WS-29296_48461_CA_SCH_20220805

Initial Abatement Action Report
D&M Grocery; Incident No.: 48461
6066 NC 704 Highway East, Sandy
Ridge, North Carolina
S&ME Project No. 22580285
PREPARED FOR:
Huffman Oil Company
P.O. Box 730
Burlington, North Carolina 27216-0730
PREPARED BY:
S&ME, Inc.
8646 W Market St, Ste 105
Greensboro, North Carolina 27409
August 5, 2022
S&ME, Inc. | 8646 W Market St, Ste 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com
August 5, 2022
Huffman Oil Company
P.O. Box 730
Burlington, NC 27216-0730
Attention: Mr. James Barnwell, III
Reference: Initial Abatement Action Report
D&M Grocery; Incident No.: 48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
Dear Mr. Barnwell:
S&ME Inc. (S&ME) is providing this Initial Abatement Action Report to summarize the provided environmental
services related to the underground storage tank (UST) system at D&M Grocery in Sandy Ridge, North Carolina.
Our services were performed in general accordance to S&ME Proposal number 22580285A dated July 13, 2022
and the existing Master Service Agreement between S&ME and Huffman Oil Company (Huffman Oil) dated
July 30, 2015.
If you have any questions, or if we can be of any additional service, please feel free to contact us.
Sincerely,
S&ME, Inc.
Lyndal Butler Wayne Watterson, P.E.
Environmental Scientist Senior Engineer
LB/WW/wj
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 i
Table of Contents
1.0 Site Identification .................................................................................................. 1
2.0 Executive Summary ............................................................................................... 2
2.1 Source, Discovery Date, Quantity and Type of Contaminant Released ................... 2
2.2 Initial Abatement Actions................................................................................................ 2
2.3 Hydrogeological Results .................................................................................................. 2
2.4 Assessment Results .......................................................................................................... 2
2.5 Risk Classification ............................................................................................................. 3
2.6 Remediation Levels .......................................................................................................... 3
3.0 Site History and Characterization ...................................................................... 3
3.1 General ............................................................................................................................... 3
3.2 UST Owner and System Data ......................................................................................... 3
3.3 Above Ground Storage Tanks......................................................................................... 4
3.4 Release Description .......................................................................................................... 4
4.0 Site Check ............................................................................................................... 5
4.1 Release Reporting ............................................................................................................. 5
4.2 Tank and Line Tightness Testing ................................................................................... 5
4.3 Site Check Procedures ...................................................................................................... 5
4.4 Initial Site Investigation ................................................................................................... 5
4.4.1 Soil Sampling ...................................................................................................................... 6
4.4.2 Water Sampling................................................................................................................... 6
4.5 Free Product ...................................................................................................................... 7
4.6 Groundwater Occurrence and Flow Direction ............................................................. 7
4.7 Analytical Results ............................................................................................................. 7
4.8 Assessment Conclusions.................................................................................................. 7
5.0 Preliminary Receptor Information ..................................................................... 8
6.0 Initial Response and Abatement Action ........................................................... 8
7.0 Conclusions and Recommendations ................................................................. 9
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 ii
List of Figures
1 US Topo Map
2 Site Map
3 Soil Analytical Results
4 Groundwater Analytical Results
5 Groundwater Elevation Contour Map
List of Additional Tables
1 Summary of Water Supply Well Sampling Results
2 Field Screening Results
3 Monitor Well Construction and Liquid Level Data
4 Summary of Soil Sampling Results
3 Summary of Groundwater Sampling Results
Appendices
Appendix I - Boring Logs, Well Construction Details and Well Construction Records
Appendix II- Groundwater Sampling Forms and Environmental Field Report
Appendix III- Analytical Report
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 2
2.0 Executive Summary
2.1 Source, Discovery Date, Quantity and Type of Contaminant Released
The suspected release source is the underground storage tank (UST) system operating at the D&M Mart
located at 6066 NC 704 Highway East. The release was discovered on May 25, 2022, upon receipt of the
analytical results for a water sample collected from a water supply well located on an adjoining property
at 6080 NC 704 Highway East. Based on the supply well analytical results, the nature of the release is
gasoline. The release quantity is unknown.
2.2 Initial Abatement Actions
Huffman Oil Company temporarily closed the 2,000-gallon premium gasoline UST by removing product
from the tank, which was last operated on February 20, 2017. The UST system at D&M Grocery was
reported as in compliance during the last inspection performed by North Carolina Department of
Environmental Quality (NCDEQ) during August 2021. S&ME is not aware of an equipment failure that
may have resulted in a release from the UST system.
Tank tightness and line tightness testing performed on 5/31/2022 resulted in passing tests for all tanks
and product lines.
On July 8, 2022, the residence located at 6080 NC 704 Highway East was disconnected from the water
supply well located on the property, and the residence was connected to the water supply well serving
6066 NC 704 Highway East (subject property). The well serving D&M Mart is located on an adjoining
property and approximately 525 feet west southwest of the UST system.
2.3 Hydrogeological Results
Groundwater occurrence underlying the UST system ranged from approximately 33 feet to 34 feet below
ground surface on July 26, 2022. Groundwater occurs above the top of bedrock. The approximate
groundwater flow direction on this date was to the southwest.
2.4 Assessment Results
Gasoline range organics and multiple VOCs were reported at concentrations greater than the
corresponding soil-to-groundwater MSCCs for soil samples MW-1, MW-2, MW-3 and P-1, representing
the UST basin and dispensers. VOC concentrations greater than the residential cleanup levels were
reported in two soil samples collected from one soil boring. VOC concentrations greater than the
residential cleanup levels were reported in one soil sample collected from one soil boring.
Analysis of groundwater samples collected from two monitoring wells, each installed in an apparent
downgradient direction relative to the UST system on July 20, 2022, detected six VOCs and three carbon-
chain fractions at concentrations greater than the corresponding NCAC 2L groundwater quality standards
(2L Standards). No Gross Contamination Level exceedances were reported.
Surface water samples were not collected.
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 3
Free product, or light non-aqueous phase liquid, was observed in monitoring well MW-1 on July 20, 2022,
at a thickness of 0.19 feet. Free product was observed in MW-1 on July 26, 2022, at a thickness of 1.43
feet. MW-1 was installed proximal to the dispenser islands.
Based on the supply well and monitoring well analytical results, the nature of the release is gasoline.
Dissolved phase VOCs have migrated horizontally to the inactive water supply well located at 6080 NC
704 Highway East and 150 feet south of the dispenser islands. The rate of migration is unknown.
Based on the analytical results representing the inactive water well located at 6080 NC 704 East, the
release impacted this receptor. On June 8, 2022, S&ME collected water samples from a water well located
approximately 300 feet southwest of the dispenser island, and at 6100 NC 704 East, and the water well
serving the subject property and located approximately 525 feet west southwest of the dispenser island.
Methyl tert-butyl ether was reported in the sample collected from the 6100 NC 704 East at an estimated
concentration of 0.45 micrograms per liter. No target VOCs were reported in the water sample collected
from the well serving 6066 NC 704 East.
2.5 Risk Classification
The risk classification has not been determined; however, the incident will likely be classified as High Risk
due to the observed presence of water supply wells proximal to the source area.
2.6 Remediation Levels
Remediation levels have not been determined, but will likely be the soil-to-groundwater MSCCs for soil,
the 2L Standards for groundwater, and 0.1 foot thickness for free product.
3.0 Site History and Characterization
3.1 General
D&M Mart is located at 6066 NC 704 Highway East near Sandy Ridge, Stokes County, North Carolina
(Figure 1). The UST system is located on the property as depicted in Figure 2.
3.2 UST Owner and System Data
UST Owner
UST ID
No.
Facility ID
No.
Name of
Owner
Street Address Telephone Dates of
Operation
1 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 4-26-1962 –
2-20-2017
2, 3 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 4-26-1962 –
present
4 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 10-1-1989 –
present
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 4
UST ID
No.
Facility ID
No.
Name of
Owner
Street Address Telephone Dates of
Operation
5 00-0-
0000009253
Huffman
Oil Co.
P.O. Box 730 – 1021 Queen
Ann Street
336-227-8881 5-3-1995 –
present
UST Information
Tank No. Last and
Previous
Contents
Capacity Construction
Details
Tank
Dimensions
Date Tanks
Installed
1 Gasoline 2,000-gallons Single-wall steel Unknown 4-26-1962
2 Gasoline 4,000-gallons Single-wall steel Unknown 4-26-1962
3 Gasoline 3,000-gallons Single-wall steel Unknown 4-26-1962
4 Kerosene 4,000-gallons Single-wall steel Unknown 10/1-1989
5 Gasoline 8,000-gallons Single-wall steel/FRP Unknown 5-3-1995
Status of
USTs
Description
of Piping and
Dispensers
Release from
UST System
Material Released Date of
Release
Release
Description
1 Temporarily
closed
Unknown Unknown Unknown Unknown
2, 3, 4, 5 Single-wall
FRP
Unknown Unknown Unknown Unknown
The kerosene UST (Tank 4) and associated kerosene dispenser are located beside each other in the
southwest portion of the common UST basin, as shown on Figure 3. The inactive gasoline UST (Tank 1) is
located in the southeast corner of the common UST basin. Three active gasoline USTs (Tanks 2, 3, 5) are
located in the north portion of the common UST basin. Two gasoline dispensers adjoin the northeast
corner of the common UST basin. Product lines are located within the common UST basin, as identified
by the overlying concrete pavement system. S&ME is not aware of prior releases or compliance issues
related to the UST system.
3.3 Above Ground Storage Tanks
One diesel above ground storage tank (AST) and associated dispenser are located approximately 100 feet
northwest of the gasoline dispenser island (Figure 3). One approximate 250-gallon heating oil AST is
located west of the southwest corner of the building.
3.4 Release Description
Mr. James Barnwell of Huffman Oil Company contacted Wayne Watterson of S&ME on May 23, 2022,
concerning well water with a reported petroleum-like odor on the adjoining Gary Sands property. S&ME
collected a water sample from the well located at 6080 NC 704 East on May 24, 2022. Analysis of the
sample resulted in VOC concentrations greater than the NCAC 2L Standards. A Health Risk Evaluation of
Water Supply (HRE) dated June 1, 2022, was provided by the NCDEQ to Mr. Gray Sands of 6080 NC 704
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 5
Highway East, in a letter dated June 2, 2022. The HRE stated that water is not recommended for any
residential use at this time. S&ME understands that the residence located at 6080 NC 704 Highway East
was disconnected from the water well on the property, and the residence was connected to the water well
serving 6066 NC 704 Highway East (subject property) on July 8, 2022.
S&ME returned to the site on June 8, 2022, to collect water samples from the water well serving 6066 NC
704 Highway East (subject property), and the well serving 6100 NC 704 East. VOCs were not detected in
the 6066 NC 704 East sample. Analysis of the samples resulted in one VOC in the 6100 NC 704 Highway
East sample at a concentration less than the NCAC 2L Standard. The approximate water supply well
locations are shown on Figure 2. Water supply well analytical results are summarized on Table 1.
Based on the water supply well analytical results, the apparent nature of the release is gasoline. S&ME is
not aware of historical releases on the subject property or of off-site releases near the subject property.
4.0 Site Check
4.1 Release Reporting
S&ME submitted a 24-Hour Report, Form UST-61, to the North Carolina Department of Environmental
Quality (NCDEQ) on May 26, 2022. The NCDEQ issued a Notice of Regulatory Requirements dated
May 26, 2022, outlining the requirement to conduct tank tightness and line tightness testing of the UST
system, and to conduct a site check.
4.2 Tank and Line Tightness Testing
Tank and line tightness testing were performed on the operating UST system located at 6066 NC 704
Highway East for Huffman Oil Company by Precision Tank Service on May 31, 2022. The results of the
tank and line tightness testing indicated a passing results for all the tanks and lines. The results of the
tank and line tightness tests were submitted to Karen Hall of the NCDEQ on June 2, 2022 by James
Barnwell.
4.3 Site Check Procedures
S&ME proposed to collect subsurface soil and groundwater samples on the subject property at apparent
downgradient locations relative to the operating UST system.
Based on the results of the compliance inspections performed on August 18, 2021 and on June 8, 2022,
and on the results of the tank and line tightness testing, actions for repair, replacement or upgrading of
the UST system have not been performed. Soil excavation has not been performed.
4.4 Initial Site Investigation
S&ME was on-site with subcontractor Environmental Drilling & Probing Services to perform soil borings
and to install monitoring wells adjacent to the gasoline UST basin and dispenser islands.
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 6
4.4.1 Soil Sampling
Four soil probes (MW-1, MW-2, MW-3 and P-1) were performed at the site on July 18-19, 2022, to assess
potential soil impacts from the UST system. Soil boring locations are shown on Figure 3. Continuous soil
samples were collected to depths ranging from 30 feet to 45 feet below ground surface (bgs) using
direct-push methods. Boring logs for the soil probes are included in Appendix I. The results for
headspace screening for volatile organic vapors performed on grab soil samples collected at intervals of 5
feet with a photo-ionization detector (PID) are summarized on each boring log and on Table 2.
Soil sample from each soil probe were selected for laboratory analysis, based on field observations and
PID results. Selected samples were transferred by hand using Nitrile gloves to laboratory-provided
containers and were placed in a chilled cooler under chain-of-custody procedures. Soil samples were
shipped to Eurofins analytical laboratory and submitted for analysis for gasoline range organics (GRO) by
Method 8015 and for VOCs by Method 8260D, as summarized on Table 4.
4.4.2 Water Sampling
Surface water samples were not collected.
Soil borings performed by air rotary drilling methods to depths ranging from 40 feet bgs to 41 feet bgs
were converted to 2-inch diameter, PVC, Type II groundwater monitoring wells. The locations of
monitoring wells MW-1, MW-2 and MW-3 are shown on Figure 4. Screened intervals ranging in length
from 15 feet to 20 feet were installed in the lowermost portion of each boring. Each well was secured
with a locked, expandable cap and encased in a cover with bolt-down lid and flush-mount concrete pad.
Well Construction details are summarized on Table 3. Well Construction Details and Well Construction
Records for monitoring wells MW-1, MW-2 and MW-3, are included in Appendix I.
On July 20, 2022, groundwater samples were collected from monitoring wells MW-1, MW-2 and MW-3.
Depth to water measurements ranged from 32.60 feet below top of casing at MW-1, to 33.83 feet below
top of casing in MW-3. Free product, or light non-aqueous phase liquid, was detected in monitoring well
MW-1 at a depth of 31.65 feet below top of casing and at a thickness of 1.43 feet.
A submersible electric pump, using dedicated polyethylene tubing, was used to purge monitoring wells
MW-2 and MW-3 by evacuating greater than three well volumes of water from the well. Groundwater
Sampling Forms are provided in Appendix II. Each groundwater sample was transferred into laboratory-
provided containers using dedicated Nitrile gloves, placed into a cooler with ice, and shipped under
chain-of-custody procedures to Eurofins analytical laboratory. The groundwater samples were submitted
for analysis for volatile petroleum hydrocarbons (VPH) by the MADEP methods, for VOCs by EPA Methods
6200B and 504.1, and for Lead by EPA Method 6010, as summarized on Table 5.
On July 25, 2022, Eurofins informed S&ME that the commercial overnight carrier delivered the sample
container to the laboratory on July 23, 2022, and the sample containers exceeded the acceptable
temperature range (16.6º C).
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 7
4.5 Free Product
Free product, or light non-aqueous phase liquid, was observed in monitoring well MW-1 on July 20, 2022,
at a thickness of 0.19 feet. Free product was observed in MW-1 on July 26, 2022, at a thickness of 1.43
feet (Environmental Field Report; Appendix II).
4.6 Groundwater Occurrence and Flow Direction
S&ME measured the relative top of casing elevations of the monitoring wells. S&ME calculated the
relative water table elevation at each monitoring well location using the top of casing elevations and the
depth of water measurements from the top of casing in monitoring wells MW-2 and MW-3, and the
depth to free product and water measurements in monitoring well MW-1. Liquid level data are
summarized on Table 3. S&ME calculated the direction of groundwater flow, based on depth to
groundwater elevations in monitoring wells MW-1, MW-2 and MW-3, to be toward the south southwest
from the source area at an estimated hydraulic gradient of 0.0606 feet per foot. Estimated groundwater
elevation contours are shown on Figure 5.
4.7 Analytical Results
As summarized in Table 4 and shown on Figure 3 Analysis of 15 soil samples collected from four soil
borings on July 18 and 19, 2022, resulted in the detection of gasoline range organics at concentrations
greater than 10 milligrams per Kilogram (mg/Kg) in six soil samples collected from soil borings MW-1,
MW-3 and P-1. The analysis resulted in the detection of 13 volatile organic compounds (VOCs) at
concentrations greater than the soil-to-groundwater Maximum Soil Contaminant Concentrations (MSCCs)
in 10 soil samples collected from soil borings MW-1, MW-2, MW-3 and P-1. Residential cleanup levels
were exceeded for four VOCs in two soil samples collected from soil boring MW-1. The
industrial/commercial cleanup level was exceeded for naphthalene in soil sample MW-1-30, collected
from a depth of 30 feet in soil boring MW-1.
As summarized in Table 5 and shown on Figure 4, multiple volatile organic compounds were reported at
concentrations greater than the corresponding 2L Standards in samples MW-2 and MW-3. One VOC not
typically associated with petroleum products, tetrachloroethene, was reported in sample MW-3 at a
concentration greater than the 2L Standard. Three carbon-chain fractions greater than the corresponding
2L Standards were reported in the groundwater sample collected from monitoring well MW-2.
The analytical report is provided in Appendix III.
4.8 Assessment Conclusions
Based on the presence of free product in monitoring well MW-1, and on the soil analytical results,
the apparent source of the release are the dispensers and product lines near the dispensers.
Based on the presence of free product in monitoring well MW-1, the vertical extent of the release
is to the saturated zone. The horizontal extent of soil impacts is unknown.
The depth to consolidated material, or top of bedrock, is greater than 45 feet bgs.
The depth to the saturated zone, is approximately 33 feet in the source area.
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 8
Initial site check activities included soil and groundwater assessment, due to the presence of
apparent impacts in a water supply well located on an adjoining property.
The extent of groundwater impacts is unknown.
Surface water samples were not collected. The nearest surface water body appears to be greater
than 500 feet from the source area.
Based on the presence of free product in monitoring well MW-1, the apparent source of free
product is likely the dispensers and associated product lines. Free product thickness was
measured at 1.43 feet one week after installation of MW-1. The extent of free product is
unknown; however, free product was not detected in monitoring well MW-2 located
approximately 15 feet from MW-1 and in a cross gradient position relative to MW-1.
Abatement actions required: recover free product from monitoring well MW-1.
Need for further investigation or remediation: additional soil and groundwater assessment,
including selected resampling of media delivered out of temperature protocol.
5.0 Preliminary Receptor Information
Water supply wells are located within 1,000 feet of the apparent source area at the D&M Grocery
property. As described in Section 3.4 above, S&ME collected water samples representing three water
supply wells observed within 500 feet of the site, including 6066, 6080 and 6100 NC 704 Highway East
(Figure 2). Apparent well structures were not observed at other properties developed near the D&M site;
however, S&ME is not aware of the availability of municipal water service to the area proximal to the site.
Therefore, other properties, if occupied, likely use well water. The preliminary receptor information
indicates a release at the D&M Grocery would be considered high risk by NCDEQ.
6.0 Initial Response and Abatement Action
Huffman Oil Company removed product from the 2,000-gallon premium gasoline tank and placed Tank 5
in temporary closure.
Tank tightness and line tightness testing of the operating UST system performed on May 31, 2022,
resulted in passing tests for all tanks and product lines. On July 8, 2022, the residence located at 6080 NC
704 Highway East was disconnected from the water supply well located on the property, and the
residence was connected to the water supply well serving 6066 NC 704 Highway East (subject property).
On July 15, 2022, the residence located at 6080 NC 704 Highway East was disconnected from the water
supply well located on the property, and the residence was connected to the water supply well serving
6066 NC 704 Highway East (subject property).
Free product recovery actions and soil excavation have not been performed.
Initial Abatement Action Report
D&M Grocery; Incident No.:48461
6066 NC 704 Highway East
Sandy Ridge, Stokes County, North Carolina
S&ME Project No. 22580285
August 5, 2022 9
7.0 Conclusions and Recommendations
Based on the initial soil and groundwater assessment results, and on the presence of free product in the
subsurface, S&ME recommends that a Limited Site Assessment be performed.
Appendices
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\ENV\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\D&M Grocery-FIGS.dwgN
0 2000 4000
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
1
22580285
JULY 2022
AS SHOWNUS TOPO MAP
SOURCE: AYERSVILLE, NC QUADRANGLE, 7.5-MINUTE SERIES US TOPO (2019).
SITE
LEGEND
- GROUNDWATER FLOW DIRECTION
N
0 200 400
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
2
22580285
JULY 2022
AS SHOWNSITE MAP
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\ENV\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
6080 NC 740 HWY E
LEGEND
- APPROXIMATE WATER SUPPLY WELL LOCATION
- APPROXIMATE UST BASIN LOCATION
SITE
6100 NC 740 HWY E
N
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
3
22580285
JULY 2022
AS SHOWNSOIL ANALYTICAL RESULTS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\ENV\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·DATE- JULY 18, 2022: MW-1-10, MW-1-20, MW-1-30, MW-3-10, MW-3-20
·DATE- JULY 19, 2022: MW-3-25, MW-3-30, MW-2-10, MW-2-20, MW-2-25, MW-2-30
AND P-1-10, P-1-20, P-1-25, P-1-30
·METHODS: 8260D, 8015 GASOLINE RANGE ORGANICS
·SEE TABLE 4 FOR SUMMARY OF RESULTS
LEGEND
- APPROXIMATE DISPENSER LOCATION
- SOIL SAMPLE LOCATION
- PROPERTY BOUNDARY
- MILLIGRAMS PER KILOGRAMS
- MAXIMUM SOIL CONTAMINANT CONCENTRATION
- UNDERGROUND STORAGE TANK NUMBER
mg/kg
MSCC
MW-3
MW-2
P-1
MW-1
GASOLINE
DISPENSERS
KEROSENE
DISPENSER
DIESEL
ABOVE-GROUND STORAGE TANK
1
1
23
5
4
MW-1 mg/kg
MW-1-10:<Soil-to-Groundwater MSCC
MW-1-20:>Residential MSCC
MW-1-30:>Industrial/Commercial MSCC
MW-2 mg/kg
MW-2-10:<Soil-to-Groundwater MSCC
MW-2-20:>Soil-to-Groundwater MSCC
MW-2-25:>Soil-to-Groundwater MSCC
MW-2-30:>Soil-to-Groundwater MSCCMW-3 mg/kg
MW-3-10:>Soil-to-Groundwater MSCC
MW-3-20:>Soil-to-Groundwater MSCC
MW-3-25:<Soil-to-Groundwater MSCC
MW-3-30:<Soil-to-Groundwater MSCC
mg/kg
P-1-10:<Soil-to-Groundwater MSCC
P-1-20:>Soil-to-Groundwater MSCC
P-1-25:>Soil-to-Groundwater MSCC
P-1-30:>Soil-to-Groundwater MSCC
P-1
N
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
4
22580285
JULY 2022
AS SHOWNGROUNDWATER ANALYTICAL RESULTS
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\ENV\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·CONSTITUENT CONCENTRATIONS GREATER THAN 2L STANDARD ARE SHOWN
·FREE PRODUCT THICKNESS IN MW-1 = 1.43 FEET ON JULY 26, 2022
·DATE: JULY 20, 2022; MW-2 & MW-3
·METHODS: 6200B, 504.1, 6010D LEAD; VOLATILE PETROLEUM HYDROCARBONS
·SEE TABLE 5 FOR SUMMARY OF RESULTS
LEGEND
- MONITORING WELL LOCATION
- APPROXIMATE DISPENSER LOCATION
- PROPERTY BOUNDARY
- MICROGRAMS PER LITERug/L
MW-3
MW-2
MW-1
MW-1 ug/L
Not Sampled (Light Non-aqueous Phase Liquid)
MW-2 ug/L
1,2,4-Trimethylbenzene 699
Benzene 995
Ethylbenzene 1,120
Xylenes, Total 7,050
Toluene 12,100
C5-C8 Aliphatics 33,700
C9-C18 Aliphatics 16,700
C9-C22 Aromatics 4,670
MW-3 ug/L
Benzene 14.4
Tetrachloroethene 3.92
N
0 50 100
(IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALE
D&M GROCERY
INCIDENT No. 48461
6066 NC 704 HIGHWAY EAST, SANDY RIDGE, STOKES COUNTY, NC
5
22580285
JULY 2022
AS SHOWNGROUNDWATER ELEVATION CONTOUR MAP
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.Drawing Path: T:\ENV\Projects\2022\22580285_Huffman Oil Company_D&M Grocery_Sandy Ridge, NC\4 ENV\CAD\D&M Grocery-FIGS.dwgSOURCE: 2018 AERIAL PHOTOGRAPH AND 2022 STOKES COUNTY, NC PARCEL DATA DOWNLOADED FROM NC ONEMAP.NC 704
HWY
NOTES
·DATE: JULY 26, 2022
·CONTOUR INTERVAL = 1 FOOT
LEGEND
- MONITORING WELL LOCATION
- APPROXIMATE DISPENSER LOCATION
- RELATIVE GROUNDWATER ELEVATION
- GROUNDWATER FLOW DIRECTION
- PROPERTY BOUNDARY
MW-3
MW-2
MW-1
68
67
66
(68.14)
(67.61)
(65.47)
(65.47)
Analytical Method 625.1
Location Compounds of
Concern
Sample Date
6080 6080 NC 704 Highway East 05/24/22 5.8 177 27.8 23.1 5.9 0.76 7.8 7.1 176 61.0 3.4 513 227
6100 Well 6100 NC 704 Highway East 06/08/22 NA <0.50 <0.50 <0.50 <0.50 0.45 J <2.0 <0.50 <0.50 <0.50 <0.50 <1.5 <100
6066 Well 6066 NC 704 Highway East 06/08/22 NA <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <1.5 <100
6 1 70 600 70 20 6 70 600 400 400 500 40
6,000 5,000 70,000 80,000 30,500 20,000 6,000 26,100 260,000 28,500 24,100 50,000 40,000
NOTES:
Analytes that are not shown were not detected
NA = Not Analyzed
Data presented in micrograms per liter
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
J- Detected but less than the reporting limit; result is an estimated concentration.
Value Concentration exceeds the 2L Standard
TABLE 1
S&ME Project No. 22580285
6066 NC 704 Highway East, Sandy Ridge, North Carolina
D&M Grocery
Summary of Water Supply Well Sampling Results
2L Standard
Gross Contamination Level n-PropylbenzeneEthylbenzeneChloroformSample ID
BenzeneIsopropylbenzeneMethyl tert-Butyl Ether (MTBE)NaphthaleneXylenes (Total)NaphthaleneVolatile Organic Compounds by Method 6200B
tert-Amyl Alcohol (TAA)Toluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneFacility ID No.: 00-0-0000009253 Date: 8/1/2022
Facility ID No.: 00-0-0000009253
4-5 9-10 14-15 19-20 24-25 29-30 34-35 39-40 44-45
MW-1 7/18/22 10.0 2.0 223.0 214.0 1,365 988.0 75.0 6.0 2.0
MW-2 7/18/22 7.2 16.3 28.2 90.9 238.0 2,031
MW-3 7/18/22 61 18 7 11.0 <1 1.6
P-1 7/19/22 27.5 38.8 160.9 364/2 654/2 1,212
Note: Readings collected with photo-ionization detector (PID) in parts per million after allowing headspace equilibration for approximately 5 minutes.
Sample
Location Date Depth of PID Reading (feet)
TABLE 2
Field Screening Results
D&M Grocery (Incident No.: 48461)
6066 NC 704 Highway East, Sandy Ridge, North Carolina
S&ME Project No. 22580285
Date: 8/2/2022
Facility ID No.: 00-0-0000009253 Date: 7/28/2022
Well
ID
Date
Installed
Screen
Interval
(ft-BGS)
Well Casing
Depth
(ft-BGS)
Total Depth
(ft-BGS)
Relative Top of
Casing Elevation*
(ft.)
Date of
Measurement
Depth To
Water (ft.
BTOC)
Depth To
Product (ft.
BTOC)
Product
Thickness (ft.)
Relative
Groundwater
Elevation (feet)
MW-1 07/19/22 25 - 40 0.5 - 25 40.0 100.00 7/26/2022 32.88 31.45 1.43 68.14
MW-2 07/19/22 20 - 40 0.3 - 20 40.0 100.27 7/26/2022 32.66 ND ND 67.61
MW-3 07/19/22 20 - 40 0.4 - 20 40.0 99.44 7/26/2022 33.97 ND ND 65.47
NOTES:
ft : feet
ft-BGS : feet below ground surface
ND - Not detected
BTOC: Below top-of-casing
*Reference Point for Elevation Measurements: MW-1, Assigned Elevation: 100.00 ft.
