 15:20 12/01/22 06:30
680-226646-12 P10-25 Solid 11/28/22 15:30 12/01/22 06:30
680-226646-13 P8-20 Solid 11/28/22 16:05 12/01/22 06:30
680-226646-14 P12-20 Solid 11/28/22 16:20 12/01/22 06:30
680-226646-15 P13-10 Solid 11/28/22 16:36 12/01/22 06:30
680-226646-16 P14-5 Solid 11/29/22 08:25 12/01/22 06:30
680-226646-17 P15-10 Solid 11/29/22 08:38 12/01/22 06:30
680-226646-18 P17-5 Solid 11/29/22 08:56 12/01/22 06:30
680-226646-19 P18-10 Solid 11/29/22 09:13 12/01/22 06:30
680-226646-20 P16-15 Solid 11/29/22 09:29 12/01/22 06:30
Eurofins SavannahPage 4 of 137 12/14/2022
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Case Narrative
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Job ID: 680-226646-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-226646-1
Comments
Per client request the sample listed as P14-15 on the Chain of Custody was changed to P14-5. Also, per client request the sample listed
as P9-20 was changed to P9-16.
Receipt
The samples were received on 12/1/2022 6:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 0.4º C, 1.2º C and 1.8º C.
GC/MS VOA
Method 8260D: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 680-753988
recovered outside control limits for the following analytes: Carbon disulfide. This analyte was biased high in the LCS and was not
detected in the associated samples; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-753988 recovered above the upper control limit for
Ethyl acetate. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-754199 recovered above the upper control limit for
Ethyl acetate. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 680-754199 was outside the method criteria for the
following analyte(s): Carbon disulfide, Tetrachloroethene and Vinyl acetate. A CCV standard at or below the reporting limit (RL) was
analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-754381 recovered above the upper control limit for
Ethyl acetate. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-754381 recovered above the upper control limit for
1,1,2-Trichloro-1,2,2-trifluoroethane, Carbon disulfide and Tetrachloroethene. The samples associated with this CCV were non-detects
for the affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-754381 recovered outside acceptance criteria, low
biased, for Vinyl acetate. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the associated
samples were non-detect for the analyte(s), the data are reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270E: The The continuing calibration verification (CCV) analyzed in batch 680-754041 was outside the method criteria for the
following surrogate: 2,4,6-Tribromophenol (Surr). The affected surrogate was however within surrogate control limits in the CCV. All
associated batch QC and samples were also within control limits for this surrogate.
Method 8270E: The minimum response factor (RF) criteria for the continuing calibration verification (CCV) analyzed in batch 680-754041
was outside criteria for the following analyte: Bis(2-chloroethyl)ether. A CCV standard at or below the reporting limit (RL) was analyzed
with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any
detection or non-detection for the affected analyte is considered estimated.
Method 8270E: The continuing calibration verification (CCV) analyzed in batch 680-754041 was outside the method criteria for the
following analytes: bis (2-chloroisopropyl) ether and Indeno[1,2,3-cd]pyrene. A CCV standard at or below the reporting limit (RL) was
analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analytes is considered estimated.
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Case Narrative
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Job ID: 680-226646-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
Method 8270E: The following analyte have been identified, in the reference method and/or via historical data, to be poor and/or erratic
performers: 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol, Benzaldehyde and Pentachlorophenol. This analyte may have a %D >20% but
must be <50%. If >50%, a CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analytes is
considered estimated.
Method 8270E: The continuing calibration verification (CCV) analyzed in batch 680-754071 was outside the method criteria for the
following surrogate: 2,4,6-Tribromophenol (Surr). The affected surrogate was however within surrogate control limits in the CCV. All
associated batch QC and samples were also within control limits for this surrogate.
Method 8270E: The continuing calibration verification (CCV) associated with batch 680-754071 recovered above the upper control limit for
2,4-Dinitrophenol, 2,4-Dinitrotoluene, 2-Nitrophenol, 3,3'-Dichlorobenzidine, 4,6-Dinitro-2-methylphenol, Bis(2-ethylhexyl) phthalate, Butyl
benzyl phthalate, Di-n-octyl phthalate and Indeno[1,2,3-cd]pyrene. The samples associated with this CCV were non-detects for the
affected analytes; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
Method 8015C: The following samples were diluted because the base dilution for methanol preserved soil analysis is 1:50: P9-16
(680-226646-11), P10-25 (680-226646-12), P8-20 (680-226646-13), P12-20 (680-226646-14), P13-10 (680-226646-15), P14-5
(680-226646-16), P15-10 (680-226646-17), P17-5 (680-226646-18), P18-10 (680-226646-19) and P16-15 (680-226646-20).
Method 8015C: The following samples were diluted because the base dilution for methanol preserved soil analysis is 1:50: P3-10
(680-226646-1), P3-25 (680-226646-2), P2-25 (680-226646-3), P4-15 (680-226646-4), P4-25 (680-226646-5), P5-10 (680-226646-6),
P5-20 (680-226646-7), P6-20 (680-226646-8), P7-25 (680-226646-9) and P11-25 (680-226646-10).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-1Client Sample ID: P3-10
Matrix: SolidDate Collected: 11/28/22 11:00
Percent Solids: 86.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00559 0.00145 mg/Kg ☼12/02/22 12:10 12/08/22 13:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1,1-Trichloroethane
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1,2,2-Tetrachloroethane
0.00559 0.00324 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00559 0.00168 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1,2-Trichloroethane
0.00559 0.00324 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1-Dichloroethane
0.00559 0.00402 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1-Dichloroethene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,1-Dichloropropene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2,3-Trichlorobenzene
0.00559 0.00201 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2,3-Trichloropropane
0.00559 0.00279 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2,4-Trichlorobenzene
0.00559 0.00279 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.01831,2,4-Trimethylbenzene
0.0112 0.00179 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2-Dibromo-3-Chloropropane
0.00559 0.00190 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2-Dichlorobenzene
0.00559 0.00257 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2-Dichloroethane
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,2-Dichloropropane
0.00559 0.00268 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.00537 J1,3,5-Trimethylbenzene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,3-Dichlorobenzene
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,3-Dichloropropane
0.00559 0.00201 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND1,4-Dichlorobenzene
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND2,2-Dichloropropane
0.0279 0.0103 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND2-Butanone (MEK)
0.00559 0.00257 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND2-Chlorotoluene
0.0279 0.0212 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND2-Hexanone
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND4-Chlorotoluene
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND4-Isopropyltoluene
0.0279 0.0201 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼ND4-Methyl-2-pentanone (MIBK)
0.0559 0.0123 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.0512 JAcetone
0.00559 0.00268 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDBenzene
0.00559 0.00190 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDBromobenzene
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDBromoform
0.00559 0.00268 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDBromomethane
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDCarbon disulfide
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDCarbon tetrachloride
0.00559 0.00156 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChlorobenzene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChlorobromomethane
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChlorodibromomethane
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChloroethane
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChloroform
0.00559 0.00268 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDChloromethane
0.00559 0.00324 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDcis-1,2-Dichloroethene
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDcis-1,3-Dichloropropene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDDibromomethane
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDDichlorobromomethane
0.0112 0.0112 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDEthyl acetate
0.00559 0.00235 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.00736Ethylbenzene
0.00559 0.00190 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDEthylene Dibromide
0.00559 0.00458 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDHexachlorobutadiene
0.00559 0.00190 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-1Client Sample ID: P3-10
Matrix: SolidDate Collected: 11/28/22 11:00
Percent Solids: 86.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00559 0.00190 mg/Kg ☼12/02/22 12:10 12/08/22 13:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0112 0.00168 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDIsopropyl ether
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDIsopropylbenzene
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDMethyl tert-butyl ether
0.0112 0.00894 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDMethylene Chloride
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.0298m-Xylene & p-Xylene
0.00559 0.00346 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.00648Naphthalene
0.00559 0.00212 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDn-Butylbenzene
0.00559 0.00480 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDn-Heptane
0.00559 0.00246 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDN-Propylbenzene
0.00559 0.00257 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.0156o-Xylene
0.00559 0.00223 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDsec-Butylbenzene
0.00559 0.00212 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDStyrene
0.00559 0.00279 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDtert-Butylbenzene
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDTetrachloroethene
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.0295Toluene
0.00559 0.00257 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDtrans-1,2-Dichloroethene
0.00559 0.00291 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDtrans-1,3-Dichloropropene
0.0112 0.00268 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDtrans-1,4-Dichloro-2-butene
0.00559 0.00201 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDTrichloroethene
0.00559 0.00346 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDTrichlorofluoromethane
0.0112 0.00615 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDVinyl acetate
0.00559 0.00313 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼NDVinyl chloride
0.0112 0.00402 mg/Kg 12/02/22 12:10 12/08/22 13:41 1☼0.0454Xylenes, Total
1,2-Dichloroethane-d4 (Surr)100 65-130 12/02/22 12:10 12/08/22 13:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:10 12/08/22 13:41 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:10 12/08/22 13:41 165-130
Toluene-d8 (Surr)106 12/02/22 12:10 12/08/22 13:41 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 1.93 1.93 mg/Kg ☼12/06/22 18:15 12/07/22 20:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.375 0.0398 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4,5-Trichlorophenol
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4,6-Trichlorophenol
0.375 0.0398 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4-Dichlorophenol
0.375 0.0500 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4-Dimethylphenol
1.93 0.943 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4-Dinitrophenol
0.375 0.0557 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,4-Dinitrotoluene
0.375 0.0477 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2,6-Dinitrotoluene
0.375 0.0398 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2-Chloronaphthalene
0.375 0.0454 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2-Chlorophenol
0.375 0.0432 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼0.0722 J2-Methylnaphthalene
0.375 0.0307 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2-Methylphenol
1.93 0.0511 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2-Nitroaniline
0.375 0.0466 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND2-Nitrophenol
0.375 0.0489 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND3 & 4 Methylphenol
0.750 0.0318 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND3,3'-Dichlorobenzidine
1.93 0.0523 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-1Client Sample ID: P3-10
Matrix: SolidDate Collected: 11/28/22 11:00
Percent Solids: 86.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 1.93 0.193 mg/Kg ☼12/06/22 18:15 12/07/22 20:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Bromophenyl phenyl ether
0.375 0.0398 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Chloro-3-methylphenol
0.750 0.0591 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Chloroaniline
0.375 0.0500 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Chlorophenyl phenyl ether
1.93 0.0557 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Nitroaniline
1.93 0.375 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼ND4-Nitrophenol
0.375 0.0466 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDAcenaphthene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDAcenaphthylene
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDAcetophenone
0.375 0.0284 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDAnthracene
0.375 0.0261 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDAtrazine
0.375 0.0659 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzaldehyde
0.375 0.0307 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzo[a]anthracene
0.375 0.0591 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzo[a]pyrene
0.375 0.0432 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzo[b]fluoranthene
0.375 0.0250 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzo[g,h,i]perylene
0.375 0.0738 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBenzo[k]fluoranthene
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDbis (2-chloroisopropyl) ether
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBis(2-chloroethoxy)methane
0.375 0.0511 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBis(2-chloroethyl)ether
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDBis(2-ethylhexyl) phthalate
0.375 0.0295 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDButyl benzyl phthalate
0.375 0.0750 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDCaprolactam
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDCarbazole
0.375 0.0239 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDChrysene
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDibenz(a,h)anthracene
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDibenzofuran
0.375 0.0420 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDiethyl phthalate
0.375 0.0386 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDimethyl phthalate
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDi-n-butyl phthalate
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDDi-n-octyl phthalate
0.375 0.0364 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDFluoranthene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDFluorene
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDHexachlorobenzene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDHexachlorobutadiene
0.375 0.0466 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDHexachlorocyclopentadiene
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDHexachloroethane
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDIndeno[1,2,3-cd]pyrene
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDIsophorone
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼0.0543 JNaphthalene
0.375 0.0295 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDNitrobenzene
0.375 0.0364 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDN-Nitrosodi-n-propylamine
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDN-Nitrosodiphenylamine
1.93 0.375 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDPentachlorophenol
0.375 0.0307 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDPhenanthrene
0.375 0.0386 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDPhenol
0.375 0.0307 mg/Kg 12/06/22 18:15 12/07/22 20:32 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-1Client Sample ID: P3-10
Matrix: SolidDate Collected: 11/28/22 11:00
Percent Solids: 86.7Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)104 21-132 12/06/22 18:15 12/07/22 20:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)72 12/06/22 18:15 12/07/22 20:32 125-130
2-Fluorophenol (Surr)58 12/06/22 18:15 12/07/22 20:32 118-130
Nitrobenzene-d5 (Surr)60 12/06/22 18:15 12/07/22 20:32 119-130
Phenol-d5 (Surr)62 12/06/22 18:15 12/07/22 20:32 121-130
Terphenyl-d14 (Surr)86 12/06/22 18:15 12/07/22 20:32 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.68 3.34 mg/Kg ☼12/12/22 09:22 12/12/22 11:34 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)75 65-125 12/12/22 09:22 12/12/22 11:34 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
30.8 F1 9.17 2.98 mg/Kg ☼12/07/22 18:30 12/08/22 18:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 72 15-139 12/07/22 18:30 12/08/22 18:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-2Client Sample ID: P3-25
Matrix: SolidDate Collected: 11/28/22 11:10
Percent Solids: 87.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00564 0.00147 mg/Kg ☼12/02/22 12:10 12/08/22 14:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1,1-Trichloroethane
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1,2,2-Tetrachloroethane
0.00564 0.00327 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00564 0.00169 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1,2-Trichloroethane
0.00564 0.00327 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1-Dichloroethane
0.00564 0.00406 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1-Dichloroethene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,1-Dichloropropene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2,3-Trichlorobenzene
0.00564 0.00203 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2,3-Trichloropropane
0.00564 0.00282 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2,4-Trichlorobenzene
0.00564 0.00282 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.01711,2,4-Trimethylbenzene
0.0113 0.00181 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2-Dibromo-3-Chloropropane
0.00564 0.00192 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2-Dichlorobenzene
0.00564 0.00260 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2-Dichloroethane
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,2-Dichloropropane
0.00564 0.00271 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.00547 J1,3,5-Trimethylbenzene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,3-Dichlorobenzene
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,3-Dichloropropane
0.00564 0.00203 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND1,4-Dichlorobenzene
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND2,2-Dichloropropane
0.0282 0.0104 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.1702-Butanone (MEK)
0.00564 0.00260 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND2-Chlorotoluene
0.0282 0.0214 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND2-Hexanone
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND4-Chlorotoluene
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND4-Isopropyltoluene
0.0282 0.0203 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼ND4-Methyl-2-pentanone (MIBK)
0.0564 0.0124 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.122Acetone
0.00564 0.00271 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDBenzene
0.00564 0.00192 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDBromobenzene
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDBromoform
0.00564 0.00271 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDBromomethane
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDCarbon disulfide
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDCarbon tetrachloride
0.00564 0.00158 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChlorobenzene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChlorobromomethane
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChlorodibromomethane
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChloroethane
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChloroform
0.00564 0.00271 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDChloromethane
0.00564 0.00327 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDcis-1,2-Dichloroethene
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDcis-1,3-Dichloropropene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDDibromomethane
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDDichlorobromomethane
0.0113 0.0113 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDEthyl acetate
0.00564 0.00237 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.00404 JEthylbenzene
0.00564 0.00192 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDEthylene Dibromide
0.00564 0.00463 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDHexachlorobutadiene
0.00564 0.00192 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-2Client Sample ID: P3-25
Matrix: SolidDate Collected: 11/28/22 11:10
Percent Solids: 87.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00564 0.00192 mg/Kg ☼12/02/22 12:10 12/08/22 14:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0113 0.00169 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDIsopropyl ether
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDIsopropylbenzene
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDMethyl tert-butyl ether
0.0113 0.00903 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDMethylene Chloride
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.0266m-Xylene & p-Xylene
0.00564 0.00350 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDNaphthalene
0.00564 0.00214 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDn-Butylbenzene
0.00564 0.00485 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDn-Heptane
0.00564 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.00248 JN-Propylbenzene
0.00564 0.00260 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.0146o-Xylene
0.00564 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDsec-Butylbenzene
0.00564 0.00214 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDStyrene
0.00564 0.00282 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDtert-Butylbenzene
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDTetrachloroethene
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.0172Toluene
0.00564 0.00260 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDtrans-1,2-Dichloroethene
0.00564 0.00293 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDtrans-1,3-Dichloropropene
0.0113 0.00271 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDtrans-1,4-Dichloro-2-butene
0.00564 0.00203 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDTrichloroethene
0.00564 0.00350 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDTrichlorofluoromethane
0.0113 0.00621 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDVinyl acetate
0.00564 0.00316 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼NDVinyl chloride
0.0113 0.00406 mg/Kg 12/02/22 12:10 12/08/22 14:04 1☼0.0412Xylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:10 12/08/22 14:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:10 12/08/22 14:04 165-130
Dibromofluoromethane (Surr)107 12/02/22 12:10 12/08/22 14:04 165-130
Toluene-d8 (Surr)105 12/02/22 12:10 12/08/22 14:04 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 1.84 1.84 mg/Kg ☼12/06/22 18:15 12/07/22 20:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.358 0.0380 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4,5-Trichlorophenol
0.358 0.0315 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4,6-Trichlorophenol
0.358 0.0380 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4-Dichlorophenol
0.358 0.0477 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4-Dimethylphenol
1.84 0.900 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4-Dinitrophenol
0.358 0.0531 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,4-Dinitrotoluene
0.358 0.0456 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2,6-Dinitrotoluene
0.358 0.0380 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Chloronaphthalene
0.358 0.0434 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Chlorophenol
0.358 0.0412 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Methylnaphthalene
0.358 0.0293 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Methylphenol
1.84 0.0488 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Nitroaniline
0.358 0.0445 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND2-Nitrophenol
0.358 0.0466 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND3 & 4 Methylphenol
0.716 0.0304 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND3,3'-Dichlorobenzidine
1.84 0.0499 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-2Client Sample ID: P3-25
Matrix: SolidDate Collected: 11/28/22 11:10
Percent Solids: 87.8Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 1.84 0.184 mg/Kg ☼12/06/22 18:15 12/07/22 20:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.358 0.0390 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Bromophenyl phenyl ether
0.358 0.0380 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Chloro-3-methylphenol
0.716 0.0564 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Chloroaniline
0.358 0.0477 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Chlorophenyl phenyl ether
1.84 0.0531 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Nitroaniline
1.84 0.358 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼ND4-Nitrophenol
0.358 0.0445 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDAcenaphthene
0.358 0.0390 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDAcenaphthylene
0.358 0.0304 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼0.0939 JAcetophenone
0.358 0.0271 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDAnthracene
0.358 0.0249 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDAtrazine
0.358 0.0629 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzaldehyde
0.358 0.0293 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzo[a]anthracene
0.358 0.0564 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzo[a]pyrene
0.358 0.0412 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzo[b]fluoranthene
0.358 0.0239 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzo[g,h,i]perylene
0.358 0.0705 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBenzo[k]fluoranthene
0.358 0.0325 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDbis (2-chloroisopropyl) ether
0.358 0.0423 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBis(2-chloroethoxy)methane
0.358 0.0488 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBis(2-chloroethyl)ether
0.358 0.0315 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDBis(2-ethylhexyl) phthalate
0.358 0.0282 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDButyl benzyl phthalate
0.358 0.0716 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDCaprolactam
0.358 0.0325 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDCarbazole
0.358 0.0228 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDChrysene
0.358 0.0423 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDibenz(a,h)anthracene
0.358 0.0358 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDibenzofuran
0.358 0.0401 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDiethyl phthalate
0.358 0.0369 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDimethyl phthalate
0.358 0.0325 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDi-n-butyl phthalate
0.358 0.0315 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDDi-n-octyl phthalate
0.358 0.0347 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDFluoranthene
0.358 0.0390 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDFluorene
0.358 0.0423 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDHexachlorobenzene
0.358 0.0390 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDHexachlorobutadiene
0.358 0.0445 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDHexachlorocyclopentadiene
0.358 0.0304 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDHexachloroethane
0.358 0.0304 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDIndeno[1,2,3-cd]pyrene
0.358 0.0358 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDIsophorone
0.358 0.0325 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDNaphthalene
0.358 0.0282 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDNitrobenzene
0.358 0.0347 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDN-Nitrosodi-n-propylamine
0.358 0.0358 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDN-Nitrosodiphenylamine
1.84 0.358 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDPentachlorophenol
0.358 0.0293 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDPhenanthrene
0.358 0.0369 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDPhenol
0.358 0.0293 mg/Kg 12/06/22 18:15 12/07/22 20:54 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-2Client Sample ID: P3-25
Matrix: SolidDate Collected: 11/28/22 11:10
Percent Solids: 87.8Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)95 21-132 12/06/22 18:15 12/07/22 20:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 12/06/22 18:15 12/07/22 20:54 125-130
2-Fluorophenol (Surr)55 12/06/22 18:15 12/07/22 20:54 118-130
Nitrobenzene-d5 (Surr)59 12/06/22 18:15 12/07/22 20:54 119-130
Phenol-d5 (Surr)57 12/06/22 18:15 12/07/22 20:54 121-130
Terphenyl-d14 (Surr)82 12/06/22 18:15 12/07/22 20:54 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.21 3.10 mg/Kg ☼12/12/22 09:22 12/12/22 13:08 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)73 65-125 12/12/22 09:22 12/12/22 13:08 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
6.46 J 9.03 2.93 mg/Kg ☼12/07/22 18:30 12/08/22 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 68 15-139 12/07/22 18:30 12/08/22 19:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-3Client Sample ID: P2-25
Matrix: SolidDate Collected: 11/28/22 11:35
Percent Solids: 81.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00664 0.00173 mg/Kg ☼12/02/22 12:10 12/08/22 14:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1,1-Trichloroethane
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1,2,2-Tetrachloroethane
0.00664 0.00385 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00664 0.00199 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1,2-Trichloroethane
0.00664 0.00385 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1-Dichloroethane
0.00664 0.00478 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1-Dichloroethene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,1-Dichloropropene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2,3-Trichlorobenzene
0.00664 0.00239 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2,3-Trichloropropane
0.00664 0.00332 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2,4-Trichlorobenzene
0.00664 0.00332 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2,4-Trimethylbenzene
0.0133 0.00212 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2-Dibromo-3-Chloropropane
0.00664 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2-Dichlorobenzene
0.00664 0.00305 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2-Dichloroethane
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,2-Dichloropropane
0.00664 0.00319 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,3,5-Trimethylbenzene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,3-Dichlorobenzene
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,3-Dichloropropane
0.00664 0.00239 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND1,4-Dichlorobenzene
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND2,2-Dichloropropane
0.0332 0.0122 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.6322-Butanone (MEK)
0.00664 0.00305 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND2-Chlorotoluene
0.0332 0.0252 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND2-Hexanone
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND4-Chlorotoluene
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND4-Isopropyltoluene
0.0332 0.0239 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼ND4-Methyl-2-pentanone (MIBK)
0.00664 0.00319 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.00477 JBenzene
0.00664 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDBromobenzene
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDBromoform
0.00664 0.00319 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDBromomethane
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDCarbon disulfide
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDCarbon tetrachloride
0.00664 0.00186 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChlorobenzene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChlorobromomethane
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChlorodibromomethane
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChloroethane
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChloroform
0.00664 0.00319 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDChloromethane
0.00664 0.00385 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDcis-1,2-Dichloroethene
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDcis-1,3-Dichloropropene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDDibromomethane
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDDichlorobromomethane
0.0133 0.0133 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDEthyl acetate
0.00664 0.00279 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDEthylbenzene
0.00664 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDEthylene Dibromide
0.00664 0.00544 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDHexachlorobutadiene
0.00664 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDHexane
0.00664 0.00226 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDIodomethane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-3Client Sample ID: P2-25
Matrix: SolidDate Collected: 11/28/22 11:35
Percent Solids: 81.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.0133 0.00199 mg/Kg ☼12/02/22 12:10 12/08/22 14:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Isopropyl ether
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDIsopropylbenzene
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.00449 JMethyl tert-butyl ether
0.0133 0.0106 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDMethylene Chloride
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.00665m-Xylene & p-Xylene
0.00664 0.00412 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDNaphthalene
0.00664 0.00252 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDn-Butylbenzene
0.00664 0.00571 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDn-Heptane
0.00664 0.00292 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDN-Propylbenzene
0.00664 0.00305 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.00456 Jo-Xylene
0.00664 0.00266 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDsec-Butylbenzene
0.00664 0.00252 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDStyrene
0.00664 0.00332 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDtert-Butylbenzene
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDTetrachloroethene
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.0172Toluene
0.00664 0.00305 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDtrans-1,2-Dichloroethene
0.00664 0.00345 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDtrans-1,3-Dichloropropene
0.0133 0.00319 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDtrans-1,4-Dichloro-2-butene
0.00664 0.00239 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDTrichloroethene
0.00664 0.00412 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDTrichlorofluoromethane
0.0133 0.00730 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDVinyl acetate
0.00664 0.00372 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼NDVinyl chloride
0.0133 0.00478 mg/Kg 12/02/22 12:10 12/08/22 14:28 1☼0.0112 JXylenes, Total
1,2-Dichloroethane-d4 (Surr)99 65-130 12/02/22 12:10 12/08/22 14:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:10 12/08/22 14:28 165-130
Dibromofluoromethane (Surr)105 12/02/22 12:10 12/08/22 14:28 165-130
Toluene-d8 (Surr)104 12/02/22 12:10 12/08/22 14:28 165-130
Method: SW846 8260D - Volatile Organic Compounds by GC/MS - RA
RL MDL
1.30 0.0672 0.0148 mg/Kg ☼12/02/22 12:10 12/07/22 20:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acetone
1,2-Dichloroethane-d4 (Surr)100 65-130 12/02/22 12:10 12/07/22 20:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 12/02/22 12:10 12/07/22 20:47 165-130
Dibromofluoromethane (Surr)105 12/02/22 12:10 12/07/22 20:47 165-130
Toluene-d8 (Surr)104 12/02/22 12:10 12/07/22 20:47 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.04 2.04 mg/Kg ☼12/06/22 18:15 12/07/22 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.396 0.0420 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4,5-Trichlorophenol
0.396 0.0348 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4,6-Trichlorophenol
0.396 0.0420 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4-Dichlorophenol
0.396 0.0527 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4-Dimethylphenol
2.04 0.995 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4-Dinitrophenol
0.396 0.0587 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,4-Dinitrotoluene
0.396 0.0503 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2,6-Dinitrotoluene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-3Client Sample ID: P2-25
Matrix: SolidDate Collected: 11/28/22 11:35
Percent Solids: 81.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.396 0.0420 mg/Kg ☼12/06/22 18:15 12/07/22 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Chloronaphthalene
0.396 0.0479 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2-Chlorophenol
0.396 0.0455 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2-Methylnaphthalene
0.396 0.0324 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2-Methylphenol
2.04 0.0539 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2-Nitroaniline
0.396 0.0491 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND2-Nitrophenol
0.396 0.0515 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND3 & 4 Methylphenol
0.791 0.0336 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND3,3'-Dichlorobenzidine
2.04 0.0551 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND3-Nitroaniline
2.04 0.204 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4,6-Dinitro-2-methylphenol
0.396 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Bromophenyl phenyl ether
0.396 0.0420 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Chloro-3-methylphenol
0.791 0.0623 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Chloroaniline
0.396 0.0527 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Chlorophenyl phenyl ether
2.04 0.0587 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Nitroaniline
2.04 0.396 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼ND4-Nitrophenol
0.396 0.0491 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDAcenaphthene
0.396 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDAcenaphthylene
0.396 0.0336 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDAcetophenone
0.396 0.0300 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDAnthracene
0.396 0.0276 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDAtrazine
0.396 0.0695 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzaldehyde
0.396 0.0324 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzo[a]anthracene
0.396 0.0623 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzo[a]pyrene
0.396 0.0455 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzo[b]fluoranthene
0.396 0.0264 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzo[g,h,i]perylene
0.396 0.0779 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBenzo[k]fluoranthene
0.396 0.0360 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDbis (2-chloroisopropyl) ether
0.396 0.0467 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBis(2-chloroethoxy)methane
0.396 0.0539 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBis(2-chloroethyl)ether
0.396 0.0348 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDBis(2-ethylhexyl) phthalate
0.396 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDButyl benzyl phthalate
0.396 0.0791 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDCaprolactam
0.396 0.0360 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDCarbazole
0.396 0.0252 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDChrysene
0.396 0.0467 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDibenz(a,h)anthracene
0.396 0.0396 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDibenzofuran
0.396 0.0443 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDiethyl phthalate
0.396 0.0408 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDimethyl phthalate
0.396 0.0360 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDi-n-butyl phthalate
0.396 0.0348 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDDi-n-octyl phthalate
0.396 0.0384 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDFluoranthene
0.396 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDFluorene
0.396 0.0467 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDHexachlorobenzene
0.396 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDHexachlorobutadiene
0.396 0.0491 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDHexachlorocyclopentadiene
0.396 0.0336 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDHexachloroethane
0.396 0.0336 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDIndeno[1,2,3-cd]pyrene
0.396 0.0396 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDIsophorone
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-3Client Sample ID: P2-25
Matrix: SolidDate Collected: 11/28/22 11:35
Percent Solids: 81.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.396 0.0360 mg/Kg ☼12/06/22 18:15 12/07/22 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Naphthalene
0.396 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDNitrobenzene
0.396 0.0384 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDN-Nitrosodi-n-propylamine
0.396 0.0396 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDN-Nitrosodiphenylamine
2.04 0.396 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDPentachlorophenol
0.396 0.0324 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDPhenanthrene
0.396 0.0408 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDPhenol
0.396 0.0324 mg/Kg 12/06/22 18:15 12/07/22 21:15 1☼NDPyrene
