WS-10241_45358_CA_IAR_20200421

Initial Abatement Action Report

In addition to reporting initial response and abatement actions and assessment actions and presenting initial site characterization, this newly created Initial Abatement Action Report must fulfill the requirements, when a release
has been discovered, for the following individual reports: Check the applicable report(s). X UST Closure Report (UST-12) with UST-2 Form (Section D)
X Post-Excavation Soil Contamination Assessment Report (Section H)
A. Site Information 1. Site Identification
Date of Report: 04/21/20 Facility I.D.: 00-0-0000001965 UST Incident Number (if known): N/A
Site Name: Performance Properties Site Street Address: 2976 North NC Hwy 16
City/Town: Millers Creek Zip Code: 28651 County: Wilkes Description of Geographical Data Point (e.g., diesel fill port): Building
Location Method (GPS, topographical map, other): Google Earth Pro Latitude (decimal degrees): 36.188268° N Longitude (decimal degrees): 81.237718 ° W
2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city, state, zip code and mailing address, if different) UST/AST/Property Owner: Millers Creek Crossroads, LLC
Address: P.O. Box 635, Jefferson, NC 28640 Tel.: [phone] UST/AST Operator: Eric Sloop dba Sloop Properties
Address: P.O. Box 897, Wilkesboro, NC 28697 Tel.: N/A Property Occupant: N/A
Consultant/Contractor: Seramur & Associates, PC Address: 165 Knoll Drive, Boone, NC 28607 Tel: [phone]
Analytical Laboratory: REDLab, LLC State Certification No. UVF Method (per REDLab) Address: 9006 Hedge Maple Road, Charlotte, NC 28269 Tel: [phone]
Analytical Laboratory: Waypoint Analytical State Certification No. 402 Address: 449 Springbrook Road, Charlotte, NC 28224 Tel: [phone]
3. Information about Release
Date Discovered: 03/04/2020 Estimated Quantity of Release: Unknown
Cause of Release: Unknown Source of Release (Dispenser/Piping/UST): Dispensers
Sizes and contents of UST system(s) from which the release occurred): Two 4,000 and One 10,000 Gallon Gasoline USTs
4. Certification
I, Keith C. Seramur, a Licensed Geologist for Seramur & Associates, PC, do certify that the information contained in this
report is correct and accurate to the best of my knowledge.
Seramur & Associates, PC. is licensed to practice geology in North Carolina. The certification number of the company or corporation is C310.
Seramur & Associates, PC
165 Knoll Drive
Boone, NC 28607
Phone: [phone] [e-mail] Cell: 828.773.0499

April 21, 2020

Ms. Karen Hall
UST Section, DWM, NC DENR
450 Hanes Mill Road, STE 300
Winston-Salem, NC 27105-7407

Subject: Initial Abatement Action Report for Performance properties, Facility ID # 1965, Millers Creek, Wilkes
County, North Carolina

Dear Ms. Hall:

Enclosed is a copy of the Initial Abatement Action Report for Performance properties.

Seramur & Associates has determined that over-excavation of soil following the UST removal effectively
remediated soil with petroleum constituents above the MSCCs. We request that NCDEQ issue a letter of “No
Further Action” for this release.

If you have any questions, please email or call me.

Sincerely,
Keith C. Seramur, P.G.
Consulting Geologist
B. Site History and Characterization 1. Site History
Table B-2 shows UST Owner/Operator Information. Table B-2: Site History - UST Owner/Operator Information Revision Date: 4/17/20 Incident Name: Performance Properties
UST ID Number 001, 002, 003 Facility ID Number 00-0-0000001965
Name of Owner/Operator Dates of Operation (mm/dd/yy to mm/dd/yy)
Millers Creek Crossroads, LLC (Owner)
Eric Sloop (Operator)
USTs 002 and 003 -- 05/11/72 to Unknown
UST 001 -- 05/10/78 to Unknown
Street Address
2976 North NC Hwy 16
City State Zip Telephone Number
Millers Creek NC 28651 N/A