Table 3
Monitor Well Construction and Liquid Level Data
S&ME Project No. 225802856066 NC 704 Highway East, Sandy Ridge, North Carolina
D&M Grocery (Incident No.: 48461)
Page 1 of 1
Method
8015 1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2-Butanone (MEK)2-Hexanone4-Isopropyltoluene4-Methyl-2-pentanone (MIBK)AcetoneBenzeneEthylbenzeneHexaneIodomethaneIsopropyl etherIsopropylbenzeneMethyl tert-butyl etherNaphthalenen-Butylbenzenen-Heptanen-Propylbenzenesec-ButylbenzeneTolueneXylenes (total)Gasoline Range OrganicsDate
Collected
Sample
Type Sample Depth
(feet)mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
MW-1-10 7/18/22 Grab 10 2.01 0.487 <1.22 <1.22 <0.244 <0.122 <2.44 <0.244 0.944 <2.44 <2.44 <0.488 <2.44 <2.44 0.188 J 0.106 J <2.44 0.319 <2.44 2.56 5.89 55.1
MW-1-20 7/18/22 Grab 20 222 57.1 <1.52 <1.52 7.36 <1.52 <3.04 1.12 78.4 1.95 <0.304 <0.609 18 <0.304 24.4 8.86 6.82 37.6 2.48 95.8 768 1,460
MW-1-30 7/18/22 Grab 30 371 129 <33.7 <33.7 5.77 J <33.7 <67.4 25.3 253 32.3 <6.74 <13.5 31.7 <6.74 45.8 29.7 67.4 94.0 <6.74 764 1,360 19,000
MW-3-10 7/18/22 Grab 10 0.0333 0.0110 <0.0360 <0.0360 <0.00720 <0.0360 0.102 0.0527 0.115 0.00631 J 0.00247 J <0.0144 0.00578 J <0.00720 <0.00720 <0.00720 0.00849 0.0128 <0.00720 1.06 0.548 E 9.57 J
MW-3-20 7/18/22 Grab 20 0.0328 0.00967 J <0.0495 <0.0495 <0.00990 <0.0495 0.0351 J 0.0331 0.0845 0.00407 J <0.00990 <0.0198 0.00513 J <0.00990 <0.00990 <0.00990 <0.00990 0.0106 <0.00990 1.68 0.422 12.1 J
MW-3-25 7/19/22 Grab 25 <0.00609 <0.00609 <0.0304 <0.0304 <0.00609 <0.0304 0.0230 J <0.00609 <0.00609 <0.00609 <0.00609 <0.0122 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 <0.00609 0.00383 J 0.00361 J <12.7 1
MW-3-30 7/19/22 Grab 30 <0.00682 <0.00682 <0.0341 <0.0341 <0.00682 <0.0341 0.0153 J <0.00682 <0.00682 <0.00682 <0.00682 <0.0136 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 <0.00682 0.00707 0.0107 J 11.4
MW-2-10 7/19/22 Grab 10 <0.00802 <0.00802 0.0519 <0.0401 <0.00802 <0.0401 0.188 <0.00802 <0.00802 <0.00802 0.00320 J <0.0160 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 <0.00802 0.00433 J <0.0160 <15.7 1
MW-2-20 7/19/22 Grab 20 <0.00894 <0.00894 1.2600 0.1870 <0.00894 0.0639 <3.28 <0.00894 <0.00894 <0.00894 0.00444 J <0.0179 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.00894 <0.0179 6.96 J
MW-2-25 7/19/22 Grab 25 0.00989 <0.00772 0.3960 0.0325 J <0.00772 <0.0386 0.494 0.00775 0.00843 0.00296 J <0.00772 <0.0154 <0.00772 <0.00772 <0.00772 <0.00772 <0.00772 0.00398 J <0.00772 0.0273 0.0533 <15.9 1
MW-2-30 7/19/22 Grab 30 0.0536 0.0245 0.0978 0.0274 J 0.0111 <0.0355 0.306 0.0102 0.0227 0.00793 <0.00710 <0.0142 0.00610 J <0.00710 0.0243 0.016 0.0175 0.0152 0.00406 J 0.0528 0.143 6.82 J
P-1-10 7/19/22 Grab 10 <0.00812 <0.00812 0.0336 J <0.0406 <0.00812 <0.0406 0.299 <0.00812 <0.00812 <0.00812 <0.00812 <0.0162 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 <0.00812 0.00449 J 0.00686 J <15.4 1
P-1-20 7/19/22 Grab 20 0.00662 J <0.00816 0.1090 <0.0408 <0.00816 <0.0408 0.589 0.0122 0.00594 J <0.00816 0.00826 <0.0163 <0.00816 0.0227 <0.00816 <0.00816 <0.00816 <0.00816 <0.00816 0.0334 0.0409 <16.5 1
P-1-25 7/19/22 Grab 25 0.0267 0.0085 0.1890 <0.402 <0.00804 <0.402 0.757 0.0536 0.0381 0.00366 J <0.00804 0.00342 J 0.00402 J 0.0517 <0.00804 <0.00804 0.00707 J 0.00583 J <0.00804 0.244 0.219 5.48 J
P-1-30 7/19/22 Grab 30 32.4 8.02 <1.74 <1.74 1.39 <1.74 <3.47 3.33 19.3 2.67 <0.347 <0.694 1.77 <0.347 3.55 1.87 4.48 5.54 0.497 64.9 105 828
6.6 6.6 16 0.17 0.12 0.42 24 0.0072 8 NSE NSE 0.32 1.3 0.085 0.2 2.4 NSE 1.4 2.2 5.4 6 NA
156 156 9,380 78.2 1,560 1,250 14,000 12 60.3 NSE NSE 156 1,560 156 5.5 782 NSE 1,560 1,560 1,250 3,120 NA
2,330 2,330 140,000 1,160 23,300 18,600 210,000 59.4 297 NSE NSE 2,330 23,300 1,820 27 11,600 NSE 23,300 23,300 18,600 46,700 NA
NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10
Notes:
NA - Not Applicable
MSCC = Maximum Soil Contaminant Concentration (March 7, 2022)
Concentration exceeds the Soil-to-Groundwater MSCC
Concentration exceeds the Residential Soil Cleanup Level
Concentration exceeds the Industrial/Commercial Soil Cleanup Level
Facility ID No.: 00-0-0000009253
Table 4
Summary of Soil Sampling Results
D&M Grocery (Incident No.: 48461)
6066 NC Highway 704 East, Sandy Ridge, North Carolina
S&ME Project No. 22580285
Date: 8/5/2022
mg/kg = milligrams per kilogram
Analytical Method
Sample ID
Constituent
Soil-to-Groundwater MSCCs
Industrial/Commercial Soil Cleanup Levels
Only detected compounds are shown.
Residential Soil Cleanup Levels
Method 8260D
Action Level
J- Detected but concentration is less than the Reporting Limit; result is an approximate value.
Facility ID No.: 00-0-0000009253
Method 504.1 6010
Constituent
Sample Date
MW-1 07/20/22
MW-2 07/20/22 <0.0184 <10.0 699 H <250 <250 995 H <250 1,120 H <250 <1,000 7,050 H <500 <250 <250 12,100 H 33,700 16,700 4,670
MW-3 07/20/22 <0.0181 11.6 90.4 29.2 2.41 14.4 0.599 56.5 5.09 5.97 291.2 E 11.0 17.8 3.92 20.0 348 404 533 F1
0.02 15 400 400 25 1 70 600 70 6 500 70 70 0.7 600 400 700 200
50 15,000 28,500 24,100 11,700 5,000 70,000 80,000 30,500 6,000 50,000 5,900 26,100 700 260,000 NSE NSE NSE
NOTES:Concentration exceeds the 2L Standards
Constituents that are not shown were not detected Concentration exceeds the Gross Contamination Levels
Data presented in micrograms per liter or mg/L
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202 (March 7, 2022)
VPH - Volatile Petroleum Hydrocarbons
E - Result exceeded calibration range1,2-Dibromoethane (Ethylene Dibromide)LeadSample ID
Not Sampled- Free Product (Light Non-aqueous Phase Liquid)C9-C22 AromaticsC9-C18 AliphaticsC5-C8 Aliphatics1,3,5-Trimethylbenzenen-ButylbenzeneBenzeneIsopropylbenzeneEthylbenzeneChloroform4-Isopropyltoluene Date: 8/5/2022
6200B MADEP-VPH
Table 5
Summary of Groundwater Sampling Results
D&M Grocery (Incident No.: 48461)
6066 NC 704 Highway East, Sandy Ridge, North CarolinaS&ME Project No. 22580285
Naphthalene1,2,4-TrimethylbenzeneToluenen-PropylbenzeneXylenes, TotalTetrachloroetheneNSE - No Gross Contamination Level established
2L Standard
Gross Contamination Level
Page 1 of 1
Appendix I- Boring Logs, Well Construction Details and Well
Construction Records
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE27.5
38.8
160.9
654.2
1212
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: P-16066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course, .,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable C. McMechen
No
5
Fill, Clayey Silt, Orange, Dry,
Yes
10
Residuum, Silt, Brown, Stained soil at 10 feet, Dry, Moist at 25 feet, wet at 30 feet, Strong Petroleum
No
15
Yes
20
Yes
25
Yes
30
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.0
223.0
1365
988.0 Yes
30
No
25
Yes
20 Sandy Silt , Brown, Micaceous Wet- 38 feet
No
15
Yes
10
Sandy Silt, Red, Brown, Micaceous
5 DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESClayey Silt, Red
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable W. Watterson
DATE DRILLED:Monday, July 18, 2022 45
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-16066 NC 704 Highway East, Sandy Ridge, NC
10.0
214.0
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE75.0
6.0
2.0
60
55
50
No
45 Boring Terminated at 45 Ft-BGS
Yes
40
35
No
DRILLING METHOD: DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESHAMMER TYPE: Not Applicable W. Watterson
SAMPLING METHOD: Macro-Core Sampler
DRILL RIG: Geoprobe 7822 DT
DRILLER: Environmental Drilling and Probing Services, LLC
PROJECT:D&M Grocery
BORING LOG: MW-16066 NC 704 Highway East, Sandy Ridge, NC
DATE DRILLED:Monday, July 18, 2022 45
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE7.2
16.3
28.2
238.0
2031
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-26066 NC 704 Highway East, Sandy Ridge, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course, .,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable C. McMechen
No
5
Fill, Clayey Silt, Orange, Dry,
Yes
10
Residuum, Silt, Brown, Dry, Moist at 25 feet, Strong Petroleum Odors at 20 feet
No
15
Yes
20
Yes
25
Yes
30
S&ME Project No. 22580285
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEOVA READINGS(PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE61.0
18.0
7.0
0.5
1.6 Yes
30
Yes
25
Yes
20
No
15
Yes
10
Residuum, Silt, Brown, Tan, Mica, Dry
No
5
Fill, Clayey Silt, Orange, Dry DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESAsphalt pavement and base course
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD:
DRILLER: Environmental Drilling and Probing Services, LLC
HAMMER TYPE: Not Applicable W. Watterson
DATE DRILLED:Tuesday, July 19, 2022 30
DRILL RIG: Geoprobe 7822 DT
PROJECT:D&M Grocery
BORING LOG: MW-36066 NC 704 Highway East, Sandy Ridge, NC
11
Well ID
MW-1
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.1 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.5 ft
0.5 to 25.0
25.0 to 40.0
Top of Seal - 21.0 0.1 ft-bgs
Top of Filter Pack - 23.0 0.1 ft-bgs
0.5 to 21.0
Top of Screen - 25.0 0.1 ft-bgs
21.0 to 23.0
Screened Interval -15.0 0.1 ft-bgs
23.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 40.5 0.1 ft-bgs
Form Revision Date:
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable
40.0
35.0
Northing (0.1 ft)Date/Time
7/19/22 12:20
Total Well Depth (0.1 ft-bgs)
31.45 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
9/1/17 2:10 PM
TBD - To Be Determined
Notes: Free product detected; lowermost screened interval length = 5 feet
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
No
For lithologic information
see attached boring log
BTOC - Below Top of Casing
Well ID
MW-2
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.1 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.3 ft
0.3 to 20.0
20.0 to 40.0
Top of Seal - 15.0 0.1 ft-bgs
Top of Filter Pack - 18.0 0.1 ft-bgs
0.3 to 15.0
Top of Screen - 20.0 0.1 ft-bgs
15.0 to 18.0
Screened Interval -20.0 0.1 ft-bgs
18.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 41.0 0.1 ft-bgs
Form Revision Date:9/1/17 2:10 PM
TBD - To Be Determined
Notes:
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
For lithologic information
see attached boring log
15
BTOC - Below Top of Casing
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
40.0
37.0
Northing (0.1 ft)Date/Time
7/19/22 13:15
Total Well Depth (0.1 ft-bgs)
32.66 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable
Well ID
MW-3
S&ME Staff
C. McMechen
Drill Rig
Canterra
Water Level at TOB (0.01 ft-bgs)Land Surface Elev. (0.01 ft)
Depth to Product (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground 0.4 ft
0.4 to 20.0
20.0 to 40.0
Top of Seal - 16.0 0.1 ft-bgs
Top of Filter Pack - 18.0 0.1 ft-bgs
0.4 to 16.0
Top of Screen - 20.0 0.1 ft-bgs
16.0 to 18.0
Screened Interval -20.0 0.1 ft-bgs
18.0 to 40.0
Bottom of Screen - 40.0 0.1 ft-bgs
Bottom of Filter Pack - 40.0 0.1 ft-bgs
Cave In - 0.1 ft-bgs
Total Boring Depth - 40.0 0.1 ft-bgs
Form Revision Date:9/1/17 2:10 PM
TBD - To Be Determined
Notes:
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
For lithologic information
see attached boring log
10
BTOC - Below Top of Casing
Air Rotary
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
2-in Sch 40 PVC (0.010)
Portland Cement T2
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
6-inch
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Project Name
48461 - D&M Grocery
Project Number
22580285
WELL CONSTRUCTION DETAIL
40.0
Dry
Northing (0.1 ft)Date/Time
7/19/22 0:00
Total Well Depth (0.1 ft-bgs)
33.97 7/26/22 13:00
Environmental Drilling & Probing Services
Easting (0.1 ft)Date/Time
Installation Date
7/19/2022
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Stokes Sandy Ridge
License Number
3307
Well Permit Number
Not applicable
Appendix II- Groundwater Sampling Forms and Environmental
Field Report
° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
31.84 ft-TOC inch
40.85 ft-TOC gal
9.01 feet gal
15 ft-GRD gal
ft-GRD
End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
Qty Container Pres.Qty Pres.
(1)
Notes:
Form Revision Date:
Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:
Project Location:
Project Number:
Source Well:
D&M Grocery
6066 NC-704, Sandy Ridge, NC 27046
22580285
MW-1
Purge Date: July 20, 2022
Analytical Data
Method Method
Did not develop/ purge or sample due to presence of free product from 31.65 ft below ToC to 31.84 ft below ToC.
9/13/17 8:00 AM
Name Signature
Cody McMechen
Date
8/3/2022
Container
Sample Method:Sample Time:
Total Volume Purged:Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
(Gal)
Stickup Height:
Well Purging Information
Purge Method:Purge Start Time:
Total Well Depth:Well Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
1.5
4.4
7.4
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter
Conductivity 1,413 1,413
7.0
µS/cm
2
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
pH 4.00, 7.00, 10.00
Air Temp:
July 20, 2022
90
Sample Time:
Sample Date:
Weather:
Locked?:
Sampled By:
Yes
Cody McMechen
Sunny
° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
32.60 ft-TOC inch
40.22 ft-TOC gal
7.62 feet gal
20 ft-GRD gal
ft-GRD
12:35 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
14:40 5.4 19.4 375
14:40
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
1 250mL P HNO3
2 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Cody McMechen 8/3/2022
Developed/ purged well until turbidity was lowered to an acceptable level.
9/13/17 8:00 AM
EDB 504.1
Name Signature Date
Metals 6010 (Total)
VPH MADEP
Analytical Data
Method Method Container
VOCs 6200
Sample Method:Bailer Sample Time:
(Gal)
15.0
Total Volume Purged:15.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 6.2
Stickup Height:
Well Purging Information
Purge Method:Submersible Pump Purge Start Time:13:30
Total Well Depth:Well Volume 1.2
Height of Water Column:3 * Well Volume 3.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather: Sunny Air Temp: 90
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?: Yes Sample Date: July 20, 2022
Sampled By: Cody McMechen Sample Time: 14:40
Project Number: 22580285 Purge Date: July 20, 2022
Source Well:MW-2 Purge Time (Min.): 55
GROUNDWATER SAMPLING FORM
Project Name: D&M Grocery
Project Location: 6066 NC-704, Sandy Ridge, NC 27046
° F
Date Time
7/20/22 14:00 4.0 10.0
7/20/22 14:00 µS/cm
33.83 ft-TOC inch
40.21 ft-TOC gal
6.38 feet gal
20 ft-GRD gal
ft-GRD
10:55 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
14:15 4.7 18.2 203
14:15
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
1 250mL P HNO3
2 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Cody McMechen 8/3/2022
Developed/ purged well until turbidity was lowered to an acceptable level.
9/13/17 8:00 AM
EDB 504.1
Name Signature Date
Metals 6010 (Total)
VPH MADEP
Analytical Data
Method Method Container
VOCs 6200
Sample Method:Bailer Sample Time:
(Gal)
10.3 No Odors
Total Volume Purged:10.3 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 5.2
Stickup Height:
Well Purging Information
Purge Method:Submersible Pump Purge Start Time:11:45
Total Well Depth:Well Volume 1.0
Height of Water Column:3 * Well Volume 3.1
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather: Sunny Air Temp: 85
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?: Yes Sample Date: July 20, 2022
Sampled By: Cody McMechen Sample Time: 14:15
Project Number: 22580285 Purge Date: July 20, 2022
Source Well:MW-3 Purge Time (Min.): 50
GROUNDWATER SAMPLING FORM
Project Name: D&M Grocery
Project Location: 6066 NC-704, Sandy Ridge, NC 27046

Hours Mileage Signature of S&ME Personnel
2 70 Wayne Watterson

S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
7/26/2022
Job Number:
22580285
Project Name:
D&M Grocery
Weather/Temperature:
Clear, hot
Project Location:
Sandy Ridge, NC
Notes By:
☒
Present at the Site:
Wayne Watterson
☐

Arrived at the property at approximately 1250.
The pads for monitoring wells MW-1, 2, and 3, installed last week, were in good condition. I asked the
store employee if there were or if there appeared to be any changes to the UST equipment since S&ME
completed the soil probes and monitoring well installations last week. He said there was no change to
the system.
I opened monitoring wells and checked depth to water/product in the monitoring wells. Information is
provided below
well Depth to water (ft) Depth to product (ft) Notes
MW-1 32.88 31.45 Used oil/water interface
for measurements
MW-2 32.66 No product Used oil/water interface
for measurements
MW-3 33.97 No product Used water level probe.
No odors or observed
product or sheen on
probe.

After taking depth to water/product measurements, I closed the wells and bolted down the well covers.

I left the site at approximately 1320.

Attachments:

Equipment Used

Appendix III- Analytical Report
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-218771-1
Client Project/Site: D&M Grocery
For:
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, North Carolina 27409
Attn: Wayne Watterson
Authorized for release by:
8/4/2022 5:25:53 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Definitions/Glossary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
E Result exceeded calibration range.
H Sample was prepped or analyzed beyond the specified holding time
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1-Surrogate recovery exceeds control limits, low biased.
GC Semi VOA
Qualifier Description
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Qualifier
S1+Surrogate recovery exceeds control limits, high biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Lab Sample ID Client Sample ID Matrix Collected Received
680-218771-1 MW-1-10 Soil 07/18/22 10:45 07/23/22 09:30
680-218771-2 MW-1-20 Soil 07/18/22 10:50 07/23/22 09:30
680-218771-3 MW-1-30 Soil 07/18/22 10:55 07/23/22 09:30
680-218771-4 MW-3-10 Soil 07/18/22 11:35 07/23/22 09:30
680-218771-5 MW-3-20 Soil 07/18/22 11:45 07/23/22 09:30
680-218771-6 MW-3-25 Soil 07/19/22 16:10 07/23/22 09:30
680-218771-7 MW-3-30 Soil 07/19/22 16:15 07/23/22 09:30
680-218771-8 MW-2-10 Soil 07/19/22 16:20 07/23/22 09:30
680-218771-9 MW-2-20 Soil 07/19/22 16:26 07/23/22 09:30
680-218771-10 MW-2-25 Soil 07/19/22 16:30 07/23/22 09:30
680-218771-11 MW-2-30 Soil 07/19/22 16:35 07/23/22 09:30
680-218771-12 P-1-10 Soil 07/19/22 16:44 07/23/22 09:30
680-218771-13 P-1-20 Soil 07/19/22 16:48 07/23/22 09:30
680-218771-14 P-1-25 Soil 07/19/22 16:50 07/23/22 09:30
680-218771-15 P-1-30 Soil 07/19/22 16:55 07/23/22 09:30
680-218771-16 MW-3 Ground Water 07/20/22 14:15 07/23/22 09:30
680-218771-17 MW-2 Ground Water 07/20/22 14:40 07/23/22 09:30
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Case Narrative
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Job ID: 680-218771-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-218771-1
Receipt
The samples were received on 7/23/2022 9:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 16.6°C
Receipt Exceptions
Received warm with very little water in cooler. Cooler was in transit for 3 days. Client was contacted and the lab received permission
to proceed with the analyses.
GC/MS VOA
Method SM6200_B: Reanalysis of the following sample(s) was performed outside of the analytical holding time due to dilutions. The
samples are one day out of hold: MW-2 (680-218771-17).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Gasoline Range Organics
Method 8015D_GRO: Surrogate recovery for the following sample was outside control limits: MW-1-20 (680-218771-2). Re-analysis was
performed and surrogate recovery was outside control limits. Sample matrix interference is suspected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method 504.1: Sample was moved to an empty vial because of sediment in the following sample: MW-3 (680-218771-16) and MW-2
(680-218771-17)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-1Client Sample ID: MW-1-10
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.244 0.0634 mg/Kg ☼07/26/22 10:32 07/27/22 18:29 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,1-Trichloroethane ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2,2-Tetrachloroethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.244 0.0732 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1,2-Trichloroethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloroethane ND
0.244 0.176 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloroethene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,1-Dichloropropene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,3-Trichlorobenzene ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,3-Trichloropropane ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,4-Trichlorobenzene ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2,4-Trimethylbenzene 2.01
0.488 0.0780 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dibromo-3-Chloropropane ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichlorobenzene ND
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichloroethane ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,2-Dichloropropane ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3,5-Trimethylbenzene 0.487
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3-Dichlorobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,3-Dichloropropane ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼1,4-Dichlorobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2,2-Dichloropropane ND
1.22 0.449 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Butanone (MEK)ND
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Chlorotoluene ND
1.22 0.927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼2-Hexanone ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Chlorotoluene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Isopropyltoluene ND
1.22 0.878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼4-Methyl-2-pentanone (MIBK)ND
2.44 0.537 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Acetone ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Benzene ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromobenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromoform ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Bromomethane ND *+
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Carbon disulfide ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Carbon tetrachloride ND
0.244 0.0683 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorobenzene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorobromomethane ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chlorodibromomethane ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloroethane ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloroform ND
0.244 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Chloromethane ND
0.244 0.141 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼cis-1,2-Dichloroethene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼cis-1,3-Dichloropropene ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Dibromomethane ND
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Dichlorobromomethane ND
0.488 0.488 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethyl acetate ND
0.244 0.102 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethylbenzene 0.944
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Ethylene Dibromide ND
0.244 0.200 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Hexachlorobutadiene ND
0.244 0.0829 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-1Client Sample ID: MW-1-10
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.244 0.0829 mg/Kg ☼07/26/22 10:32 07/27/22 18:29 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.488 0.0732 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Isopropyl ether ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Isopropylbenzene ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Methyl tert-butyl ether ND *+
0.488 0.390 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Methylene Chloride ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼m-Xylene & p-Xylene 3.97
0.244 0.151 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Naphthalene 0.188 J
0.244 0.0927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼n-Butylbenzene 0.106 J
0.244 0.210 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼n-Heptane ND
0.244 0.107 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼N-Propylbenzene 0.319
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼o-Xylene 1.92
0.244 0.0976 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼sec-Butylbenzene ND
0.244 0.0927 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Styrene ND
0.244 0.122 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼tert-Butylbenzene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Tetrachloroethene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Toluene 2.56
0.244 0.112 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,2-Dichloroethene ND
0.244 0.127 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,3-Dichloropropene ND
0.488 0.117 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼trans-1,4-Dichloro-2-butene ND
0.244 0.0878 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Trichloroethene ND
0.244 0.151 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Trichlorofluoromethane ND
0.488 0.268 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Vinyl acetate ND
0.244 0.137 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Vinyl chloride ND
0.488 0.176 mg/Kg 07/26/22 10:32 07/27/22 18:29 40☼Xylenes, Total 5.89
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 18:29 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 07/26/22 10:32 07/27/22 18:29 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 18:29 4065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 18:29 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
55.1 14.1 3.52 mg/Kg ☼07/26/22 10:32 07/28/22 15:36 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 15:36 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.304 0.0791 mg/Kg ☼07/26/22 10:32 07/26/22 20:13 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,1-Trichloroethane ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2,2-Tetrachloroethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.304 0.0913 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1,2-Trichloroethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloroethane ND
0.304 0.219 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloroethene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,1-Dichloropropene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,3-Trichlorobenzene ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,3-Trichloropropane ND
0.304 0.152 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2,4-Trichlorobenzene ND
0.609 0.0974 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dibromo-3-Chloropropane ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichlorobenzene ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichloroethane ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,2-Dichloropropane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,3-Dichlorobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,3-Dichloropropane ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼1,4-Dichlorobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2,2-Dichloropropane ND
1.52 0.560 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Butanone (MEK)ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Chlorotoluene ND
1.52 1.16 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼2-Hexanone ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Chlorotoluene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Isopropyltoluene 7.36
1.52 1.10 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼4-Methyl-2-pentanone (MIBK)ND
3.04 0.670 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Acetone ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Benzene 1.12
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromobenzene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromoform ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Bromomethane ND *+
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Carbon disulfide ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Carbon tetrachloride ND
0.304 0.0852 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorobenzene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorobromomethane ND
0.304 0.128 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chlorodibromomethane ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloroethane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloroform ND
0.304 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Chloromethane ND
0.304 0.177 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼cis-1,2-Dichloroethene ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼cis-1,3-Dichloropropene ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Dibromomethane ND
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Dichlorobromomethane ND
0.609 0.609 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Ethyl acetate ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Ethylene Dibromide ND
0.304 0.250 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Hexachlorobutadiene ND
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Hexane 1.95
0.304 0.103 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Iodomethane ND
0.609 0.0913 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Isopropyl ether ND
0.304 0.134 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Methyl tert-butyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Methylene Chloride ND 0.609 0.487 mg/Kg ☼07/26/22 10:32 07/26/22 20:13 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.304 0.116 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼n-Butylbenzene 8.86
0.304 0.262 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼n-Heptane 6.82
0.304 0.122 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼sec-Butylbenzene 2.48
0.304 0.116 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Styrene ND
0.304 0.152 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼tert-Butylbenzene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Tetrachloroethene ND
0.304 0.140 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,2-Dichloroethene ND
0.304 0.158 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,3-Dichloropropene ND
0.609 0.146 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼trans-1,4-Dichloro-2-butene ND
0.304 0.110 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Trichloroethene ND
0.304 0.189 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Trichlorofluoromethane ND
0.609 0.335 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Vinyl acetate ND
0.304 0.170 mg/Kg 07/26/22 10:32 07/26/22 20:13 40☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)90 65-130 07/26/22 10:32 07/26/22 20:13 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)113 07/26/22 10:32 07/26/22 20:13 4065-130
Dibromofluoromethane (Surr)90 07/26/22 10:32 07/26/22 20:13 4065-130
Toluene-d8 (Surr)92 07/26/22 10:32 07/26/22 20:13 4065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 222 7.61 3.80 mg/Kg ☼07/26/22 10:32 07/27/22 16:28 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.61 3.65 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼1,3,5-Trimethylbenzene 57.1
7.61 3.20 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Ethylbenzene 78.4
7.61 3.35 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Isopropylbenzene 18.0
7.61 4.72 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Naphthalene 24.4
7.61 3.35 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼N-Propylbenzene 37.6
7.61 3.50 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼o-Xylene 147
7.61 3.96 mg/Kg 07/26/22 10:32 07/27/22 16:28 1000☼Toluene 95.8
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 16:28 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 16:28 100065-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 16:28 100065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 16:28 100065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL2
RL MDL
m-Xylene & p-Xylene 521 38.0 16.7 mg/Kg ☼07/26/22 10:32 08/01/22 17:33 5000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
76.1 27.4 mg/Kg 07/26/22 10:32 08/01/22 17:33 5000☼Xylenes, Total 768
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 08/01/22 17:33 5000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 07/26/22 10:32 08/01/22 17:33 500065-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 08/01/22 17:33 500065-130