2,4,6-Tribromophenol (Surr)84 21-132 12/06/22 18:15 12/07/22 21:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 12/06/22 18:15 12/07/22 21:15 125-130
2-Fluorophenol (Surr)55 12/06/22 18:15 12/07/22 21:15 118-130
Nitrobenzene-d5 (Surr)57 12/06/22 18:15 12/07/22 21:15 119-130
Phenol-d5 (Surr)56 12/06/22 18:15 12/07/22 21:15 121-130
Terphenyl-d14 (Surr)76 12/06/22 18:15 12/07/22 21:15 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 7.46 3.73 mg/Kg ☼12/12/22 09:22 12/12/22 13:39 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)78 65-125 12/12/22 09:22 12/12/22 13:39 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
4.39 J 9.69 3.15 mg/Kg ☼12/07/22 18:30 12/08/22 19:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 55 15-139 12/07/22 18:30 12/08/22 19:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-4Client Sample ID: P4-15
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00621 0.00161 mg/Kg ☼12/02/22 12:10 12/08/22 14:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1,1-Trichloroethane
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1,2,2-Tetrachloroethane
0.00621 0.00360 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00621 0.00186 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1,2-Trichloroethane
0.00621 0.00360 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1-Dichloroethane
0.00621 0.00447 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1-Dichloroethene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,1-Dichloropropene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2,3-Trichlorobenzene
0.00621 0.00223 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2,3-Trichloropropane
0.00621 0.00310 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2,4-Trichlorobenzene
0.00621 0.00310 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2,4-Trimethylbenzene
0.0124 0.00199 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2-Dibromo-3-Chloropropane
0.00621 0.00211 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2-Dichlorobenzene
0.00621 0.00285 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2-Dichloroethane
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,2-Dichloropropane
0.00621 0.00298 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,3,5-Trimethylbenzene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,3-Dichlorobenzene
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,3-Dichloropropane
0.00621 0.00223 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND1,4-Dichlorobenzene
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND2,2-Dichloropropane
0.0310 0.0114 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼0.03512-Butanone (MEK)
0.00621 0.00285 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND2-Chlorotoluene
0.0310 0.0236 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND2-Hexanone
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND4-Chlorotoluene
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND4-Isopropyltoluene
0.0310 0.0223 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼ND4-Methyl-2-pentanone (MIBK)
0.0621 0.0137 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼0.0904Acetone
0.00621 0.00298 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDBenzene
0.00621 0.00211 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDBromobenzene
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDBromoform
0.00621 0.00298 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDBromomethane
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDCarbon disulfide
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDCarbon tetrachloride
0.00621 0.00174 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChlorobenzene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChlorobromomethane
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChlorodibromomethane
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChloroethane
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChloroform
0.00621 0.00298 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDChloromethane
0.00621 0.00360 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDcis-1,2-Dichloroethene
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDcis-1,3-Dichloropropene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDDibromomethane
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDDichlorobromomethane
0.0124 0.0124 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDEthyl acetate
0.00621 0.00261 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDEthylbenzene
0.00621 0.00211 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDEthylene Dibromide
0.00621 0.00509 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDHexachlorobutadiene
0.00621 0.00211 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-4Client Sample ID: P4-15
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
0.00430 J 0.00621 0.00211 mg/Kg ☼12/02/22 12:10 12/08/22 14:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0124 0.00186 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDIsopropyl ether
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDIsopropylbenzene
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDMethyl tert-butyl ether
0.0124 0.00993 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDMethylene Chloride
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDm-Xylene & p-Xylene
0.00621 0.00385 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDNaphthalene
0.00621 0.00236 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDn-Butylbenzene
0.00621 0.00534 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDn-Heptane
0.00621 0.00273 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDN-Propylbenzene
0.00621 0.00285 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDo-Xylene
0.00621 0.00248 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDsec-Butylbenzene
0.00621 0.00236 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDStyrene
0.00621 0.00310 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDtert-Butylbenzene
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDTetrachloroethene
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDToluene
0.00621 0.00285 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDtrans-1,2-Dichloroethene
0.00621 0.00323 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDtrans-1,3-Dichloropropene
0.0124 0.00298 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDtrans-1,4-Dichloro-2-butene
0.00621 0.00223 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDTrichloroethene
0.00621 0.00385 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDTrichlorofluoromethane
0.0124 0.00683 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDVinyl acetate
0.00621 0.00348 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDVinyl chloride
0.0124 0.00447 mg/Kg 12/02/22 12:10 12/08/22 14:52 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)100 65-130 12/02/22 12:10 12/08/22 14:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:10 12/08/22 14:52 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:10 12/08/22 14:52 165-130
Toluene-d8 (Surr)105 12/02/22 12:10 12/08/22 14:52 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 1.90 1.90 mg/Kg ☼12/06/22 18:15 12/07/22 21:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.368 0.0390 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4,5-Trichlorophenol
0.368 0.0323 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4,6-Trichlorophenol
0.368 0.0390 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4-Dichlorophenol
0.368 0.0490 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4-Dimethylphenol
1.90 0.925 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4-Dinitrophenol
0.368 0.0546 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,4-Dinitrotoluene
0.368 0.0468 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2,6-Dinitrotoluene
0.368 0.0390 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Chloronaphthalene
0.368 0.0446 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Chlorophenol
0.368 0.0424 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Methylnaphthalene
0.368 0.0301 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Methylphenol
1.90 0.0502 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Nitroaniline
0.368 0.0457 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND2-Nitrophenol
0.368 0.0479 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND3 & 4 Methylphenol
0.736 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND3,3'-Dichlorobenzidine
1.90 0.0513 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-4Client Sample ID: P4-15
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 1.90 0.190 mg/Kg ☼12/06/22 18:15 12/07/22 21:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.368 0.0401 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Bromophenyl phenyl ether
0.368 0.0390 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Chloro-3-methylphenol
0.736 0.0580 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Chloroaniline
0.368 0.0490 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Chlorophenyl phenyl ether
1.90 0.0546 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Nitroaniline
1.90 0.368 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼ND4-Nitrophenol
0.368 0.0457 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDAcenaphthene
0.368 0.0401 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDAcenaphthylene
0.368 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDAcetophenone
0.368 0.0279 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDAnthracene
0.368 0.0256 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDAtrazine
0.368 0.0647 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzaldehyde
0.368 0.0301 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzo[a]anthracene
0.368 0.0580 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzo[a]pyrene
0.368 0.0424 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzo[b]fluoranthene
0.368 0.0245 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzo[g,h,i]perylene
0.368 0.0725 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBenzo[k]fluoranthene
0.368 0.0334 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDbis (2-chloroisopropyl) ether
0.368 0.0435 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBis(2-chloroethoxy)methane
0.368 0.0502 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBis(2-chloroethyl)ether
0.368 0.0323 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDBis(2-ethylhexyl) phthalate
0.368 0.0290 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDButyl benzyl phthalate
0.368 0.0736 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDCaprolactam
0.368 0.0334 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDCarbazole
0.368 0.0234 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDChrysene
0.368 0.0435 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDibenz(a,h)anthracene
0.368 0.0368 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDibenzofuran
0.368 0.0412 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDiethyl phthalate
0.368 0.0379 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDimethyl phthalate
0.368 0.0334 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDi-n-butyl phthalate
0.368 0.0323 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDDi-n-octyl phthalate
0.368 0.0357 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDFluoranthene
0.368 0.0401 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDFluorene
0.368 0.0435 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDHexachlorobenzene
0.368 0.0401 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDHexachlorobutadiene
0.368 0.0457 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDHexachlorocyclopentadiene
0.368 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDHexachloroethane
0.368 0.0312 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDIndeno[1,2,3-cd]pyrene
0.368 0.0368 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDIsophorone
0.368 0.0334 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDNaphthalene
0.368 0.0290 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDNitrobenzene
0.368 0.0357 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDN-Nitrosodi-n-propylamine
0.368 0.0368 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDN-Nitrosodiphenylamine
1.90 0.368 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDPentachlorophenol
0.368 0.0301 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDPhenanthrene
0.368 0.0379 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDPhenol
0.368 0.0301 mg/Kg 12/06/22 18:15 12/07/22 21:36 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-4Client Sample ID: P4-15
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)97 21-132 12/06/22 18:15 12/07/22 21:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)72 12/06/22 18:15 12/07/22 21:36 125-130
2-Fluorophenol (Surr)62 12/06/22 18:15 12/07/22 21:36 118-130
Nitrobenzene-d5 (Surr)65 12/06/22 18:15 12/07/22 21:36 119-130
Phenol-d5 (Surr)63 12/06/22 18:15 12/07/22 21:36 121-130
Terphenyl-d14 (Surr)84 12/06/22 18:15 12/07/22 21:36 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.96 3.48 mg/Kg ☼12/12/22 09:22 12/12/22 14:10 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)76 65-125 12/12/22 09:22 12/12/22 14:10 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
9.94 9.12 2.97 mg/Kg ☼12/07/22 18:30 12/08/22 19:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 59 15-139 12/07/22 18:30 12/08/22 19:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-5Client Sample ID: P4-25
Matrix: SolidDate Collected: 11/28/22 12:05
Percent Solids: 87.1Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00633 0.00165 mg/Kg ☼12/02/22 12:10 12/08/22 15:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1,1-Trichloroethane
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1,2,2-Tetrachloroethane
0.00633 0.00367 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00633 0.00190 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1,2-Trichloroethane
0.00633 0.00367 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1-Dichloroethane
0.00633 0.00456 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1-Dichloroethene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,1-Dichloropropene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2,3-Trichlorobenzene
0.00633 0.00228 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2,3-Trichloropropane
0.00633 0.00317 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2,4-Trichlorobenzene
0.00633 0.00317 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2,4-Trimethylbenzene
0.0127 0.00203 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2-Dibromo-3-Chloropropane
0.00633 0.00215 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2-Dichlorobenzene
0.00633 0.00291 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2-Dichloroethane
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,2-Dichloropropane
0.00633 0.00304 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,3,5-Trimethylbenzene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,3-Dichlorobenzene
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,3-Dichloropropane
0.00633 0.00228 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND1,4-Dichlorobenzene
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND2,2-Dichloropropane
0.0317 0.0116 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼0.0158 J2-Butanone (MEK)
0.00633 0.00291 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND2-Chlorotoluene
0.0317 0.0241 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND2-Hexanone
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND4-Chlorotoluene
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND4-Isopropyltoluene
0.0317 0.0228 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼ND4-Methyl-2-pentanone (MIBK)
0.0633 0.0139 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼0.0288 JAcetone
0.00633 0.00304 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDBenzene
0.00633 0.00215 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDBromobenzene
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDBromoform
0.00633 0.00304 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDBromomethane
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDCarbon disulfide
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDCarbon tetrachloride
0.00633 0.00177 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChlorobenzene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChlorobromomethane
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChlorodibromomethane
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChloroethane
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChloroform
0.00633 0.00304 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDChloromethane
0.00633 0.00367 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDcis-1,2-Dichloroethene
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDcis-1,3-Dichloropropene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDDibromomethane
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDDichlorobromomethane
0.0127 0.0127 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDEthyl acetate
0.00633 0.00266 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDEthylbenzene
0.00633 0.00215 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDEthylene Dibromide
0.00633 0.00519 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDHexachlorobutadiene
0.00633 0.00215 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-5Client Sample ID: P4-25
Matrix: SolidDate Collected: 11/28/22 12:05
Percent Solids: 87.1Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00633 0.00215 mg/Kg ☼12/02/22 12:10 12/08/22 15:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0127 0.00190 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDIsopropyl ether
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDIsopropylbenzene
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDMethyl tert-butyl ether
0.0127 0.0101 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDMethylene Chloride
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDm-Xylene & p-Xylene
0.00633 0.00393 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDNaphthalene
0.00633 0.00241 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDn-Butylbenzene
0.00633 0.00544 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDn-Heptane
0.00633 0.00279 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDN-Propylbenzene
0.00633 0.00291 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDo-Xylene
0.00633 0.00253 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDsec-Butylbenzene
0.00633 0.00241 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDStyrene
0.00633 0.00317 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDtert-Butylbenzene
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDTetrachloroethene
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼0.00488 JToluene
0.00633 0.00291 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDtrans-1,2-Dichloroethene
0.00633 0.00329 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDtrans-1,3-Dichloropropene
0.0127 0.00304 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDtrans-1,4-Dichloro-2-butene
0.00633 0.00228 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDTrichloroethene
0.00633 0.00393 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDTrichlorofluoromethane
0.0127 0.00696 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDVinyl acetate
0.00633 0.00355 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDVinyl chloride
0.0127 0.00456 mg/Kg 12/02/22 12:10 12/08/22 15:16 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:10 12/08/22 15:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 12/02/22 12:10 12/08/22 15:16 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:10 12/08/22 15:16 165-130
Toluene-d8 (Surr)104 12/02/22 12:10 12/08/22 15:16 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 1.88 1.88 mg/Kg ☼12/06/22 18:15 12/07/22 21:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.366 0.0388 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4,5-Trichlorophenol
0.366 0.0321 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4,6-Trichlorophenol
0.366 0.0388 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4-Dichlorophenol
0.366 0.0488 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4-Dimethylphenol
1.88 0.920 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4-Dinitrophenol
0.366 0.0543 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,4-Dinitrotoluene
0.366 0.0466 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2,6-Dinitrotoluene
0.366 0.0388 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Chloronaphthalene
0.366 0.0443 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Chlorophenol
0.366 0.0421 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Methylnaphthalene
0.366 0.0299 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Methylphenol
1.88 0.0499 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Nitroaniline
0.366 0.0454 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND2-Nitrophenol
0.366 0.0477 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND3 & 4 Methylphenol
0.732 0.0310 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND3,3'-Dichlorobenzidine
1.88 0.0510 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-5Client Sample ID: P4-25
Matrix: SolidDate Collected: 11/28/22 12:05
Percent Solids: 87.1Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 1.88 0.188 mg/Kg ☼12/06/22 18:15 12/07/22 21:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.366 0.0399 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Bromophenyl phenyl ether
0.366 0.0388 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Chloro-3-methylphenol
0.732 0.0576 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Chloroaniline
0.366 0.0488 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Chlorophenyl phenyl ether
1.88 0.0543 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Nitroaniline
1.88 0.366 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼ND4-Nitrophenol
0.366 0.0454 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDAcenaphthene
0.366 0.0399 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDAcenaphthylene
0.366 0.0310 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDAcetophenone
0.366 0.0277 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDAnthracene
0.366 0.0255 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDAtrazine
0.366 0.0643 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzaldehyde
0.366 0.0299 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzo[a]anthracene
0.366 0.0576 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzo[a]pyrene
0.366 0.0421 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzo[b]fluoranthene
0.366 0.0244 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzo[g,h,i]perylene
0.366 0.0720 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBenzo[k]fluoranthene
0.366 0.0333 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDbis (2-chloroisopropyl) ether
0.366 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBis(2-chloroethoxy)methane
0.366 0.0499 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBis(2-chloroethyl)ether
0.366 0.0321 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDBis(2-ethylhexyl) phthalate
0.366 0.0288 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDButyl benzyl phthalate
0.366 0.0732 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDCaprolactam
0.366 0.0333 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDCarbazole
0.366 0.0233 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDChrysene
0.366 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDibenz(a,h)anthracene
0.366 0.0366 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDibenzofuran
0.366 0.0410 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDiethyl phthalate
0.366 0.0377 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDimethyl phthalate
0.366 0.0333 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDi-n-butyl phthalate
0.366 0.0321 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDDi-n-octyl phthalate
0.366 0.0355 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDFluoranthene
0.366 0.0399 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDFluorene
0.366 0.0432 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDHexachlorobenzene
0.366 0.0399 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDHexachlorobutadiene
0.366 0.0454 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDHexachlorocyclopentadiene
0.366 0.0310 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDHexachloroethane
0.366 0.0310 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDIndeno[1,2,3-cd]pyrene
0.366 0.0366 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDIsophorone
0.366 0.0333 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDNaphthalene
0.366 0.0288 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDNitrobenzene
0.366 0.0355 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDN-Nitrosodi-n-propylamine
0.366 0.0366 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDN-Nitrosodiphenylamine
1.88 0.366 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDPentachlorophenol
0.366 0.0299 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDPhenanthrene
0.366 0.0377 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDPhenol
0.366 0.0299 mg/Kg 12/06/22 18:15 12/07/22 21:58 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-5Client Sample ID: P4-25
Matrix: SolidDate Collected: 11/28/22 12:05
Percent Solids: 87.1Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)80 21-132 12/06/22 18:15 12/07/22 21:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)60 12/06/22 18:15 12/07/22 21:58 125-130
2-Fluorophenol (Surr)51 12/06/22 18:15 12/07/22 21:58 118-130
Nitrobenzene-d5 (Surr)53 12/06/22 18:15 12/07/22 21:58 119-130
Phenol-d5 (Surr)52 12/06/22 18:15 12/07/22 21:58 121-130
Terphenyl-d14 (Surr)72 12/06/22 18:15 12/07/22 21:58 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.81 3.40 mg/Kg ☼12/12/22 09:22 12/12/22 14:41 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)77 65-125 12/12/22 09:22 12/12/22 14:41 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
ND 8.95 2.91 mg/Kg ☼12/07/22 18:30 12/08/22 19:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 51 15-139 12/07/22 18:30 12/08/22 19:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-6Client Sample ID: P5-10
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00610 0.00159 mg/Kg ☼12/02/22 12:11 12/08/22 15:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1,1-Trichloroethane
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1,2,2-Tetrachloroethane
0.00610 0.00354 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00610 0.00183 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1,2-Trichloroethane
0.00610 0.00354 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1-Dichloroethane
0.00610 0.00439 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1-Dichloroethene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,1-Dichloropropene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2,3-Trichlorobenzene
0.00610 0.00220 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2,3-Trichloropropane
0.00610 0.00305 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2,4-Trichlorobenzene
0.00610 0.00305 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2,4-Trimethylbenzene
0.0122 0.00195 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2-Dibromo-3-Chloropropane
0.00610 0.00207 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2-Dichlorobenzene
0.00610 0.00281 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2-Dichloroethane
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,2-Dichloropropane
0.00610 0.00293 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,3,5-Trimethylbenzene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,3-Dichlorobenzene
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,3-Dichloropropane
0.00610 0.00220 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND1,4-Dichlorobenzene
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND2,2-Dichloropropane
0.0305 0.0112 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND2-Butanone (MEK)
0.00610 0.00281 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND2-Chlorotoluene
0.0305 0.0232 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND2-Hexanone
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND4-Chlorotoluene
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND4-Isopropyltoluene
0.0305 0.0220 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼ND4-Methyl-2-pentanone (MIBK)
0.0610 0.0134 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼0.0286 JAcetone
0.00610 0.00293 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDBenzene
0.00610 0.00207 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDBromobenzene
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDBromoform
0.00610 0.00293 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDBromomethane
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDCarbon disulfide
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDCarbon tetrachloride
0.00610 0.00171 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChlorobenzene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChlorobromomethane
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChlorodibromomethane
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChloroethane
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChloroform
0.00610 0.00293 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDChloromethane
0.00610 0.00354 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDcis-1,2-Dichloroethene
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDcis-1,3-Dichloropropene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDDibromomethane
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDDichlorobromomethane
0.0122 0.0122 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDEthyl acetate
0.00610 0.00256 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDEthylbenzene
0.00610 0.00207 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDEthylene Dibromide
0.00610 0.00500 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDHexachlorobutadiene
0.00610 0.00207 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-6Client Sample ID: P5-10
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00610 0.00207 mg/Kg ☼12/02/22 12:11 12/08/22 15:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0122 0.00183 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDIsopropyl ether
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDIsopropylbenzene
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDMethyl tert-butyl ether
0.0122 0.00976 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDMethylene Chloride
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDm-Xylene & p-Xylene
0.00610 0.00378 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDNaphthalene
0.00610 0.00232 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDn-Butylbenzene
0.00610 0.00525 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDn-Heptane
0.00610 0.00268 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDN-Propylbenzene
0.00610 0.00281 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDo-Xylene
0.00610 0.00244 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDsec-Butylbenzene
0.00610 0.00232 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDStyrene
0.00610 0.00305 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDtert-Butylbenzene
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDTetrachloroethene
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDToluene
0.00610 0.00281 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDtrans-1,2-Dichloroethene
0.00610 0.00317 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDtrans-1,3-Dichloropropene
0.0122 0.00293 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDtrans-1,4-Dichloro-2-butene
0.00610 0.00220 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDTrichloroethene
0.00610 0.00378 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDTrichlorofluoromethane
0.0122 0.00671 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDVinyl acetate
0.00610 0.00342 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDVinyl chloride
0.0122 0.00439 mg/Kg 12/02/22 12:11 12/08/22 15:40 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 15:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 15:40 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 15:40 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/08/22 15:40 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 1.93 1.93 mg/Kg ☼12/06/22 18:15 12/07/22 22:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.375 0.0397 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4,5-Trichlorophenol
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4,6-Trichlorophenol
0.375 0.0397 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4-Dichlorophenol
0.375 0.0499 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4-Dimethylphenol
1.93 0.942 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4-Dinitrophenol
0.375 0.0556 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,4-Dinitrotoluene
0.375 0.0477 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2,6-Dinitrotoluene
0.375 0.0397 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Chloronaphthalene
0.375 0.0454 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Chlorophenol
0.375 0.0431 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Methylnaphthalene
0.375 0.0306 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Methylphenol
1.93 0.0511 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Nitroaniline
0.375 0.0465 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND2-Nitrophenol
0.375 0.0488 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND3 & 4 Methylphenol
0.749 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND3,3'-Dichlorobenzidine
1.93 0.0522 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-6Client Sample ID: P5-10
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 1.93 0.193 mg/Kg ☼12/06/22 18:15 12/07/22 22:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Bromophenyl phenyl ether
0.375 0.0397 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Chloro-3-methylphenol
0.749 0.0590 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Chloroaniline
0.375 0.0499 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Chlorophenyl phenyl ether
1.93 0.0556 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Nitroaniline
1.93 0.375 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼ND4-Nitrophenol
0.375 0.0465 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDAcenaphthene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDAcenaphthylene
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDAcetophenone
0.375 0.0284 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDAnthracene
0.375 0.0261 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDAtrazine
0.375 0.0658 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzaldehyde
0.375 0.0306 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzo[a]anthracene
0.375 0.0590 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzo[a]pyrene
0.375 0.0431 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzo[b]fluoranthene
0.375 0.0250 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzo[g,h,i]perylene
0.375 0.0738 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBenzo[k]fluoranthene
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDbis (2-chloroisopropyl) ether
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBis(2-chloroethoxy)methane
0.375 0.0511 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBis(2-chloroethyl)ether
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDBis(2-ethylhexyl) phthalate
0.375 0.0295 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDButyl benzyl phthalate
0.375 0.0749 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDCaprolactam
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDCarbazole
0.375 0.0238 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDChrysene
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDibenz(a,h)anthracene
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDibenzofuran
0.375 0.0420 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDiethyl phthalate
0.375 0.0386 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDimethyl phthalate
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDi-n-butyl phthalate
0.375 0.0329 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDDi-n-octyl phthalate
0.375 0.0363 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDFluoranthene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDFluorene
0.375 0.0443 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDHexachlorobenzene
0.375 0.0409 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDHexachlorobutadiene
0.375 0.0465 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDHexachlorocyclopentadiene
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDHexachloroethane
0.375 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDIndeno[1,2,3-cd]pyrene
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDIsophorone
0.375 0.0341 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDNaphthalene
0.375 0.0295 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDNitrobenzene
0.375 0.0363 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDN-Nitrosodi-n-propylamine
0.375 0.0375 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDN-Nitrosodiphenylamine
1.93 0.375 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDPentachlorophenol
0.375 0.0306 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDPhenanthrene
0.375 0.0386 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDPhenol
0.375 0.0306 mg/Kg 12/06/22 18:15 12/07/22 22:19 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-6Client Sample ID: P5-10
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)96 21-132 12/06/22 18:15 12/07/22 22:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)75 12/06/22 18:15 12/07/22 22:19 125-130
2-Fluorophenol (Surr)63 12/06/22 18:15 12/07/22 22:19 118-130
Nitrobenzene-d5 (Surr)66 12/06/22 18:15 12/07/22 22:19 119-130
Phenol-d5 (Surr)64 12/06/22 18:15 12/07/22 22:19 121-130
Terphenyl-d14 (Surr)88 12/06/22 18:15 12/07/22 22:19 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.94 3.47 mg/Kg ☼12/12/22 09:22 12/12/22 15:12 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)73 65-125 12/12/22 09:22 12/12/22 15:12 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
7.78 J 9.34 3.04 mg/Kg ☼12/07/22 18:30 12/08/22 20:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 48 15-139 12/07/22 18:30 12/08/22 20:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-7Client Sample ID: P5-20
Matrix: SolidDate Collected: 11/28/22 12:25
Percent Solids: 82.9Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00605 0.00157 mg/Kg ☼12/02/22 12:11 12/08/22 16:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1,1-Trichloroethane
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1,2,2-Tetrachloroethane
0.00605 0.00351 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00605 0.00181 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1,2-Trichloroethane
0.00605 0.00351 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1-Dichloroethane
0.00605 0.00435 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1-Dichloroethene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,1-Dichloropropene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2,3-Trichlorobenzene
0.00605 0.00218 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2,3-Trichloropropane
0.00605 0.00302 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2,4-Trichlorobenzene
0.00605 0.00302 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2,4-Trimethylbenzene
0.0121 0.00194 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2-Dibromo-3-Chloropropane
0.00605 0.00206 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2-Dichlorobenzene
0.00605 0.00278 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2-Dichloroethane
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,2-Dichloropropane
0.00605 0.00290 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,3,5-Trimethylbenzene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,3-Dichlorobenzene
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,3-Dichloropropane
0.00605 0.00218 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND1,4-Dichlorobenzene
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND2,2-Dichloropropane
0.0302 0.0111 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼0.3192-Butanone (MEK)
0.00605 0.00278 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND2-Chlorotoluene
0.0302 0.0230 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND2-Hexanone
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND4-Chlorotoluene
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND4-Isopropyltoluene
0.0302 0.0218 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼ND4-Methyl-2-pentanone (MIBK)
0.0605 0.0133 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼0.462Acetone
0.00605 0.00290 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDBenzene
0.00605 0.00206 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDBromobenzene
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDBromoform
0.00605 0.00290 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDBromomethane
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDCarbon disulfide
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDCarbon tetrachloride
0.00605 0.00169 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChlorobenzene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChlorobromomethane
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChlorodibromomethane
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChloroethane
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChloroform
0.00605 0.00290 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDChloromethane
0.00605 0.00351 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDcis-1,2-Dichloroethene
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDcis-1,3-Dichloropropene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDDibromomethane
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDDichlorobromomethane
0.0121 0.0121 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDEthyl acetate
0.00605 0.00254 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDEthylbenzene
0.00605 0.00206 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDEthylene Dibromide
0.00605 0.00496 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDHexachlorobutadiene
0.00605 0.00206 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-7Client Sample ID: P5-20
Matrix: SolidDate Collected: 11/28/22 12:25
Percent Solids: 82.9Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00605 0.00206 mg/Kg ☼12/02/22 12:11 12/08/22 16:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0121 0.00181 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDIsopropyl ether
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDIsopropylbenzene
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDMethyl tert-butyl ether
0.0121 0.00968 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDMethylene Chloride
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDm-Xylene & p-Xylene
0.00605 0.00375 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDNaphthalene
0.00605 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDn-Butylbenzene
0.00605 0.00520 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDn-Heptane
0.00605 0.00266 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDN-Propylbenzene
0.00605 0.00278 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDo-Xylene
0.00605 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDsec-Butylbenzene
0.00605 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDStyrene
0.00605 0.00302 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDtert-Butylbenzene
