WS-28371_47623_CA_LSA_20210331

LIMITED SITE ASSESSMENT

QUALITY MART 42
1465 RIVER RIDGE ROAD
CLEMMONS, FORSYTH COUNTY, NC
GROUNDWATER INCIDENT: PENDING FACILITY ID: 00-0-0000036651

MARCH 31, 2021
UST OWNER/OPERATOR:
Quality Oil Company, LLC
P.O. Box 2736
Winston-Salem, NC 27102-2736 Phone Number: [phone]
PROPERTY OWNER:
Quality Oil Company, LLC P.O. Box 2736 Winston-Salem, NC 27102-2736 Phone Number: [phone]
CONSULTANT:
Paragon Environmental Consultants, Inc.
P. O. Box 157
Thomasville, NC 27361-0157
Phone Number: [phone]
RELEASE INFORMATION:
Date Discovered: February 4, 2021 Estimated Quantity of Release: Unknown Cause of Release: Spill Bucket Failure Source of Release: Highway Diesel UST Spill Bucket Size and Contents: One (1) 10,000 Gallon Diesel UST Latitude: N 36.07514000o Longitude: W 80.38994699o

The Limited Site Assessment for this site has been prepared by Paragon Environmental
Consultants, Inc. under the direct supervision of a licensed geologist. All activities
performed on this project were conducted under my direct supervision:
Benjamin W. Robinson, L.G.
North Carolina License #2466

March 31, 2021

Jon Shutt
Quality Oil Company, LLC P.O. Box 2736 Winston-Salem, NC 27102-2736 Reference: Limited Site Assessment Quality Mart 42 1465 River Ridge Road Clemmons, Forsyth County, NC Groundwater Incident # Pending Facility ID # 00-0-0000036651

Dear Mr. Shutt:
In accordance with the requirements of a correspondence dated March 11, 2021 from the
North Carolina Department of Environmental Quality (NCDEQ), contained herein is a
Limited Site Assessment for the release which occurred at the above referenced facility.
These activities have been conducted following the discovery of petroleum above the
action limits beneath the spill bucket on the highway diesel underground storage tank
(UST) at 1465 River Ridge Road. All activities were conducted in accordance with
NCDEQ guidelines and the requirements of 15A NCAC 2L .0115.
Mr. Shutt, if you have questions regarding this report, please contact our office.

Sincerely,
Benjamin W. Robinson, L.G. Paragon Environmental Consultants, Inc.

R21-2104A
PARAGON
Environmental Consultants, Inc.
P.O. Box 157 • Thomasville, NC 27361-0157
Business Ph: [phone] • Fax: [phone]
TABLE OF CONTENTS

Page 1.0 SITE HISTORY AND SOURCE CHARACTERIZATION 1 2.0 RISK CHARACTERIZATION 1 3.0 RECEPTOR INFORMATION 4 4.0 SITE GEOLOGY AND HYDROGEOLOGY 6 5.0 SAMPLING RESULTS 7 6.0 CONCLUSIONS AND RECOMMENDATIONS 8 LIST OF FIGURES

Figure 1: Project Location/U.S.G.S. Topographic Map
Figure 2: Site Layout and UST Locations
Figure 3: Supply Well Locations Map
Figure 4: Subsurface Utilities Map
Figure 5: Adjacent Properties Map
Figure 6: Site Layout and Soil Samples Location
Figure 7: Site Layout and Monitor Well Location
LIST OF TABLES

Table 1: Site History Table 2: Water Supply Well Information Table 3: Adjacent Property Owners Table 4: Summary of Soil Analytical Results Table 5: Monitoring Well Information and Groundwater Elevation Table 6: Summary of Groundwater Analytical Results

APPENDICES

Appendix A: Soil Boring Log Appendix B: Well Construction Record Appendix C: Standard Operating Procedures Appendix D: Laboratory Analytical Results
Page - 1
LIMITED SITE ASSESSMENT Quality Mart 42 1465 River Ridge Road Clemmons, NC 1.0. - SITE HISTORY AND SOURCE CHARACTERIZATION Quality Oil Company, LLC owns and operates a UST system at 1465 River Ridge Road in Clemmons, NC which is referred to as Quality Mart 42. This property contains one permanent structure which is utilized as a convenience store. Figure 1 illustrates the location of this facility on the Clemmons Quadrangle U.S.G.S. Topographic Map. A compliance inspection noted damage to the spill bucket on the diesel and regular gasoline USTs and directed site check soil sampling. Figure 2 illustrates the site layout and the existing UST locations. Soil samples were collected by Paragon Environmental Consultants, Inc. on January 27, 2021 beneath the spill bucket on the diesel and regular gasoline USTs. The diesel UST spill bucket samples showed a maximum contaminant concentration of 6,300 milligrams per kilogram by EPA Method 3550 and 460 mg/kg by EPA Method 5030. This facility contains one (1) 20,000 gallon gasoline UST, one (1) 12,000 gallon gasoline UST, and one (1) 15,000 gallon two-compartment UST with a 10,000 gallon diesel compartment and a 5,000 gallon gasoline compartment which are used for the retail sale of petroleum. Information regarding the ownership of the regulated USTs which are located at this facility is contained in Table 1.

2.0 - RISK CHARACTERIZATION AND LAND USE FORM

Part I Groundwater/Surface water/Vapor impact High Risk

1. Has discharge or release contaminated any water supply wells including any used
for non-drinking purposes?
NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the discharge or release?

NO

3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the discharge or release?

NO

Page - 2

4. Does groundwater within 500 feet of the source area of the discharge or release have the potential for future use in that there is no other source of water supply other than the groundwater?

NO

5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space or pose any other serious threat to
public health, public safety or the environment?
NO 6. Are there any factors that would cause the discharge or release to pose an imminent danger to public health, public safety or the environment?

NONE KNOWN

Intermediate Risk

7. Is a surface body located within 500 feet of the source area of the discharge or
release?
NO

If yes, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?

N/A

8. Is the source area of the discharge or release located within a designated wellhead protection area as defined in 42 USC 300h-7(e)?

NO
9. Is the discharge or release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of North Carolina" published by the Department in 1985?

NO

If yes, is the source area of the discharge or release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water?

N/A

Page - 3
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established (see Table 7 in guidelines) by the department?

NO Part II-Land Use

Property containing Source Area of Discharge or Release

The questions below pertain to the property containing the source area of the release.

1. Does the property contain one or more primary or secondary residences (permanent
or temporary)?
NO

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly?

NO

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped?

YES, THE PROPERTY IS OPERATED AS A CONVENIENCE STORE
4. Do children visit the property?

YES

Explain. CHILDREN MAY VISIT THE STORE FOR LIMITED PERIODS OF TIME 5. Is access to the property reliably restricted consistent with its use?

YES

6. Do pavement, buildings, or other structures cap the contaminated soil?

YES

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future?

THE UST SYSTEM AS WELL AS THE ASPHALT AND CONCRETE PAVING
WILL REMAIN IN PLACE

Page - 4
7. What is the zoning status of the property?

COMMERCIAL 8. Is the use of the property likely to change in the next 20 years?

NO Property Surrounding Source Area of Discharge or Release.

9. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)

APPROXIMATELY 800 FEET TO THE EAST
10. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly?

IMMANUEL BAPTIST CHURCH IS LOCATED APPROXIMATELY 950 FEET TO THE SOUTH 11. What is the zoning status of properties in the surrounding areas?

COMMERCIAL / RESIDENTIAL

12. Briefly characterize the use and activities of the land in the surrounding area.
COMMERCIAL / RESIDENTIAL

3.0 - RECEPTOR INFORMATION

3.1 Water Supply Wells

A supply well survey has been conducted within a radius of 1,000 feet from the release
area. During this reconnaissance, five (5) water supply wells were identified within this
radius, however, these wells are out of service and not in use for consumption. No supply
wells were found to be located within a radius of 250 feet from the release area. Figure 3
illustrates the locations of the supply wells, and Table 2 lists the owners and addresses for
the wells within 1,000 feet of the release source.

3.2 Public Water Supplies

Public water supplies are available to all of the surrounding properties within a radius of 1,500 feet from 1465 River Ridge Road.

Page - 5
3.3 Surface Water

The partial U.S.G.S. map included as Figure 1 indicates that surface waters in the vicinity of the release area generally drain towards Blanket Creek located approximately 1,500 feet to the west. Blanket Creek drains into the Yadkin River approximately 22,000 feet to the southwest. The Yadkin River is situated within the Yadkin Pee-Dee River Drainage Basin.

3.4 Wellhead Protection Areas
No wellhead protection areas are known to exist within the area of this release. 3.5 Deep Aquifers in the Coastal Plain Physiographic Region

This release is not located in the coastal plain.

3.6 Subsurface Structures

Subsurface utilities in the form of the USTs, product lines, and electrical conduits are located above the petroleum affected area at this facility. The building located on the impacted property does not have a basement; however, other subsurface utilities are present in the form of electric, water, and sewer lines. Figure 4 illustrates the locations of all known subsurface utilities. 3.7 Land Use

The possibility of human exposure to soil contamination at Quality Mart 42 is minimal.
The marginally impacted soils beneath the spill bucket are capped by concrete and will not
allow exposure to persons at the store property. The facility lies within an area used for
commercial and residential purposes.

3.8 Property Owners and Occupants

Figure 5 illustrates the surrounding properties, and Table 3 contains information regarding the adjacent property owners. This information was obtained from the Forsyth County Tax Department’s records.

Page - 6
4.0 - SITE GEOLOGY AND HYDROGEOLOGY

4.1 Site Geology

The site is situated in the Piedmont Region of the North Carolina Slate Belt. According to the Geological Map of North Carolina local bedrock geology of the region consists of Late Proterozoic to Cambrian aged metamorphosed granitic bedrock. Competent bedrock was not encountered to a depth of 45 feet below land surface which was the maximum depth explored during the subsurface investigation.

4.2 Soils Investigation

The soils at the project site consist of varying amounts of clay and silt. Two soil samples were obtained from the directly above the top of the UST immediately adjacent to the spill bucket that contained the fill port of the regular gasoline UST at this subject facility. Paragon collected samples from both the east and west sides of this spill bucket at depths of approximately two feet below surface grade. The regular spill bucket samples were labeled as Regular Spill Bucket – A (RSB-A) and Regular Spill Bucket – B (RSB-B). RSB-A was collected from the east side of the spill bucket (nearest to Lewisville-Clemmons Road) and RSB-B was collected from the west side of the spill bucket (nearest to the Quality Mart 42 building). Two soil samples were obtained from the directly above the top of the UST immediately adjacent to the spill bucket that contained the fill port of the diesel UST at this subject facility. Paragon collected samples from both the east and west sides of this spill bucket at depths of approximately two feet below surface grade. The diesel spill bucket samples were labeled as Diesel Spill Bucket – A (DSB-A) and Diesel Spill Bucket – B (DSB-B). DSB-A was collected from the east side of the spill bucket (nearest to Lewisville-Clemmons Road) and DSB-B was collected from the west side of the spill bucket (nearest to the Quality Mart 42 building). The spill bucket assessment soil samples were submitted to Meritech, Inc. for laboratory analysis by EPA Methods 5030. EPA Method 5030 tests for total petroleum hydrocarbons (TPH) from low boiling-point fuels such as gasoline, aviation fuel, and gasohol. The current action level for EPA Method 5030 constituents is 50 milligrams per kilogram (mg/kg). The soil samples from the diesel spill bucket were also analyzed according to EPA Method 3550. EPA Method 3550 tests for TPH from high boiling-point fuels such as diesel, kerosene, and fuel oil. The current action level for Method 3550 constituents is 100 mg/kg. Soil sample RSB-A was reported at a concentration of 335 mg/kg by EPA Method 5030. This TPH level exceeds the NCDEQ 5030 action level of 50 mg/kg. Soil sample RSB-B was below the laboratory detection limit by EPA Method 5030. Soil sample DSB-A was reported with at a concentration of 6,300 mg/kg by EPA Method 3550 and a concentration of 460 mg/kg by EPA Method 5030. These TPH levels exceed the NCDEQ 5030 action level of 50 mg/kg and the NCDEQ 3550 action level of 100 mg/kg. Soil sample DSB-B was detected at a concentration of 3,940 mg/kg by EPA Method 3550 and a concentration of 287 mg/kg by EPA Method 5030. These TPH levels exceed the NCDEQ 5030 action level of 50 mg/kg and the NCDEQ 3550 action level of 100 mg/kg.

Page - 7
A soil boring log for the boring advanced for monitor well installation at the site is contained as Appendix A. Two “Risk-Based” samples were collected for laboratory analyses from the monitor well boring at depths of 15 and 25 feet below land surface. These samples, labeled as MW1-15 and MW1-25, were analyzed by EPA Methods 8260 and 8270, as well as for Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons (EPH) by MADEP methods. All compounds according to EPA Methods 8260 and 8270, as well as all carbon fraction classes by VPH and EPH were below the lowest Maximum Soil Contaminant Concentrations (MSCCs) in both samples. Figure 6 illustrates the location of the soil samples collected at 1465 River Ridge Road, and Table 4 summarizes the analytical results for the “Risk-Based” soil samples obtained at Quality Mart 42. Appendix D contains a copy of the laboratory analytical report and the chain-of-custody record for the soil samples collected by Paragon at this subject site. 5.0 - SAMPLING RESULTS

5.1 Monitor Well Installation

One North Carolina Type II groundwater monitoring well has been installed at the site. Figure 7 illustrates the site layout and the location of the monitor well which was labeled as MW-1. The monitoring well was constructed of 2-inch Schedule 40 PVC pipe with 20 feet of 0.010 inch slotted screen. Based on the assumption that the contaminants being addressed were primarily hydrocarbon constituents with specific gravities of less than 1.0, the groundwater monitoring well was installed so that the screened interval intersected the shallow groundwater table at the time of installation. Table 5 summarizes the monitoring well information and groundwater elevation as measured on March 16, 2021, and Appendix B contains a copy of the well construction record for this monitor well.

5.2 Groundwater Analyses
Following installation, the monitoring well was developed and sampled in accordance with Paragon’s Standard Operating Procedures which are contained as Appendix C. The groundwater sample was submitted to Waypoint Analytical, LLC for laboratory analysis according to EPA Methods 6200B plus Oxygenates and 625 plus Tentatively Identified Compounds (TICs). The groundwater sample was also analyzed by MADEP methods for VPH and EPH, as well as for Lead. According to the analytical results for monitor well MW-1, Benzene, MTBE, Naphthalene, tert-Butyl Alcohol (TBA), as well as three carbon fraction classes were reported at concentrations in excess of the 2L Standards. Benzene was reported at a concentration of 50.4 micrograms per Liter (ug/L), which is over the 2L Standard of 1 ug/L. MTBE was listed at a level of 43.7 ug/L, in excess of the 2L Standard of 20 ug/L. Naphthalene was
shown at a concentration of 14.9 ug/L, above the 2L Standard of 6 ug/L. tert-Butyl Alcohol
(TBA) was reported at a concentration of 283 ug/L, in excess of the 2L Standard of 10
ug/L.. C5-C8 Volatile Aliphatics were listed at a level of 1,010 ug/L, which exceeds the
2L Standard of 400 ug/L. C9-C18 Aliphatics, which has a 2L Standard of 700 ug/L, was
reported at a concentration of 890 ug/L. C9-C22 Aromatics were shown at a level of 258
ug/L, which is over the 2L Standard of 200 ug/L. All other constituents by EPA Methods
6200B and 625, as well as Lead, were below the 2L Standards. There were no Gross
Contaminant Level (GCL) violations. Table 6 summarizes the groundwater analytical
results, and Appendix D contains a copy of the laboratory analytical report and the chain-
of-custody record for the groundwater sample.
Page - 8
6.0 - CONCLUSIONS AND RECOMMENDATIONS

6.1 General Summary

Limited Site Assessment activities at Quality Mart 42 have been completed. From a review of all information gathered during this project, Paragon Environmental Consultants, Inc. makes the following conclusions:

o A petroleum release of unknown quantity has occurred at this site. Soil samples collected from the monitor well boring were below the lowest MSCCs.

o One groundwater monitoring well was constructed at the site during this investigation. Free product was not observed in monitor well MW-1.

o The analytical results for the groundwater sample from MW-1 indicated four 6200B
compounds and three carbon fraction classes in excess of the 2L Standards, but
below the GCLs.

6.2 Recommendations

Based upon a review of all information gathered during this project, Paragon makes the following recommendations:

o Since the remaining in-situ soils are below the lowest MSCCs and the groundwater concentrations are below the GCLs, a notice of No Further Action should be issued for the subject site. Public notification and deed recordation will be required due to the groundwater contamination in excess of the 2L Standards.

o A copy of this report should be forwarded to the following address:

Winston-Salem Regional Office - UST Section
450 W. Hanes Mill Road – Suite 300
Winston-Salem, NC 27105

6.3 Limitations
This report has been prepared for the exclusive use of Quality Oil Company, LLC for the specific application to the referenced site located in Forsyth County, North Carolina. The evaluation was conducted based on the scope of work and level of effort desired by the client and with resources adequate only for the scope of work. Our findings have been developed in accordance with generally accepted standards for Limited Site Assessments
in the State of North Carolina, available information, and our professional judgment. No
other warranty is expressed or implied.

The data presented in this report are indicative of conditions at the precise locations
sampled and the time the sample was collected. Additionally, the data obtained from the
samples would be interpreted as meaningful with respect to the parameters in the laboratory
reports. No additional information can be logically inferred from this data.

FIGURES

TABLES

TABLE 1: SITE HISTORY QUALITY MART 42 1465 RIVER RIDGE ROAD CLEMMONS, NC Property Owner: Quality Oil Company, LLC P.O. Box 2736 Winston-Salem, NC 27102-2736 UST Owner: Quality Oil Company, LLC P.O. Box 2736 Winston-Salem, NC 27102-2736 UST Operator: Quality Oil Company, LLC P.O. Box 2736 Winston-Salem, NC 27102-2736 UST Information:

Tank Installation Size Closure UST Tank
No Date (Gal) Date Status Contents
1 7/1/2004 20,000 Not Applicable In Use Gasoline
2 7/1/2004 12,000 Not Applicable In Use Gasoline
3 7/1/2004 10,000 Not Applicable In Use Diesel
4 7/1/2004 5,000 Not Applicable In Use Gasoline

M21-2104H
TABLE 2
WATER SUPPLY WELL INFORMATION
1,000' Radius
Quality Mart 42
Clemmons, North Carolina
Well
Identification SW-1 SW-2 SW-3 SW-4 SW-5
Owner Name Impulse Energy, LLC Muslim Ass. Of The Triad Impulse Energy, LLC Impulse Energy, LLC Impulse Energy, LLC
Owner Mailing 6778 River Center Drive 1435 Lake Cottage Road 6778 River Center Drive 6778 River Center Drive 6778 River Center Drive
Address Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012
Telephone #Unknown Unknown Unknown Unknown Unknown
Use of Well Out of Service Out of Service Out of Service Out of Service Out of Service
Physical Address 5911 Immanuel Road 1435 Lake Cottage Road 5931 Immanuel Road 5921 Immanuel Road 5941 Immanuel Road
Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012 Clemmons, NC 27012
Depth of Casing Unknown Unknown Unknown Unknown Unknown
Well Screen Interval Unknown Unknown Unknown Unknown Unknown
Feet from Source 805'810'875'890'900'
X21-2104C
TABLE 3: ADJACENT PROPERTY OWNERS QUALITY MART 42 1465 RIVER RIDGE ROAD CLEMMONS, NORTH CAROLINA SITE ID OWNER INFO 1 Quality Oil Company, LLC P.O. Box 2736 Linwood, NC 27102-2736 (Project Location) 2 Mid-State Petroleum Realty, LLC P.O. Box 1618 Jamestown, NC 27282 (1455 River Ridge Road) 3 Circle K Stores, Inc. 2440 Whitehall Park Drive, Suite 800 Charlotte, NC 28273 (1415 Lewisville-Clemmons Road) 4 Mas O Menos, LLC 2511 South Cook Road Sioux Falls, SD 57103 (1423 Lewisville-Clemmons Road) 5 Chase Resources, LLC P.O. Box 5598 Winston-Salem, NC 27113 (1469 River Ridge Road) 6 Clemmons River Ridge, LLC 69 Sandra Lane Wayne, NJ 07470 (1430 River Ridge Road) M21-2104P
TABLE 4
Summary of Soil Analytical Results
Quality Mart 42
Clemmons, North Carolina
Constituent MW1-15 MW1-25 Lowest MSCCs
Date 3/15/2021 3/15/2021
Method 8260 (mg/kg)
Acetone BDL 0.03 24
Benzene BDL BDL 0.0056
n-Butylbenzene BDL BDL 4.3
sec-Butylbenzene BDL BDL 3.3
Ethylbenzene BDL BDL 4.9
Isopropylbenzene BDL BDL 1.7
p-Isopropyltoluene BDL BDL 0.12
Methylene Chloride BDL BDL 0.02
Methyl Ethyl Ketone (MEK)BDL 0.006 16
Naphthalene BDL BDL 0.16
Toluene BDL BDL 4.3
1,2,4-Trimethylbenzene BDL BDL 8.5
1,3,5-Trimethylbenzene BDL BDL 8.3
Xylenes (total)BDL BDL 4.6
Method 8270 (mg/kg)
Benzo(a)anthracene 0.06 0.058 0.35
Benzo(a)pyrene 0.075 0.083 0.096
Benzo(b)flouranthene 0.101 0.123 1.2
Benzo(g,h,i)perylene 0.064 0.066 6,400
Benzo(k)flouranthene BDL 0.031 12
Chrysene 0.087 0.091 39
Fluoranthene 0.234 0.259 290
Indeno(1.2.3-cd)pyrene BDL BDL 3.4
Naphthalene BDL BDL 0.16
Phenanthrene 0.116 0.12 56
Pyrene 0.191 0.215 270
Aliphatic Fraction Classes (mg/kg)
C5-C8 Volatile Aliphatics BDL BDL 68
C9-C12 Volatile Aliphatics BDL BDL NSE
C9-C18 Extractable Aliphatics BDL BDL NSE
C9-C18 Aliphatics (total)BDL BDL 540
C19-C36 Extractable Aliphatics BDL BDL NSE
Aromatic Fraction Classes (mg/kg)
C9-C10 Volatile Aromatics BDL BDL NSE
C11-C22 Extractable Aromatics BDL BDL NSE
C9-C22 Aromatics (total)BDL BDL 31
BDL= Below Detection Limits
NSE = No Standard Established X21-2104
TABLE 5