Toluene-d8 (Surr)97 07/26/22 10:32 08/01/22 17:33 500065-130
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-2Client Sample ID: MW-1-20
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
1460 157 39.3 mg/Kg ☼07/26/22 10:32 07/29/22 19:45 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 68 S1-70-131 07/26/22 10:32 07/29/22 19:45 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-3Client Sample ID: MW-1-30
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 6.74 1.75 mg/Kg ☼07/26/22 10:32 07/27/22 16:52 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,1-Trichloroethane ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2,2-Tetrachloroethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
6.74 2.02 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1,2-Trichloroethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloroethane ND
6.74 4.85 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloroethene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,1-Dichloropropene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,3-Trichlorobenzene ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,3-Trichloropropane ND
6.74 3.37 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2,4-Trichlorobenzene ND
13.5 2.16 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dibromo-3-Chloropropane ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichlorobenzene ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichloroethane ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,2-Dichloropropane ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3,5-Trimethylbenzene 129
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3-Dichlorobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,3-Dichloropropane ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼1,4-Dichlorobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2,2-Dichloropropane ND
33.7 12.4 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Butanone (MEK)ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Chlorotoluene ND
33.7 25.6 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼2-Hexanone ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Chlorotoluene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Isopropyltoluene 5.77 J
33.7 24.3 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼4-Methyl-2-pentanone (MIBK)ND
67.4 14.8 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Acetone ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Benzene 25.3
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromobenzene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromoform ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Bromomethane ND *+
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Carbon disulfide ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Carbon tetrachloride ND
6.74 1.89 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorobenzene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorobromomethane ND
6.74 2.83 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chlorodibromomethane ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloroethane ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloroform ND
6.74 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Chloromethane ND
6.74 3.91 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼cis-1,2-Dichloroethene ND
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼cis-1,3-Dichloropropene ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Dibromomethane ND
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Dichlorobromomethane ND
13.5 13.5 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Ethyl acetate ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Ethylene Dibromide ND
6.74 5.53 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Hexachlorobutadiene ND
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Hexane 32.3
6.74 2.29 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Iodomethane ND
13.5 2.02 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Isopropyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-3Client Sample ID: MW-1-30
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropylbenzene 31.7 6.74 2.97 mg/Kg ☼07/26/22 10:32 07/27/22 16:52 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Methyl tert-butyl ether ND *+
13.5 10.8 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Methylene Chloride ND
6.74 4.18 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Naphthalene 45.8
6.74 2.56 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼n-Butylbenzene 29.7
6.74 5.80 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼n-Heptane 67.4
6.74 2.97 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼N-Propylbenzene 94.0
6.74 2.70 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼sec-Butylbenzene ND
6.74 2.56 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Styrene ND
6.74 3.37 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼tert-Butylbenzene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Tetrachloroethene ND
6.74 3.10 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,2-Dichloroethene ND
6.74 3.51 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,3-Dichloropropene ND
13.5 3.24 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼trans-1,4-Dichloro-2-butene ND
6.74 2.43 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Trichloroethene ND
6.74 4.18 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Trichlorofluoromethane ND
13.5 7.42 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Vinyl acetate ND
6.74 3.77 mg/Kg 07/26/22 10:32 07/27/22 16:52 1000☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)98 65-130 07/26/22 10:32 07/27/22 16:52 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 16:52 100065-130
Dibromofluoromethane (Surr)99 07/26/22 10:32 07/27/22 16:52 100065-130
Toluene-d8 (Surr)99 07/26/22 10:32 07/27/22 16:52 100065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 371 33.7 16.9 mg/Kg ☼07/26/22 10:32 07/28/22 21:33 5000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
33.7 14.2 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Ethylbenzene 253
33.7 14.8 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼m-Xylene & p-Xylene 951
33.7 15.5 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼o-Xylene 411
33.7 17.5 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Toluene 764
67.4 24.3 mg/Kg 07/26/22 10:32 07/28/22 21:33 5000☼Xylenes, Total 1360
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/28/22 21:33 5000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 07/26/22 10:32 07/28/22 21:33 500065-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/28/22 21:33 500065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/28/22 21:33 500065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
19000 2730 683 mg/Kg ☼07/26/22 10:32 08/01/22 16:14 20000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 80 70-131 07/26/22 10:32 08/01/22 16:14 20000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-4Client Sample ID: MW-3-10
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00720 0.00187 mg/Kg ☼07/26/22 10:32 07/26/22 15:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,1-Trichloroethane ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2,2-Tetrachloroethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00720 0.00216 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1,2-Trichloroethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloroethane ND
0.00720 0.00519 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloroethene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,1-Dichloropropene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,3-Trichlorobenzene ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,3-Trichloropropane ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,4-Trichlorobenzene ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2,4-Trimethylbenzene 0.0333
0.0144 0.00230 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dibromo-3-Chloropropane ND
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichlorobenzene ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichloroethane ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,2-Dichloropropane ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3,5-Trimethylbenzene 0.0110
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3-Dichlorobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,3-Dichloropropane ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼1,4-Dichlorobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2,2-Dichloropropane ND
0.0360 0.0133 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Butanone (MEK)ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Chlorotoluene ND
0.0360 0.0274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼2-Hexanone ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Chlorotoluene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Isopropyltoluene ND
0.0360 0.0259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼4-Methyl-2-pentanone (MIBK)ND
0.0720 0.0158 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Acetone 0.102
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Benzene 0.0527
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromobenzene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromoform ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Bromomethane ND *+
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Carbon disulfide ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Carbon tetrachloride ND
0.00720 0.00202 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorobenzene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorobromomethane ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chlorodibromomethane ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloroethane ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloroform ND
0.00720 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Chloromethane ND
0.00720 0.00418 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼cis-1,2-Dichloroethene ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼cis-1,3-Dichloropropene ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Dibromomethane ND
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Dichlorobromomethane ND
0.0144 0.0144 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethyl acetate ND
0.00720 0.00303 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethylbenzene 0.115
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Ethylene Dibromide ND
0.00720 0.00591 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Hexachlorobutadiene ND
0.00720 0.00245 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Hexane 0.00631 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-4Client Sample ID: MW-3-10
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00247 J 0.00720 0.00245 mg/Kg ☼07/26/22 10:32 07/26/22 15:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0144 0.00216 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Isopropyl ether ND
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Isopropylbenzene 0.00578 J
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Methyl tert-butyl ether ND *+
0.0144 0.0115 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Methylene Chloride ND
0.00720 0.00447 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Naphthalene ND
0.00720 0.00274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼n-Butylbenzene ND
0.00720 0.00619 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼n-Heptane 0.00849
0.00720 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼N-Propylbenzene 0.0128
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼o-Xylene 0.161
0.00720 0.00288 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼sec-Butylbenzene ND
0.00720 0.00274 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Styrene ND
0.00720 0.00360 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼tert-Butylbenzene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Tetrachloroethene ND
0.00720 0.00331 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,2-Dichloroethene ND
0.00720 0.00375 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,3-Dichloropropene ND
0.0144 0.00346 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼trans-1,4-Dichloro-2-butene ND
0.00720 0.00259 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Trichloroethene ND
0.00720 0.00447 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Trichlorofluoromethane ND
0.0144 0.00792 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Vinyl acetate ND
0.00720 0.00403 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Vinyl chloride ND
0.0144 0.00519 mg/Kg 07/26/22 10:32 07/26/22 15:23 1☼Xylenes, Total 0.548 E
1,2-Dichloroethane-d4 (Surr)105 65-130 07/26/22 10:32 07/26/22 15:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/26/22 15:23 165-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 07/26/22 15:23 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/26/22 15:23 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
m-Xylene & p-Xylene 0.715 0.281 0.124 mg/Kg ☼07/26/22 10:32 07/27/22 18:53 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.281 0.146 mg/Kg 07/26/22 10:32 07/27/22 18:53 40☼Toluene 1.06
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/27/22 18:53 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 18:53 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 18:53 4065-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/27/22 18:53 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
9.57 J 14.1 3.53 mg/Kg ☼07/26/22 10:32 08/01/22 14:25 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 08/01/22 14:25 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-5Client Sample ID: MW-3-20
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00990 0.00257 mg/Kg ☼07/26/22 10:32 07/26/22 15:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,1-Trichloroethane ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2,2-Tetrachloroethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00990 0.00297 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1,2-Trichloroethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloroethane ND
0.00990 0.00713 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloroethene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,1-Dichloropropene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,3-Trichlorobenzene ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,3-Trichloropropane ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,4-Trichlorobenzene ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2,4-Trimethylbenzene 0.0328
0.0198 0.00317 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dibromo-3-Chloropropane ND
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichlorobenzene ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichloroethane ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,2-Dichloropropane ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3,5-Trimethylbenzene 0.00967 J
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3-Dichlorobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,3-Dichloropropane ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼1,4-Dichlorobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2,2-Dichloropropane ND
0.0495 0.0182 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Butanone (MEK)ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Chlorotoluene ND
0.0495 0.0376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼2-Hexanone ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Chlorotoluene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Isopropyltoluene ND
0.0495 0.0356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼4-Methyl-2-pentanone (MIBK)ND
0.0990 0.0218 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Acetone 0.0351 J
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Benzene 0.0331
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromobenzene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromoform ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Bromomethane ND *+
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Carbon disulfide ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Carbon tetrachloride ND
0.00990 0.00277 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorobenzene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorobromomethane ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chlorodibromomethane ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloroethane ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloroform ND
0.00990 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Chloromethane ND
0.00990 0.00574 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼cis-1,2-Dichloroethene ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼cis-1,3-Dichloropropene ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Dibromomethane ND
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Dichlorobromomethane ND
0.0198 0.0198 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethyl acetate ND
0.00990 0.00416 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethylbenzene 0.0845
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Ethylene Dibromide ND
0.00990 0.00812 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Hexachlorobutadiene ND
0.00990 0.00337 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Hexane 0.00407 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-5Client Sample ID: MW-3-20
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00990 0.00337 mg/Kg ☼07/26/22 10:32 07/26/22 15:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0198 0.00297 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Isopropyl ether ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Isopropylbenzene 0.00513 J
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Methyl tert-butyl ether ND *+
0.0198 0.0158 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Methylene Chloride ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼m-Xylene & p-Xylene 0.286
0.00990 0.00614 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Naphthalene ND
0.00990 0.00376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼n-Butylbenzene ND
0.00990 0.00851 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼n-Heptane ND
0.00990 0.00436 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼N-Propylbenzene 0.0106
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼o-Xylene 0.136
0.00990 0.00396 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼sec-Butylbenzene ND
0.00990 0.00376 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Styrene ND
0.00990 0.00495 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼tert-Butylbenzene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Tetrachloroethene ND
0.00990 0.00455 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,2-Dichloroethene ND
0.00990 0.00515 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,3-Dichloropropene ND
0.0198 0.00475 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼trans-1,4-Dichloro-2-butene ND
0.00990 0.00356 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Trichloroethene ND
0.00990 0.00614 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Trichlorofluoromethane ND
0.0198 0.0109 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Vinyl acetate ND
0.00990 0.00554 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Vinyl chloride ND
0.0198 0.00713 mg/Kg 07/26/22 10:32 07/26/22 15:47 1☼Xylenes, Total 0.422
1,2-Dichloroethane-d4 (Surr)108 65-130 07/26/22 10:32 07/26/22 15:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)111 07/26/22 10:32 07/26/22 15:47 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 15:47 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 15:47 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Toluene 1.68 0.394 0.205 mg/Kg ☼07/26/22 10:32 07/27/22 19:17 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)100 65-130 07/26/22 10:32 07/27/22 19:17 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 19:17 4065-130
Dibromofluoromethane (Surr)97 07/26/22 10:32 07/27/22 19:17 4065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 19:17 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
12.1 J 21.2 5.30 mg/Kg ☼07/26/22 10:32 07/29/22 17:57 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 77 70-131 07/26/22 10:32 07/29/22 17:57 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-6Client Sample ID: MW-3-25
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00609 0.00158 mg/Kg ☼07/26/22 10:32 07/26/22 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,1-Trichloroethane ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2,2-Tetrachloroethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00609 0.00183 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1,2-Trichloroethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloroethane ND
0.00609 0.00438 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloroethene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,1-Dichloropropene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,3-Trichlorobenzene ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,3-Trichloropropane ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,4-Trichlorobenzene ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2,4-Trimethylbenzene ND
0.0122 0.00195 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dibromo-3-Chloropropane ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichlorobenzene ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichloroethane ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,2-Dichloropropane ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3,5-Trimethylbenzene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3-Dichlorobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,3-Dichloropropane ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼1,4-Dichlorobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2,2-Dichloropropane ND
0.0304 0.0112 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Butanone (MEK)ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Chlorotoluene ND
0.0304 0.0231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼2-Hexanone ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Chlorotoluene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Isopropyltoluene ND
0.0304 0.0219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼4-Methyl-2-pentanone (MIBK)ND
0.0609 0.0134 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Acetone 0.0230 J
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Benzene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromobenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromoform ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Bromomethane ND *+
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Carbon disulfide ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Carbon tetrachloride ND
0.00609 0.00170 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorobenzene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorobromomethane ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chlorodibromomethane ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloroethane ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloroform ND
0.00609 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Chloromethane ND
0.00609 0.00353 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼cis-1,2-Dichloroethene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼cis-1,3-Dichloropropene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Dibromomethane ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Dichlorobromomethane ND
0.0122 0.0122 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethyl acetate ND
0.00609 0.00256 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethylbenzene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Ethylene Dibromide ND
0.00609 0.00499 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Hexachlorobutadiene ND
0.00609 0.00207 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-6Client Sample ID: MW-3-25
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00609 0.00207 mg/Kg ☼07/26/22 10:32 07/26/22 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0122 0.00183 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Isopropyl ether ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Isopropylbenzene ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Methyl tert-butyl ether ND *+
0.0122 0.00974 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Methylene Chloride ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼m-Xylene & p-Xylene 0.00361 J
0.00609 0.00377 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Naphthalene ND
0.00609 0.00231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼n-Butylbenzene ND
0.00609 0.00524 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼n-Heptane ND
0.00609 0.00268 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼N-Propylbenzene ND
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼o-Xylene ND
0.00609 0.00244 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼sec-Butylbenzene ND
0.00609 0.00231 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Styrene ND
0.00609 0.00304 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼tert-Butylbenzene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Tetrachloroethene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Toluene 0.00383 J
0.00609 0.00280 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,2-Dichloroethene ND
0.00609 0.00317 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,3-Dichloropropene ND
0.0122 0.00292 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼trans-1,4-Dichloro-2-butene ND
0.00609 0.00219 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Trichloroethene ND
0.00609 0.00377 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Trichlorofluoromethane ND
0.0122 0.00670 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Vinyl acetate ND
0.00609 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Vinyl chloride ND
0.0122 0.00438 mg/Kg 07/26/22 10:32 07/26/22 16:11 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 07/26/22 16:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 16:11 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 16:11 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 16:11 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 12.7 3.19 mg/Kg ☼07/26/22 10:32 07/29/22 18:19 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 81 70-131 07/26/22 10:32 07/29/22 18:19 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-7Client Sample ID: MW-3-30
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00682 0.00177 mg/Kg ☼07/26/22 10:32 07/26/22 16:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,1-Trichloroethane ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2,2-Tetrachloroethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00682 0.00205 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1,2-Trichloroethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloroethane ND
0.00682 0.00491 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloroethene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,1-Dichloropropene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,3-Trichlorobenzene ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,3-Trichloropropane ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,4-Trichlorobenzene ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2,4-Trimethylbenzene ND
0.0136 0.00218 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dibromo-3-Chloropropane ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichlorobenzene ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichloroethane ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,2-Dichloropropane ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3,5-Trimethylbenzene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3-Dichlorobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,3-Dichloropropane ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼1,4-Dichlorobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2,2-Dichloropropane ND
0.0341 0.0125 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Butanone (MEK)ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Chlorotoluene ND
0.0341 0.0259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼2-Hexanone ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Chlorotoluene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Isopropyltoluene ND
0.0341 0.0245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼4-Methyl-2-pentanone (MIBK)ND
0.0682 0.0150 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Acetone 0.0153 J
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Benzene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromobenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromoform ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Bromomethane ND *+
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Carbon disulfide ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Carbon tetrachloride ND
0.00682 0.00191 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorobenzene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorobromomethane ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chlorodibromomethane ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloroethane ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloroform ND
0.00682 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Chloromethane ND
0.00682 0.00395 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼cis-1,2-Dichloroethene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼cis-1,3-Dichloropropene ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Dibromomethane ND
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Dichlorobromomethane ND
0.0136 0.0136 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethyl acetate ND
0.00682 0.00286 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethylbenzene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Ethylene Dibromide ND
0.00682 0.00559 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Hexachlorobutadiene ND
0.00682 0.00232 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-7Client Sample ID: MW-3-30
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00682 0.00232 mg/Kg ☼07/26/22 10:32 07/26/22 16:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0136 0.00205 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Isopropyl ether ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Isopropylbenzene ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Methyl tert-butyl ether ND *+
0.0136 0.0109 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Methylene Chloride ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼m-Xylene & p-Xylene 0.00657 J
0.00682 0.00423 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Naphthalene ND
0.00682 0.00259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼n-Butylbenzene ND
0.00682 0.00586 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼n-Heptane ND
0.00682 0.00300 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼N-Propylbenzene ND
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼o-Xylene 0.00409 J
0.00682 0.00273 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼sec-Butylbenzene ND
0.00682 0.00259 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Styrene ND
0.00682 0.00341 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼tert-Butylbenzene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Tetrachloroethene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Toluene 0.00707
0.00682 0.00314 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,2-Dichloroethene ND
0.00682 0.00355 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,3-Dichloropropene ND
0.0136 0.00327 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼trans-1,4-Dichloro-2-butene ND
0.00682 0.00245 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Trichloroethene ND
0.00682 0.00423 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Trichlorofluoromethane ND
0.0136 0.00750 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Vinyl acetate ND
0.00682 0.00382 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Vinyl chloride ND
0.0136 0.00491 mg/Kg 07/26/22 10:32 07/26/22 16:35 1☼Xylenes, Total 0.0107 J