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDTetrachloroethene
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼0.00427 JToluene
0.00605 0.00278 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDtrans-1,2-Dichloroethene
0.00605 0.00314 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDtrans-1,3-Dichloropropene
0.0121 0.00290 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDtrans-1,4-Dichloro-2-butene
0.00605 0.00218 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDTrichloroethene
0.00605 0.00375 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDTrichlorofluoromethane
0.0121 0.00665 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDVinyl acetate
0.00605 0.00339 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDVinyl chloride
0.0121 0.00435 mg/Kg 12/02/22 12:11 12/08/22 16:03 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 16:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 12/02/22 12:11 12/08/22 16:03 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 16:03 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 16:03 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.01 2.01 mg/Kg ☼12/06/22 18:15 12/07/22 22:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.389 0.0413 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4,5-Trichlorophenol
0.389 0.0342 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4,6-Trichlorophenol
0.389 0.0413 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4-Dichlorophenol
0.389 0.0519 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4-Dimethylphenol
2.01 0.979 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4-Dinitrophenol
0.389 0.0578 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,4-Dinitrotoluene
0.389 0.0495 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2,6-Dinitrotoluene
0.389 0.0413 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Chloronaphthalene
0.389 0.0472 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Chlorophenol
0.389 0.0448 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Methylnaphthalene
0.389 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Methylphenol
2.01 0.0531 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Nitroaniline
0.389 0.0484 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND2-Nitrophenol
0.389 0.0507 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND3 & 4 Methylphenol
0.778 0.0330 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND3,3'-Dichlorobenzidine
2.01 0.0543 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-7Client Sample ID: P5-20
Matrix: SolidDate Collected: 11/28/22 12:25
Percent Solids: 82.9Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.01 0.201 mg/Kg ☼12/06/22 18:15 12/07/22 22:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.389 0.0425 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Bromophenyl phenyl ether
0.389 0.0413 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Chloro-3-methylphenol
0.778 0.0613 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Chloroaniline
0.389 0.0519 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Chlorophenyl phenyl ether
2.01 0.0578 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Nitroaniline
2.01 0.389 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼ND4-Nitrophenol
0.389 0.0484 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDAcenaphthene
0.389 0.0425 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDAcenaphthylene
0.389 0.0330 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDAcetophenone
0.389 0.0295 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDAnthracene
0.389 0.0271 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDAtrazine
0.389 0.0684 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzaldehyde
0.389 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzo[a]anthracene
0.389 0.0613 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzo[a]pyrene
0.389 0.0448 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzo[b]fluoranthene
0.389 0.0259 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzo[g,h,i]perylene
0.389 0.0767 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBenzo[k]fluoranthene
0.389 0.0354 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDbis (2-chloroisopropyl) ether
0.389 0.0460 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBis(2-chloroethoxy)methane
0.389 0.0531 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBis(2-chloroethyl)ether
0.389 0.0342 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDBis(2-ethylhexyl) phthalate
0.389 0.0307 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDButyl benzyl phthalate
0.389 0.0778 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDCaprolactam
0.389 0.0354 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDCarbazole
0.389 0.0248 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDChrysene
0.389 0.0460 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDibenz(a,h)anthracene
0.389 0.0389 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDibenzofuran
0.389 0.0436 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDiethyl phthalate
0.389 0.0401 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDimethyl phthalate
0.389 0.0354 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDi-n-butyl phthalate
0.389 0.0342 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDDi-n-octyl phthalate
0.389 0.0377 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDFluoranthene
0.389 0.0425 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDFluorene
0.389 0.0460 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDHexachlorobenzene
0.389 0.0425 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDHexachlorobutadiene
0.389 0.0484 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDHexachlorocyclopentadiene
0.389 0.0330 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDHexachloroethane
0.389 0.0330 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDIndeno[1,2,3-cd]pyrene
0.389 0.0389 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDIsophorone
0.389 0.0354 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDNaphthalene
0.389 0.0307 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDNitrobenzene
0.389 0.0377 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDN-Nitrosodi-n-propylamine
0.389 0.0389 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDN-Nitrosodiphenylamine
2.01 0.389 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDPentachlorophenol
0.389 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDPhenanthrene
0.389 0.0401 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDPhenol
0.389 0.0318 mg/Kg 12/06/22 18:15 12/07/22 22:41 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-7Client Sample ID: P5-20
Matrix: SolidDate Collected: 11/28/22 12:25
Percent Solids: 82.9Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)90 21-132 12/06/22 18:15 12/07/22 22:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)62 12/06/22 18:15 12/07/22 22:41 125-130
2-Fluorophenol (Surr)54 12/06/22 18:15 12/07/22 22:41 118-130
Nitrobenzene-d5 (Surr)55 12/06/22 18:15 12/07/22 22:41 119-130
Phenol-d5 (Surr)57 12/06/22 18:15 12/07/22 22:41 121-130
Terphenyl-d14 (Surr)81 12/06/22 18:15 12/07/22 22:41 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.06 4.03 mg/Kg ☼12/12/22 09:22 12/12/22 16:55 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)75 65-125 12/12/22 09:22 12/12/22 16:55 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
3.83 J 9.41 3.06 mg/Kg ☼12/07/22 18:30 12/08/22 20:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 33 15-139 12/07/22 18:30 12/08/22 20:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-8Client Sample ID: P6-20
Matrix: SolidDate Collected: 11/28/22 13:52
Percent Solids: 78.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00574 0.00149 mg/Kg ☼12/02/22 12:11 12/08/22 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1,1-Trichloroethane
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1,2,2-Tetrachloroethane
0.00574 0.00333 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00574 0.00172 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1,2-Trichloroethane
0.00574 0.00333 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1-Dichloroethane
0.00574 0.00414 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1-Dichloroethene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,1-Dichloropropene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2,3-Trichlorobenzene
0.00574 0.00207 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2,3-Trichloropropane
0.00574 0.00287 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2,4-Trichlorobenzene
0.00574 0.00287 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2,4-Trimethylbenzene
0.0115 0.00184 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2-Dibromo-3-Chloropropane
0.00574 0.00195 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2-Dichlorobenzene
0.00574 0.00264 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2-Dichloroethane
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,2-Dichloropropane
0.00574 0.00276 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,3,5-Trimethylbenzene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,3-Dichlorobenzene
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,3-Dichloropropane
0.00574 0.00207 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND1,4-Dichlorobenzene
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND2,2-Dichloropropane
0.0287 0.0106 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.3582-Butanone (MEK)
0.00574 0.00264 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND2-Chlorotoluene
0.0287 0.0218 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.02882-Hexanone
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND4-Chlorotoluene
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND4-Isopropyltoluene
0.0287 0.0207 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼ND4-Methyl-2-pentanone (MIBK)
0.0574 0.0126 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.565Acetone
0.00574 0.00276 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.00653Benzene
0.00574 0.00195 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDBromobenzene
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDBromoform
0.00574 0.00276 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDBromomethane
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDCarbon disulfide
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDCarbon tetrachloride
0.00574 0.00161 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChlorobenzene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChlorobromomethane
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChlorodibromomethane
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChloroethane
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChloroform
0.00574 0.00276 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDChloromethane
0.00574 0.00333 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDcis-1,2-Dichloroethene
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDcis-1,3-Dichloropropene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDDibromomethane
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDDichlorobromomethane
0.0115 0.0115 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDEthyl acetate
0.00574 0.00241 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDEthylbenzene
0.00574 0.00195 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDEthylene Dibromide
0.00574 0.00471 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDHexachlorobutadiene
0.00574 0.00195 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-8Client Sample ID: P6-20
Matrix: SolidDate Collected: 11/28/22 13:52
Percent Solids: 78.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00574 0.00195 mg/Kg ☼12/02/22 12:11 12/08/22 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0115 0.00172 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDIsopropyl ether
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDIsopropylbenzene
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.00817Methyl tert-butyl ether
0.0115 0.00919 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDMethylene Chloride
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.00506 Jm-Xylene & p-Xylene
0.00574 0.00356 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDNaphthalene
0.00574 0.00218 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDn-Butylbenzene
0.00574 0.00494 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDn-Heptane
0.00574 0.00253 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDN-Propylbenzene
0.00574 0.00264 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.00436 Jo-Xylene
0.00574 0.00230 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDsec-Butylbenzene
0.00574 0.00218 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDStyrene
0.00574 0.00287 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDtert-Butylbenzene
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDTetrachloroethene
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.0157Toluene
0.00574 0.00264 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDtrans-1,2-Dichloroethene
0.00574 0.00299 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDtrans-1,3-Dichloropropene
0.0115 0.00276 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDtrans-1,4-Dichloro-2-butene
0.00574 0.00207 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDTrichloroethene
0.00574 0.00356 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDTrichlorofluoromethane
0.0115 0.00632 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDVinyl acetate
0.00574 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼NDVinyl chloride
0.0115 0.00414 mg/Kg 12/02/22 12:11 12/08/22 16:27 1☼0.00942 JXylenes, Total
1,2-Dichloroethane-d4 (Surr)99 65-130 12/02/22 12:11 12/08/22 16:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 16:27 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 16:27 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 16:27 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.13 2.13 mg/Kg ☼12/06/22 18:15 12/07/22 23:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.413 0.0438 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4,5-Trichlorophenol
0.413 0.0363 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4,6-Trichlorophenol
0.413 0.0438 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4-Dichlorophenol
0.413 0.0550 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4-Dimethylphenol
2.13 1.04 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4-Dinitrophenol
0.413 0.0613 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,4-Dinitrotoluene
0.413 0.0525 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2,6-Dinitrotoluene
0.413 0.0438 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Chloronaphthalene
0.413 0.0500 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Chlorophenol
0.413 0.0475 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Methylnaphthalene
0.413 0.0338 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Methylphenol
2.13 0.0563 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Nitroaniline
0.413 0.0513 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND2-Nitrophenol
0.413 0.0538 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND3 & 4 Methylphenol
0.825 0.0350 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND3,3'-Dichlorobenzidine
2.13 0.0575 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-8Client Sample ID: P6-20
Matrix: SolidDate Collected: 11/28/22 13:52
Percent Solids: 78.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.13 0.213 mg/Kg ☼12/06/22 18:15 12/07/22 23:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.413 0.0450 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Bromophenyl phenyl ether
0.413 0.0438 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Chloro-3-methylphenol
0.825 0.0650 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Chloroaniline
0.413 0.0550 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Chlorophenyl phenyl ether
2.13 0.0613 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Nitroaniline
2.13 0.413 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼ND4-Nitrophenol
0.413 0.0513 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDAcenaphthene
0.413 0.0450 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDAcenaphthylene
0.413 0.0350 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDAcetophenone
0.413 0.0313 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDAnthracene
0.413 0.0288 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDAtrazine
0.413 0.0725 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzaldehyde
0.413 0.0338 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzo[a]anthracene
0.413 0.0650 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzo[a]pyrene
0.413 0.0475 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzo[b]fluoranthene
0.413 0.0275 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzo[g,h,i]perylene
0.413 0.0813 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBenzo[k]fluoranthene
0.413 0.0375 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDbis (2-chloroisopropyl) ether
0.413 0.0488 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBis(2-chloroethoxy)methane
0.413 0.0563 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBis(2-chloroethyl)ether
0.413 0.0363 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDBis(2-ethylhexyl) phthalate
0.413 0.0325 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDButyl benzyl phthalate
0.413 0.0825 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDCaprolactam
0.413 0.0375 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDCarbazole
0.413 0.0263 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDChrysene
0.413 0.0488 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDibenz(a,h)anthracene
0.413 0.0413 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDibenzofuran
0.413 0.0463 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDiethyl phthalate
0.413 0.0425 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDimethyl phthalate
0.413 0.0375 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDi-n-butyl phthalate
0.413 0.0363 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDDi-n-octyl phthalate
0.413 0.0400 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDFluoranthene
0.413 0.0450 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDFluorene
0.413 0.0488 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDHexachlorobenzene
0.413 0.0450 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDHexachlorobutadiene
0.413 0.0513 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDHexachlorocyclopentadiene
0.413 0.0350 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDHexachloroethane
0.413 0.0350 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDIndeno[1,2,3-cd]pyrene
0.413 0.0413 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDIsophorone
0.413 0.0375 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDNaphthalene
0.413 0.0325 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDNitrobenzene
0.413 0.0400 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDN-Nitrosodi-n-propylamine
0.413 0.0413 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDN-Nitrosodiphenylamine
2.13 0.413 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDPentachlorophenol
0.413 0.0338 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDPhenanthrene
0.413 0.0425 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDPhenol
0.413 0.0338 mg/Kg 12/06/22 18:15 12/07/22 23:02 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-8Client Sample ID: P6-20
Matrix: SolidDate Collected: 11/28/22 13:52
Percent Solids: 78.7Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)74 21-132 12/06/22 18:15 12/07/22 23:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)62 12/06/22 18:15 12/07/22 23:02 125-130
2-Fluorophenol (Surr)50 12/06/22 18:15 12/07/22 23:02 118-130
Nitrobenzene-d5 (Surr)55 12/06/22 18:15 12/07/22 23:02 119-130
Phenol-d5 (Surr)51 12/06/22 18:15 12/07/22 23:02 121-130
Terphenyl-d14 (Surr)72 12/06/22 18:15 12/07/22 23:02 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 7.34 3.67 mg/Kg ☼12/12/22 09:22 12/12/22 17:26 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)76 65-125 12/12/22 09:22 12/12/22 17:26 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
5.81 J 10.0 3.26 mg/Kg ☼12/07/22 18:30 12/08/22 20:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 59 15-139 12/07/22 18:30 12/08/22 20:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-9Client Sample ID: P7-25
Matrix: SolidDate Collected: 11/28/22 14:20
Percent Solids: 76.3Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00672 0.00175 mg/Kg ☼12/02/22 12:11 12/08/22 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1,1-Trichloroethane
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1,2,2-Tetrachloroethane
0.00672 0.00390 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00672 0.00202 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1,2-Trichloroethane
0.00672 0.00390 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1-Dichloroethane
0.00672 0.00484 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1-Dichloroethene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,1-Dichloropropene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2,3-Trichlorobenzene
0.00672 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2,3-Trichloropropane
0.00672 0.00336 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2,4-Trichlorobenzene
0.00672 0.00336 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2,4-Trimethylbenzene
0.0134 0.00215 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2-Dibromo-3-Chloropropane
0.00672 0.00228 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2-Dichlorobenzene
0.00672 0.00309 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2-Dichloroethane
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,2-Dichloropropane
0.00672 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,3,5-Trimethylbenzene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,3-Dichlorobenzene
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,3-Dichloropropane
0.00672 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND1,4-Dichlorobenzene
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND2,2-Dichloropropane
0.0336 0.0124 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.8682-Butanone (MEK)
0.00672 0.00309 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND2-Chlorotoluene
0.0336 0.0255 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.05952-Hexanone
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND4-Chlorotoluene
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND4-Isopropyltoluene
0.0336 0.0242 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼ND4-Methyl-2-pentanone (MIBK)
2.76 0.607 mg/Kg 12/02/22 12:11 12/09/22 18:31 40☼NDAcetone
0.00672 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.00323 JBenzene
0.00672 0.00228 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDBromobenzene
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDBromoform
0.00672 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDBromomethane
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDCarbon disulfide
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDCarbon tetrachloride
0.00672 0.00188 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChlorobenzene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChlorobromomethane
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChlorodibromomethane
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChloroethane
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChloroform
0.00672 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDChloromethane
0.00672 0.00390 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDcis-1,2-Dichloroethene
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDcis-1,3-Dichloropropene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDDibromomethane
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDDichlorobromomethane
0.0134 0.0134 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDEthyl acetate
0.00672 0.00282 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDEthylbenzene
0.00672 0.00228 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDEthylene Dibromide
0.00672 0.00551 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDHexachlorobutadiene
0.00672 0.00228 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-9Client Sample ID: P7-25
Matrix: SolidDate Collected: 11/28/22 14:20
Percent Solids: 76.3Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
0.00233 J 0.00672 0.00228 mg/Kg ☼12/02/22 12:11 12/08/22 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0134 0.00202 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDIsopropyl ether
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDIsopropylbenzene
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.00331 JMethyl tert-butyl ether
0.0134 0.0107 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDMethylene Chloride
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.00585 Jm-Xylene & p-Xylene
0.00672 0.00416 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDNaphthalene
0.00672 0.00255 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDn-Butylbenzene
0.00672 0.00578 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDn-Heptane
0.00672 0.00296 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDN-Propylbenzene
0.00672 0.00309 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.00403 Jo-Xylene
0.00672 0.00269 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDsec-Butylbenzene
0.00672 0.00255 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDStyrene
0.00672 0.00336 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDtert-Butylbenzene
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDTetrachloroethene
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.0147Toluene
0.00672 0.00309 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDtrans-1,2-Dichloroethene
0.00672 0.00349 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDtrans-1,3-Dichloropropene
0.0134 0.00322 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDtrans-1,4-Dichloro-2-butene
0.00672 0.00242 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDTrichloroethene
0.00672 0.00416 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDTrichlorofluoromethane
0.0134 0.00739 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDVinyl acetate
0.00672 0.00376 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼NDVinyl chloride
0.0134 0.00484 mg/Kg 12/02/22 12:11 12/08/22 16:51 1☼0.00988 JXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 65-130 12/02/22 12:11 12/08/22 16:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)95 12/02/22 12:11 12/09/22 18:31 4065-130
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 16:51 165-130
4-Bromofluorobenzene (Surr)96 12/02/22 12:11 12/09/22 18:31 4065-130
Dibromofluoromethane (Surr)108 12/02/22 12:11 12/08/22 16:51 165-130
Dibromofluoromethane (Surr)101 12/02/22 12:11 12/09/22 18:31 4065-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 16:51 165-130
Toluene-d8 (Surr)106 12/02/22 12:11 12/09/22 18:31 4065-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.14 2.14 mg/Kg ☼12/06/22 18:15 12/07/22 23:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.416 0.0441 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4,5-Trichlorophenol
0.416 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4,6-Trichlorophenol
0.416 0.0441 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4-Dichlorophenol
0.416 0.0555 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4-Dimethylphenol
2.14 1.05 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4-Dinitrophenol
0.416 0.0618 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,4-Dinitrotoluene
0.416 0.0530 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2,6-Dinitrotoluene
0.416 0.0441 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2-Chloronaphthalene
0.416 0.0504 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2-Chlorophenol
0.416 0.0479 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2-Methylnaphthalene
0.416 0.0341 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2-Methylphenol
2.14 0.0568 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND2-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-9Client Sample ID: P7-25
Matrix: SolidDate Collected: 11/28/22 14:20
Percent Solids: 76.3Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.416 0.0517 mg/Kg ☼12/06/22 18:15 12/07/22 23:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Nitrophenol
0.416 0.0542 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND3 & 4 Methylphenol
0.832 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND3,3'-Dichlorobenzidine
2.14 0.0580 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND3-Nitroaniline
2.14 0.214 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4,6-Dinitro-2-methylphenol
0.416 0.0454 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Bromophenyl phenyl ether
0.416 0.0441 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Chloro-3-methylphenol
0.832 0.0656 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Chloroaniline
0.416 0.0555 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Chlorophenyl phenyl ether
2.14 0.0618 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Nitroaniline
2.14 0.416 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼ND4-Nitrophenol
0.416 0.0517 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDAcenaphthene
0.416 0.0454 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDAcenaphthylene
0.416 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDAcetophenone
0.416 0.0315 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDAnthracene
0.416 0.0290 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDAtrazine
0.416 0.0731 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzaldehyde
0.416 0.0341 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzo[a]anthracene
0.416 0.0656 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzo[a]pyrene
0.416 0.0479 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzo[b]fluoranthene
0.416 0.0277 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzo[g,h,i]perylene
0.416 0.0820 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBenzo[k]fluoranthene
0.416 0.0378 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDbis (2-chloroisopropyl) ether
0.416 0.0492 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBis(2-chloroethoxy)methane
0.416 0.0568 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBis(2-chloroethyl)ether
0.416 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDBis(2-ethylhexyl) phthalate
0.416 0.0328 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDButyl benzyl phthalate
0.416 0.0832 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDCaprolactam
0.416 0.0378 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDCarbazole
0.416 0.0265 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDChrysene
0.416 0.0492 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDibenz(a,h)anthracene
0.416 0.0416 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDibenzofuran
0.416 0.0467 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDiethyl phthalate
0.416 0.0429 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDimethyl phthalate
0.416 0.0378 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDi-n-butyl phthalate
0.416 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDDi-n-octyl phthalate
0.416 0.0404 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDFluoranthene
0.416 0.0454 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDFluorene
0.416 0.0492 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDHexachlorobenzene
0.416 0.0454 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDHexachlorobutadiene
0.416 0.0517 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDHexachlorocyclopentadiene
0.416 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDHexachloroethane
0.416 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDIndeno[1,2,3-cd]pyrene
0.416 0.0416 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDIsophorone
0.416 0.0378 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDNaphthalene
0.416 0.0328 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDNitrobenzene
0.416 0.0404 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDN-Nitrosodi-n-propylamine
0.416 0.0416 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDN-Nitrosodiphenylamine
2.14 0.416 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDPentachlorophenol
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-9Client Sample ID: P7-25
Matrix: SolidDate Collected: 11/28/22 14:20
Percent Solids: 76.3Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.416 0.0341 mg/Kg ☼12/06/22 18:15 12/07/22 23:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Phenanthrene
0.416 0.0429 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDPhenol
0.416 0.0341 mg/Kg 12/06/22 18:15 12/07/22 23:24 1☼NDPyrene
2,4,6-Tribromophenol (Surr)84 21-132 12/06/22 18:15 12/07/22 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 12/06/22 18:15 12/07/22 23:24 125-130
2-Fluorophenol (Surr)54 12/06/22 18:15 12/07/22 23:24 118-130
Nitrobenzene-d5 (Surr)58 12/06/22 18:15 12/07/22 23:24 119-130
Phenol-d5 (Surr)56 12/06/22 18:15 12/07/22 23:24 121-130
Terphenyl-d14 (Surr)78 12/06/22 18:15 12/07/22 23:24 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.02 4.01 mg/Kg ☼12/12/22 09:22 12/12/22 17:58 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)78 65-125 12/12/22 09:22 12/12/22 17:58 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
5.90 J 10.2 3.31 mg/Kg ☼12/07/22 18:30 12/08/22 20:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 62 15-139 12/07/22 18:30 12/08/22 20:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-10Client Sample ID: P11-25
Matrix: SolidDate Collected: 11/28/22 14:40
Percent Solids: 74.6Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00648 0.00169 mg/Kg ☼12/02/22 12:11 12/08/22 17:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1,1-Trichloroethane
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1,2,2-Tetrachloroethane
0.00648 0.00376 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00648 0.00194 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1,2-Trichloroethane
0.00648 0.00376 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1-Dichloroethane
0.00648 0.00467 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1-Dichloroethene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,1-Dichloropropene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2,3-Trichlorobenzene
0.00648 0.00233 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2,3-Trichloropropane
0.00648 0.00324 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2,4-Trichlorobenzene
0.00648 0.00324 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2,4-Trimethylbenzene
0.0130 0.00207 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2-Dibromo-3-Chloropropane
0.00648 0.00220 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2-Dichlorobenzene
0.00648 0.00298 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2-Dichloroethane
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,2-Dichloropropane
0.00648 0.00311 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,3,5-Trimethylbenzene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,3-Dichlorobenzene
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,3-Dichloropropane
0.00648 0.00233 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND1,4-Dichlorobenzene
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND2,2-Dichloropropane
0.0324 0.0119 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.5482-Butanone (MEK)
0.00648 0.00298 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND2-Chlorotoluene
0.0324 0.0246 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.05842-Hexanone
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND4-Chlorotoluene
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼ND4-Isopropyltoluene
0.0324 0.0233 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.0274 J4-Methyl-2-pentanone (MIBK)
0.0648 0.0143 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼1.14Acetone
0.00648 0.00311 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.00489 JBenzene
0.00648 0.00220 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDBromobenzene
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDBromoform
0.00648 0.00311 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDBromomethane
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDCarbon disulfide
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDCarbon tetrachloride
0.00648 0.00181 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChlorobenzene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChlorobromomethane
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChlorodibromomethane
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChloroethane
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChloroform
0.00648 0.00311 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDChloromethane
0.00648 0.00376 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDcis-1,2-Dichloroethene
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDcis-1,3-Dichloropropene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDDibromomethane
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDDichlorobromomethane
0.0130 0.0130 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDEthyl acetate
0.00648 0.00272 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDEthylbenzene
0.00648 0.00220 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDEthylene Dibromide
0.00648 0.00531 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDHexachlorobutadiene
0.00648 0.00220 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-10Client Sample ID: P11-25
Matrix: SolidDate Collected: 11/28/22 14:40
Percent Solids: 74.6Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
0.00233 J 0.00648 0.00220 mg/Kg ☼12/02/22 12:11 12/08/22 17:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0130 0.00194 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDIsopropyl ether
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDIsopropylbenzene
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDMethyl tert-butyl ether
0.0130 0.0104 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDMethylene Chloride
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.00934m-Xylene & p-Xylene
0.00648 0.00402 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDNaphthalene
0.00648 0.00246 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDn-Butylbenzene
0.00648 0.00557 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDn-Heptane
0.00648 0.00285 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDN-Propylbenzene
0.00648 0.00298 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.00513 Jo-Xylene
0.00648 0.00259 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDsec-Butylbenzene
0.00648 0.00246 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDStyrene
0.00648 0.00324 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDtert-Butylbenzene
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDTetrachloroethene
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.0187Toluene
0.00648 0.00298 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDtrans-1,2-Dichloroethene
0.00648 0.00337 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDtrans-1,3-Dichloropropene
0.0130 0.00311 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDtrans-1,4-Dichloro-2-butene
0.00648 0.00233 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDTrichloroethene
0.00648 0.00402 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDTrichlorofluoromethane
0.0130 0.00713 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDVinyl acetate
0.00648 0.00363 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼NDVinyl chloride
0.0130 0.00467 mg/Kg 12/02/22 12:11 12/08/22 17:15 1☼0.0145Xylenes, Total
1,2-Dichloroethane-d4 (Surr)100 65-130 12/02/22 12:11 12/08/22 17:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 17:15 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 17:15 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 17:15 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.22 2.22 mg/Kg ☼12/06/22 18:15 12/07/22 23:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.431 0.0457 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4,5-Trichlorophenol
0.431 0.0379 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4,6-Trichlorophenol
0.431 0.0457 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4-Dichlorophenol
0.431 0.0575 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4-Dimethylphenol
2.22 1.08 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4-Dinitrophenol
0.431 0.0640 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,4-Dinitrotoluene
0.431 0.0549 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2,6-Dinitrotoluene
0.431 0.0457 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Chloronaphthalene
0.431 0.0523 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Chlorophenol
0.431 0.0497 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Methylnaphthalene
0.431 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Methylphenol
2.22 0.0588 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Nitroaniline
0.431 0.0536 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND2-Nitrophenol
0.431 0.0562 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND3 & 4 Methylphenol
0.863 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND3,3'-Dichlorobenzidine
2.22 0.0601 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-10Client Sample ID: P11-25
Matrix: SolidDate Collected: 11/28/22 14:40
Percent Solids: 74.6Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.22 0.222 mg/Kg ☼12/06/22 18:15 12/07/22 23:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.431 0.0470 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Bromophenyl phenyl ether
0.431 0.0457 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Chloro-3-methylphenol
0.863 0.0680 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Chloroaniline
0.431 0.0575 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Chlorophenyl phenyl ether
2.22 0.0640 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Nitroaniline
2.22 0.431 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼ND4-Nitrophenol
0.431 0.0536 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDAcenaphthene
0.431 0.0470 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDAcenaphthylene
0.431 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDAcetophenone
0.431 0.0327 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDAnthracene
0.431 0.0301 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDAtrazine
0.431 0.0758 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzaldehyde
0.431 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzo[a]anthracene
0.431 0.0680 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzo[a]pyrene
0.431 0.0497 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzo[b]fluoranthene
0.431 0.0288 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzo[g,h,i]perylene
0.431 0.0849 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBenzo[k]fluoranthene
0.431 0.0392 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDbis (2-chloroisopropyl) ether
0.431 0.0510 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBis(2-chloroethoxy)methane
0.431 0.0588 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBis(2-chloroethyl)ether
0.431 0.0379 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDBis(2-ethylhexyl) phthalate
0.431 0.0340 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDButyl benzyl phthalate
0.431 0.0863 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDCaprolactam
0.431 0.0392 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDCarbazole
0.431 0.0274 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDChrysene
0.431 0.0510 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDibenz(a,h)anthracene
0.431 0.0431 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDibenzofuran
0.431 0.0484 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDiethyl phthalate
0.431 0.0444 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDimethyl phthalate
0.431 0.0392 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDi-n-butyl phthalate
0.431 0.0379 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDDi-n-octyl phthalate
0.431 0.0418 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDFluoranthene
0.431 0.0470 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDFluorene
0.431 0.0510 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDHexachlorobenzene
0.431 0.0470 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDHexachlorobutadiene
0.431 0.0536 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDHexachlorocyclopentadiene
0.431 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDHexachloroethane
0.431 0.0366 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDIndeno[1,2,3-cd]pyrene
0.431 0.0431 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDIsophorone
0.431 0.0392 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDNaphthalene
0.431 0.0340 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDNitrobenzene
0.431 0.0418 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDN-Nitrosodi-n-propylamine
0.431 0.0431 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDN-Nitrosodiphenylamine
2.22 0.431 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDPentachlorophenol
0.431 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDPhenanthrene
0.431 0.0444 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDPhenol
0.431 0.0353 mg/Kg 12/06/22 18:15 12/07/22 23:46 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-10Client Sample ID: P11-25
Matrix: SolidDate Collected: 11/28/22 14:40
Percent Solids: 74.6Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)84 21-132 12/06/22 18:15 12/07/22 23:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)70 12/06/22 18:15 12/07/22 23:46 125-130
2-Fluorophenol (Surr)57 12/06/22 18:15 12/07/22 23:46 118-130
Nitrobenzene-d5 (Surr)65 12/06/22 18:15 12/07/22 23:46 119-130
Phenol-d5 (Surr)59 12/06/22 18:15 12/07/22 23:46 121-130
Terphenyl-d14 (Surr)83 12/06/22 18:15 12/07/22 23:46 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 7.91 3.96 mg/Kg ☼12/12/22 09:22 12/12/22 18:29 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)74 65-125 12/12/22 09:22 12/12/22 18:29 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
4.38 J 10.6 3.44 mg/Kg ☼12/07/22 18:30 12/08/22 21:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 62 15-139 12/07/22 18:30 12/08/22 21:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-11Client Sample ID: P9-16
Matrix: SolidDate Collected: 11/28/22 15:20
Percent Solids: 81.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00627 0.00163 mg/Kg ☼12/02/22 12:11 12/08/22 17:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1,1-Trichloroethane
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1,2,2-Tetrachloroethane
0.00627 0.00364 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00627 0.00188 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1,2-Trichloroethane
0.00627 0.00364 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1-Dichloroethane
0.00627 0.00451 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1-Dichloroethene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,1-Dichloropropene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2,3-Trichlorobenzene
0.00627 0.00226 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2,3-Trichloropropane
0.00627 0.00313 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2,4-Trichlorobenzene
0.00627 0.00313 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2,4-Trimethylbenzene
0.0125 0.00201 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2-Dibromo-3-Chloropropane
0.00627 0.00213 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2-Dichlorobenzene
0.00627 0.00288 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2-Dichloroethane
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,2-Dichloropropane
0.00627 0.00301 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,3,5-Trimethylbenzene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,3-Dichlorobenzene
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,3-Dichloropropane
0.00627 0.00226 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND1,4-Dichlorobenzene
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND2,2-Dichloropropane
0.0313 0.0115 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼0.03412-Butanone (MEK)
0.00627 0.00288 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND2-Chlorotoluene
0.0313 0.0238 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND2-Hexanone
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND4-Chlorotoluene
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND4-Isopropyltoluene
0.0313 0.0226 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼ND4-Methyl-2-pentanone (MIBK)
0.0627 0.0138 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼0.325Acetone
0.00627 0.00301 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDBenzene
0.00627 0.00213 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDBromobenzene
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDBromoform
0.00627 0.00301 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDBromomethane
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDCarbon disulfide
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDCarbon tetrachloride
0.00627 0.00176 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChlorobenzene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChlorobromomethane
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChlorodibromomethane
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChloroethane
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChloroform
0.00627 0.00301 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDChloromethane
0.00627 0.00364 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDcis-1,2-Dichloroethene
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDcis-1,3-Dichloropropene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDDibromomethane
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDDichlorobromomethane
0.0125 0.0125 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDEthyl acetate
0.00627 0.00263 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDEthylbenzene
0.00627 0.00213 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDEthylene Dibromide
0.00627 0.00514 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDHexachlorobutadiene
0.00627 0.00213 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-11Client Sample ID: P9-16
Matrix: SolidDate Collected: 11/28/22 15:20
Percent Solids: 81.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00627 0.00213 mg/Kg ☼12/02/22 12:11 12/08/22 17:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0125 0.00188 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDIsopropyl ether
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDIsopropylbenzene
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDMethyl tert-butyl ether
0.0125 0.0100 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDMethylene Chloride
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDm-Xylene & p-Xylene
0.00627 0.00389 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDNaphthalene
0.00627 0.00238 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDn-Butylbenzene
0.00627 0.00539 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDn-Heptane
0.00627 0.00276 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDN-Propylbenzene
0.00627 0.00288 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDo-Xylene
0.00627 0.00251 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDsec-Butylbenzene
0.00627 0.00238 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDStyrene
0.00627 0.00313 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDtert-Butylbenzene
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDTetrachloroethene
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDToluene
0.00627 0.00288 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDtrans-1,2-Dichloroethene
0.00627 0.00326 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDtrans-1,3-Dichloropropene
0.0125 0.00301 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDtrans-1,4-Dichloro-2-butene
0.00627 0.00226 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDTrichloroethene
0.00627 0.00389 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDTrichlorofluoromethane
0.0125 0.00690 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDVinyl acetate
0.00627 0.00351 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDVinyl chloride
0.0125 0.00451 mg/Kg 12/02/22 12:11 12/08/22 17:39 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 17:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 17:39 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 17:39 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 17:39 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.00 2.00 mg/Kg ☼12/06/22 18:15 12/08/22 00:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.389 0.0412 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4,5-Trichlorophenol
0.389 0.0341 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4,6-Trichlorophenol
0.389 0.0412 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4-Dichlorophenol
0.389 0.0518 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4-Dimethylphenol
2.00 0.977 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4-Dinitrophenol
0.389 0.0577 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,4-Dinitrotoluene
0.389 0.0495 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2,6-Dinitrotoluene
0.389 0.0412 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Chloronaphthalene
0.389 0.0471 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Chlorophenol
0.389 0.0447 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Methylnaphthalene
0.389 0.0318 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Methylphenol
2.00 0.0530 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Nitroaniline
0.389 0.0483 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND2-Nitrophenol
0.389 0.0506 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND3 & 4 Methylphenol
0.777 0.0330 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND3,3'-Dichlorobenzidine
2.00 0.0542 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-11Client Sample ID: P9-16
Matrix: SolidDate Collected: 11/28/22 15:20
Percent Solids: 81.8Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.00 0.200 mg/Kg ☼12/06/22 18:15 12/08/22 00:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.389 0.0424 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Bromophenyl phenyl ether
0.389 0.0412 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Chloro-3-methylphenol
0.777 0.0612 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Chloroaniline
0.389 0.0518 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Chlorophenyl phenyl ether
2.00 0.0577 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Nitroaniline
2.00 0.389 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼ND4-Nitrophenol
0.389 0.0483 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDAcenaphthene
0.389 0.0424 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDAcenaphthylene
0.389 0.0330 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDAcetophenone
0.389 0.0294 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDAnthracene
0.389 0.0271 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDAtrazine
0.389 0.0683 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzaldehyde
0.389 0.0318 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzo[a]anthracene
0.389 0.0612 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzo[a]pyrene
0.389 0.0447 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzo[b]fluoranthene
0.389 0.0259 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzo[g,h,i]perylene
0.389 0.0765 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBenzo[k]fluoranthene
0.389 0.0353 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDbis (2-chloroisopropyl) ether
0.389 0.0459 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBis(2-chloroethoxy)methane
0.389 0.0530 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBis(2-chloroethyl)ether
0.389 0.0341 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDBis(2-ethylhexyl) phthalate
0.389 0.0306 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDButyl benzyl phthalate
0.389 0.0777 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDCaprolactam
0.389 0.0353 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDCarbazole
0.389 0.0247 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDChrysene
0.389 0.0459 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDibenz(a,h)anthracene
0.389 0.0389 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDibenzofuran
0.389 0.0436 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDiethyl phthalate
0.389 0.0400 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDimethyl phthalate
0.389 0.0353 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDi-n-butyl phthalate
0.389 0.0341 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDDi-n-octyl phthalate
0.389 0.0377 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDFluoranthene
0.389 0.0424 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDFluorene
0.389 0.0459 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDHexachlorobenzene
0.389 0.0424 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDHexachlorobutadiene
0.389 0.0483 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDHexachlorocyclopentadiene
0.389 0.0330 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDHexachloroethane
0.389 0.0330 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDIndeno[1,2,3-cd]pyrene
0.389 0.0389 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDIsophorone
0.389 0.0353 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDNaphthalene
0.389 0.0306 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDNitrobenzene
0.389 0.0377 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDN-Nitrosodi-n-propylamine
0.389 0.0389 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDN-Nitrosodiphenylamine
2.00 0.389 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDPentachlorophenol
0.389 0.0318 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDPhenanthrene
0.389 0.0400 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDPhenol
0.389 0.0318 mg/Kg 12/06/22 18:15 12/08/22 00:07 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-11Client Sample ID: P9-16
Matrix: SolidDate Collected: 11/28/22 15:20
Percent Solids: 81.8Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)91 21-132 12/06/22 18:15 12/08/22 00:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)68 12/06/22 18:15 12/08/22 00:07 125-130
2-Fluorophenol (Surr)59 12/06/22 18:15 12/08/22 00:07 118-130
Nitrobenzene-d5 (Surr)60 12/06/22 18:15 12/08/22 00:07 119-130
Phenol-d5 (Surr)59 12/06/22 18:15 12/08/22 00:07 121-130
Terphenyl-d14 (Surr)79 12/06/22 18:15 12/08/22 00:07 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 7.17 3.58 mg/Kg ☼12/12/22 13:20 12/12/22 15:40 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)99 65-125 12/12/22 13:20 12/12/22 15:40 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
ND 9.66 3.14 mg/Kg ☼12/07/22 18:30 12/08/22 21:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 56 15-139 12/07/22 18:30 12/08/22 21:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-12Client Sample ID: P10-25
Matrix: SolidDate Collected: 11/28/22 15:30
Percent Solids: 81.0Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00617 0.00160 mg/Kg ☼12/02/22 12:11 12/08/22 18:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1,1-Trichloroethane
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1,2,2-Tetrachloroethane
0.00617 0.00358 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00617 0.00185 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1,2-Trichloroethane
0.00617 0.00358 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1-Dichloroethane
0.00617 0.00444 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1-Dichloroethene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,1-Dichloropropene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2,3-Trichlorobenzene
0.00617 0.00222 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2,3-Trichloropropane
0.00617 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2,4-Trichlorobenzene
0.00617 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2,4-Trimethylbenzene
0.0123 0.00197 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2-Dibromo-3-Chloropropane
0.00617 0.00210 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2-Dichlorobenzene
0.00617 0.00284 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2-Dichloroethane
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,2-Dichloropropane
0.00617 0.00296 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,3,5-Trimethylbenzene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,3-Dichlorobenzene
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,3-Dichloropropane
0.00617 0.00222 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND1,4-Dichlorobenzene
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND2,2-Dichloropropane
0.0308 0.0113 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.03982-Butanone (MEK)
0.00617 0.00284 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND2-Chlorotoluene
0.0308 0.0234 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND2-Hexanone
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND4-Chlorotoluene
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND4-Isopropyltoluene
0.0308 0.0222 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼ND4-Methyl-2-pentanone (MIBK)
0.0617 0.0136 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.0697Acetone
0.00617 0.00296 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.00788Benzene
0.00617 0.00210 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDBromobenzene
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDBromoform
0.00617 0.00296 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDBromomethane
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDCarbon disulfide
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDCarbon tetrachloride
0.00617 0.00173 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChlorobenzene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChlorobromomethane
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChlorodibromomethane
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChloroethane
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChloroform
0.00617 0.00296 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDChloromethane
0.00617 0.00358 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDcis-1,2-Dichloroethene
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDcis-1,3-Dichloropropene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDDibromomethane
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDDichlorobromomethane
0.0123 0.0123 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDEthyl acetate
0.00617 0.00259 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.00285 JEthylbenzene
0.00617 0.00210 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDEthylene Dibromide
0.00617 0.00506 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDHexachlorobutadiene
0.00617 0.00210 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.00544 JHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-12Client Sample ID: P10-25
Matrix: SolidDate Collected: 11/28/22 15:30
Percent Solids: 81.0Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00617 0.00210 mg/Kg ☼12/02/22 12:11 12/08/22 18:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0123 0.00185 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDIsopropyl ether
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDIsopropylbenzene
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDMethyl tert-butyl ether
0.0123 0.00986 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDMethylene Chloride
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.0121m-Xylene & p-Xylene
0.00617 0.00382 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDNaphthalene
0.00617 0.00234 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDn-Butylbenzene
0.00617 0.00530 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDn-Heptane
0.00617 0.00271 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDN-Propylbenzene
0.00617 0.00284 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.00710o-Xylene
0.00617 0.00247 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDsec-Butylbenzene
0.00617 0.00234 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDStyrene
0.00617 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDtert-Butylbenzene
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDTetrachloroethene
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.0337Toluene
0.00617 0.00284 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDtrans-1,2-Dichloroethene
0.00617 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDtrans-1,3-Dichloropropene
0.0123 0.00296 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDtrans-1,4-Dichloro-2-butene
0.00617 0.00222 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDTrichloroethene
0.00617 0.00382 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDTrichlorofluoromethane
0.0123 0.00678 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDVinyl acetate
0.00617 0.00345 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼NDVinyl chloride
0.0123 0.00444 mg/Kg 12/02/22 12:11 12/08/22 18:03 1☼0.0192Xylenes, Total
1,2-Dichloroethane-d4 (Surr)99 65-130 12/02/22 12:11 12/08/22 18:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/08/22 18:03 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/08/22 18:03 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 18:03 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.01 2.01 mg/Kg ☼12/06/22 18:15 12/08/22 00:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.391 0.0415 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4,5-Trichlorophenol
0.391 0.0344 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4,6-Trichlorophenol
0.391 0.0415 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4-Dichlorophenol
0.391 0.0521 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4-Dimethylphenol
2.01 0.983 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4-Dinitrophenol
0.391 0.0581 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,4-Dinitrotoluene
0.391 0.0498 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2,6-Dinitrotoluene
0.391 0.0415 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Chloronaphthalene
0.391 0.0474 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Chlorophenol
0.391 0.0450 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Methylnaphthalene
0.391 0.0320 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Methylphenol
2.01 0.0533 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Nitroaniline
0.391 0.0486 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND2-Nitrophenol
0.391 0.0509 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND3 & 4 Methylphenol
0.782 0.0332 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND3,3'-Dichlorobenzidine
2.01 0.0545 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-12Client Sample ID: P10-25
Matrix: SolidDate Collected: 11/28/22 15:30
Percent Solids: 81.0Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.01 0.201 mg/Kg ☼12/06/22 18:15 12/08/22 00:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.391 0.0427 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Bromophenyl phenyl ether
0.391 0.0415 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Chloro-3-methylphenol
0.782 0.0616 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Chloroaniline
0.391 0.0521 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Chlorophenyl phenyl ether
2.01 0.0581 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Nitroaniline
2.01 0.391 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼ND4-Nitrophenol
0.391 0.0486 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDAcenaphthene
0.391 0.0427 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDAcenaphthylene
0.391 0.0332 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDAcetophenone
0.391 0.0296 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDAnthracene
0.391 0.0272 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDAtrazine
0.391 0.0687 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzaldehyde
0.391 0.0320 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzo[a]anthracene
0.391 0.0616 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzo[a]pyrene
0.391 0.0450 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzo[b]fluoranthene
0.391 0.0261 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzo[g,h,i]perylene
0.391 0.0770 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBenzo[k]fluoranthene
0.391 0.0355 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDbis (2-chloroisopropyl) ether
0.391 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBis(2-chloroethoxy)methane
0.391 0.0533 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBis(2-chloroethyl)ether
0.391 0.0344 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDBis(2-ethylhexyl) phthalate
0.391 0.0308 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDButyl benzyl phthalate
0.391 0.0782 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDCaprolactam
0.391 0.0355 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDCarbazole
0.391 0.0249 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDChrysene
0.391 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDibenz(a,h)anthracene
0.391 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDibenzofuran
0.391 0.0438 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDiethyl phthalate
0.391 0.0403 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDimethyl phthalate
0.391 0.0355 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDi-n-butyl phthalate
0.391 0.0344 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDDi-n-octyl phthalate
0.391 0.0379 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDFluoranthene
0.391 0.0427 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDFluorene
0.391 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDHexachlorobenzene
0.391 0.0427 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDHexachlorobutadiene
0.391 0.0486 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDHexachlorocyclopentadiene
0.391 0.0332 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDHexachloroethane
0.391 0.0332 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDIndeno[1,2,3-cd]pyrene
0.391 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDIsophorone
0.391 0.0355 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDNaphthalene
0.391 0.0308 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDNitrobenzene
0.391 0.0379 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDN-Nitrosodi-n-propylamine
0.391 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDN-Nitrosodiphenylamine
2.01 0.391 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDPentachlorophenol
0.391 0.0320 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDPhenanthrene
0.391 0.0403 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDPhenol
0.391 0.0320 mg/Kg 12/06/22 18:15 12/08/22 00:29 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-12Client Sample ID: P10-25
Matrix: SolidDate Collected: 11/28/22 15:30
Percent Solids: 81.0Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)92 21-132 12/06/22 18:15 12/08/22 00:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)71 12/06/22 18:15 12/08/22 00:29 125-130
2-Fluorophenol (Surr)58 12/06/22 18:15 12/08/22 00:29 118-130
Nitrobenzene-d5 (Surr)62 12/06/22 18:15 12/08/22 00:29 119-130
Phenol-d5 (Surr)61 12/06/22 18:15 12/08/22 00:29 121-130
Terphenyl-d14 (Surr)86 12/06/22 18:15 12/08/22 00:29 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.03 4.02 mg/Kg ☼12/12/22 13:20 12/12/22 16:00 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)97 65-125 12/12/22 13:20 12/12/22 16:00 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
5.91 J 9.70 3.15 mg/Kg ☼12/07/22 18:30 12/08/22 21:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 64 15-139 12/07/22 18:30 12/08/22 21:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-13Client Sample ID: P8-20
Matrix: SolidDate Collected: 11/28/22 16:05
Percent Solids: 75.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00642 0.00167 mg/Kg ☼12/02/22 12:11 12/08/22 18:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1,1-Trichloroethane
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1,2,2-Tetrachloroethane
0.00642 0.00372 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00642 0.00193 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1,2-Trichloroethane
0.00642 0.00372 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1-Dichloroethane
0.00642 0.00462 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1-Dichloroethene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,1-Dichloropropene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2,3-Trichlorobenzene
0.00642 0.00231 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2,3-Trichloropropane
0.00642 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2,4-Trichlorobenzene
0.00642 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2,4-Trimethylbenzene
0.0128 0.00205 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2-Dibromo-3-Chloropropane
0.00642 0.00218 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2-Dichlorobenzene
0.00642 0.00295 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2-Dichloroethane
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,2-Dichloropropane
0.00642 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,3,5-Trimethylbenzene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,3-Dichlorobenzene
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,3-Dichloropropane
0.00642 0.00231 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND1,4-Dichlorobenzene
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND2,2-Dichloropropane
0.0321 0.0118 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼0.2142-Butanone (MEK)
0.00642 0.00295 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND2-Chlorotoluene
0.0321 0.0244 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND2-Hexanone
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND4-Chlorotoluene
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND4-Isopropyltoluene
0.0321 0.0231 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼ND4-Methyl-2-pentanone (MIBK)
0.0642 0.0141 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼0.371Acetone
0.00642 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDBenzene
0.00642 0.00218 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDBromobenzene
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDBromoform
0.00642 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDBromomethane
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDCarbon disulfide
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDCarbon tetrachloride
0.00642 0.00180 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChlorobenzene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChlorobromomethane
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChlorodibromomethane
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChloroethane
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChloroform
0.00642 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDChloromethane
0.00642 0.00372 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDcis-1,2-Dichloroethene
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDcis-1,3-Dichloropropene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDDibromomethane
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDDichlorobromomethane
0.0128 0.0128 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDEthyl acetate
0.00642 0.00270 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDEthylbenzene
0.00642 0.00218 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDEthylene Dibromide
0.00642 0.00526 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDHexachlorobutadiene
0.00642 0.00218 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-13Client Sample ID: P8-20
Matrix: SolidDate Collected: 11/28/22 16:05
Percent Solids: 75.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
0.00267 J 0.00642 0.00218 mg/Kg ☼12/02/22 12:11 12/08/22 18:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0128 0.00193 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDIsopropyl ether
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDIsopropylbenzene
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDMethyl tert-butyl ether
0.0128 0.0103 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDMethylene Chloride
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼0.00327 Jm-Xylene & p-Xylene
0.00642 0.00398 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDNaphthalene
0.00642 0.00244 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDn-Butylbenzene
0.00642 0.00552 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDn-Heptane
0.00642 0.00282 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDN-Propylbenzene
0.00642 0.00295 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDo-Xylene
0.00642 0.00257 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDsec-Butylbenzene
0.00642 0.00244 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDStyrene
0.00642 0.00321 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDtert-Butylbenzene
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDTetrachloroethene
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼0.00513 JToluene
0.00642 0.00295 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDtrans-1,2-Dichloroethene
0.00642 0.00334 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDtrans-1,3-Dichloropropene
0.0128 0.00308 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDtrans-1,4-Dichloro-2-butene
0.00642 0.00231 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDTrichloroethene
0.00642 0.00398 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDTrichlorofluoromethane
0.0128 0.00706 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDVinyl acetate
0.00642 0.00360 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDVinyl chloride
0.0128 0.00462 mg/Kg 12/02/22 12:11 12/08/22 18:27 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 18:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 12/02/22 12:11 12/08/22 18:27 165-130
Dibromofluoromethane (Surr)107 12/02/22 12:11 12/08/22 18:27 165-130
Toluene-d8 (Surr)105 12/02/22 12:11 12/08/22 18:27 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.22 2.22 mg/Kg ☼12/06/22 18:15 12/08/22 00:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.430 0.0456 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4,5-Trichlorophenol
0.430 0.0378 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4,6-Trichlorophenol
0.430 0.0456 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4-Dichlorophenol
0.430 0.0573 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4-Dimethylphenol
2.22 1.08 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4-Dinitrophenol
0.430 0.0639 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,4-Dinitrotoluene
0.430 0.0547 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2,6-Dinitrotoluene
0.430 0.0456 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Chloronaphthalene
0.430 0.0521 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Chlorophenol
0.430 0.0495 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Methylnaphthalene
0.430 0.0352 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Methylphenol
2.22 0.0587 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Nitroaniline
0.430 0.0534 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND2-Nitrophenol
0.430 0.0560 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND3 & 4 Methylphenol
0.860 0.0365 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND3,3'-Dichlorobenzidine
2.22 0.0600 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-13Client Sample ID: P8-20
Matrix: SolidDate Collected: 11/28/22 16:05
Percent Solids: 75.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.22 0.222 mg/Kg ☼12/06/22 18:15 12/08/22 00:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.430 0.0469 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Bromophenyl phenyl ether
0.430 0.0456 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Chloro-3-methylphenol
0.860 0.0678 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Chloroaniline
0.430 0.0573 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Chlorophenyl phenyl ether
2.22 0.0639 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Nitroaniline
2.22 0.430 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼ND4-Nitrophenol
0.430 0.0534 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDAcenaphthene
0.430 0.0469 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDAcenaphthylene
0.430 0.0365 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDAcetophenone
0.430 0.0326 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDAnthracene
0.430 0.0300 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDAtrazine
0.430 0.0756 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzaldehyde
0.430 0.0352 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzo[a]anthracene
0.430 0.0678 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzo[a]pyrene
0.430 0.0495 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzo[b]fluoranthene
0.430 0.0287 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzo[g,h,i]perylene
0.430 0.0847 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBenzo[k]fluoranthene
0.430 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDbis (2-chloroisopropyl) ether
0.430 0.0508 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBis(2-chloroethoxy)methane
0.430 0.0587 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBis(2-chloroethyl)ether
0.430 0.0378 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDBis(2-ethylhexyl) phthalate
0.430 0.0339 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDButyl benzyl phthalate
0.430 0.0860 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDCaprolactam
0.430 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDCarbazole
0.430 0.0274 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDChrysene
0.430 0.0508 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDibenz(a,h)anthracene
0.430 0.0430 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDibenzofuran
0.430 0.0482 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDiethyl phthalate
0.430 0.0443 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDimethyl phthalate
0.430 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDi-n-butyl phthalate
0.430 0.0378 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDDi-n-octyl phthalate
0.430 0.0417 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDFluoranthene
0.430 0.0469 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDFluorene
0.430 0.0508 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDHexachlorobenzene
0.430 0.0469 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDHexachlorobutadiene
0.430 0.0534 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDHexachlorocyclopentadiene
0.430 0.0365 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDHexachloroethane
0.430 0.0365 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDIndeno[1,2,3-cd]pyrene
0.430 0.0430 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDIsophorone
0.430 0.0391 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDNaphthalene
0.430 0.0339 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDNitrobenzene
0.430 0.0417 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDN-Nitrosodi-n-propylamine
0.430 0.0430 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDN-Nitrosodiphenylamine
2.22 0.430 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDPentachlorophenol
0.430 0.0352 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDPhenanthrene
0.430 0.0443 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDPhenol
0.430 0.0352 mg/Kg 12/06/22 18:15 12/08/22 00:51 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-13Client Sample ID: P8-20
Matrix: SolidDate Collected: 11/28/22 16:05
Percent Solids: 75.7Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)86 21-132 12/06/22 18:15 12/08/22 00:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 12/06/22 18:15 12/08/22 00:51 125-130
2-Fluorophenol (Surr)56 12/06/22 18:15 12/08/22 00:51 118-130
Nitrobenzene-d5 (Surr)61 12/06/22 18:15 12/08/22 00:51 119-130
Phenol-d5 (Surr)57 12/06/22 18:15 12/08/22 00:51 121-130
Terphenyl-d14 (Surr)80 12/06/22 18:15 12/08/22 00:51 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 7.72 3.86 mg/Kg ☼12/12/22 13:20 12/12/22 16:26 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)98 65-125 12/12/22 13:20 12/12/22 16:26 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
3.60 J 10.4 3.38 mg/Kg ☼12/07/22 18:30 12/08/22 21:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 64 15-139 12/07/22 18:30 12/08/22 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-14Client Sample ID: P12-20
Matrix: SolidDate Collected: 11/28/22 16:20
Percent Solids: 78.5Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00693 0.00180 mg/Kg ☼12/02/22 12:11 12/08/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1,1-Trichloroethane
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1,2,2-Tetrachloroethane
0.00693 0.00402 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00693 0.00208 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1,2-Trichloroethane
0.00693 0.00402 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1-Dichloroethane
0.00693 0.00499 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1-Dichloroethene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,1-Dichloropropene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2,3-Trichlorobenzene
0.00693 0.00250 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2,3-Trichloropropane
0.00693 0.00347 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2,4-Trichlorobenzene
0.00693 0.00347 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2,4-Trimethylbenzene
0.0139 0.00222 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2-Dibromo-3-Chloropropane
0.00693 0.00236 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2-Dichlorobenzene
0.00693 0.00319 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2-Dichloroethane
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,2-Dichloropropane
0.00693 0.00333 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,3,5-Trimethylbenzene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,3-Dichlorobenzene
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,3-Dichloropropane
0.00693 0.00250 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND1,4-Dichlorobenzene
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND2,2-Dichloropropane
0.0347 0.0128 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼0.3002-Butanone (MEK)
0.00693 0.00319 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND2-Chlorotoluene
0.0347 0.0263 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND2-Hexanone
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND4-Chlorotoluene
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND4-Isopropyltoluene
0.0347 0.0250 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼ND4-Methyl-2-pentanone (MIBK)
0.0693 0.0153 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼0.219Acetone
0.00693 0.00333 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDBenzene
0.00693 0.00236 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDBromobenzene
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDBromoform
0.00693 0.00333 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDBromomethane
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDCarbon disulfide
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDCarbon tetrachloride
0.00693 0.00194 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChlorobenzene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChlorobromomethane
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChlorodibromomethane
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChloroethane
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChloroform
0.00693 0.00333 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDChloromethane
0.00693 0.00402 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDcis-1,2-Dichloroethene
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDcis-1,3-Dichloropropene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDDibromomethane
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDDichlorobromomethane
0.0139 0.0139 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDEthyl acetate
0.00693 0.00291 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDEthylbenzene
0.00693 0.00236 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDEthylene Dibromide
0.00693 0.00569 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDHexachlorobutadiene
0.00693 0.00236 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-14Client Sample ID: P12-20
Matrix: SolidDate Collected: 11/28/22 16:20
Percent Solids: 78.5Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00693 0.00236 mg/Kg ☼12/02/22 12:11 12/08/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0139 0.00208 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDIsopropyl ether
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDIsopropylbenzene
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDMethyl tert-butyl ether
0.0139 0.0111 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDMethylene Chloride
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDm-Xylene & p-Xylene
0.00693 0.00430 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDNaphthalene
0.00693 0.00263 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDn-Butylbenzene
0.00693 0.00596 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDn-Heptane
0.00693 0.00305 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDN-Propylbenzene
0.00693 0.00319 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDo-Xylene
0.00693 0.00277 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDsec-Butylbenzene
0.00693 0.00263 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDStyrene
0.00693 0.00347 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDtert-Butylbenzene
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDTetrachloroethene
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDToluene
0.00693 0.00319 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDtrans-1,2-Dichloroethene
0.00693 0.00361 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDtrans-1,3-Dichloropropene
0.0139 0.00333 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDtrans-1,4-Dichloro-2-butene
0.00693 0.00250 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDTrichloroethene
0.00693 0.00430 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDTrichlorofluoromethane
0.0139 0.00763 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDVinyl acetate
0.00693 0.00388 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDVinyl chloride
0.0139 0.00499 mg/Kg 12/02/22 12:11 12/08/22 18:50 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 18:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 12/02/22 12:11 12/08/22 18:50 165-130
Dibromofluoromethane (Surr)105 12/02/22 12:11 12/08/22 18:50 165-130
Toluene-d8 (Surr)106 12/02/22 12:11 12/08/22 18:50 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.12 2.12 mg/Kg ☼12/06/22 18:15 12/08/22 00:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.411 0.0435 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4,5-Trichlorophenol
0.411 0.0361 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4,6-Trichlorophenol
0.411 0.0435 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4-Dichlorophenol
0.411 0.0547 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4-Dimethylphenol
2.12 1.03 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4-Dinitrophenol
0.411 0.0610 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,4-Dinitrotoluene
0.411 0.0523 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2,6-Dinitrotoluene
0.411 0.0435 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Chloronaphthalene
0.411 0.0498 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Chlorophenol
0.411 0.0473 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Methylnaphthalene
0.411 0.0336 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Methylphenol
2.12 0.0560 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Nitroaniline
0.411 0.0510 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND2-Nitrophenol
0.411 0.0535 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND3 & 4 Methylphenol
0.821 0.0348 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND3,3'-Dichlorobenzidine
2.12 0.0572 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-14Client Sample ID: P12-20
Matrix: SolidDate Collected: 11/28/22 16:20
Percent Solids: 78.5Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.12 0.212 mg/Kg ☼12/06/22 18:15 12/08/22 00:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.411 0.0448 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Bromophenyl phenyl ether
0.411 0.0435 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Chloro-3-methylphenol
0.821 0.0647 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Chloroaniline
0.411 0.0547 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Chlorophenyl phenyl ether
2.12 0.0610 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Nitroaniline
2.12 0.411 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼ND4-Nitrophenol
0.411 0.0510 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDAcenaphthene
0.411 0.0448 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDAcenaphthylene
0.411 0.0348 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDAcetophenone
0.411 0.0311 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDAnthracene
0.411 0.0286 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDAtrazine
0.411 0.0722 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzaldehyde
0.411 0.0336 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzo[a]anthracene
0.411 0.0647 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzo[a]pyrene
0.411 0.0473 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzo[b]fluoranthene
0.411 0.0274 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzo[g,h,i]perylene
0.411 0.0809 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBenzo[k]fluoranthene
0.411 0.0373 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDbis (2-chloroisopropyl) ether
0.411 0.0485 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBis(2-chloroethoxy)methane
0.411 0.0560 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBis(2-chloroethyl)ether
0.411 0.0361 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDBis(2-ethylhexyl) phthalate
0.411 0.0323 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDButyl benzyl phthalate
0.411 0.0821 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDCaprolactam
0.411 0.0373 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDCarbazole
0.411 0.0261 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDChrysene
0.411 0.0485 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDibenz(a,h)anthracene
0.411 0.0411 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDibenzofuran
0.411 0.0460 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDiethyl phthalate
0.411 0.0423 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDimethyl phthalate
0.411 0.0373 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDi-n-butyl phthalate
0.411 0.0361 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDDi-n-octyl phthalate
0.411 0.0398 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDFluoranthene
0.411 0.0448 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDFluorene
0.411 0.0485 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDHexachlorobenzene
0.411 0.0448 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDHexachlorobutadiene
0.411 0.0510 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDHexachlorocyclopentadiene
0.411 0.0348 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDHexachloroethane
0.411 0.0348 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDIndeno[1,2,3-cd]pyrene
0.411 0.0411 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDIsophorone
0.411 0.0373 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDNaphthalene
0.411 0.0323 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDNitrobenzene
0.411 0.0398 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDN-Nitrosodi-n-propylamine
0.411 0.0411 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDN-Nitrosodiphenylamine
2.12 0.411 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDPentachlorophenol
0.411 0.0336 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDPhenanthrene
0.411 0.0423 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDPhenol
0.411 0.0336 mg/Kg 12/06/22 18:15 12/08/22 00:34 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-14Client Sample ID: P12-20
Matrix: SolidDate Collected: 11/28/22 16:20
Percent Solids: 78.5Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)94 21-132 12/06/22 18:15 12/08/22 00:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)74 12/06/22 18:15 12/08/22 00:34 125-130
2-Fluorophenol (Surr)68 12/06/22 18:15 12/08/22 00:34 118-130
Nitrobenzene-d5 (Surr)66 12/06/22 18:15 12/08/22 00:34 119-130
Phenol-d5 (Surr)71 12/06/22 18:15 12/08/22 00:34 121-130
Terphenyl-d14 (Surr)92 12/06/22 18:15 12/08/22 00:34 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.53 4.26 mg/Kg ☼12/12/22 13:20 12/12/22 16:55 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)97 65-125 12/12/22 13:20 12/12/22 16:55 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
ND 10.1 3.27 mg/Kg ☼12/07/22 18:30 12/08/22 22:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 39 15-139 12/07/22 18:30 12/08/22 22:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-15Client Sample ID: P13-10
Matrix: SolidDate Collected: 11/28/22 16:36
Percent Solids: 71.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00707 0.00184 mg/Kg ☼12/02/22 12:11 12/08/22 19:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1,1-Trichloroethane
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1,2,2-Tetrachloroethane
0.00707 0.00410 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00707 0.00212 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1,2-Trichloroethane
0.00707 0.00410 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1-Dichloroethane
0.00707 0.00509 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1-Dichloroethene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,1-Dichloropropene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2,3-Trichlorobenzene
0.00707 0.00255 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2,3-Trichloropropane
0.00707 0.00354 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2,4-Trichlorobenzene
0.00707 0.00354 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2,4-Trimethylbenzene
0.0141 0.00226 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2-Dibromo-3-Chloropropane
0.00707 0.00240 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2-Dichlorobenzene
0.00707 0.00325 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2-Dichloroethane
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,2-Dichloropropane
0.00707 0.00339 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,3,5-Trimethylbenzene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,3-Dichlorobenzene
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,3-Dichloropropane
0.00707 0.00255 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND1,4-Dichlorobenzene
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND2,2-Dichloropropane
0.0354 0.0130 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND2-Butanone (MEK)
0.00707 0.00325 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND2-Chlorotoluene
0.0354 0.0269 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND2-Hexanone
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND4-Chlorotoluene
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND4-Isopropyltoluene
0.0354 0.0255 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼ND4-Methyl-2-pentanone (MIBK)
0.0707 0.0156 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼0.0580 JAcetone
0.00707 0.00339 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDBenzene
0.00707 0.00240 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDBromobenzene
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDBromoform
0.00707 0.00339 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDBromomethane
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDCarbon disulfide
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDCarbon tetrachloride
0.00707 0.00198 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChlorobenzene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChlorobromomethane
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChlorodibromomethane
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChloroethane
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChloroform
0.00707 0.00339 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDChloromethane
0.00707 0.00410 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDcis-1,2-Dichloroethene
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDcis-1,3-Dichloropropene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDDibromomethane
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDDichlorobromomethane
0.0141 0.0141 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDEthyl acetate
0.00707 0.00297 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDEthylbenzene
0.00707 0.00240 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDEthylene Dibromide
0.00707 0.00580 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDHexachlorobutadiene
0.00707 0.00240 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-15Client Sample ID: P13-10
Matrix: SolidDate Collected: 11/28/22 16:36
Percent Solids: 71.7Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00707 0.00240 mg/Kg ☼12/02/22 12:11 12/08/22 19:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0141 0.00212 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDIsopropyl ether
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDIsopropylbenzene
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDMethyl tert-butyl ether
0.0141 0.0113 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDMethylene Chloride
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDm-Xylene & p-Xylene
0.00707 0.00438 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDNaphthalene
0.00707 0.00269 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDn-Butylbenzene
0.00707 0.00608 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDn-Heptane
0.00707 0.00311 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDN-Propylbenzene
0.00707 0.00325 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDo-Xylene
0.00707 0.00283 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDsec-Butylbenzene
0.00707 0.00269 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDStyrene
0.00707 0.00354 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDtert-Butylbenzene
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDTetrachloroethene
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDToluene
0.00707 0.00325 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDtrans-1,2-Dichloroethene
0.00707 0.00368 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDtrans-1,3-Dichloropropene
0.0141 0.00339 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDtrans-1,4-Dichloro-2-butene
0.00707 0.00255 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDTrichloroethene
0.00707 0.00438 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDTrichlorofluoromethane
0.0141 0.00778 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDVinyl acetate
0.00707 0.00396 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDVinyl chloride
0.0141 0.00509 mg/Kg 12/02/22 12:11 12/08/22 19:14 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/08/22 19:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 12/02/22 12:11 12/08/22 19:14 165-130
Dibromofluoromethane (Surr)105 12/02/22 12:11 12/08/22 19:14 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/08/22 19:14 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.24 2.24 mg/Kg ☼12/06/22 18:15 12/08/22 00:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.436 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4,5-Trichlorophenol
0.436 0.0383 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4,6-Trichlorophenol
0.436 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4-Dichlorophenol
0.436 0.0581 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4-Dimethylphenol
2.24 1.10 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4-Dinitrophenol
0.436 0.0647 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,4-Dinitrotoluene
0.436 0.0554 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2,6-Dinitrotoluene
0.436 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Chloronaphthalene
0.436 0.0528 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Chlorophenol
0.436 0.0502 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Methylnaphthalene
0.436 0.0356 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Methylphenol
2.24 0.0594 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Nitroaniline
0.436 0.0541 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND2-Nitrophenol
0.436 0.0568 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND3 & 4 Methylphenol
0.871 0.0370 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND3,3'-Dichlorobenzidine
2.24 0.0607 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-15Client Sample ID: P13-10
Matrix: SolidDate Collected: 11/28/22 16:36
Percent Solids: 71.7Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.24 0.224 mg/Kg ☼12/06/22 18:15 12/08/22 00:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.436 0.0475 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Bromophenyl phenyl ether
0.436 0.0462 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Chloro-3-methylphenol
0.871 0.0686 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Chloroaniline
0.436 0.0581 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Chlorophenyl phenyl ether
2.24 0.0647 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Nitroaniline
2.24 0.436 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼ND4-Nitrophenol
0.436 0.0541 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDAcenaphthene
0.436 0.0475 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDAcenaphthylene
0.436 0.0370 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDAcetophenone
0.436 0.0330 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDAnthracene
0.436 0.0304 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDAtrazine
0.436 0.0766 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzaldehyde
0.436 0.0356 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzo[a]anthracene
0.436 0.0686 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzo[a]pyrene
0.436 0.0502 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzo[b]fluoranthene
0.436 0.0290 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzo[g,h,i]perylene
0.436 0.0858 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBenzo[k]fluoranthene
0.436 0.0396 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDbis (2-chloroisopropyl) ether
0.436 0.0515 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBis(2-chloroethoxy)methane
0.436 0.0594 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBis(2-chloroethyl)ether
0.436 0.0383 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDBis(2-ethylhexyl) phthalate
0.436 0.0343 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDButyl benzyl phthalate
0.436 0.0871 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDCaprolactam
0.436 0.0396 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDCarbazole
0.436 0.0277 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDChrysene
0.436 0.0515 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDibenz(a,h)anthracene
0.436 0.0436 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDibenzofuran
0.436 0.0488 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDiethyl phthalate
0.436 0.0449 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDimethyl phthalate
0.436 0.0396 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDi-n-butyl phthalate
0.436 0.0383 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDDi-n-octyl phthalate
0.436 0.0422 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDFluoranthene
0.436 0.0475 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDFluorene
0.436 0.0515 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDHexachlorobenzene
0.436 0.0475 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDHexachlorobutadiene
0.436 0.0541 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDHexachlorocyclopentadiene
0.436 0.0370 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDHexachloroethane
0.436 0.0370 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDIndeno[1,2,3-cd]pyrene
0.436 0.0436 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDIsophorone
0.436 0.0396 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDNaphthalene
0.436 0.0343 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDNitrobenzene
0.436 0.0422 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDN-Nitrosodi-n-propylamine
0.436 0.0436 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDN-Nitrosodiphenylamine
2.24 0.436 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDPentachlorophenol
0.436 0.0356 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDPhenanthrene
0.436 0.0449 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDPhenol
0.436 0.0356 mg/Kg 12/06/22 18:15 12/08/22 00:58 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-15Client Sample ID: P13-10
Matrix: SolidDate Collected: 11/28/22 16:36
Percent Solids: 71.7Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)52 21-132 12/06/22 18:15 12/08/22 00:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 12/06/22 18:15 12/08/22 00:58 125-130
2-Fluorophenol (Surr)45 12/06/22 18:15 12/08/22 00:58 118-130
Nitrobenzene-d5 (Surr)58 12/06/22 18:15 12/08/22 00:58 119-130
Phenol-d5 (Surr)53 12/06/22 18:15 12/08/22 00:58 121-130
Terphenyl-d14 (Surr)82 12/06/22 18:15 12/08/22 00:58 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 9.00 4.50 mg/Kg ☼12/12/22 13:20 12/12/22 17:20 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)97 65-125 12/12/22 13:20 12/12/22 17:20 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
16.6 10.8 3.53 mg/Kg ☼12/07/22 18:30 12/08/22 22:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 55 15-139 12/07/22 18:30 12/08/22 22:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-16Client Sample ID: P14-5
Matrix: SolidDate Collected: 11/29/22 08:25
Percent Solids: 79.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00669 0.00174 mg/Kg ☼12/02/22 12:11 12/08/22 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1,1-Trichloroethane
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1,2,2-Tetrachloroethane
0.00669 0.00388 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00669 0.00201 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1,2-Trichloroethane
0.00669 0.00388 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1-Dichloroethane
0.00669 0.00482 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1-Dichloroethene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,1-Dichloropropene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2,3-Trichlorobenzene
0.00669 0.00241 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2,3-Trichloropropane
0.00669 0.00335 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2,4-Trichlorobenzene
0.00669 0.00335 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2,4-Trimethylbenzene
0.0134 0.00214 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2-Dibromo-3-Chloropropane
0.00669 0.00228 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2-Dichlorobenzene
0.00669 0.00308 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2-Dichloroethane
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,2-Dichloropropane
0.00669 0.00321 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,3,5-Trimethylbenzene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,3-Dichlorobenzene
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,3-Dichloropropane
0.00669 0.00241 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND1,4-Dichlorobenzene
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND2,2-Dichloropropane
0.0335 0.0123 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND2-Butanone (MEK)
0.00669 0.00308 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND2-Chlorotoluene
0.0335 0.0254 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND2-Hexanone
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND4-Chlorotoluene
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND4-Isopropyltoluene
0.0335 0.0241 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼ND4-Methyl-2-pentanone (MIBK)
0.0669 0.0147 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼0.0453 JAcetone
0.00669 0.00321 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDBenzene
0.00669 0.00228 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDBromobenzene
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDBromoform
0.00669 0.00321 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDBromomethane
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDCarbon disulfide
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDCarbon tetrachloride
0.00669 0.00187 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChlorobenzene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChlorobromomethane
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChlorodibromomethane
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChloroethane
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChloroform
0.00669 0.00321 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDChloromethane
0.00669 0.00388 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDcis-1,2-Dichloroethene
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDcis-1,3-Dichloropropene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDDibromomethane
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDDichlorobromomethane
0.0134 0.0134 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDEthyl acetate
0.00669 0.00281 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDEthylbenzene
0.00669 0.00228 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDEthylene Dibromide
0.00669 0.00549 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDHexachlorobutadiene
0.00669 0.00228 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-16Client Sample ID: P14-5
Matrix: SolidDate Collected: 11/29/22 08:25
Percent Solids: 79.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00669 0.00228 mg/Kg ☼12/02/22 12:11 12/08/22 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0134 0.00201 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDIsopropyl ether
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDIsopropylbenzene
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDMethyl tert-butyl ether
0.0134 0.0107 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDMethylene Chloride
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDm-Xylene & p-Xylene
0.00669 0.00415 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDNaphthalene
0.00669 0.00254 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDn-Butylbenzene
0.00669 0.00576 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDn-Heptane
0.00669 0.00295 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDN-Propylbenzene
0.00669 0.00308 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDo-Xylene
0.00669 0.00268 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDsec-Butylbenzene
0.00669 0.00254 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDStyrene
0.00669 0.00335 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDtert-Butylbenzene
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDTetrachloroethene
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDToluene
0.00669 0.00308 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDtrans-1,2-Dichloroethene
0.00669 0.00348 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDtrans-1,3-Dichloropropene
0.0134 0.00321 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDtrans-1,4-Dichloro-2-butene
0.00669 0.00241 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDTrichloroethene
0.00669 0.00415 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDTrichlorofluoromethane
0.0134 0.00736 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDVinyl acetate
0.00669 0.00375 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDVinyl chloride
0.0134 0.00482 mg/Kg 12/02/22 12:11 12/08/22 19:38 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)99 65-130 12/02/22 12:11 12/08/22 19:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 12/02/22 12:11 12/08/22 19:38 165-130
Dibromofluoromethane (Surr)104 12/02/22 12:11 12/08/22 19:38 165-130
Toluene-d8 (Surr)106 12/02/22 12:11 12/08/22 19:38 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.06 2.06 mg/Kg ☼12/06/22 18:15 12/08/22 01:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.400 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4,5-Trichlorophenol
0.400 0.0352 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4,6-Trichlorophenol
0.400 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4-Dichlorophenol
0.400 0.0534 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4-Dimethylphenol
2.06 1.01 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4-Dinitrophenol
0.400 0.0595 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,4-Dinitrotoluene
0.400 0.0510 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2,6-Dinitrotoluene
0.400 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2-Chloronaphthalene
0.400 0.0485 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2-Chlorophenol
0.400 0.0461 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼0.0921 J2-Methylnaphthalene
0.400 0.0328 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2-Methylphenol
2.06 0.0546 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2-Nitroaniline
0.400 0.0497 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND2-Nitrophenol
0.400 0.0522 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND3 & 4 Methylphenol
0.801 0.0340 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND3,3'-Dichlorobenzidine
2.06 0.0558 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-16Client Sample ID: P14-5
Matrix: SolidDate Collected: 11/29/22 08:25
Percent Solids: 79.8Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.06 0.206 mg/Kg ☼12/06/22 18:15 12/08/22 01:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.400 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Bromophenyl phenyl ether
0.400 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Chloro-3-methylphenol
0.801 0.0631 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Chloroaniline
0.400 0.0534 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Chlorophenyl phenyl ether
2.06 0.0595 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Nitroaniline
2.06 0.400 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼ND4-Nitrophenol
0.400 0.0497 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDAcenaphthene
0.400 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDAcenaphthylene
0.400 0.0340 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDAcetophenone
0.400 0.0303 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDAnthracene
0.400 0.0279 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDAtrazine
0.400 0.0704 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzaldehyde
0.400 0.0328 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzo[a]anthracene
0.400 0.0631 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzo[a]pyrene
0.400 0.0461 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzo[b]fluoranthene
0.400 0.0267 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzo[g,h,i]perylene
0.400 0.0789 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBenzo[k]fluoranthene
0.400 0.0364 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDbis (2-chloroisopropyl) ether
0.400 0.0473 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBis(2-chloroethoxy)methane
0.400 0.0546 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBis(2-chloroethyl)ether
0.400 0.0352 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDBis(2-ethylhexyl) phthalate
0.400 0.0315 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDButyl benzyl phthalate
0.400 0.0801 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDCaprolactam
0.400 0.0364 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDCarbazole
0.400 0.0255 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDChrysene
0.400 0.0473 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDibenz(a,h)anthracene
0.400 0.0400 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDibenzofuran
0.400 0.0449 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDiethyl phthalate
0.400 0.0413 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDimethyl phthalate
0.400 0.0364 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDi-n-butyl phthalate
0.400 0.0352 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDDi-n-octyl phthalate
0.400 0.0388 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDFluoranthene
0.400 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDFluorene
0.400 0.0473 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDHexachlorobenzene
0.400 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDHexachlorobutadiene
0.400 0.0497 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDHexachlorocyclopentadiene
0.400 0.0340 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDHexachloroethane
0.400 0.0340 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDIndeno[1,2,3-cd]pyrene
0.400 0.0400 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDIsophorone
0.400 0.0364 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDNaphthalene
0.400 0.0315 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDNitrobenzene
0.400 0.0388 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDN-Nitrosodi-n-propylamine
0.400 0.0400 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDN-Nitrosodiphenylamine
2.06 0.400 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDPentachlorophenol
0.400 0.0328 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDPhenanthrene
0.400 0.0413 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDPhenol
0.400 0.0328 mg/Kg 12/06/22 18:15 12/08/22 01:23 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-16Client Sample ID: P14-5
Matrix: SolidDate Collected: 11/29/22 08:25
Percent Solids: 79.8Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)77 21-132 12/06/22 18:15 12/08/22 01:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)62 12/06/22 18:15 12/08/22 01:23 125-130
2-Fluorophenol (Surr)55 12/06/22 18:15 12/08/22 01:23 118-130
Nitrobenzene-d5 (Surr)55 12/06/22 18:15 12/08/22 01:23 119-130
Phenol-d5 (Surr)60 12/06/22 18:15 12/08/22 01:23 121-130
Terphenyl-d14 (Surr)86 12/06/22 18:15 12/08/22 01:23 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 6.78 3.39 mg/Kg ☼12/12/22 13:20 12/12/22 17:49 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)98 65-125 12/12/22 13:20 12/12/22 17:49 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
3.72 J 9.75 3.17 mg/Kg ☼12/07/22 18:30 12/08/22 22:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 58 15-139 12/07/22 18:30 12/08/22 22:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-17Client Sample ID: P15-10
Matrix: SolidDate Collected: 11/29/22 08:38
Percent Solids: 78.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00673 0.00175 mg/Kg ☼12/02/22 12:11 12/09/22 16:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1,1-Trichloroethane
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1,2,2-Tetrachloroethane
0.00673 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00673 0.00202 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1,2-Trichloroethane
0.00673 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1-Dichloroethane
0.00673 0.00485 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1-Dichloroethene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,1-Dichloropropene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2,3-Trichlorobenzene
0.00673 0.00242 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2,3-Trichloropropane
0.00673 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2,4-Trichlorobenzene
0.00673 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2,4-Trimethylbenzene
0.0135 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2-Dibromo-3-Chloropropane
0.00673 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2-Dichlorobenzene
0.00673 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2-Dichloroethane
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,2-Dichloropropane
0.00673 0.00323 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,3,5-Trimethylbenzene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,3-Dichlorobenzene
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,3-Dichloropropane
0.00673 0.00242 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND1,4-Dichlorobenzene
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND2,2-Dichloropropane
0.0337 0.0124 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND2-Butanone (MEK)
0.00673 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND2-Chlorotoluene
0.0337 0.0256 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND2-Hexanone
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND4-Chlorotoluene
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND4-Isopropyltoluene
0.0337 0.0242 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼ND4-Methyl-2-pentanone (MIBK)
0.0673 0.0148 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼0.0411 JAcetone
0.00673 0.00323 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDBenzene
0.00673 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDBromobenzene
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDBromoform
0.00673 0.00323 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDBromomethane
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDCarbon disulfide
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDCarbon tetrachloride
0.00673 0.00189 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChlorobenzene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChlorobromomethane
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChlorodibromomethane
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChloroethane
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChloroform
0.00673 0.00323 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDChloromethane
0.00673 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDcis-1,2-Dichloroethene
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDcis-1,3-Dichloropropene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDDibromomethane
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDDichlorobromomethane
0.0135 0.0135 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDEthyl acetate
0.00673 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDEthylbenzene
0.00673 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDEthylene Dibromide
0.00673 0.00552 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDHexachlorobutadiene
0.00673 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-17Client Sample ID: P15-10
Matrix: SolidDate Collected: 11/29/22 08:38
Percent Solids: 78.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00673 0.00229 mg/Kg ☼12/02/22 12:11 12/09/22 16:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0135 0.00202 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDIsopropyl ether
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDIsopropylbenzene
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDMethyl tert-butyl ether
0.0135 0.0108 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDMethylene Chloride
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDm-Xylene & p-Xylene
0.00673 0.00418 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDNaphthalene
0.00673 0.00256 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDn-Butylbenzene
0.00673 0.00579 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDn-Heptane
0.00673 0.00296 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDN-Propylbenzene
0.00673 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDo-Xylene
0.00673 0.00269 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDsec-Butylbenzene
0.00673 0.00256 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDStyrene
0.00673 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDtert-Butylbenzene
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDTetrachloroethene
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDToluene
0.00673 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDtrans-1,2-Dichloroethene
0.00673 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDtrans-1,3-Dichloropropene
0.0135 0.00323 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDtrans-1,4-Dichloro-2-butene
0.00673 0.00242 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDTrichloroethene
0.00673 0.00418 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDTrichlorofluoromethane
0.0135 0.00741 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDVinyl acetate
0.00673 0.00377 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDVinyl chloride
0.0135 0.00485 mg/Kg 12/02/22 12:11 12/09/22 16:09 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 65-130 12/02/22 12:11 12/09/22 16:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/09/22 16:09 165-130
Dibromofluoromethane (Surr)107 12/02/22 12:11 12/09/22 16:09 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/09/22 16:09 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.12 2.12 mg/Kg ☼12/06/22 18:15 12/08/22 01:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4,5-Trichlorophenol
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4,6-Trichlorophenol
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4-Dichlorophenol
0.412 0.0550 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4-Dimethylphenol
2.12 1.04 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4-Dinitrophenol
0.412 0.0612 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,4-Dinitrotoluene
0.412 0.0525 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2,6-Dinitrotoluene
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Chloronaphthalene
0.412 0.0500 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Chlorophenol
0.412 0.0475 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Methylnaphthalene
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Methylphenol
2.12 0.0562 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Nitroaniline
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND2-Nitrophenol
0.412 0.0537 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND3 & 4 Methylphenol
0.825 0.0350 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND3,3'-Dichlorobenzidine
2.12 0.0575 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-17Client Sample ID: P15-10
Matrix: SolidDate Collected: 11/29/22 08:38
Percent Solids: 78.8Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.12 0.212 mg/Kg ☼12/06/22 18:15 12/08/22 01:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.412 0.0450 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Bromophenyl phenyl ether