Monitoring Well Information and Groundwater Elevation
Quality Mart 42
Clemmons, NC
Well Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater Elevation
MW-1 100.00 75.00 55.00 33.67 66.33
Note: All measurements taken in feet and based on an arbitrary benchmark of 100.00 feet; groundwater levels measured on March 16, 2021.
X21-2104B
TABLE 6
Summary of Groundwater Analytical Results
Quality Mart 42
Clemmons, North Carolina
Constituent MW-1 2L Standard GCL

Date 3/16/2021
Methods 6200B (ug/L)
Benzene 50.4 1 5,000
Toluene 560 600 260,000
Ethylbenzene 57.8 600 84,500
Xylenes (total)392 500 85,500
BTEX (total)1,060.2 NSE NSE
Acetone 32.8 6,000 6,000,000
Bromomethane 0.691 100 100,000
2-Butanone 17.8 4,000 4,000,000
n-Butylbenzene 0.757 70 6,900
sec-Butylbenzene 0.546 70 8,500
Ethanol 2,000 4,000 4,000,000
2-Hexanone 8.64 40 40,000
Isopropylbenzene 19.2 70 25,000
Isopropyl Ether (IPE)8.36 70 70,000
p-Isopropyltoluene 0.374 25 11,700
Methyl Isobutyl Ketone (MIBK)3.62 100 100,000
Methyl tert-Butyl Ether (MTBE)43.7 20 20,000
Naphthalene 14.9 6 6,000
n-Propylbenzene 9.47 70 30,000
tert-Butyl Alcohol (TBA)283 10 10,000
tert-Amyl Methyl Ether (TAME)1.16 128 12,800
1,2,4-Trimethylbenzene 84.6 400 28,500
1,3,5 Trimethylbenzene 22.4 400 25,000
Method 625 (ug/L)
Acenaphthene BDL 80 2,120
Anthracene BDL 2,000 2,000
Naphthalene 8.39 6 6,000
TICs (total)BDL NSE NSE
Metals (ug/L)
Lead BDL 15 15,000
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 1,010 400 400,000
C9-C12 Volatile Aliphatics 890 NSE NSE
C9-C18 Extractable Aliphatics BDL NSE NSE
C9-C18 Aliphatics (total)890 700 700,000
C19-C36 Extractable Aliphatics BDL 10,000 10,000,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics 258 NSE NSE
C11-C22 Extractable Aromatics BDL NSE NSE
C9-C22 Aromatics (total)258 200 200,000
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established X21-2104A

APPENDIX A

SOIL BORING LOG

SOIL BORING LOG
Paragon Environmental Consultants, Inc.
Job Name:Quality Mart 42
Address:1465 River Ridge Road Clemmons, NC
Job No:P-2104
Start Date:3/15/2021
Driller:Innovative Environmental Technologies, Inc.
Boring No.:MW-1
Comments:
Sample Depth Blow OVA
Number (ft.)Soil Description (color, soil type, moisture)Counts (ppm)
MW-1 5 Red/orange, CLAY with silt, damp N/A
10 Red/orange, CLAY with silt, damp N/A
15 Red/orange, CLAY with silt, damp N/A
20 Tan, SILT with clay, damp N/A
25 Tan, SILT with clay, damp N/A
30 Tan, SILT with clay, damp N/A
35 Tan, SILT with clay, damp N/A
40 Tan, SILT with clay, damp N/A
45 Tan, SILT with clay, moist N/A
P-2104A
Soil Boring Terminated at 45'

APPENDIX B
WELL CONSTRUCTION RECORD
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
3/15/2021 MW-1
Quality Mart #42
1465 River Ridge Dr. Clemmons 27012
Forsyth
36 4 30.40 80 23 24.00
45
33.67
8
Auger
3/18/2021
33.67 45
0 25 2 sch40 pvc
25 45 2 0.010 sch40 pvc
3
0
23
23
3
45
Bentonite
Cement
#2 Sand Poured
Poured/500LB
See Consultant Logs
Poured/65LB

APPENDIX C

STANDARD OPERATING PROCEDURES

STANDARD OPERATING PROCEDURES
PARAGON ENVIRONMENTAL CONSULTANTS, INC.

I. SOIL SAMPLE PROCEDURES
1. Collect all samples using disposable Latex gloves. Gloves are not to be re- used. 2. Place samples into laboratory supplied glassware following requirements for specific analysis. 3. Label samples with sample ID, date, time, and job number. Immediately place samples on ice or in refrigerator to be cooled to approximately 4 degrees Celsius. 4. Store all samples on ice or refrigerate until samples are delivered to the laboratory. 5. Complete a chain of custody record for samples to be submitted to laboratory. Sign and date the chain of custody when samples are relinquished in accordance with EPA chain of custody protocol. II. GROUNDWATER SAMPLING 1. Use new disposable bailer and new nylon string to develop well and collect sample. Handle bailer and string with Latex gloves. 2. Develop well by removing 3 well volumes of water. Dispose of water in accordance with NCDEQ guidelines. 3. Following well development obtain samples in laboratory supplied glassware following requirements for specific analysis. 4. Handle, store, and transport samples in same manner as for soil samples. See items I.3, I.4, and I.5 above. III. EQUIPMENT CONTAMINATION 1. Decontaminate augers, split spoons, and other sampling equipment by the following procedure: A. Soap and tap water wash B. Tap water rinse C. Distilled deionized water rinse D. Isopropyl alcohol rinse E. Distilled water rinse 2. Use new disposable sampling equipment whenever practical.
SOP

APPENDIX D

LABORATORY ANALYTICAL RESULTS

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/30/2021
Paragon Environmental Consultants, Inc. Brandon Moore
PO Box 157 Thomasville, NC, 27361
Ref: Analytical Testing
Lab Report Number: 21-076-0036 Client Project Description: Quality Mart 42
P-2104
Dear Brandon Moore:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/17/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 83
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202137735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202099012State ProgramSouth Carolina
Page 1 of 1 00016/21-076-0036
Page 2 of 83
Report Number:
Sample Summary Table
Client Project Description:
21-076-0036
Quality Mart 42
P-2104
Lab No Client Sample ID Matrix Date Collected Date Received
03/15/2021 13:00Solids 94974 MW1-15 03/17/2021 16:10
03/15/2021 13:20Solids 94975 MW1-25 03/17/2021 16:10
03/16/2021 15:00Aqueous 94976 MW-1 03/17/2021 16:10
03/16/2021Aqueous 94977 Trip Blank 03/17/2021 16:10
Page 3 of 83
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-076-0036
Report Limit
Project:Quality Mart 42
V 94974MW1-15
J0.060 03/23/2021 12:138270EBenzo(a)anthracene mg/Kg - dry 0.010
J0.075 03/23/2021 12:138270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.101 03/23/2021 12:138270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.064 03/23/2021 12:138270EBenzo(g,h,i)perylene mg/Kg - dry 0.008
J0.087 03/23/2021 12:138270EChrysenemg/Kg - dry 0.010
J0.234 03/23/2021 12:138270EFluoranthenemg/Kg - dry 0.009
J0.116 03/23/2021 12:138270EPhenanthrenemg/Kg - dry 0.009
J0.191 03/23/2021 12:138270EPyrenemg/Kg - dry 0.012
22.0 03/22/2021 16:25SW-DRYWT Moisture %
V 94975MW1-25
0.030 03/19/2021 16:268260DAcetonemg/Kg - dry 0.017
J0.006 03/19/2021 16:268260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.001
J0.058 03/23/2021 12:368270EBenzo(a)anthracene mg/Kg - dry 0.009
J0.083 03/23/2021 12:368270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.123 03/23/2021 12:368270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.066 03/23/2021 12:368270EBenzo(g,h,i)perylene mg/Kg - dry 0.007
J0.031 03/23/2021 12:368270EBenzo(k)fluoranthene mg/Kg - dry 0.008
J0.091 03/23/2021 12:368270EChrysenemg/Kg - dry 0.009
J0.259 03/23/2021 12:368270EFluoranthenemg/Kg - dry 0.008
J0.120 03/23/2021 12:368270EPhenanthrenemg/Kg - dry 0.008
J0.215 03/23/2021 12:368270EPyrenemg/Kg - dry 0.011
16.4 03/22/2021 16:25SW-DRYWT Moisture %
V 94976MW-1
32.8 03/26/2021 16:026200BAcetoneµg/L 0.310
50.4 03/26/2021 16:026200BBenzeneµg/L 0.048
J0.691 03/26/2021 16:026200BBromomethaneµg/L 0.180
0.757 03/26/2021 16:026200Bn-Butylbenzene µg/L 0.076
0.546 03/26/2021 16:026200Bsec-Butyl benzene µg/L 0.076
8.36 03/26/2021 16:026200BDi-Isopropyl Ether (DIPE)µg/L 0.500
2000 03/26/2021 16:026200BEthanolµg/L 27.0
57.8 03/26/2021 16:026200BEthylbenzeneµg/L 0.061
8.64 03/26/2021 16:026200B2-Hexanone µg/L 0.065
19.2 03/26/2021 16:026200BIsopropylbenzeneµg/L 0.054
J0.374 03/26/2021 16:026200B4-Isopropyl toluene µg/L 0.089
17.8 03/26/2021 16:026200BMethyl Ethyl Ketone (MEK)µg/L 0.240
43.7 03/26/2021 16:026200BMethyl tert-butyl ether (MTBE)µg/L 0.042
Page 4 of 83
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-076-0036
Report Limit
Project:Quality Mart 42
V 94976MW-1
3.62 03/26/2021 16:026200B4-Methyl-2-Pentanone µg/L 0.078
14.9 03/26/2021 16:026200BNaphthaleneµg/L 0.190
9.47 03/26/2021 16:026200Bn-Propylbenzene µg/L 0.087
J28303/26/2021 15:386200Btert-Butyl Alcohol (TBA)µg/L 64.0
J1.16 03/26/2021 16:026200Btert-Amyl Methyl Ether (TAME)µg/L 0.100
560 03/26/2021 15:386200BTolueneµg/L 4.40
84.6 03/26/2021 16:026200B1,2,4-Trimethylbenzene µg/L 0.054
22.4 03/26/2021 16:026200B1,3,5-Trimethylbenzene µg/L 0.076
133 03/26/2021 15:386200Bo-Xylene µg/L 4.40
259 03/26/2021 15:386200Bm,p-Xylene µg/L 12.0
392 03/26/2021 15:386200BXylene (Total)µg/L 4.40
J8.39 03/23/2021 14:39625.1 Naphthalene µg/L 4.18
1010 03/23/2021 09:40MADEP-VPH Aliphatic C5-C8 µg/L 40.1
890 03/22/2021 12:25MADEP-VPH Aliphatic C9-C12 µg/L 3.88
258 03/22/2021 12:25MADEP-VPH Aromatic C9-C10 µg/L 4.19
V 94977Trip Blank
JB2.22 03/26/2021 13:166200BAcetoneµg/L 0.310
Page 5 of 83

Client: Paragon Environmental Consultants, Inc. CASE NARRATIVE
Project: Quality Mart 42 Lab Report Number: 21-076-0036
Date: 3/26/2021
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 94963 Analyte: Benzidine
QC Batch No: V2172 Analyte did not recover in MS and/or MSD.
Analyte: Benzidine
QC Batch No: V2172 Analyte did not recover in MS and/or MSD.
Analyte: Benzoic Acid
QC Batch No: V2172 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 35.8 ug/l which calculates to a recovery of 35.7% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V2172
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 48.9 ug/l which calculates to a recovery of 44.8% which is within the acceptable recovery range.
Analyte: Pentachlorophenol QC Batch No: V2172 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 41.6 ug/l which calculates to a recovery of 41% which is within the acceptable recovery range.
Analyte: Pentachlorophenol QC Batch No: V2172
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 33.9 ug/l which calculates to a recovery of 31% which is within the acceptable recovery range. Analyte: Benzoic Acid
QC Batch No: V2172/V2025 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual
result was 7.70 ug/l which calculates to a recovery of 15.3% which is within the acceptable recovery range. Analyte: Pentachlorophenol QC Batch No: V2172/V2025 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 17 ug/l which calculates to a recovery of 34% which is within the acceptable recovery range.
Massachusetts EPH Method MADEP-EPH Sample 94958 Analyte: Chlorooctadecane QC Batch No: V1975
Page 6 of 83

Surrogate recovery below range. Sample was used for MS/MSD. MS/MSD surrogate recoveries passed. No
more sample remaining. No further action taken.
Analyte: Aliphatic C19-C36 QC Batch No: V1974/V1932
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Aliphatic C19-C36 QC Batch No: V1974/V1932
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Aliphatic C19-C36 QC Batch No: V1975/V1932
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acetone QC Batch No: V2019/V2018 CCV result is above control limits but within method parameters. Result is reported but considered estimated.
Analyte: Bromomethane
QC Batch No: V2019/V2018 CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found accetable. Result is reported but considered estimated. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 95105
Analyte: 2,4-Dinitrophenol QC Batch No: V2161
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 1210 ug/kg which calculates to a recovery of 73.8% which is within the acceptable recovery range. Analyte: 2,4-Dinitrophenol QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 1240 ug/kg which calculates to a recovery of 75% which is within the acceptable recovery range. Analyte: 3,3`-Dichlorobenzidine QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 490 ug/kg which calculates to a recovery of 29.6% which is within the acceptable recovery range. Analyte: 3,3`-Dichlorobenzidine QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 586 ug/kg which calculates to a recovery of 35.7% which is within the acceptable recovery range.
Page 7 of 83

Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 1140 ug/kg which calculates to a recovery of 69.6% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V2161
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 1150 ug/kg which calculates to a recovery of 65.8% which is within the acceptable recovery range.
Analyte: Aniline
QC Batch No: V2161 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid
QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 1230 ug/kg which calculates to a recovery of 74% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V2161
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 1320 ug/kg which calculates to a recovery of 80% which is within the acceptable recovery range. Analyte: Pyridine
QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 135 ug/kg which calculates to a recovery of 8% which is not within the acceptable recovery range. Analyte: Pyridine QC Batch No: V2161 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 48.4 ug/kg which calculates to a recovery of 3% which is not within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol
QC Batch No: V2161/V2005 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 952 ug/kg which calculates to a recovery of 57% which is within the acceptable recovery range. Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V2161/V2005
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 1090 ug/kg which calculates to a recovery of 65% which is within the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V2161/V2005 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 476 ug/kg which calculates to a recovery of 28% which is within the acceptable recovery range.
Page 8 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.0 %Moisture 1 03/22/21 16:25 SW-DRYWTEDV
<10.3 mg/Kg - dry 10.3 61.3Aliphatic C19-C36 1 03/22/21 20:55 MADEP-EPHZRC
<2.03 mg/Kg - dry 2.03 10.3Aliphatic C5-C8 100 03/18/21 15:19 MADEP-VPHTBL
<0.902 mg/Kg - dry 0.902 10.3Aliphatic C9-C12 100 03/18/21 15:19 MADEP-VPHTBL
<3.06 mg/Kg - dry 3.06 61.3Aliphatic C9-C18 1 03/22/21 20:55 MADEP-EPHZRC
<16.7 mg/Kg - dry 16.7 61.3
Aromatic C11-C22 1 03/22/21 20:55 MADEP-EPHZRC
<0.964 mg/Kg - dry 0.964 10.3Aromatic C9-C10 100 03/18/21 15:19 MADEP-VPHTBL
Surrogate: 2,5-Dibromotoluene (FID)106 Limits: 70-130%03/18/21 15:19100 TBL V1923
Surrogate: 2,5-Dibromotoluene (PID)101 Limits: 70-130%03/18/21 15:19100 TBL V1923
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 9 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.019 mg/Kg - dry 0.019 0.025Acetone 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.025Acrylonitrile 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/19/21 15:56 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/19/21 15:56 V2019TBL
<0.003 mg/Kg - dry 0.003 0.012
Bromomethane 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 03/19/21 15:56 V2019TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chloroform 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/19/21 15:56 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dichloroethane 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/19/21 15:56 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2-Dichloropropane 1 03/19/21 15:56 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/19/21 15:56 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.006trans-1,3-Dichloropropene 1 03/19/21 15:56 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.006Ethylbenzene 1 03/19/21 15:56 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.064Ethyl Tertiary Butyl Ether (ETBE)1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/19/21 15:56 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0004 mg/Kg - dry 0.0004 0.0252-Hexanone 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.025Methyl Ethyl Ketone (MEK)1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/19/21 15:56 V2019TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 03/19/21 15:56 V2019TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.012Naphthalene 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.006
n-Propylbenzene 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 03/19/21 15:56 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0121,2,3-Trichlorobenzene 1 03/19/21 15:56 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.012
1,2,4-Trichlorobenzene 1 03/19/21 15:56 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/19/21 15:56 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/19/21 15:56 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/19/21 15:56 V2019TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/19/21 15:56 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/19/21 15:56 V2019
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/19/21 15:561 TBL V2019
Surrogate: Dibromofluoromethane 100 Limits: 84-123%03/19/21 15:561 TBL V2019
Surrogate: Toluene-d8 96.1 Limits: 76-129%03/19/21 15:561 TBL V2019
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.019 mg/Kg - dry 0.019 0.846Acenaphthene 1 03/23/21 12:13 V2161JMV
<0.016 mg/Kg - dry 0.016 0.846Acenaphthylene 1 03/23/21 12:13 V2161JMV
<0.208 mg/Kg - dry 0.208 0.846Aniline 1 03/23/21 12:13 V2161JMV
<0.009 mg/Kg - dry 0.009 0.846Anthracene 1 03/23/21 12:13 V2161JMV
0.060 J mg/Kg - dry 0.010 0.846Benzo(a)anthracene 1 03/23/21 12:13 V2161JMV
0.075 J mg/Kg - dry 0.007 0.846Benzo(a)pyrene 1 03/23/21 12:13 V2161JMV
0.101 J
mg/Kg - dry 0.007 0.846
Benzo(b)fluoranthene 1 03/23/21 12:13 V2161JMV
0.064 J mg/Kg - dry 0.008 0.846Benzo(g,h,i)perylene 1 03/23/21 12:13 V2161JMV
<0.008 mg/Kg - dry 0.008 0.846Benzo(k)fluoranthene 1 03/23/21 12:13 V2161JMV
<0.702 mg/Kg - dry 0.702 2.56Benzoic Acid 1 03/23/21 12:13 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.158 mg/Kg - dry 0.158 0.846Benzyl alcohol 1 03/23/21 12:13 V2161JMV
<0.161 mg/Kg - dry 0.161 0.846Bis(2-Chloroethoxy)methane 1 03/23/21 12:13 V2161JMV
<0.135 mg/Kg - dry 0.135 0.846Bis(2-Chloroethyl)ether 1 03/23/21 12:13 V2161JMV
<0.151 mg/Kg - dry 0.151 0.423Bis(2-Chloroisopropyl)ether 1 03/23/21 12:13 V2161JMV
<0.191 mg/Kg - dry 0.191 0.846Bis(2-ethylhexyl)phthalate 1 03/23/21 12:13 V2161JMV
<0.198 mg/Kg - dry 0.198 0.8464-Bromophenyl phenyl ether 1 03/23/21 12:13 V2161JMV
<0.146 mg/Kg - dry 0.146 0.423Butyl benzyl phthalate 1 03/23/21 12:13 V2161JMV
<0.161 mg/Kg - dry 0.161 0.8464-Chloro-3-methylphenol 1 03/23/21 12:13 V2161JMV
<0.102 mg/Kg - dry 0.102 0.423
4-Chloroaniline 1 03/23/21 12:13 V2161JMV
<0.206 mg/Kg - dry 0.206 0.8462-Chloronaphthalene 1 03/23/21 12:13 V2161JMV
<0.161 mg/Kg - dry 0.161 0.8462-Chlorophenol 1 03/23/21 12:13 V2161JMV
<0.258 mg/Kg - dry 0.258 1.284-Chlorophenyl phenyl ether 1 03/23/21 12:13 V2161JMV
0.087 J mg/Kg - dry 0.010 0.846Chrysene 1 03/23/21 12:13 V2161JMV
<0.024 mg/Kg - dry 0.024 0.846Dibenz(a,h)anthracene 1 03/23/21 12:13 V2161JMV
<0.022 mg/Kg - dry 0.022 0.846Dibenzofuran 1 03/23/21 12:13 V2161JMV
<0.137 mg/Kg - dry 0.137 0.846
1,2-Dichlorobenzene 1 03/23/21 12:13 V2161JMV
<0.124 mg/Kg - dry 0.124 0.8461,3-Dichlorobenzene 1 03/23/21 12:13 V2161JMV
<0.133 mg/Kg - dry 0.133 0.4231,4-Dichlorobenzene 1 03/23/21 12:13 V2161JMV
<0.167 mg/Kg - dry 0.167 0.8463,3'-Dichlorobenzidine 1 03/23/21 12:13 V2161JMV
<0.165 mg/Kg - dry 0.165 0.8462,4-Dichlorophenol 1 03/23/21 12:13 V2161JMV
<0.217 mg/Kg - dry 0.217 0.846Diethyl phthalate 1 03/23/21 12:13 V2161JMV
<0.202 mg/Kg - dry 0.202 0.846Dimethyl phthalate 1 03/23/21 12:13 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.175 mg/Kg - dry 0.175 0.4232,4-Dimethylphenol 1 03/23/21 12:13 V2161JMV
<0.210 mg/Kg - dry 0.210 0.846Di-n-butyl phthalate 1 03/23/21 12:13 V2161JMV
<0.466 mg/Kg - dry 0.466 1.924,6-Dinitro-2-methylphenol 1 03/23/21 12:13 V2161JMV
<0.496 mg/Kg - dry 0.496 1.922,4-Dinitrophenol 1 03/23/21 12:13 V2161JMV
<0.224 mg/Kg - dry 0.224 0.8462,4-Dinitrotoluene 1 03/23/21 12:13 V2161JMV
<0.219 mg/Kg - dry 0.219 0.8462,6-Dinitrotoluene 1 03/23/21 12:13 V2161JMV
<0.219 mg/Kg - dry 0.219 0.423Di-n-Octyl Phthalate 1 03/23/21 12:13 V2161JMV
0.234 J mg/Kg - dry 0.009 0.846Fluoranthene 1 03/23/21 12:13 V2161JMV
<0.018 mg/Kg - dry 0.018 0.846
Fluorene 1 03/23/21 12:13 V2161JMV
<0.185 mg/Kg - dry 0.185 0.846Hexachlorobenzene 1 03/23/21 12:13 V2161JMV
<0.191 mg/Kg - dry 0.191 0.846Hexachlorobutadiene 1 03/23/21 12:13 V2161JMV
<0.291 mg/Kg - dry 0.291 0.846Hexachlorocyclopentadiene 1 03/23/21 12:13 V2161JMV
<0.133 mg/Kg - dry 0.133 0.846Hexachloroethane 1 03/23/21 12:13 V2161JMV
<0.023 mg/Kg - dry 0.023 0.846Indeno(1,2,3-cd)pyrene 1 03/23/21 12:13 V2161JMV
<0.182 mg/Kg - dry 0.182 0.846Isophorone 1 03/23/21 12:13 V2161JMV
<0.012 mg/Kg - dry 0.012 0.846
1-Methylnaphthalene 1 03/23/21 12:13 V2161JMV
<0.016 mg/Kg - dry 0.016 0.8462-Methylnaphthalene 1 03/23/21 12:13 V2161JMV
<0.161 mg/Kg - dry 0.161 0.8462-Methylphenol 1 03/23/21 12:13 V2161JMV
<0.183 mg/Kg - dry 0.183 0.8463&4 Methylphenol 1 03/23/21 12:13 V2161JMV
<0.017 mg/Kg - dry 0.017 0.846Naphthalene 1 03/23/21 12:13 V2161JMV
<0.182 mg/Kg - dry 0.182 0.8462-Nitroaniline 1 03/23/21 12:13 V2161JMV
<0.153 mg/Kg - dry 0.153 0.8463-Nitroaniline 1 03/23/21 12:13 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-15
94974 Matrix:
3/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.132 mg/Kg - dry 0.132 0.4234-Nitroaniline 1 03/23/21 12:13 V2161JMV
<0.179 mg/Kg - dry 0.179 0.423Nitrobenzene 1 03/23/21 12:13 V2161JMV
<0.141 mg/Kg - dry 0.141 0.8462-Nitrophenol 1 03/23/21 12:13 V2161JMV
<0.208 mg/Kg - dry 0.208 0.8464-Nitrophenol 1 03/23/21 12:13 V2161JMV
<0.007 mg/Kg - dry 0.007 0.217N-Nitrosodimethylamine 1 03/23/21 12:13 V2161JMV
<0.232 mg/Kg - dry 0.232 0.846N-Nitrosodiphenylamine 1 03/23/21 12:13 V2161JMV
<0.194 mg/Kg - dry 0.194 0.846N-Nitroso-di-n-propylamine 1 03/23/21 12:13 V2161JMV
<0.539 mg/Kg - dry 0.539 1.28Pentachlorophenol 1 03/23/21 12:13 V2161JMV
0.116 J
mg/Kg - dry 0.009 0.846
Phenanthrene 1 03/23/21 12:13 V2161JMV
<0.138 mg/Kg - dry 0.138 0.846Phenol 1 03/23/21 12:13 V2161JMV
0.191 J mg/Kg - dry 0.012 0.846Pyrene 1 03/23/21 12:13 V2161JMV
<0.080 mg/Kg - dry 0.080 0.423Pyridine 1 03/23/21 12:13 V2161JMV
<0.150 mg/Kg - dry 0.150 0.8461,2,4-Trichlorobenzene 1 03/23/21 12:13 V2161JMV
<0.179 mg/Kg - dry 0.179 0.8462,4,5-Trichlorophenol 1 03/23/21 12:13 V2161JMV
<0.205 mg/Kg - dry 0.205 0.8462,4,6-Trichlorophenol 1 03/23/21 12:13 V2161JMV
Surrogate: 2-Fluorobiphenyl 88.0 Limits: 44-115%03/23/21 12:131 JMV V2161
Surrogate: 2-Fluorophenol 68.8 Limits: 35-115%03/23/21 12:131 JMV V2161
Surrogate: Nitrobenzene-d5 76.6 Limits: 37-122%03/23/21 12:131 JMV V2161
Surrogate: 4-Terphenyl-d14 83.8 Limits: 54-127%03/23/21 12:131 JMV V2161
Surrogate: 2,4,6-Tribromophenol 72.7 Limits: 39-132%03/23/21 12:131 JMV V2161
Surrogate: Phenol-d5 68.5 Limits: 34-121%03/23/21 12:131 JMV V2161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.4 %Moisture 1 03/22/21 16:25 SW-DRYWTEDV
<9.84 mg/Kg - dry 9.84 58.5Aliphatic C19-C36 1 03/22/21 21:32 MADEP-EPHZRC
<1.89 mg/Kg - dry 1.89 9.57Aliphatic C5-C8 100 03/18/21 15:49 MADEP-VPHTBL
<842 µg/Kg - dry 842 9570Aliphatic C9-C12 100 03/18/21 15:49 MADEP-VPHTBL
<2.93 mg/Kg - dry 2.93 58.5Aliphatic C9-C18 1 03/22/21 21:32 MADEP-EPHZRC
<15.9 mg/Kg - dry 15.9 58.5
Aromatic C11-C22 1 03/22/21 21:32 MADEP-EPHZRC
<900 µg/Kg - dry 900 9570Aromatic C9-C10 100 03/18/21 15:49 MADEP-VPHTBL
Surrogate: 2,5-Dibromotoluene (FID)110 Limits: 70-130%03/18/21 15:49100 TBL V1923
Surrogate: 2,5-Dibromotoluene (PID)105 Limits: 70-130%03/18/21 15:49100 TBL V1923
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
0.030 mg/Kg - dry 0.017 0.023Acetone 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.023Acrylonitrile 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005Benzene 1 03/19/21 16:26 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromobenzene 1 03/19/21 16:26 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromodichloromethane 1 03/19/21 16:26 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromoform 1 03/19/21 16:26 V2019TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.005tert-Butyl benzene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Disulfide 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005Chlorobenzene 1 03/19/21 16:26 V2019TBL
<0.0004 mg/Kg - dry 0.0004 0.005
Chlorodibromomethane 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chloroform 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011Chloromethane 1 03/19/21 16:26 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0052-Chlorotoluene 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0054-Chlorotoluene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 03/19/21 16:26 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0111,2-Dibromo-3-Chloropropane 1 03/19/21 16:26 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dibromoethane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dichlorobenzene 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichlorobenzene 1 03/19/21 16:26 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,4-Dichlorobenzene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0051,1-Dichloroethane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dichloroethane 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0051,1-Dichloroethene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2-Dichloropropane 1 03/19/21 16:26 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichloropropane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0052,2-Dichloropropane 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/19/21 16:26 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.005trans-1,3-Dichloropropene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005Ethylbenzene 1 03/19/21 16:26 V2019TBL
<0.0005 mg/Kg - dry 0.0005 0.059Ethyl Tertiary Butyl Ether (ETBE)1 03/19/21 16:26 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.011Hexachlorobutadiene 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 03/19/21 16:26 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0004 mg/Kg - dry 0.0004 0.0232-Hexanone 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.005Isopropylbenzene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/19/21 16:26 V2019TBL
0.006 J mg/Kg - dry 0.001 0.023Methyl Ethyl Ketone (MEK)1 03/19/21 16:26 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.005Methyl tert-butyl ether (MTBE)1 03/19/21 16:26 V2019TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 03/19/21 16:26 V2019TBL
<0.005 mg/Kg - dry 0.005 0.011Methylene Chloride 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.011Naphthalene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.005
n-Propylbenzene 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005Styrene 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,1,1,2-Tetrachloroethane 1 03/19/21 16:26 V2019TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 03/19/21 16:26 V2019TBL
<0.0010 mg/Kg - dry 0.0010 0.005Toluene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0111,2,3-Trichlorobenzene 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,4-Trichlorobenzene 1 03/19/21 16:26 V2019TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1,1-Trichloroethane 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011Trichlorofluoromethane 1 03/19/21 16:26 V2019TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2,3-Trichloropropane 1 03/19/21 16:26 V2019TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,3,5-Trimethylbenzene 1 03/19/21 16:26 V2019TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V2018 03/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Acetate 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011Vinyl Chloride 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 03/19/21 16:26 V2019TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 03/19/21 16:26 V2019TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 03/19/21 16:26 V2019
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%03/19/21 16:261 TBL V2019
Surrogate: Dibromofluoromethane 105 Limits: 84-123%03/19/21 16:261 TBL V2019
Surrogate: Toluene-d8 97.4 Limits: 76-129%03/19/21 16:261 TBL V2019
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.018 mg/Kg - dry 0.018 0.790Acenaphthene 1 03/23/21 12:36 V2161JMV
<0.015 mg/Kg - dry 0.015 0.790Acenaphthylene 1 03/23/21 12:36 V2161JMV
<0.194 mg/Kg - dry 0.194 0.790Aniline 1 03/23/21 12:36 V2161JMV
<0.008 mg/Kg - dry 0.008 0.790Anthracene 1 03/23/21 12:36 V2161JMV
0.058 J mg/Kg - dry 0.009 0.790Benzo(a)anthracene 1 03/23/21 12:36 V2161JMV
0.083 J mg/Kg - dry 0.007 0.790Benzo(a)pyrene 1 03/23/21 12:36 V2161JMV
0.123 J
mg/Kg - dry 0.007 0.790
Benzo(b)fluoranthene 1 03/23/21 12:36 V2161JMV
0.066 J mg/Kg - dry 0.007 0.790Benzo(g,h,i)perylene 1 03/23/21 12:36 V2161JMV