1,2-Dichloroethane-d4 (Surr)107 65-130 07/26/22 10:32 07/26/22 16:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 16:35 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/26/22 16:35 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 16:35 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
11.4 J 15.1 3.78 mg/Kg ☼07/26/22 10:32 07/28/22 17:46 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/28/22 17:46 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-8Client Sample ID: MW-2-10
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00802 0.00208 mg/Kg ☼07/26/22 10:32 07/26/22 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,1-Trichloroethane ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2,2-Tetrachloroethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00802 0.00241 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1,2-Trichloroethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloroethane ND
0.00802 0.00577 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloroethene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,1-Dichloropropene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,3-Trichlorobenzene ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,3-Trichloropropane ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,4-Trichlorobenzene ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2,4-Trimethylbenzene ND
0.0160 0.00257 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dibromo-3-Chloropropane ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichlorobenzene ND
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichloroethane ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,2-Dichloropropane ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3,5-Trimethylbenzene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3-Dichlorobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,3-Dichloropropane ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼1,4-Dichlorobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2,2-Dichloropropane ND
0.0401 0.0148 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Butanone (MEK)0.0519
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Chlorotoluene ND
0.0401 0.0305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼2-Hexanone ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Chlorotoluene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Isopropyltoluene ND
0.0401 0.0289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼4-Methyl-2-pentanone (MIBK)ND
0.0802 0.0176 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Acetone 0.188
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Benzene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromobenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromoform ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Bromomethane ND *+
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Carbon disulfide ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Carbon tetrachloride ND
0.00802 0.00224 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorobenzene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorobromomethane ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chlorodibromomethane ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloroethane ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloroform ND
0.00802 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Chloromethane ND
0.00802 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼cis-1,2-Dichloroethene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼cis-1,3-Dichloropropene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Dibromomethane ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Dichlorobromomethane ND
0.0160 0.0160 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethyl acetate ND
0.00802 0.00337 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethylbenzene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Ethylene Dibromide ND
0.00802 0.00657 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Hexachlorobutadiene ND
0.00802 0.00273 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-8Client Sample ID: MW-2-10
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00320 J 0.00802 0.00273 mg/Kg ☼07/26/22 10:32 07/26/22 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0160 0.00241 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Isopropyl ether ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Isopropylbenzene ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Methyl tert-butyl ether ND *+
0.0160 0.0128 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Methylene Chloride ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼m-Xylene & p-Xylene ND
0.00802 0.00497 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Naphthalene ND
0.00802 0.00305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼n-Butylbenzene ND
0.00802 0.00690 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼n-Heptane ND
0.00802 0.00353 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼N-Propylbenzene ND
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼o-Xylene ND
0.00802 0.00321 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼sec-Butylbenzene ND
0.00802 0.00305 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Styrene ND
0.00802 0.00401 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼tert-Butylbenzene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Tetrachloroethene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Toluene 0.00433 J
0.00802 0.00369 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,2-Dichloroethene ND
0.00802 0.00417 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,3-Dichloropropene ND
0.0160 0.00385 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼trans-1,4-Dichloro-2-butene ND
0.00802 0.00289 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Trichloroethene ND
0.00802 0.00497 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Trichlorofluoromethane ND
0.0160 0.00882 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Vinyl acetate ND
0.00802 0.00449 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Vinyl chloride ND
0.0160 0.00577 mg/Kg 07/26/22 10:32 07/26/22 17:00 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)104 65-130 07/26/22 10:32 07/26/22 17:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/26/22 17:00 165-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/26/22 17:00 165-130
Toluene-d8 (Surr)106 07/26/22 10:32 07/26/22 17:00 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.7 3.93 mg/Kg ☼07/26/22 10:32 07/28/22 18:08 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/28/22 18:08 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-9Client Sample ID: MW-2-20
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00894 0.00233 mg/Kg ☼07/26/22 10:32 07/26/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,1-Trichloroethane ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2,2-Tetrachloroethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00894 0.00268 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1,2-Trichloroethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloroethane ND
0.00894 0.00644 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloroethene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,1-Dichloropropene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,3-Trichlorobenzene ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,3-Trichloropropane ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,4-Trichlorobenzene ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2,4-Trimethylbenzene ND
0.0179 0.00286 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dibromo-3-Chloropropane ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichlorobenzene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichloroethane ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,2-Dichloropropane ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3,5-Trimethylbenzene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3-Dichlorobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,3-Dichloropropane ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼1,4-Dichlorobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2,2-Dichloropropane ND
0.0447 0.0165 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Butanone (MEK)1.26
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Chlorotoluene ND
0.0447 0.0340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼2-Hexanone 0.187
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Chlorotoluene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Isopropyltoluene ND
0.0447 0.0322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼4-Methyl-2-pentanone (MIBK)0.0639
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Benzene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromobenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromoform ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Bromomethane ND *+
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Carbon disulfide ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Carbon tetrachloride ND
0.00894 0.00250 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorobenzene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorobromomethane ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chlorodibromomethane ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloroethane ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloroform ND
0.00894 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Chloromethane ND
0.00894 0.00519 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼cis-1,2-Dichloroethene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼cis-1,3-Dichloropropene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Dibromomethane ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Dichlorobromomethane ND
0.0179 0.0179 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethyl acetate ND
0.00894 0.00376 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethylbenzene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Ethylene Dibromide ND
0.00894 0.00733 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Hexachlorobutadiene ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Hexane ND
0.00894 0.00304 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Iodomethane 0.00444 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-9Client Sample ID: MW-2-20
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropyl ether ND 0.0179 0.00268 mg/Kg ☼07/26/22 10:32 07/26/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Isopropylbenzene ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Methyl tert-butyl ether ND *+
0.0179 0.0143 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Methylene Chloride ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼m-Xylene & p-Xylene ND
0.00894 0.00554 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Naphthalene ND
0.00894 0.00340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼n-Butylbenzene ND
0.00894 0.00769 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼n-Heptane ND
0.00894 0.00393 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼N-Propylbenzene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼o-Xylene ND
0.00894 0.00358 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼sec-Butylbenzene ND
0.00894 0.00340 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Styrene ND
0.00894 0.00447 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼tert-Butylbenzene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Tetrachloroethene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Toluene ND
0.00894 0.00411 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,2-Dichloroethene ND
0.00894 0.00465 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,3-Dichloropropene ND
0.0179 0.00429 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼trans-1,4-Dichloro-2-butene ND
0.00894 0.00322 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Trichloroethene ND
0.00894 0.00554 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Trichlorofluoromethane ND
0.0179 0.00984 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Vinyl acetate ND
0.00894 0.00501 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Vinyl chloride ND
0.0179 0.00644 mg/Kg 07/26/22 10:32 07/26/22 17:24 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)104 65-130 07/26/22 10:32 07/26/22 17:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 07/26/22 10:32 07/26/22 17:24 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/26/22 17:24 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 17:24 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Acetone ND 3.28 0.721 mg/Kg ☼07/26/22 10:32 08/01/22 17:55 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)109 65-130 07/26/22 10:32 08/01/22 17:55 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 07/26/22 10:32 08/01/22 17:55 4065-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 08/01/22 17:55 4065-130
Toluene-d8 (Surr)93 07/26/22 10:32 08/01/22 17:55 4065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
6.96 J 13.6 3.40 mg/Kg ☼07/26/22 10:32 07/28/22 18:30 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 84 70-131 07/26/22 10:32 07/28/22 18:30 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-10Client Sample ID: MW-2-25
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00772 0.00201 mg/Kg ☼07/26/22 10:32 07/27/22 13:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,1-Trichloroethane ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2,2-Tetrachloroethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00772 0.00232 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1,2-Trichloroethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloroethane ND
0.00772 0.00556 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloroethene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,1-Dichloropropene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,3-Trichlorobenzene ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,3-Trichloropropane ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,4-Trichlorobenzene ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2,4-Trimethylbenzene 0.00989
0.0154 0.00247 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dibromo-3-Chloropropane ND
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichlorobenzene ND
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichloroethane ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,2-Dichloropropane ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3,5-Trimethylbenzene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3-Dichlorobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,3-Dichloropropane ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼1,4-Dichlorobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2,2-Dichloropropane ND
0.0386 0.0142 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Butanone (MEK)0.396
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Chlorotoluene ND
0.0386 0.0294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼2-Hexanone 0.0325 J
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Chlorotoluene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Isopropyltoluene ND
0.0386 0.0278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼4-Methyl-2-pentanone (MIBK)ND
0.0772 0.0170 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Acetone 0.494
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Benzene 0.00775
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromobenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromoform ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Bromomethane ND *+
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Carbon disulfide ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Carbon tetrachloride ND
0.00772 0.00216 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorobenzene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorobromomethane ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chlorodibromomethane ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloroethane ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloroform ND
0.00772 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Chloromethane ND
0.00772 0.00448 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼cis-1,2-Dichloroethene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼cis-1,3-Dichloropropene ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Dibromomethane ND
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Dichlorobromomethane ND
0.0154 0.0154 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethyl acetate ND
0.00772 0.00324 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethylbenzene 0.00843
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Ethylene Dibromide ND
0.00772 0.00633 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Hexachlorobutadiene ND
0.00772 0.00263 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Hexane 0.00296 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-10Client Sample ID: MW-2-25
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00772 0.00263 mg/Kg ☼07/26/22 10:32 07/27/22 13:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0154 0.00232 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Isopropyl ether ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Isopropylbenzene ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Methyl tert-butyl ether ND *+
0.0154 0.0124 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Methylene Chloride ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼m-Xylene & p-Xylene 0.0355
0.00772 0.00479 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Naphthalene ND
0.00772 0.00294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼n-Butylbenzene ND
0.00772 0.00664 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼n-Heptane ND
0.00772 0.00340 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼N-Propylbenzene 0.00398 J
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼o-Xylene 0.0178
0.00772 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼sec-Butylbenzene ND
0.00772 0.00294 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Styrene ND
0.00772 0.00386 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼tert-Butylbenzene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Tetrachloroethene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Toluene 0.0273
0.00772 0.00355 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,2-Dichloroethene ND
0.00772 0.00402 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,3-Dichloropropene ND
0.0154 0.00371 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼trans-1,4-Dichloro-2-butene ND
0.00772 0.00278 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Trichloroethene ND
0.00772 0.00479 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Trichlorofluoromethane ND
0.0154 0.00850 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Vinyl acetate ND
0.00772 0.00433 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Vinyl chloride ND
0.0154 0.00556 mg/Kg 07/26/22 10:32 07/27/22 13:16 1☼Xylenes, Total 0.0533
1,2-Dichloroethane-d4 (Surr)106 65-130 07/26/22 10:32 07/27/22 13:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 13:16 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 13:16 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 13:16 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.9 3.97 mg/Kg ☼07/26/22 10:32 07/28/22 18:51 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 18:51 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-11Client Sample ID: MW-2-30
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00710 0.00185 mg/Kg ☼07/26/22 10:32 07/26/22 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,1-Trichloroethane ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2,2-Tetrachloroethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00710 0.00213 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1,2-Trichloroethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloroethane ND
0.00710 0.00511 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloroethene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,1-Dichloropropene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,3-Trichlorobenzene ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,3-Trichloropropane ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,4-Trichlorobenzene ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2,4-Trimethylbenzene 0.0536
0.0142 0.00227 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dibromo-3-Chloropropane ND
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichlorobenzene ND
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichloroethane ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,2-Dichloropropane ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3,5-Trimethylbenzene 0.0245
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3-Dichlorobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,3-Dichloropropane ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼1,4-Dichlorobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2,2-Dichloropropane ND
0.0355 0.0131 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Butanone (MEK)0.0978
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Chlorotoluene ND
0.0355 0.0270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼2-Hexanone 0.0274 J
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Chlorotoluene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Isopropyltoluene 0.0111
0.0355 0.0256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼4-Methyl-2-pentanone (MIBK)ND
0.0710 0.0156 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Acetone 0.306
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Benzene 0.0102
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromobenzene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromoform ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Bromomethane ND *+
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Carbon disulfide ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Carbon tetrachloride ND
0.00710 0.00199 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorobenzene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorobromomethane ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chlorodibromomethane ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloroethane ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloroform ND
0.00710 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Chloromethane ND
0.00710 0.00412 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼cis-1,2-Dichloroethene ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼cis-1,3-Dichloropropene ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Dibromomethane ND
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Dichlorobromomethane ND
0.0142 0.0142 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethyl acetate ND
0.00710 0.00298 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethylbenzene 0.0227
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Ethylene Dibromide ND
0.00710 0.00582 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Hexachlorobutadiene ND
0.00710 0.00241 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Hexane 0.00793
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-11Client Sample ID: MW-2-30
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00710 0.00241 mg/Kg ☼07/26/22 10:32 07/26/22 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0142 0.00213 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Isopropyl ether ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Isopropylbenzene 0.00610 J
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Methyl tert-butyl ether ND *+
0.0142 0.0114 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Methylene Chloride ND
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼m-Xylene & p-Xylene 0.0830
0.00710 0.00440 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Naphthalene 0.0243
0.00710 0.00270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼n-Butylbenzene 0.0160
0.00710 0.00611 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼n-Heptane 0.0175
0.00710 0.00313 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼N-Propylbenzene 0.0152
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼o-Xylene 0.0603
0.00710 0.00284 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼sec-Butylbenzene 0.00406 J
0.00710 0.00270 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Styrene ND
0.00710 0.00355 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼tert-Butylbenzene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Tetrachloroethene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Toluene 0.0528
0.00710 0.00327 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,2-Dichloroethene ND
0.00710 0.00369 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,3-Dichloropropene ND
0.0142 0.00341 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼trans-1,4-Dichloro-2-butene ND
0.00710 0.00256 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Trichloroethene ND
0.00710 0.00440 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Trichlorofluoromethane ND
0.0142 0.00781 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Vinyl acetate ND
0.00710 0.00398 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Vinyl chloride ND
0.0142 0.00511 mg/Kg 07/26/22 10:32 07/26/22 18:12 1☼Xylenes, Total 0.143
1,2-Dichloroethane-d4 (Surr)103 65-130 07/26/22 10:32 07/26/22 18:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 07/26/22 10:32 07/26/22 18:12 165-130
Dibromofluoromethane (Surr)103 07/26/22 10:32 07/26/22 18:12 165-130
Toluene-d8 (Surr)103 07/26/22 10:32 07/26/22 18:12 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
6.82 J 14.1 3.51 mg/Kg ☼07/26/22 10:32 07/28/22 19:13 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:13 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-12Client Sample ID: P-1-10
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00812 0.00211 mg/Kg ☼07/26/22 10:32 07/27/22 13:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,1-Trichloroethane ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2,2-Tetrachloroethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00812 0.00244 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1,2-Trichloroethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloroethane ND
0.00812 0.00585 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloroethene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,1-Dichloropropene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,3-Trichlorobenzene ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,3-Trichloropropane ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,4-Trichlorobenzene ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2,4-Trimethylbenzene ND
0.0162 0.00260 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dibromo-3-Chloropropane ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichlorobenzene ND
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichloroethane ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,2-Dichloropropane ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3,5-Trimethylbenzene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3-Dichlorobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,3-Dichloropropane ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼1,4-Dichlorobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2,2-Dichloropropane ND
0.0406 0.0149 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Butanone (MEK)0.0336 J
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Chlorotoluene ND
0.0406 0.0309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼2-Hexanone ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Chlorotoluene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Isopropyltoluene ND
0.0406 0.0292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼4-Methyl-2-pentanone (MIBK)ND
0.0812 0.0179 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Acetone 0.299
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Benzene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromobenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromoform ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Bromomethane ND *+
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Carbon disulfide ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Carbon tetrachloride ND
0.00812 0.00227 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorobenzene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorobromomethane ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chlorodibromomethane ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloroethane ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloroform ND
0.00812 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Chloromethane ND
0.00812 0.00471 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼cis-1,2-Dichloroethene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼cis-1,3-Dichloropropene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Dibromomethane ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Dichlorobromomethane ND
0.0162 0.0162 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethyl acetate ND
0.00812 0.00341 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethylbenzene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Ethylene Dibromide ND
0.00812 0.00666 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Hexachlorobutadiene ND
0.00812 0.00276 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-12Client Sample ID: P-1-10
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00812 0.00276 mg/Kg ☼07/26/22 10:32 07/27/22 13:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0162 0.00244 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Isopropyl ether ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Isopropylbenzene ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Methyl tert-butyl ether ND *+
0.0162 0.0130 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Methylene Chloride ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼m-Xylene & p-Xylene 0.00686 J
0.00812 0.00503 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Naphthalene ND
0.00812 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼n-Butylbenzene ND
0.00812 0.00698 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼n-Heptane ND
0.00812 0.00357 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼N-Propylbenzene ND
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼o-Xylene ND
0.00812 0.00325 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼sec-Butylbenzene ND
0.00812 0.00309 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Styrene ND
0.00812 0.00406 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼tert-Butylbenzene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Tetrachloroethene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Toluene 0.00449 J
0.00812 0.00373 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,2-Dichloroethene ND
0.00812 0.00422 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,3-Dichloropropene ND
0.0162 0.00390 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼trans-1,4-Dichloro-2-butene ND
0.00812 0.00292 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Trichloroethene ND
0.00812 0.00503 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Trichlorofluoromethane ND
0.0162 0.00893 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Vinyl acetate ND
0.00812 0.00455 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Vinyl chloride ND
0.0162 0.00585 mg/Kg 07/26/22 10:32 07/27/22 13:40 1☼Xylenes, Total 0.00686 J
1,2-Dichloroethane-d4 (Surr)107 65-130 07/26/22 10:32 07/27/22 13:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/26/22 10:32 07/27/22 13:40 165-130
Dibromofluoromethane (Surr)101 07/26/22 10:32 07/27/22 13:40 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 13:40 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 15.4 3.84 mg/Kg ☼07/26/22 10:32 07/28/22 19:35 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:35 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-13Client Sample ID: P-1-20
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00816 0.00212 mg/Kg ☼07/26/22 10:32 07/26/22 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,1-Trichloroethane ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2,2-Tetrachloroethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00816 0.00245 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1,2-Trichloroethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloroethane ND