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Chloro-3-methylphenol
0.825 0.0650 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Chloroaniline
0.412 0.0550 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Chlorophenyl phenyl ether
2.12 0.0612 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Nitroaniline
2.12 0.412 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼ND4-Nitrophenol
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDAcenaphthene
0.412 0.0450 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDAcenaphthylene
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDAcetophenone
0.412 0.0312 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDAnthracene
0.412 0.0287 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDAtrazine
0.412 0.0725 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzaldehyde
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzo[a]anthracene
0.412 0.0650 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzo[a]pyrene
0.412 0.0475 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzo[b]fluoranthene
0.412 0.0275 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzo[g,h,i]perylene
0.412 0.0812 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBenzo[k]fluoranthene
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDbis (2-chloroisopropyl) ether
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBis(2-chloroethoxy)methane
0.412 0.0562 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBis(2-chloroethyl)ether
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDBis(2-ethylhexyl) phthalate
0.412 0.0325 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDButyl benzyl phthalate
0.412 0.0825 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDCaprolactam
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDCarbazole
0.412 0.0262 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDChrysene
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDibenz(a,h)anthracene
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDibenzofuran
0.412 0.0462 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDiethyl phthalate
0.412 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDimethyl phthalate
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDi-n-butyl phthalate
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDDi-n-octyl phthalate
0.412 0.0400 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDFluoranthene
0.412 0.0450 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDFluorene
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDHexachlorobenzene
0.412 0.0450 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDHexachlorobutadiene
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDHexachlorocyclopentadiene
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDHexachloroethane
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDIndeno[1,2,3-cd]pyrene
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDIsophorone
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDNaphthalene
0.412 0.0325 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDNitrobenzene
0.412 0.0400 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDN-Nitrosodi-n-propylamine
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDN-Nitrosodiphenylamine
2.12 0.412 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDPentachlorophenol
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDPhenanthrene
0.412 0.0425 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDPhenol
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 01:47 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-17Client Sample ID: P15-10
Matrix: SolidDate Collected: 11/29/22 08:38
Percent Solids: 78.8Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)80 21-132 12/06/22 18:15 12/08/22 01:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)70 12/06/22 18:15 12/08/22 01:47 125-130
2-Fluorophenol (Surr)60 12/06/22 18:15 12/08/22 01:47 118-130
Nitrobenzene-d5 (Surr)62 12/06/22 18:15 12/08/22 01:47 119-130
Phenol-d5 (Surr)65 12/06/22 18:15 12/08/22 01:47 121-130
Terphenyl-d14 (Surr)87 12/06/22 18:15 12/08/22 01:47 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.85 4.42 mg/Kg ☼12/12/22 13:20 12/12/22 18:17 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)100 65-125 12/12/22 13:20 12/12/22 18:17 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
11.1 10.0 3.26 mg/Kg ☼12/07/22 18:30 12/08/22 22:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 62 15-139 12/07/22 18:30 12/08/22 22:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-18Client Sample ID: P17-5
Matrix: SolidDate Collected: 11/29/22 08:56
Percent Solids: 77.2Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00489 0.00127 mg/Kg ☼12/02/22 12:11 12/09/22 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1,1-Trichloroethane
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1,2,2-Tetrachloroethane
0.00489 0.00284 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00489 0.00147 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1,2-Trichloroethane
0.00489 0.00284 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1-Dichloroethane
0.00489 0.00352 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1-Dichloroethene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,1-Dichloropropene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2,3-Trichlorobenzene
0.00489 0.00176 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2,3-Trichloropropane
0.00489 0.00245 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2,4-Trichlorobenzene
0.00489 0.00245 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2,4-Trimethylbenzene
0.00978 0.00156 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2-Dibromo-3-Chloropropane
0.00489 0.00166 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2-Dichlorobenzene
0.00489 0.00225 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2-Dichloroethane
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,2-Dichloropropane
0.00489 0.00235 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,3,5-Trimethylbenzene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,3-Dichlorobenzene
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,3-Dichloropropane
0.00489 0.00176 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND1,4-Dichlorobenzene
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND2,2-Dichloropropane
0.0245 0.00900 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND2-Butanone (MEK)
0.00489 0.00225 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND2-Chlorotoluene
0.0245 0.0186 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND2-Hexanone
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND4-Chlorotoluene
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND4-Isopropyltoluene
0.0245 0.0176 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼ND4-Methyl-2-pentanone (MIBK)
0.0489 0.0108 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼0.0801Acetone
0.00489 0.00235 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDBenzene
0.00489 0.00166 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDBromobenzene
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDBromoform
0.00489 0.00235 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDBromomethane
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDCarbon disulfide
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDCarbon tetrachloride
0.00489 0.00137 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChlorobenzene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChlorobromomethane
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChlorodibromomethane
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChloroethane
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChloroform
0.00489 0.00235 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDChloromethane
0.00489 0.00284 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDcis-1,2-Dichloroethene
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDcis-1,3-Dichloropropene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDDibromomethane
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDDichlorobromomethane
0.00978 0.00978 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDEthyl acetate
0.00489 0.00205 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDEthylbenzene
0.00489 0.00166 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDEthylene Dibromide
0.00489 0.00401 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDHexachlorobutadiene
0.00489 0.00166 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-18Client Sample ID: P17-5
Matrix: SolidDate Collected: 11/29/22 08:56
Percent Solids: 77.2Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00489 0.00166 mg/Kg ☼12/02/22 12:11 12/09/22 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.00978 0.00147 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDIsopropyl ether
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDIsopropylbenzene
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDMethyl tert-butyl ether
0.00978 0.00782 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDMethylene Chloride
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDm-Xylene & p-Xylene
0.00489 0.00303 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDNaphthalene
0.00489 0.00186 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDn-Butylbenzene
0.00489 0.00421 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDn-Heptane
0.00489 0.00215 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDN-Propylbenzene
0.00489 0.00225 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDo-Xylene
0.00489 0.00196 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDsec-Butylbenzene
0.00489 0.00186 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDStyrene
0.00489 0.00245 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDtert-Butylbenzene
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDTetrachloroethene
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDToluene
0.00489 0.00225 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDtrans-1,2-Dichloroethene
0.00489 0.00254 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDtrans-1,3-Dichloropropene
0.00978 0.00235 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDtrans-1,4-Dichloro-2-butene
0.00489 0.00176 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDTrichloroethene
0.00489 0.00303 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDTrichlorofluoromethane
0.00978 0.00538 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDVinyl acetate
0.00489 0.00274 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDVinyl chloride
0.00978 0.00352 mg/Kg 12/02/22 12:11 12/09/22 16:33 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)102 65-130 12/02/22 12:11 12/09/22 16:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)101 12/02/22 12:11 12/09/22 16:33 165-130
Dibromofluoromethane (Surr)107 12/02/22 12:11 12/09/22 16:33 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/09/22 16:33 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.12 2.12 mg/Kg ☼12/06/22 18:15 12/08/22 02:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4,5-Trichlorophenol
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4,6-Trichlorophenol
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4-Dichlorophenol
0.412 0.0549 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4-Dimethylphenol
2.12 1.04 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4-Dinitrophenol
0.412 0.0612 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,4-Dinitrotoluene
0.412 0.0524 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2,6-Dinitrotoluene
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Chloronaphthalene
0.412 0.0499 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Chlorophenol
0.412 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Methylnaphthalene
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Methylphenol
2.12 0.0562 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Nitroaniline
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND2-Nitrophenol
0.412 0.0537 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND3 & 4 Methylphenol
0.824 0.0350 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND3,3'-Dichlorobenzidine
2.12 0.0574 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-18Client Sample ID: P17-5
Matrix: SolidDate Collected: 11/29/22 08:56
Percent Solids: 77.2Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.12 0.212 mg/Kg ☼12/06/22 18:15 12/08/22 02:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.412 0.0449 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Bromophenyl phenyl ether
0.412 0.0437 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Chloro-3-methylphenol
0.824 0.0649 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Chloroaniline
0.412 0.0549 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Chlorophenyl phenyl ether
2.12 0.0612 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Nitroaniline
2.12 0.412 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼ND4-Nitrophenol
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDAcenaphthene
0.412 0.0449 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDAcenaphthylene
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDAcetophenone
0.412 0.0312 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDAnthracene
0.412 0.0287 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDAtrazine
0.412 0.0724 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzaldehyde
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzo[a]anthracene
0.412 0.0649 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzo[a]pyrene
0.412 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzo[b]fluoranthene
0.412 0.0275 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzo[g,h,i]perylene
0.412 0.0811 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBenzo[k]fluoranthene
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDbis (2-chloroisopropyl) ether
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBis(2-chloroethoxy)methane
0.412 0.0562 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBis(2-chloroethyl)ether
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDBis(2-ethylhexyl) phthalate
0.412 0.0325 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDButyl benzyl phthalate
0.412 0.0824 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDCaprolactam
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDCarbazole
0.412 0.0262 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDChrysene
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDibenz(a,h)anthracene
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDibenzofuran
0.412 0.0462 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDiethyl phthalate
0.412 0.0424 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDimethyl phthalate
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDi-n-butyl phthalate
0.412 0.0362 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDDi-n-octyl phthalate
0.412 0.0399 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDFluoranthene
0.412 0.0449 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDFluorene
0.412 0.0487 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDHexachlorobenzene
0.412 0.0449 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDHexachlorobutadiene
0.412 0.0512 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDHexachlorocyclopentadiene
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDHexachloroethane
0.412 0.0350 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDIndeno[1,2,3-cd]pyrene
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDIsophorone
0.412 0.0375 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDNaphthalene
0.412 0.0325 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDNitrobenzene
0.412 0.0399 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDN-Nitrosodi-n-propylamine
0.412 0.0412 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDN-Nitrosodiphenylamine
2.12 0.412 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDPentachlorophenol
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDPhenanthrene
0.412 0.0424 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDPhenol
0.412 0.0337 mg/Kg 12/06/22 18:15 12/08/22 02:10 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-18Client Sample ID: P17-5
Matrix: SolidDate Collected: 11/29/22 08:56
Percent Solids: 77.2Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)93 21-132 12/06/22 18:15 12/08/22 02:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)73 12/06/22 18:15 12/08/22 02:10 125-130
2-Fluorophenol (Surr)67 12/06/22 18:15 12/08/22 02:10 118-130
Nitrobenzene-d5 (Surr)64 12/06/22 18:15 12/08/22 02:10 119-130
Phenol-d5 (Surr)71 12/06/22 18:15 12/08/22 02:10 121-130
Terphenyl-d14 (Surr)87 12/06/22 18:15 12/08/22 02:10 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
6.62 6.53 3.27 mg/Kg ☼12/12/22 13:20 12/12/22 19:09 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 -
C10]
a,a,a-Trifluorotoluene (fid)100 65-125 12/12/22 13:20 12/12/22 19:09 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
4.62 J 10.2 3.32 mg/Kg ☼12/07/22 18:30 12/08/22 23:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 34 15-139 12/07/22 18:30 12/08/22 23:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-19Client Sample ID: P18-10
Matrix: SolidDate Collected: 11/29/22 09:13
Percent Solids: 73.0Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00674 0.00175 mg/Kg ☼12/02/22 12:11 12/09/22 16:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1,1-Trichloroethane
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1,2,2-Tetrachloroethane
0.00674 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00674 0.00202 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1,2-Trichloroethane
0.00674 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1-Dichloroethane
0.00674 0.00485 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1-Dichloroethene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,1-Dichloropropene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2,3-Trichlorobenzene
0.00674 0.00243 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2,3-Trichloropropane
0.00674 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2,4-Trichlorobenzene
0.00674 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2,4-Trimethylbenzene
0.0135 0.00216 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2-Dibromo-3-Chloropropane
0.00674 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2-Dichlorobenzene
0.00674 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2-Dichloroethane
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,2-Dichloropropane
0.00674 0.00324 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,3,5-Trimethylbenzene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,3-Dichlorobenzene
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,3-Dichloropropane
0.00674 0.00243 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND1,4-Dichlorobenzene
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND2,2-Dichloropropane
0.0337 0.0124 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼0.0199 J2-Butanone (MEK)
0.00674 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND2-Chlorotoluene
0.0337 0.0256 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND2-Hexanone
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND4-Chlorotoluene
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND4-Isopropyltoluene
0.0337 0.0243 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼ND4-Methyl-2-pentanone (MIBK)
0.0674 0.0148 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼0.127Acetone
0.00674 0.00324 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDBenzene
0.00674 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDBromobenzene
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDBromoform
0.00674 0.00324 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDBromomethane
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDCarbon disulfide
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDCarbon tetrachloride
0.00674 0.00189 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChlorobenzene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChlorobromomethane
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChlorodibromomethane
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChloroethane
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChloroform
0.00674 0.00324 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDChloromethane
0.00674 0.00391 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDcis-1,2-Dichloroethene
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDcis-1,3-Dichloropropene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDDibromomethane
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDDichlorobromomethane
0.0135 0.0135 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDEthyl acetate
0.00674 0.00283 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDEthylbenzene
0.00674 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDEthylene Dibromide
0.00674 0.00553 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDHexachlorobutadiene
0.00674 0.00229 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-19Client Sample ID: P18-10
Matrix: SolidDate Collected: 11/29/22 09:13
Percent Solids: 73.0Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 0.00674 0.00229 mg/Kg ☼12/02/22 12:11 12/09/22 16:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0135 0.00202 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDIsopropyl ether
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDIsopropylbenzene
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDMethyl tert-butyl ether
0.0135 0.0108 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDMethylene Chloride
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDm-Xylene & p-Xylene
0.00674 0.00418 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDNaphthalene
0.00674 0.00256 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDn-Butylbenzene
0.00674 0.00580 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDn-Heptane
0.00674 0.00297 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDN-Propylbenzene
0.00674 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDo-Xylene
0.00674 0.00270 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDsec-Butylbenzene
0.00674 0.00256 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDStyrene
0.00674 0.00337 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDtert-Butylbenzene
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDTetrachloroethene
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDToluene
0.00674 0.00310 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDtrans-1,2-Dichloroethene
0.00674 0.00350 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDtrans-1,3-Dichloropropene
0.0135 0.00324 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDtrans-1,4-Dichloro-2-butene
0.00674 0.00243 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDTrichloroethene
0.00674 0.00418 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDTrichlorofluoromethane
0.0135 0.00741 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDVinyl acetate
0.00674 0.00377 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDVinyl chloride
0.0135 0.00485 mg/Kg 12/02/22 12:11 12/09/22 16:56 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/09/22 16:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 12/02/22 12:11 12/09/22 16:56 165-130
Dibromofluoromethane (Surr)106 12/02/22 12:11 12/09/22 16:56 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/09/22 16:56 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.24 2.24 mg/Kg ☼12/06/22 18:15 12/08/22 02:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.435 0.0461 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4,5-Trichlorophenol
0.435 0.0382 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4,6-Trichlorophenol
0.435 0.0461 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4-Dichlorophenol
0.435 0.0580 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4-Dimethylphenol
2.24 1.09 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4-Dinitrophenol
0.435 0.0646 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,4-Dinitrotoluene
0.435 0.0553 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2,6-Dinitrotoluene
0.435 0.0461 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Chloronaphthalene
0.435 0.0527 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Chlorophenol
0.435 0.0501 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Methylnaphthalene
0.435 0.0356 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Methylphenol
2.24 0.0593 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Nitroaniline
0.435 0.0540 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND2-Nitrophenol
0.435 0.0566 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND3 & 4 Methylphenol
0.870 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND3,3'-Dichlorobenzidine
2.24 0.0606 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-19Client Sample ID: P18-10
Matrix: SolidDate Collected: 11/29/22 09:13
Percent Solids: 73.0Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.24 0.224 mg/Kg ☼12/06/22 18:15 12/08/22 02:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.435 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Bromophenyl phenyl ether
0.435 0.0461 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Chloro-3-methylphenol
0.870 0.0685 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Chloroaniline
0.435 0.0580 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Chlorophenyl phenyl ether
2.24 0.0646 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Nitroaniline
2.24 0.435 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼ND4-Nitrophenol
0.435 0.0540 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDAcenaphthene
0.435 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDAcenaphthylene
0.435 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDAcetophenone
0.435 0.0329 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDAnthracene
0.435 0.0303 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDAtrazine
0.435 0.0764 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzaldehyde
0.435 0.0356 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzo[a]anthracene
0.435 0.0685 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzo[a]pyrene
0.435 0.0501 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzo[b]fluoranthene
0.435 0.0290 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzo[g,h,i]perylene
0.435 0.0856 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBenzo[k]fluoranthene
0.435 0.0395 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDbis (2-chloroisopropyl) ether
0.435 0.0514 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBis(2-chloroethoxy)methane
0.435 0.0593 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBis(2-chloroethyl)ether
0.435 0.0382 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDBis(2-ethylhexyl) phthalate
0.435 0.0343 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDButyl benzyl phthalate
0.435 0.0870 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDCaprolactam
0.435 0.0395 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDCarbazole
0.435 0.0277 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDChrysene
0.435 0.0514 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDibenz(a,h)anthracene
0.435 0.0435 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDibenzofuran
0.435 0.0487 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDiethyl phthalate
0.435 0.0448 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDimethyl phthalate
0.435 0.0395 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDi-n-butyl phthalate
0.435 0.0382 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDDi-n-octyl phthalate
0.435 0.0422 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDFluoranthene
0.435 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDFluorene
0.435 0.0514 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDHexachlorobenzene
0.435 0.0474 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDHexachlorobutadiene
0.435 0.0540 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDHexachlorocyclopentadiene
0.435 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDHexachloroethane
0.435 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDIndeno[1,2,3-cd]pyrene
0.435 0.0435 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDIsophorone
0.435 0.0395 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDNaphthalene
0.435 0.0343 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDNitrobenzene
0.435 0.0422 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDN-Nitrosodi-n-propylamine
0.435 0.0435 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDN-Nitrosodiphenylamine
2.24 0.435 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDPentachlorophenol
0.435 0.0356 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDPhenanthrene
0.435 0.0448 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDPhenol
0.435 0.0356 mg/Kg 12/06/22 18:15 12/08/22 02:35 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-19Client Sample ID: P18-10
Matrix: SolidDate Collected: 11/29/22 09:13
Percent Solids: 73.0Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)67 21-132 12/06/22 18:15 12/08/22 02:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)68 12/06/22 18:15 12/08/22 02:35 125-130
2-Fluorophenol (Surr)54 12/06/22 18:15 12/08/22 02:35 118-130
Nitrobenzene-d5 (Surr)61 12/06/22 18:15 12/08/22 02:35 119-130
Phenol-d5 (Surr)60 12/06/22 18:15 12/08/22 02:35 121-130
Terphenyl-d14 (Surr)86 12/06/22 18:15 12/08/22 02:35 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.88 4.44 mg/Kg ☼12/12/22 13:20 12/12/22 19:35 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)98 65-125 12/12/22 13:20 12/12/22 19:35 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
5.19 J 10.8 3.52 mg/Kg ☼12/07/22 18:30 12/08/22 23:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 37 15-139 12/07/22 18:30 12/08/22 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-20Client Sample ID: P16-15
Matrix: SolidDate Collected: 11/29/22 09:29
Percent Solids: 76.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 0.00634 0.00165 mg/Kg ☼12/02/22 12:11 12/09/22 17:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1,1-Trichloroethane
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1,2,2-Tetrachloroethane
0.00634 0.00368 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
0.00634 0.00190 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1,2-Trichloroethane
0.00634 0.00368 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1-Dichloroethane
0.00634 0.00456 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1-Dichloroethene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,1-Dichloropropene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2,3-Trichlorobenzene
0.00634 0.00228 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2,3-Trichloropropane
0.00634 0.00317 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2,4-Trichlorobenzene
0.00634 0.00317 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2,4-Trimethylbenzene
0.0127 0.00203 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2-Dibromo-3-Chloropropane
0.00634 0.00216 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2-Dichlorobenzene
0.00634 0.00292 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2-Dichloroethane
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,2-Dichloropropane
0.00634 0.00304 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,3,5-Trimethylbenzene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,3-Dichlorobenzene
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,3-Dichloropropane
0.00634 0.00228 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND1,4-Dichlorobenzene
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND2,2-Dichloropropane
0.0317 0.0117 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼0.0129 J2-Butanone (MEK)
0.00634 0.00292 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND2-Chlorotoluene
0.0317 0.0241 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND2-Hexanone
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND4-Chlorotoluene
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND4-Isopropyltoluene
0.0317 0.0228 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼ND4-Methyl-2-pentanone (MIBK)
0.0634 0.0139 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼0.121Acetone
0.00634 0.00304 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDBenzene
0.00634 0.00216 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDBromobenzene
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDBromoform
0.00634 0.00304 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDBromomethane
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDCarbon disulfide
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDCarbon tetrachloride
0.00634 0.00178 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChlorobenzene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChlorobromomethane
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChlorodibromomethane
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChloroethane
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChloroform
0.00634 0.00304 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDChloromethane
0.00634 0.00368 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDcis-1,2-Dichloroethene
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDcis-1,3-Dichloropropene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDDibromomethane
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDDichlorobromomethane
0.0127 0.0127 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDEthyl acetate
0.00634 0.00266 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDEthylbenzene
0.00634 0.00216 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDEthylene Dibromide
0.00634 0.00520 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDHexachlorobutadiene
0.00634 0.00216 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDHexane
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-20Client Sample ID: P16-15
Matrix: SolidDate Collected: 11/29/22 09:29
Percent Solids: 76.8Date Received: 12/01/22 06:30
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
0.00269 J 0.00634 0.00216 mg/Kg ☼12/02/22 12:11 12/09/22 17:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Iodomethane
0.0127 0.00190 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDIsopropyl ether
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDIsopropylbenzene
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDMethyl tert-butyl ether
0.0127 0.0101 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDMethylene Chloride
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDm-Xylene & p-Xylene
0.00634 0.00393 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDNaphthalene
0.00634 0.00241 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDn-Butylbenzene
0.00634 0.00545 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDn-Heptane
0.00634 0.00279 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDN-Propylbenzene
0.00634 0.00292 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDo-Xylene
0.00634 0.00254 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDsec-Butylbenzene
0.00634 0.00241 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDStyrene
0.00634 0.00317 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDtert-Butylbenzene
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDTetrachloroethene
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDToluene
0.00634 0.00292 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDtrans-1,2-Dichloroethene
0.00634 0.00330 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDtrans-1,3-Dichloropropene
0.0127 0.00304 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDtrans-1,4-Dichloro-2-butene
0.00634 0.00228 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDTrichloroethene
0.00634 0.00393 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDTrichlorofluoromethane
0.0127 0.00697 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDVinyl acetate
0.00634 0.00355 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDVinyl chloride
0.0127 0.00456 mg/Kg 12/02/22 12:11 12/09/22 17:20 1☼NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)101 65-130 12/02/22 12:11 12/09/22 17:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 12/02/22 12:11 12/09/22 17:20 165-130
Dibromofluoromethane (Surr)105 12/02/22 12:11 12/09/22 17:20 165-130
Toluene-d8 (Surr)104 12/02/22 12:11 12/09/22 17:20 165-130
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 2.09 2.09 mg/Kg ☼12/06/22 18:15 12/08/22 02:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
0.406 0.0431 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4,5-Trichlorophenol
0.406 0.0357 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4,6-Trichlorophenol
0.406 0.0431 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4-Dichlorophenol
0.406 0.0541 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4-Dimethylphenol
2.09 1.02 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4-Dinitrophenol
0.406 0.0603 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,4-Dinitrotoluene
0.406 0.0517 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2,6-Dinitrotoluene
0.406 0.0431 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Chloronaphthalene
0.406 0.0492 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Chlorophenol
0.406 0.0468 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Methylnaphthalene
0.406 0.0332 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Methylphenol
2.09 0.0554 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Nitroaniline
0.406 0.0504 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND2-Nitrophenol
0.406 0.0529 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND3 & 4 Methylphenol
0.812 0.0345 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND3,3'-Dichlorobenzidine
2.09 0.0566 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND3-Nitroaniline
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-20Client Sample ID: P16-15
Matrix: SolidDate Collected: 11/29/22 09:29
Percent Solids: 76.8Date Received: 12/01/22 06:30
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 2.09 0.209 mg/Kg ☼12/06/22 18:15 12/08/22 02:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4,6-Dinitro-2-methylphenol
0.406 0.0443 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Bromophenyl phenyl ether
0.406 0.0431 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Chloro-3-methylphenol
0.812 0.0640 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Chloroaniline
0.406 0.0541 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Chlorophenyl phenyl ether
2.09 0.0603 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Nitroaniline
2.09 0.406 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼ND4-Nitrophenol
0.406 0.0504 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDAcenaphthene
0.406 0.0443 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDAcenaphthylene
0.406 0.0345 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDAcetophenone
0.406 0.0308 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDAnthracene
0.406 0.0283 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDAtrazine
0.406 0.0714 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzaldehyde
0.406 0.0332 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzo[a]anthracene
0.406 0.0640 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzo[a]pyrene
0.406 0.0468 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzo[b]fluoranthene
0.406 0.0271 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzo[g,h,i]perylene
0.406 0.0800 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBenzo[k]fluoranthene
0.406 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDbis (2-chloroisopropyl) ether
0.406 0.0480 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBis(2-chloroethoxy)methane
0.406 0.0554 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBis(2-chloroethyl)ether
0.406 0.0357 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDBis(2-ethylhexyl) phthalate
0.406 0.0320 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDButyl benzyl phthalate
0.406 0.0812 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDCaprolactam
0.406 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDCarbazole
0.406 0.0258 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDChrysene
0.406 0.0480 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDibenz(a,h)anthracene
0.406 0.0406 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDibenzofuran
0.406 0.0455 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDiethyl phthalate
0.406 0.0418 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDimethyl phthalate
0.406 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDi-n-butyl phthalate
0.406 0.0357 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDDi-n-octyl phthalate
0.406 0.0394 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDFluoranthene
0.406 0.0443 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDFluorene
0.406 0.0480 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDHexachlorobenzene
0.406 0.0443 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDHexachlorobutadiene
0.406 0.0504 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDHexachlorocyclopentadiene
0.406 0.0345 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDHexachloroethane
0.406 0.0345 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDIndeno[1,2,3-cd]pyrene
0.406 0.0406 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDIsophorone
0.406 0.0369 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDNaphthalene
0.406 0.0320 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDNitrobenzene
0.406 0.0394 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDN-Nitrosodi-n-propylamine
0.406 0.0406 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDN-Nitrosodiphenylamine
2.09 0.406 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDPentachlorophenol
0.406 0.0332 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDPhenanthrene
0.406 0.0418 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDPhenol
0.406 0.0332 mg/Kg 12/06/22 18:15 12/08/22 02:59 1☼NDPyrene
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Client Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Lab Sample ID: 680-226646-20Client Sample ID: P16-15
Matrix: SolidDate Collected: 11/29/22 09:29
Percent Solids: 76.8Date Received: 12/01/22 06:30
2,4,6-Tribromophenol (Surr)65 21-132 12/06/22 18:15 12/08/22 02:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)73 12/06/22 18:15 12/08/22 02:59 125-130
2-Fluorophenol (Surr)59 12/06/22 18:15 12/08/22 02:59 118-130
Nitrobenzene-d5 (Surr)65 12/06/22 18:15 12/08/22 02:59 119-130
Phenol-d5 (Surr)66 12/06/22 18:15 12/08/22 02:59 121-130
Terphenyl-d14 (Surr)89 12/06/22 18:15 12/08/22 02:59 131-133
Method: SW846 8015C - Gasoline Range Organics (GRO) (GC)
RL MDL
ND 8.19 4.10 mg/Kg ☼12/12/22 13:20 12/12/22 20:01 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Gasoline Range Organics [C6 - C10]
a,a,a-Trifluorotoluene (fid)98 65-125 12/12/22 13:20 12/12/22 20:01 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL MDL