0.031 J mg/Kg - dry 0.008 0.790Benzo(k)fluoranthene 1 03/23/21 12:36 V2161JMV
<0.655 mg/Kg - dry 0.655 2.39Benzoic Acid 1 03/23/21 12:36 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.148 mg/Kg - dry 0.148 0.790Benzyl alcohol 1 03/23/21 12:36 V2161JMV
<0.150 mg/Kg - dry 0.150 0.790Bis(2-Chloroethoxy)methane 1 03/23/21 12:36 V2161JMV
<0.126 mg/Kg - dry 0.126 0.790Bis(2-Chloroethyl)ether 1 03/23/21 12:36 V2161JMV
<0.141 mg/Kg - dry 0.141 0.395Bis(2-Chloroisopropyl)ether 1 03/23/21 12:36 V2161JMV
<0.178 mg/Kg - dry 0.178 0.790Bis(2-ethylhexyl)phthalate 1 03/23/21 12:36 V2161JMV
<0.185 mg/Kg - dry 0.185 0.7904-Bromophenyl phenyl ether 1 03/23/21 12:36 V2161JMV
<0.136 mg/Kg - dry 0.136 0.395Butyl benzyl phthalate 1 03/23/21 12:36 V2161JMV
<0.150 mg/Kg - dry 0.150 0.7904-Chloro-3-methylphenol 1 03/23/21 12:36 V2161JMV
<0.095 mg/Kg - dry 0.095 0.395
4-Chloroaniline 1 03/23/21 12:36 V2161JMV
<0.192 mg/Kg - dry 0.192 0.7902-Chloronaphthalene 1 03/23/21 12:36 V2161JMV
<0.150 mg/Kg - dry 0.150 0.7902-Chlorophenol 1 03/23/21 12:36 V2161JMV
<0.241 mg/Kg - dry 0.241 1.204-Chlorophenyl phenyl ether 1 03/23/21 12:36 V2161JMV
0.091 J mg/Kg - dry 0.009 0.790Chrysene 1 03/23/21 12:36 V2161JMV
<0.022 mg/Kg - dry 0.022 0.790Dibenz(a,h)anthracene 1 03/23/21 12:36 V2161JMV
<0.021 mg/Kg - dry 0.021 0.790Dibenzofuran 1 03/23/21 12:36 V2161JMV
<0.127 mg/Kg - dry 0.127 0.790
1,2-Dichlorobenzene 1 03/23/21 12:36 V2161JMV
<0.116 mg/Kg - dry 0.116 0.7901,3-Dichlorobenzene 1 03/23/21 12:36 V2161JMV
<0.124 mg/Kg - dry 0.124 0.3951,4-Dichlorobenzene 1 03/23/21 12:36 V2161JMV
<0.156 mg/Kg - dry 0.156 0.7903,3'-Dichlorobenzidine 1 03/23/21 12:36 V2161JMV
<0.154 mg/Kg - dry 0.154 0.7902,4-Dichlorophenol 1 03/23/21 12:36 V2161JMV
<0.203 mg/Kg - dry 0.203 0.790Diethyl phthalate 1 03/23/21 12:36 V2161JMV
<0.188 mg/Kg - dry 0.188 0.790Dimethyl phthalate 1 03/23/21 12:36 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.163 mg/Kg - dry 0.163 0.3952,4-Dimethylphenol 1 03/23/21 12:36 V2161JMV
<0.196 mg/Kg - dry 0.196 0.790Di-n-butyl phthalate 1 03/23/21 12:36 V2161JMV
<0.435 mg/Kg - dry 0.435 1.794,6-Dinitro-2-methylphenol 1 03/23/21 12:36 V2161JMV
<0.462 mg/Kg - dry 0.462 1.792,4-Dinitrophenol 1 03/23/21 12:36 V2161JMV
<0.209 mg/Kg - dry 0.209 0.7902,4-Dinitrotoluene 1 03/23/21 12:36 V2161JMV
<0.204 mg/Kg - dry 0.204 0.7902,6-Dinitrotoluene 1 03/23/21 12:36 V2161JMV
<0.205 mg/Kg - dry 0.205 0.395Di-n-Octyl Phthalate 1 03/23/21 12:36 V2161JMV
0.259 J mg/Kg - dry 0.008 0.790Fluoranthene 1 03/23/21 12:36 V2161JMV
<0.017 mg/Kg - dry 0.017 0.790
Fluorene 1 03/23/21 12:36 V2161JMV
<0.173 mg/Kg - dry 0.173 0.790Hexachlorobenzene 1 03/23/21 12:36 V2161JMV
<0.178 mg/Kg - dry 0.178 0.790Hexachlorobutadiene 1 03/23/21 12:36 V2161JMV
<0.271 mg/Kg - dry 0.271 0.790Hexachlorocyclopentadiene 1 03/23/21 12:36 V2161JMV
<0.124 mg/Kg - dry 0.124 0.790Hexachloroethane 1 03/23/21 12:36 V2161JMV
<0.022 mg/Kg - dry 0.022 0.790Indeno(1,2,3-cd)pyrene 1 03/23/21 12:36 V2161JMV
<0.169 mg/Kg - dry 0.169 0.790Isophorone 1 03/23/21 12:36 V2161JMV
<0.012 mg/Kg - dry 0.012 0.790
1-Methylnaphthalene 1 03/23/21 12:36 V2161JMV
<0.015 mg/Kg - dry 0.015 0.7902-Methylnaphthalene 1 03/23/21 12:36 V2161JMV
<0.150 mg/Kg - dry 0.150 0.7902-Methylphenol 1 03/23/21 12:36 V2161JMV
<0.171 mg/Kg - dry 0.171 0.7903&4 Methylphenol 1 03/23/21 12:36 V2161JMV
<0.016 mg/Kg - dry 0.016 0.790Naphthalene 1 03/23/21 12:36 V2161JMV
<0.169 mg/Kg - dry 0.169 0.7902-Nitroaniline 1 03/23/21 12:36 V2161JMV
<0.143 mg/Kg - dry 0.143 0.7903-Nitroaniline 1 03/23/21 12:36 V2161JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW1-25
94975 Matrix:
3/15/2021 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V2005 03/22/21 08:18
<0.123 mg/Kg - dry 0.123 0.3954-Nitroaniline 1 03/23/21 12:36 V2161JMV
<0.167 mg/Kg - dry 0.167 0.395Nitrobenzene 1 03/23/21 12:36 V2161JMV
<0.131 mg/Kg - dry 0.131 0.7902-Nitrophenol 1 03/23/21 12:36 V2161JMV
<0.194 mg/Kg - dry 0.194 0.7904-Nitrophenol 1 03/23/21 12:36 V2161JMV
<0.006 mg/Kg - dry 0.006 0.203N-Nitrosodimethylamine 1 03/23/21 12:36 V2161JMV
<0.216 mg/Kg - dry 0.216 0.790N-Nitrosodiphenylamine 1 03/23/21 12:36 V2161JMV
<0.181 mg/Kg - dry 0.181 0.790N-Nitroso-di-n-propylamine 1 03/23/21 12:36 V2161JMV
<0.503 mg/Kg - dry 0.503 1.20Pentachlorophenol 1 03/23/21 12:36 V2161JMV
0.120 J
mg/Kg - dry 0.008 0.790
Phenanthrene 1 03/23/21 12:36 V2161JMV
<0.129 mg/Kg - dry 0.129 0.790Phenol 1 03/23/21 12:36 V2161JMV
0.215 J mg/Kg - dry 0.011 0.790Pyrene 1 03/23/21 12:36 V2161JMV
<0.075 mg/Kg - dry 0.075 0.395Pyridine 1 03/23/21 12:36 V2161JMV
<0.139 mg/Kg - dry 0.139 0.7901,2,4-Trichlorobenzene 1 03/23/21 12:36 V2161JMV
<0.167 mg/Kg - dry 0.167 0.7902,4,5-Trichlorophenol 1 03/23/21 12:36 V2161JMV
<0.191 mg/Kg - dry 0.191 0.7902,4,6-Trichlorophenol 1 03/23/21 12:36 V2161JMV
Surrogate: 2-Fluorobiphenyl 90.4 Limits: 44-115%03/23/21 12:361 JMV V2161
Surrogate: 2-Fluorophenol 71.3 Limits: 35-115%03/23/21 12:361 JMV V2161
Surrogate: Nitrobenzene-d5 74.3 Limits: 37-122%03/23/21 12:361 JMV V2161
Surrogate: 4-Terphenyl-d14 85.6 Limits: 54-127%03/23/21 12:361 JMV V2161
Surrogate: 2,4,6-Tribromophenol 73.4 Limits: 39-132%03/23/21 12:361 JMV V2161
Surrogate: Phenol-d5 69.5 Limits: 34-121%03/23/21 12:361 JMV V2161
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.260 µg/L 0.260 1.00Lead 1 03/22/21 20:27 6020BMMR
<126 µg/L 126 515Aliphatic C19-C36 1 03/23/21 01:10 MADEP-EPHZRC
1010 µg/L 40.1 500Aliphatic C5-C8 10 03/23/21 09:40 MADEP-VPHTBL
890 µg/L 3.88 50.0Aliphatic C9-C12 1 03/22/21 12:25 MADEP-VPHTBL
<23.9 µg/L 23.9 361Aliphatic C9-C18 1 03/23/21 01:10 MADEP-EPHZRC
<82.8 µg/L 82.8 258
Aromatic C11-C22 1 03/23/21 01:10 MADEP-EPHZRC
258 µg/L 4.19 50.0Aromatic C9-C10 1 03/22/21 12:25 MADEP-VPHTBL
Surrogate: 2,5-Dibromotoluene (FID)86.0 Limits: 70-130%03/22/21 12:251 TBL V2090
Surrogate: 2,5-Dibromotoluene (PID)83.7 Limits: 70-130%03/22/21 12:251 TBL V2090
Surrogate: 2,5-Dibromotoluene (FID)89.9 Limits: 70-130%03/23/21 09:4010 TBL V2090
Surrogate: 2,5-Dibromotoluene (PID)85.2 Limits: 70-130%03/23/21 09:4010 TBL V2090
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
32.8 µg/L 0.310 10.0Acetone 1 03/26/21 16:02 V2317JLB
50.4 µg/L 0.048 0.500Benzene 1 03/26/21 16:02 V2317JLB
<0.057 µg/L 0.057 0.500Bromobenzene 1 03/26/21 16:02 V2317JLB
<0.140 µg/L 0.140 0.500Bromochloromethane 1 03/26/21 16:02 V2317JLB
<0.062 µg/L 0.062 0.500Bromodichloromethane 1 03/26/21 16:02 V2317JLB
<0.040 µg/L 0.040 0.500Bromoform 1 03/26/21 16:02 V2317JLB
0.691 J µg/L 0.180 1.00Bromomethane 1 03/26/21 16:02 V2317JLB
0.757 µg/L 0.076 0.500n-Butylbenzene 1 03/26/21 16:02 V2317JLB
0.546 µg/L 0.076 0.500
sec-Butyl benzene 1 03/26/21 16:02 V2317JLB
<0.088 µg/L 0.088 0.500tert-Butyl benzene 1 03/26/21 16:02 V2317JLB
<0.110 µg/L 0.110 0.500Carbon Tetrachloride 1 03/26/21 16:02 V2317JLB
<0.062 µg/L 0.062 0.500Chlorobenzene 1 03/26/21 16:02 V2317JLB
<0.080 µg/L 0.080 0.500Chlorodibromomethane 1 03/26/21 16:02 V2317JLB
<0.220 µg/L 0.220 0.500Chloroethane 1 03/26/21 16:02 V2317JLB
<0.076 µg/L 0.076 0.500Chloroform 1 03/26/21 16:02 V2317JLB
<0.079 µg/L 0.079 0.500
Chloromethane 1 03/26/21 16:02 V2317JLB
<0.066 µg/L 0.066 0.5002-Chlorotoluene 1 03/26/21 16:02 V2317JLB
<0.050 µg/L 0.050 0.5004-Chlorotoluene 1 03/26/21 16:02 V2317JLB
8.36 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/26/21 16:02 V2317JLB
<0.170 µg/L 0.170 2.001,2-Dibromo-3-Chloropropane 1 03/26/21 16:02 V2317JLB
<0.051 µg/L 0.051 0.5001,2-Dibromoethane 1 03/26/21 16:02 V2317JLB
<0.065 µg/L 0.065 0.500Dibromomethane 1 03/26/21 16:02 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
<0.076 µg/L 0.076 0.5001,2-Dichlorobenzene 1 03/26/21 16:02 V2317JLB
<0.054 µg/L 0.054 0.5001,3-Dichlorobenzene 1 03/26/21 16:02 V2317JLB
<0.050 µg/L 0.050 0.5001,4-Dichlorobenzene 1 03/26/21 16:02 V2317JLB
<0.110 µg/L 0.110 1.00Dichlorodifluoromethane 1 03/26/21 16:02 V2317JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethane 1 03/26/21 16:02 V2317JLB
<0.066 µg/L 0.066 0.5001,2-Dichloroethane 1 03/26/21 16:02 V2317JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethene 1 03/26/21 16:02 V2317JLB
<0.056 µg/L 0.056 0.500cis-1,2-Dichloroethene 1 03/26/21 16:02 V2317JLB
<0.070 µg/L 0.070 0.500
trans-1,2-Dichloroethene 1 03/26/21 16:02 V2317JLB
<0.110 µg/L 0.110 0.5001,2-Dichloropropane 1 03/26/21 16:02 V2317JLB
<0.043 µg/L 0.043 0.5001,3-Dichloropropane 1 03/26/21 16:02 V2317JLB
<0.110 µg/L 0.110 2.002,2-Dichloropropane 1 03/26/21 16:02 V2317JLB
<0.051 µg/L 0.051 0.5001,1-Dichloropropene 1 03/26/21 16:02 V2317JLB
<0.079 µg/L 0.079 0.500cis-1,3-Dichloropropene 1 03/26/21 16:02 V2317JLB
<0.120 µg/L 0.120 0.500trans-1,3-Dichloropropene 1 03/26/21 16:02 V2317JLB
2000 µg/L 27.0 200
Ethanol 1 03/26/21 16:02 V2317JLB
57.8 µg/L 0.061 0.500Ethylbenzene 1 03/26/21 16:02 V2317JLB
<0.160 µg/L 0.160 3.00Hexachlorobutadiene 1 03/26/21 16:02 V2317JLB
8.64 µg/L 0.065 1.002-Hexanone 1 03/26/21 16:02 V2317JLB
19.2 µg/L 0.054 0.500Isopropylbenzene 1 03/26/21 16:02 V2317JLB
0.374 J µg/L 0.089 0.5004-Isopropyl toluene 1 03/26/21 16:02 V2317JLB
17.8 µg/L 0.240 5.00Methyl Ethyl Ketone (MEK)1 03/26/21 16:02 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
43.7 µg/L 0.042 1.00Methyl tert-butyl ether (MTBE)1 03/26/21 16:02 V2317JLB
3.62 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/26/21 16:02 V2317JLB
<0.083 µg/L 0.083 2.00Methylene Chloride 1 03/26/21 16:02 V2317JLB
14.9 µg/L 0.190 1.00Naphthalene 1 03/26/21 16:02 V2317JLB
9.47 µg/L 0.087 0.500n-Propylbenzene 1 03/26/21 16:02 V2317JLB
<0.047 µg/L 0.047 0.500Styrene 1 03/26/21 16:02 V2317JLB
283 J µg/L 64.0 1000tert-Butyl Alcohol (TBA)100 03/26/21 15:38 V2317JLB
<0.250 µg/L 0.250 10.0tert-Butyl formate (TBF)1 03/26/21 16:02 V2317JLB
<0.720 µg/L 0.720 10.0
tert-Amyl alcohol (TAA)1 03/26/21 16:02 V2317JLB
1.16 J µg/L 0.100 10.0tert-Amyl Methyl Ether (TAME)1 03/26/21 16:02 V2317JLB
<0.110 µg/L 0.110 0.5001,1,1,2-Tetrachloroethane 1 03/26/21 16:02 V2317JLB
<0.036 µg/L 0.036 0.5001,1,2,2-Tetrachloroethane 1 03/26/21 16:02 V2317JLB
<0.098 µg/L 0.098 0.500Tetrachloroethene 1 03/26/21 16:02 V2317JLB
560 µg/L 4.40 50.0Toluene 100 03/26/21 15:38 V2317JLB
<0.400 µg/L 0.400 0.5001,2,3-Trichlorobenzene 1 03/26/21 16:02 V2317JLB
<0.130 µg/L 0.130 0.500
1,2,4-Trichlorobenzene 1 03/26/21 16:02 V2317JLB
<0.061 µg/L 0.061 0.5001,1,1-Trichloroethane 1 03/26/21 16:02 V2317JLB
<0.066 µg/L 0.066 0.5001,1,2-Trichloroethane 1 03/26/21 16:02 V2317JLB
<0.078 µg/L 0.078 0.500Trichloroethene 1 03/26/21 16:02 V2317JLB
<0.062 µg/L 0.062 0.500Trichlorofluoromethane 1 03/26/21 16:02 V2317JLB
<0.140 µg/L 0.140 0.5001,2,3-Trichloropropane 1 03/26/21 16:02 V2317JLB
84.6 µg/L 0.054 0.5001,2,4-Trimethylbenzene 1 03/26/21 16:02 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
22.4 µg/L 0.076 0.5001,3,5-Trimethylbenzene 1 03/26/21 16:02 V2317JLB
<0.060 µg/L 0.060 5.00Vinyl Acetate 1 03/26/21 16:02 V2317JLB
<0.097 µg/L 0.097 0.500Vinyl Chloride 1 03/26/21 16:02 V2317JLB
133 µg/L 4.40 50.0o-Xylene 100 03/26/21 15:38 V2317JLB
259 µg/L 12.0 100m,p-Xylene 100 03/26/21 15:38 V2317JLB
392 µg/L 4.40 50.0Xylene (Total)100 03/26/21 15:38 V2317
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%03/26/21 16:021 JLB V2317
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%03/26/21 16:021 JLB V2317
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%03/26/21 16:021 JLB V2317
Surrogate: Toluene-d8 100 Limits: 70-130%03/26/21 16:021 JLB V2317
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%03/26/21 15:38100 JLB V2317
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%03/26/21 15:38100 JLB V2317
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%03/26/21 15:38100 JLB V2317
Surrogate: Toluene-d8 103 Limits: 70-130%03/26/21 15:38100 JLB V2317
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V2025 03/22/21 10:30
<4.39 µg/L 4.39 10.2Acenaphthene 1 03/23/21 14:39 V2172JMV
<4.49 µg/L 4.49 20.4Acenaphthylene 1 03/23/21 14:39 V2172JMV
<4.69 µg/L 4.69 10.2Anthracene 1 03/23/21 14:39 V2172JMV
<4.18 µg/L 4.18 10.2Benzidine 1 03/23/21 14:39 V2172JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V2025 03/22/21 10:30
<3.26 µg/L 3.26 10.2Benzo(a)anthracene 1 03/23/21 14:39 V2172JMV
<3.57 µg/L 3.57 10.2Benzo(a)pyrene 1 03/23/21 14:39 V2172JMV
<3.57 µg/L 3.57 10.2Benzo(b)fluoranthene 1 03/23/21 14:39 V2172JMV
<3.67 µg/L 3.67 10.2Benzo(g,h,i)perylene 1 03/23/21 14:39 V2172JMV
<2.65 µg/L 2.65 10.2Benzo(k)fluoranthene 1 03/23/21 14:39 V2172JMV
<19.4 µg/L 19.4 102Benzoic Acid 1 03/23/21 14:39 V2172JMV
<2.55 µg/L 2.55 10.2Benzyl alcohol 1 03/23/21 14:39 V2172JMV
<3.88 µg/L 3.88 10.2Bis(2-Chloroethoxy)methane 1 03/23/21 14:39 V2172JMV
<2.65 µg/L 2.65 10.2
Bis(2-Chloroethyl)ether 1 03/23/21 14:39 V2172JMV
<2.86 µg/L 2.86 10.2Bis(2-Chloroisopropyl)ether 1 03/23/21 14:39 V2172JMV
<3.77 µg/L 3.77 10.2Bis(2-ethylhexyl)phthalate 1 03/23/21 14:39 V2172JMV
<4.49 µg/L 4.49 20.44-Bromophenyl phenyl ether 1 03/23/21 14:39 V2172JMV
<2.96 µg/L 2.96 10.2Butyl benzyl phthalate 1 03/23/21 14:39 V2172JMV
<2.96 µg/L 2.96 10.24-Chloro-3-methylphenol 1 03/23/21 14:39 V2172JMV
<4.79 µg/L 4.79 20.42-Chloronaphthalene 1 03/23/21 14:39 V2172JMV
<2.75 µg/L 2.75 10.2
2-Chlorophenol 1 03/23/21 14:39 V2172JMV
<4.79 µg/L 4.79 20.44-Chlorophenyl phenyl ether 1 03/23/21 14:39 V2172JMV
<3.37 µg/L 3.37 10.2Chrysene 1 03/23/21 14:39 V2172JMV
<5.81 µg/L 5.81 20.4Dibenz(a,h)anthracene 1 03/23/21 14:39 V2172JMV
<4.28 µg/L 4.28 20.4Dibenzofuran 1 03/23/21 14:39 V2172JMV
<2.45 µg/L 2.45 10.21,2-Dichlorobenzene 1 03/23/21 14:39 V2172JMV
<3.98 µg/L 3.98 10.21,3-Dichlorobenzene 1 03/23/21 14:39 V2172JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V2025 03/22/21 10:30
<4.18 µg/L 4.18 10.21,4-Dichlorobenzene 1 03/23/21 14:39 V2172JMV
<3.98 µg/L 3.98 10.23,3'-Dichlorobenzidine 1 03/23/21 14:39 V2172JMV
<2.65 µg/L 2.65 10.22,4-Dichlorophenol 1 03/23/21 14:39 V2172JMV
<4.28 µg/L 4.28 20.4Diethyl phthalate 1 03/23/21 14:39 V2172JMV
<4.18 µg/L 4.18 10.2Dimethyl phthalate 1 03/23/21 14:39 V2172JMV
<5.00 µg/L 5.00 10.22,4-Dimethylphenol 1 03/23/21 14:39 V2172JMV
<4.39 µg/L 4.39 10.2Di-n-butyl phthalate 1 03/23/21 14:39 V2172JMV
<11.2 µg/L 11.2 30.64,6-Dinitro-2-methylphenol 1 03/23/21 14:39 V2172JMV
<12.2 µg/L 12.2 30.6
2,4-Dinitrophenol 1 03/23/21 14:39 V2172JMV
<4.28 µg/L 4.28 10.22,4-Dinitrotoluene 1 03/23/21 14:39 V2172JMV
<3.98 µg/L 3.98 20.42,6-Dinitrotoluene 1 03/23/21 14:39 V2172JMV
<4.59 µg/L 4.59 10.2Di-n-Octyl Phthalate 1 03/23/21 14:39 V2172JMV
<4.08 µg/L 4.08 10.2Fluoranthene 1 03/23/21 14:39 V2172JMV
<5.10 µg/L 5.10 10.2Fluorene 1 03/23/21 14:39 V2172JMV
<3.98 µg/L 3.98 20.4Hexachlorobenzene 1 03/23/21 14:39 V2172JMV
<4.59 µg/L 4.59 20.4
Hexachlorobutadiene 1 03/23/21 14:39 V2172JMV
<7.45 µg/L 7.45 20.4Hexachlorocyclopentadiene 1 03/23/21 14:39 V2172JMV
<3.77 µg/L 3.77 10.2Hexachloroethane 1 03/23/21 14:39 V2172JMV
<2.65 µg/L 2.65 10.2Indeno(1,2,3-cd)pyrene 1 03/23/21 14:39 V2172JMV
<4.18 µg/L 4.18 10.2Isophorone 1 03/23/21 14:39 V2172JMV
8.39 J µg/L 4.18 10.2Naphthalene 1 03/23/21 14:39 V2172JMV
<3.88 µg/L 3.88 10.2Nitrobenzene 1 03/23/21 14:39 V2172JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:MW-1
94976 Matrix:
3/16/2021 15:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V2025 03/22/21 10:30
<2.65 µg/L 2.65 10.22-Nitrophenol 1 03/23/21 14:39 V2172JMV
<2.65 µg/L 2.65 10.24-Nitrophenol 1 03/23/21 14:39 V2172JMV
<4.49 µg/L 4.49 20.4N-Nitrosodiphenylamine 1 03/23/21 14:39 V2172JMV
<3.37 µg/L 3.37 20.4N-Nitroso-di-n-propylamine 1 03/23/21 14:39 V2172JMV
<11.2 µg/L 11.2 51.0Pentachlorophenol 1 03/23/21 14:39 V2172JMV
<3.98 µg/L 3.98 10.2Phenanthrene 1 03/23/21 14:39 V2172JMV
<1.43 µg/L 1.43 10.2Phenol 1 03/23/21 14:39 V2172JMV
<3.57 µg/L 3.57 10.2Pyrene 1 03/23/21 14:39 V2172JMV
<3.06 µg/L 3.06 10.2
1,2,4-Trichlorobenzene 1 03/23/21 14:39 V2172JMV
<4.59 µg/L 4.59 20.42,4,6-Trichlorophenol 1 03/23/21 14:39 V2172JMV
Surrogate: 2-Fluorobiphenyl 65.5 Limits: 49-118%03/23/21 14:391 JMV V2172
Surrogate: 2-Fluorophenol 27.4 Limits: 22-84%03/23/21 14:391 JMV V2172
Surrogate: Nitrobenzene-d5 62.5 Limits: 43-123%03/23/21 14:391 JMV V2172
Surrogate: 4-Terphenyl-d14 79.4 Limits: 49-151%03/23/21 14:391 JMV V2172
Surrogate: 2,4,6-Tribromophenol 55.8 Limits: 31-144%03/23/21 14:391 JMV V2172
Surrogate: Phenol-d5 19.2 Limits: 10-63%03/23/21 14:391 JMV V2172
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94977 Matrix:
3/16/2021 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<4.01 µg/L 4.01 50.0Aliphatic C5-C8 1 03/24/21 08:03 MADEP-VPHTBL
<3.88 µg/L 3.88 50.0Aliphatic C9-C12 1 03/24/21 08:03 MADEP-VPHTBL
<4.19 µg/L 4.19 50.0Aromatic C9-C10 1 03/24/21 08:03 MADEP-VPHTBL
Surrogate: 2,5-Dibromotoluene (FID)93.1 Limits: 70-130%03/24/21 08:031 TBL V2123