0.00816 0.00587 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloroethene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,1-Dichloropropene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,3-Trichlorobenzene ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,3-Trichloropropane ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,4-Trichlorobenzene ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2,4-Trimethylbenzene 0.00662 J
0.0163 0.00261 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dibromo-3-Chloropropane ND
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichlorobenzene ND
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichloroethane ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,2-Dichloropropane ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3,5-Trimethylbenzene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3-Dichlorobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,3-Dichloropropane ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼1,4-Dichlorobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2,2-Dichloropropane ND
0.0408 0.0150 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Butanone (MEK)0.109
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Chlorotoluene ND
0.0408 0.0310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼2-Hexanone ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Chlorotoluene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Isopropyltoluene ND
0.0408 0.0294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼4-Methyl-2-pentanone (MIBK)ND
0.0816 0.0179 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Acetone 0.589
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Benzene 0.0122
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromobenzene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromoform ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Bromomethane ND *+
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Carbon disulfide ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Carbon tetrachloride ND
0.00816 0.00228 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorobenzene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorobromomethane ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chlorodibromomethane ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloroethane ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloroform ND
0.00816 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Chloromethane ND
0.00816 0.00473 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼cis-1,2-Dichloroethene ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼cis-1,3-Dichloropropene ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Dibromomethane ND
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Dichlorobromomethane ND
0.0163 0.0163 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethyl acetate ND
0.00816 0.00343 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethylbenzene 0.00594 J
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Ethylene Dibromide ND
0.00816 0.00669 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Hexachlorobutadiene ND
0.00816 0.00277 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Hexane ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-13Client Sample ID: P-1-20
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane 0.00826 0.00816 0.00277 mg/Kg ☼07/26/22 10:32 07/26/22 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0163 0.00245 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Isopropyl ether ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Isopropylbenzene ND
0.00806 0.00355 mg/Kg 07/26/22 10:32 08/01/22 16:26 1☼Methyl tert-butyl ether 0.0227
0.0163 0.0130 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Methylene Chloride ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼m-Xylene & p-Xylene 0.0226
0.00816 0.00506 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Naphthalene ND
0.00816 0.00310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼n-Butylbenzene ND
0.00816 0.00701 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼n-Heptane ND
0.00816 0.00359 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼N-Propylbenzene ND
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼o-Xylene 0.0183
0.00816 0.00326 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼sec-Butylbenzene ND
0.00816 0.00310 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Styrene ND
0.00816 0.00408 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼tert-Butylbenzene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Tetrachloroethene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Toluene 0.0334
0.00816 0.00375 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,2-Dichloroethene ND
0.00816 0.00424 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,3-Dichloropropene ND
0.0163 0.00391 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼trans-1,4-Dichloro-2-butene ND
0.00816 0.00294 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Trichloroethene ND
0.00816 0.00506 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Trichlorofluoromethane ND
0.0163 0.00897 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Vinyl acetate ND
0.00816 0.00457 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Vinyl chloride ND
0.0163 0.00587 mg/Kg 07/26/22 10:32 07/26/22 19:00 1☼Xylenes, Total 0.0409
1,2-Dichloroethane-d4 (Surr)102 65-130 07/26/22 10:32 07/26/22 19:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)112 07/26/22 10:32 08/01/22 16:26 165-130
4-Bromofluorobenzene (Surr)106 07/26/22 10:32 07/26/22 19:00 165-130
4-Bromofluorobenzene (Surr)98 07/26/22 10:32 08/01/22 16:26 165-130
Dibromofluoromethane (Surr)99 07/26/22 10:32 07/26/22 19:00 165-130
Dibromofluoromethane (Surr)103 07/26/22 10:32 08/01/22 16:26 165-130
Toluene-d8 (Surr)105 07/26/22 10:32 07/26/22 19:00 165-130
Toluene-d8 (Surr)100 07/26/22 10:32 08/01/22 16:26 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 - C10]ND 16.5 4.13 mg/Kg ☼07/26/22 10:32 07/28/22 19:57 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/26/22 10:32 07/28/22 19:57 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-14Client Sample ID: P-1-25
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00804 0.00209 mg/Kg ☼07/26/22 10:32 07/26/22 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,1-Trichloroethane ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2,2-Tetrachloroethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00804 0.00241 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1,2-Trichloroethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloroethane ND
0.00804 0.00579 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloroethene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,1-Dichloropropene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,3-Trichlorobenzene ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,3-Trichloropropane ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,4-Trichlorobenzene ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2,4-Trimethylbenzene 0.0267
0.0161 0.00257 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dibromo-3-Chloropropane ND
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichlorobenzene ND
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichloroethane ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,2-Dichloropropane ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3,5-Trimethylbenzene 0.00848
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3-Dichlorobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,3-Dichloropropane ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼1,4-Dichlorobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2,2-Dichloropropane ND
0.0402 0.0148 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Butanone (MEK)0.189
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Chlorotoluene ND
0.0402 0.0306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼2-Hexanone ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Chlorotoluene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Isopropyltoluene ND
0.0402 0.0289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼4-Methyl-2-pentanone (MIBK)ND
0.0804 0.0177 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Acetone 0.757
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Benzene 0.0536
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromobenzene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromoform ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Bromomethane ND *+
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Carbon disulfide ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Carbon tetrachloride ND
0.00804 0.00225 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorobenzene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorobromomethane ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chlorodibromomethane ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloroethane ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloroform ND
0.00804 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Chloromethane ND
0.00804 0.00466 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼cis-1,2-Dichloroethene ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼cis-1,3-Dichloropropene ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Dibromomethane ND
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Dichlorobromomethane ND
0.0161 0.0161 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethyl acetate ND
0.00804 0.00338 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethylbenzene 0.0381
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Ethylene Dibromide ND
0.00804 0.00659 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Hexachlorobutadiene ND
0.00804 0.00273 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Hexane 0.00366 J
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-14Client Sample ID: P-1-25
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Iodomethane ND 0.00804 0.00273 mg/Kg ☼07/26/22 10:32 07/26/22 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0161 0.00241 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Isopropyl ether 0.00342 J
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Isopropylbenzene 0.00402 J
0.00828 0.00364 mg/Kg 07/26/22 10:32 08/01/22 16:47 1☼Methyl tert-butyl ether 0.0517
0.0161 0.0129 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Methylene Chloride ND
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼m-Xylene & p-Xylene 0.131
0.00804 0.00499 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Naphthalene ND
0.00804 0.00306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼n-Butylbenzene ND
0.00804 0.00692 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼n-Heptane 0.00707 J
0.00804 0.00354 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼N-Propylbenzene 0.00583 J
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼o-Xylene 0.0883
0.00804 0.00322 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼sec-Butylbenzene ND
0.00804 0.00306 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Styrene ND
0.00804 0.00402 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼tert-Butylbenzene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Tetrachloroethene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Toluene 0.244
0.00804 0.00370 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,2-Dichloroethene ND
0.00804 0.00418 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,3-Dichloropropene ND
0.0161 0.00386 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼trans-1,4-Dichloro-2-butene ND
0.00804 0.00289 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Trichloroethene ND
0.00804 0.00499 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Trichlorofluoromethane ND
0.0161 0.00885 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Vinyl acetate ND
0.00804 0.00450 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Vinyl chloride ND
0.0161 0.00579 mg/Kg 07/26/22 10:32 07/26/22 19:25 1☼Xylenes, Total 0.219
1,2-Dichloroethane-d4 (Surr)103 65-130 07/26/22 10:32 07/26/22 19:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)113 07/26/22 10:32 08/01/22 16:47 165-130
4-Bromofluorobenzene (Surr)105 07/26/22 10:32 07/26/22 19:25 165-130
4-Bromofluorobenzene (Surr)95 07/26/22 10:32 08/01/22 16:47 165-130
Dibromofluoromethane (Surr)102 07/26/22 10:32 07/26/22 19:25 165-130
Dibromofluoromethane (Surr)104 07/26/22 10:32 08/01/22 16:47 165-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/26/22 19:25 165-130
Toluene-d8 (Surr)98 07/26/22 10:32 08/01/22 16:47 165-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
5.48 J 16.3 4.07 mg/Kg ☼07/26/22 10:32 07/28/22 20:18 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 77 70-131 07/26/22 10:32 07/28/22 20:18 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-15Client Sample ID: P-1-30
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.347 0.0902 mg/Kg ☼07/26/22 10:32 07/26/22 21:02 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,1-Trichloroethane ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2,2-Tetrachloroethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.347 0.104 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1,2-Trichloroethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloroethane ND
0.347 0.250 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloroethene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,1-Dichloropropene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,3-Trichlorobenzene ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,3-Trichloropropane ND
0.347 0.174 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2,4-Trichlorobenzene ND
0.694 0.111 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dibromo-3-Chloropropane ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichlorobenzene ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichloroethane ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,2-Dichloropropane ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3,5-Trimethylbenzene 8.02
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3-Dichlorobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,3-Dichloropropane ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼1,4-Dichlorobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2,2-Dichloropropane ND
1.74 0.639 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Butanone (MEK)ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Chlorotoluene ND
1.74 1.32 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼2-Hexanone ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Chlorotoluene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Isopropyltoluene 1.39
1.74 1.25 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼4-Methyl-2-pentanone (MIBK)ND
3.47 0.764 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Acetone ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Benzene 3.33
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromobenzene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromoform ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Bromomethane ND *+
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Carbon disulfide ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Carbon tetrachloride ND
0.347 0.0972 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorobenzene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorobromomethane ND
0.347 0.146 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chlorodibromomethane ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloroethane ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloroform ND
0.347 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Chloromethane ND
0.347 0.201 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼cis-1,2-Dichloroethene ND
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼cis-1,3-Dichloropropene ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Dibromomethane ND
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Dichlorobromomethane ND
0.694 0.694 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Ethyl acetate ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Ethylene Dibromide ND
0.347 0.285 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Hexachlorobutadiene ND
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Hexane 2.67
0.347 0.118 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Iodomethane ND
0.694 0.104 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Isopropyl ether ND
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-15Client Sample ID: P-1-30
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropylbenzene 1.77 0.347 0.153 mg/Kg ☼07/26/22 10:32 07/26/22 21:02 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Methyl tert-butyl ether ND
0.694 0.555 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Methylene Chloride ND
0.347 0.215 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Naphthalene 3.55
0.347 0.132 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼n-Butylbenzene 1.87
0.347 0.298 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼n-Heptane 4.48
0.347 0.153 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼N-Propylbenzene 5.54
0.347 0.139 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼sec-Butylbenzene 0.497
0.347 0.132 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Styrene ND
0.347 0.174 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼tert-Butylbenzene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Tetrachloroethene ND
0.347 0.160 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,2-Dichloroethene ND
0.347 0.180 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,3-Dichloropropene ND
0.694 0.167 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼trans-1,4-Dichloro-2-butene ND
0.347 0.125 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Trichloroethene ND
0.347 0.215 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Trichlorofluoromethane ND
0.694 0.382 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Vinyl acetate ND
0.347 0.194 mg/Kg 07/26/22 10:32 07/26/22 21:02 40☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)92 65-130 07/26/22 10:32 07/26/22 21:02 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 07/26/22 10:32 07/26/22 21:02 4065-130
Dibromofluoromethane (Surr)95 07/26/22 10:32 07/26/22 21:02 4065-130
Toluene-d8 (Surr)99 07/26/22 10:32 07/26/22 21:02 4065-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
1,2,4-Trimethylbenzene 32.4 4.34 2.17 mg/Kg ☼07/26/22 10:32 07/27/22 17:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.34 1.82 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Ethylbenzene 19.3
4.34 1.91 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼m-Xylene & p-Xylene 75.2
4.34 2.00 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼o-Xylene 31.1
4.34 2.26 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Toluene 64.9
8.68 3.12 mg/Kg 07/26/22 10:32 07/27/22 17:16 500☼Xylenes, Total 106
1,2-Dichloroethane-d4 (Surr)99 65-130 07/26/22 10:32 07/27/22 17:16 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/26/22 10:32 07/27/22 17:16 50065-130
Dibromofluoromethane (Surr)100 07/26/22 10:32 07/27/22 17:16 50065-130
Toluene-d8 (Surr)104 07/26/22 10:32 07/27/22 17:16 50065-130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
RL MDL
Gasoline Range Organics [C6 -
C10]
828 169 42.3 mg/Kg ☼07/26/22 10:32 07/29/22 21:12 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
a,a,a-Trifluorotoluene 79 70-131 07/26/22 10:32 07/29/22 21:12 1000
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/03/22 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.190 ug/L 08/03/22 18:06 11,1,1-Trichloroethane ND
0.500 0.100 ug/L 08/03/22 18:06 11,1,2,2-Tetrachloroethane ND
0.500 0.140 ug/L 08/03/22 18:06 11,1,2-Trichloroethane ND
0.500 0.180 ug/L 08/03/22 18:06 11,1-Dichloroethane ND
0.500 0.180 ug/L 08/03/22 18:06 11,1-Dichloroethene ND
0.500 0.200 ug/L 08/03/22 18:06 11,1-Dichloropropene ND
1.00 0.770 ug/L 08/03/22 18:06 11,2,3-Trichlorobenzene ND
0.500 0.120 ug/L 08/03/22 18:06 11,2,3-Trichloropropane ND
0.500 0.350 ug/L 08/03/22 18:06 11,2,4-Trichlorobenzene ND
0.500 0.140 ug/L 08/03/22 18:06 11,2,4-Trimethylbenzene 90.4
0.500 0.120 ug/L 08/03/22 18:06 11,2-Dichlorobenzene ND
0.500 0.160 ug/L 08/03/22 18:06 11,2-Dichloroethane ND
0.500 0.230 ug/L 08/03/22 18:06 11,2-Dichloroethene, Total ND
0.500 0.160 ug/L 08/03/22 18:06 11,2-Dichloropropane ND
0.500 0.160 ug/L 08/03/22 18:06 11,3,5-Trimethylbenzene 29.2
0.500 0.160 ug/L 08/03/22 18:06 11,3-Dichlorobenzene ND
0.500 0.140 ug/L 08/03/22 18:06 11,3-Dichloropropane ND
0.500 0.220 ug/L 08/03/22 18:06 11,3-Dichloropropene, Total ND
0.500 0.120 ug/L 08/03/22 18:06 11,4-Dichlorobenzene ND
0.500 0.180 ug/L 08/03/22 18:06 12,2-Dichloropropane ND
10.0 5.20 ug/L 08/03/22 18:06 12-Butanone (MEK)ND
0.500 0.160 ug/L 08/03/22 18:06 12-Chlorotoluene ND
10.0 5.00 ug/L 08/03/22 18:06 12-Hexanone ND
20.0 9.10 ug/L 08/03/22 18:06 13,3-Dimethyl-1-butanol ND
0.500 0.160 ug/L 08/03/22 18:06 14-Chlorotoluene ND
0.500 0.180 ug/L 08/03/22 18:06 14-Isopropyltoluene 2.41
10.0 5.20 ug/L 08/03/22 18:06 14-Methyl-2-pentanone (MIBK)ND
20.0 5.60 ug/L 08/03/22 18:06 1AcetoneND
0.500 0.180 ug/L 08/03/22 18:06 1Benzene14.4
0.500 0.140 ug/L 08/03/22 18:06 1BromobenzeneND
0.500 0.180 ug/L 08/03/22 18:06 1BromoformND
5.00 2.30 ug/L 08/03/22 18:06 1BromomethaneND
0.500 0.220 ug/L 08/03/22 18:06 1Carbon tetrachloride ND
0.500 0.160 ug/L 08/03/22 18:06 1ChlorobenzeneND
0.500 0.130 ug/L 08/03/22 18:06 1ChlorobromomethaneND
1.00 0.460 ug/L 08/03/22 18:06 1ChlorodibromomethaneND
10.0 4.10 ug/L 08/03/22 18:06 1ChloroethaneND
0.500 0.380 ug/L 08/03/22 18:06 1Chloroform0.599
0.500 0.100 ug/L 08/03/22 18:06 1ChloromethaneND
0.500 0.0640 ug/L 08/03/22 18:06 1cis-1,2-Dichloroethene ND
0.500 0.110 ug/L 08/03/22 18:06 1cis-1,3-Dichloropropene ND
0.500 0.170 ug/L 08/03/22 18:06 1DibromomethaneND
1.00 0.410 ug/L 08/03/22 18:06 1DichlorobromomethaneND
0.500 0.0910 ug/L 08/03/22 18:06 1DichlorodifluoromethaneND
0.500 0.140 ug/L 08/03/22 18:06 1DichlorofluoromethaneND
200 140 ug/L 08/03/22 18:06 1EthanolND
0.500 0.0920 ug/L 08/03/22 18:06 1Ethyl ether ND
0.500 0.170 ug/L 08/03/22 18:06 1Ethylbenzene56.5
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Ethylene Dibromide ND 0.500 0.170 ug/L 08/03/22 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.0580 ug/L 08/03/22 18:06 1Isopropyl ether ND
0.500 0.180 ug/L 08/03/22 18:06 1Isopropylbenzene5.09
0.500 0.110 ug/L 08/03/22 18:06 1Methyl tert-butyl ether ND
0.500 0.150 ug/L 08/03/22 18:06 1Methylene Chloride ND
0.500 0.180 ug/L 08/03/22 18:06 1m-Xylene & p-Xylene 209 E
2.00 1.20 ug/L 08/03/22 18:06 1Naphthalene5.97
1.00 0.160 ug/L 08/03/22 18:06 1n-Butylbenzene 11.0
0.500 0.180 ug/L 08/03/22 18:06 1N-Propylbenzene 17.8
0.500 0.150 ug/L 08/03/22 18:06 1o-Xylene 82.2
1.00 0.170 ug/L 08/03/22 18:06 1sec-Butylbenzene ND
0.500 0.170 ug/L 08/03/22 18:06 1StyreneND
5.00 1.90 ug/L 08/03/22 18:06 1t-Amyl alcohol ND
0.500 0.0790 ug/L 08/03/22 18:06 1Tert-amyl methyl ether ND
0.500 0.0580 ug/L 08/03/22 18:06 1Tert-butyl ethyl ether ND
5.00 1.76 ug/L 08/03/22 18:06 1tert-Butyl Formate ND
0.500 0.180 ug/L 08/03/22 18:06 1tert-Butylbenzene ND
0.500 0.220 ug/L 08/03/22 18:06 1Tetrachloroethene3.92
0.500 0.200 ug/L 08/03/22 18:06 1Toluene20.0
0.500 0.170 ug/L 08/03/22 18:06 1trans-1,2-Dichloroethene ND
0.500 0.120 ug/L 08/03/22 18:06 1trans-1,3-Dichloropropene ND
0.500 0.200 ug/L 08/03/22 18:06 1TrichloroetheneND
0.500 0.140 ug/L 08/03/22 18:06 1TrichlorofluoromethaneND
1.00 0.640 ug/L 08/03/22 18:06 1Vinyl acetate ND
0.500 0.120 ug/L 08/03/22 18:06 1Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)95 70-130 08/03/22 18:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 08/03/22 18:06 170-130
Dibromofluoromethane (Surr)98 08/03/22 18:06 170-130
Toluene-d8 (Surr)102 08/03/22 18:06 170-130
Method: SM6200-B - Volatile Organic Compounds - DL
RL MDL
m-Xylene & p-Xylene 169 H 2.50 0.900 ug/L 08/04/22 13:42 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)93 70-130 08/04/22 13:42 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 08/04/22 13:42 570-130
Dibromofluoromethane (Surr)99 08/04/22 13:42 570-130
Toluene-d8 (Surr)105 08/04/22 13:42 570-130
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 348 130 130 ug/L 08/02/22 10:10 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
35.0 35.0 ug/L 08/02/22 10:10 5C9-C10 Aromatics 533 F1
55.0 55.0 ug/L 08/02/22 10:10 5C9-C12 Aliphatics 404
a,a,a-Trifluorotoluene (fid)101 70-130 08/02/22 10:10 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)101 08/02/22 10:10 570-130
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-16Client Sample ID: MW-3
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
1,2-Dibromoethane (EDB)ND 0.0181 0.00503 ug/L 07/25/22 11:15 07/25/22 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane 89 p 70-130 07/25/22 11:15 07/25/22 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP) - Total Recoverable
RL MDL
Lead, Total 11.6 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1,1,1,2-Tetrachloroethane ND H 250 75.0 ug/L 08/04/22 13:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
250 95.0 ug/L 08/04/22 13:16 5001,1,1-Trichloroethane ND H
250 50.0 ug/L 08/04/22 13:16 5001,1,2,2-Tetrachloroethane ND H
250 70.0 ug/L 08/04/22 13:16 5001,1,2-Trichloroethane ND H
250 90.0 ug/L 08/04/22 13:16 5001,1-Dichloroethane ND H
250 90.0 ug/L 08/04/22 13:16 5001,1-Dichloroethene ND H
250 100 ug/L 08/04/22 13:16 5001,1-Dichloropropene ND H
500 385 ug/L 08/04/22 13:16 5001,2,3-Trichlorobenzene ND H
250 60.0 ug/L 08/04/22 13:16 5001,2,3-Trichloropropane ND H
250 175 ug/L 08/04/22 13:16 5001,2,4-Trichlorobenzene ND H
250 70.0 ug/L 08/04/22 13:16 5001,2,4-Trimethylbenzene 699 H
250 60.0 ug/L 08/04/22 13:16 5001,2-Dichlorobenzene ND H
250 80.0 ug/L 08/04/22 13:16 5001,2-Dichloroethane ND H
250 115 ug/L 08/04/22 13:16 5001,2-Dichloroethene, Total ND H
250 80.0 ug/L 08/04/22 13:16 5001,2-Dichloropropane ND H
250 80.0 ug/L 08/04/22 13:16 5001,3,5-Trimethylbenzene ND H
250 80.0 ug/L 08/04/22 13:16 5001,3-Dichlorobenzene ND H
250 70.0 ug/L 08/04/22 13:16 5001,3-Dichloropropane ND H
250 110 ug/L 08/04/22 13:16 5001,3-Dichloropropene, Total ND H
250 60.0 ug/L 08/04/22 13:16 5001,4-Dichlorobenzene ND H
250 90.0 ug/L 08/04/22 13:16 5002,2-Dichloropropane ND H
5000 2600 ug/L 08/04/22 13:16 5002-Butanone (MEK)ND H
250 80.0 ug/L 08/04/22 13:16 5002-Chlorotoluene ND H
5000 2500 ug/L 08/04/22 13:16 5002-Hexanone ND H
10000 4550 ug/L 08/04/22 13:16 5003,3-Dimethyl-1-butanol ND H
250 80.0 ug/L 08/04/22 13:16 5004-Chlorotoluene ND H
250 90.0 ug/L 08/04/22 13:16 5004-Isopropyltoluene ND H
5000 2600 ug/L 08/04/22 13:16 5004-Methyl-2-pentanone (MIBK)ND H
10000 2800 ug/L 08/04/22 13:16 500AcetoneNDH
250 90.0 ug/L 08/04/22 13:16 500Benzene995H
250 70.0 ug/L 08/04/22 13:16 500BromobenzeneNDH
250 90.0 ug/L 08/04/22 13:16 500BromoformNDH
2500 1150 ug/L 08/04/22 13:16 500BromomethaneNDH
250 110 ug/L 08/04/22 13:16 500Carbon tetrachloride ND H
250 80.0 ug/L 08/04/22 13:16 500ChlorobenzeneNDH
250 65.0 ug/L 08/04/22 13:16 500ChlorobromomethaneNDH
500 230 ug/L 08/04/22 13:16 500ChlorodibromomethaneNDH
5000 2050 ug/L 08/04/22 13:16 500ChloroethaneNDH
250 190 ug/L 08/04/22 13:16 500ChloroformNDH
250 50.0 ug/L 08/04/22 13:16 500ChloromethaneNDH
250 32.0 ug/L 08/04/22 13:16 500cis-1,2-Dichloroethene ND H
250 55.0 ug/L 08/04/22 13:16 500cis-1,3-Dichloropropene ND H
250 85.0 ug/L 08/04/22 13:16 500DibromomethaneNDH
500 205 ug/L 08/04/22 13:16 500DichlorobromomethaneNDH
250 45.5 ug/L 08/04/22 13:16 500DichlorodifluoromethaneNDH
250 70.0 ug/L 08/04/22 13:16 500DichlorofluoromethaneNDH
100000 70000 ug/L 08/04/22 13:16 500EthanolNDH
250 46.0 ug/L 08/04/22 13:16 500Ethyl ether ND H
250 85.0 ug/L 08/04/22 13:16 500Ethylbenzene1120H
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
Ethylene Dibromide ND H 250 85.0 ug/L 08/04/22 13:16 500
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
250 29.0 ug/L 08/04/22 13:16 500Isopropyl ether ND H
250 90.0 ug/L 08/04/22 13:16 500IsopropylbenzeneNDH
250 55.0 ug/L 08/04/22 13:16 500Methyl tert-butyl ether ND H
250 75.0 ug/L 08/04/22 13:16 500Methylene Chloride ND H
250 90.0 ug/L 08/04/22 13:16 500m-Xylene & p-Xylene 4640 H
1000 600 ug/L 08/04/22 13:16 500NaphthaleneNDH
500 80.0 ug/L 08/04/22 13:16 500n-Butylbenzene ND H
250 90.0 ug/L 08/04/22 13:16 500N-Propylbenzene ND H
250 75.0 ug/L 08/04/22 13:16 500o-Xylene 2410 H
500 85.0 ug/L 08/04/22 13:16 500sec-Butylbenzene ND H
250 85.0 ug/L 08/04/22 13:16 500StyreneNDH
2500 950 ug/L 08/04/22 13:16 500t-Amyl alcohol ND H
250 39.5 ug/L 08/04/22 13:16 500Tert-amyl methyl ether ND H
250 29.0 ug/L 08/04/22 13:16 500Tert-butyl ethyl ether ND H
2500 880 ug/L 08/04/22 13:16 500tert-Butyl Formate ND H
250 90.0 ug/L 08/04/22 13:16 500tert-Butylbenzene ND H
250 110 ug/L 08/04/22 13:16 500TetrachloroetheneNDH
250 100 ug/L 08/04/22 13:16 500Toluene12100H
250 85.0 ug/L 08/04/22 13:16 500trans-1,2-Dichloroethene ND H
250 60.0 ug/L 08/04/22 13:16 500trans-1,3-Dichloropropene ND H
250 100 ug/L 08/04/22 13:16 500TrichloroetheneNDH
250 70.0 ug/L 08/04/22 13:16 500TrichlorofluoromethaneNDH
500 320 ug/L 08/04/22 13:16 500Vinyl acetate ND H
250 60.0 ug/L 08/04/22 13:16 500Vinyl chloride ND H
1,2-Dichloroethane-d4 (Surr)93 70-130 08/04/22 13:16 500
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 08/04/22 13:16 50070-130
Dibromofluoromethane (Surr)98 08/04/22 13:16 50070-130
Toluene-d8 (Surr)105 08/04/22 13:16 50070-130
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 33700 2600 2600 ug/L 08/02/22 15:32 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
700 700 ug/L 08/02/22 15:32 100C9-C10 Aromatics 4670
1100 1100 ug/L 08/02/22 15:32 100C9-C12 Aliphatics 16700
a,a,a-Trifluorotoluene (fid)95 70-130 08/02/22 15:32 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 08/02/22 15:32 10070-130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
1,2-Dibromoethane (EDB)ND 0.0184 0.00510 ug/L 07/25/22 11:15 07/25/22 19:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Pentachloroethane 160 p S1+70-130 07/25/22 11:15 07/25/22 19:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Lab Sample ID: 680-218771-17Client Sample ID: MW-2
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Method: 6010D - Metals (ICP) - Total Recoverable
RL MDL
Lead, Total ND 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-732600/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/26/22 13:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/26/22 13:22 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/26/22 13:22 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/26/22 13:22 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/26/22 13:22 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/26/22 13:22 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/26/22 13:22 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/26/22 13:22 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/26/22 13:22 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/26/22 13:22 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/26/22 13:22 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/26/22 13:22 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/26/22 13:22 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/26/22 13:22 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/26/22 13:22 12-Hexanone
ND 0.002100.00500 mg/Kg 07/26/22 13:22 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/26/22 13:22 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/26/22 13:22 1Acetone
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Benzene
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Bromoform
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Bromomethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/26/22 13:22 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Chloroethane
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Chloroform
ND 0.002400.00500 mg/Kg 07/26/22 13:22 1Chloromethane
ND 0.002900.00500 mg/Kg 07/26/22 13:22 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/26/22 13:22 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/26/22 13:22 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/26/22 13:22 1Hexachlorobutadiene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732600/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