3.45 J 10.3 3.35 mg/Kg ☼12/07/22 18:30 12/08/22 23:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 40 15-139 12/07/22 18:30 12/08/22 23:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-753988/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 12/07/22 14:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 12/07/22 14:03 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 12/07/22 14:03 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 12/07/22 14:03 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 12/07/22 14:03 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 12/07/22 14:03 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 12/07/22 14:03 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 12/07/22 14:03 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 12/07/22 14:03 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 12/07/22 14:03 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 12/07/22 14:03 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 12/07/22 14:03 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 12/07/22 14:03 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 12/07/22 14:03 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 12/07/22 14:03 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/07/22 14:03 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 12/07/22 14:03 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/07/22 14:03 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 12/07/22 14:03 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 12/07/22 14:03 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 12/07/22 14:03 12-Hexanone
ND 0.002100.00500 mg/Kg 12/07/22 14:03 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 12/07/22 14:03 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 12/07/22 14:03 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 12/07/22 14:03 1Acetone
ND 0.002400.00500 mg/Kg 12/07/22 14:03 1Benzene
ND 0.001700.00500 mg/Kg 12/07/22 14:03 1Bromobenzene
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1Bromoform
ND 0.002400.00500 mg/Kg 12/07/22 14:03 1Bromomethane
ND 0.002100.00500 mg/Kg 12/07/22 14:03 1Carbon disulfide
ND 0.002100.00500 mg/Kg 12/07/22 14:03 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 12/07/22 14:03 1Chlorobenzene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 12/07/22 14:03 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1Chloroethane
ND 0.002000.00500 mg/Kg 12/07/22 14:03 1Chloroform
ND 0.002400.00500 mg/Kg 12/07/22 14:03 1Chloromethane
ND 0.002900.00500 mg/Kg 12/07/22 14:03 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 1Dibromomethane
ND 0.002000.00500 mg/Kg 12/07/22 14:03 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 12/07/22 14:03 1Ethyl acetate
ND 0.002100.00500 mg/Kg 12/07/22 14:03 1Ethylbenzene
ND 0.001700.00500 mg/Kg 12/07/22 14:03 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 12/07/22 14:03 1Hexachlorobutadiene
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-753988/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
RL MDL
Hexane ND 0.00500 0.00170 mg/Kg 12/07/22 14:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 12/07/22 14:03 1Iodomethane
ND 0.001500.0100 mg/Kg 12/07/22 14:03 1Isopropyl ether
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 12/07/22 14:03 1Methylene Chloride
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 12/07/22 14:03 1Naphthalene
ND 0.001900.00500 mg/Kg 12/07/22 14:03 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 12/07/22 14:03 1n-Heptane
ND 0.002200.00500 mg/Kg 12/07/22 14:03 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 12/07/22 14:03 1o-Xylene
ND 0.002000.00500 mg/Kg 12/07/22 14:03 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 12/07/22 14:03 1Styrene
ND 0.002500.00500 mg/Kg 12/07/22 14:03 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 12/07/22 14:03 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 12/07/22 14:03 1Toluene
ND 0.002300.00500 mg/Kg 12/07/22 14:03 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 12/07/22 14:03 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 12/07/22 14:03 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 12/07/22 14:03 1Trichloroethene
ND 0.003100.00500 mg/Kg 12/07/22 14:03 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 12/07/22 14:03 1Vinyl acetate
ND 0.002800.00500 mg/Kg 12/07/22 14:03 1Vinyl chloride
ND 0.003600.0100 mg/Kg 12/07/22 14:03 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)94 65-130 12/07/22 14:03 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
95 12/07/22 14:03 14-Bromofluorobenzene (Surr)65-130
102 12/07/22 14:03 1Dibromofluoromethane (Surr)65-130
107 12/07/22 14:03 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-753988/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
1,1,1,2-Tetrachloroethane 0.0500 0.05711 mg/Kg 114 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.05407 mg/Kg 108 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05128 mg/Kg 103 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06404 mg/Kg 128 70 -130
1,1,2-Trichloroethane 0.0500 0.05119 mg/Kg 102 56 -146
1,1-Dichloroethane 0.0500 0.05126 mg/Kg 103 70 -130
1,1-Dichloroethene 0.0500 0.06134 mg/Kg 123 69 -130
1,1-Dichloropropene 0.0500 0.05406 mg/Kg 108 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05337 mg/Kg 107 70 -130
1,2,3-Trichloropropane 0.0500 0.05436 mg/Kg 109 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05511 mg/Kg 110 70 -130
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-753988/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
1,2,4-Trimethylbenzene 0.0500 0.05392 mg/Kg 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.04825 mg/Kg 96 42 -145
1,2-Dichlorobenzene 0.0500 0.05367 mg/Kg 107 70 -130
1,2-Dichloroethane 0.0500 0.05194 mg/Kg 104 68 -139
1,2-Dichloropropane 0.0500 0.05059 mg/Kg 101 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05476 mg/Kg 110 70 -130
1,3-Dichlorobenzene 0.0500 0.05415 mg/Kg 108 70 -130
1,3-Dichloropropane 0.0500 0.05273 mg/Kg 105 54 -150
1,4-Dichlorobenzene 0.0500 0.05306 mg/Kg 106 70 -130
2,2-Dichloropropane 0.0500 0.05355 mg/Kg 107 70 -130
2-Butanone (MEK)0.250 0.2201 mg/Kg 88 40 -150
2-Chlorotoluene 0.0500 0.05269 mg/Kg 105 70 -130
2-Hexanone 0.250 0.2191 mg/Kg 88 30 -150
4-Chlorotoluene 0.0500 0.04811 mg/Kg 96 70 -130
4-Isopropyltoluene 0.0500 0.05083 mg/Kg 102 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2253 mg/Kg 90 34 -150
Acetone 0.250 0.2251 mg/Kg 90 10 -150
Benzene 0.0500 0.05435 mg/Kg 109 70 -130
Bromobenzene 0.0500 0.05857 mg/Kg 117 70 -130
Bromoform 0.0500 0.05532 mg/Kg 111 68 -130
Bromomethane 0.0500 0.05901 mg/Kg 118 70 -130
Carbon disulfide 0.0500 0.06704 *+mg/Kg 134 70 -130
Carbon tetrachloride 0.0500 0.05643 mg/Kg 113 70 -130
Chlorobenzene 0.0500 0.05689 mg/Kg 114 70 -130
Chlorobromomethane 0.0500 0.06090 mg/Kg 122 66 -130
Chlorodibromomethane 0.0500 0.05499 mg/Kg 110 64 -133
Chloroethane 0.0500 0.05508 mg/Kg 110 70 -130
Chloroform 0.0500 0.05180 mg/Kg 104 70 -130
Chloromethane 0.0500 0.04831 mg/Kg 97 70 -130
cis-1,2-Dichloroethene 0.0500 0.05069 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.05057 mg/Kg 101 70 -130
Dibromomethane 0.0500 0.05645 mg/Kg 113 59 -142
Dichlorobromomethane 0.0500 0.05074 mg/Kg 101 70 -130
Ethylbenzene 0.0500 0.05424 mg/Kg 108 70 -130
Ethylene Dibromide 0.0500 0.05577 mg/Kg 112 48 -150
Hexachlorobutadiene 0.0500 0.05774 mg/Kg 115 70 -130
Hexane 0.0500 0.05677 mg/Kg 114 70 -130
Iodomethane 0.0500 0.05893 mg/Kg 118 65 -138
Isopropylbenzene 0.0500 0.05663 mg/Kg 113 70 -130
Methyl tert-butyl ether 0.0500 0.05371 mg/Kg 107 70 -130
Methylene Chloride 0.0500 0.05592 mg/Kg 112 54 -149
m-Xylene & p-Xylene 0.0500 0.05335 mg/Kg 107 70 -130
Naphthalene 0.0500 0.05061 mg/Kg 101 46 -150
n-Butylbenzene 0.0500 0.04855 mg/Kg 97 70 -130
n-Heptane 0.0500 0.05408 mg/Kg 108 70 -130
N-Propylbenzene 0.0500 0.05395 mg/Kg 108 70 -130
o-Xylene 0.0500 0.05437 mg/Kg 109 70 -130
sec-Butylbenzene 0.0500 0.05481 mg/Kg 110 69 -142
Styrene 0.0500 0.05575 mg/Kg 112 70 -130
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-753988/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
tert-Butylbenzene 0.0500 0.05651 mg/Kg 113 67 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tetrachloroethene 0.0500 0.06159 mg/Kg 123 70 -130
Toluene 0.0500 0.05505 mg/Kg 110 70 -130
trans-1,2-Dichloroethene 0.0500 0.05679 mg/Kg 114 67 -130
trans-1,3-Dichloropropene 0.0500 0.05204 mg/Kg 104 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04779 mg/Kg 96 54 -150
Trichloroethene 0.0500 0.05788 mg/Kg 116 70 -130
Trichlorofluoromethane 0.0500 0.06130 mg/Kg 123 70 -130
Vinyl acetate 0.100 0.07959 mg/Kg 80 53 -150
Vinyl chloride 0.0500 0.05174 mg/Kg 103 70 -130
Xylenes, Total 0.100 0.1077 mg/Kg 108 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
994-Bromofluorobenzene (Surr)65 -130
110Dibromofluoromethane (Surr)65 -130
110Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-753988/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
1,1,1,2-Tetrachloroethane 0.0500 0.05666 mg/Kg 113 70 -130 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.05430 mg/Kg 109 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05023 mg/Kg 100 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06329 mg/Kg 127 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.05041 mg/Kg 101 56 -146 2 30
1,1-Dichloroethane 0.0500 0.05036 mg/Kg 101 70 -130 2 30
1,1-Dichloroethene 0.0500 0.05976 mg/Kg 120 69 -130 3 50
1,1-Dichloropropene 0.0500 0.05346 mg/Kg 107 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05293 mg/Kg 106 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.05297 mg/Kg 106 64 -130 3 30
1,2,4-Trichlorobenzene 0.0500 0.05339 mg/Kg 107 70 -130 3 30
1,2,4-Trimethylbenzene 0.0500 0.05413 mg/Kg 108 70 -130 0 30
1,2-Dibromo-3-Chloropropane 0.0500 0.04649 mg/Kg 93 42 -145 4 30
1,2-Dichlorobenzene 0.0500 0.05381 mg/Kg 108 70 -130 0 30
1,2-Dichloroethane 0.0500 0.05127 mg/Kg 103 68 -139 1 30
1,2-Dichloropropane 0.0500 0.04987 mg/Kg 100 70 -130 1 30
1,3,5-Trimethylbenzene 0.0500 0.05479 mg/Kg 110 70 -130 0 30
1,3-Dichlorobenzene 0.0500 0.05342 mg/Kg 107 70 -130 1 30
1,3-Dichloropropane 0.0500 0.05154 mg/Kg 103 54 -150 2 30
1,4-Dichlorobenzene 0.0500 0.05235 mg/Kg 105 70 -130 1 30
2,2-Dichloropropane 0.0500 0.05249 mg/Kg 105 70 -130 2 30
2-Butanone (MEK)0.250 0.2126 mg/Kg 85 40 -150 4 30
2-Chlorotoluene 0.0500 0.05302 mg/Kg 106 70 -130 1 30
2-Hexanone 0.250 0.2101 mg/Kg 84 30 -150 4 30
4-Chlorotoluene 0.0500 0.04736 mg/Kg 95 70 -130 2 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-753988/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
4-Isopropyltoluene 0.0500 0.05092 mg/Kg 102 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Methyl-2-pentanone (MIBK)0.250 0.2187 mg/Kg 87 34 -150 3 30
Acetone 0.250 0.2134 mg/Kg 85 10 -150 5 50
Benzene 0.0500 0.05395 mg/Kg 108 70 -130 1 30
Bromobenzene 0.0500 0.05838 mg/Kg 117 70 -130 0 30
Bromoform 0.0500 0.05439 mg/Kg 109 68 -130 2 30
Bromomethane 0.0500 0.05924 mg/Kg 118 70 -130 0 30
Carbon disulfide 0.0500 0.06621 *+mg/Kg 132 70 -130 1 30
Carbon tetrachloride 0.0500 0.05571 mg/Kg 111 70 -130 1 30
Chlorobenzene 0.0500 0.05673 mg/Kg 113 70 -130 0 30
Chlorobromomethane 0.0500 0.05899 mg/Kg 118 66 -130 3 30
Chlorodibromomethane 0.0500 0.05374 mg/Kg 107 64 -133 2 30
Chloroethane 0.0500 0.05352 mg/Kg 107 70 -130 3 30
Chloroform 0.0500 0.05161 mg/Kg 103 70 -130 0 30
Chloromethane 0.0500 0.04702 mg/Kg 94 70 -130 3 30
cis-1,2-Dichloroethene 0.0500 0.05050 mg/Kg 101 70 -130 0 30
cis-1,3-Dichloropropene 0.0500 0.05020 mg/Kg 100 70 -130 1 30
Dibromomethane 0.0500 0.05517 mg/Kg 110 59 -142 2 30
Dichlorobromomethane 0.0500 0.05018 mg/Kg 100 70 -130 1 30
Ethylbenzene 0.0500 0.05403 mg/Kg 108 70 -130 0 30
Ethylene Dibromide 0.0500 0.05458 mg/Kg 109 48 -150 2 30
Hexachlorobutadiene 0.0500 0.05718 mg/Kg 114 70 -130 1 30
Hexane 0.0500 0.05765 mg/Kg 115 70 -130 2 30
Iodomethane 0.0500 0.05807 mg/Kg 116 65 -138 1 30
Isopropylbenzene 0.0500 0.05618 mg/Kg 112 70 -130 1 30
Methyl tert-butyl ether 0.0500 0.05260 mg/Kg 105 70 -130 2 30
Methylene Chloride 0.0500 0.05595 mg/Kg 112 54 -149 0 30
m-Xylene & p-Xylene 0.0500 0.05314 mg/Kg 106 70 -130 0 30
Naphthalene 0.0500 0.04971 mg/Kg 99 46 -150 2 30
n-Butylbenzene 0.0500 0.04815 mg/Kg 96 70 -130 1 30
n-Heptane 0.0500 0.05403 mg/Kg 108 70 -130 0 30
N-Propylbenzene 0.0500 0.05450 mg/Kg 109 70 -130 1 30
o-Xylene 0.0500 0.05349 mg/Kg 107 70 -130 2 30
sec-Butylbenzene 0.0500 0.05489 mg/Kg 110 69 -142 0 30
Styrene 0.0500 0.05584 mg/Kg 112 70 -130 0 30
tert-Butylbenzene 0.0500 0.05615 mg/Kg 112 67 -145 1 30
Tetrachloroethene 0.0500 0.06140 mg/Kg 123 70 -130 0 30
Toluene 0.0500 0.05472 mg/Kg 109 70 -130 1 30
trans-1,2-Dichloroethene 0.0500 0.05566 mg/Kg 111 67 -130 2 30
trans-1,3-Dichloropropene 0.0500 0.05103 mg/Kg 102 54 -150 2 30
trans-1,4-Dichloro-2-butene 0.0500 0.04675 mg/Kg 93 54 -150 2 30
Trichloroethene 0.0500 0.05791 mg/Kg 116 70 -130 0 30
Trichlorofluoromethane 0.0500 0.05927 mg/Kg 119 70 -130 3 30
Vinyl acetate 0.100 0.07691 mg/Kg 77 53 -150 3 30
Vinyl chloride 0.0500 0.05069 mg/Kg 101 70 -130 2 30
Xylenes, Total 0.100 0.1066 mg/Kg 107 70 -130 1 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-753988/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 753988
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)65 -130
109Dibromofluoromethane (Surr)65 -130
108Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-754199/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 12/08/22 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 12/08/22 13:17 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 12/08/22 13:17 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 12/08/22 13:17 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 12/08/22 13:17 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 12/08/22 13:17 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 12/08/22 13:17 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 12/08/22 13:17 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 12/08/22 13:17 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 12/08/22 13:17 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 12/08/22 13:17 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 12/08/22 13:17 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 12/08/22 13:17 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 12/08/22 13:17 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 12/08/22 13:17 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/08/22 13:17 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 12/08/22 13:17 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/08/22 13:17 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 12/08/22 13:17 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 12/08/22 13:17 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 12/08/22 13:17 12-Hexanone
ND 0.002100.00500 mg/Kg 12/08/22 13:17 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 12/08/22 13:17 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 12/08/22 13:17 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 12/08/22 13:17 1Acetone
ND 0.002400.00500 mg/Kg 12/08/22 13:17 1Benzene
ND 0.001700.00500 mg/Kg 12/08/22 13:17 1Bromobenzene
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1Bromoform
ND 0.002400.00500 mg/Kg 12/08/22 13:17 1Bromomethane
ND 0.002100.00500 mg/Kg 12/08/22 13:17 1Carbon disulfide
ND 0.002100.00500 mg/Kg 12/08/22 13:17 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 12/08/22 13:17 1Chlorobenzene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 12/08/22 13:17 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1Chloroethane
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754199/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
RL MDL
Chloroform ND 0.00500 0.00200 mg/Kg 12/08/22 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002400.00500 mg/Kg 12/08/22 13:17 1Chloromethane
ND 0.002900.00500 mg/Kg 12/08/22 13:17 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 1Dibromomethane
ND 0.002000.00500 mg/Kg 12/08/22 13:17 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 12/08/22 13:17 1Ethyl acetate
ND 0.002100.00500 mg/Kg 12/08/22 13:17 1Ethylbenzene
ND 0.001700.00500 mg/Kg 12/08/22 13:17 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 12/08/22 13:17 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 12/08/22 13:17 1Hexane
ND 0.001700.00500 mg/Kg 12/08/22 13:17 1Iodomethane
ND 0.001500.0100 mg/Kg 12/08/22 13:17 1Isopropyl ether
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 12/08/22 13:17 1Methylene Chloride
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 12/08/22 13:17 1Naphthalene
ND 0.001900.00500 mg/Kg 12/08/22 13:17 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 12/08/22 13:17 1n-Heptane
ND 0.002200.00500 mg/Kg 12/08/22 13:17 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 12/08/22 13:17 1o-Xylene
ND 0.002000.00500 mg/Kg 12/08/22 13:17 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 12/08/22 13:17 1Styrene
ND 0.002500.00500 mg/Kg 12/08/22 13:17 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 12/08/22 13:17 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 12/08/22 13:17 1Toluene
ND 0.002300.00500 mg/Kg 12/08/22 13:17 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 12/08/22 13:17 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 12/08/22 13:17 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 12/08/22 13:17 1Trichloroethene
ND 0.003100.00500 mg/Kg 12/08/22 13:17 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 12/08/22 13:17 1Vinyl acetate
ND 0.002800.00500 mg/Kg 12/08/22 13:17 1Vinyl chloride
ND 0.003600.0100 mg/Kg 12/08/22 13:17 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)92 65-130 12/08/22 13:17 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 12/08/22 13:17 14-Bromofluorobenzene (Surr)65-130
103 12/08/22 13:17 1Dibromofluoromethane (Surr)65-130
107 12/08/22 13:17 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754199/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
1,1,1,2-Tetrachloroethane 0.0500 0.05501 mg/Kg 110 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754199/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
1,1,1-Trichloroethane 0.0500 0.05105 mg/Kg 102 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 0.0500 0.04910 mg/Kg 98 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.05906 mg/Kg 118 70 -130
1,1,2-Trichloroethane 0.0500 0.04955 mg/Kg 99 56 -146
1,1-Dichloroethane 0.0500 0.04904 mg/Kg 98 70 -130
1,1-Dichloroethene 0.0500 0.05672 mg/Kg 113 69 -130
1,1-Dichloropropene 0.0500 0.05102 mg/Kg 102 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05238 mg/Kg 105 70 -130
1,2,3-Trichloropropane 0.0500 0.05142 mg/Kg 103 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05317 mg/Kg 106 70 -130
1,2,4-Trimethylbenzene 0.0500 0.05423 mg/Kg 108 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04510 mg/Kg 90 42 -145
1,2-Dichlorobenzene 0.0500 0.05201 mg/Kg 104 70 -130
1,2-Dichloroethane 0.0500 0.04974 mg/Kg 99 68 -139
1,2-Dichloropropane 0.0500 0.04941 mg/Kg 99 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05415 mg/Kg 108 70 -130
1,3-Dichlorobenzene 0.0500 0.05144 mg/Kg 103 70 -130
1,3-Dichloropropane 0.0500 0.05029 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.05058 mg/Kg 101 70 -130
2,2-Dichloropropane 0.0500 0.04909 mg/Kg 98 70 -130
2-Butanone (MEK)0.250 0.2102 mg/Kg 84 40 -150
2-Chlorotoluene 0.0500 0.05205 mg/Kg 104 70 -130
2-Hexanone 0.250 0.2132 mg/Kg 85 30 -150
4-Chlorotoluene 0.0500 0.04780 mg/Kg 96 70 -130
4-Isopropyltoluene 0.0500 0.04929 mg/Kg 99 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2186 mg/Kg 87 34 -150
Acetone 0.250 0.2174 mg/Kg 87 10 -150
Benzene 0.0500 0.05219 mg/Kg 104 70 -130
Bromobenzene 0.0500 0.05757 mg/Kg 115 70 -130
Bromoform 0.0500 0.05260 mg/Kg 105 68 -130
Bromomethane 0.0500 0.05717 mg/Kg 114 70 -130
Carbon disulfide 0.0500 0.06221 mg/Kg 124 70 -130
Carbon tetrachloride 0.0500 0.05273 mg/Kg 105 70 -130
Chlorobenzene 0.0500 0.05495 mg/Kg 110 70 -130
Chlorobromomethane 0.0500 0.05700 mg/Kg 114 66 -130
Chlorodibromomethane 0.0500 0.05277 mg/Kg 106 64 -133
Chloroethane 0.0500 0.05053 mg/Kg 101 70 -130
Chloroform 0.0500 0.05042 mg/Kg 101 70 -130
Chloromethane 0.0500 0.04509 mg/Kg 90 70 -130
cis-1,2-Dichloroethene 0.0500 0.04906 mg/Kg 98 70 -130
cis-1,3-Dichloropropene 0.0500 0.04893 mg/Kg 98 70 -130
Dibromomethane 0.0500 0.05342 mg/Kg 107 59 -142
Dichlorobromomethane 0.0500 0.04917 mg/Kg 98 70 -130
Ethylbenzene 0.0500 0.05309 mg/Kg 106 70 -130
Ethylene Dibromide 0.0500 0.05420 mg/Kg 108 48 -150
Hexachlorobutadiene 0.0500 0.05732 mg/Kg 115 70 -130
Hexane 0.0500 0.05458 mg/Kg 109 70 -130
Iodomethane 0.0500 0.05648 mg/Kg 113 65 -138
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754199/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
Isopropylbenzene 0.0500 0.05555 mg/Kg 111 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methyl tert-butyl ether 0.0500 0.05125 mg/Kg 103 70 -130
Methylene Chloride 0.0500 0.05357 mg/Kg 107 54 -149
m-Xylene & p-Xylene 0.0500 0.05302 mg/Kg 106 70 -130
Naphthalene 0.0500 0.04852 mg/Kg 97 46 -150
n-Butylbenzene 0.0500 0.04751 mg/Kg 95 70 -130
n-Heptane 0.0500 0.05177 mg/Kg 104 70 -130
N-Propylbenzene 0.0500 0.05292 mg/Kg 106 70 -130
o-Xylene 0.0500 0.05285 mg/Kg 106 70 -130
sec-Butylbenzene 0.0500 0.05509 mg/Kg 110 69 -142
Styrene 0.0500 0.05469 mg/Kg 109 70 -130
tert-Butylbenzene 0.0500 0.05570 mg/Kg 111 67 -145
Tetrachloroethene 0.0500 0.06250 mg/Kg 125 70 -130
Toluene 0.0500 0.05364 mg/Kg 107 70 -130
trans-1,2-Dichloroethene 0.0500 0.05364 mg/Kg 107 67 -130
trans-1,3-Dichloropropene 0.0500 0.05007 mg/Kg 100 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04538 mg/Kg 91 54 -150
Trichloroethene 0.0500 0.05652 mg/Kg 113 70 -130
Trichlorofluoromethane 0.0500 0.05489 mg/Kg 110 70 -130
Vinyl acetate 0.100 0.07545 mg/Kg 75 53 -150
Vinyl chloride 0.0500 0.04834 mg/Kg 97 70 -130
Xylenes, Total 0.100 0.1059 mg/Kg 106 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr)65 -130
106Dibromofluoromethane (Surr)65 -130
106Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754199/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
1,1,1,2-Tetrachloroethane 0.0500 0.05747 mg/Kg 115 70 -130 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.05281 mg/Kg 106 70 -130 3 30
1,1,2,2-Tetrachloroethane 0.0500 0.05169 mg/Kg 103 64 -130 5 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06162 mg/Kg 123 70 -130 4 40
1,1,2-Trichloroethane 0.0500 0.05121 mg/Kg 102 56 -146 3 30
1,1-Dichloroethane 0.0500 0.05040 mg/Kg 101 70 -130 3 30
1,1-Dichloroethene 0.0500 0.05786 mg/Kg 116 69 -130 2 50
1,1-Dichloropropene 0.0500 0.05241 mg/Kg 105 70 -130 3 30
1,2,3-Trichlorobenzene 0.0500 0.05511 mg/Kg 110 70 -130 5 30
1,2,3-Trichloropropane 0.0500 0.05513 mg/Kg 110 64 -130 7 30
1,2,4-Trichlorobenzene 0.0500 0.05548 mg/Kg 111 70 -130 4 30
1,2,4-Trimethylbenzene 0.0500 0.05474 mg/Kg 109 70 -130 1 30
1,2-Dibromo-3-Chloropropane 0.0500 0.04876 mg/Kg 98 42 -145 8 30
1,2-Dichlorobenzene 0.0500 0.05437 mg/Kg 109 70 -130 4 30
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754199/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
1,2-Dichloroethane 0.0500 0.05158 mg/Kg 103 68 -139 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloropropane 0.0500 0.04995 mg/Kg 100 70 -130 1 30
1,3,5-Trimethylbenzene 0.0500 0.05432 mg/Kg 109 70 -130 0 30
1,3-Dichlorobenzene 0.0500 0.05485 mg/Kg 110 70 -130 6 30
1,3-Dichloropropane 0.0500 0.05175 mg/Kg 103 54 -150 3 30
1,4-Dichlorobenzene 0.0500 0.05338 mg/Kg 107 70 -130 5 30
2,2-Dichloropropane 0.0500 0.05050 mg/Kg 101 70 -130 3 30
2-Butanone (MEK)0.250 0.2181 mg/Kg 87 40 -150 4 30
2-Chlorotoluene 0.0500 0.05302 mg/Kg 106 70 -130 2 30
2-Hexanone 0.250 0.2175 mg/Kg 87 30 -150 2 30
4-Chlorotoluene 0.0500 0.04832 mg/Kg 97 70 -130 1 30
4-Isopropyltoluene 0.0500 0.05064 mg/Kg 101 70 -130 3 30
4-Methyl-2-pentanone (MIBK)0.250 0.2231 mg/Kg 89 34 -150 2 30
Acetone 0.250 0.2152 mg/Kg 86 10 -150 1 50
Benzene 0.0500 0.05344 mg/Kg 107 70 -130 2 30
Bromobenzene 0.0500 0.05910 mg/Kg 118 70 -130 3 30
Bromoform 0.0500 0.05428 mg/Kg 109 68 -130 3 30
Bromomethane 0.0500 0.05831 mg/Kg 117 70 -130 2 30
Carbon disulfide 0.0500 0.06374 mg/Kg 127 70 -130 2 30
Carbon tetrachloride 0.0500 0.05441 mg/Kg 109 70 -130 3 30
Chlorobenzene 0.0500 0.05706 mg/Kg 114 70 -130 4 30
Chlorobromomethane 0.0500 0.05882 mg/Kg 118 66 -130 3 30
Chlorodibromomethane 0.0500 0.05406 mg/Kg 108 64 -133 2 30
Chloroethane 0.0500 0.05295 mg/Kg 106 70 -130 5 30
Chloroform 0.0500 0.05170 mg/Kg 103 70 -130 2 30
Chloromethane 0.0500 0.04737 mg/Kg 95 70 -130 5 30
cis-1,2-Dichloroethene 0.0500 0.05027 mg/Kg 101 70 -130 2 30
cis-1,3-Dichloropropene 0.0500 0.05014 mg/Kg 100 70 -130 2 30
Dibromomethane 0.0500 0.05538 mg/Kg 111 59 -142 4 30
Dichlorobromomethane 0.0500 0.05007 mg/Kg 100 70 -130 2 30
Ethylbenzene 0.0500 0.05403 mg/Kg 108 70 -130 2 30
Ethylene Dibromide 0.0500 0.05519 mg/Kg 110 48 -150 2 30
Hexachlorobutadiene 0.0500 0.05682 mg/Kg 114 70 -130 1 30
Hexane 0.0500 0.05504 mg/Kg 110 70 -130 1 30
Iodomethane 0.0500 0.05842 mg/Kg 117 65 -138 3 30
Isopropylbenzene 0.0500 0.05548 mg/Kg 111 70 -130 0 30
Methyl tert-butyl ether 0.0500 0.05276 mg/Kg 106 70 -130 3 30
Methylene Chloride 0.0500 0.05461 mg/Kg 109 54 -149 2 30
m-Xylene & p-Xylene 0.0500 0.05324 mg/Kg 106 70 -130 0 30
Naphthalene 0.0500 0.05124 mg/Kg 102 46 -150 5 30
n-Butylbenzene 0.0500 0.04778 mg/Kg 96 70 -130 1 30
n-Heptane 0.0500 0.05222 mg/Kg 104 70 -130 1 30
N-Propylbenzene 0.0500 0.05377 mg/Kg 108 70 -130 2 30
o-Xylene 0.0500 0.05416 mg/Kg 108 70 -130 2 30
sec-Butylbenzene 0.0500 0.05403 mg/Kg 108 69 -142 2 30
Styrene 0.0500 0.05567 mg/Kg 111 70 -130 2 30
tert-Butylbenzene 0.0500 0.05559 mg/Kg 111 67 -145 0 30
Tetrachloroethene 0.0500 0.06304 mg/Kg 126 70 -130 1 30
Toluene 0.0500 0.05481 mg/Kg 110 70 -130 2 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754199/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754199
trans-1,2-Dichloroethene 0.0500 0.05587 mg/Kg 112 67 -130 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 0.0500 0.05125 mg/Kg 103 54 -150 2 30
trans-1,4-Dichloro-2-butene 0.0500 0.04707 mg/Kg 94 54 -150 4 30
Trichloroethene 0.0500 0.05754 mg/Kg 115 70 -130 2 30
Trichlorofluoromethane 0.0500 0.05902 mg/Kg 118 70 -130 7 30
Vinyl acetate 0.100 0.07674 mg/Kg 77 53 -150 2 30
Vinyl chloride 0.0500 0.05041 mg/Kg 101 70 -130 4 30
Xylenes, Total 0.100 0.1074 mg/Kg 107 70 -130 1 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)65 -130
110Dibromofluoromethane (Surr)65 -130
108Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-754381/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 12/09/22 12:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 12/09/22 12:35 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 12/09/22 12:35 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 12/09/22 12:35 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 12/09/22 12:35 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 12/09/22 12:35 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 12/09/22 12:35 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 12/09/22 12:35 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 12/09/22 12:35 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 12/09/22 12:35 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 12/09/22 12:35 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 12/09/22 12:35 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 12/09/22 12:35 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 12/09/22 12:35 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 12/09/22 12:35 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/09/22 12:35 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 12/09/22 12:35 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 12/09/22 12:35 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 12/09/22 12:35 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 12/09/22 12:35 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 12/09/22 12:35 12-Hexanone
ND 0.002100.00500 mg/Kg 12/09/22 12:35 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 12/09/22 12:35 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 12/09/22 12:35 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 12/09/22 12:35 1Acetone
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754381/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
RL MDL
Benzene ND 0.00500 0.00240 mg/Kg 12/09/22 12:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 12/09/22 12:35 1Bromobenzene
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1Bromoform
ND 0.002400.00500 mg/Kg 12/09/22 12:35 1Bromomethane
ND 0.002100.00500 mg/Kg 12/09/22 12:35 1Carbon disulfide
ND 0.002100.00500 mg/Kg 12/09/22 12:35 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 12/09/22 12:35 1Chlorobenzene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 12/09/22 12:35 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1Chloroethane
ND 0.002000.00500 mg/Kg 12/09/22 12:35 1Chloroform
ND 0.002400.00500 mg/Kg 12/09/22 12:35 1Chloromethane
ND 0.002900.00500 mg/Kg 12/09/22 12:35 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 1Dibromomethane
ND 0.002000.00500 mg/Kg 12/09/22 12:35 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 12/09/22 12:35 1Ethyl acetate
ND 0.002100.00500 mg/Kg 12/09/22 12:35 1Ethylbenzene
ND 0.001700.00500 mg/Kg 12/09/22 12:35 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 12/09/22 12:35 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 12/09/22 12:35 1Hexane
ND 0.001700.00500 mg/Kg 12/09/22 12:35 1Iodomethane
ND 0.001500.0100 mg/Kg 12/09/22 12:35 1Isopropyl ether
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 12/09/22 12:35 1Methylene Chloride
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 12/09/22 12:35 1Naphthalene
ND 0.001900.00500 mg/Kg 12/09/22 12:35 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 12/09/22 12:35 1n-Heptane
ND 0.002200.00500 mg/Kg 12/09/22 12:35 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 12/09/22 12:35 1o-Xylene
ND 0.002000.00500 mg/Kg 12/09/22 12:35 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 12/09/22 12:35 1Styrene
ND 0.002500.00500 mg/Kg 12/09/22 12:35 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 12/09/22 12:35 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 12/09/22 12:35 1Toluene
ND 0.002300.00500 mg/Kg 12/09/22 12:35 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 12/09/22 12:35 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 12/09/22 12:35 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 12/09/22 12:35 1Trichloroethene
ND 0.003100.00500 mg/Kg 12/09/22 12:35 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 12/09/22 12:35 1Vinyl acetate
ND 0.002800.00500 mg/Kg 12/09/22 12:35 1Vinyl chloride
ND 0.003600.0100 mg/Kg 12/09/22 12:35 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)91 65-130 12/09/22 12:35 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754381/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
4-Bromofluorobenzene (Surr)94 65-130 12/09/22 12:35 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 12/09/22 12:35 1Dibromofluoromethane (Surr)65-130
105 12/09/22 12:35 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754381/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
1,1,1,2-Tetrachloroethane 0.0500 0.05692 mg/Kg 114 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.05279 mg/Kg 106 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05066 mg/Kg 101 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06161 mg/Kg 123 70 -130
1,1,2-Trichloroethane 0.0500 0.04949 mg/Kg 99 56 -146
1,1-Dichloroethane 0.0500 0.04937 mg/Kg 99 70 -130
1,1-Dichloroethene 0.0500 0.05867 mg/Kg 117 69 -130
1,1-Dichloropropene 0.0500 0.05279 mg/Kg 106 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05251 mg/Kg 105 70 -130
1,2,3-Trichloropropane 0.0500 0.05446 mg/Kg 109 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05428 mg/Kg 109 70 -130
1,2,4-Trimethylbenzene 0.0500 0.05541 mg/Kg 111 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04657 mg/Kg 93 42 -145
1,2-Dichlorobenzene 0.0500 0.05337 mg/Kg 107 70 -130
1,2-Dichloroethane 0.0500 0.04996 mg/Kg 100 68 -139
1,2-Dichloropropane 0.0500 0.04880 mg/Kg 98 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05517 mg/Kg 110 70 -130
1,3-Dichlorobenzene 0.0500 0.05315 mg/Kg 106 70 -130
1,3-Dichloropropane 0.0500 0.05059 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.05188 mg/Kg 104 70 -130
2,2-Dichloropropane 0.0500 0.05128 mg/Kg 103 70 -130
2-Butanone (MEK)0.250 0.2099 mg/Kg 84 40 -150
2-Chlorotoluene 0.0500 0.05346 mg/Kg 107 70 -130
2-Hexanone 0.250 0.2111 mg/Kg 84 30 -150
4-Chlorotoluene 0.0500 0.04834 mg/Kg 97 70 -130
4-Isopropyltoluene 0.0500 0.05172 mg/Kg 103 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2186 mg/Kg 87 34 -150
Acetone 0.250 0.2148 mg/Kg 86 10 -150
Benzene 0.0500 0.05308 mg/Kg 106 70 -130
Bromobenzene 0.0500 0.05890 mg/Kg 118 70 -130
Bromoform 0.0500 0.05454 mg/Kg 109 68 -130
Bromomethane 0.0500 0.05615 mg/Kg 112 70 -130
Carbon disulfide 0.0500 0.06388 mg/Kg 128 70 -130
Carbon tetrachloride 0.0500 0.05518 mg/Kg 110 70 -130
Chlorobenzene 0.0500 0.05667 mg/Kg 113 70 -130
Chlorobromomethane 0.0500 0.05731 mg/Kg 115 66 -130
Chlorodibromomethane 0.0500 0.05300 mg/Kg 106 64 -133
Chloroethane 0.0500 0.05105 mg/Kg 102 70 -130
Chloroform 0.0500 0.05042 mg/Kg 101 70 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754381/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
Chloromethane 0.0500 0.04464 mg/Kg 89 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
cis-1,2-Dichloroethene 0.0500 0.04896 mg/Kg 98 70 -130
cis-1,3-Dichloropropene 0.0500 0.04848 mg/Kg 97 70 -130
Dibromomethane 0.0500 0.05380 mg/Kg 108 59 -142
Dichlorobromomethane 0.0500 0.04870 mg/Kg 97 70 -130
Ethylbenzene 0.0500 0.05453 mg/Kg 109 70 -130
Ethylene Dibromide 0.0500 0.05387 mg/Kg 108 48 -150
Hexachlorobutadiene 0.0500 0.05861 mg/Kg 117 70 -130
Hexane 0.0500 0.05619 mg/Kg 112 70 -130
Iodomethane 0.0500 0.05643 mg/Kg 113 65 -138
Isopropylbenzene 0.0500 0.05689 mg/Kg 114 70 -130
Methyl tert-butyl ether 0.0500 0.05107 mg/Kg 102 70 -130
Methylene Chloride 0.0500 0.05267 mg/Kg 105 54 -149
m-Xylene & p-Xylene 0.0500 0.05408 mg/Kg 108 70 -130
Naphthalene 0.0500 0.04909 mg/Kg 98 46 -150
n-Butylbenzene 0.0500 0.04958 mg/Kg 99 70 -130
n-Heptane 0.0500 0.05370 mg/Kg 107 70 -130
N-Propylbenzene 0.0500 0.05522 mg/Kg 110 70 -130
o-Xylene 0.0500 0.05371 mg/Kg 107 70 -130
sec-Butylbenzene 0.0500 0.05618 mg/Kg 112 69 -142
Styrene 0.0500 0.05612 mg/Kg 112 70 -130
tert-Butylbenzene 0.0500 0.05799 mg/Kg 116 67 -145
Tetrachloroethene 0.0500 0.06272 mg/Kg 125 70 -130
Toluene 0.0500 0.05476 mg/Kg 110 70 -130
trans-1,2-Dichloroethene 0.0500 0.05416 mg/Kg 108 67 -130
trans-1,3-Dichloropropene 0.0500 0.04996 mg/Kg 100 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04689 mg/Kg 94 54 -150
Trichloroethene 0.0500 0.05651 mg/Kg 113 70 -130
Trichlorofluoromethane 0.0500 0.05536 mg/Kg 111 70 -130
Vinyl acetate 0.100 0.07505 mg/Kg 75 53 -150
Vinyl chloride 0.0500 0.04728 mg/Kg 95 70 -130
Xylenes, Total 0.100 0.1078 mg/Kg 108 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)65 -130
106Dibromofluoromethane (Surr)65 -130
108Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754381/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
1,1,1,2-Tetrachloroethane 0.0500 0.05559 mg/Kg 111 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.05233 mg/Kg 105 70 -130 1 30
1,1,2,2-Tetrachloroethane 0.0500 0.05133 mg/Kg 103 64 -130 1 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.06095 mg/Kg 122 70 -130 1 40
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754381/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
1,1,2-Trichloroethane 0.0500 0.04993 mg/Kg 100 56 -146 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1-Dichloroethane 0.0500 0.04947 mg/Kg 99 70 -130 0 30
1,1-Dichloroethene 0.0500 0.05845 mg/Kg 117 69 -130 0 50
1,1-Dichloropropene 0.0500 0.05276 mg/Kg 106 70 -130 0 30
1,2,3-Trichlorobenzene 0.0500 0.05285 mg/Kg 106 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.05331 mg/Kg 107 64 -130 2 30
1,2,4-Trichlorobenzene 0.0500 0.05513 mg/Kg 110 70 -130 2 30
1,2,4-Trimethylbenzene 0.0500 0.05379 mg/Kg 108 70 -130 3 30
1,2-Dibromo-3-Chloropropane 0.0500 0.04968 mg/Kg 99 42 -145 6 30
1,2-Dichlorobenzene 0.0500 0.05415 mg/Kg 108 70 -130 1 30
1,2-Dichloroethane 0.0500 0.04960 mg/Kg 99 68 -139 1 30
1,2-Dichloropropane 0.0500 0.04903 mg/Kg 98 70 -130 0 30
1,3,5-Trimethylbenzene 0.0500 0.05384 mg/Kg 108 70 -130 2 30
1,3-Dichlorobenzene 0.0500 0.05349 mg/Kg 107 70 -130 1 30
1,3-Dichloropropane 0.0500 0.05099 mg/Kg 102 54 -150 1 30
1,4-Dichlorobenzene 0.0500 0.05349 mg/Kg 107 70 -130 3 30
2,2-Dichloropropane 0.0500 0.05131 mg/Kg 103 70 -130 0 30
2-Butanone (MEK)0.250 0.2085 mg/Kg 83 40 -150 1 30
2-Chlorotoluene 0.0500 0.05244 mg/Kg 105 70 -130 2 30
2-Hexanone 0.250 0.2140 mg/Kg 86 30 -150 1 30
4-Chlorotoluene 0.0500 0.04762 mg/Kg 95 70 -130 1 30
4-Isopropyltoluene 0.0500 0.05107 mg/Kg 102 70 -130 1 30
4-Methyl-2-pentanone (MIBK)0.250 0.2201 mg/Kg 88 34 -150 1 30
Acetone 0.250 0.2134 mg/Kg 85 10 -150 1 50
Benzene 0.0500 0.05208 mg/Kg 104 70 -130 2 30
Bromobenzene 0.0500 0.05732 mg/Kg 115 70 -130 3 30
Bromoform 0.0500 0.05342 mg/Kg 107 68 -130 2 30
Bromomethane 0.0500 0.05844 mg/Kg 117 70 -130 4 30
Carbon disulfide 0.0500 0.06415 mg/Kg 128 70 -130 0 30
Carbon tetrachloride 0.0500 0.05459 mg/Kg 109 70 -130 1 30
Chlorobenzene 0.0500 0.05532 mg/Kg 111 70 -130 2 30
Chlorobromomethane 0.0500 0.05767 mg/Kg 115 66 -130 1 30
Chlorodibromomethane 0.0500 0.05282 mg/Kg 106 64 -133 0 30
Chloroethane 0.0500 0.05425 mg/Kg 109 70 -130 6 30
Chloroform 0.0500 0.04986 mg/Kg 100 70 -130 1 30
Chloromethane 0.0500 0.04662 mg/Kg 93 70 -130 4 30
cis-1,2-Dichloroethene 0.0500 0.04987 mg/Kg 100 70 -130 2 30
cis-1,3-Dichloropropene 0.0500 0.04855 mg/Kg 97 70 -130 0 30
Dibromomethane 0.0500 0.05313 mg/Kg 106 59 -142 1 30
Dichlorobromomethane 0.0500 0.04912 mg/Kg 98 70 -130 1 30
Ethylbenzene 0.0500 0.05318 mg/Kg 106 70 -130 2 30
Ethylene Dibromide 0.0500 0.05396 mg/Kg 108 48 -150 0 30
Hexachlorobutadiene 0.0500 0.05807 mg/Kg 116 70 -130 1 30
Hexane 0.0500 0.05336 mg/Kg 107 70 -130 5 30
Iodomethane 0.0500 0.05777 mg/Kg 116 65 -138 2 30
Isopropylbenzene 0.0500 0.05527 mg/Kg 111 70 -130 3 30
Methyl tert-butyl ether 0.0500 0.05082 mg/Kg 102 70 -130 0 30
Methylene Chloride 0.0500 0.05382 mg/Kg 108 54 -149 2 30
m-Xylene & p-Xylene 0.0500 0.05265 mg/Kg 105 70 -130 3 30
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-754381/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754381
Naphthalene 0.0500 0.05027 mg/Kg 101 46 -150 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
n-Butylbenzene 0.0500 0.04890 mg/Kg 98 70 -130 1 30
n-Heptane 0.0500 0.05274 mg/Kg 105 70 -130 2 30
N-Propylbenzene 0.0500 0.05349 mg/Kg 107 70 -130 3 30
o-Xylene 0.0500 0.05278 mg/Kg 106 70 -130 2 30
sec-Butylbenzene 0.0500 0.05497 mg/Kg 110 69 -142 2 30
Styrene 0.0500 0.05453 mg/Kg 109 70 -130 3 30
tert-Butylbenzene 0.0500 0.05527 mg/Kg 111 67 -145 5 30
Tetrachloroethene 0.0500 0.06153 mg/Kg 123 70 -130 2 30
Toluene 0.0500 0.05356 mg/Kg 107 70 -130 2 30
trans-1,2-Dichloroethene 0.0500 0.05677 mg/Kg 114 67 -130 5 30
trans-1,3-Dichloropropene 0.0500 0.05025 mg/Kg 101 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04651 mg/Kg 93 54 -150 1 30
Trichloroethene 0.0500 0.05615 mg/Kg 112 70 -130 1 30
Trichlorofluoromethane 0.0500 0.06036 mg/Kg 121 70 -130 9 30
Vinyl acetate 0.100 0.07379 mg/Kg 74 53 -150 2 30
Vinyl chloride 0.0500 0.05088 mg/Kg 102 70 -130 7 30
Xylenes, Total 0.100 0.1054 mg/Kg 105 70 -130 2 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
994-Bromofluorobenzene (Surr)65 -130
107Dibromofluoromethane (Surr)65 -130
106Toluene-d8 (Surr)65 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-753897/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
RL MDL
1,1'-Biphenyl ND 1.60 1.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03300.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4,5-Trichlorophenol
ND 0.02740.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4,6-Trichlorophenol
ND 0.03300.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4-Dichlorophenol
ND 0.04150.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4-Dimethylphenol
ND 0.7841.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4-Dinitrophenol
ND 0.04630.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,4-Dinitrotoluene
ND 0.03960.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12,6-Dinitrotoluene
ND 0.03300.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Chloronaphthalene
ND 0.03780.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Chlorophenol
ND 0.03590.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Methylnaphthalene
ND 0.02550.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Methylphenol
ND 0.04251.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Nitroaniline
ND 0.03870.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 12-Nitrophenol
ND 0.04060.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 13 & 4 Methylphenol
ND 0.02640.623 mg/Kg 12/06/22 18:15 12/07/22 15:26 13,3'-Dichlorobenzidine
ND 0.04341.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 13-Nitroaniline
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-753897/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
RL MDL
4,6-Dinitro-2-methylphenol ND 1.60 0.160 mg/Kg 12/06/22 18:15 12/07/22 15:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03400.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Bromophenyl phenyl ether
ND 0.03300.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Chloro-3-methylphenol
ND 0.04910.623 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Chloroaniline
ND 0.04150.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Chlorophenyl phenyl ether
ND 0.04631.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Nitroaniline
ND 0.3121.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 14-Nitrophenol
ND 0.03870.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Acenaphthene
ND 0.03400.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Acenaphthylene
ND 0.02640.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Acetophenone
ND 0.02360.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Anthracene
ND 0.02170.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Atrazine
ND 0.05480.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzaldehyde
ND 0.02550.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzo[a]anthracene
ND 0.04910.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzo[a]pyrene
ND 0.03590.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzo[b]fluoranthene
ND 0.02080.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzo[g,h,i]perylene
ND 0.06140.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Benzo[k]fluoranthene
ND 0.02830.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1bis (2-chloroisopropyl) ether
ND 0.03680.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Bis(2-chloroethoxy)methane
ND 0.04250.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Bis(2-chloroethyl)ether
ND 0.02740.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Bis(2-ethylhexyl) phthalate
ND 0.02450.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Butyl benzyl phthalate
ND 0.06230.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Caprolactam
ND 0.02830.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Carbazole
ND 0.01980.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Chrysene
ND 0.03680.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Dibenz(a,h)anthracene
ND 0.03120.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Dibenzofuran
ND 0.03490.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Diethyl phthalate
ND 0.03210.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Dimethyl phthalate
ND 0.02830.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Di-n-butyl phthalate
ND 0.02740.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Di-n-octyl phthalate
ND 0.03020.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Fluoranthene
ND 0.03400.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Fluorene
ND 0.03680.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Hexachlorobenzene
ND 0.03400.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Hexachlorobutadiene
ND 0.03870.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Hexachlorocyclopentadiene
ND 0.02640.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Hexachloroethane
ND 0.02640.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Indeno[1,2,3-cd]pyrene
ND 0.03120.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Isophorone
ND 0.02830.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Naphthalene
ND 0.02450.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Nitrobenzene
ND 0.03020.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1N-Nitrosodi-n-propylamine
ND 0.03120.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1N-Nitrosodiphenylamine