Surrogate: 2,5-Dibromotoluene (PID)87.7 Limits: 70-130%03/24/21 08:031 TBL V2123
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94977 Matrix:
3/16/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
2.22 JB µg/L 0.310 10.0Acetone 1 03/26/21 13:16 V2317JLB
<0.048 µg/L 0.048 0.500Benzene 1 03/26/21 13:16 V2317JLB
<0.057 µg/L 0.057 0.500Bromobenzene 1 03/26/21 13:16 V2317JLB
<0.140 µg/L 0.140 0.500Bromochloromethane 1 03/26/21 13:16 V2317JLB
<0.062 µg/L 0.062 0.500Bromodichloromethane 1 03/26/21 13:16 V2317JLB
<0.040 µg/L 0.040 0.500Bromoform 1 03/26/21 13:16 V2317JLB
<0.180 µg/L 0.180 1.00Bromomethane 1 03/26/21 13:16 V2317JLB
<0.076 µg/L 0.076 0.500n-Butylbenzene 1 03/26/21 13:16 V2317JLB
<0.076 µg/L 0.076 0.500
sec-Butyl benzene 1 03/26/21 13:16 V2317JLB
<0.088 µg/L 0.088 0.500tert-Butyl benzene 1 03/26/21 13:16 V2317JLB
<0.110 µg/L 0.110 0.500Carbon Tetrachloride 1 03/26/21 13:16 V2317JLB
<0.062 µg/L 0.062 0.500Chlorobenzene 1 03/26/21 13:16 V2317JLB
<0.080 µg/L 0.080 0.500Chlorodibromomethane 1 03/26/21 13:16 V2317JLB
<0.220 µg/L 0.220 0.500Chloroethane 1 03/26/21 13:16 V2317JLB
<0.076 µg/L 0.076 0.500Chloroform 1 03/26/21 13:16 V2317JLB
<0.079 µg/L 0.079 0.500
Chloromethane 1 03/26/21 13:16 V2317JLB
<0.066 µg/L 0.066 0.5002-Chlorotoluene 1 03/26/21 13:16 V2317JLB
<0.050 µg/L 0.050 0.5004-Chlorotoluene 1 03/26/21 13:16 V2317JLB
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 03/26/21 13:16 V2317JLB
<0.170 µg/L 0.170 2.001,2-Dibromo-3-Chloropropane 1 03/26/21 13:16 V2317JLB
<0.051 µg/L 0.051 0.5001,2-Dibromoethane 1 03/26/21 13:16 V2317JLB
<0.065 µg/L 0.065 0.500Dibromomethane 1 03/26/21 13:16 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94977 Matrix:
3/16/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
<0.076 µg/L 0.076 0.5001,2-Dichlorobenzene 1 03/26/21 13:16 V2317JLB
<0.054 µg/L 0.054 0.5001,3-Dichlorobenzene 1 03/26/21 13:16 V2317JLB
<0.050 µg/L 0.050 0.5001,4-Dichlorobenzene 1 03/26/21 13:16 V2317JLB
<0.110 µg/L 0.110 1.00Dichlorodifluoromethane 1 03/26/21 13:16 V2317JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethane 1 03/26/21 13:16 V2317JLB
<0.066 µg/L 0.066 0.5001,2-Dichloroethane 1 03/26/21 13:16 V2317JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethene 1 03/26/21 13:16 V2317JLB
<0.056 µg/L 0.056 0.500cis-1,2-Dichloroethene 1 03/26/21 13:16 V2317JLB
<0.070 µg/L 0.070 0.500
trans-1,2-Dichloroethene 1 03/26/21 13:16 V2317JLB
<0.110 µg/L 0.110 0.5001,2-Dichloropropane 1 03/26/21 13:16 V2317JLB
<0.043 µg/L 0.043 0.5001,3-Dichloropropane 1 03/26/21 13:16 V2317JLB
<0.110 µg/L 0.110 2.002,2-Dichloropropane 1 03/26/21 13:16 V2317JLB
<0.051 µg/L 0.051 0.5001,1-Dichloropropene 1 03/26/21 13:16 V2317JLB
<0.079 µg/L 0.079 0.500cis-1,3-Dichloropropene 1 03/26/21 13:16 V2317JLB
<0.120 µg/L 0.120 0.500trans-1,3-Dichloropropene 1 03/26/21 13:16 V2317JLB
<27.0 µg/L 27.0 200
Ethanol 1 03/26/21 13:16 V2317JLB
<0.061 µg/L 0.061 0.500Ethylbenzene 1 03/26/21 13:16 V2317JLB
<0.160 µg/L 0.160 3.00Hexachlorobutadiene 1 03/26/21 13:16 V2317JLB
<0.065 µg/L 0.065 1.002-Hexanone 1 03/26/21 13:16 V2317JLB
<0.054 µg/L 0.054 0.500Isopropylbenzene 1 03/26/21 13:16 V2317JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/26/21 13:16 V2317JLB
<0.240 µg/L 0.240 5.00Methyl Ethyl Ketone (MEK)1 03/26/21 13:16 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94977 Matrix:
3/16/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
<0.042 µg/L 0.042 1.00Methyl tert-butyl ether (MTBE)1 03/26/21 13:16 V2317JLB
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 03/26/21 13:16 V2317JLB
<0.083 µg/L 0.083 2.00Methylene Chloride 1 03/26/21 13:16 V2317JLB
<0.190 µg/L 0.190 1.00Naphthalene 1 03/26/21 13:16 V2317JLB
<0.087 µg/L 0.087 0.500n-Propylbenzene 1 03/26/21 13:16 V2317JLB
<0.047 µg/L 0.047 0.500Styrene 1 03/26/21 13:16 V2317JLB
<0.640 µg/L 0.640 10.0tert-Butyl Alcohol (TBA)1 03/26/21 13:16 V2317JLB
<0.250 µg/L 0.250 10.0tert-Butyl formate (TBF)1 03/26/21 13:16 V2317JLB
<0.720 µg/L 0.720 10.0
tert-Amyl alcohol (TAA)1 03/26/21 13:16 V2317JLB
<0.100 µg/L 0.100 10.0tert-Amyl Methyl Ether (TAME)1 03/26/21 13:16 V2317JLB
<0.110 µg/L 0.110 0.5001,1,1,2-Tetrachloroethane 1 03/26/21 13:16 V2317JLB
<0.036 µg/L 0.036 0.5001,1,2,2-Tetrachloroethane 1 03/26/21 13:16 V2317JLB
<0.098 µg/L 0.098 0.500Tetrachloroethene 1 03/26/21 13:16 V2317JLB
<0.044 µg/L 0.044 0.500Toluene 1 03/26/21 13:16 V2317JLB
<0.400 µg/L 0.400 0.5001,2,3-Trichlorobenzene 1 03/26/21 13:16 V2317JLB
<0.130 µg/L 0.130 0.500
1,2,4-Trichlorobenzene 1 03/26/21 13:16 V2317JLB
<0.061 µg/L 0.061 0.5001,1,1-Trichloroethane 1 03/26/21 13:16 V2317JLB
<0.066 µg/L 0.066 0.5001,1,2-Trichloroethane 1 03/26/21 13:16 V2317JLB
<0.078 µg/L 0.078 0.500Trichloroethene 1 03/26/21 13:16 V2317JLB
<0.062 µg/L 0.062 0.500Trichlorofluoromethane 1 03/26/21 13:16 V2317JLB
<0.140 µg/L 0.140 0.5001,2,3-Trichloropropane 1 03/26/21 13:16 V2317JLB
<0.054 µg/L 0.054 0.5001,2,4-Trimethylbenzene 1 03/26/21 13:16 V2317JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 83
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27361
21-076-0036
01156
Paragon Environmental Consultants, Inc.
PO Box 157
Brandon Moore
Thomasville
Angela D Overcash
Senior Project Manager
P-2104 Received : 03/17/2021
Quality Mart 42
Report Date : 03/30/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94977 Matrix:
3/16/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V2316 03/26/21 09:00
<0.076 µg/L 0.076 0.5001,3,5-Trimethylbenzene 1 03/26/21 13:16 V2317JLB
<0.060 µg/L 0.060 5.00Vinyl Acetate 1 03/26/21 13:16 V2317JLB
<0.097 µg/L 0.097 0.500Vinyl Chloride 1 03/26/21 13:16 V2317JLB
<0.044 µg/L 0.044 0.500o-Xylene 1 03/26/21 13:16 V2317JLB
<0.120 µg/L 0.120 1.00m,p-Xylene 1 03/26/21 13:16 V2317JLB
<0.044 µg/L 0.044 0.500Xylene (Total)1 03/26/21 13:16 V2317
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%03/26/21 13:161 JLB V2317
Surrogate: Dibromofluoromethane 100 Limits: 70-130%03/26/21 13:161 JLB V2317
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%03/26/21 13:161 JLB V2317
Surrogate: Toluene-d8 99.8 Limits: 70-130%03/26/21 13:161 JLB V2317
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 83
Sample ID Report Lab No
LRB 21-076-0036 LRB
Paramater Result Units
Dilution
Factor Method Analysis Date/Time Analyst Batch ID
Hexadecanoic Acid 14.53 ug/L 1 625.1 3/23/2021 10:34 JMV V2025
Sample ID Report Lab No
MW-1 21-076-0036 94976
Paramater Result Units
Dilution
Factor Method Analysis Date/Time Analyst Batch ID
Methyl Pentanol 10.42 ug/L 1 625.1 3/23/2021 14:39 JMV V2025
Toluene 106.6 ug/L 1 625.1 3/23/2021 14:39 JMV V2025
p-Xylene 41.41 ug/L 1 625.1 3/23/2021 14:39 JMV V2025
Ethyl Methyl Benzene 12.59 ug/L 1 625.1 3/23/2021 14:39 JMV V2025
Trimethyl Benzene 31.61 ug/L 1 625.1 3/23/2021 14:39 JMV V2025
Page 38 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-06.D
Acq On : 23 Mar 2021 10:34
Operator : JVOGEL
Sample : LRB-V2025
Misc :
ALS Vial : 6 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 3 n-Hexadecanoic acid Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
8.016 14.53 ppb 549762 Phenanthrene-d10 7.545
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 n-Hexadecanoic acid 256 C16H32O2 000057-10-3 99
2 n-Hexadecanoic acid 256 C16H32O2 000057-10-3 96
3 n-Hexadecanoic acid 256 C16H32O2 000057-10-3 95
4 Tetradecanoic acid $$ Myristic a... 228 C14H28O2 000544-63-8 90
5 Heptadecanoic acid 270 C17H34O2 000506-12-7 87
20 40 60 80 100 120 140 160 180 200 220 240 260 280
0
5000
m/z-->
Abundance Scan 1042 (8.016 min): F032321-06.D\data.ms (-1038) (-)
73.043.1
129.1
213.2 256.397.0 157.2 185.2
281.1
20 40 60 80 100 120 140 160 180 200 220 240 260 280
0
5000
m/z-->
Abundance #123966: n-Hexadecanoic acid
73.0
129.0 256.0
43.0
213.0
157.097.0 185.0
20 40 60 80 100 120 140 160 180 200 220 240 260 280
0
5000
m/z-->
Abundance #123965: n-Hexadecanoic acid
43.0 73.0
256.0
129.0
213.097.0 157.0 185.0
20 40 60 80 100 120 140 160 180 200 220 240 260 280
0
5000
m/z-->
Abundance #123964: n-Hexadecanoic acid
43.0 73.0
129.097.0 213.0 256.0171.0
7.60 7.80 8.00 8.20 8.40
m/z 73.05 100.00%
7.60 7.80 8.00 8.20 8.40
m/z 43.10 83.50%
7.60 7.80 8.00 8.20 8.40
m/z 60.10 77.79%
7.60 7.80 8.00 8.20 8.40
m/z 41.05 70.94%
7.60 7.80 8.00 8.20 8.40
m/z 55.05 68.88%
F030521_FL.M Thu Mar 25 12:43:50 2021 Page: 7Page 39 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-17.D
Acq On : 23 Mar 2021 14:39
Operator : JVOGEL
Sample : V 94976-V2025
Misc :
ALS Vial : 17 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 1 2-Pentanol, 2-methyl- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
1.975 10.42 ppb 273979 1,4-Dichlorobenzene-d4 3.622
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 2-Pentanol, 2-methyl- 102 C6H14O 000590-36-3 83
2 2-Pentanol, 2-methyl- 102 C6H14O 000590-36-3 74
3 2-Pentanol, 2-methyl- 102 C6H14O 000590-36-3 72
4 2-Butanol, 2,3-dimethyl- 102 C6H14O 000594-60-5 59
5 3-Pentanol, 2,2-dimethyl- $$ 2,2... 116 C7H16O 003970-62-5 56
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance Scan 15 (1.975 min): F032321-17.D\data.ms (-7) (-)
59.1
87.141.1
105.0 165.1 206.9
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance #109760: 2-Pentanol, 2-methyl-
59.0
87.0
41.0
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance #109758: 2-Pentanol, 2-methyl-
59.0
87.041.0
18.0
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance #109759: 2-Pentanol, 2-methyl-
59.0
87.0
41.0
2.00 2.10 2.20 2.30 2.40
m/z 59.10 100.00%
2.00 2.10 2.20 2.30 2.40
m/z 87.10 31.77%
2.00 2.10 2.20 2.30 2.40
m/z 43.10 29.97%
2.00 2.10 2.20 2.30 2.40
m/z 45.05 25.66%
2.00 2.10 2.20 2.30 2.40
m/z 41.10 23.68%
F030521_FL.M Thu Mar 25 12:44:48 2021 Page: 5Page 40 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-17.D
Acq On : 23 Mar 2021 14:39
Operator : JVOGEL
Sample : V 94976-V2025
Misc :
ALS Vial : 17 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 2 Toluene Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
2.151 106.46 ppb 2799490 1,4-Dichlorobenzene-d4 3.622
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 Toluene 92 C7H8 000108-88-3 91
2 Toluene 92 C7H8 000108-88-3 91
3 Spiro[2,4]hepta-4,6-diene $$ Spi... 92 C7H8 000765-46-8 91
4 Toluene $$ Benzene, methyl $$ Me... 92 C7H8 000108-88-3 91
5 Toluene 92 C7H8 000108-88-3 87
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance Scan 45 (2.151 min): F032321-17.D\data.ms (-36) (-)
91.1
65.139.0 51.0 74.0 109.0
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #109013: Toluene
91.0
39.0 65.051.027.0 77.0
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #109014: Toluene
91.0
65.039.0 51.027.0 77.0
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #1110: Spiro[2,4]hepta-4,6-diene $$ Spiro[2.4]hepta-4,6-diene
91.0
65.039.0 51.027.0 77.0
2.00 2.20 2.40 2.60
m/z 91.10 100.00%
2.00 2.20 2.40 2.60
m/z 92.10 59.30%
2.00 2.20 2.40 2.60
m/z 65.10 13.09%
2.00 2.20 2.40 2.60
m/z 39.05 11.28%
2.00 2.20 2.40 2.60
m/z 63.10 9.84%
F030521_FL.M Thu Mar 25 12:44:49 2021 Page: 6Page 41 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-17.D
Acq On : 23 Mar 2021 14:39
Operator : JVOGEL
Sample : V 94976-V2025
Misc :
ALS Vial : 17 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 4 p-Xylene Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
2.845 41.41 ppb 1089060 1,4-Dichlorobenzene-d4 3.622
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 p-Xylene 106 C8H10 000106-42-3 97
2 Benzene, 1,3-dimethyl- 106 C8H10 000108-38-3 97
3 p-Xylene 106 C8H10 000106-42-3 94
4 Benzene, 1,3-dimethyl- 106 C8H10 000108-38-3 94
5 p-Xylene 106 C8H10 000106-42-3 94
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance Scan 163 (2.845 min): F032321-17.D\data.ms (-157) (-)
91.1
106.1
77.051.139.1 65.1
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #110025: p-Xylene
91.0
106.0
77.051.039.0 65.027.0
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #110012: Benzene, 1,3-dimethyl-
91.0
106.0
39.0 77.051.0 65.027.0
20 30 40 50 60 70 80 90 100 110
0
5000
m/z-->
Abundance #110021: p-Xylene
91.0
106.0
77.051.039.0 65.027.0
2.60 2.80 3.00 3.20
m/z 91.10 100.00%
2.60 2.80 3.00 3.20
m/z 106.05 44.63%
2.60 2.80 3.00 3.20
m/z 105.10 18.67%
2.60 2.80 3.00 3.20
m/z 77.05 13.23%
2.60 2.80 3.00 3.20
m/z 51.10 9.11%
F030521_FL.M Thu Mar 25 12:44:51 2021 Page: 8Page 42 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-17.D
Acq On : 23 Mar 2021 14:39
Operator : JVOGEL
Sample : V 94976-V2025
Misc :
ALS Vial : 17 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 6 Benzene, 1-ethyl-2-methyl- Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
3.381 12.59 ppb 331104 1,4-Dichlorobenzene-d4 3.622
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 Benzene, 1-ethyl-2-methyl- 120 C9H12 000611-14-3 94
2 Benzene, 1-ethyl-2-methyl- $$ To... 120 C9H12 000611-14-3 93
3 Benzene, 1-ethyl-2-methyl- 120 C9H12 000611-14-3 93
4 Benzene, 1-ethyl-2-methyl- 120 C9H12 000611-14-3 93
5 Benzene, 1,2,3-trimethyl- 120 C9H12 000526-73-8 90
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance Scan 254 (3.381 min): F032321-17.D\data.ms (-249) (-)
105.1
77.039.0 59.0 121.1 170.9141.9 199.9
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance #111385: Benzene, 1-ethyl-2-methyl-
105.0
77.039.0 121.059.0
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance#4792: Benzene, 1-ethyl-2-methyl- $$ Toluene, o-ethyl- $$ o-Ethylmethyl
105.0
39.0 77.0 121.059.0
20 40 60 80 100 120 140 160 180 200
0
5000
m/z-->
Abundance #111384: Benzene, 1-ethyl-2-methyl-
105.0
77.039.0 121.059.0
3.00 3.20 3.40 3.60 3.80
m/z 105.10 100.00%
3.00 3.20 3.40 3.60 3.80
m/z 120.10 29.40%
3.00 3.20 3.40 3.60 3.80
m/z 77.05 13.08%
3.00 3.20 3.40 3.60 3.80
m/z 91.10 12.45%
3.00 3.20 3.40 3.60 3.80
m/z 79.10 10.60%
F030521_FL.M Thu Mar 25 12:44:52 2021 Page: 10Page 43 of 83
Library Search Compound Report
Data Path : S:\SMS\SMS-F\Data\032321\
Data File : F032321-17.D
Acq On : 23 Mar 2021 14:39
Operator : JVOGEL
Sample : V 94976-V2025
Misc :
ALS Vial : 17 Sample Multiplier: 1
Quant Method : S:\SMS\SMS-F\Method\F030521_FL.M
Quant Title : 8270 / 625 INITIAL CALIBRATION
TIC Library : S:\Misc\NIST129K.L
TIC Integration Parameters: RTEINT.P
*********************************************************************
Peak Number 7 Benzene, 1,2,3-trimethyl- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
3.481 31.61 ppb 831272 1,4-Dichlorobenzene-d4 3.622
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 Benzene, 1,2,3-trimethyl- 120 C9H12 000526-73-8 97
2 Benzene, 1,3,5-trimethyl- 120 C9H12 000108-67-8 97
3 Benzene, 1,3,5-trimethyl- 120 C9H12 000108-67-8 95
4 Benzene, 1,2,3-trimethyl- $$ Hem... 120 C9H12 000526-73-8 95
5 Benzene, 1,3,5-trimethyl- 120 C9H12 000108-67-8 94
10 20 30 40 50 60 70 80 90 100 110 120 130
0
5000
m/z-->
Abundance Scan 271 (3.481 min): F032321-17.D\data.ms (-266) (-)
105.1
120.1
77.1 91.139.0 51.0 63.1
10 20 30 40 50 60 70 80 90 100 110 120 130
0
5000
m/z-->
Abundance #111401: Benzene, 1,2,3-trimethyl-
105.0
120.0
77.0 91.039.0 51.027.0 65.015.0
10 20 30 40 50 60 70 80 90 100 110 120 130
0
5000
m/z-->
Abundance #111397: Benzene, 1,3,5-trimethyl-
105.0
120.0
77.0 91.039.0 51.0 65.027.0
10 20 30 40 50 60 70 80 90 100 110 120 130
0
5000
m/z-->
Abundance #111399: Benzene, 1,3,5-trimethyl-
105.0
120.0
79.039.0 91.051.027.0 65.0
3.20 3.40 3.60 3.80
m/z 105.10 100.00%
3.20 3.40 3.60 3.80
m/z 120.10 45.74%
3.20 3.40 3.60 3.80
m/z 77.10 14.19%
3.20 3.40 3.60 3.80
m/z 119.10 11.99%
3.20 3.40 3.60 3.80
m/z 91.10 11.89%
F030521_FL.M Thu Mar 25 12:44:53 2021 Page: 11Page 44 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Metals Analyses
6020B
V2069QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V1936
Associated Lab Samples: 94976
LRB-V1936 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/22/21 20:071.000.260<0.260µg/LLead
LCS-V1936Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.096.2100µg/LLead 80-120
V 94976-MS-V1936 V 94976-MSD-V1936Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
96.1 96.096.4100100< 0.260µg/LLead 96.0 75-125 0.3 20.0
V 94976-PDS-V1936Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/22/21 21:0096.047.9µg/LLead
Page 1 of 37Date:03/30/2021 03:02 PM
Page 45 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
Associated Lab Samples: 94976, 94977
LRB-V2316 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/21 12:5210.00.3101.24µg/LAcetone
03/26/21 12:520.5000.048<0.048µg/LBenzene
03/26/21 12:520.5000.057<0.057µg/LBromobenzene
03/26/21 12:520.5000.140<0.140µg/LBromochloromethane
03/26/21 12:520.5000.062<0.062µg/LBromodichloromethane
03/26/21 12:520.5000.040<0.040µg/LBromoform
03/26/21 12:521.000.180<0.180µg/LBromomethane
03/26/21 12:520.5000.076<0.076µg/Ln-Butylbenzene