2. Site History – UST System and Other Release Information Table B-1 lists information about the former UST systems.
Table B-1: Site History – UST System and Other Release Information0 Revision Date: 4/17/20 Incident Number and Name: Performance Properties Facility ID#: 00-0-0000001965
UST ID Number
Current/Last Contents
Previous Contents
Capacity (in
gallons)
Construction Details
Tank Dimensions
Description of Associated
Piping and Pumps
Date Tank
Installed
Status of UST

Was release associated
with UST System?
001 Gasoline, Gasoline Mix Gasoline, Gasoline Mix
10,000 Single Wall Steel 17.1’ x 10.0’ European suction 05/10/78 Closed by removal on 03/04/20
Yes
002 Gasoline,
Gasoline Mix
Gasoline,
Gasoline Mix
4,000 Single Wall
Steel
24.4’ x 5.4’ European
suction
05/11/72 Closed by
removal on 03/04/20
Yes
003 Gasoline, Gasoline Mix Gasoline, Gasoline Mix
4,000 Single Wall Steel 24.4’ x 5.4’ European suction 05/11/72 Closed by removal on 03/04/20
Yes
N/A Heating
Oil/Fuel
Heating
Oil/Fuel
250 Single Wall
Steel
3.2’ x 3.7’ Copper
product lines
Unknown Closed by
removal 03/04/20
N/A

AST ID Number
Current/Last Contents
Previous Contents
Capacity (in gallons)
Construction Details
Tank Dimensions
Description of Associated Piping and Pumps
Date Tank Installed
Status of UST
Was release associated with UST System?
N/A Heating Oil/Fuel Heating Oil/Fuel 450 Single Wall Steel 3.1’ x 5.1’ Copper product lines
Unknown Closed by removal on 03/04/20
No
N/A Diesel Diesel 2,000 Single Wall Steel 7.1’ x 9.1’ Steel product
lines
Unknown Closed by removal
on 03/04/20
No

Incident Number Material Released Date of Release Description of Release
Not Known Gasoline Discovered
03/04/20
Staining and petroleum odors were observed in soil under the dispenser
islands.
The petroleum USTs 001, 002 and 003 were located on the north side of the building (Figure 3).

USTs 002 and 003 were last operated by Sloop Properties and according to the NC UST Database they were installed in 1972. These were two 4,000-gallon gasoline USTs. UST 001 was also operated by Sloop Properties and was installed in 1978. This was a 10,000-gallon gasoline UST. No release incident number
has been associated with this UST system. 3. There are no known spills or releases from non-UST sources at the subject property prior to the release
discovered on March 4, 2020. 4. Provide a comprehensive description of the release, including date discovered, cause and source (including
tank identification number and contents), and the relationship of historical UST releases, non-UST releases, and off-site releases (indicate incident number) to contamination from current release.
The USTs were permanently closed by removal on March 4, 2020. Staining and petroleum odors were observed below the dispensers at both islands. High concentrations of petroleum vapors were measured with a Photoionization Detector (PID) in soil samples collected from underneath four of the six dispensers.
Seramur & Associates is not aware of any non-UST releases or off-site releases that could be contributing to contamination from current release.
5. Provide a brief description of site characteristics (including status of facility (active or inactive), land use of site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.) The facility is currently inactive, and the UST system was temporarily closed for an unknown amount of time. The Performance Properties building is being demolished by the new owners, Millers Creek Crossroads, LLC. Surrounding land use is primarily commercial with some residential properties located
east of the property. A public water supply is available to the subject property and surrounding properties. Groundwater was not observed in the UST excavations.
The property is located within a small valley in Millers Creek. The nearest body of water is Millers Creek,
located less than a half-mile to the south. There is very little vegetation on the property apart from grass along the east side of the property, near NC Hwy 16. The soil consists of sandy silt in the source area up to
a depth of 13.7 feet. Bedrock was not encountered and depth to bedrock is unknown. Bedrock in this area is mapped as the Alligator Back Formation that is described as interbedded mica schist and gneiss (Rankin,
D. W., Espenshade, G. H., Neuman, R. B., 1972. Geologic map of the west half of the Winston-Salem Quadrangle, North Carolina, Virginia, and Tennessee. U. S. Geological Survey, Map I-709-A, scale 1:
250,000).
6. Summarize initial abatement actions, assessment activities, and corrective actions performed to date and list all reports previously submitted.
The USTs were permanently closed by removal on March 4, 2020. Soil removed from the UST excavation
was screened in the field for petroleum vapors with a calibrated Photoionization Detector (PID). Excavated soil was temporarily stockpiled near the excavation. Three soil samples were collected from below each of
the two 4,000-gallon gasoline USTs. Two soil samples were collected from below the 10,000-gallon gasoline UST. One soil sample was collected under each of the six former dispensers, and five samples
along the product lines to the former dispensers (Figure 4). During the UST excavation work a 250-gallon heating oil UST was discovered in the side of the excavation. This UST was also removed, and one soil
sample was collected adjacent to the 250-gallon heating oil UST. A total of 20 soil samples were collected and shipped to the laboratory for analysis using the UVF Method for total petroleum as hydrocarbons,
gasoline range organics and diesel range organics (TPH GRO and DRO).