RL MDL
Hexane ND 0.00500 0.00170 mg/Kg 07/26/22 13:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 07/26/22 13:22 1Iodomethane
ND 0.001500.0100 mg/Kg 07/26/22 13:22 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/26/22 13:22 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/26/22 13:22 1Naphthalene
ND 0.001900.00500 mg/Kg 07/26/22 13:22 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/26/22 13:22 1n-Heptane
ND 0.002200.00500 mg/Kg 07/26/22 13:22 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 1o-Xylene
ND 0.002000.00500 mg/Kg 07/26/22 13:22 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/26/22 13:22 1Styrene
ND 0.002500.00500 mg/Kg 07/26/22 13:22 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1Toluene
ND 0.002300.00500 mg/Kg 07/26/22 13:22 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/26/22 13:22 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/26/22 13:22 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/26/22 13:22 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/26/22 13:22 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/26/22 13:22 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/26/22 13:22 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/26/22 13:22 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)100 65-130 07/26/22 13:22 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
110 07/26/22 13:22 14-Bromofluorobenzene (Surr)65-130
101 07/26/22 13:22 1Dibromofluoromethane (Surr)65-130
107 07/26/22 13:22 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,1,1,2-Tetrachloroethane 0.0500 0.04761 mg/Kg 95 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04518 mg/Kg 90 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04978 mg/Kg 100 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04578 mg/Kg 92 70 -130
1,1,2-Trichloroethane 0.0500 0.05066 mg/Kg 101 56 -146
1,1-Dichloroethane 0.0500 0.05049 mg/Kg 101 70 -130
1,1-Dichloroethene 0.0500 0.04679 mg/Kg 94 69 -130
1,1-Dichloropropene 0.0500 0.04601 mg/Kg 92 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05303 mg/Kg 106 70 -130
1,2,3-Trichloropropane 0.0500 0.04879 mg/Kg 98 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05239 mg/Kg 105 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,2,4-Trimethylbenzene 0.0500 0.04663 mg/Kg 93 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.05142 mg/Kg 103 42 -145
1,2-Dichlorobenzene 0.0500 0.05122 mg/Kg 102 70 -130
1,2-Dichloroethane 0.0500 0.05022 mg/Kg 100 68 -139
1,2-Dichloropropane 0.0500 0.05098 mg/Kg 102 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04560 mg/Kg 91 70 -130
1,3-Dichlorobenzene 0.0500 0.05126 mg/Kg 103 70 -130
1,3-Dichloropropane 0.0500 0.04915 mg/Kg 98 54 -150
1,4-Dichlorobenzene 0.0500 0.05119 mg/Kg 102 70 -130
2,2-Dichloropropane 0.0500 0.04697 mg/Kg 94 70 -130
2-Butanone (MEK)0.250 0.2582 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.04914 mg/Kg 98 70 -130
2-Hexanone 0.250 0.2647 mg/Kg 106 30 -150
4-Chlorotoluene 0.0500 0.04498 mg/Kg 90 70 -130
4-Isopropyltoluene 0.0500 0.04858 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2613 mg/Kg 105 34 -150
Acetone 0.250 0.2717 mg/Kg 109 10 -150
Benzene 0.0500 0.04846 mg/Kg 97 70 -130
Bromobenzene 0.0500 0.04763 mg/Kg 95 70 -130
Bromoform 0.0500 0.04638 mg/Kg 93 68 -130
Bromomethane 0.0500 0.06967 *+mg/Kg 139 70 -130
Carbon disulfide 0.0500 0.04775 mg/Kg 95 70 -130
Carbon tetrachloride 0.0500 0.04337 mg/Kg 87 70 -130
Chlorobenzene 0.0500 0.04938 mg/Kg 99 70 -130
Chlorobromomethane 0.0500 0.04663 mg/Kg 93 66 -130
Chlorodibromomethane 0.0500 0.04814 mg/Kg 96 64 -133
Chloroethane 0.0500 0.05507 mg/Kg 110 70 -130
Chloroform 0.0500 0.05162 mg/Kg 103 70 -130
Chloromethane 0.0500 0.04756 mg/Kg 95 70 -130
cis-1,2-Dichloroethene 0.0500 0.05072 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.04996 mg/Kg 100 70 -130
Dibromomethane 0.0500 0.04917 mg/Kg 98 59 -142
Dichlorobromomethane 0.0500 0.04986 mg/Kg 100 70 -130
Ethyl acetate 0.100 0.1022 mg/Kg 102 70 -130
Ethylbenzene 0.0500 0.04970 mg/Kg 99 70 -130
Ethylene Dibromide 0.0500 0.04811 mg/Kg 96 48 -150
Hexachlorobutadiene 0.0500 0.04597 mg/Kg 92 70 -130
Hexane 0.0500 0.04668 mg/Kg 93 70 -130
Iodomethane 0.0500 0.05034 mg/Kg 101 65 -138
Isopropyl ether 0.0500 0.05026 mg/Kg 101 50 -150
Isopropylbenzene 0.0500 0.04674 mg/Kg 93 70 -130
Methyl tert-butyl ether 0.0500 0.07066 *+mg/Kg 141 70 -130
Methylene Chloride 0.0500 0.04632 mg/Kg 93 54 -149
m-Xylene & p-Xylene 0.0500 0.04992 mg/Kg 100 70 -130
Naphthalene 0.0500 0.05408 mg/Kg 108 46 -150
n-Butylbenzene 0.0500 0.04951 mg/Kg 99 70 -130
n-Heptane 0.0500 0.04421 mg/Kg 88 70 -130
N-Propylbenzene 0.0500 0.04685 mg/Kg 94 70 -130
o-Xylene 0.0500 0.05081 mg/Kg 102 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732600/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
sec-Butylbenzene 0.0500 0.04525 mg/Kg 91 69 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Styrene 0.0500 0.04852 mg/Kg 97 70 -130
tert-Butylbenzene 0.0500 0.04460 mg/Kg 89 67 -145
Tetrachloroethene 0.0500 0.05467 mg/Kg 109 70 -130
Toluene 0.0500 0.04736 mg/Kg 95 70 -130
trans-1,2-Dichloroethene 0.0500 0.04918 mg/Kg 98 67 -130
trans-1,3-Dichloropropene 0.0500 0.04796 mg/Kg 96 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04931 mg/Kg 99 54 -150
Trichloroethene 0.0500 0.04649 mg/Kg 93 70 -130
Trichlorofluoromethane 0.0500 0.04860 mg/Kg 97 70 -130
Vinyl acetate 0.100 0.1044 mg/Kg 104 53 -150
Vinyl chloride 0.0500 0.05217 mg/Kg 104 70 -130
Xylenes, Total 0.100 0.1007 mg/Kg 101 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
1124-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
1,1,1,2-Tetrachloroethane 0.0500 0.04760 mg/Kg 95 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04525 mg/Kg 91 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05103 mg/Kg 102 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04554 mg/Kg 91 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.05138 mg/Kg 103 56 -146 1 30
1,1-Dichloroethane 0.0500 0.05114 mg/Kg 102 70 -130 1 30
1,1-Dichloroethene 0.0500 0.04661 mg/Kg 93 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04535 mg/Kg 91 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05342 mg/Kg 107 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.05003 mg/Kg 100 64 -130 3 30
1,2,4-Trichlorobenzene 0.0500 0.05181 mg/Kg 104 70 -130 1 30
1,2,4-Trimethylbenzene 0.0500 0.04424 mg/Kg 88 70 -130 5 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05391 mg/Kg 108 42 -145 5 30
1,2-Dichlorobenzene 0.0500 0.05222 mg/Kg 104 70 -130 2 30
1,2-Dichloroethane 0.0500 0.05101 mg/Kg 102 68 -139 2 30
1,2-Dichloropropane 0.0500 0.05227 mg/Kg 105 70 -130 2 30
1,3,5-Trimethylbenzene 0.0500 0.04363 mg/Kg 87 70 -130 4 30
1,3-Dichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130 0 30
1,3-Dichloropropane 0.0500 0.05113 mg/Kg 102 54 -150 4 30
1,4-Dichlorobenzene 0.0500 0.05175 mg/Kg 104 70 -130 1 30
2,2-Dichloropropane 0.0500 0.04695 mg/Kg 94 70 -130 0 30
2-Butanone (MEK)0.250 0.2661 mg/Kg 106 40 -150 3 30
2-Chlorotoluene 0.0500 0.04722 mg/Kg 94 70 -130 4 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
2-Hexanone 0.250 0.2742 mg/Kg 110 30 -150 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 0.0500 0.04395 mg/Kg 88 70 -130 2 30
4-Isopropyltoluene 0.0500 0.04605 mg/Kg 92 70 -130 5 30
4-Methyl-2-pentanone (MIBK)0.250 0.2691 mg/Kg 108 34 -150 3 30
Acetone 0.250 0.2746 mg/Kg 110 10 -150 1 50
Benzene 0.0500 0.04910 mg/Kg 98 70 -130 1 30
Bromobenzene 0.0500 0.04700 mg/Kg 94 70 -130 1 30
Bromoform 0.0500 0.04783 mg/Kg 96 68 -130 3 30
Bromomethane 0.0500 0.07191 *+mg/Kg 144 70 -130 3 30
Carbon disulfide 0.0500 0.04790 mg/Kg 96 70 -130 0 30
Carbon tetrachloride 0.0500 0.04381 mg/Kg 88 70 -130 1 30
Chlorobenzene 0.0500 0.04884 mg/Kg 98 70 -130 1 30
Chlorobromomethane 0.0500 0.04851 mg/Kg 97 66 -130 4 30
Chlorodibromomethane 0.0500 0.04874 mg/Kg 97 64 -133 1 30
Chloroethane 0.0500 0.05595 mg/Kg 112 70 -130 2 30
Chloroform 0.0500 0.05259 mg/Kg 105 70 -130 2 30
Chloromethane 0.0500 0.04787 mg/Kg 96 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.05159 mg/Kg 103 70 -130 2 30
cis-1,3-Dichloropropene 0.0500 0.05093 mg/Kg 102 70 -130 2 30
Dibromomethane 0.0500 0.05003 mg/Kg 100 59 -142 2 30
Dichlorobromomethane 0.0500 0.05047 mg/Kg 101 70 -130 1 30
Ethyl acetate 0.100 0.1053 mg/Kg 105 70 -130 3 30
Ethylbenzene 0.0500 0.04805 mg/Kg 96 70 -130 3 30
Ethylene Dibromide 0.0500 0.04917 mg/Kg 98 48 -150 2 30
Hexachlorobutadiene 0.0500 0.04058 mg/Kg 81 70 -130 12 30
Hexane 0.0500 0.04618 mg/Kg 92 70 -130 1 30
Iodomethane 0.0500 0.05191 mg/Kg 104 65 -138 3 30
Isopropyl ether 0.0500 0.05093 mg/Kg 102 50 -150 1 30
Isopropylbenzene 0.0500 0.04478 mg/Kg 90 70 -130 4 30
Methyl tert-butyl ether 0.0500 0.07311 *+mg/Kg 146 70 -130 3 30
Methylene Chloride 0.0500 0.04780 mg/Kg 96 54 -149 3 30
m-Xylene & p-Xylene 0.0500 0.04844 mg/Kg 97 70 -130 3 30
Naphthalene 0.0500 0.05626 mg/Kg 113 46 -150 4 30
n-Butylbenzene 0.0500 0.04566 mg/Kg 91 70 -130 8 30
n-Heptane 0.0500 0.04334 mg/Kg 87 70 -130 2 30
N-Propylbenzene 0.0500 0.04394 mg/Kg 88 70 -130 6 30
o-Xylene 0.0500 0.04945 mg/Kg 99 70 -130 3 30
sec-Butylbenzene 0.0500 0.04148 mg/Kg 83 69 -142 9 30
Styrene 0.0500 0.04795 mg/Kg 96 70 -130 1 30
tert-Butylbenzene 0.0500 0.04247 mg/Kg 85 67 -145 5 30
Tetrachloroethene 0.0500 0.05345 mg/Kg 107 70 -130 2 30
Toluene 0.0500 0.04790 mg/Kg 96 70 -130 1 30
trans-1,2-Dichloroethene 0.0500 0.04960 mg/Kg 99 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04924 mg/Kg 98 54 -150 3 30
trans-1,4-Dichloro-2-butene 0.0500 0.04916 mg/Kg 98 54 -150 0 30
Trichloroethene 0.0500 0.04621 mg/Kg 92 70 -130 1 30
Trichlorofluoromethane 0.0500 0.04853 mg/Kg 97 70 -130 0 30
Vinyl acetate 0.100 0.1066 mg/Kg 107 53 -150 2 30
Vinyl chloride 0.0500 0.05310 mg/Kg 106 70 -130 2 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732600/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732600
Xylenes, Total 0.100 0.09789 mg/Kg 98 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
1144-Bromofluorobenzene (Surr)65 -130
100Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-732793/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/27/22 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/27/22 12:15 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/27/22 12:15 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/27/22 12:15 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/27/22 12:15 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/27/22 12:15 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/27/22 12:15 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/27/22 12:15 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/27/22 12:15 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/27/22 12:15 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/27/22 12:15 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/27/22 12:15 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/27/22 12:15 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/27/22 12:15 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/27/22 12:15 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/27/22 12:15 12-Hexanone
ND 0.002100.00500 mg/Kg 07/27/22 12:15 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/27/22 12:15 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/27/22 12:15 1Acetone
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Benzene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Bromoform
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Bromomethane
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/27/22 12:15 1Chlorobenzene
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732793/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
RL MDL
Chlorobromomethane ND 0.00500 0.00200 mg/Kg 07/27/22 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Chloroethane
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Chloroform
ND 0.002400.00500 mg/Kg 07/27/22 12:15 1Chloromethane
ND 0.002900.00500 mg/Kg 07/27/22 12:15 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/27/22 12:15 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/27/22 12:15 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/27/22 12:15 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Hexane
ND 0.001700.00500 mg/Kg 07/27/22 12:15 1Iodomethane
ND 0.001500.0100 mg/Kg 07/27/22 12:15 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/27/22 12:15 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/27/22 12:15 1Naphthalene
ND 0.001900.00500 mg/Kg 07/27/22 12:15 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/27/22 12:15 1n-Heptane
ND 0.002200.00500 mg/Kg 07/27/22 12:15 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 1o-Xylene
ND 0.002000.00500 mg/Kg 07/27/22 12:15 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/27/22 12:15 1Styrene
ND 0.002500.00500 mg/Kg 07/27/22 12:15 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1Toluene
ND 0.002300.00500 mg/Kg 07/27/22 12:15 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/27/22 12:15 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/27/22 12:15 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/27/22 12:15 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/27/22 12:15 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/27/22 12:15 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/27/22 12:15 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/27/22 12:15 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)98 65-130 07/27/22 12:15 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
109 07/27/22 12:15 14-Bromofluorobenzene (Surr)65-130
99 07/27/22 12:15 1Dibromofluoromethane (Surr)65-130
106 07/27/22 12:15 1Toluene-d8 (Surr)65-130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732793/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,1,1,2-Tetrachloroethane 0.0500 0.04642 mg/Kg 93 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04392 mg/Kg 88 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04747 mg/Kg 95 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04462 mg/Kg 89 70 -130
1,1,2-Trichloroethane 0.0500 0.04911 mg/Kg 98 56 -146
1,1-Dichloroethane 0.0500 0.04951 mg/Kg 99 70 -130
1,1-Dichloroethene 0.0500 0.04672 mg/Kg 93 69 -130
1,1-Dichloropropene 0.0500 0.04532 mg/Kg 91 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05149 mg/Kg 103 70 -130
1,2,3-Trichloropropane 0.0500 0.04632 mg/Kg 93 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05154 mg/Kg 103 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04682 mg/Kg 94 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04723 mg/Kg 94 42 -145
1,2-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,2-Dichloroethane 0.0500 0.04879 mg/Kg 98 68 -139
1,2-Dichloropropane 0.0500 0.05029 mg/Kg 101 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04588 mg/Kg 92 70 -130
1,3-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,3-Dichloropropane 0.0500 0.04830 mg/Kg 97 54 -150
1,4-Dichlorobenzene 0.0500 0.05079 mg/Kg 102 70 -130
2,2-Dichloropropane 0.0500 0.04591 mg/Kg 92 70 -130
2-Butanone (MEK)0.250 0.2413 mg/Kg 97 40 -150
2-Chlorotoluene 0.0500 0.04859 mg/Kg 97 70 -130
2-Hexanone 0.250 0.2463 mg/Kg 99 30 -150
4-Chlorotoluene 0.0500 0.04517 mg/Kg 90 70 -130
4-Isopropyltoluene 0.0500 0.04855 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2428 mg/Kg 97 34 -150
Acetone 0.250 0.2500 mg/Kg 100 10 -150
Benzene 0.0500 0.04809 mg/Kg 96 70 -130
Bromobenzene 0.0500 0.04705 mg/Kg 94 70 -130
Bromoform 0.0500 0.04431 mg/Kg 89 68 -130
Bromomethane 0.0500 0.06823 *+mg/Kg 136 70 -130
Carbon disulfide 0.0500 0.04677 mg/Kg 94 70 -130
Carbon tetrachloride 0.0500 0.04244 mg/Kg 85 70 -130
Chlorobenzene 0.0500 0.04831 mg/Kg 97 70 -130
Chlorobromomethane 0.0500 0.04656 mg/Kg 93 66 -130
Chlorodibromomethane 0.0500 0.04649 mg/Kg 93 64 -133
Chloroethane 0.0500 0.05435 mg/Kg 109 70 -130
Chloroform 0.0500 0.04889 mg/Kg 98 70 -130
Chloromethane 0.0500 0.04525 mg/Kg 90 70 -130
cis-1,2-Dichloroethene 0.0500 0.04945 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04942 mg/Kg 99 70 -130
Dibromomethane 0.0500 0.04822 mg/Kg 96 59 -142
Dichlorobromomethane 0.0500 0.04864 mg/Kg 97 70 -130
Ethyl acetate 0.100 0.09684 mg/Kg 97 70 -130
Ethylbenzene 0.0500 0.04837 mg/Kg 97 70 -130
Ethylene Dibromide 0.0500 0.04673 mg/Kg 93 48 -150
Hexachlorobutadiene 0.0500 0.04628 mg/Kg 93 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732793/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
Hexane 0.0500 0.04551 mg/Kg 91 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Iodomethane 0.0500 0.04788 mg/Kg 96 65 -138
Isopropyl ether 0.0500 0.04969 mg/Kg 99 50 -150
Isopropylbenzene 0.0500 0.04617 mg/Kg 92 70 -130
Methyl tert-butyl ether 0.0500 0.06987 *+mg/Kg 140 70 -130
Methylene Chloride 0.0500 0.04593 mg/Kg 92 54 -149
m-Xylene & p-Xylene 0.0500 0.04818 mg/Kg 96 70 -130
Naphthalene 0.0500 0.05146 mg/Kg 103 46 -150
n-Butylbenzene 0.0500 0.05008 mg/Kg 100 70 -130
n-Heptane 0.0500 0.04286 mg/Kg 86 70 -130
N-Propylbenzene 0.0500 0.04676 mg/Kg 94 70 -130
o-Xylene 0.0500 0.04934 mg/Kg 99 70 -130
sec-Butylbenzene 0.0500 0.04477 mg/Kg 90 69 -142
Styrene 0.0500 0.04736 mg/Kg 95 70 -130
tert-Butylbenzene 0.0500 0.04401 mg/Kg 88 67 -145
Tetrachloroethene 0.0500 0.05026 mg/Kg 101 70 -130
Toluene 0.0500 0.04748 mg/Kg 95 70 -130
trans-1,2-Dichloroethene 0.0500 0.04762 mg/Kg 95 67 -130
trans-1,3-Dichloropropene 0.0500 0.04693 mg/Kg 94 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04659 mg/Kg 93 54 -150
Trichloroethene 0.0500 0.04612 mg/Kg 92 70 -130
Trichlorofluoromethane 0.0500 0.04561 mg/Kg 91 70 -130
Vinyl acetate 0.100 0.1030 mg/Kg 103 53 -150
Vinyl chloride 0.0500 0.04981 mg/Kg 100 70 -130
Xylenes, Total 0.100 0.09752 mg/Kg 98 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)65 -130
98Dibromofluoromethane (Surr)65 -130
101Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,1,1,2-Tetrachloroethane 0.0500 0.04682 mg/Kg 94 70 -130 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04419 mg/Kg 88 70 -130 1 30
1,1,2,2-Tetrachloroethane 0.0500 0.04744 mg/Kg 95 64 -130 0 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04432 mg/Kg 89 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.04842 mg/Kg 97 56 -146 1 30
1,1-Dichloroethane 0.0500 0.04985 mg/Kg 100 70 -130 1 30
1,1-Dichloroethene 0.0500 0.04682 mg/Kg 94 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04490 mg/Kg 90 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05099 mg/Kg 102 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.04638 mg/Kg 93 64 -130 0 30
1,2,4-Trichlorobenzene 0.0500 0.05143 mg/Kg 103 70 -130 0 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
1,2,4-Trimethylbenzene 0.0500 0.04561 mg/Kg 91 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dibromo-3-Chloropropane 0.0500 0.04823 mg/Kg 96 42 -145 2 30
1,2-Dichlorobenzene 0.0500 0.05044 mg/Kg 101 70 -130 1 30
1,2-Dichloroethane 0.0500 0.04860 mg/Kg 97 68 -139 0 30
1,2-Dichloropropane 0.0500 0.04997 mg/Kg 100 70 -130 1 30
1,3,5-Trimethylbenzene 0.0500 0.04449 mg/Kg 89 70 -130 3 30
1,3-Dichlorobenzene 0.0500 0.04994 mg/Kg 100 70 -130 0 30
1,3-Dichloropropane 0.0500 0.04848 mg/Kg 97 54 -150 0 30
1,4-Dichlorobenzene 0.0500 0.05048 mg/Kg 101 70 -130 1 30
2,2-Dichloropropane 0.0500 0.04616 mg/Kg 92 70 -130 1 30
2-Butanone (MEK)0.250 0.2410 mg/Kg 96 40 -150 0 30
2-Chlorotoluene 0.0500 0.04816 mg/Kg 96 70 -130 1 30
2-Hexanone 0.250 0.2498 mg/Kg 100 30 -150 1 30
4-Chlorotoluene 0.0500 0.04464 mg/Kg 89 70 -130 1 30
4-Isopropyltoluene 0.0500 0.04716 mg/Kg 94 70 -130 3 30
4-Methyl-2-pentanone (MIBK)0.250 0.2428 mg/Kg 97 34 -150 0 30
Acetone 0.250 0.2494 mg/Kg 100 10 -150 0 50
Benzene 0.0500 0.04806 mg/Kg 96 70 -130 0 30
Bromobenzene 0.0500 0.04619 mg/Kg 92 70 -130 2 30
Bromoform 0.0500 0.04440 mg/Kg 89 68 -130 0 30
Bromomethane 0.0500 0.06516 mg/Kg 130 70 -130 5 30
Carbon disulfide 0.0500 0.04706 mg/Kg 94 70 -130 1 30
Carbon tetrachloride 0.0500 0.04240 mg/Kg 85 70 -130 0 30
Chlorobenzene 0.0500 0.04799 mg/Kg 96 70 -130 1 30
Chlorobromomethane 0.0500 0.04681 mg/Kg 94 66 -130 1 30
Chlorodibromomethane 0.0500 0.04644 mg/Kg 93 64 -133 0 30
Chloroethane 0.0500 0.05225 mg/Kg 104 70 -130 4 30
Chloroform 0.0500 0.04914 mg/Kg 98 70 -130 0 30
Chloromethane 0.0500 0.04381 mg/Kg 88 70 -130 3 30
cis-1,2-Dichloroethene 0.0500 0.04970 mg/Kg 99 70 -130 0 30
cis-1,3-Dichloropropene 0.0500 0.04920 mg/Kg 98 70 -130 0 30
Dibromomethane 0.0500 0.04790 mg/Kg 96 59 -142 1 30
Dichlorobromomethane 0.0500 0.04851 mg/Kg 97 70 -130 0 30
Ethyl acetate 0.100 0.09674 mg/Kg 97 70 -130 0 30
Ethylbenzene 0.0500 0.04818 mg/Kg 96 70 -130 0 30
Ethylene Dibromide 0.0500 0.04619 mg/Kg 92 48 -150 1 30
Hexachlorobutadiene 0.0500 0.04418 mg/Kg 88 70 -130 5 30
Hexane 0.0500 0.04500 mg/Kg 90 70 -130 1 30
Iodomethane 0.0500 0.04861 mg/Kg 97 65 -138 2 30
Isopropyl ether 0.0500 0.04964 mg/Kg 99 50 -150 0 30
Isopropylbenzene 0.0500 0.04498 mg/Kg 90 70 -130 3 30
Methyl tert-butyl ether 0.0500 0.06982 *+mg/Kg 140 70 -130 0 30
Methylene Chloride 0.0500 0.04600 mg/Kg 92 54 -149 0 30
m-Xylene & p-Xylene 0.0500 0.04823 mg/Kg 96 70 -130 0 30
Naphthalene 0.0500 0.05328 mg/Kg 107 46 -150 3 30
n-Butylbenzene 0.0500 0.04810 mg/Kg 96 70 -130 4 30
n-Heptane 0.0500 0.04225 mg/Kg 84 70 -130 1 30
N-Propylbenzene 0.0500 0.04494 mg/Kg 90 70 -130 4 30
o-Xylene 0.0500 0.04948 mg/Kg 99 70 -130 0 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732793/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732793
sec-Butylbenzene 0.0500 0.04312 mg/Kg 86 69 -142 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Styrene 0.0500 0.04720 mg/Kg 94 70 -130 0 30
tert-Butylbenzene 0.0500 0.04339 mg/Kg 87 67 -145 1 30
Tetrachloroethene 0.0500 0.05004 mg/Kg 100 70 -130 0 30
Toluene 0.0500 0.04754 mg/Kg 95 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.04737 mg/Kg 95 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04719 mg/Kg 94 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04692 mg/Kg 94 54 -150 1 30
Trichloroethene 0.0500 0.04505 mg/Kg 90 70 -130 2 30
Trichlorofluoromethane 0.0500 0.04547 mg/Kg 91 70 -130 0 30
Vinyl acetate 0.100 0.1026 mg/Kg 103 53 -150 0 30
Vinyl chloride 0.0500 0.04923 mg/Kg 98 70 -130 1 30
Xylenes, Total 0.100 0.09771 mg/Kg 98 70 -130 0 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
1084-Bromofluorobenzene (Surr)65 -130
98Dibromofluoromethane (Surr)65 -130
102Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/28/22 13:55 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/28/22 13:55 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/28/22 13:55 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/28/22 13:55 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/28/22 13:55 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/28/22 13:55 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/28/22 13:55 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/28/22 13:55 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/28/22 13:55 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/28/22 13:55 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/28/22 13:55 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/28/22 13:55 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/28/22 13:55 12-Chlorotoluene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
2-Hexanone ND 0.0250 0.0190 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002100.00500 mg/Kg 07/28/22 13:55 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/28/22 13:55 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/28/22 13:55 1Acetone
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Benzene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Bromoform
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Bromomethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/28/22 13:55 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Chloroethane
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Chloroform
ND 0.002400.00500 mg/Kg 07/28/22 13:55 1Chloromethane
ND 0.002900.00500 mg/Kg 07/28/22 13:55 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 07/28/22 13:55 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/28/22 13:55 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/28/22 13:55 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Hexane
ND 0.001700.00500 mg/Kg 07/28/22 13:55 1Iodomethane
ND 0.001500.0100 mg/Kg 07/28/22 13:55 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/28/22 13:55 1Methylene Chloride
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 07/28/22 13:55 1Naphthalene
ND 0.001900.00500 mg/Kg 07/28/22 13:55 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/28/22 13:55 1n-Heptane
ND 0.002200.00500 mg/Kg 07/28/22 13:55 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 1o-Xylene
ND 0.002000.00500 mg/Kg 07/28/22 13:55 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/28/22 13:55 1Styrene
ND 0.002500.00500 mg/Kg 07/28/22 13:55 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1Toluene
ND 0.002300.00500 mg/Kg 07/28/22 13:55 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/28/22 13:55 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/28/22 13:55 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/28/22 13:55 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/28/22 13:55 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/28/22 13:55 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/28/22 13:55 1Vinyl chloride
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-732966/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
RL MDL
Xylenes, Total ND 0.0100 0.00360 mg/Kg 07/28/22 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1,2-Dichloroethane-d4 (Surr)98 65-130 07/28/22 13:55 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 07/28/22 13:55 14-Bromofluorobenzene (Surr)65-130
99 07/28/22 13:55 1Dibromofluoromethane (Surr)65-130
106 07/28/22 13:55 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732966/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
1,1,1,2-Tetrachloroethane 0.0500 0.04602 mg/Kg 92 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04414 mg/Kg 88 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04782 mg/Kg 96 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04404 mg/Kg 88 70 -130
1,1,2-Trichloroethane 0.0500 0.04855 mg/Kg 97 56 -146
1,1-Dichloroethane 0.0500 0.04920 mg/Kg 98 70 -130
1,1-Dichloroethene 0.0500 0.04531 mg/Kg 91 69 -130
1,1-Dichloropropene 0.0500 0.04497 mg/Kg 90 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130
1,2,3-Trichloropropane 0.0500 0.04576 mg/Kg 92 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04586 mg/Kg 92 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04722 mg/Kg 94 42 -145
1,2-Dichlorobenzene 0.0500 0.04960 mg/Kg 99 70 -130
1,2-Dichloroethane 0.0500 0.04844 mg/Kg 97 68 -139
1,2-Dichloropropane 0.0500 0.05025 mg/Kg 101 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04547 mg/Kg 91 70 -130
1,3-Dichlorobenzene 0.0500 0.05006 mg/Kg 100 70 -130
1,3-Dichloropropane 0.0500 0.04829 mg/Kg 97 54 -150
1,4-Dichlorobenzene 0.0500 0.05047 mg/Kg 101 70 -130
2,2-Dichloropropane 0.0500 0.04591 mg/Kg 92 70 -130
2-Butanone (MEK)0.250 0.2460 mg/Kg 98 40 -150
2-Chlorotoluene 0.0500 0.04848 mg/Kg 97 70 -130
2-Hexanone 0.250 0.2512 mg/Kg 100 30 -150
4-Chlorotoluene 0.0500 0.04472 mg/Kg 89 70 -130
4-Isopropyltoluene 0.0500 0.04862 mg/Kg 97 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2495 mg/Kg 100 34 -150
Acetone 0.250 0.2536 mg/Kg 101 10 -150
Benzene 0.0500 0.04766 mg/Kg 95 70 -130
Bromobenzene 0.0500 0.04606 mg/Kg 92 70 -130
Bromoform 0.0500 0.04420 mg/Kg 88 68 -130
Bromomethane 0.0500 0.06740 *+mg/Kg 135 70 -130
Carbon disulfide 0.0500 0.04560 mg/Kg 91 70 -130
Carbon tetrachloride 0.0500 0.04292 mg/Kg 86 70 -130
Chlorobenzene 0.0500 0.04770 mg/Kg 95 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732966/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
Chlorobromomethane 0.0500 0.04570 mg/Kg 91 66 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chlorodibromomethane 0.0500 0.04655 mg/Kg 93 64 -133
Chloroethane 0.0500 0.05657 mg/Kg 113 70 -130
Chloroform 0.0500 0.04848 mg/Kg 97 70 -130
Chloromethane 0.0500 0.04513 mg/Kg 90 70 -130
cis-1,2-Dichloroethene 0.0500 0.04940 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04867 mg/Kg 97 70 -130
Dibromomethane 0.0500 0.04657 mg/Kg 93 59 -142
Dichlorobromomethane 0.0500 0.04862 mg/Kg 97 70 -130
Ethyl acetate 0.100 0.09874 mg/Kg 99 70 -130
Ethylbenzene 0.0500 0.04767 mg/Kg 95 70 -130
Ethylene Dibromide 0.0500 0.04640 mg/Kg 93 48 -150
Hexachlorobutadiene 0.0500 0.04671 mg/Kg 93 70 -130
Hexane 0.0500 0.04471 mg/Kg 89 70 -130
Iodomethane 0.0500 0.04759 mg/Kg 95 65 -138
Isopropyl ether 0.0500 0.04844 mg/Kg 97 50 -150
Isopropylbenzene 0.0500 0.04602 mg/Kg 92 70 -130
Methyl tert-butyl ether 0.0500 0.06904 *+mg/Kg 138 70 -130
Methylene Chloride 0.0500 0.04516 mg/Kg 90 54 -149
m-Xylene & p-Xylene 0.0500 0.04770 mg/Kg 95 70 -130
Naphthalene 0.0500 0.05151 mg/Kg 103 46 -150
n-Butylbenzene 0.0500 0.05015 mg/Kg 100 70 -130
n-Heptane 0.0500 0.04295 mg/Kg 86 70 -130
N-Propylbenzene 0.0500 0.04647 mg/Kg 93 70 -130
o-Xylene 0.0500 0.04857 mg/Kg 97 70 -130
sec-Butylbenzene 0.0500 0.04488 mg/Kg 90 69 -142
Styrene 0.0500 0.04657 mg/Kg 93 70 -130
tert-Butylbenzene 0.0500 0.04419 mg/Kg 88 67 -145
Tetrachloroethene 0.0500 0.04660 mg/Kg 93 70 -130
Toluene 0.0500 0.04691 mg/Kg 94 70 -130
trans-1,2-Dichloroethene 0.0500 0.04766 mg/Kg 95 67 -130
trans-1,3-Dichloropropene 0.0500 0.04690 mg/Kg 94 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04708 mg/Kg 94 54 -150
Trichloroethene 0.0500 0.04544 mg/Kg 91 70 -130
Trichlorofluoromethane 0.0500 0.04633 mg/Kg 93 70 -130
Vinyl acetate 0.100 0.1043 mg/Kg 104 53 -150
Vinyl chloride 0.0500 0.04784 mg/Kg 96 70 -130
Xylenes, Total 0.100 0.09627 mg/Kg 96 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
1074-Bromofluorobenzene (Surr)65 -130
97Dibromofluoromethane (Surr)65 -130
100Toluene-d8 (Surr)65 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732966/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
1,1,1,2-Tetrachloroethane 0.0500 0.04672 mg/Kg 93 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04502 mg/Kg 90 70 -130 2 30
1,1,2,2-Tetrachloroethane 0.0500 0.04886 mg/Kg 98 64 -130 2 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04540 mg/Kg 91 70 -130 3 40
1,1,2-Trichloroethane 0.0500 0.04976 mg/Kg 100 56 -146 2 30
1,1-Dichloroethane 0.0500 0.05097 mg/Kg 102 70 -130 4 30
1,1-Dichloroethene 0.0500 0.04669 mg/Kg 93 69 -130 3 50
1,1-Dichloropropene 0.0500 0.04649 mg/Kg 93 70 -130 3 30
1,2,3-Trichlorobenzene 0.0500 0.05173 mg/Kg 103 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.04830 mg/Kg 97 64 -130 5 30
1,2,4-Trichlorobenzene 0.0500 0.05184 mg/Kg 104 70 -130 1 30
1,2,4-Trimethylbenzene 0.0500 0.04605 mg/Kg 92 70 -130 0 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05080 mg/Kg 102 42 -145 7 30
1,2-Dichlorobenzene 0.0500 0.05094 mg/Kg 102 70 -130 3 30
1,2-Dichloroethane 0.0500 0.04975 mg/Kg 100 68 -139 3 30
1,2-Dichloropropane 0.0500 0.05104 mg/Kg 102 70 -130 2 30
1,3,5-Trimethylbenzene 0.0500 0.04545 mg/Kg 91 70 -130 0 30
1,3-Dichlorobenzene 0.0500 0.05141 mg/Kg 103 70 -130 3 30
1,3-Dichloropropane 0.0500 0.04907 mg/Kg 98 54 -150 2 30
1,4-Dichlorobenzene 0.0500 0.05155 mg/Kg 103 70 -130 2 30
2,2-Dichloropropane 0.0500 0.04709 mg/Kg 94 70 -130 3 30
2-Butanone (MEK)0.250 0.2545 mg/Kg 102 40 -150 3 30
2-Chlorotoluene 0.0500 0.04882 mg/Kg 98 70 -130 1 30
2-Hexanone 0.250 0.2618 mg/Kg 105 30 -150 4 30
4-Chlorotoluene 0.0500 0.04549 mg/Kg 91 70 -130 2 30
4-Isopropyltoluene 0.0500 0.04820 mg/Kg 96 70 -130 1 30
4-Methyl-2-pentanone (MIBK)0.250 0.2566 mg/Kg 103 34 -150 3 30
Acetone 0.250 0.2660 mg/Kg 106 10 -150 5 50
Benzene 0.0500 0.04857 mg/Kg 97 70 -130 2 30
Bromobenzene 0.0500 0.04722 mg/Kg 94 70 -130 2 30
Bromoform 0.0500 0.04492 mg/Kg 90 68 -130 2 30
Bromomethane 0.0500 0.06936 *+mg/Kg 139 70 -130 3 30
Carbon disulfide 0.0500 0.04745 mg/Kg 95 70 -130 4 30
Carbon tetrachloride 0.0500 0.04393 mg/Kg 88 70 -130 2 30
Chlorobenzene 0.0500 0.04882 mg/Kg 98 70 -130 2 30
Chlorobromomethane 0.0500 0.04711 mg/Kg 94 66 -130 3 30
Chlorodibromomethane 0.0500 0.04696 mg/Kg 94 64 -133 1 30
Chloroethane 0.0500 0.05826 mg/Kg 117 70 -130 3 30
Chloroform 0.0500 0.04956 mg/Kg 99 70 -130 2 30
Chloromethane 0.0500 0.04590 mg/Kg 92 70 -130 2 30
cis-1,2-Dichloroethene 0.0500 0.05114 mg/Kg 102 70 -130 3 30
cis-1,3-Dichloropropene 0.0500 0.04986 mg/Kg 100 70 -130 2 30
Dibromomethane 0.0500 0.04943 mg/Kg 99 59 -142 6 30
Dichlorobromomethane 0.0500 0.04964 mg/Kg 99 70 -130 2 30
Ethyl acetate 0.100 0.1021 mg/Kg 102 70 -130 3 30