03/26/21 12:520.5000.076<0.076µg/Lsec-Butyl benzene
03/26/21 12:520.5000.088<0.088µg/Ltert-Butyl benzene
03/26/21 12:520.5000.110<0.110µg/LCarbon Tetrachloride
03/26/21 12:520.5000.062<0.062µg/LChlorobenzene
03/26/21 12:520.5000.080<0.080µg/LChlorodibromomethane
03/26/21 12:520.5000.220<0.220µg/LChloroethane
03/26/21 12:520.5000.076<0.076µg/LChloroform
03/26/21 12:520.5000.079<0.079µg/LChloromethane
03/26/21 12:520.5000.066<0.066µg/L2-Chlorotoluene
03/26/21 12:520.5000.050<0.050µg/L4-Chlorotoluene
03/26/21 12:520.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
03/26/21 12:522.000.170<0.170µg/L1,2-Dibromo-3-Chloropropane
03/26/21 12:520.5000.051<0.051µg/L1,2-Dibromoethane
03/26/21 12:520.5000.065<0.065µg/LDibromomethane
03/26/21 12:520.5000.076<0.076µg/L1,2-Dichlorobenzene
03/26/21 12:520.5000.054<0.054µg/L1,3-Dichlorobenzene
03/26/21 12:520.5000.050<0.050µg/L1,4-Dichlorobenzene
03/26/21 12:521.000.110<0.110µg/LDichlorodifluoromethane
03/26/21 12:520.5000.083<0.083µg/L1,1-Dichloroethane
Page 2 of 37Date:03/30/2021 03:02 PM
Page 46 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
Associated Lab Samples: 94976, 94977
LRB-V2316 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/21 12:520.5000.066<0.066µg/L1,2-Dichloroethane
03/26/21 12:520.5000.083<0.083µg/L1,1-Dichloroethene
03/26/21 12:520.5000.056<0.056µg/Lcis-1,2-Dichloroethene
03/26/21 12:520.5000.070<0.070µg/Ltrans-1,2-Dichloroethene
03/26/21 12:520.5000.110<0.110µg/L1,2-Dichloropropane
03/26/21 12:520.5000.043<0.043µg/L1,3-Dichloropropane
03/26/21 12:522.000.110<0.110µg/L2,2-Dichloropropane
03/26/21 12:520.5000.051<0.051µg/L1,1-Dichloropropene
03/26/21 12:520.5000.079<0.079µg/Lcis-1,3-Dichloropropene
03/26/21 12:520.5000.120<0.120µg/Ltrans-1,3-Dichloropropene
03/26/21 12:5220027.0<27.0µg/LEthanol
03/26/21 12:520.5000.061<0.061µg/LEthylbenzene
03/26/21 12:523.000.160<0.160µg/LHexachlorobutadiene
03/26/21 12:521.000.065<0.065µg/L2-Hexanone
03/26/21 12:520.5000.054<0.054µg/LIsopropylbenzene
03/26/21 12:520.5000.089<0.089µg/L4-Isopropyl toluene
03/26/21 12:525.000.240<0.240µg/LMethyl Ethyl Ketone (MEK)
03/26/21 12:521.000.042<0.042µg/LMethyl tert-butyl ether (MTBE)
03/26/21 12:521.000.078<0.078µg/L4-Methyl-2-Pentanone
03/26/21 12:522.000.083<0.083µg/LMethylene Chloride
03/26/21 12:521.000.190<0.190µg/LNaphthalene
03/26/21 12:520.5000.087<0.087µg/Ln-Propylbenzene
03/26/21 12:520.5000.047<0.047µg/LStyrene
03/26/21 12:5210.00.640<0.640µg/Ltert-Butyl Alcohol (TBA)
03/26/21 12:5210.00.250<0.250µg/Ltert-Butyl formate (TBF)
03/26/21 12:5210.00.720<0.720µg/Ltert-Amyl alcohol (TAA)
03/26/21 12:5210.00.100<0.100µg/Ltert-Amyl Methyl Ether (TAME)
Page 3 of 37Date:03/30/2021 03:02 PM
Page 47 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
Associated Lab Samples: 94976, 94977
LRB-V2316 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/21 12:520.5000.110<0.110µg/L1,1,1,2-Tetrachloroethane
03/26/21 12:520.5000.036<0.036µg/L1,1,2,2-Tetrachloroethane
03/26/21 12:520.5000.098<0.098µg/LTetrachloroethene
03/26/21 12:520.5000.044<0.044µg/LToluene
03/26/21 12:520.5000.400<0.400µg/L1,2,3-Trichlorobenzene
03/26/21 12:520.5000.130<0.130µg/L1,2,4-Trichlorobenzene
03/26/21 12:520.5000.061<0.061µg/L1,1,1-Trichloroethane
03/26/21 12:520.5000.066<0.066µg/L1,1,2-Trichloroethane
03/26/21 12:520.5000.078<0.078µg/LTrichloroethene
03/26/21 12:520.5000.062<0.062µg/LTrichlorofluoromethane
03/26/21 12:520.5000.140<0.140µg/L1,2,3-Trichloropropane
03/26/21 12:520.5000.054<0.054µg/L1,2,4-Trimethylbenzene
03/26/21 12:520.5000.076<0.076µg/L1,3,5-Trimethylbenzene
03/26/21 12:525.000.060<0.060µg/LVinyl Acetate
03/26/21 12:520.5000.097<0.097µg/LVinyl Chloride
03/26/21 12:520.5000.044<0.044µg/Lo-Xylene
03/26/21 12:521.000.120<0.120µg/Lm,p-Xylene
03/26/21 12:524-Bromofluorobenzene (S)105 70-130
03/26/21 12:52Dibromofluoromethane (S)102 70-130
03/26/21 12:521,2-Dichloroethane - d4 (S)103 70-130
03/26/21 12:52Toluene-d8 (S)101 70-130
LCS-V2316 LCSD-V2316Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.7 91.796.238.540.0µg/LAcetone 40-160 4.7 20.0
Page 4 of 37Date:03/30/2021 03:02 PM
Page 48 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
LCS-V2316 LCSD-V2316Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.4 10210420.820.0µg/LBenzene 70-130 1.9 20.0
20.8 10410721.320.0µg/LBromobenzene 70-130 2.3 20.0
20.2 10110621.220.0µg/LBromochloromethane 70-130 4.8 20.0
20.3 10210521.020.0µg/LBromodichloromethane 70-130 3.3 20.0
19.3 96.510520.920.0µg/LBromoform 70-130 7.9 20.0
18.2 91.093.018.620.0µg/LBromomethane 60-140 2.1 20.0
20.4 10210521.020.0µg/Ln-Butylbenzene 70-130 2.8 20.0
20.2 10110420.720.0µg/Lsec-Butyl benzene 70-130 2.4 20.0
20.0 10010320.520.0µg/Ltert-Butyl benzene 70-130 2.4 20.0
20.9 10510921.720.0µg/LCarbon Tetrachloride 70-130 3.7 20.0
19.9 99.510420.720.0µg/LChlorobenzene 70-130 3.9 20.0
20.9 10511021.920.0µg/LChlorodibromomethane 70-130 4.6 20.0
21.7 10911222.320.0µg/LChloroethane 60-140 2.7 20.0
20.8 10410821.520.0µg/LChloroform 70-130 3.3 20.0
20.0 10010520.920.0µg/LChloromethane 60-140 4.4 20.0
20.2 10110420.820.0µg/L2-Chlorotoluene 70-130 2.9 20.0
20.4 10210521.020.0µg/L4-Chlorotoluene 70-130 2.8 20.0
20.1 10110521.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.3 20.0
19.4 97.010420.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 6.4 20.0
20.9 10510921.820.0µg/L1,2-Dibromoethane 70-130 4.2 20.0
20.9 10510821.520.0µg/LDibromomethane 70-130 2.8 20.0
20.2 10110420.720.0µg/L1,2-Dichlorobenzene 70-130 2.4 20.0
20.4 10210621.120.0µg/L1,3-Dichlorobenzene 70-130 3.3 20.0
20.0 10010220.420.0µg/L1,4-Dichlorobenzene 70-130 1.9 20.0
22.4 11211723.320.0µg/LDichlorodifluoromethane 60-140 3.9 20.0
20.4 10210420.820.0µg/L1,1-Dichloroethane 70-130 1.9 20.0
Page 5 of 37Date:03/30/2021 03:02 PM
Page 49 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
LCS-V2316 LCSD-V2316Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10410921.820.0µg/L1,2-Dichloroethane 70-130 4.6 20.0
20.7 10411021.920.0µg/L1,1-Dichloroethene 70-130 5.6 20.0
20.7 10410621.220.0µg/Lcis-1,2-Dichloroethene 70-130 2.3 20.0
20.0 10010721.320.0µg/Ltrans-1,2-Dichloroethene 70-130 6.2 20.0
20.1 10110320.620.0µg/L1,2-Dichloropropane 70-130 2.4 20.0
21.4 10711222.420.0µg/L1,3-Dichloropropane 70-130 4.5 20.0
21.3 10711021.920.0µg/L2,2-Dichloropropane 70-130 2.7 20.0
20.8 10410721.320.0µg/L1,1-Dichloropropene 70-130 2.3 20.0
20.7 10410621.220.0µg/Lcis-1,3-Dichloropropene 70-130 2.3 20.0
20.6 10310821.620.0µg/Ltrans-1,3-Dichloropropene 70-130 4.7 20.0
508 102105527500µg/LEthanol 60-140 3.6 20.0
20.2 10110420.720.0µg/LEthylbenzene 70-130 2.4 20.0
19.3 96.510220.420.0µg/LHexachlorobutadiene 70-130 5.5 20.0
18.7 93.510120.220.0µg/L2-Hexanone 60-140 7.7 20.0
20.3 10210521.020.0µg/LIsopropylbenzene 70-130 3.3 20.0
19.8 99.010220.420.0µg/L4-Isopropyl toluene 70-130 2.9 20.0
19.7 98.510420.820.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.4 20.0
20.7 10411021.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 5.6 20.0
18.2 91.010220.320.0µg/L4-Methyl-2-Pentanone 60-140 10.9 20.0
19.3 96.510120.220.0µg/LMethylene Chloride 70-130 4.5 20.0
20.4 10210921.720.0µg/LNaphthalene 70-130 6.1 20.0
20.6 10310521.020.0µg/Ln-Propylbenzene 70-130 1.9 20.0
20.5 10310621.120.0µg/LStyrene 70-130 2.8 20.0
38.9 97.210642.240.0µg/Ltert-Butyl Alcohol (TBA)70-130 8.1 20.0
41.3 10311144.540.0µg/Ltert-Butyl formate (TBF)70-130 7.4 20.0
20.3 10210521.020.0µg/Ltert-Amyl alcohol (TAA)70-130 3.3 20.0
Page 6 of 37Date:03/30/2021 03:02 PM
Page 50 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V2317QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V2316
LCS-V2316 LCSD-V2316Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
42.8 10711144.340.0µg/Ltert-Amyl Methyl Ether (TAME)70-130 3.4 20.0
20.5 10310420.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.9 20.0
19.4 97.010621.120.0µg/L1,1,2,2-Tetrachloroethane 70-130 8.3 20.0
20.3 10210320.620.0µg/LTetrachloroethene 70-130 1.4 20.0
20.1 10110420.820.0µg/LToluene 70-130 3.4 20.0
20.9 10511422.820.0µg/L1,2,3-Trichlorobenzene 70-130 8.6 20.0
20.2 10110521.020.0µg/L1,2,4-Trichlorobenzene 70-130 3.8 20.0
20.5 10310921.820.0µg/L1,1,1-Trichloroethane 70-130 6.1 20.0
19.5 97.510520.920.0µg/L1,1,2-Trichloroethane 70-130 6.9 20.0
20.3 10210520.920.0µg/LTrichloroethene 70-130 2.9 20.0
21.4 10711322.620.0µg/LTrichlorofluoromethane 60-140 5.4 20.0
20.8 10411022.020.0µg/L1,2,3-Trichloropropane 70-130 5.6 20.0
20.2 10110621.220.0µg/L1,2,4-Trimethylbenzene 70-130 4.8 20.0
20.0 10010320.520.0µg/L1,3,5-Trimethylbenzene 70-130 2.4 20.0
20.6 10311122.120.0µg/LVinyl Acetate 60-140 7.0 20.0
20.0 10010621.220.0µg/LVinyl Chloride 60-140 5.8 20.0
20.4 10210420.720.0µg/Lo-Xylene 70-130 1.4 20.0
41.8 10510843.140.0µg/Lm,p-Xylene 70-130 3.0 20.0
1031024-Bromofluorobenzene (S)70-130
98.899.4Dibromofluoromethane (S)70-130
1031061,2-Dichloroethane - d4 (S)70-130
103102Toluene-d8 (S)70-130
Page 7 of 37Date:03/30/2021 03:02 PM
Page 51 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
Associated Lab Samples: 94976
LRB-V2025 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:3410.04.30<4.30µg/LAcenaphthene
03/23/21 10:3420.04.40<4.40µg/LAcenaphthylene
03/23/21 10:3410.04.60<4.60µg/LAnthracene
03/23/21 10:3410.04.10<4.10µg/LBenzidine
03/23/21 10:3410.03.20<3.20µg/LBenzo(a)anthracene
03/23/21 10:3410.03.50<3.50µg/LBenzo(a)pyrene
03/23/21 10:3410.03.50<3.50µg/LBenzo(b)fluoranthene
03/23/21 10:3410.03.60<3.60µg/LBenzo(g,h,i)perylene
03/23/21 10:3410.02.60<2.60µg/LBenzo(k)fluoranthene
03/23/21 10:3410019.0<19.0µg/LBenzoic Acid
03/23/21 10:3410.02.50<2.50µg/LBenzyl alcohol
03/23/21 10:3410.03.80<3.80µg/LBis(2-Chloroethoxy)methane
03/23/21 10:3410.02.60<2.60µg/LBis(2-Chloroethyl)ether
03/23/21 10:3410.02.80<2.80µg/LBis(2-Chloroisopropyl)ether
03/23/21 10:3410.03.70<3.70µg/LBis(2-ethylhexyl)phthalate
03/23/21 10:3420.04.40<4.40µg/L4-Bromophenyl phenyl ether
03/23/21 10:3410.02.90<2.90µg/LButyl benzyl phthalate
03/23/21 10:3410.02.90<2.90µg/L4-Chloro-3-methylphenol
03/23/21 10:3420.04.70<4.70µg/L2-Chloronaphthalene
03/23/21 10:3410.02.70<2.70µg/L2-Chlorophenol
03/23/21 10:3420.04.70<4.70µg/L4-Chlorophenyl phenyl ether
03/23/21 10:3410.03.30<3.30µg/LChrysene
03/23/21 10:3420.05.70<5.70µg/LDibenz(a,h)anthracene
03/23/21 10:3420.04.20<4.20µg/LDibenzofuran
03/23/21 10:3410.02.40<2.40µg/L1,2-Dichlorobenzene
03/23/21 10:3410.03.90<3.90µg/L1,3-Dichlorobenzene
03/23/21 10:3410.04.10<4.10µg/L1,4-Dichlorobenzene
Page 8 of 37Date:03/30/2021 03:02 PM
Page 52 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
Associated Lab Samples: 94976
LRB-V2025 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:3410.03.90<3.90µg/L3,3'-Dichlorobenzidine
03/23/21 10:3410.02.60<2.60µg/L2,4-Dichlorophenol
03/23/21 10:3420.04.20<4.20µg/LDiethyl phthalate
03/23/21 10:3410.04.10<4.10µg/LDimethyl phthalate
03/23/21 10:3410.04.90<4.90µg/L2,4-Dimethylphenol
03/23/21 10:3410.04.30<4.30µg/LDi-n-butyl phthalate
03/23/21 10:3430.011.0<11.0µg/L4,6-Dinitro-2-methylphenol
03/23/21 10:3430.012.0<12.0µg/L2,4-Dinitrophenol
03/23/21 10:3410.04.20<4.20µg/L2,4-Dinitrotoluene
03/23/21 10:3420.03.90<3.90µg/L2,6-Dinitrotoluene
03/23/21 10:3410.04.50<4.50µg/LDi-n-Octyl Phthalate
03/23/21 10:3410.04.00<4.00µg/LFluoranthene
03/23/21 10:3410.05.00<5.00µg/LFluorene
03/23/21 10:3420.03.90<3.90µg/LHexachlorobenzene
03/23/21 10:3420.04.50<4.50µg/LHexachlorobutadiene
03/23/21 10:3420.07.30<7.30µg/LHexachlorocyclopentadiene
03/23/21 10:3410.03.70<3.70µg/LHexachloroethane
03/23/21 10:3410.02.60<2.60µg/LIndeno(1,2,3-cd)pyrene
03/23/21 10:3410.04.10<4.10µg/LIsophorone
03/23/21 10:3410.04.10<4.10µg/LNaphthalene
03/23/21 10:3410.03.80<3.80µg/LNitrobenzene
03/23/21 10:3410.02.60<2.60µg/L2-Nitrophenol
03/23/21 10:3410.02.60<2.60µg/L4-Nitrophenol
03/23/21 10:3420.04.40<4.40µg/LN-Nitrosodiphenylamine
03/23/21 10:3420.03.30<3.30µg/LN-Nitroso-di-n-propylamine
03/23/21 10:3450.011.0<11.0µg/LPentachlorophenol
03/23/21 10:3410.03.90<3.90µg/LPhenanthrene
Page 9 of 37Date:03/30/2021 03:02 PM
Page 53 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
Associated Lab Samples: 94976
LRB-V2025 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:3410.01.40<1.40µg/LPhenol
03/23/21 10:3410.03.50<3.50µg/LPyrene
03/23/21 10:3410.03.00<3.00µg/L1,2,4-Trichlorobenzene
03/23/21 10:3420.04.50<4.50µg/L2,4,6-Trichlorophenol
03/23/21 10:342-Fluorobiphenyl (S)53.4 49-118
03/23/21 10:342-Fluorophenol (S)22.1 22-84
03/23/21 10:34Nitrobenzene-d5 (S)46.0 43-123
03/23/21 10:344-Terphenyl-d14 (S)81.0 49-151
03/23/21 10:342,4,6-Tribromophenol (S)46.8 31-144
03/23/21 10:34Phenol-d5 (S)17.0 10-63
LCS-V2025Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.648.350.0µg/LAcenaphthene 47-145
10351.450.0µg/LAcenaphthylene 33-145
10452.050.0µg/LAnthracene 27-133
22.411.250.0µg/LBenzidine 15-150
98.449.250.0µg/LBenzo(a)anthracene 33-143
12060.050.0µg/LBenzo(a)pyrene 17-163
10250.850.0µg/LBenzo(b)fluoranthene 24-159
10150.750.0µg/LBenzo(g,h,i)perylene 10-219
10150.750.0µg/LBenzo(k)fluoranthene 11-162
0.0*<19.050.0µg/LBenzoic Acid 10-125
66.633.350.0µg/LBenzyl alcohol 16-107
99.649.850.0µg/LBis(2-Chloroethoxy)methane 33-184
85.442.750.0µg/LBis(2-Chloroethyl)ether 12-158
Page 10 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 54 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
LCS-V2025Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.644.350.0µg/LBis(2-Chloroisopropyl)ether 36-166
10452.150.0µg/LBis(2-ethylhexyl)phthalate 10-158
95.647.850.0µg/L4-Bromophenyl phenyl ether 53-127
10452.250.0µg/LButyl benzyl phthalate 10-152
69.634.850.0µg/L4-Chloro-3-methylphenol 22-147
82.241.150.0µg/L2-Chloronaphthalene 60-118
66.233.150.0µg/L2-Chlorophenol 23-134
93.046.550.0µg/L4-Chlorophenyl phenyl ether 25-158
10552.450.0µg/LChrysene 17-168
58.429.250.0µg/LDibenz(a,h)anthracene 10-227
93.846.950.0µg/LDibenzofuran 39-114
60.630.350.0µg/L1,2-Dichlorobenzene 32-129
59.029.550.0µg/L1,3-Dichlorobenzene 20-124
59.429.750.0µg/L1,4-Dichlorobenzene 20-124
10653.150.0µg/L3,3'-Dichlorobenzidine 10-262
68.434.250.0µg/L2,4-Dichlorophenol 39-135
91.645.850.0µg/LDiethyl phthalate 10-114
93.246.650.0µg/LDimethyl phthalate 10-112
71.635.850.0µg/L2,4-Dimethylphenol 32-119
99.649.850.0µg/LDi-n-butyl phthalate 10-118
78.039.050.0µg/L4,6-Dinitro-2-methylphenol 10-181
68.834.450.0µg/L2,4-Dinitrophenol 10-191
10653.250.0µg/L2,4-Dinitrotoluene 39-139
10653.050.0µg/L2,6-Dinitrotoluene 50-158
10150.750.0µg/LDi-n-Octyl Phthalate 10-146
99.049.550.0µg/LFluoranthene 26-137
10050.250.0µg/LFluorene 59-121
Page 11 of 37Date:03/30/2021 03:02 PM
Page 55 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
LCS-V2025Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
84.642.350.0µg/LHexachlorobenzene 10-152
56.028.050.0µg/LHexachlorobutadiene 24-116
70.435.250.0µg/LHexachlorocyclopentadiene 32-117
57.628.850.0µg/LHexachloroethane 40-113
96.848.450.0µg/LIndeno(1,2,3-cd)pyrene 10-171
64.832.450.0µg/LIsophorone 21-196
73.436.750.0µg/LNaphthalene 21-133
68.834.450.0µg/LNitrobenzene 35-180
69.834.950.0µg/L2-Nitrophenol 29-182
35.617.850.0µg/L4-Nitrophenol 10-132
11959.450.0µg/LN-Nitrosodiphenylamine 69-152
91.045.550.0µg/LN-Nitroso-di-n-propylamine 10-230
0.0*17.050.0µg/LPentachlorophenol 14-176
10351.650.0µg/LPhenanthrene 54-120
28.414.250.0µg/LPhenol 10-112
11155.750.0µg/LPyrene 52-115
57.228.650.0µg/L1,2,4-Trichlorobenzene 44-142
75.637.850.0µg/L2,4,6-Trichlorophenol 37-144
90.42-Fluorobiphenyl (S)49-118
38.12-Fluorophenol (S)22-84
70.4Nitrobenzene-d5 (S)43-123
93.84-Terphenyl-d14 (S)49-151
70.82,4,6-Tribromophenol (S)31-144
28.1Phenol-d5 (S)10-63
Page 12 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 56 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
V 94963-MS-V2025 V 94963-MSD-V2025Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
94.1 94.178.7109100< 8.60µg/LAcenaphthene 72.2 47-145 17.8 33.0
98.8 98.882.8109100< 8.80µg/LAcenaphthylene 75.9 33-145 17.6 30.0
106 10690.3109100< 9.20µg/LAnthracene 82.8 27-133 15.9 27.0
<8.20 0.0*<8.90109100< 8.20µg/LBenzidine 0.0*15-150 0.0 50.0
99.0 99.089.4109100< 6.40µg/LBenzo(a)anthracene 82.0 33-143 10.1 18.0
120 120105109100< 7.00µg/LBenzo(a)pyrene 96.3 17-163 13.3 21.0
103 10389.3109100< 7.00µg/LBenzo(b)fluoranthene 81.9 24-159 14.2 34.0
103 10389.2109100< 7.20µg/LBenzo(g,h,i)perylene 81.8 10-219 14.3 27.0
102 10289.7109100< 5.20µg/LBenzo(k)fluoranthene 82.2 11-162 12.8 39.0
<38.0 0.0*48.9109100< 38.0µg/LBenzoic Acid 0.0*10-125 0.0 51.0
77.0 77.065.9109100< 5.00µg/LBenzyl alcohol 60.4 16-107 15.5 37.0
97.8 97.881.9109100< 7.60µg/LBis(2-Chloroethoxy)methane 75.1 33-184 17.6 30.0
82.6 82.667.9109100< 5.20µg/LBis(2-Chloroethyl)ether 62.2 12-158 19.5 33.0
85.8 85.869.1109100< 5.60µg/LBis(2-Chloroisopropyl)ether 63.3 36-166 21.5 34.0