The PID detected petroleum vapors in soil samples collected below the dispensers. Laboratory analysis
detected TPH DRO concentrations above NCDEQ Action Levels in the soil samples collected from the
below the dispensers. Petroleum constituents were not detected above the NCDEQ Action Levels in soil samples collected from the UST excavation or along the product lines. Soil contamination appeared to be limited to the area around and under the two dispenser islands.
Seramur & Associates re-mobilized to the site on Friday, March 20, 2020 to supervise over-excavation of contaminated soil around the dispenser islands. A total of 102.29 tons of contaminated soil was excavated
from below the dispenser islands. Vannoy Construction transported the contaminated soil excavated from the dispenser islands to Evo Corporation: Environmental and Industrial Services, located in Winston Salem, NC. Five post-excavation soil samples were collected from the final excavation, four from the sidewalls
and one from the center of the excavation. These soil samples were analyzed for petroleum constituents
using EPA Methods 8260 and 8270 and the MADEP VPH and EPH methods. Petroleum constituents were not detected at concentrations above the residential or soil to groundwater MSCCs. Clean fill brought in
from offsite was later used to backfill the excavation.
C. Site Check Report A site check report has not been completed.
D. UST Closure Report
The UST-2 form is included in Appendix A.
1. Describe preparations for closure including steps taken to notify authorities, permits obtained, and steps taken to clean and purge the tanks.
A Utility locate request was made to NC One-Call. Seramur & Associates personnel made site visits to document the utility locations and check the content of the USTs. A UST closure permit was obtained from the Wilkes County Building Inspection Office.
The atmosphere in the USTs were checked for explosive vapors with an Explosimeter. The Lower
Explosive Limit (LEL) readings for the gasoline USTs were below 10%. Residual fuel was pumped from the three USTs by Zebra Environmental & Industrial Services. The tanks were cleaned with a pressure
washer using soap and water after the fuel had been removed. This water-fuel mix was then also removed from the tanks by Zebra Environmental & Industrial Services and is included in the 918 gallons of residual
liquids.
The tanks were excavated and removed from the site. Vannoy Construction transported the USTs to Triad Metal Recyclers in Yadkinville, NC for disposal.
2. Describe the closure procedure referencing site and sampling location maps and cross-sections presented in Section J of this report. Clearly state how the selection of sample types and locations was influenced by the nature of the stored substance, the type of initial alarm or cause for suspicion, the type of backfill, the depth to groundwater, and other factors appropriate for identifying the presence and source of a release. If presence of groundwater or bedrock require the installation and sampling of monitoring well(s), describe the process.
Seramur & Associates mobilized to the site to excavate the tank pit and collect soil samples on February 28, March 2 and March 4, 2020. Soil was excavated from the sides of and both ends of each UST. The
USTs were then removed from the excavation using chains and the trackhoe. Soil samples were collected from below each UST, along the product lines, and from below each dispenser (Figures 4, 6 and 7). A total
of 20 soil samples were collected to be analyzed for TPH GRO and DRO.