Ethylbenzene 0.0500 0.04913 mg/Kg 98 70 -130 3 30
Ethylene Dibromide 0.0500 0.04744 mg/Kg 95 48 -150 2 30
Hexachlorobutadiene 0.0500 0.04615 mg/Kg 92 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732966/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 732966
Hexane 0.0500 0.04479 mg/Kg 90 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Iodomethane 0.0500 0.05036 mg/Kg 101 65 -138 6 30
Isopropyl ether 0.0500 0.04821 mg/Kg 96 50 -150 0 30
Isopropylbenzene 0.0500 0.04614 mg/Kg 92 70 -130 0 30
Methyl tert-butyl ether 0.0500 0.07013 *+mg/Kg 140 70 -130 2 30
Methylene Chloride 0.0500 0.04644 mg/Kg 93 54 -149 3 30
m-Xylene & p-Xylene 0.0500 0.04920 mg/Kg 98 70 -130 3 30
Naphthalene 0.0500 0.05275 mg/Kg 106 46 -150 2 30
n-Butylbenzene 0.0500 0.05013 mg/Kg 100 70 -130 0 30
n-Heptane 0.0500 0.04350 mg/Kg 87 70 -130 1 30
N-Propylbenzene 0.0500 0.04626 mg/Kg 93 70 -130 0 30
o-Xylene 0.0500 0.04959 mg/Kg 99 70 -130 2 30
sec-Butylbenzene 0.0500 0.04466 mg/Kg 89 69 -142 0 30
Styrene 0.0500 0.04770 mg/Kg 95 70 -130 2 30
tert-Butylbenzene 0.0500 0.04438 mg/Kg 89 67 -145 0 30
Tetrachloroethene 0.0500 0.05099 mg/Kg 102 70 -130 9 30
Toluene 0.0500 0.04786 mg/Kg 96 70 -130 2 30
trans-1,2-Dichloroethene 0.0500 0.04967 mg/Kg 99 67 -130 4 30
trans-1,3-Dichloropropene 0.0500 0.04738 mg/Kg 95 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04930 mg/Kg 99 54 -150 5 30
Trichloroethene 0.0500 0.04651 mg/Kg 93 70 -130 2 30
Trichlorofluoromethane 0.0500 0.04689 mg/Kg 94 70 -130 1 30
Vinyl acetate 0.100 0.1035 mg/Kg 103 53 -150 1 30
Vinyl chloride 0.0500 0.04889 mg/Kg 98 70 -130 2 30
Xylenes, Total 0.100 0.09879 mg/Kg 99 70 -130 3 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
1114-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 08/01/22 16:03 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 08/01/22 16:03 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 08/01/22 16:03 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 08/01/22 16:03 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 08/01/22 16:03 11,2,4-Trichlorobenzene
Eurofins Savannah
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
1,2,4-Trimethylbenzene ND 0.00500 0.00250 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001600.0100 mg/Kg 08/01/22 16:03 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 08/01/22 16:03 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 08/01/22 16:03 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 08/01/22 16:03 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 08/01/22 16:03 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 08/01/22 16:03 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 08/01/22 16:03 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 08/01/22 16:03 12-Hexanone
ND 0.002100.00500 mg/Kg 08/01/22 16:03 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 08/01/22 16:03 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 08/01/22 16:03 1Acetone
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Benzene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Bromobenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Bromoform
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Bromomethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Carbon disulfide
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 08/01/22 16:03 1Chlorobenzene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Chloroethane
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Chloroform
ND 0.002400.00500 mg/Kg 08/01/22 16:03 1Chloromethane
ND 0.002900.00500 mg/Kg 08/01/22 16:03 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Dibromomethane
ND 0.002000.00500 mg/Kg 08/01/22 16:03 1Dichlorobromomethane
ND 0.01000.0100 mg/Kg 08/01/22 16:03 1Ethyl acetate
ND 0.002100.00500 mg/Kg 08/01/22 16:03 1Ethylbenzene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 08/01/22 16:03 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Hexane
ND 0.001700.00500 mg/Kg 08/01/22 16:03 1Iodomethane
ND 0.001500.0100 mg/Kg 08/01/22 16:03 1Isopropyl ether
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 08/01/22 16:03 1Methylene Chloride
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1m-Xylene & p-Xylene
ND 0.003100.00500 mg/Kg 08/01/22 16:03 1Naphthalene
ND 0.001900.00500 mg/Kg 08/01/22 16:03 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 08/01/22 16:03 1n-Heptane
ND 0.002200.00500 mg/Kg 08/01/22 16:03 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 1o-Xylene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733530/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
RL MDL
sec-Butylbenzene ND 0.00500 0.00200 mg/Kg 08/01/22 16:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001900.00500 mg/Kg 08/01/22 16:03 1Styrene
ND 0.002500.00500 mg/Kg 08/01/22 16:03 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1Toluene
ND 0.002300.00500 mg/Kg 08/01/22 16:03 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 08/01/22 16:03 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 08/01/22 16:03 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 08/01/22 16:03 1Trichloroethene
ND 0.003100.00500 mg/Kg 08/01/22 16:03 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 08/01/22 16:03 1Vinyl acetate
ND 0.002800.00500 mg/Kg 08/01/22 16:03 1Vinyl chloride
ND 0.003600.0100 mg/Kg 08/01/22 16:03 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)107 65-130 08/01/22 16:03 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 08/01/22 16:03 14-Bromofluorobenzene (Surr)65-130
104 08/01/22 16:03 1Dibromofluoromethane (Surr)65-130
100 08/01/22 16:03 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,1,1,2-Tetrachloroethane 0.0500 0.05364 mg/Kg 107 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04891 mg/Kg 98 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05396 mg/Kg 108 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04828 mg/Kg 97 70 -130
1,1,2-Trichloroethane 0.0500 0.04954 mg/Kg 99 56 -146
1,1-Dichloroethane 0.0500 0.05002 mg/Kg 100 70 -130
1,1-Dichloroethene 0.0500 0.05195 mg/Kg 104 69 -130
1,1-Dichloropropene 0.0500 0.04947 mg/Kg 99 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05339 mg/Kg 107 70 -130
1,2,3-Trichloropropane 0.0500 0.05563 mg/Kg 111 64 -130
1,2,4-Trichlorobenzene 0.0500 0.04933 mg/Kg 99 70 -130
1,2,4-Trimethylbenzene 0.0500 0.05678 mg/Kg 114 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.05425 mg/Kg 108 42 -145
1,2-Dichlorobenzene 0.0500 0.05019 mg/Kg 100 70 -130
1,2-Dichloroethane 0.0500 0.05031 mg/Kg 101 68 -139
1,2-Dichloropropane 0.0500 0.05287 mg/Kg 106 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05632 mg/Kg 113 70 -130
1,3-Dichlorobenzene 0.0500 0.04927 mg/Kg 99 70 -130
1,3-Dichloropropane 0.0500 0.05070 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.04842 mg/Kg 97 70 -130
2,2-Dichloropropane 0.0500 0.05024 mg/Kg 100 70 -130
2-Butanone (MEK)0.250 0.2579 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.05567 mg/Kg 111 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
2-Hexanone 0.250 0.2323 mg/Kg 93 30 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
4-Chlorotoluene 0.0500 0.05476 mg/Kg 110 70 -130
4-Isopropyltoluene 0.0500 0.04969 mg/Kg 99 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2506 mg/Kg 100 34 -150
Acetone 0.250 0.2474 mg/Kg 99 10 -150
Benzene 0.0500 0.05006 mg/Kg 100 70 -130
Bromobenzene 0.0500 0.05549 mg/Kg 111 70 -130
Bromoform 0.0500 0.05532 mg/Kg 111 68 -130
Bromomethane 0.0500 0.05517 mg/Kg 110 70 -130
Carbon disulfide 0.0500 0.05260 mg/Kg 105 70 -130
Carbon tetrachloride 0.0500 0.04800 mg/Kg 96 70 -130
Chlorobenzene 0.0500 0.05045 mg/Kg 101 70 -130
Chlorobromomethane 0.0500 0.05102 mg/Kg 102 66 -130
Chlorodibromomethane 0.0500 0.05252 mg/Kg 105 64 -133
Chloroethane 0.0500 0.04867 mg/Kg 97 70 -130
Chloroform 0.0500 0.04878 mg/Kg 98 70 -130
Chloromethane 0.0500 0.05148 mg/Kg 103 70 -130
cis-1,2-Dichloroethene 0.0500 0.05026 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.05236 mg/Kg 105 70 -130
Dibromomethane 0.0500 0.05195 mg/Kg 104 59 -142
Dichlorobromomethane 0.0500 0.05096 mg/Kg 102 70 -130
Ethylbenzene 0.0500 0.04886 mg/Kg 98 70 -130
Ethylene Dibromide 0.0500 0.04980 mg/Kg 100 48 -150
Hexachlorobutadiene 0.0500 0.04698 mg/Kg 94 70 -130
Hexane 0.0500 0.04527 mg/Kg 91 70 -130
Iodomethane 0.0500 0.05813 mg/Kg 116 65 -138
Isopropylbenzene 0.0500 0.05148 mg/Kg 103 70 -130
Methyl tert-butyl ether 0.0500 0.05181 mg/Kg 104 70 -130
Methylene Chloride 0.0500 0.05051 mg/Kg 101 54 -149
m-Xylene & p-Xylene 0.0500 0.04874 mg/Kg 97 70 -130
Naphthalene 0.0500 0.05456 mg/Kg 109 46 -150
n-Butylbenzene 0.0500 0.04887 mg/Kg 98 70 -130
n-Heptane 0.0500 0.04806 mg/Kg 96 70 -130
N-Propylbenzene 0.0500 0.05337 mg/Kg 107 70 -130
o-Xylene 0.0500 0.04868 mg/Kg 97 70 -130
sec-Butylbenzene 0.0500 0.05572 mg/Kg 111 69 -142
Styrene 0.0500 0.04754 mg/Kg 95 70 -130
tert-Butylbenzene 0.0500 0.05513 mg/Kg 110 67 -145
Tetrachloroethene 0.0500 0.05030 mg/Kg 101 70 -130
Toluene 0.0500 0.04913 mg/Kg 98 70 -130
trans-1,2-Dichloroethene 0.0500 0.05019 mg/Kg 100 67 -130
trans-1,3-Dichloropropene 0.0500 0.05309 mg/Kg 106 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.05589 mg/Kg 112 54 -150
Trichloroethene 0.0500 0.04892 mg/Kg 98 70 -130
Trichlorofluoromethane 0.0500 0.05250 mg/Kg 105 70 -130
Vinyl acetate 0.100 0.1517 *+mg/Kg 152 53 -150
Vinyl chloride 0.0500 0.05026 mg/Kg 101 70 -130
Xylenes, Total 0.100 0.09742 mg/Kg 97 70 -130
Eurofins Savannah
Page 60 of 96 8/4/2022
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733530/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)65 -130
102Dibromofluoromethane (Surr)65 -130
112Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733530/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
1,1,1,2-Tetrachloroethane 0.0500 0.05256 mg/Kg 105 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04881 mg/Kg 98 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05128 mg/Kg 103 64 -130 5 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04933 mg/Kg 99 70 -130 2 40
1,1,2-Trichloroethane 0.0500 0.04936 mg/Kg 99 56 -146 0 30
1,1-Dichloroethane 0.0500 0.05000 mg/Kg 100 70 -130 0 30
1,1-Dichloroethene 0.0500 0.05186 mg/Kg 104 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04971 mg/Kg 99 70 -130 0 30
1,2,3-Trichlorobenzene 0.0500 0.05796 mg/Kg 116 70 -130 8 30
1,2,3-Trichloropropane 0.0500 0.05149 mg/Kg 103 64 -130 8 30
1,2,4-Trichlorobenzene 0.0500 0.05063 mg/Kg 101 70 -130 3 30
1,2,4-Trimethylbenzene 0.0500 0.05062 mg/Kg 101 70 -130 11 30
1,2-Dibromo-3-Chloropropane 0.0500 0.06249 mg/Kg 125 42 -145 14 30
1,2-Dichlorobenzene 0.0500 0.05143 mg/Kg 103 70 -130 2 30
1,2-Dichloroethane 0.0500 0.04978 mg/Kg 100 68 -139 1 30
1,2-Dichloropropane 0.0500 0.04694 mg/Kg 94 70 -130 12 30
1,3,5-Trimethylbenzene 0.0500 0.04973 mg/Kg 99 70 -130 12 30
1,3-Dichlorobenzene 0.0500 0.05112 mg/Kg 102 70 -130 4 30
1,3-Dichloropropane 0.0500 0.05008 mg/Kg 100 54 -150 1 30
1,4-Dichlorobenzene 0.0500 0.05018 mg/Kg 100 70 -130 4 30
2,2-Dichloropropane 0.0500 0.05007 mg/Kg 100 70 -130 0 30
2-Butanone (MEK)0.250 0.2591 mg/Kg 104 40 -150 0 30
2-Chlorotoluene 0.0500 0.05079 mg/Kg 102 70 -130 9 30
2-Hexanone 0.250 0.2409 mg/Kg 96 30 -150 4 30
4-Chlorotoluene 0.0500 0.04929 mg/Kg 99 70 -130 10 30
4-Isopropyltoluene 0.0500 0.05106 mg/Kg 102 70 -130 3 30
4-Methyl-2-pentanone (MIBK)0.250 0.2527 mg/Kg 101 34 -150 1 30
Acetone 0.250 0.2457 mg/Kg 98 10 -150 1 50
Benzene 0.0500 0.05027 mg/Kg 101 70 -130 0 30
Bromobenzene 0.0500 0.05144 mg/Kg 103 70 -130 8 30
Bromoform 0.0500 0.05109 mg/Kg 102 68 -130 8 30
Bromomethane 0.0500 0.05582 mg/Kg 112 70 -130 1 30
Carbon disulfide 0.0500 0.05263 mg/Kg 105 70 -130 0 30
Carbon tetrachloride 0.0500 0.04842 mg/Kg 97 70 -130 1 30
Chlorobenzene 0.0500 0.05072 mg/Kg 101 70 -130 1 30
Chlorobromomethane 0.0500 0.05139 mg/Kg 103 66 -130 1 30
Chlorodibromomethane 0.0500 0.05280 mg/Kg 106 64 -133 1 30
Chloroethane 0.0500 0.04629 mg/Kg 93 70 -130 5 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733530/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733530
Chloroform 0.0500 0.04968 mg/Kg 99 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 0.0500 0.05074 mg/Kg 101 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.04990 mg/Kg 100 70 -130 1 30
cis-1,3-Dichloropropene 0.0500 0.04839 mg/Kg 97 70 -130 8 30
Dibromomethane 0.0500 0.04707 mg/Kg 94 59 -142 10 30
Dichlorobromomethane 0.0500 0.04786 mg/Kg 96 70 -130 6 30
Ethylbenzene 0.0500 0.05128 mg/Kg 103 70 -130 5 30
Ethylene Dibromide 0.0500 0.05028 mg/Kg 101 48 -150 1 30
Hexachlorobutadiene 0.0500 0.05258 mg/Kg 105 70 -130 11 30
Hexane 0.0500 0.04551 mg/Kg 91 70 -130 1 30
Iodomethane 0.0500 0.05928 mg/Kg 119 65 -138 2 30
Isopropylbenzene 0.0500 0.05059 mg/Kg 101 70 -130 2 30
Methyl tert-butyl ether 0.0500 0.05209 mg/Kg 104 70 -130 1 30
Methylene Chloride 0.0500 0.05073 mg/Kg 101 54 -149 0 30
m-Xylene & p-Xylene 0.0500 0.04939 mg/Kg 99 70 -130 1 30
Naphthalene 0.0500 0.05501 mg/Kg 110 46 -150 1 30
n-Butylbenzene 0.0500 0.04969 mg/Kg 99 70 -130 2 30
n-Heptane 0.0500 0.05038 mg/Kg 101 70 -130 5 30
N-Propylbenzene 0.0500 0.04992 mg/Kg 100 70 -130 7 30
o-Xylene 0.0500 0.04977 mg/Kg 100 70 -130 2 30
sec-Butylbenzene 0.0500 0.05184 mg/Kg 104 69 -142 7 30
Styrene 0.0500 0.04862 mg/Kg 97 70 -130 2 30
tert-Butylbenzene 0.0500 0.05145 mg/Kg 103 67 -145 7 30
Tetrachloroethene 0.0500 0.05258 mg/Kg 105 70 -130 4 30
Toluene 0.0500 0.04899 mg/Kg 98 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.05101 mg/Kg 102 67 -130 2 30
trans-1,3-Dichloropropene 0.0500 0.05242 mg/Kg 105 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04913 mg/Kg 98 54 -150 13 30
Trichloroethene 0.0500 0.04895 mg/Kg 98 70 -130 0 30
Trichlorofluoromethane 0.0500 0.05228 mg/Kg 105 70 -130 0 30
Vinyl acetate 0.100 0.1490 mg/Kg 149 53 -150 2 30
Vinyl chloride 0.0500 0.04991 mg/Kg 100 70 -130 1 30
Xylenes, Total 0.100 0.09916 mg/Kg 99 70 -130 2 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)65 -130
103Dibromofluoromethane (Surr)65 -130
97Toluene-d8 (Surr)65 -130
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1900.500 ug/L 08/03/22 17:40 11,1,1-Trichloroethane
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
1,1,2,2-Tetrachloroethane ND 0.500 0.100 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1400.500 ug/L 08/03/22 17:40 11,1,2-Trichloroethane
ND 0.1800.500 ug/L 08/03/22 17:40 11,1-Dichloroethane
ND 0.1800.500 ug/L 08/03/22 17:40 11,1-Dichloroethene
ND 0.2000.500 ug/L 08/03/22 17:40 11,1-Dichloropropene
ND 0.7701.00 ug/L 08/03/22 17:40 11,2,3-Trichlorobenzene
ND 0.1200.500 ug/L 08/03/22 17:40 11,2,3-Trichloropropane
ND 0.3500.500 ug/L 08/03/22 17:40 11,2,4-Trichlorobenzene
ND 0.1400.500 ug/L 08/03/22 17:40 11,2,4-Trimethylbenzene
ND 0.1200.500 ug/L 08/03/22 17:40 11,2-Dichlorobenzene
ND 0.1600.500 ug/L 08/03/22 17:40 11,2-Dichloroethane
ND 0.2300.500 ug/L 08/03/22 17:40 11,2-Dichloroethene, Total
ND 0.1600.500 ug/L 08/03/22 17:40 11,2-Dichloropropane
ND 0.1600.500 ug/L 08/03/22 17:40 11,3,5-Trimethylbenzene
ND 0.1600.500 ug/L 08/03/22 17:40 11,3-Dichlorobenzene
ND 0.1400.500 ug/L 08/03/22 17:40 11,3-Dichloropropane
ND 0.2200.500 ug/L 08/03/22 17:40 11,3-Dichloropropene, Total
ND 0.1200.500 ug/L 08/03/22 17:40 11,4-Dichlorobenzene
ND 0.1800.500 ug/L 08/03/22 17:40 12,2-Dichloropropane
ND 5.2010.0 ug/L 08/03/22 17:40 12-Butanone (MEK)
ND 0.1600.500 ug/L 08/03/22 17:40 12-Chlorotoluene
ND 5.0010.0 ug/L 08/03/22 17:40 12-Hexanone
ND 9.1020.0 ug/L 08/03/22 17:40 13,3-Dimethyl-1-butanol
ND 0.1600.500 ug/L 08/03/22 17:40 14-Chlorotoluene
ND 0.1800.500 ug/L 08/03/22 17:40 14-Isopropyltoluene
ND 5.2010.0 ug/L 08/03/22 17:40 14-Methyl-2-pentanone (MIBK)
ND 5.6020.0 ug/L 08/03/22 17:40 1Acetone
ND 0.1800.500 ug/L 08/03/22 17:40 1Benzene
ND 0.1400.500 ug/L 08/03/22 17:40 1Bromobenzene
ND 0.1800.500 ug/L 08/03/22 17:40 1Bromoform
ND 2.305.00 ug/L 08/03/22 17:40 1Bromomethane
ND 0.2200.500 ug/L 08/03/22 17:40 1Carbon tetrachloride
ND 0.1600.500 ug/L 08/03/22 17:40 1Chlorobenzene
ND 0.1300.500 ug/L 08/03/22 17:40 1Chlorobromomethane
ND 0.4601.00 ug/L 08/03/22 17:40 1Chlorodibromomethane
ND 4.1010.0 ug/L 08/03/22 17:40 1Chloroethane
ND 0.3800.500 ug/L 08/03/22 17:40 1Chloroform
ND 0.1000.500 ug/L 08/03/22 17:40 1Chloromethane
ND 0.06400.500 ug/L 08/03/22 17:40 1cis-1,2-Dichloroethene
ND 0.1100.500 ug/L 08/03/22 17:40 1cis-1,3-Dichloropropene
ND 0.1700.500 ug/L 08/03/22 17:40 1Dibromomethane
ND 0.4101.00 ug/L 08/03/22 17:40 1Dichlorobromomethane
ND 0.09100.500 ug/L 08/03/22 17:40 1Dichlorodifluoromethane
ND 0.1400.500 ug/L 08/03/22 17:40 1Dichlorofluoromethane
ND 140200 ug/L 08/03/22 17:40 1Ethanol
ND 0.09200.500 ug/L 08/03/22 17:40 1Ethyl ether
ND 0.1700.500 ug/L 08/03/22 17:40 1Ethylbenzene
ND 0.1700.500 ug/L 08/03/22 17:40 1Ethylene Dibromide
ND 0.05800.500 ug/L 08/03/22 17:40 1Isopropyl ether
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-733831/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
RL MDL
Isopropylbenzene ND 0.500 0.180 ug/L 08/03/22 17:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1100.500 ug/L 08/03/22 17:40 1Methyl tert-butyl ether
ND 0.1500.500 ug/L 08/03/22 17:40 1Methylene Chloride
ND 0.1800.500 ug/L 08/03/22 17:40 1m-Xylene & p-Xylene
ND 1.202.00 ug/L 08/03/22 17:40 1Naphthalene
ND 0.1601.00 ug/L 08/03/22 17:40 1n-Butylbenzene
ND 0.1800.500 ug/L 08/03/22 17:40 1N-Propylbenzene
ND 0.1500.500 ug/L 08/03/22 17:40 1o-Xylene
ND 0.1701.00 ug/L 08/03/22 17:40 1sec-Butylbenzene
ND 0.1700.500 ug/L 08/03/22 17:40 1Styrene
ND 1.905.00 ug/L 08/03/22 17:40 1t-Amyl alcohol
ND 0.07900.500 ug/L 08/03/22 17:40 1Tert-amyl methyl ether
ND 0.05800.500 ug/L 08/03/22 17:40 1Tert-butyl ethyl ether
ND 1.765.00 ug/L 08/03/22 17:40 1tert-Butyl Formate
ND 0.1800.500 ug/L 08/03/22 17:40 1tert-Butylbenzene
ND 0.2200.500 ug/L 08/03/22 17:40 1Tetrachloroethene
ND 0.2000.500 ug/L 08/03/22 17:40 1Toluene
ND 0.1700.500 ug/L 08/03/22 17:40 1trans-1,2-Dichloroethene
ND 0.1200.500 ug/L 08/03/22 17:40 1trans-1,3-Dichloropropene
ND 0.2000.500 ug/L 08/03/22 17:40 1Trichloroethene
ND 0.1400.500 ug/L 08/03/22 17:40 1Trichlorofluoromethane
ND 0.6401.00 ug/L 08/03/22 17:40 1Vinyl acetate
ND 0.1200.500 ug/L 08/03/22 17:40 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr)97 70-130 08/03/22 17:40 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 08/03/22 17:40 14-Bromofluorobenzene (Surr)70-130
99 08/03/22 17:40 1Dibromofluoromethane (Surr)70-130
106 08/03/22 17:40 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,1,1,2-Tetrachloroethane 25.0 26.90 ug/L 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 25.0 25.17 ug/L 101 70 -130
1,1,2,2-Tetrachloroethane 25.0 25.43 ug/L 102 70 -130
1,1,2-Trichloroethane 25.0 23.62 ug/L 94 70 -130
1,1-Dichloroethane 25.0 23.66 ug/L 95 70 -130
1,1-Dichloroethene 25.0 24.97 ug/L 100 70 -130
1,1-Dichloropropene 25.0 24.02 ug/L 96 70 -130
1,2,3-Trichlorobenzene 25.0 25.19 ug/L 101 70 -130
1,2,3-Trichloropropane 25.0 25.16 ug/L 101 70 -130
1,2,4-Trichlorobenzene 25.0 24.93 ug/L 100 70 -130
1,2,4-Trimethylbenzene 25.0 25.79 ug/L 103 70 -130
1,2-Dichlorobenzene 25.0 24.90 ug/L 100 70 -130
1,2-Dichloroethane 25.0 23.26 ug/L 93 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,2-Dichloroethene, Total 50.0 48.31 ug/L 97 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloropropane 25.0 23.55 ug/L 94 70 -130
1,3,5-Trimethylbenzene 25.0 25.96 ug/L 104 70 -130
1,3-Dichlorobenzene 25.0 25.48 ug/L 102 70 -130
1,3-Dichloropropane 25.0 23.65 ug/L 95 70 -130
1,3-Dichloropropene, Total 50.0 52.38 ug/L 105 70 -130
1,4-Dichlorobenzene 25.0 24.93 ug/L 100 70 -130
2,2-Dichloropropane 25.0 26.04 ug/L 104 70 -130
2-Butanone (MEK)125 117.6 ug/L 94 70 -130
2-Chlorotoluene 25.0 25.51 ug/L 102 70 -130
2-Hexanone 125 122.8 ug/L 98 70 -130
3,3-Dimethyl-1-butanol 100 104.7 ug/L 105 70 -130
4-Chlorotoluene 25.0 25.27 ug/L 101 70 -130
4-Isopropyltoluene 25.0 26.64 ug/L 107 70 -130
4-Methyl-2-pentanone (MIBK)125 121.7 ug/L 97 70 -130
Acetone 125 123.8 ug/L 99 70 -130
Benzene 25.0 23.49 ug/L 94 70 -130
Bromobenzene 25.0 25.57 ug/L 102 70 -130
Bromoform 25.0 29.65 ug/L 119 70 -130
Bromomethane 25.0 29.14 ug/L 117 70 -130
Carbon tetrachloride 25.0 25.63 ug/L 103 70 -130
Chlorobenzene 25.0 24.44 ug/L 98 70 -130
Chlorobromomethane 25.0 24.42 ug/L 98 70 -130
Chlorodibromomethane 25.0 26.79 ug/L 107 70 -130
Chloroethane 25.0 25.13 ug/L 101 70 -130
Chloroform 25.0 24.24 ug/L 97 70 -130
Chloromethane 25.0 23.42 ug/L 94 70 -130
cis-1,2-Dichloroethene 25.0 23.84 ug/L 95 70 -130
cis-1,3-Dichloropropene 25.0 26.05 ug/L 104 70 -130
Dibromomethane 25.0 24.62 ug/L 98 70 -130
Dichlorobromomethane 25.0 25.80 ug/L 103 70 -130
Dichlorodifluoromethane 25.0 23.10 ug/L 92 70 -130
Dichlorofluoromethane 25.0 24.12 ug/L 96 70 -130
Ethanol 1000 929.0 ug/L 93 70 -130
Ethyl ether 25.0 23.87 ug/L 95 70 -130
Ethylbenzene 25.0 25.76 ug/L 103 70 -130
Ethylene Dibromide 25.0 24.74 ug/L 99 70 -130
Isopropyl ether 25.0 23.37 ug/L 93 70 -130
Isopropylbenzene 25.0 26.64 ug/L 107 70 -130
Methyl tert-butyl ether 25.0 24.24 ug/L 97 70 -130
Methylene Chloride 25.0 24.67 ug/L 99 70 -130
m-Xylene & p-Xylene 25.0 25.64 ug/L 103 70 -130
Naphthalene 25.0 26.46 ug/L 106 70 -130
n-Butylbenzene 25.0 25.62 ug/L 102 70 -130
N-Propylbenzene 25.0 25.91 ug/L 104 70 -130
o-Xylene 25.0 25.80 ug/L 103 70 -130
sec-Butylbenzene 25.0 26.67 ug/L 107 70 -130
Styrene 25.0 26.73 ug/L 107 70 -130
t-Amyl alcohol 250 234.3 ug/L 94 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733831/1015
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
Tert-amyl methyl ether 25.0 24.56 ug/L 98 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Tert-butyl ethyl ether 25.0 24.47 ug/L 98 70 -130
tert-Butyl Formate 100 107.5 ug/L 107 70 -130
tert-Butylbenzene 25.0 26.34 ug/L 105 70 -130
Tetrachloroethene 25.0 24.19 ug/L 97 70 -130
Toluene 25.0 23.94 ug/L 96 70 -130
trans-1,2-Dichloroethene 25.0 24.47 ug/L 98 70 -130
trans-1,3-Dichloropropene 25.0 26.33 ug/L 105 70 -130
Trichloroethene 25.0 24.54 ug/L 98 70 -130
Trichlorofluoromethane 25.0 25.84 ug/L 103 70 -130
Vinyl acetate 50.0 51.35 ug/L 103 70 -130
Vinyl chloride 25.0 22.84 ug/L 91 70 -130
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
1,1,1,2-Tetrachloroethane 25.0 26.45 ug/L 106 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 25.0 24.30 ug/L 97 70 -130 3 30
1,1,2,2-Tetrachloroethane 25.0 24.94 ug/L 100 70 -130 2 30
1,1,2-Trichloroethane 25.0 23.41 ug/L 94 70 -130 1 30
1,1-Dichloroethane 25.0 23.04 ug/L 92 70 -130 3 30
1,1-Dichloroethene 25.0 24.25 ug/L 97 70 -130 3 30
1,1-Dichloropropene 25.0 22.95 ug/L 92 70 -130 5 30
1,2,3-Trichlorobenzene 25.0 25.47 ug/L 102 70 -130 1 30
1,2,3-Trichloropropane 25.0 24.92 ug/L 100 70 -130 1 30
1,2,4-Trichlorobenzene 25.0 24.77 ug/L 99 70 -130 1 30
1,2,4-Trimethylbenzene 25.0 25.73 ug/L 103 70 -130 0 50
1,2-Dichlorobenzene 25.0 24.50 ug/L 98 70 -130 2 30
1,2-Dichloroethane 25.0 23.19 ug/L 93 70 -130 0 30
1,2-Dichloroethene, Total 50.0 46.76 ug/L 94 70 -130 3 30
1,2-Dichloropropane 25.0 23.01 ug/L 92 70 -130 2 30
1,3,5-Trimethylbenzene 25.0 25.65 ug/L 103 70 -130 1 50
1,3-Dichlorobenzene 25.0 24.82 ug/L 99 70 -130 3 30
1,3-Dichloropropane 25.0 23.45 ug/L 94 70 -130 1 30
1,3-Dichloropropene, Total 50.0 51.38 ug/L 103 70 -130 2 50
1,4-Dichlorobenzene 25.0 24.48 ug/L 98 70 -130 2 30
2,2-Dichloropropane 25.0 24.94 ug/L 100 70 -130 4 30
2-Butanone (MEK)125 116.6 ug/L 93 70 -130 1 30
2-Chlorotoluene 25.0 24.76 ug/L 99 70 -130 3 30
2-Hexanone 125 123.6 ug/L 99 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
3,3-Dimethyl-1-butanol 100 107.4 ug/L 107 70 -130 3
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 25.0 24.91 ug/L 100 70 -130 1 30
4-Isopropyltoluene 25.0 25.69 ug/L 103 70 -130 4 50
4-Methyl-2-pentanone (MIBK)125 121.2 ug/L 97 70 -130 0 30
Acetone 125 123.1 ug/L 98 70 -130 1 50
Benzene 25.0 22.81 ug/L 91 70 -130 3 30
Bromobenzene 25.0 25.16 ug/L 101 70 -130 2 30
Bromoform 25.0 29.61 ug/L 118 70 -130 0 30
Bromomethane 25.0 27.65 ug/L 111 70 -130 5 50
Carbon tetrachloride 25.0 24.53 ug/L 98 70 -130 4 30
Chlorobenzene 25.0 23.69 ug/L 95 70 -130 3 30
Chlorobromomethane 25.0 23.56 ug/L 94 70 -130 4 30
Chlorodibromomethane 25.0 26.51 ug/L 106 70 -130 1 50
Chloroethane 25.0 23.65 ug/L 95 70 -130 6 40
Chloroform 25.0 23.39 ug/L 94 70 -130 4 30
Chloromethane 25.0 22.86 ug/L 91 70 -130 2 30
cis-1,2-Dichloroethene 25.0 22.96 ug/L 92 70 -130 4 30
cis-1,3-Dichloropropene 25.0 25.56 ug/L 102 70 -130 2 30
Dibromomethane 25.0 24.14 ug/L 97 70 -130 2 30
Dichlorobromomethane 25.0 25.46 ug/L 102 70 -130 1 30
Dichlorodifluoromethane 25.0 22.45 ug/L 90 70 -130 3 50
Dichlorofluoromethane 25.0 23.20 ug/L 93 70 -130 4 50
Ethanol 1000 936.3 ug/L 94 70 -130 1 50
Ethyl ether 25.0 23.59 ug/L 94 70 -130 1 50
Ethylbenzene 25.0 24.83 ug/L 99 70 -130 4 30
Ethylene Dibromide 25.0 24.37 ug/L 97 70 -130 2 30
Isopropyl ether 25.0 23.06 ug/L 92 70 -130 1 50
Isopropylbenzene 25.0 25.52 ug/L 102 70 -130 4 30
Methyl tert-butyl ether 25.0 24.30 ug/L 97 70 -130 0 30
Methylene Chloride 25.0 24.06 ug/L 96 70 -130 3 30
m-Xylene & p-Xylene 25.0 24.97 ug/L 100 70 -130 3 30
Naphthalene 25.0 27.18 ug/L 109 70 -130 3 30
n-Butylbenzene 25.0 24.86 ug/L 99 70 -130 3 30
N-Propylbenzene 25.0 25.07 ug/L 100 70 -130 3 30
o-Xylene 25.0 25.25 ug/L 101 70 -130 2 30
sec-Butylbenzene 25.0 25.91 ug/L 104 70 -130 3 30
Styrene 25.0 26.10 ug/L 104 70 -130 2 30
t-Amyl alcohol 250 234.8 ug/L 94 70 -130 0 30
Tert-amyl methyl ether 25.0 24.52 ug/L 98 70 -130 0 30
Tert-butyl ethyl ether 25.0 24.23 ug/L 97 70 -130 1 30
tert-Butyl Formate 100 105.0 ug/L 105 70 -130 2
tert-Butylbenzene 25.0 25.61 ug/L 102 70 -130 3 30
Tetrachloroethene 25.0 23.24 ug/L 93 70 -130 4 30
Toluene 25.0 23.17 ug/L 93 70 -130 3 30
trans-1,2-Dichloroethene 25.0 23.81 ug/L 95 70 -130 3 30
trans-1,3-Dichloropropene 25.0 25.82 ug/L 103 70 -130 2 50
Trichloroethene 25.0 23.77 ug/L 95 70 -130 3 30
Trichlorofluoromethane 25.0 24.75 ug/L 99 70 -130 4 30
Vinyl acetate 50.0 48.06 ug/L 96 70 -130 7 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733831/16
Matrix: Water Prep Type: Total/NA
Analysis Batch: 733831
Vinyl chloride 25.0 22.21 ug/L 89 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)70 -130
99Dibromofluoromethane (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-734030/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
RL MDL
1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/04/22 11:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1900.500 ug/L 08/04/22 11:08 11,1,1-Trichloroethane
ND 0.1000.500 ug/L 08/04/22 11:08 11,1,2,2-Tetrachloroethane
ND 0.1400.500 ug/L 08/04/22 11:08 11,1,2-Trichloroethane
ND 0.1800.500 ug/L 08/04/22 11:08 11,1-Dichloroethane
ND 0.1800.500 ug/L 08/04/22 11:08 11,1-Dichloroethene
ND 0.2000.500 ug/L 08/04/22 11:08 11,1-Dichloropropene
ND 0.7701.00 ug/L 08/04/22 11:08 11,2,3-Trichlorobenzene
ND 0.1200.500 ug/L 08/04/22 11:08 11,2,3-Trichloropropane
ND 0.3500.500 ug/L 08/04/22 11:08 11,2,4-Trichlorobenzene
ND 0.1400.500 ug/L 08/04/22 11:08 11,2,4-Trimethylbenzene
ND 0.1200.500 ug/L 08/04/22 11:08 11,2-Dichlorobenzene
ND 0.1600.500 ug/L 08/04/22 11:08 11,2-Dichloroethane
ND 0.2300.500 ug/L 08/04/22 11:08 11,2-Dichloroethene, Total
ND 0.1600.500 ug/L 08/04/22 11:08 11,2-Dichloropropane
ND 0.1600.500 ug/L 08/04/22 11:08 11,3,5-Trimethylbenzene
ND 0.1600.500 ug/L 08/04/22 11:08 11,3-Dichlorobenzene
ND 0.1400.500 ug/L 08/04/22 11:08 11,3-Dichloropropane
ND 0.2200.500 ug/L 08/04/22 11:08 11,3-Dichloropropene, Total
ND 0.1200.500 ug/L 08/04/22 11:08 11,4-Dichlorobenzene
ND 0.1800.500 ug/L 08/04/22 11:08 12,2-Dichloropropane
ND 5.2010.0 ug/L 08/04/22 11:08 12-Butanone (MEK)
ND 0.1600.500 ug/L 08/04/22 11:08 12-Chlorotoluene
ND 5.0010.0 ug/L 08/04/22 11:08 12-Hexanone
ND 9.1020.0 ug/L 08/04/22 11:08 13,3-Dimethyl-1-butanol
ND 0.1600.500 ug/L 08/04/22 11:08 14-Chlorotoluene
ND 0.1800.500 ug/L 08/04/22 11:08 14-Isopropyltoluene
ND 5.2010.0 ug/L 08/04/22 11:08 14-Methyl-2-pentanone (MIBK)
ND 5.6020.0 ug/L 08/04/22 11:08 1Acetone
ND 0.1800.500 ug/L 08/04/22 11:08 1Benzene
ND 0.1400.500 ug/L 08/04/22 11:08 1Bromobenzene
ND 0.1800.500 ug/L 08/04/22 11:08 1Bromoform
ND 2.305.00 ug/L 08/04/22 11:08 1Bromomethane
ND 0.2200.500 ug/L 08/04/22 11:08 1Carbon tetrachloride
ND 0.1600.500 ug/L 08/04/22 11:08 1Chlorobenzene
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-734030/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
RL MDL
Chlorobromomethane ND 0.500 0.130 ug/L 08/04/22 11:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.4601.00 ug/L 08/04/22 11:08 1Chlorodibromomethane
ND 4.1010.0 ug/L 08/04/22 11:08 1Chloroethane
ND 0.3800.500 ug/L 08/04/22 11:08 1Chloroform
ND 0.1000.500 ug/L 08/04/22 11:08 1Chloromethane
ND 0.06400.500 ug/L 08/04/22 11:08 1cis-1,2-Dichloroethene
ND 0.1100.500 ug/L 08/04/22 11:08 1cis-1,3-Dichloropropene
ND 0.1700.500 ug/L 08/04/22 11:08 1Dibromomethane
ND 0.4101.00 ug/L 08/04/22 11:08 1Dichlorobromomethane
ND 0.09100.500 ug/L 08/04/22 11:08 1Dichlorodifluoromethane
ND 0.1400.500 ug/L 08/04/22 11:08 1Dichlorofluoromethane
ND 140200 ug/L 08/04/22 11:08 1Ethanol
ND 0.09200.500 ug/L 08/04/22 11:08 1Ethyl ether
ND 0.1700.500 ug/L 08/04/22 11:08 1Ethylbenzene
ND 0.1700.500 ug/L 08/04/22 11:08 1Ethylene Dibromide
ND 0.05800.500 ug/L 08/04/22 11:08 1Isopropyl ether
ND 0.1800.500 ug/L 08/04/22 11:08 1Isopropylbenzene
ND 0.1100.500 ug/L 08/04/22 11:08 1Methyl tert-butyl ether
ND 0.1500.500 ug/L 08/04/22 11:08 1Methylene Chloride
ND 0.1800.500 ug/L 08/04/22 11:08 1m-Xylene & p-Xylene
ND 1.202.00 ug/L 08/04/22 11:08 1Naphthalene
ND 0.1601.00 ug/L 08/04/22 11:08 1n-Butylbenzene
ND 0.1800.500 ug/L 08/04/22 11:08 1N-Propylbenzene
ND 0.1500.500 ug/L 08/04/22 11:08 1o-Xylene
ND 0.1701.00 ug/L 08/04/22 11:08 1sec-Butylbenzene
ND 0.1700.500 ug/L 08/04/22 11:08 1Styrene
ND 1.905.00 ug/L 08/04/22 11:08 1t-Amyl alcohol
ND 0.07900.500 ug/L 08/04/22 11:08 1Tert-amyl methyl ether
ND 0.05800.500 ug/L 08/04/22 11:08 1Tert-butyl ethyl ether
ND 1.765.00 ug/L 08/04/22 11:08 1tert-Butyl Formate
ND 0.1800.500 ug/L 08/04/22 11:08 1tert-Butylbenzene
ND 0.2200.500 ug/L 08/04/22 11:08 1Tetrachloroethene
ND 0.2000.500 ug/L 08/04/22 11:08 1Toluene
ND 0.1700.500 ug/L 08/04/22 11:08 1trans-1,2-Dichloroethene
ND 0.1200.500 ug/L 08/04/22 11:08 1trans-1,3-Dichloropropene
ND 0.2000.500 ug/L 08/04/22 11:08 1Trichloroethene
ND 0.1400.500 ug/L 08/04/22 11:08 1Trichlorofluoromethane
ND 0.6401.00 ug/L 08/04/22 11:08 1Vinyl acetate
ND 0.1200.500 ug/L 08/04/22 11:08 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr)94 70-130 08/04/22 11:08 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
102 08/04/22 11:08 14-Bromofluorobenzene (Surr)70-130
98 08/04/22 11:08 1Dibromofluoromethane (Surr)70-130
106 08/04/22 11:08 1Toluene-d8 (Surr)70-130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-734030/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,1,1,2-Tetrachloroethane 25.0 26.89 ug/L 108 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 25.0 23.56 ug/L 94 70 -130
1,1,2,2-Tetrachloroethane 25.0 23.19 ug/L 93 70 -130
1,1,2-Trichloroethane 25.0 22.28 ug/L 89 70 -130
1,1-Dichloroethane 25.0 21.87 ug/L 87 70 -130
1,1-Dichloroethene 25.0 23.75 ug/L 95 70 -130
1,1-Dichloropropene 25.0 22.53 ug/L 90 70 -130
1,2,3-Trichlorobenzene 25.0 21.87 ug/L 87 70 -130
1,2,3-Trichloropropane 25.0 23.11 ug/L 92 70 -130
1,2,4-Trichlorobenzene 25.0 23.28 ug/L 93 70 -130
1,2,4-Trimethylbenzene 25.0 24.52 ug/L 98 70 -130
1,2-Dichlorobenzene 25.0 25.04 ug/L 100 70 -130
1,2-Dichloroethane 25.0 21.41 ug/L 86 70 -130
1,2-Dichloroethene, Total 50.0 45.18 ug/L 90 70 -130
1,2-Dichloropropane 25.0 21.89 ug/L 88 70 -130
1,3,5-Trimethylbenzene 25.0 24.59 ug/L 98 70 -130
1,3-Dichlorobenzene 25.0 25.44 ug/L 102 70 -130
1,3-Dichloropropane 25.0 22.12 ug/L 88 70 -130
1,3-Dichloropropene, Total 50.0 49.69 ug/L 99 70 -130
1,4-Dichlorobenzene 25.0 25.00 ug/L 100 70 -130
2,2-Dichloropropane 25.0 25.11 ug/L 100 70 -130
2-Butanone (MEK)125 98.91 ug/L 79 70 -130
2-Chlorotoluene 25.0 24.36 ug/L 97 70 -130
2-Hexanone 125 106.0 ug/L 85 70 -130
3,3-Dimethyl-1-butanol 100 91.11 ug/L 91 70 -130
4-Chlorotoluene 25.0 24.34 ug/L 97 70 -130
4-Isopropyltoluene 25.0 26.37 ug/L 105 70 -130
4-Methyl-2-pentanone (MIBK)125 107.1 ug/L 86 70 -130
Acetone 125 110.7 ug/L 89 70 -130
Benzene 25.0 22.29 ug/L 89 70 -130
Bromobenzene 25.0 25.13 ug/L 101 70 -130
Bromoform 25.0 28.52 ug/L 114 70 -130
Bromomethane 25.0 25.35 ug/L 101 70 -130
Carbon tetrachloride 25.0 24.25 ug/L 97 70 -130
Chlorobenzene 25.0 23.93 ug/L 96 70 -130
Chlorobromomethane 25.0 22.95 ug/L 92 70 -130
Chlorodibromomethane 25.0 25.58 ug/L 102 70 -130
Chloroethane 25.0 22.26 ug/L 89 70 -130
Chloroform 25.0 22.38 ug/L 90 70 -130