105 10595.7109100< 7.40µg/LBis(2-ethylhexyl)phthalate 87.7 10-158 9.2 21.0
97.0 97.081.9109100< 8.80µg/L4-Bromophenyl phenyl ether 75.1 53-127 16.8 21.0
107 10796.4109100< 5.80µg/LButyl benzyl phthalate 88.4 10-152 10.4 23.0
68.7 68.760.5109100< 5.80µg/L4-Chloro-3-methylphenol 55.5 22-147 12.6 25.0
78.0 78.063.8109100< 9.40µg/L2-Chloronaphthalene 58.5*60-118 20.0 30.0
67.6 67.654.8109100< 5.40µg/L2-Chlorophenol 50.2 23-134 20.9 37.0
92.4 92.476.6109100< 9.40µg/L4-Chlorophenyl phenyl ether 70.2 25-158 18.6 29.0
105 10593.7109100< 6.60µg/LChrysene 85.9 17-168 11.3 30.0
58.9 58.950.9109100< 11.4µg/LDibenz(a,h)anthracene 46.6 10-227 14.5 28.0
90.4 90.476.1109100< 8.40µg/LDibenzofuran 69.8 39-114 17.1 23.0
60.6 60.651.0109100< 4.80µg/L1,2-Dichlorobenzene 46.7 32-129 17.2 34.0
59.4 59.449.9109100< 7.80µg/L1,3-Dichlorobenzene 45.7 20-124 17.3 36.0
Page 13 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 57 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
V 94963-MS-V2025 V 94963-MSD-V2025Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
58.4 58.449.5109100< 8.20µg/L1,4-Dichlorobenzene 45.4 20-124 16.4 35.0
82.4 82.471.2109100< 7.80µg/L3,3'-Dichlorobenzidine 65.3 10-262 14.5 34.0
67.1 67.156.1109100< 5.20µg/L2,4-Dichlorophenol 51.4 39-135 17.8 31.0
92.0 92.080.9109100< 8.40µg/LDiethyl phthalate 74.2 10-114 12.8 22.0
93.1 93.180.9109100< 8.20µg/LDimethyl phthalate 74.2 10-112 14.0 25.0
67.4 67.455.6109100< 9.80µg/L2,4-Dimethylphenol 51.0 32-119 19.1 36.0
101 10191.1109100< 8.60µg/LDi-n-butyl phthalate 83.5 10-118 10.3 24.0
82.1 82.172.4109100< 22.0µg/L4,6-Dinitro-2-methylphenol 66.4 10-181 12.5 35.0
81.2 81.274.3109100< 24.0µg/L2,4-Dinitrophenol 68.1 10-191 8.8 41.0
106 10693.6109100< 8.40µg/L2,4-Dinitrotoluene 85.8 39-139 12.4 24.0
106 10690.2109100< 7.80µg/L2,6-Dinitrotoluene 82.7 50-158 16.1 28.0
103 10391.3109100< 9.00µg/LDi-n-Octyl Phthalate 83.7 10-146 12.0 21.0
101 10189.6109100< 8.00µg/LFluoranthene 82.2 26-137 11.9 26.0
98.3 98.384.0109100< 10.0µg/LFluorene 77.0 59-121 15.6 30.0
84.0 84.071.8109100< 7.80µg/LHexachlorobenzene 65.8 10-152 15.6 29.0
55.9 55.948.5109100< 9.00µg/LHexachlorobutadiene 44.4 24-116 14.1 35.0
70.5 70.558.0109100< 14.6µg/LHexachlorocyclopentadiene 53.2 32-117 19.4 36.0
57.3 57.347.1109100< 7.40µg/LHexachloroethane 43.2 40-113 19.5 37.0
99.3 99.388.3109100< 5.20µg/LIndeno(1,2,3-cd)pyrene 81.0 10-171 11.7 34.0
62.4 62.453.3109100< 8.20µg/LIsophorone 48.8 21-196 15.7 27.0
71.6 71.660.5109100< 8.20µg/LNaphthalene 55.5 21-133 16.8 35.0
68.0 68.057.3109100< 7.60µg/LNitrobenzene 52.5 35-180 17.0 34.0
68.2 68.256.7109100< 5.20µg/L2-Nitrophenol 52.0 29-182 18.4 33.0
49.0 49.049.2109100< 5.20µg/L4-Nitrophenol 45.1 10-132 0.4 40.0
98.4 98.480.1109100< 8.80µg/LN-Nitrosodiphenylamine 73.4 69-152 20.5 26.0
85.9 85.970.9109100< 6.60µg/LN-Nitroso-di-n-propylamine 65.0 10-230 19.1 33.0
Page 14 of 37Date:03/30/2021 03:02 PM
Page 58 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V2172QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V2025
V 94963-MS-V2025 V 94963-MSD-V2025Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
41.6 0.0*33.9109100< 22.0µg/LPentachlorophenol 0.0*14-176 0.0 36.0
104 10490.5109100< 7.80µg/LPhenanthrene 83.0 54-120 13.8 23.0
44.6 44.642.3109100< 2.80µg/LPhenol 38.8 10-112 5.2 43.0
113 11399.9109100< 7.00µg/LPyrene 91.6 52-115 12.3 31.0
58.4 58.447.3109100< 6.00µg/L1,2,4-Trichlorobenzene 43.3*44-142 21.0 30.0
73.2 73.261.1109100< 9.00µg/L2,4,6-Trichlorophenol 56.0 37-144 18.0 30.0
85.62-Fluorobiphenyl (S)64.7 49-118
50.52-Fluorophenol (S)40.9 22-84
68.2Nitrobenzene-d5 (S)52.4 43-123
87.74-Terphenyl-d14 (S)72.1 49-151
71.52,4,6-Tribromophenol (S)54.3 31-144
43.3Phenol-d5 (S)38.5 10-63
Page 15 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 59 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
Associated Lab Samples: 94974, 94975
LRB-V2018 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/19/21 11:040.0200.015<0.015mg/KgAcetone
03/19/21 11:040.0200.0009<0.0009mg/KgAcrolein
03/19/21 11:040.0200.001<0.001mg/KgAcrylonitrile
03/19/21 11:040.0050.0008<0.0008mg/KgBenzene
03/19/21 11:040.0050.0007<0.0007mg/KgBromobenzene
03/19/21 11:040.0050.0008<0.0008mg/KgBromochloromethane
03/19/21 11:040.0050.0005<0.0005mg/KgBromodichloromethane
03/19/21 11:040.0050.0004<0.0004mg/KgBromoform
03/19/21 11:040.0100.002<0.002mg/KgBromomethane
03/19/21 11:040.0050.0005<0.0005mg/Kgn-Butylbenzene
03/19/21 11:040.0050.0005<0.0005mg/Kgsec-Butyl benzene
03/19/21 11:040.0050.0006<0.0006mg/Kgtert-Butyl benzene
03/19/21 11:040.0050.0009<0.0009mg/KgCarbon Disulfide
03/19/21 11:040.0050.0010<0.0010mg/KgCarbon Tetrachloride
03/19/21 11:040.0050.0008<0.0008mg/KgChlorobenzene
03/19/21 11:040.0050.0003<0.0003mg/KgChlorodibromomethane
03/19/21 11:040.0100.0010<0.0010mg/KgChloroethane
03/19/21 11:040.0050.0006<0.0006mg/KgChloroform
03/19/21 11:040.0100.001<0.001mg/KgChloromethane
03/19/21 11:040.0050.0007<0.0007mg/Kg2-Chlorotoluene
03/19/21 11:040.0050.0006<0.0006mg/Kg4-Chlorotoluene
03/19/21 11:040.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/19/21 11:040.0100.0006<0.0006mg/Kg1,2-Dibromo-3-Chloropropane
03/19/21 11:040.0050.0005<0.0005mg/Kg1,2-Dibromoethane
03/19/21 11:040.0050.0006<0.0006mg/KgDibromomethane
03/19/21 11:040.0050.0006<0.0006mg/Kg1,2-Dichlorobenzene
03/19/21 11:040.0050.0006<0.0006mg/Kg1,3-Dichlorobenzene
Page 16 of 37Date:03/30/2021 03:02 PM
Page 60 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
Associated Lab Samples: 94974, 94975
LRB-V2018 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/19/21 11:040.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/19/21 11:040.0100.001<0.001mg/KgDichlorodifluoromethane
03/19/21 11:040.0050.0009<0.0009mg/Kg1,1-Dichloroethane
03/19/21 11:040.0050.0006<0.0006mg/Kg1,2-Dichloroethane
03/19/21 11:040.0050.0009<0.0009mg/Kg1,1-Dichloroethene
03/19/21 11:040.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/19/21 11:040.0050.0010<0.0010mg/Kgtrans-1,2-Dichloroethene
03/19/21 11:040.0050.0008<0.0008mg/Kg1,2-Dichloropropane
03/19/21 11:040.0050.0004<0.0004mg/Kg1,3-Dichloropropane
03/19/21 11:040.0050.0006<0.0006mg/Kg2,2-Dichloropropane
03/19/21 11:040.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/19/21 11:040.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/19/21 11:040.0050.0004<0.0004mg/Kgtrans-1,3-Dichloropropene
03/19/21 11:040.0050.0008<0.0008mg/KgEthylbenzene
03/19/21 11:040.0500.0004<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/19/21 11:040.0100.0008<0.0008mg/KgHexachlorobutadiene
03/19/21 11:040.0100.0006<0.0006mg/Kgn-Hexane
03/19/21 11:040.0200.0004<0.0004mg/Kg2-Hexanone
03/19/21 11:040.0050.0006<0.0006mg/KgIsopropylbenzene
03/19/21 11:040.0050.001<0.001mg/Kg4-Isopropyl toluene
03/19/21 11:040.0200.001<0.001mg/KgMethyl Ethyl Ketone (MEK)
03/19/21 11:040.0050.0007<0.0007mg/KgMethyl tert-butyl ether (MTBE)
03/19/21 11:040.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/19/21 11:040.0100.005<0.005mg/KgMethylene Chloride
03/19/21 11:040.0100.0005<0.0005mg/KgNaphthalene
03/19/21 11:040.0050.0007<0.0007mg/Kgn-Propylbenzene
03/19/21 11:040.0050.0005<0.0005mg/KgStyrene
Page 17 of 37Date:03/30/2021 03:02 PM
Page 61 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
Associated Lab Samples: 94974, 94975
LRB-V2018 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/19/21 11:040.0050.0006<0.0006mg/Kg1,1,1,2-Tetrachloroethane
03/19/21 11:040.0050.0004<0.0004mg/Kg1,1,2,2-Tetrachloroethane
03/19/21 11:040.0050.0009<0.0009mg/KgTetrachloroethene
03/19/21 11:040.0050.0008<0.0008mg/KgToluene
03/19/21 11:040.0100.0007<0.0007mg/Kg1,2,3-Trichlorobenzene
03/19/21 11:040.0100.0005<0.0005mg/Kg1,2,4-Trichlorobenzene
03/19/21 11:040.0050.0007<0.0007mg/Kg1,1,1-Trichloroethane
03/19/21 11:040.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/19/21 11:040.0050.0010<0.0010mg/KgTrichloroethene
03/19/21 11:040.0100.001<0.001mg/KgTrichlorofluoromethane
03/19/21 11:040.0050.0006<0.0006mg/Kg1,2,3-Trichloropropane
03/19/21 11:040.0050.0006<0.0006mg/Kg1,3,5-Trimethylbenzene
03/19/21 11:040.0100.0005<0.0005mg/KgVinyl Acetate
03/19/21 11:040.0100.0010<0.0010mg/KgVinyl Chloride
03/19/21 11:040.0050.0005<0.0005mg/Kgo-Xylene
03/19/21 11:040.0100.001<0.001mg/Kgm,p-Xylene
03/19/21 11:044-Bromofluorobenzene (S)103 70-130
03/19/21 11:04Dibromofluoromethane (S)100 84-123
03/19/21 11:04Toluene-d8 (S)96.8 76-129
LCS-V2018 LCSD-V2018Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.111 1111190.1190.100mg/KgAcetone 29-198 6.9 20
0.102 1021050.1050.100mg/KgAcrolein 70-130 2.8 20
0.097 97.21010.1010.100mg/KgAcrylonitrile 65-134 3.8 20
Page 18 of 37Date:03/30/2021 03:02 PM
Page 62 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
LCS-V2018 LCSD-V2018Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.894.80.0470.050mg/KgBenzene 74-127 5.4 20
0.044 89.494.80.0470.050mg/KgBromobenzene 73-125 5.8 20
0.047 94.897.00.0480.050mg/KgBromochloromethane 72-134 2.2 20
0.046 93.897.20.0480.050mg/KgBromodichloromethane 75-122 3.5 20
0.046 93.698.40.0490.050mg/KgBromoform 66-135 5.0 20
0.038 76.675.60.0370.050mg/KgBromomethane 20-180 1.3 20
0.044 88.494.40.0470.050mg/Kgn-Butylbenzene 65-135 6.5 20
0.042 85.493.00.0460.050mg/Kgsec-Butyl benzene 66-131 8.5 20
0.043 86.293.20.0460.050mg/Kgtert-Butyl benzene 67-132 7.8 20
0.043 86.092.40.0460.050mg/KgCarbon Disulfide 61-129 7.1 20
0.043 86.293.20.0460.050mg/KgCarbon Tetrachloride 64-143 7.8 20
0.044 89.694.00.0470.050mg/KgChlorobenzene 74-118 4.7 20
0.046 92.095.20.0470.050mg/KgChlorodibromomethane 73-122 3.4 20
0.042 85.888.80.0440.050mg/KgChloroethane 33-149 3.4 20
0.046 93.094.40.0470.050mg/KgChloroform 73-127 1.4 20
0.043 87.891.40.0450.050mg/KgChloromethane 45-143 4.0 20
0.044 89.895.00.0470.050mg/Kg2-Chlorotoluene 67-124 5.6 20
0.045 90.095.00.0470.050mg/Kg4-Chlorotoluene 71-126 5.4 20
0.046 93.096.80.0480.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.0 20
0.047 94.098.60.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.7 20
0.046 92.694.80.0470.050mg/Kg1,2-Dibromoethane 70-132 2.3 20
0.049 98.296.00.0480.050mg/KgDibromomethane 74-133 2.2 20
0.045 90.694.20.0470.050mg/Kg1,2-Dichlorobenzene 72-123 3.8 20
0.044 89.695.20.0470.050mg/Kg1,3-Dichlorobenzene 71-120 6.0 20
0.045 90.694.20.0470.050mg/Kg1,4-Dichlorobenzene 71-123 3.8 20
0.042 84.095.40.0470.050mg/KgDichlorodifluoromethane 26-146 12.7 20
Page 19 of 37Date:03/30/2021 03:02 PM
Page 63 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
LCS-V2018 LCSD-V2018Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.695.60.0470.050mg/Kg1,1-Dichloroethane 74-127 5.3 20
0.048 97.698.40.0490.050mg/Kg1,2-Dichloroethane 68-128 0.8 20
0.040 81.691.60.0450.050mg/Kg1,1-Dichloroethene 67-149 11.5 20
0.044 89.692.40.0460.050mg/Kgcis-1,2-Dichloroethene 76-134 3.0 20
0.044 88.093.40.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.9 20
0.045 90.298.00.0490.050mg/Kg1,2-Dichloropropane 73-130 8.2 20
0.045 91.094.60.0470.050mg/Kg1,3-Dichloropropane 75-124 3.8 20
0.045 91.496.60.0480.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.042 85.895.20.0470.050mg/Kg1,1-Dichloropropene 71-130 10.3 20
0.048 96.697.80.0480.050mg/Kgcis-1,3-Dichloropropene 71-125 1.2 20
0.047 95.697.80.0480.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.2 20
0.044 88.494.20.0470.050mg/KgEthylbenzene 74-128 6.3 20
0.097 97.51000.1000.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.5 20
0.043 86.491.60.0450.050mg/KgHexachlorobutadiene 64-125 5.8 20
0.044 88.61030.0510.050mg/Kgn-Hexane 70-130 14.8 20
0.048 96.81050.0520.050mg/Kg2-Hexanone 61-157 8.1 20
0.042 85.893.40.0460.050mg/KgIsopropylbenzene 68-126 8.4 20
0.043 87.496.00.0480.050mg/Kg4-Isopropyl toluene 68-129 9.3 20
0.050 1021040.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.3 20
0.048 96.098.80.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.8 20
0.048 97.01010.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 4.4 20
0.045 90.294.00.0470.050mg/KgMethylene Chloride 74-129 4.1 20
0.046 92.094.40.0470.050mg/KgNaphthalene 57-157 2.5 20
0.044 89.095.00.0470.050mg/Kgn-Propylbenzene 67-130 6.5 20
0.045 91.097.20.0480.050mg/KgStyrene 77-121 6.5 20
0.047 94.098.00.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.1 20
Page 20 of 37Date:03/30/2021 03:02 PM
Page 64 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V2019QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V2018
LCS-V2018 LCSD-V2018Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.496.60.0480.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 4.4 20
0.044 88.690.20.0450.050mg/KgTetrachloroethene 68-130 1.7 20
0.045 90.295.20.0470.050mg/KgToluene 71-129 5.3 20
0.046 92.295.20.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.2 20
0.045 91.093.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.1 20
0.044 88.295.20.0470.050mg/Kg1,1,1-Trichloroethane 67-131 7.6 20
0.047 94.495.40.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.0 20
0.045 90.697.60.0480.050mg/KgTrichloroethene 75-133 7.4 20
0.044 88.497.20.0480.050mg/KgTrichlorofluoromethane 44-146 9.4 20
0.045 91.896.00.0480.050mg/Kg1,2,3-Trichloropropane 60-137 4.4 20
0.042 85.893.40.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.4 20
0.051 1041070.0530.050mg/KgVinyl Acetate 85-161 3.2 20
0.043 86.090.60.0450.050mg/KgVinyl Chloride 48-147 5.2 20
0.045 90.894.40.0470.050mg/Kgo-Xylene 74-126 3.8 20
0.088 88.694.80.0940.100mg/Kgm,p-Xylene 75-124 6.7 20
98.498.44-Bromofluorobenzene (S)70-130
10398.6Dibromofluoromethane (S)84-123
98.296.8Toluene-d8 (S)76-129
Page 21 of 37Date:03/30/2021 03:02 PM
Page 65 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
Associated Lab Samples: 94974, 94975
LRB-V2005 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:430.6600.015<0.015mg/KgAcenaphthene
03/23/21 10:430.6600.013<0.013mg/KgAcenaphthylene
03/23/21 10:430.6600.163<0.163mg/KgAniline
03/23/21 10:430.6600.007<0.007mg/KgAnthracene
03/23/21 10:430.6600.007<0.007mg/KgBenzo(a)anthracene
03/23/21 10:430.6600.005<0.005mg/KgBenzo(a)pyrene
03/23/21 10:430.6600.006<0.006mg/KgBenzo(b)fluoranthene
03/23/21 10:430.6600.006<0.006mg/KgBenzo(g,h,i)perylene
03/23/21 10:430.6600.007<0.007mg/KgBenzo(k)fluoranthene
03/23/21 10:432.000.548<0.548mg/KgBenzoic Acid
03/23/21 10:430.6600.124<0.124mg/KgBenzyl alcohol
03/23/21 10:430.6600.126<0.126mg/KgBis(2-Chloroethoxy)methane
03/23/21 10:430.6600.106<0.106mg/KgBis(2-Chloroethyl)ether
03/23/21 10:430.3300.118<0.118mg/KgBis(2-Chloroisopropyl)ether
03/23/21 10:430.6600.149<0.149mg/KgBis(2-ethylhexyl)phthalate
03/23/21 10:430.6600.155<0.155mg/Kg4-Bromophenyl phenyl ether
03/23/21 10:430.3300.114<0.114mg/KgButyl benzyl phthalate
03/23/21 10:430.6600.126<0.126mg/Kg4-Chloro-3-methylphenol
03/23/21 10:430.3300.080<0.080mg/Kg4-Chloroaniline
03/23/21 10:430.6600.161<0.161mg/Kg2-Chloronaphthalene
03/23/21 10:430.6600.126<0.126mg/Kg2-Chlorophenol
03/23/21 10:431.000.202<0.202mg/Kg4-Chlorophenyl phenyl ether
03/23/21 10:430.6600.007<0.007mg/KgChrysene
03/23/21 10:430.6600.019<0.019mg/KgDibenz(a,h)anthracene
03/23/21 10:430.6600.017<0.017mg/KgDibenzofuran
03/23/21 10:430.6600.107<0.107mg/Kg1,2-Dichlorobenzene
03/23/21 10:430.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 22 of 37Date:03/30/2021 03:02 PM
Page 66 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
Associated Lab Samples: 94974, 94975
LRB-V2005 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:430.3300.104<0.104mg/Kg1,4-Dichlorobenzene
03/23/21 10:430.6600.131<0.131mg/Kg3,3'-Dichlorobenzidine
03/23/21 10:430.6600.129<0.129mg/Kg2,4-Dichlorophenol
03/23/21 10:430.6600.170<0.170mg/KgDiethyl phthalate
03/23/21 10:430.6600.158<0.158mg/KgDimethyl phthalate
03/23/21 10:430.3300.137<0.137mg/Kg2,4-Dimethylphenol
03/23/21 10:430.6600.164<0.164mg/KgDi-n-butyl phthalate
03/23/21 10:431.500.364<0.364mg/Kg4,6-Dinitro-2-methylphenol
03/23/21 10:431.500.387<0.387mg/Kg2,4-Dinitrophenol
03/23/21 10:430.6600.175<0.175mg/Kg2,4-Dinitrotoluene
03/23/21 10:430.6600.171<0.171mg/Kg2,6-Dinitrotoluene
03/23/21 10:430.3300.171<0.171mg/KgDi-n-Octyl Phthalate
03/23/21 10:430.6600.007<0.007mg/KgFluoranthene
03/23/21 10:430.6600.014<0.014mg/KgFluorene
03/23/21 10:430.6600.145<0.145mg/KgHexachlorobenzene
03/23/21 10:430.6600.149<0.149mg/KgHexachlorobutadiene
03/23/21 10:430.6600.227<0.227mg/KgHexachlorocyclopentadiene
03/23/21 10:430.6600.104<0.104mg/KgHexachloroethane
03/23/21 10:430.6600.018<0.018mg/KgIndeno(1,2,3-cd)pyrene
03/23/21 10:430.6600.142<0.142mg/KgIsophorone
03/23/21 10:430.6600.010<0.010mg/Kg1-Methylnaphthalene
03/23/21 10:430.6600.012<0.012mg/Kg2-Methylnaphthalene
03/23/21 10:430.6600.126<0.126mg/Kg2-Methylphenol
03/23/21 10:430.6600.143<0.143mg/Kg3&4 Methylphenol
03/23/21 10:430.6600.014<0.014mg/KgNaphthalene