ND 0.3121.60 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Pentachlorophenol
ND 0.02550.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Phenanthrene
ND 0.03210.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Phenol
ND 0.02550.312 mg/Kg 12/06/22 18:15 12/07/22 15:26 1Pyrene
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-753897/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
2,4,6-Tribromophenol (Surr)89 21-132 12/07/22 15:26 1
MB MB
Surrogate
12/06/22 18:15
Dil FacPreparedAnalyzedQualifierLimits%Recovery
65 12/06/22 18:15 12/07/22 15:26 12-Fluorobiphenyl (Surr)25-130
52 12/06/22 18:15 12/07/22 15:26 12-Fluorophenol (Surr)18-130
54 12/06/22 18:15 12/07/22 15:26 1Nitrobenzene-d5 (Surr)19-130
53 12/06/22 18:15 12/07/22 15:26 1Phenol-d5 (Surr)21-130
82 12/06/22 18:15 12/07/22 15:26 1Terphenyl-d14 (Surr)31-133
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-753897/22-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
1,1'-Biphenyl 6.49 4.407 mg/Kg 68 32 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4,5-Trichlorophenol 6.49 5.556 mg/Kg 86 33 -130
2,4,6-Trichlorophenol 6.49 5.447 mg/Kg 84 31 -130
2,4-Dichlorophenol 6.49 4.977 mg/Kg 77 30 -130
2,4-Dimethylphenol 6.49 4.578 mg/Kg 71 34 -130
2,4-Dinitrophenol 13.0 15.12 mg/Kg 116 10 -130
2,4-Dinitrotoluene 6.49 5.566 mg/Kg 86 34 -130
2,6-Dinitrotoluene 6.49 5.230 mg/Kg 81 33 -130
2-Chloronaphthalene 6.49 4.590 mg/Kg 71 30 -130
2-Chlorophenol 6.49 4.186 mg/Kg 64 28 -130
2-Methylnaphthalene 6.49 4.493 mg/Kg 69 28 -130
2-Methylphenol 6.49 4.256 mg/Kg 66 30 -130
2-Nitroaniline 6.49 4.810 mg/Kg 74 26 -130
2-Nitrophenol 6.49 4.436 mg/Kg 68 24 -130
3 & 4 Methylphenol 6.49 4.215 mg/Kg 65 31 -130
3,3'-Dichlorobenzidine 6.49 6.570 mg/Kg 101 10 -130
3-Nitroaniline 6.49 4.996 mg/Kg 77 10 -130
4,6-Dinitro-2-methylphenol 13.0 14.10 mg/Kg 109 22 -130
4-Bromophenyl phenyl ether 6.49 5.461 mg/Kg 84 32 -130
4-Chloro-3-methylphenol 6.49 5.312 mg/Kg 82 31 -130
4-Chloroaniline 6.49 4.314 mg/Kg 66 10 -130
4-Chlorophenyl phenyl ether 6.49 5.224 mg/Kg 80 32 -130
4-Nitroaniline 6.49 5.396 mg/Kg 83 25 -130
4-Nitrophenol 13.0 12.36 mg/Kg 95 25 -130
Acenaphthene 6.49 4.670 mg/Kg 72 33 -130
Acenaphthylene 6.49 4.928 mg/Kg 76 34 -130
Acetophenone 6.49 4.229 mg/Kg 65 28 -130
Anthracene 6.49 5.181 mg/Kg 80 39 -130
Atrazine 6.49 5.084 mg/Kg 78 27 -130
Benzaldehyde 6.49 2.187 mg/Kg 34 10 -130
Benzo[a]anthracene 6.49 5.841 mg/Kg 90 40 -130
Benzo[a]pyrene 6.49 5.311 mg/Kg 82 37 -131
Benzo[b]fluoranthene 6.49 5.078 mg/Kg 78 35 -130
Benzo[g,h,i]perylene 6.49 5.701 mg/Kg 88 39 -130
Benzo[k]fluoranthene 6.49 5.444 mg/Kg 84 35 -130
bis (2-chloroisopropyl) ether 6.49 3.061 mg/Kg 47 12 -130
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-753897/22-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
Bis(2-chloroethoxy)methane 6.49 3.965 mg/Kg 61 29 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Bis(2-chloroethyl)ether 6.49 3.254 mg/Kg 50 18 -130
Bis(2-ethylhexyl) phthalate 6.49 5.473 mg/Kg 84 39 -130
Butyl benzyl phthalate 6.49 5.504 mg/Kg 85 38 -130
Caprolactam 6.49 4.394 mg/Kg 68 27 -148
Carbazole 6.49 5.390 mg/Kg 83 43 -130
Chrysene 6.49 5.354 mg/Kg 82 40 -130
Dibenz(a,h)anthracene 6.49 5.853 mg/Kg 90 37 -130
Dibenzofuran 6.49 4.808 mg/Kg 74 34 -130
Diethyl phthalate 6.49 5.391 mg/Kg 83 36 -130
Dimethyl phthalate 6.49 5.237 mg/Kg 81 36 -130
Di-n-butyl phthalate 6.49 5.298 mg/Kg 82 39 -130
Di-n-octyl phthalate 6.49 5.634 mg/Kg 87 38 -131
Fluoranthene 6.49 5.496 mg/Kg 85 38 -130
Fluorene 6.49 5.045 mg/Kg 78 34 -130
Hexachlorobenzene 6.49 5.460 mg/Kg 84 28 -130
Hexachlorobutadiene 6.49 4.603 mg/Kg 71 22 -130
Hexachlorocyclopentadiene 6.49 5.007 mg/Kg 77 11 -130
Hexachloroethane 6.49 3.475 mg/Kg 54 21 -130
Indeno[1,2,3-cd]pyrene 6.49 6.830 mg/Kg 105 40 -130
Isophorone 6.49 4.097 mg/Kg 63 26 -130
Naphthalene 6.49 4.158 mg/Kg 64 25 -130
Nitrobenzene 6.49 3.995 mg/Kg 62 25 -130
N-Nitrosodi-n-propylamine 6.49 3.807 mg/Kg 59 24 -130
N-Nitrosodiphenylamine 6.49 4.878 mg/Kg 75 37 -130
Pentachlorophenol 13.0 14.62 mg/Kg 113 16 -135
Phenanthrene 6.49 4.961 mg/Kg 76 38 -130
Phenol 6.49 3.660 mg/Kg 56 27 -130
Pyrene 6.49 5.473 mg/Kg 84 40 -130
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
712-Fluorobiphenyl (Surr)25 -130
592-Fluorophenol (Surr)18 -130
63Nitrobenzene-d5 (Surr)19 -130
61Phenol-d5 (Surr)21 -130
88Terphenyl-d14 (Surr)31 -133
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
1,1'-Biphenyl ND 7.38 4.657 mg/Kg 63 32 -130☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
2,4,5-Trichlorophenol ND 7.38 5.691 mg/Kg 77 33 -130☼
2,4,6-Trichlorophenol ND 7.38 5.720 mg/Kg 78 31 -130☼
2,4-Dichlorophenol ND 7.38 5.238 mg/Kg 71 30 -130☼
2,4-Dimethylphenol ND 7.38 4.702 mg/Kg 64 34 -130☼
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Page 105 of 137 12/14/2022
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
2,4-Dinitrophenol ND 14.8 16.37 mg/Kg 111 10 -130☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
2,4-Dinitrotoluene ND 7.38 5.497 mg/Kg 75 34 -130☼
2,6-Dinitrotoluene ND 7.38 5.511 mg/Kg 75 33 -130☼
2-Chloronaphthalene ND 7.38 4.733 mg/Kg 64 30 -130☼
2-Chlorophenol ND 7.38 4.016 mg/Kg 54 28 -130☼
2-Methylnaphthalene 0.0722 J 7.38 4.707 mg/Kg 63 28 -130☼
2-Methylphenol ND 7.38 4.363 mg/Kg 59 30 -130☼
2-Nitroaniline ND 7.38 4.948 mg/Kg 67 26 -130☼
2-Nitrophenol ND 7.38 4.491 mg/Kg 61 24 -130☼
3 & 4 Methylphenol ND 7.38 4.434 mg/Kg 60 31 -130☼
3,3'-Dichlorobenzidine ND 7.38 5.772 mg/Kg 78 10 -130☼
3-Nitroaniline ND 7.38 4.942 mg/Kg 67 10 -130☼
4,6-Dinitro-2-methylphenol ND 14.8 14.33 mg/Kg 97 22 -130☼
4-Bromophenyl phenyl ether ND 7.38 5.609 mg/Kg 76 32 -130☼
4-Chloro-3-methylphenol ND 7.38 5.598 mg/Kg 76 31 -130☼
4-Chloroaniline ND 7.38 4.197 mg/Kg 57 10 -130☼
4-Chlorophenyl phenyl ether ND 7.38 5.353 mg/Kg 73 32 -130☼
4-Nitroaniline ND 7.38 5.079 mg/Kg 69 25 -130☼
4-Nitrophenol ND 14.8 11.85 mg/Kg 80 25 -130☼
Acenaphthene ND 7.38 4.848 mg/Kg 66 33 -130☼
Acenaphthylene ND 7.38 5.168 mg/Kg 70 34 -130☼
Acetophenone ND 7.38 4.243 mg/Kg 58 28 -130☼
Anthracene ND 7.38 5.243 mg/Kg 71 39 -130☼
Atrazine ND 7.38 5.314 mg/Kg 72 27 -130☼
Benzaldehyde ND 7.38 2.361 mg/Kg 32 10 -130☼
Benzo[a]anthracene ND 7.38 5.734 mg/Kg 78 40 -130☼
Benzo[a]pyrene ND 7.38 5.225 mg/Kg 71 37 -131☼
Benzo[b]fluoranthene ND 7.38 4.847 mg/Kg 66 35 -130☼
Benzo[g,h,i]perylene ND 7.38 5.319 mg/Kg 72 39 -130☼
Benzo[k]fluoranthene ND 7.38 5.211 mg/Kg 71 35 -130☼
bis (2-chloroisopropyl) ether ND 7.38 3.031 mg/Kg 41 12 -130☼
Bis(2-chloroethoxy)methane ND 7.38 3.942 mg/Kg 53 29 -130☼
Bis(2-chloroethyl)ether ND 7.38 3.178 mg/Kg 43 18 -130☼
Bis(2-ethylhexyl) phthalate ND 7.38 5.566 mg/Kg 75 39 -130☼
Butyl benzyl phthalate ND 7.38 5.484 mg/Kg 74 38 -130☼
Caprolactam ND 7.38 4.524 mg/Kg 61 27 -148☼
Carbazole ND 7.38 5.289 mg/Kg 72 43 -130☼
Chrysene ND 7.38 5.523 mg/Kg 75 40 -130☼
Dibenz(a,h)anthracene ND 7.38 5.552 mg/Kg 75 37 -130☼
Dibenzofuran ND 7.38 5.125 mg/Kg 69 34 -130☼
Diethyl phthalate ND 7.38 5.490 mg/Kg 74 36 -130☼
Dimethyl phthalate ND 7.38 5.293 mg/Kg 72 36 -130☼
Di-n-butyl phthalate ND 7.38 5.235 mg/Kg 71 39 -130☼
Di-n-octyl phthalate ND 7.38 5.777 mg/Kg 78 38 -131☼
Fluoranthene ND 7.38 5.601 mg/Kg 76 38 -130☼
Fluorene ND 7.38 5.329 mg/Kg 72 34 -130☼
Hexachlorobenzene ND 7.38 5.696 mg/Kg 77 28 -130☼
Hexachlorobutadiene ND 7.38 4.705 mg/Kg 64 22 -130☼
Hexachlorocyclopentadiene ND 7.38 5.211 mg/Kg 71 11 -130☼
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
Hexachloroethane ND 7.38 3.545 mg/Kg 48 21 -130☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Indeno[1,2,3-cd]pyrene ND 7.38 6.778 mg/Kg 92 40 -130☼
Isophorone ND 7.38 4.121 mg/Kg 56 26 -130☼
Naphthalene 0.0543 J 7.38 4.349 mg/Kg 58 25 -130☼
Nitrobenzene ND 7.38 4.035 mg/Kg 55 25 -130☼
N-Nitrosodi-n-propylamine ND 7.38 3.858 mg/Kg 52 24 -130☼
N-Nitrosodiphenylamine ND 7.38 4.916 mg/Kg 67 37 -130☼
Pentachlorophenol ND 14.8 14.92 mg/Kg 101 16 -135☼
Phenanthrene ND 7.38 5.097 mg/Kg 69 38 -130☼
Phenol ND 7.38 3.817 mg/Kg 52 27 -130☼
Pyrene ND 7.38 5.614 mg/Kg 76 40 -130☼
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
94
MS MS
Qualifier Limits%Recovery
642-Fluorobiphenyl (Surr)25 -130
542-Fluorophenol (Surr)18 -130
54Nitrobenzene-d5 (Surr)19 -130
55Phenol-d5 (Surr)21 -130
78Terphenyl-d14 (Surr)31 -133
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
1,1'-Biphenyl ND 7.58 5.106 mg/Kg 67 32 -130 9 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
2,4,5-Trichlorophenol ND 7.58 6.359 mg/Kg 84 33 -130 11 50☼
2,4,6-Trichlorophenol ND 7.58 6.311 mg/Kg 83 31 -130 10 50☼
2,4-Dichlorophenol ND 7.58 5.864 mg/Kg 77 30 -130 11 50☼
2,4-Dimethylphenol ND 7.58 5.260 mg/Kg 69 34 -130 11 50☼
2,4-Dinitrophenol ND 15.2 18.37 mg/Kg 121 10 -130 12 50☼
2,4-Dinitrotoluene ND 7.58 5.952 mg/Kg 79 34 -130 8 50☼
2,6-Dinitrotoluene ND 7.58 5.684 mg/Kg 75 33 -130 3 50☼
2-Chloronaphthalene ND 7.58 5.196 mg/Kg 69 30 -130 9 50☼
2-Chlorophenol ND 7.58 4.629 mg/Kg 61 28 -130 14 50☼
2-Methylnaphthalene 0.0722 J 7.58 5.435 mg/Kg 71 28 -130 14 50☼
2-Methylphenol ND 7.58 4.656 mg/Kg 61 30 -130 6 50☼
2-Nitroaniline ND 7.58 5.275 mg/Kg 70 26 -130 6 50☼
2-Nitrophenol ND 7.58 4.950 mg/Kg 65 24 -130 10 50☼
3 & 4 Methylphenol ND 7.58 4.633 mg/Kg 61 31 -130 4 50☼
3,3'-Dichlorobenzidine ND 7.58 6.112 mg/Kg 81 10 -130 6 50☼
3-Nitroaniline ND 7.58 5.204 mg/Kg 69 10 -130 5 50☼
4,6-Dinitro-2-methylphenol ND 15.2 15.75 mg/Kg 104 22 -130 9 50☼
4-Bromophenyl phenyl ether ND 7.58 6.011 mg/Kg 79 32 -130 7 50☼
4-Chloro-3-methylphenol ND 7.58 6.197 mg/Kg 82 31 -130 10 50☼
4-Chloroaniline ND 7.58 4.244 mg/Kg 56 10 -130 1 50☼
4-Chlorophenyl phenyl ether ND 7.58 5.901 mg/Kg 78 32 -130 10 50☼
4-Nitroaniline ND 7.58 5.424 mg/Kg 72 25 -130 7 50☼
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
4-Nitrophenol ND 15.2 13.42 mg/Kg 89 25 -130 12 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Acenaphthene ND 7.58 5.290 mg/Kg 70 33 -130 9 50☼
Acenaphthylene ND 7.58 5.719 mg/Kg 75 34 -130 10 50☼
Acetophenone ND 7.58 4.813 mg/Kg 64 28 -130 13 50☼
Anthracene ND 7.58 5.602 mg/Kg 74 39 -130 7 50☼
Atrazine ND 7.58 5.689 mg/Kg 75 27 -130 7 50☼
Benzaldehyde ND 7.58 2.619 mg/Kg 35 10 -130 10 50☼
Benzo[a]anthracene ND 7.58 6.420 mg/Kg 85 40 -130 11 50☼
Benzo[a]pyrene ND 7.58 5.795 mg/Kg 76 37 -131 10 50☼
Benzo[b]fluoranthene ND 7.58 5.779 mg/Kg 76 35 -130 18 50☼
Benzo[g,h,i]perylene ND 7.58 5.603 mg/Kg 74 39 -130 5 50☼
Benzo[k]fluoranthene ND 7.58 5.323 mg/Kg 70 35 -130 2 50☼
bis (2-chloroisopropyl) ether ND 7.58 3.337 mg/Kg 44 12 -130 10 50☼
Bis(2-chloroethoxy)methane ND 7.58 4.283 mg/Kg 57 29 -130 8 50☼
Bis(2-chloroethyl)ether ND 7.58 3.539 mg/Kg 47 18 -130 11 50☼
Bis(2-ethylhexyl) phthalate ND 7.58 6.091 mg/Kg 80 39 -130 9 50☼
Butyl benzyl phthalate ND 7.58 6.082 mg/Kg 80 38 -130 10 50☼
Caprolactam ND 7.58 4.765 mg/Kg 63 27 -148 5 50☼
Carbazole ND 7.58 5.766 mg/Kg 76 43 -130 9 50☼
Chrysene ND 7.58 5.872 mg/Kg 77 40 -130 6 50☼
Dibenz(a,h)anthracene ND 7.58 5.808 mg/Kg 77 37 -130 4 50☼
Dibenzofuran ND 7.58 5.514 mg/Kg 73 34 -130 7 50☼
Diethyl phthalate ND 7.58 5.959 mg/Kg 79 36 -130 8 50☼
Dimethyl phthalate ND 7.58 5.668 mg/Kg 75 36 -130 7 50☼
Di-n-butyl phthalate ND 7.58 5.582 mg/Kg 74 39 -130 6 50☼
Di-n-octyl phthalate ND 7.58 6.530 mg/Kg 86 38 -131 12 50☼
Fluoranthene ND 7.58 6.072 mg/Kg 80 38 -130 8 50☼
Fluorene ND 7.58 5.688 mg/Kg 75 34 -130 7 50☼
Hexachlorobenzene ND 7.58 6.144 mg/Kg 81 28 -130 8 50☼
Hexachlorobutadiene ND 7.58 5.380 mg/Kg 71 22 -130 13 50☼
Hexachlorocyclopentadiene ND 7.58 6.027 mg/Kg 80 11 -130 15 50☼
Hexachloroethane ND 7.58 4.113 mg/Kg 54 21 -130 15 50☼
Indeno[1,2,3-cd]pyrene ND 7.58 7.501 mg/Kg 99 40 -130 10 50☼
Isophorone ND 7.58 4.461 mg/Kg 59 26 -130 8 50☼
Naphthalene 0.0543 J 7.58 4.882 mg/Kg 64 25 -130 12 50☼
Nitrobenzene ND 7.58 4.557 mg/Kg 60 25 -130 12 50☼
N-Nitrosodi-n-propylamine ND 7.58 4.208 mg/Kg 56 24 -130 9 50☼
N-Nitrosodiphenylamine ND 7.58 5.390 mg/Kg 71 37 -130 9 50☼
Pentachlorophenol ND 15.2 16.17 mg/Kg 107 16 -135 8 50☼
Phenanthrene ND 7.58 5.455 mg/Kg 72 38 -130 7 50☼
Phenol ND 7.58 4.228 mg/Kg 56 27 -130 10 50☼
Pyrene ND 7.58 6.068 mg/Kg 80 40 -130 8 50☼
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
98
MSD MSD
Qualifier Limits%Recovery
702-Fluorobiphenyl (Surr)25 -130
582-Fluorophenol (Surr)18 -130
58Nitrobenzene-d5 (Surr)19 -130
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754041 Prep Batch: 753897
Phenol-d5 (Surr)21 -130
Surrogate
60
MSD MSD
Qualifier Limits%Recovery
82Terphenyl-d14 (Surr)31 -133
Method: 8015C - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-604548/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604442 Prep Batch: 604548
RL MDL
Gasoline Range Organics [C6 - C10]ND 0.100 0.0500 mg/Kg 12/12/22 09:22 12/12/22 09:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)75 65-125 12/12/22 09:53 1
MB MB
Surrogate
12/12/22 09:22
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-604548/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604442 Prep Batch: 604548
Gasoline Range Organics [C6 -
C10]
1.00 0.8837 mg/Kg 88 62 -141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604442 Prep Batch: 604548
Gasoline Range Organics [C6 -
C10]
ND 66.8 66.90 mg/Kg 100 10 -150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
93
MS MS
Qualifier Limits%Recovery
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604442 Prep Batch: 604548
Gasoline Range Organics [C6 -
C10]
ND 66.8 68.70 mg/Kg 103 10 -150 3 32☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
95
MSD MSD
Qualifier Limits%Recovery
Eurofins Savannah
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8015C - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-604549/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604441 Prep Batch: 604549
RL MDL
Gasoline Range Organics [C6 - C10]ND 0.100 0.0500 mg/Kg 12/12/22 13:20 12/12/22 14:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene (fid)99 65-125 12/12/22 14:55 1
MB MB
Surrogate
12/12/22 13:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-604549/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604441 Prep Batch: 604549
Gasoline Range Organics [C6 -
C10]
1.00 1.099 mg/Kg 110 62 -141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: P14-5Lab Sample ID: 680-226646-16 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604441 Prep Batch: 604549
Gasoline Range Organics [C6 -
C10]
ND 67.8 76.33 mg/Kg 113 10 -150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
102
MS MS
Qualifier Limits%Recovery
Client Sample ID: P14-5Lab Sample ID: 680-226646-16 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 604441 Prep Batch: 604549
Gasoline Range Organics [C6 -
C10]
ND 67.8 75.62 mg/Kg 112 10 -150 1 32☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene (fid)65 -125
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
Method: 8015D - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-754086/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754237 Prep Batch: 754086
RL MDL
Diesel Range Organics [C10-C28]ND 7.92 2.58 mg/Kg 12/07/22 18:30 12/08/22 18:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method: 8015D - Diesel Range Organics (DRO) (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-754086/21-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754237 Prep Batch: 754086
o-Terphenyl 53 15-139 12/08/22 18:15 1
MB MB
Surrogate
12/07/22 18:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-754086/22-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754237 Prep Batch: 754086
Diesel Range Organics
[C10-C28]
33.0 24.71 mg/Kg 75 26 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
78
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754237 Prep Batch: 754086
Diesel Range Organics
[C10-C28]
30.8 F1 37.4 82.78 F1 mg/Kg 139 26 -133☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
91
MS MS
Qualifier Limits%Recovery
Client Sample ID: P3-10Lab Sample ID: 680-226646-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 754237 Prep Batch: 754086
Diesel Range Organics
[C10-C28]
30.8 F1 37.9 61.91 mg/Kg 82 26 -133 29 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
o-Terphenyl 15 -139
Surrogate
89
MSD MSD
Qualifier Limits%Recovery
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
GC/MS VOA
Prep Batch: 753374
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035A680-226646-1 P3-10 Total/NA
Solid 5035A680-226646-2 P3-25 Total/NA
Solid 5035A680-226646-3 - RA P2-25 Total/NA
Solid 5035A680-226646-3 P2-25 Total/NA
Solid 5035A680-226646-4 P4-15 Total/NA
Solid 5035A680-226646-5 P4-25 Total/NA
Solid 5035A680-226646-6 P5-10 Total/NA
Solid 5035A680-226646-7 P5-20 Total/NA
Solid 5035A680-226646-8 P6-20 Total/NA
Solid 5035A680-226646-9 P7-25 Total/NA
Solid 5035A680-226646-9 P7-25 Total/NA
Solid 5035A680-226646-10 P11-25 Total/NA
Solid 5035A680-226646-11 P9-16 Total/NA
Solid 5035A680-226646-12 P10-25 Total/NA
Solid 5035A680-226646-13 P8-20 Total/NA
Solid 5035A680-226646-14 P12-20 Total/NA
Solid 5035A680-226646-15 P13-10 Total/NA
Solid 5035A680-226646-16 P14-5 Total/NA
Solid 5035A680-226646-17 P15-10 Total/NA
Solid 5035A680-226646-18 P17-5 Total/NA
Solid 5035A680-226646-19 P18-10 Total/NA
Solid 5035A680-226646-20 P16-15 Total/NA
Analysis Batch: 753988
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 753374680-226646-3 - RA P2-25 Total/NA
Solid 8260DMB 680-753988/8 Method Blank Total/NA
Solid 8260DLCS 680-753988/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-753988/6 Lab Control Sample Dup Total/NA
Analysis Batch: 754199
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 753374680-226646-1 P3-10 Total/NA
Solid 8260D 753374680-226646-2 P3-25 Total/NA
Solid 8260D 753374680-226646-3 P2-25 Total/NA
Solid 8260D 753374680-226646-4 P4-15 Total/NA
Solid 8260D 753374680-226646-5 P4-25 Total/NA
Solid 8260D 753374680-226646-6 P5-10 Total/NA
Solid 8260D 753374680-226646-7 P5-20 Total/NA
Solid 8260D 753374680-226646-8 P6-20 Total/NA
Solid 8260D 753374680-226646-9 P7-25 Total/NA
Solid 8260D 753374680-226646-10 P11-25 Total/NA
Solid 8260D 753374680-226646-11 P9-16 Total/NA
Solid 8260D 753374680-226646-12 P10-25 Total/NA
Solid 8260D 753374680-226646-13 P8-20 Total/NA
Solid 8260D 753374680-226646-14 P12-20 Total/NA
Solid 8260D 753374680-226646-15 P13-10 Total/NA
Solid 8260D 753374680-226646-16 P14-5 Total/NA
Solid 8260DMB 680-754199/8 Method Blank Total/NA
Solid 8260DLCS 680-754199/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-754199/6 Lab Control Sample Dup Total/NA
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
GC/MS VOA
Analysis Batch: 754381
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 753374680-226646-9 P7-25 Total/NA
Solid 8260D 753374680-226646-17 P15-10 Total/NA
Solid 8260D 753374680-226646-18 P17-5 Total/NA
Solid 8260D 753374680-226646-19 P18-10 Total/NA
Solid 8260D 753374680-226646-20 P16-15 Total/NA
Solid 8260DMB 680-754381/8 Method Blank Total/NA
Solid 8260DLCS 680-754381/5 Lab Control Sample Total/NA
Solid 8260DLCSD 680-754381/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 753897
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-226646-1 P3-10 Total/NA
Solid 3546680-226646-2 P3-25 Total/NA
Solid 3546680-226646-3 P2-25 Total/NA
Solid 3546680-226646-4 P4-15 Total/NA
Solid 3546680-226646-5 P4-25 Total/NA
Solid 3546680-226646-6 P5-10 Total/NA
Solid 3546680-226646-7 P5-20 Total/NA
Solid 3546680-226646-8 P6-20 Total/NA
Solid 3546680-226646-9 P7-25 Total/NA
Solid 3546680-226646-10 P11-25 Total/NA
Solid 3546680-226646-11 P9-16 Total/NA
Solid 3546680-226646-12 P10-25 Total/NA
Solid 3546680-226646-13 P8-20 Total/NA
Solid 3546680-226646-14 P12-20 Total/NA
Solid 3546680-226646-15 P13-10 Total/NA
Solid 3546680-226646-16 P14-5 Total/NA
Solid 3546680-226646-17 P15-10 Total/NA
Solid 3546680-226646-18 P17-5 Total/NA
Solid 3546680-226646-19 P18-10 Total/NA
Solid 3546680-226646-20 P16-15 Total/NA
Solid 3546MB 680-753897/21-A Method Blank Total/NA
Solid 3546LCS 680-753897/22-A Lab Control Sample Total/NA
Solid 3546680-226646-1 MS P3-10 Total/NA
Solid 3546680-226646-1 MSD P3-10 Total/NA
Analysis Batch: 754041
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 753897680-226646-1 P3-10 Total/NA
Solid 8270E 753897680-226646-2 P3-25 Total/NA
Solid 8270E 753897680-226646-3 P2-25 Total/NA
Solid 8270E 753897680-226646-4 P4-15 Total/NA
Solid 8270E 753897680-226646-5 P4-25 Total/NA
Solid 8270E 753897680-226646-6 P5-10 Total/NA
Solid 8270E 753897680-226646-7 P5-20 Total/NA
Solid 8270E 753897680-226646-8 P6-20 Total/NA
Solid 8270E 753897680-226646-9 P7-25 Total/NA
Solid 8270E 753897680-226646-10 P11-25 Total/NA
Solid 8270E 753897680-226646-11 P9-16 Total/NA
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
GC/MS Semi VOA (Continued)
Analysis Batch: 754041 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 753897680-226646-12 P10-25 Total/NA
Solid 8270E 753897680-226646-13 P8-20 Total/NA
Solid 8270E 753897MB 680-753897/21-A Method Blank Total/NA
Solid 8270E 753897LCS 680-753897/22-A Lab Control Sample Total/NA
Solid 8270E 753897680-226646-1 MS P3-10 Total/NA
Solid 8270E 753897680-226646-1 MSD P3-10 Total/NA
Analysis Batch: 754071
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 753897680-226646-14 P12-20 Total/NA
Solid 8270E 753897680-226646-15 P13-10 Total/NA
Solid 8270E 753897680-226646-16 P14-5 Total/NA
Solid 8270E 753897680-226646-17 P15-10 Total/NA
Solid 8270E 753897680-226646-18 P17-5 Total/NA
Solid 8270E 753897680-226646-19 P18-10 Total/NA
Solid 8270E 753897680-226646-20 P16-15 Total/NA
GC VOA
Analysis Batch: 604441
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 604549680-226646-11 P9-16 Total/NA
Solid 8015C 604549680-226646-12 P10-25 Total/NA
Solid 8015C 604549680-226646-13 P8-20 Total/NA
Solid 8015C 604549680-226646-14 P12-20 Total/NA
Solid 8015C 604549680-226646-15 P13-10 Total/NA
Solid 8015C 604549680-226646-16 P14-5 Total/NA
Solid 8015C 604549680-226646-17 P15-10 Total/NA
Solid 8015C 604549680-226646-18 P17-5 Total/NA
Solid 8015C 604549680-226646-19 P18-10 Total/NA
Solid 8015C 604549680-226646-20 P16-15 Total/NA
Solid 8015C 604549MB 400-604549/2-A Method Blank Total/NA
Solid 8015C 604549LCS 400-604549/1-A Lab Control Sample Total/NA
Solid 8015C 604549680-226646-16 MS P14-5 Total/NA
Solid 8015C 604549680-226646-16 MSD P14-5 Total/NA
Analysis Batch: 604442
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 604548680-226646-1 P3-10 Total/NA
Solid 8015C 604548680-226646-2 P3-25 Total/NA
Solid 8015C 604548680-226646-3 P2-25 Total/NA
Solid 8015C 604548680-226646-4 P4-15 Total/NA
Solid 8015C 604548680-226646-5 P4-25 Total/NA
Solid 8015C 604548680-226646-6 P5-10 Total/NA
Solid 8015C 604548680-226646-7 P5-20 Total/NA
Solid 8015C 604548680-226646-8 P6-20 Total/NA
Solid 8015C 604548680-226646-9 P7-25 Total/NA
Solid 8015C 604548680-226646-10 P11-25 Total/NA
Solid 8015C 604548MB 400-604548/2-A Method Blank Total/NA
Solid 8015C 604548LCS 400-604548/1-A Lab Control Sample Total/NA
Solid 8015C 604548680-226646-1 MS P3-10 Total/NA
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
GC VOA (Continued)
Analysis Batch: 604442 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015C 604548680-226646-1 MSD P3-10 Total/NA
Prep Batch: 604548
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035680-226646-1 P3-10 Total/NA
Solid 5035680-226646-2 P3-25 Total/NA
Solid 5035680-226646-3 P2-25 Total/NA
Solid 5035680-226646-4 P4-15 Total/NA
Solid 5035680-226646-5 P4-25 Total/NA
Solid 5035680-226646-6 P5-10 Total/NA
Solid 5035680-226646-7 P5-20 Total/NA
Solid 5035680-226646-8 P6-20 Total/NA
Solid 5035680-226646-9 P7-25 Total/NA
Solid 5035680-226646-10 P11-25 Total/NA
Solid 5035AMB 400-604548/2-A Method Blank Total/NA
Solid 5035ALCS 400-604548/1-A Lab Control Sample Total/NA
Solid 5035680-226646-1 MS P3-10 Total/NA
Solid 5035680-226646-1 MSD P3-10 Total/NA
Prep Batch: 604549
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035680-226646-11 P9-16 Total/NA
Solid 5035680-226646-12 P10-25 Total/NA
Solid 5035680-226646-13 P8-20 Total/NA
Solid 5035680-226646-14 P12-20 Total/NA
Solid 5035680-226646-15 P13-10 Total/NA
Solid 5035680-226646-16 P14-5 Total/NA
Solid 5035680-226646-17 P15-10 Total/NA
Solid 5035680-226646-18 P17-5 Total/NA
Solid 5035680-226646-19 P18-10 Total/NA
Solid 5035680-226646-20 P16-15 Total/NA
Solid 5035AMB 400-604549/2-A Method Blank Total/NA
Solid 5035ALCS 400-604549/1-A Lab Control Sample Total/NA
Solid 5035680-226646-16 MS P14-5 Total/NA
Solid 5035680-226646-16 MSD P14-5 Total/NA
GC Semi VOA
Prep Batch: 754086
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-226646-1 P3-10 Total/NA
Solid 3546680-226646-2 P3-25 Total/NA
Solid 3546680-226646-3 P2-25 Total/NA
Solid 3546680-226646-4 P4-15 Total/NA
Solid 3546680-226646-5 P4-25 Total/NA
Solid 3546680-226646-6 P5-10 Total/NA
Solid 3546680-226646-7 P5-20 Total/NA
Solid 3546680-226646-8 P6-20 Total/NA
Solid 3546680-226646-9 P7-25 Total/NA
Solid 3546680-226646-10 P11-25 Total/NA
Solid 3546680-226646-11 P9-16 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
GC Semi VOA (Continued)
Prep Batch: 754086 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-226646-12 P10-25 Total/NA
Solid 3546680-226646-13 P8-20 Total/NA
Solid 3546680-226646-14 P12-20 Total/NA
Solid 3546680-226646-15 P13-10 Total/NA
Solid 3546680-226646-16 P14-5 Total/NA
Solid 3546680-226646-17 P15-10 Total/NA
Solid 3546680-226646-18 P17-5 Total/NA
Solid 3546680-226646-19 P18-10 Total/NA
Solid 3546680-226646-20 P16-15 Total/NA
Solid 3546MB 680-754086/21-A Method Blank Total/NA
Solid 3546LCS 680-754086/22-A Lab Control Sample Total/NA
Solid 3546680-226646-1 MS P3-10 Total/NA
Solid 3546680-226646-1 MSD P3-10 Total/NA
Analysis Batch: 754237
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015D 754086680-226646-1 P3-10 Total/NA
Solid 8015D 754086680-226646-2 P3-25 Total/NA
Solid 8015D 754086680-226646-3 P2-25 Total/NA
Solid 8015D 754086680-226646-4 P4-15 Total/NA
Solid 8015D 754086680-226646-5 P4-25 Total/NA
Solid 8015D 754086680-226646-6 P5-10 Total/NA
Solid 8015D 754086680-226646-7 P5-20 Total/NA
Solid 8015D 754086680-226646-8 P6-20 Total/NA
Solid 8015D 754086680-226646-9 P7-25 Total/NA
Solid 8015D 754086680-226646-10 P11-25 Total/NA
Solid 8015D 754086680-226646-11 P9-16 Total/NA
Solid 8015D 754086680-226646-12 P10-25 Total/NA
Solid 8015D 754086680-226646-13 P8-20 Total/NA
Solid 8015D 754086680-226646-14 P12-20 Total/NA
Solid 8015D 754086680-226646-15 P13-10 Total/NA
Solid 8015D 754086680-226646-16 P14-5 Total/NA
Solid 8015D 754086680-226646-17 P15-10 Total/NA
Solid 8015D 754086680-226646-18 P17-5 Total/NA
Solid 8015D 754086680-226646-19 P18-10 Total/NA
Solid 8015D 754086680-226646-20 P16-15 Total/NA
Solid 8015D 754086MB 680-754086/21-A Method Blank Total/NA
Solid 8015D 754086LCS 680-754086/22-A Lab Control Sample Total/NA
Solid 8015D 754086680-226646-1 MS P3-10 Total/NA
Solid 8015D 754086680-226646-1 MSD P3-10 Total/NA
General Chemistry
Analysis Batch: 754290
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-226646-1 P3-10 Total/NA
Solid Moisture680-226646-2 P3-25 Total/NA
Solid Moisture680-226646-3 P2-25 Total/NA
Solid Moisture680-226646-4 P4-15 Total/NA
Solid Moisture680-226646-5 P4-25 Total/NA
Solid Moisture680-226646-6 P5-10 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
General Chemistry (Continued)
Analysis Batch: 754290 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-226646-7 P5-20 Total/NA
Solid Moisture680-226646-8 P6-20 Total/NA
Solid Moisture680-226646-9 P7-25 Total/NA
Solid Moisture680-226646-10 P11-25 Total/NA
Solid Moisture680-226646-11 P9-16 Total/NA
Solid Moisture680-226646-12 P10-25 Total/NA
Solid Moisture680-226646-13 P8-20 Total/NA
Solid Moisture680-226646-14 P12-20 Total/NA
Solid Moisture680-226646-15 P13-10 Total/NA
Solid Moisture680-226646-16 P14-5 Total/NA
Solid Moisture680-226646-17 P15-10 Total/NA
Solid Moisture680-226646-18 P17-5 Total/NA
Solid Moisture680-226646-19 P18-10 Total/NA
Solid Moisture680-226646-20 P16-15 Total/NA
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P3-10 Lab Sample ID: 680-226646-1
Matrix: SolidDate Collected: 11/28/22 11:00
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P3-10 Lab Sample ID: 680-226646-1
Matrix: SolidDate Collected: 11/28/22 11:00
Percent Solids: 86.7Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:10 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.162 g 5 mL
Analysis 8260D 1 754199 12/08/22 13:41 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.23 g 1 mL
Analysis 8270E 1 754041 12/07/22 20:32 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.88 g 5.0 g
Analysis 8015C 50 604442 12/12/22 11:34 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.20 g 1 mL
Analysis 8015D 1 754237 12/08/22 18:46 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P3-25 Lab Sample ID: 680-226646-2
Matrix: SolidDate Collected: 11/28/22 11:10
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P3-25 Lab Sample ID: 680-226646-2
Matrix: SolidDate Collected: 11/28/22 11:10
Percent Solids: 87.8Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:10 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.045 g 5 mL
Analysis 8260D 1 754199 12/08/22 14:04 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.75 g 1 mL
Analysis 8270E 1 754041 12/07/22 20:54 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 5.163 g 5.0 g
Analysis 8015C 50 604442 12/12/22 13:08 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.27 g 1 mL
Analysis 8015D 1 754237 12/08/22 19:02 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P2-25 Lab Sample ID: 680-226646-3
Matrix: SolidDate Collected: 11/28/22 11:35
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P2-25 Lab Sample ID: 680-226646-3
Matrix: SolidDate Collected: 11/28/22 11:35
Percent Solids: 81.7Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:10RA EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.554 g 5 mL
Analysis 8260D RA 1 753988 12/07/22 20:47 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 753374 12/02/22 12:10 FES EET SAVTotal/NA 4.61 g 5 mL
Analysis 8260D 1 754199 12/08/22 14:28 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.32 g 1 mL
Analysis 8270E 1 754041 12/07/22 21:15 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.828 g 5.0 g
Analysis 8015C 50 604442 12/12/22 13:39 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.33 g 1 mL
Analysis 8015D 1 754237 12/08/22 19:17 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P4-15 Lab Sample ID: 680-226646-4
Matrix: SolidDate Collected: 11/28/22 12:03
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P4-15 Lab Sample ID: 680-226646-4
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:10 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.652 g 5 mL
Analysis 8260D 1 754199 12/08/22 14:52 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.54 g 1 mL
Analysis 8270E 1 754041 12/07/22 21:36 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.666 g 5.0 g
Analysis 8015C 50 604442 12/12/22 14:10 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P4-15 Lab Sample ID: 680-226646-4
Matrix: SolidDate Collected: 11/28/22 12:03
Percent Solids: 86.6Date Received: 12/01/22 06:30
Prep 3546 MJ12/07/22 18:30 EET SAV754086
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.38 g 1 mL
Analysis 8015D 1 754237 12/08/22 19:33 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P4-25 Lab Sample ID: 680-226646-5
Matrix: SolidDate Collected: 11/28/22 12:05
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P4-25 Lab Sample ID: 680-226646-5
Matrix: SolidDate Collected: 11/28/22 12:05
Percent Solids: 87.1Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:10 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.534 g 5 mL
Analysis 8260D 1 754199 12/08/22 15:16 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.54 g 1 mL
Analysis 8270E 1 754041 12/07/22 21:58 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.732 g 5.0 g
Analysis 8015C 50 604442 12/12/22 14:41 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.78 g 1 mL
Analysis 8015D 1 754237 12/08/22 19:48 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P5-10 Lab Sample ID: 680-226646-6
Matrix: SolidDate Collected: 11/28/22 12:20
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P5-10 Lab Sample ID: 680-226646-6
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.815 g 5 mL
Analysis 8260D 1 754199 12/08/22 15:40 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P5-10 Lab Sample ID: 680-226646-6
Matrix: SolidDate Collected: 11/28/22 12:20
Percent Solids: 85.1Date Received: 12/01/22 06:30
Prep 3546 MJ12/06/22 18:15 EET SAV753897
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.53 g 1 mL
Analysis 8270E 1 754041 12/07/22 22:19 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.845 g 5.0 g
Analysis 8015C 50 604442 12/12/22 15:12 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.20 g 1 mL
Analysis 8015D 1 754237 12/08/22 20:03 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P5-20 Lab Sample ID: 680-226646-7
Matrix: SolidDate Collected: 11/28/22 12:25
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P5-20 Lab Sample ID: 680-226646-7
Matrix: SolidDate Collected: 11/28/22 12:25
Percent Solids: 82.9Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.99 g 5 mL
Analysis 8260D 1 754199 12/08/22 16:03 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.35 g 1 mL
Analysis 8270E 1 754041 12/07/22 22:41 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 4.294 g 5.0 g
Analysis 8015C 50 604442 12/12/22 16:55 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.80 g 1 mL
Analysis 8015D 1 754237 12/08/22 20:19 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P6-20 Lab Sample ID: 680-226646-8
Matrix: SolidDate Collected: 11/28/22 13:52
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P6-20 Lab Sample ID: 680-226646-8
Matrix: SolidDate Collected: 11/28/22 13:52
Percent Solids: 78.7Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.532 g 5 mL
Analysis 8260D 1 754199 12/08/22 16:27 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.25 g 1 mL
Analysis 8270E 1 754041 12/07/22 23:02 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 5.313 g 5.0 g
Analysis 8015C 50 604442 12/12/22 17:26 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.38 g 1 mL
Analysis 8015D 1 754237 12/08/22 20:34 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P7-25 Lab Sample ID: 680-226646-9
Matrix: SolidDate Collected: 11/28/22 14:20
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P7-25 Lab Sample ID: 680-226646-9
Matrix: SolidDate Collected: 11/28/22 14:20
Percent Solids: 76.3Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.875 g 5 mL
Analysis 8260D 1 754199 12/08/22 16:51 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 753374 12/02/22 12:11 FES EET SAVTotal/NA 4.748 g 5 mL
Analysis 8260D 40 754381 12/09/22 18:31 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.58 g 1 mL
Analysis 8270E 1 754041 12/07/22 23:24 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 5.064 g 5.0 g
Analysis 8015C 50 604442 12/12/22 17:58 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.88 g 1 mL
Analysis 8015D 1 754237 12/08/22 20:50 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P11-25 Lab Sample ID: 680-226646-10
Matrix: SolidDate Collected: 11/28/22 14:40
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P11-25 Lab Sample ID: 680-226646-10
Matrix: SolidDate Collected: 11/28/22 14:40
Percent Solids: 74.6Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.169 g 5 mL
Analysis 8260D 1 754199 12/08/22 17:15 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.38 g 1 mL
Analysis 8270E 1 754041 12/07/22 23:46 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604548 12/12/22 09:22 PD EET PENTotal/NA 5.392 g 5.0 g
Analysis 8015C 50 604442 12/12/22 18:29 SAB EET PENTotal/NA 5 mL 5 mL
CH_JOANInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.42 g 1 mL
Analysis 8015D 1 754237 12/08/22 21:05 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P9-16 Lab Sample ID: 680-226646-11
Matrix: SolidDate Collected: 11/28/22 15:20
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P9-16 Lab Sample ID: 680-226646-11
Matrix: SolidDate Collected: 11/28/22 15:20
Percent Solids: 81.8Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.877 g 5 mL
Analysis 8260D 1 754199 12/08/22 17:39 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.58 g 1 mL
Analysis 8270E 1 754041 12/08/22 00:07 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 5.052 g 5.0 g
Analysis 8015C 50 604441 12/12/22 15:40 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.37 g 1 mL
Analysis 8015D 1 754237 12/08/22 21:21 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P10-25 Lab Sample ID: 680-226646-12
Matrix: SolidDate Collected: 11/28/22 15:30
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P10-25 Lab Sample ID: 680-226646-12
Matrix: SolidDate Collected: 11/28/22 15:30
Percent Solids: 81.0Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.009 g 5 mL
Analysis 8260D 1 754199 12/08/22 18:03 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.64 g 1 mL
Analysis 8270E 1 754041 12/08/22 00:29 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.503 g 5.0 g
Analysis 8015C 50 604441 12/12/22 16:00 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.55 g 1 mL
Analysis 8015D 1 754237 12/08/22 21:36 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P8-20 Lab Sample ID: 680-226646-13
Matrix: SolidDate Collected: 11/28/22 16:05
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P8-20 Lab Sample ID: 680-226646-13
Matrix: SolidDate Collected: 11/28/22 16:05
Percent Solids: 75.7Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.143 g 5 mL
Analysis 8260D 1 754199 12/08/22 18:27 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.20 g 1 mL
Analysis 8270E 1 754041 12/08/22 00:51 T1C EET SAVTotal/NA 1 mL 1 mL
CMSKInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 5.398 g 5.0 g
Analysis 8015C 50 604441 12/12/22 16:26 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.50 g 1 mL
Analysis 8015D 1 754237 12/08/22 21:51 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P12-20 Lab Sample ID: 680-226646-14
Matrix: SolidDate Collected: 11/28/22 16:20
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P12-20 Lab Sample ID: 680-226646-14
Matrix: SolidDate Collected: 11/28/22 16:20
Percent Solids: 78.5Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.594 g 5 mL
Analysis 8260D 1 754199 12/08/22 18:50 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.36 g 1 mL
Analysis 8270E 1 754071 12/08/22 00:34 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.449 g 5.0 g
Analysis 8015C 50 604441 12/12/22 16:55 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.42 g 1 mL
Analysis 8015D 1 754237 12/08/22 22:07 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P13-10 Lab Sample ID: 680-226646-15
Matrix: SolidDate Collected: 11/28/22 16:36
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P13-10 Lab Sample ID: 680-226646-15
Matrix: SolidDate Collected: 11/28/22 16:36
Percent Solids: 71.7Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.93 g 5 mL
Analysis 8260D 1 754199 12/08/22 19:14 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.85 g 1 mL
Analysis 8270E 1 754071 12/08/22 00:58 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.964 g 5.0 g
Analysis 8015C 50 604441 12/12/22 17:20 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.86 g 1 mL
Analysis 8015D 1 754237 12/08/22 22:22 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P14-5 Lab Sample ID: 680-226646-16
Matrix: SolidDate Collected: 11/29/22 08:25
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P14-5 Lab Sample ID: 680-226646-16
Matrix: SolidDate Collected: 11/29/22 08:25
Percent Solids: 79.8Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.683 g 5 mL
Analysis 8260D 1 754199 12/08/22 19:38 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.50 g 1 mL
Analysis 8270E 1 754071 12/08/22 01:23 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 5.689 g 5.0 g
Analysis 8015C 50 604441 12/12/22 17:49 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.85 g 1 mL
Analysis 8015D 1 754237 12/08/22 22:38 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P15-10 Lab Sample ID: 680-226646-17
Matrix: SolidDate Collected: 11/29/22 08:38
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P15-10 Lab Sample ID: 680-226646-17
Matrix: SolidDate Collected: 11/29/22 08:38
Percent Solids: 78.8Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.71 g 5 mL
Analysis 8260D 1 754381 12/09/22 16:09 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.23 g 1 mL
Analysis 8270E 1 754071 12/08/22 01:47 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.227 g 5.0 g
Analysis 8015C 50 604441 12/12/22 18:17 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.40 g 1 mL
Analysis 8015D 1 754237 12/08/22 22:53 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P17-5 Lab Sample ID: 680-226646-18
Matrix: SolidDate Collected: 11/29/22 08:56
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P17-5 Lab Sample ID: 680-226646-18
Matrix: SolidDate Collected: 11/29/22 08:56
Percent Solids: 77.2Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.62 g 5 mL
Analysis 8260D 1 754381 12/09/22 16:33 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.56 g 1 mL
Analysis 8270E 1 754071 12/08/22 02:10 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 6.402 g 5.0 g
Analysis 8015C 50 604441 12/12/22 19:09 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.41 g 1 mL
Analysis 8015D 1 754237 12/08/22 23:09 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P18-10 Lab Sample ID: 680-226646-19
Matrix: SolidDate Collected: 11/29/22 09:13
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P18-10 Lab Sample ID: 680-226646-19
Matrix: SolidDate Collected: 11/29/22 09:13
Percent Solids: 73.0Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.079 g 5 mL
Analysis 8260D 1 754381 12/09/22 16:56 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.59 g 1 mL
Analysis 8270E 1 754071 12/08/22 02:35 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.87 g 5.0 g
Analysis 8015C 50 604441 12/12/22 19:35 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.33 g 1 mL
Analysis 8015D 1 754237 12/08/22 23:24 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Client Sample ID: P16-15 Lab Sample ID: 680-226646-20
Matrix: SolidDate Collected: 11/29/22 09:29
Date Received: 12/01/22 06:30
Analysis Moisture TD12/08/22 18:151 EET SAV754290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P16-15 Lab Sample ID: 680-226646-20
Matrix: SolidDate Collected: 11/29/22 09:29
Percent Solids: 76.8Date Received: 12/01/22 06:30
Prep 5035A FES12/02/22 12:11 EET SAV753374
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.133 g 5 mL
Analysis 8260D 1 754381 12/09/22 17:20 Y1S EET SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 753897 12/06/22 18:15 MJ EET SAVTotal/NA 15.87 g 1 mL
Analysis 8270E 1 754071 12/08/22 02:59 T1C EET SAVTotal/NA 1 mL 1 mL
CMSNInstrument ID:
Prep 5035 604549 12/12/22 13:20 PD EET PENTotal/NA 4.87 g 5.0 g
Analysis 8015C 50 604441 12/12/22 20:01 SAB EET PENTotal/NA 5 mL 5 mL
CH_RITAInstrument ID:
Prep 3546 754086 12/07/22 18:30 MJ EET SAVTotal/NA 30.29 g 1 mL
Analysis 8015D 1 754237 12/08/22 23:39 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-226646-1
Project/Site: D&M Market
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Laboratory: Eurofins Pensacola
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 314 12-31-22
Eurofins Savannah
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Method Summary
Job ID: 680-226646-1Client: S&ME, Inc.
Project/Site: D&M Market
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS EET SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)EET SAV
SW8468015CGasoline Range Organics (GRO) (GC)EET PEN
SW8468015DDiesel Range Organics (DRO) (GC)EET SAV
EPAMoisturePercent Moisture EET SAV
SW8463546Microwave Extraction EET SAV
SW8465035Closed System Purge and Trap EET PEN
SW8465035AClosed System Purge & Trap EET SAV
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-226646-1
Login Number: 226646
Question Answer Comment
Creator: Padayao, Abigail
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-226646-1
Login Number: 226646
Question Answer Comment
Creator: Whitley, Adrian
List Source: Eurofins Pensacola
List Creation: 12/12/22 09:51 AMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.5°C IR8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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