Chloromethane 25.0 21.95 ug/L 88 70 -130
cis-1,2-Dichloroethene 25.0 22.11 ug/L 88 70 -130
cis-1,3-Dichloropropene 25.0 24.81 ug/L 99 70 -130
Dibromomethane 25.0 22.72 ug/L 91 70 -130
Dichlorobromomethane 25.0 24.28 ug/L 97 70 -130
Dichlorodifluoromethane 25.0 21.58 ug/L 86 70 -130
Dichlorofluoromethane 25.0 23.65 ug/L 95 70 -130
Ethanol 1000 869.2 ug/L 87 70 -130
Ethyl ether 25.0 21.71 ug/L 87 70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-734030/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
Ethylbenzene 25.0 24.98 ug/L 100 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Ethylene Dibromide 25.0 23.14 ug/L 93 70 -130
Isopropyl ether 25.0 21.80 ug/L 87 70 -130
Isopropylbenzene 25.0 25.68 ug/L 103 70 -130
Methyl tert-butyl ether 25.0 22.01 ug/L 88 70 -130
Methylene Chloride 25.0 23.50 ug/L 94 70 -130
m-Xylene & p-Xylene 25.0 24.88 ug/L 100 70 -130
Naphthalene 25.0 23.26 ug/L 93 70 -130
n-Butylbenzene 25.0 25.51 ug/L 102 70 -130
N-Propylbenzene 25.0 24.83 ug/L 99 70 -130
o-Xylene 25.0 25.07 ug/L 100 70 -130
sec-Butylbenzene 25.0 25.47 ug/L 102 70 -130
Styrene 25.0 25.71 ug/L 103 70 -130
t-Amyl alcohol 250 209.7 ug/L 84 70 -130
Tert-amyl methyl ether 25.0 22.75 ug/L 91 70 -130
Tert-butyl ethyl ether 25.0 22.63 ug/L 91 70 -130
tert-Butyl Formate 100 101.6 ug/L 102 70 -130
tert-Butylbenzene 25.0 25.30 ug/L 101 70 -130
Tetrachloroethene 25.0 23.70 ug/L 95 70 -130
Toluene 25.0 22.70 ug/L 91 70 -130
trans-1,2-Dichloroethene 25.0 23.07 ug/L 92 70 -130
trans-1,3-Dichloropropene 25.0 24.88 ug/L 100 70 -130
Trichloroethene 25.0 23.48 ug/L 94 70 -130
Trichlorofluoromethane 25.0 25.18 ug/L 101 70 -130
Vinyl acetate 50.0 49.11 ug/L 98 70 -130
Vinyl chloride 25.0 22.01 ug/L 88 70 -130
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)70 -130
97Dibromofluoromethane (Surr)70 -130
105Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,1,1,2-Tetrachloroethane 25.0 26.26 ug/L 105 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 25.0 22.96 ug/L 92 70 -130 3 30
1,1,2,2-Tetrachloroethane 25.0 23.63 ug/L 95 70 -130 2 30
1,1,2-Trichloroethane 25.0 22.43 ug/L 90 70 -130 1 30
1,1-Dichloroethane 25.0 21.45 ug/L 86 70 -130 2 30
1,1-Dichloroethene 25.0 22.96 ug/L 92 70 -130 3 30
1,1-Dichloropropene 25.0 21.83 ug/L 87 70 -130 3 30
1,2,3-Trichlorobenzene 25.0 21.83 ug/L 87 70 -130 0 30
1,2,3-Trichloropropane 25.0 23.72 ug/L 95 70 -130 3 30
1,2,4-Trichlorobenzene 25.0 23.02 ug/L 92 70 -130 1 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
1,2,4-Trimethylbenzene 25.0 23.73 ug/L 95 70 -130 3 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichlorobenzene 25.0 24.26 ug/L 97 70 -130 3 30
1,2-Dichloroethane 25.0 21.46 ug/L 86 70 -130 0 30
1,2-Dichloroethene, Total 50.0 44.03 ug/L 88 70 -130 3 30
1,2-Dichloropropane 25.0 21.63 ug/L 87 70 -130 1 30
1,3,5-Trimethylbenzene 25.0 23.94 ug/L 96 70 -130 3 50
1,3-Dichlorobenzene 25.0 24.72 ug/L 99 70 -130 3 30
1,3-Dichloropropane 25.0 22.17 ug/L 89 70 -130 0 30
1,3-Dichloropropene, Total 50.0 49.28 ug/L 99 70 -130 1 50
1,4-Dichlorobenzene 25.0 24.25 ug/L 97 70 -130 3 30
2,2-Dichloropropane 25.0 23.95 ug/L 96 70 -130 5 30
2-Butanone (MEK)125 102.6 ug/L 82 70 -130 4 30
2-Chlorotoluene 25.0 23.75 ug/L 95 70 -130 3 30
2-Hexanone 125 110.5 ug/L 88 70 -130 4 30
3,3-Dimethyl-1-butanol 100 94.43 ug/L 94 70 -130 4
4-Chlorotoluene 25.0 23.51 ug/L 94 70 -130 3 30
4-Isopropyltoluene 25.0 25.37 ug/L 101 70 -130 4 50
4-Methyl-2-pentanone (MIBK)125 110.3 ug/L 88 70 -130 3 30
Acetone 125 111.6 ug/L 89 70 -130 1 50
Benzene 25.0 21.68 ug/L 87 70 -130 3 30
Bromobenzene 25.0 24.63 ug/L 99 70 -130 2 30
Bromoform 25.0 29.30 ug/L 117 70 -130 3 30
Bromomethane 25.0 24.05 ug/L 96 70 -130 5 50
Carbon tetrachloride 25.0 23.38 ug/L 94 70 -130 4 30
Chlorobenzene 25.0 23.53 ug/L 94 70 -130 2 30
Chlorobromomethane 25.0 22.94 ug/L 92 70 -130 0 30
Chlorodibromomethane 25.0 25.46 ug/L 102 70 -130 0 50
Chloroethane 25.0 20.96 ug/L 84 70 -130 6 40
Chloroform 25.0 22.01 ug/L 88 70 -130 2 30
Chloromethane 25.0 21.25 ug/L 85 70 -130 3 30
cis-1,2-Dichloroethene 25.0 21.73 ug/L 87 70 -130 2 30
cis-1,3-Dichloropropene 25.0 24.45 ug/L 98 70 -130 1 30
Dibromomethane 25.0 22.73 ug/L 91 70 -130 0 30
Dichlorobromomethane 25.0 24.06 ug/L 96 70 -130 1 30
Dichlorodifluoromethane 25.0 20.51 ug/L 82 70 -130 5 50
Dichlorofluoromethane 25.0 22.31 ug/L 89 70 -130 6 50
Ethanol 1000 873.2 ug/L 87 70 -130 0 50
Ethyl ether 25.0 21.49 ug/L 86 70 -130 1 50
Ethylbenzene 25.0 24.22 ug/L 97 70 -130 3 30
Ethylene Dibromide 25.0 23.33 ug/L 93 70 -130 1 30
Isopropyl ether 25.0 21.66 ug/L 87 70 -130 1 50
Isopropylbenzene 25.0 25.06 ug/L 100 70 -130 2 30
Methyl tert-butyl ether 25.0 22.24 ug/L 89 70 -130 1 30
Methylene Chloride 25.0 23.01 ug/L 92 70 -130 2 30
m-Xylene & p-Xylene 25.0 24.31 ug/L 97 70 -130 2 30
Naphthalene 25.0 23.50 ug/L 94 70 -130 1 30
n-Butylbenzene 25.0 24.51 ug/L 98 70 -130 4 30
N-Propylbenzene 25.0 24.09 ug/L 96 70 -130 3 30
o-Xylene 25.0 24.46 ug/L 98 70 -130 2 30
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-734030/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 734030
sec-Butylbenzene 25.0 24.55 ug/L 98 70 -130 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Styrene 25.0 25.21 ug/L 101 70 -130 2 30
t-Amyl alcohol 250 218.7 ug/L 87 70 -130 4 30
Tert-amyl methyl ether 25.0 22.92 ug/L 92 70 -130 1 30
Tert-butyl ethyl ether 25.0 22.66 ug/L 91 70 -130 0 30
tert-Butyl Formate 100 102.4 ug/L 102 70 -130 1
tert-Butylbenzene 25.0 24.64 ug/L 99 70 -130 3 30
Tetrachloroethene 25.0 23.12 ug/L 92 70 -130 2 30
Toluene 25.0 22.27 ug/L 89 70 -130 2 30
trans-1,2-Dichloroethene 25.0 22.31 ug/L 89 70 -130 3 30
trans-1,3-Dichloropropene 25.0 24.83 ug/L 99 70 -130 0 50
Trichloroethene 25.0 22.67 ug/L 91 70 -130 4 30
Trichlorofluoromethane 25.0 24.06 ug/L 96 70 -130 5 30
Vinyl acetate 50.0 48.64 ug/L 97 70 -130 1 30
Vinyl chloride 25.0 21.20 ug/L 85 70 -130 4 30
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)70 -130
97Dibromofluoromethane (Surr)70 -130
104Toluene-d8 (Surr)70 -130
Method: 8015D - Gasoline Range Organics (GRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-733048/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 07/28/22 15:12 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 72 70-131 07/28/22 15:12 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733048/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
Gasoline Range Organics [C6 -
C10]
40.0 40.19 mg/Kg 100 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8015D - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733048/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733048
Gasoline Range Organics [C6 -
C10]
40.0 38.07 mg/Kg 95 64 -133 5 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-733231/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 07/29/22 14:51 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 78 70-131 07/29/22 14:51 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733231/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
Gasoline Range Organics [C6 -
C10]
50.0 54.75 mg/Kg 110 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733231/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733231
Gasoline Range Organics [C6 -
C10]
50.0 50.23 mg/Kg 100 64 -133 9 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-733517/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
RL MDL
Gasoline Range Organics [C6 - C10]ND 10.0 2.50 mg/Kg 08/01/22 12:51 100
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
a,a,a-Trifluorotoluene 81 70-131 08/01/22 12:51 100
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 8015D - Gasoline Range Organics (GRO) (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-733517/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
Gasoline Range Organics [C6 -
C10]
50.0 47.58 mg/Kg 95 64 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene 70 -131
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-733517/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 733517
Gasoline Range Organics [C6 -
C10]
50.0 49.29 mg/Kg 99 64 -133 4 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
a,a,a-Trifluorotoluene 70 -131
Surrogate
106
LCSD LCSD
Qualifier Limits%Recovery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-587039/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
RL MDL
C5-C8 Aliphatics ND 26.0 26.0 ug/L 08/01/22 17:42 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 7.007.00 ug/L 08/01/22 17:42 1C9-C10 Aromatics
ND 11.011.0 ug/L 08/01/22 17:42 1C9-C12 Aliphatics
a,a,a-Trifluorotoluene (fid)94 70-130 08/01/22 17:42 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 08/01/22 17:42 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-587039/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 300 309.8 ug/L 103 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.0 53.47 ug/L 107 70 -130
C9-C12 Aliphatics 350 349.0 ug/L 100 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
94a,a,a-Trifluorotoluene (pid)70 -130
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-587039/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 300 298.8 ug/L 100 70 -130 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.0 50.83 ug/L 102 70 -130 5 25
C9-C12 Aliphatics 350 327.2 ug/L 93 70 -130 6 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
94a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-3Lab Sample ID: 680-218771-16 MS
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 348 1500 1828 ug/L 99 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C9-C10 Aromatics 533 F1 250 742.9 ug/L 84 70 -130
C9-C12 Aliphatics 404 1750 2120 ug/L 98 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
MS MS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: MW-3Lab Sample ID: 680-218771-16 MSD
Matrix: Ground Water Prep Type: Total/NA
Analysis Batch: 587039
C5-C8 Aliphatics 348 1500 1770 ug/L 95 70 -130 3 25
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 533 F1 250 701.4 F1 ug/L 67 70 -130 6 25
C9-C12 Aliphatics 404 1750 1903 ug/L 86 70 -130 11 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
MSD MSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-732468/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
RL MDL
1,2-Dibromoethane (EDB)ND 0.0180 0.00500 ug/L 07/25/22 11:15 07/25/22 16:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Pentachloroethane 111 70-130 07/25/22 16:49 1
MB MB
Surrogate
07/25/22 11:15
Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732468/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
1,2-Dibromoethane (EDB)0.100 0.08743 ug/L 87 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Pentachloroethane 70 -130
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-732468/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 732532 Prep Batch: 732468
1,2-Dibromoethane (EDB)0.100 0.08092 ug/L 81 70 -130 8 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Pentachloroethane 70 -130
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 680-732357/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 732619 Prep Batch: 732357
RL MDL
Lead, Total ND 10.0 6.60 ug/L 07/25/22 06:08 07/25/22 20:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-732357/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 732619 Prep Batch: 732357
Lead, Total 505 443.4 ug/L 88 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC/MS VOA
Analysis Batch: 732600
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-2 MW-1-20 Total/NA
Soil 8260D 732626680-218771-4 MW-3-10 Total/NA
Soil 8260D 732626680-218771-5 MW-3-20 Total/NA
Soil 8260D 732626680-218771-6 MW-3-25 Total/NA
Soil 8260D 732626680-218771-7 MW-3-30 Total/NA
Soil 8260D 732626680-218771-8 MW-2-10 Total/NA
Soil 8260D 732626680-218771-9 MW-2-20 Total/NA
Soil 8260D 732626680-218771-11 MW-2-30 Total/NA
Soil 8260D 732626680-218771-13 P-1-20 Total/NA
Soil 8260D 732626680-218771-14 P-1-25 Total/NA
Soil 8260D 732626680-218771-15 P-1-30 Total/NA
Solid 8260DMB 680-732600/8 Method Blank Total/NA
Solid 8260DLCS 680-732600/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732600/5 Lab Control Sample Dup Total/NA
Prep Batch: 732626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-218771-1 MW-1-10 Total/NA
Soil 5035A680-218771-2 - DL2 MW-1-20 Total/NA
Soil 5035A680-218771-2 - DL MW-1-20 Total/NA
Soil 5035A680-218771-2 MW-1-20 Total/NA
Soil 5035A680-218771-3 MW-1-30 Total/NA
Soil 5035A680-218771-3 - DL MW-1-30 Total/NA
Soil 5035A680-218771-4 MW-3-10 Total/NA
Soil 5035A680-218771-4 - DL MW-3-10 Total/NA
Soil 5035A680-218771-5 MW-3-20 Total/NA
Soil 5035A680-218771-5 - DL MW-3-20 Total/NA
Soil 5035A680-218771-6 MW-3-25 Total/NA
Soil 5035A680-218771-7 MW-3-30 Total/NA
Soil 5035A680-218771-8 MW-2-10 Total/NA
Soil 5035A680-218771-9 - DL MW-2-20 Total/NA
Soil 5035A680-218771-9 MW-2-20 Total/NA
Soil 5035A680-218771-10 MW-2-25 Total/NA
Soil 5035A680-218771-11 MW-2-30 Total/NA
Soil 5035A680-218771-12 P-1-10 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-15 P-1-30 Total/NA
Soil 5035A680-218771-15 - DL P-1-30 Total/NA
Analysis Batch: 732793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-1 MW-1-10 Total/NA
Soil 8260D 732626680-218771-2 - DL MW-1-20 Total/NA
Soil 8260D 732626680-218771-3 MW-1-30 Total/NA
Soil 8260D 732626680-218771-4 - DL MW-3-10 Total/NA
Soil 8260D 732626680-218771-5 - DL MW-3-20 Total/NA
Soil 8260D 732626680-218771-10 MW-2-25 Total/NA
Soil 8260D 732626680-218771-12 P-1-10 Total/NA
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC/MS VOA (Continued)
Analysis Batch: 732793 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-15 - DL P-1-30 Total/NA
Solid 8260DMB 680-732793/8 Method Blank Total/NA
Solid 8260DLCS 680-732793/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732793/5 Lab Control Sample Dup Total/NA
Analysis Batch: 732966
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-3 - DL MW-1-30 Total/NA
Solid 8260DMB 680-732966/8 Method Blank Total/NA
Solid 8260DLCS 680-732966/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-732966/5 Lab Control Sample Dup Total/NA
Analysis Batch: 733530
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 732626680-218771-2 - DL2 MW-1-20 Total/NA
Soil 8260D 732626680-218771-9 - DL MW-2-20 Total/NA
Soil 8260D 732626680-218771-13 P-1-20 Total/NA
Soil 8260D 732626680-218771-14 P-1-25 Total/NA
Solid 8260DMB 680-733530/8 Method Blank Total/NA
Solid 8260DLCS 680-733530/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-733530/5 Lab Control Sample Dup Total/NA
Analysis Batch: 733831
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water SM6200-B680-218771-16 MW-3 Total/NA
Water SM6200-BMB 680-733831/19 Method Blank Total/NA
Water SM6200-BLCS 680-733831/1015 Lab Control Sample Total/NA
Water SM6200-BLCSD 680-733831/16 Lab Control Sample Dup Total/NA
Analysis Batch: 734030
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water SM6200-B680-218771-16 - DL MW-3 Total/NA
Ground Water SM6200-B680-218771-17 MW-2 Total/NA
Water SM6200-BMB 680-734030/7 Method Blank Total/NA
Water SM6200-BLCS 680-734030/3 Lab Control Sample Total/NA
Water SM6200-BLCSD 680-734030/4 Lab Control Sample Dup Total/NA
GC VOA
Analysis Batch: 587039
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MAVPH680-218771-16 MW-3 Total/NA
Ground Water MAVPH680-218771-17 MW-2 Total/NA
Water MAVPHMB 400-587039/2 Method Blank Total/NA
Water MAVPHLCS 400-587039/3 Lab Control Sample Total/NA
Water MAVPHLCSD 400-587039/4 Lab Control Sample Dup Total/NA
Ground Water MAVPH680-218771-16 MS MW-3 Total/NA
Ground Water MAVPH680-218771-16 MSD MW-3 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC VOA
Prep Batch: 732626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-218771-1 MW-1-10 Total/NA
Soil 5035A680-218771-2 MW-1-20 Total/NA
Soil 5035A680-218771-3 MW-1-30 Total/NA
Soil 5035A680-218771-4 MW-3-10 Total/NA
Soil 5035A680-218771-5 MW-3-20 Total/NA
Soil 5035A680-218771-6 MW-3-25 Total/NA
Soil 5035A680-218771-7 MW-3-30 Total/NA
Soil 5035A680-218771-8 MW-2-10 Total/NA
Soil 5035A680-218771-9 MW-2-20 Total/NA
Soil 5035A680-218771-10 MW-2-25 Total/NA
Soil 5035A680-218771-11 MW-2-30 Total/NA
Soil 5035A680-218771-12 P-1-10 Total/NA
Soil 5035A680-218771-13 P-1-20 Total/NA
Soil 5035A680-218771-14 P-1-25 Total/NA
Soil 5035A680-218771-15 P-1-30 Total/NA
Analysis Batch: 733048
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-1 MW-1-10 Total/NA
Soil 8015D 732626680-218771-7 MW-3-30 Total/NA
Soil 8015D 732626680-218771-8 MW-2-10 Total/NA
Soil 8015D 732626680-218771-9 MW-2-20 Total/NA
Soil 8015D 732626680-218771-10 MW-2-25 Total/NA
Soil 8015D 732626680-218771-11 MW-2-30 Total/NA
Soil 8015D 732626680-218771-12 P-1-10 Total/NA
Soil 8015D 732626680-218771-13 P-1-20 Total/NA
Soil 8015D 732626680-218771-14 P-1-25 Total/NA
Solid 8015DMB 680-733048/7 Method Blank Total/NA
Solid 8015DLCS 680-733048/5 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733048/6 Lab Control Sample Dup Total/NA
Analysis Batch: 733231
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-2 MW-1-20 Total/NA
Soil 8015D 732626680-218771-5 MW-3-20 Total/NA
Soil 8015D 732626680-218771-6 MW-3-25 Total/NA
Soil 8015D 732626680-218771-15 P-1-30 Total/NA
Solid 8015DMB 680-733231/7 Method Blank Total/NA
Solid 8015DLCS 680-733231/9 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733231/10 Lab Control Sample Dup Total/NA
Analysis Batch: 733517
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8015D 732626680-218771-3 MW-1-30 Total/NA
Soil 8015D 732626680-218771-4 MW-3-10 Total/NA
Solid 8015DMB 680-733517/7 Method Blank Total/NA
Solid 8015DLCS 680-733517/5 Lab Control Sample Total/NA
Solid 8015DLCSD 680-733517/6 Lab Control Sample Dup Total/NA
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QC Association Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
GC Semi VOA
Prep Batch: 732468
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1680-218771-16 MW-3 Total/NA
Ground Water 504.1680-218771-17 MW-2 Total/NA
Water 504.1MB 680-732468/3-A Method Blank Total/NA
Water 504.1LCS 680-732468/4-A Lab Control Sample Total/NA
Water 504.1LCSD 680-732468/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 732532
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 504.1 732468680-218771-16 MW-3 Total/NA
Ground Water 504.1 732468680-218771-17 MW-2 Total/NA
Water 504.1 732468MB 680-732468/3-A Method Blank Total/NA
Water 504.1 732468LCS 680-732468/4-A Lab Control Sample Total/NA
Water 504.1 732468LCSD 680-732468/5-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 732357
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 3005A680-218771-16 MW-3 Total Recoverable
Ground Water 3005A680-218771-17 MW-2 Total Recoverable
Water 3005AMB 680-732357/1-A Method Blank Total Recoverable
Water 3005ALCS 680-732357/2-A Lab Control Sample Total Recoverable
Analysis Batch: 732619
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water 6010D 732357680-218771-16 MW-3 Total Recoverable
Ground Water 6010D 732357680-218771-17 MW-2 Total Recoverable
Water 6010D 732357MB 680-732357/1-A Method Blank Total Recoverable
Water 6010D 732357LCS 680-732357/2-A Lab Control Sample Total Recoverable
General Chemistry
Analysis Batch: 733216
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture680-218771-1 MW-1-10 Total/NA
Soil Moisture680-218771-2 MW-1-20 Total/NA
Soil Moisture680-218771-3 MW-1-30 Total/NA
Soil Moisture680-218771-4 MW-3-10 Total/NA
Soil Moisture680-218771-5 MW-3-20 Total/NA
Soil Moisture680-218771-6 MW-3-25 Total/NA
Soil Moisture680-218771-7 MW-3-30 Total/NA
Soil Moisture680-218771-8 MW-2-10 Total/NA
Soil Moisture680-218771-9 MW-2-20 Total/NA
Soil Moisture680-218771-10 MW-2-25 Total/NA
Soil Moisture680-218771-11 MW-2-30 Total/NA
Soil Moisture680-218771-12 P-1-10 Total/NA
Soil Moisture680-218771-13 P-1-20 Total/NA
Soil Moisture680-218771-14 P-1-25 Total/NA
Soil Moisture680-218771-15 P-1-30 Total/NA
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-1-10 Lab Sample ID: 680-218771-1
Matrix: SoilDate Collected: 07/18/22 10:45
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-10 Lab Sample ID: 680-218771-1
Matrix: SoilDate Collected: 07/18/22 10:45
Percent Solids: 82.5Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.014 g 5 mL
Analysis 8260D 40 732793 07/27/22 18:29 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.071 g 5 mL
Analysis 8015D 100 733048 07/28/22 15:36 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-1-20 Lab Sample ID: 680-218771-2
Matrix: SoilDate Collected: 07/18/22 10:50
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-20 Lab Sample ID: 680-218771-2
Matrix: SoilDate Collected: 07/18/22 10:50
Percent Solids: 73.1Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32DL2 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.928 g 5 mL
Analysis 8260D DL2 5000 733530 08/01/22 17:33 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.928 g 5 mL
Analysis 8260D 40 732600 07/26/22 20:13 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.928 g 5 mL
Analysis 8260D DL 1000 732793 07/27/22 16:28 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.68 g 5 mL
Analysis 8015D 1000 733231 07/29/22 19:45 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-1-30 Lab Sample ID: 680-218771-3
Matrix: SoilDate Collected: 07/18/22 10:55
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-1-30 Lab Sample ID: 680-218771-3
Matrix: SoilDate Collected: 07/18/22 10:55
Percent Solids: 75.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.519 g 5 mL
Analysis 8260D 1000 732793 07/27/22 16:52 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 6.519 g 5 mL
Analysis 8260D DL 5000 732966 07/28/22 21:33 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 6.401 g 5 mL
Analysis 8015D 20000 733517 08/01/22 16:14 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-10 Lab Sample ID: 680-218771-4
Matrix: SoilDate Collected: 07/18/22 11:35
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-10 Lab Sample ID: 680-218771-4
Matrix: SoilDate Collected: 07/18/22 11:35
Percent Solids: 76.7Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.739 g 5 mL
Analysis 8260D 1 732600 07/26/22 15:23 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.917 g 5 mL
Analysis 8260D DL 40 732793 07/27/22 18:53 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.892 g 5 mL
Analysis 8015D 100 733517 08/01/22 14:25 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3-20 Lab Sample ID: 680-218771-5
Matrix: SoilDate Collected: 07/18/22 11:45
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-20 Lab Sample ID: 680-218771-5
Matrix: SoilDate Collected: 07/18/22 11:45
Percent Solids: 63.3Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.64 g 5 mL
Analysis 8260D 1 732600 07/26/22 15:47 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.69 g 5 mL
Analysis 8260D DL 40 732793 07/27/22 19:17 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.128 g 5 mL
Analysis 8015D 100 733231 07/29/22 17:57 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-25 Lab Sample ID: 680-218771-6
Matrix: SoilDate Collected: 07/19/22 16:10
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-3-25 Lab Sample ID: 680-218771-6
Matrix: SoilDate Collected: 07/19/22 16:10
Percent Solids: 86.9Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.396 g 5 mL
Analysis 8260D 1 732600 07/26/22 16:11 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.125 g 5 mL
Analysis 8015D 100 733231 07/29/22 18:19 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3-30 Lab Sample ID: 680-218771-7
Matrix: SoilDate Collected: 07/19/22 16:15
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3-30 Lab Sample ID: 680-218771-7
Matrix: SoilDate Collected: 07/19/22 16:15
Percent Solids: 79.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.699 g 5 mL
Analysis 8260D 1 732600 07/26/22 16:35 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.018 g 5 mL
Analysis 8015D 100 733048 07/28/22 17:46 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-10 Lab Sample ID: 680-218771-8
Matrix: SoilDate Collected: 07/19/22 16:20
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-10 Lab Sample ID: 680-218771-8
Matrix: SoilDate Collected: 07/19/22 16:20
Percent Solids: 77.8Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.875 g 5 mL
Analysis 8260D 1 732600 07/26/22 17:00 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.997 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:08 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32DL TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.661 g 5 mL
Analysis 8260D DL 40 733530 08/01/22 17:55 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.05 g 5 mL
Analysis 8260D 1 732600 07/26/22 17:24 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-2-20 Lab Sample ID: 680-218771-9
Matrix: SoilDate Collected: 07/19/22 16:26
Percent Solids: 71.4Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.156 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:30 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-25 Lab Sample ID: 680-218771-10
Matrix: SoilDate Collected: 07/19/22 16:30
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-25 Lab Sample ID: 680-218771-10
Matrix: SoilDate Collected: 07/19/22 16:30
Percent Solids: 76.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.323 g 5 mL
Analysis 8260D 1 732793 07/27/22 13:16 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.149 g 5 mL
Analysis 8015D 100 733048 07/28/22 18:51 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-2-30 Lab Sample ID: 680-218771-11
Matrix: SoilDate Collected: 07/19/22 16:35
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: MW-2-30 Lab Sample ID: 680-218771-11
Matrix: SoilDate Collected: 07/19/22 16:35
Percent Solids: 83.1Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.948 g 5 mL
Analysis 8260D 1 732600 07/26/22 18:12 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.008 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:13 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: P-1-10 Lab Sample ID: 680-218771-12
Matrix: SoilDate Collected: 07/19/22 16:44
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-10 Lab Sample ID: 680-218771-12
Matrix: SoilDate Collected: 07/19/22 16:44
Percent Solids: 77.2Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.87 g 5 mL
Analysis 8260D 1 732793 07/27/22 13:40 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.217 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:35 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-20 Lab Sample ID: 680-218771-13
Matrix: SoilDate Collected: 07/19/22 16:48
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-20 Lab Sample ID: 680-218771-13
Matrix: SoilDate Collected: 07/19/22 16:48
Percent Solids: 76.5Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.014 g 5 mL
Analysis 8260D 1 733530 08/01/22 16:26 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.941 g 5 mL
Analysis 8260D 1 732600 07/26/22 19:00 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 4.868 g 5 mL
Analysis 8015D 100 733048 07/28/22 19:57 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-25 Lab Sample ID: 680-218771-14
Matrix: SoilDate Collected: 07/19/22 16:50
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: P-1-25 Lab Sample ID: 680-218771-14
Matrix: SoilDate Collected: 07/19/22 16:50
Percent Solids: 75.6Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.955 g 5 mL
Analysis 8260D 1 733530 08/01/22 16:47 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.141 g 5 mL
Analysis 8260D 1 732600 07/26/22 19:25 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.071 g 5 mL
Analysis 8015D 100 733048 07/28/22 20:18 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: P-1-30 Lab Sample ID: 680-218771-15
Matrix: SoilDate Collected: 07/19/22 16:55
Date Received: 07/23/22 09:30
Analysis Moisture WRB07/29/22 13:101 TAL SAV733216
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1-30 Lab Sample ID: 680-218771-15
Matrix: SoilDate Collected: 07/19/22 16:55
Percent Solids: 68.7Date Received: 07/23/22 09:30
Prep 5035A FES07/26/22 10:32 TAL SAV732626
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.679 g 5 mL
Analysis 8260D 40 732600 07/26/22 21:02 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A DL 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.679 g 5 mL
Analysis 8260D DL 500 732793 07/27/22 17:16 UI TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 5035A 732626 07/26/22 10:32 FES TAL SAVTotal/NA 5.884 g 5 mL
Analysis 8015D 1000 733231 07/29/22 21:12 DBM TAL SAVTotal/NA 5 mL 5 mL
CVGWFID1Instrument ID:
Client Sample ID: MW-3 Lab Sample ID: 680-218771-16
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Analysis SM6200-B SMP08/03/22 18:061 TAL SAV733831
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSO2
Analysis SM6200-B DL 5 734030 08/04/22 13:42 SMP TAL SAVTotal/NA 5 mL 5 mL
CMSO2Instrument ID:
Analysis MAVPH 5 587039 08/02/22 10:10 SAB EETSE PENTotal/NA 5 mL 5 mL
CH_CAROLInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Client Sample ID: MW-3 Lab Sample ID: 680-218771-16
Matrix: Ground WaterDate Collected: 07/20/22 14:15
Date Received: 07/23/22 09:30
Prep 504.1 IB07/25/22 11:15 TAL SAV732468
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 34.8 mL 2 mL
Analysis 504.1 1 732532 07/25/22 18:58 JCK TAL SAVTotal/NA
CSGXInstrument ID:
Prep 3005A 732357 07/25/22 06:08 RR TAL SAVTotal Recoverable 50 mL 50 mL
Analysis 6010D 1 732619 07/25/22 20:30 BCB TAL SAVTotal Recoverable
ICPHInstrument ID:
Client Sample ID: MW-2 Lab Sample ID: 680-218771-17
Matrix: Ground WaterDate Collected: 07/20/22 14:40
Date Received: 07/23/22 09:30
Analysis SM6200-B SMP08/04/22 13:16500 TAL SAV734030
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSO2
Analysis MAVPH 100 587039 08/02/22 15:32 SAB EETSE PENTotal/NA 5 mL 5 mL
CH_CAROLInstrument ID:
Prep 504.1 732468 07/25/22 11:15 IB TAL SAVTotal/NA 34.3 mL 2 mL
Analysis 504.1 1 732532 07/25/22 19:07 JCK TAL SAVTotal/NA
CSGXInstrument ID:
Prep 3005A 732357 07/25/22 06:08 RR TAL SAVTotal Recoverable 50 mL 50 mL
Analysis 6010D 1 732619 07/25/22 20:33 BCB TAL SAVTotal Recoverable
ICPHInstrument ID:
Laboratory References:
EETSE PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-218771-1
Project/Site: D&M Grocery
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Alabama State 40150 06-30-23
ANAB ISO/IEC 17025 L2471 02-23-23
Arkansas DEQ State 88-0689 09-01-22
California State 2510 06-30-23
Florida NELAP E81010 06-30-23
Georgia State E81010(FL)06-30-23
Illinois NELAP 200041 10-09-22
Kansas NELAP E-10253 10-31-22
Kentucky (UST)State 53 06-30-23
Kentucky (WW)State KY98030 12-31-22
Louisiana (All)NELAP 30976 06-30-23
Louisiana (DW)State LA017 12-31-22
Maryland State 233 09-30-22
Michigan State 9912 06-30-23
North Carolina (WW/SW)State 314 12-31-22
Oklahoma NELAP 9810 08-31-22
Pennsylvania NELAP 68-00467 01-31-23
South Carolina State 96026 06-30-23
Tennessee State TN02907 06-30-23
Texas NELAP T104704286 09-30-22
US Fish & Wildlife US Federal Programs A22340 06-30-23
USDA US Federal Programs P330-21-00056 05-17-24
Virginia NELAP 460166 06-14-23
West Virginia DEP State 136 03-31-23
Eurofins Savannah
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Method Summary
Job ID: 680-218771-1Client: S&ME, Inc.
Project/Site: D&M Grocery
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL SAV
SMSM6200-B Volatile Organic Compounds TAL SAV
SW8468015DGasoline Range Organics (GRO) (GC)TAL SAV
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EETSE PEN
EPA-DW504.1 EDB, DBCP and 1,2,3-TCP (GC)TAL SAV
SW8466010DMetals (ICP)TAL SAV
EPAMoisturePercent Moisture TAL SAV
SW8463005APreparation, Total Recoverable or Dissolved Metals TAL SAV
SW8465030BPurge and Trap EETSE PEN
SW8465035AClosed System Purge & Trap TAL SAV
SW8465035AClosed System Purge & Trap/Field Methanol TAL SAV
EPA-DW504.1 Microextraction TAL SAV
SMSM6200-B Purge and Trap TAL SAV
Protocol References:
EPA = US Environmental Protection Agency
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
MA DEP = Massachusetts Department Of Environmental Protection
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EETSE PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-218771-1
Login Number: 218771
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
FalseCooler Temperature is acceptable.Cooler temperature outside required temperature
criteria.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-218771-1
Login Number: 218771
Question Answer Comment
Creator: Roberts, Alexis J
List Source: Eurofins Pensacola
List Creation: 07/27/22 02:36 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.7°C IR8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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