03/23/21 10:430.6600.142<0.142mg/Kg2-Nitroaniline
03/23/21 10:430.6600.120<0.120mg/Kg3-Nitroaniline
Page 23 of 37Date:03/30/2021 03:02 PM
Page 67 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
Associated Lab Samples: 94974, 94975
LRB-V2005 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/23/21 10:430.3300.103<0.103mg/Kg4-Nitroaniline
03/23/21 10:430.3300.140<0.140mg/KgNitrobenzene
03/23/21 10:430.6600.110<0.110mg/Kg2-Nitrophenol
03/23/21 10:430.6600.163<0.163mg/Kg4-Nitrophenol
03/23/21 10:430.1700.005<0.005mg/KgN-Nitrosodimethylamine
03/23/21 10:430.6600.181<0.181mg/KgN-Nitrosodiphenylamine
03/23/21 10:430.6600.152<0.152mg/KgN-Nitroso-di-n-propylamine
03/23/21 10:431.000.421<0.421mg/KgPentachlorophenol
03/23/21 10:430.6600.007<0.007mg/KgPhenanthrene
03/23/21 10:430.6600.108<0.108mg/KgPhenol
03/23/21 10:430.6600.009<0.009mg/KgPyrene
03/23/21 10:430.3300.063<0.063mg/KgPyridine
03/23/21 10:430.6600.117<0.117mg/Kg1,2,4-Trichlorobenzene
03/23/21 10:430.6600.140<0.140mg/Kg2,4,5-Trichlorophenol
03/23/21 10:430.6600.160<0.160mg/Kg2,4,6-Trichlorophenol
03/23/21 10:432-Fluorobiphenyl (S)100 44-115
03/23/21 10:432-Fluorophenol (S)80.7 35-115
03/23/21 10:43Nitrobenzene-d5 (S)92.2 37-122
03/23/21 10:434-Terphenyl-d14 (S)96.4 54-127
03/23/21 10:432,4,6-Tribromophenol (S)73.8 39-132
03/23/21 10:43Phenol-d5 (S)78.9 34-121
LCS-V2005Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.01.471.67mg/KgAcenaphthene 40-123
95.21.591.67mg/KgAcenaphthylene 32-132
Page 24 of 37Date:03/30/2021 03:02 PM
Page 68 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
LCS-V2005Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.61.581.67mg/KgAniline 12-197
96.41.611.67mg/KgAnthracene 47-123
90.41.511.67mg/KgBenzo(a)anthracene 49-126
1171.951.67mg/KgBenzo(a)pyrene 45-129
99.41.661.67mg/KgBenzo(b)fluoranthene 45-132
1061.771.67mg/KgBenzo(g,h,i)perylene 43-134
99.41.661.67mg/KgBenzo(k)fluoranthene 47-132
0.0*<0.5481.67mg/KgBenzoic Acid 10-83
83.21.391.67mg/KgBenzyl alcohol 29-122
97.61.631.67mg/KgBis(2-Chloroethoxy)methane 36-121
84.41.411.67mg/KgBis(2-Chloroethyl)ether 31-120
93.41.561.67mg/KgBis(2-Chloroisopropyl)ether 33-131
92.81.551.67mg/KgBis(2-ethylhexyl)phthalate 51-133
92.21.541.67mg/Kg4-Bromophenyl phenyl ether 46-124
94.61.581.67mg/KgButyl benzyl phthalate 48-132
65.81.101.67mg/Kg4-Chloro-3-methylphenol 45-122
70.61.181.67mg/Kg4-Chloroaniline 17-106
76.61.281.67mg/Kg2-Chloronaphthalene 41-114
68.81.151.67mg/Kg2-Chlorophenol 34-121
85.61.431.67mg/Kg4-Chlorophenyl phenyl ether 45-121
96.41.611.67mg/KgChrysene 50-124
64.01.071.67mg/KgDibenz(a,h)anthracene 45-134
86.21.441.67mg/KgDibenzofuran 44-120
66.41.111.67mg/Kg1,2-Dichlorobenzene 33-117
67.01.121.67mg/Kg1,3-Dichlorobenzene 30-115
65.21.091.67mg/Kg1,4-Dichlorobenzene 31-115
67.01.121.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 25 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 69 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
LCS-V2005Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
68.21.141.67mg/Kg2,4-Dichlorophenol 40-122
83.81.401.67mg/KgDiethyl phthalate 50-124
85.01.421.67mg/KgDimethyl phthalate 48-124
70.01.171.67mg/Kg2,4-Dimethylphenol 30-127
91.61.531.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.091.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*0.9521.67mg/Kg2,4-Dinitrophenol 27-129
92.21.541.67mg/Kg2,4-Dinitrotoluene 48-126
89.81.501.67mg/Kg2,6-Dinitrotoluene 46-124
94.61.581.67mg/KgDi-n-Octyl Phthalate 45-140
94.01.571.67mg/KgFluoranthene 50-127
88.61.481.67mg/KgFluorene 43-125
82.61.381.67mg/KgHexachlorobenzene 45-122
67.01.121.67mg/KgHexachlorobutadiene 32-123
74.81.251.67mg/KgHexachlorocyclopentadiene 32-117
65.21.091.67mg/KgHexachloroethane 28-117
99.41.661.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
61.01.021.67mg/KgIsophorone 30-122
79.01.321.67mg/Kg1-Methylnaphthalene 40-119
74.81.251.67mg/Kg2-Methylnaphthalene 38-122
73.01.221.67mg/Kg2-Methylphenol 32-122
63.41.061.67mg/Kg3&4 Methylphenol 34-119
75.41.261.67mg/KgNaphthalene 35-123
91.01.521.67mg/Kg2-Nitroaniline 44-127
85.61.431.67mg/Kg3-Nitroaniline 33-119
83.21.391.67mg/Kg4-Nitroaniline 63-147
73.01.221.67mg/KgNitrobenzene 34-122
Page 26 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 70 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
LCS-V2005Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
64.61.081.67mg/Kg2-Nitrophenol 36-123
75.41.261.67mg/Kg4-Nitrophenol 30-132
64.01.071.67mg/KgN-Nitrosodimethylamine 10-146
1081.811.67mg/KgN-Nitrosodiphenylamine 38-127
79.01.321.67mg/KgN-Nitroso-di-n-propylamine 36-120
83.81.401.67mg/KgPentachlorophenol 25-133
95.81.601.67mg/KgPhenanthrene 50-121
65.21.091.67mg/KgPhenol 34-121
1021.701.67mg/KgPyrene 47-127
52.60.8791.67mg/KgPyridine 10-60
64.01.071.67mg/Kg1,2,4-Trichlorobenzene 34-118
72.41.211.67mg/Kg2,4,5-Trichlorophenol 41-124
73.01.221.67mg/Kg2,4,6-Trichlorophenol 39-126
86.82-Fluorobiphenyl (S)44-115
69.32-Fluorophenol (S)35-115
71.2Nitrobenzene-d5 (S)37-122
87.44-Terphenyl-d14 (S)54-127
70.22,4,6-Tribromophenol (S)39-132
68.4Phenol-d5 (S)34-121
V 95105-MS-V2005 V 95105-MSD-V2005Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.44 87.21.391.641.65<0.015mg/KgAcenaphthene 84.7 40-123 3.5 20
1.57 95.11.511.641.65<0.013mg/KgAcenaphthylene 92.0 32-132 3.8 20
1.02 61.81.351.641.65<0.163mg/KgAniline 82.3 12-197 27.8*20
Page 27 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 71 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
V 95105-MS-V2005 V 95105-MSD-V2005Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.54 93.31.511.641.650.046mg/KgAnthracene 92.0 47-123 1.9 20
1.40 84.81.351.641.650.098mg/KgBenzo(a)anthracene 82.3 49-126 3.6 20
1.85 1121.791.641.650.130mg/KgBenzo(a)pyrene 109 45-129 3.2 20
1.50 90.91.491.641.650.136mg/KgBenzo(b)fluoranthene 90.8 45-132 0.6 20
1.68 1021.611.641.650.238mg/KgBenzo(g,h,i)perylene 98.1 43-134 4.2 20
1.61 97.51.521.641.650.142mg/KgBenzo(k)fluoranthene 92.6 47-132 5.7 20
1.32 0.0*1.231.641.65<0.548mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.42 86.01.441.641.65<0.124mg/KgBenzyl alcohol 87.8 29-122 1.3 20
1.60 96.91.511.641.65<0.126mg/KgBis(2-Chloroethoxy)methane 92.0 36-121 5.7 20
1.41 85.41.361.641.65<0.106mg/KgBis(2-Chloroethyl)ether 82.9 31-120 3.6 20
1.55 93.91.471.641.65<0.118mg/KgBis(2-Chloroisopropyl)ether 89.6 33-131 5.2 20
1.45 87.81.421.641.65<0.149mg/KgBis(2-ethylhexyl)phthalate 86.5 51-133 2.0 20
1.42 86.01.431.641.65<0.155mg/Kg4-Bromophenyl phenyl ether 87.1 46-124 0.7 20
1.44 87.21.391.641.65<0.114mg/KgButyl benzyl phthalate 84.7 48-132 3.5 20
1.05 63.61.031.641.65<0.126mg/Kg4-Chloro-3-methylphenol 62.8 45-122 1.9 20
1.03 62.41.131.641.65<0.080mg/Kg4-Chloroaniline 68.9 17-106 9.2 20
1.29 78.11.241.641.65<0.161mg/Kg2-Chloronaphthalene 75.6 41-114 3.9 20
1.14 69.01.111.641.65<0.126mg/Kg2-Chlorophenol 67.6 34-121 2.6 20
1.37 83.01.361.641.65<0.202mg/Kg4-Chlorophenyl phenyl ether 82.9 45-121 0.7 20
1.51 91.51.441.641.650.085mg/KgChrysene 87.8 50-124 4.7 20
0.929 56.30.8711.641.650.276mg/KgDibenz(a,h)anthracene 53.1 45-134 6.4 20
1.41 85.41.371.641.65<0.017mg/KgDibenzofuran 83.5 44-120 2.8 20
1.14 69.01.081.641.65<0.107mg/Kg1,2-Dichlorobenzene 65.8 33-117 5.4 20
1.11 67.21.051.641.65<0.097mg/Kg1,3-Dichlorobenzene 64.0 30-115 5.5 20
1.09 66.01.021.641.65<0.104mg/Kg1,4-Dichlorobenzene 62.1 31-115 6.6 20
0.490 0.0*0.5861.641.65<0.131mg/Kg3,3'-Dichlorobenzidine 0.0*22-121 0.0 20
Page 28 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 72 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
V 95105-MS-V2005 V 95105-MSD-V2005Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.12 67.81.081.641.65<0.129mg/Kg2,4-Dichlorophenol 65.8 40-122 3.6 20
1.35 81.81.311.641.65<0.170mg/KgDiethyl phthalate 79.8 50-124 3.0 20
1.38 83.61.341.641.65<0.158mg/KgDimethyl phthalate 81.7 48-124 2.9 30
1.16 70.31.141.641.65<0.137mg/Kg2,4-Dimethylphenol 69.5 30-127 1.7 20
1.48 89.61.421.641.65<0.164mg/KgDi-n-butyl phthalate 86.5 51-128 4.1 20
1.15 0.0*1.141.641.65<0.364mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.24 0.0*1.211.641.65<0.387mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.47 89.01.421.641.65<0.175mg/Kg2,4-Dinitrotoluene 86.5 48-126 3.4 20
1.44 87.21.441.641.65<0.171mg/Kg2,6-Dinitrotoluene 87.8 46-124 0.0 20
1.50 90.91.451.641.65<0.171mg/KgDi-n-Octyl Phthalate 88.4 45-140 3.3 20
1.48 89.61.431.641.650.034mg/KgFluoranthene 87.1 50-127 3.4 20
1.40 84.81.401.641.65<0.014mg/KgFluorene 85.3 43-125 0.0 20
1.31 79.31.301.641.65<0.145mg/KgHexachlorobenzene 79.2 45-122 0.7 20
1.14 69.01.061.641.65<0.149mg/KgHexachlorobutadiene 64.6 32-123 7.2 20
1.38 83.61.301.641.65<0.227mg/KgHexachlorocyclopentadiene 79.2 32-117 5.9 20
1.11 67.21.031.641.65<0.104mg/KgHexachloroethane 62.8 28-117 7.4 20
1.57 95.11.511.641.650.254mg/KgIndeno(1,2,3-cd)pyrene 92.0 45-133 3.8 20
1.02 61.80.9741.641.65<0.142mg/KgIsophorone 59.3 30-122 4.6 20
1.29 78.11.241.641.65<0.010mg/Kg1-Methylnaphthalene 75.6 40-119 3.9 20
1.21 73.31.181.641.65<0.012mg/Kg2-Methylnaphthalene 71.9 38-122 2.5 20
1.18 71.51.171.641.65<0.126mg/Kg2-Methylphenol 71.3 32-122 0.8 20
1.03 62.41.031.641.65<0.143mg/Kg3&4 Methylphenol 62.8 34-119 0.0 20
1.27 76.91.201.641.65<0.014mg/KgNaphthalene 73.1 35-123 5.6 20
1.50 90.91.471.641.65<0.142mg/Kg2-Nitroaniline 89.6 44-127 2.0 20
1.33 80.61.361.641.65<0.120mg/Kg3-Nitroaniline 82.9 33-119 2.2 20
1.32 80.01.321.641.650.138mg/Kg4-Nitroaniline 80.4 63-147 0.0 20
Page 29 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 73 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V2161QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V2005
V 95105-MS-V2005 V 95105-MSD-V2005Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.20 72.71.131.641.65<0.140mg/KgNitrobenzene 68.9 34-122 6.0 20
1.06 64.21.001.641.65<0.110mg/Kg2-Nitrophenol 60.9 32-123 5.8 20
1.26 76.31.231.641.65<0.163mg/Kg4-Nitrophenol 75.0 30-132 2.4 20
1.05 63.60.9881.641.65<0.005mg/KgN-Nitrosodimethylamine 60.2 10-146 6.0 30
1.75 1061.701.641.65<0.181mg/KgN-Nitrosodiphenylamine 104 38-127 2.8 20
1.31 79.31.271.641.65<0.152mg/KgN-Nitroso-di-n-propylamine 77.4 36-120 3.1 20
1.53 92.71.491.641.65<0.421mg/KgPentachlorophenol 90.8 25-133 2.6 20
1.52 92.11.491.641.65<0.007mg/KgPhenanthrene 90.8 50-121 1.9 20
1.06 64.21.041.641.65<0.108mg/KgPhenol 63.4 34-121 1.9 20
1.52 92.11.471.641.650.034mg/KgPyrene 89.6 47-127 3.3 20
<0.063 0.0*0.1351.641.65<0.063mg/KgPyridine 0.0*10-60 0.0 20
1.09 66.01.011.641.65<0.117mg/Kg1,2,4-Trichlorobenzene 61.5 34-118 7.6 20
1.18 71.51.201.641.65<0.140mg/Kg2,4,5-Trichlorophenol 73.1 41-124 1.6 20
1.24 75.11.191.641.65<0.160mg/Kg2,4,6-Trichlorophenol 72.5 39-126 4.1 20
85.42-Fluorobiphenyl (S)82.3 44-115
66.92-Fluorophenol (S)64.3 35-115
71.5Nitrobenzene-d5 (S)65.2 37-122
77.54-Terphenyl-d14 (S)75.6 54-127
68.72,4,6-Tribromophenol (S)66.1 39-132
65.1Phenol-d5 (S)62.5 34-121
Page 30 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 74 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V1975QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V1924
Associated Lab Samples: 94976
LRB-V1924 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/22/21 18:30500122<122µg/LAliphatic C19-C36
03/22/21 18:3035023.2<23.2µg/LAliphatic C9-C18
03/22/21 18:3025080.2<80.2µg/LAromatic C11-C22
03/22/21 18:302-Fluorobiphenyl (S)75.5 40-140
03/22/21 18:302-Bromonaphthalene (S)73.5 40-140
03/22/21 18:30Chlorooctadecane (S)62.5 40-140
03/22/21 18:30OTP Surrogate (S)63.0 40-140
LCS-V1924Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
156*1250800µg/LAliphatic C19-C36 40-140
92.8557600µg/LAliphatic C9-C18 40-140
76.413001700µg/LAromatic C11-C22 40-140
84.22-Fluorobiphenyl (S)40-140
84.72-Bromonaphthalene (S)40-140
65.0Chlorooctadecane (S)40-140
63.5OTP Surrogate (S)40-140
V 94958-MS-V1924 V 94958-MSD-V1924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2000 125257016301600< 244µg/LAliphatic C19-C36 158*40-140 24.9 50.0
776 64.6111012201200< 46.4µg/LAliphatic C9-C18 90.9 40-140 35.4 50.0
2000 58.8244034703400< 160µg/LAromatic C11-C22 70.3 40-140 19.8 50.0
87.02-Fluorobiphenyl (S)77.6 40-140
Page 31 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 75 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V1975QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V1924
V 94958-MS-V1924 V 94958-MSD-V1924Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
88.12-Bromonaphthalene (S)78.3 40-140
46.2Chlorooctadecane (S)55.6 40-140
49.0OTP Surrogate (S)53.1 40-140
Page 32 of 37Date:03/30/2021 03:02 PM
Page 76 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V1974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V1932
Associated Lab Samples: 94974, 94975
LRB-V1932 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/22/21 16:4150.08.42<8.42mg/KgAliphatic C19-C36
03/22/21 16:4150.02.50<2.50mg/KgAliphatic C9-C18
03/22/21 16:4150.013.6<13.6mg/KgAromatic C11-C22
03/22/21 16:412-Fluorobiphenyl (S)88.0 40-140
03/22/21 16:412-Bromonaphthalene (S)87.0 40-140
03/22/21 16:41Chlorooctadecane (S)58.5 40-140
03/22/21 16:41OTP Surrogate (S)70.5 40-140
LCS-V1932 LCSD-V1932Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
122 153*144*11580.0mg/KgAliphatic C19-C36 40-140 5.9 50
57.8 96.397.058.260.0mg/KgAliphatic C9-C18 40-140 0.6 50
139 81.770.5120170mg/KgAromatic C11-C22 40-140 14.6 50
95.287.52-Fluorobiphenyl (S)40-140
96.788.02-Bromonaphthalene (S)40-140
54.554.5Chlorooctadecane (S)40-140
77.570.5OTP Surrogate (S)40-140
Page 33 of 37* QC Fail Date:03/30/2021 03:02 PM
Page 77 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V1923QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V1922
Associated Lab Samples: 94974, 94975
LRB-V1922 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/18/21 14:508.001.58<1.58mg/KgAliphatic C5-C8
03/18/21 14:508.000.704<0.704mg/KgAliphatic C9-C12
03/18/21 14:508.000.752<0.752mg/KgAromatic C9-C10
03/18/21 14:502,5-Dibromotoluene (FID) (S)94.3 70-130
03/18/21 14:502,5-Dibromotoluene (PID) (S)90.1 70-130
LCS-V1922 LCSD-V1922Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.4 91.884.327.032.0mg/KgAliphatic C5-C8 70-130 8.5 50
33.9 10610333.132.0mg/KgAliphatic C9-C12 70-130 2.3 50
10.9 10296.210.310.7mg/KgAromatic C9-C10 70-130 5.6 50
82.886.22,5-Dibromotoluene (FID) (S)70-130
85.187.62,5-Dibromotoluene (PID) (S)70-130
Page 34 of 37Date:03/30/2021 03:02 PM
Page 78 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V2090QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V2088
Associated Lab Samples: 94976
LRB-V2088 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/22/21 09:4650.04.01<4.01µg/LAliphatic C5-C8
03/22/21 09:4650.03.88<3.88µg/LAliphatic C9-C12
03/22/21 09:4650.04.19<4.19µg/LAromatic C9-C10
03/22/21 09:462,5-Dibromotoluene (FID) (S)87.7 70-130
03/22/21 09:462,5-Dibromotoluene (PID) (S)85.8 70-130
LCS-V2088 LCSD-V2088Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
298 99.398.0294300µg/LAliphatic C5-C8 70-130 1.3 50.0
333 111110329300µg/LAliphatic C9-C12 70-130 1.2 50.0
96.2 96.295.395.3100µg/LAromatic C9-C10 70-130 0.9 50.0
83.682.02,5-Dibromotoluene (FID) (S)70-130
82.480.52,5-Dibromotoluene (PID) (S)70-130
Page 35 of 37Date:03/30/2021 03:02 PM
Page 79 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V2123QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V2122
Associated Lab Samples: 94977
LRB-V2122 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/24/21 07:3450.04.01<4.01µg/LAliphatic C5-C8
03/24/21 07:3450.03.88<3.88µg/LAliphatic C9-C12
03/24/21 07:3450.04.19<4.19µg/LAromatic C9-C10
03/24/21 07:342,5-Dibromotoluene (FID) (S)93.2 70-130
03/24/21 07:342,5-Dibromotoluene (PID) (S)88.1 70-130
LCS-V2122 LCSD-V2122Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
316 10599.3298300µg/LAliphatic C5-C8 70-130 5.8 50.0
344 115109328300µg/LAliphatic C9-C12 70-130 4.7 50.0
96.0 96.093.793.7100µg/LAromatic C9-C10 70-130 2.4 50.0
85.585.92,5-Dibromotoluene (FID) (S)70-130
81.882.22,5-Dibromotoluene (PID) (S)70-130
Page 36 of 37Date:03/30/2021 03:02 PM
Page 80 of 83
Quality Control Data
21-076-0036Report No:
Project Description:
Client ID:Paragon Environmental Consultants, Inc.
Quality Mart 42
Dry Weight Determination
SW-DRYWT
V2061QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94974-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/22/21 16:250.922.222.0%Moisture
Page 37 of 37Date:03/30/2021 03:02 PM
Page 81 of 83
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-076-0036
Paragon Environmental Consultants, Inc.
01156
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.0C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Talon J Yelton Date & Time:03/17/2021 16:27:47
Special precautions or instructions included?
Comments:
Page 82 of 83
Page 83 of 83