The soil samples collected from the tank excavation were collected using the trackhoe bucket. The soil samples collected from below the dispensers were collected using a decontaminated stainless-steel spoon.
The samples collected beneath the product lines and the small heating oil UST were collected with decontaminated hand augers. The extent of the excavation and locations of soil samples are shown on
Figures 3, 4 and 6. The UST excavation measured approximately 34’ x 38’ and the dispenser island
excavation measured approximately 26’ x 30’. All soil samples were collected while wearing a new pair of
disposable Nitrile gloves. The soil samples were placed in containers provided by the lab, labeled and placed on ice. A chain of custody was initiated, and the samples were shipped via FedEx to REDLab, LLC in Charlotte, NC for analysis using the UVF Method.
Seramur & Associates, PC re-mobilized to the site to excavate contaminated soil below the dispenser islands and collect additional soil samples on March 20, 2020 (Figure 5). Five samples were collected from
the former dispenser island excavation and analyzed for petroleum constituents using EPA Methods 8260 and 8270 and the MADEP VPH and EPH methods. Contaminated soil was excavated from below the former dispensers (extent of excavation is shown on Figures 7 and 8). Soil samples were collected from
each side wall and at the center of the excavation (Figure 5).
The confirmation samples collected from the dispenser excavation were collected using the trackhoe
bucket. The extent of the excavation and locations of soil samples are shown on Figures 5, 7 and 8. All soil samples were collected while wearing a new pair of disposable Nitrile gloves. The soil samples were placed in containers provided by the lab, labeled and placed on ice. A chain of custody was initiated, and the samples were shipped via FedEx to Waypoint Analytical (formerly Prism Laboratories Inc.) in Charlotte,
NC for analysis.
The selection of sample types and locations was not influenced by the nature of the stored substance. Depth to groundwater is not known. Groundwater was not encountered in the excavation. The UST
excavation was backfilled with excavated soil as well as clean fill obtained from off site. The dispenser islands’ excavation was backfilled with clean fill obtained from off site.
3. Note the amount of residual material pumped from the tank and describe the storage, sampling and disposal of the residual material and the disposal of the tank, pumps and piping.
Residual fuel was removed from the three USTs by Zebra Environmental & Industrial Services prior to the closures. A total of 918 gallons of a petroleum/water mix were removed from the USTs and ASTs.
The tanks were excavated and removed from the site. The USTs were cleaned with a pressure washer and
detergent. Vannoy Construction transported the USTs to Triad Metal Recyclers, LLC in Yadkinville, NC for disposal.
5. If a release is determined, document initial response actions.
A petroleum odor and staining were noted in surface soil below the two dispenser islands west of the former Performance Property building. Soil excavation was limited to the volume of soil that was necessary
to remove contamination at the former dispensers.
Soil samples collected below the USTs, samples S-13 through S-21, detected petroleum constituent concentrations below NCDEQ Action Levels (Figures 3 and 4). Elevated petroleum constituent
concentrations were measured in soil samples S-1 through S-6, collected from the dispenser islands during the UST closure (Figure 4). Petroleum constituent concentrations above NCDEQ Action Levels were
detected in soil samples S-2, S-3, S-4 and S-5 (Figures 3, 4 and 7).
Seramur & Associates, PC re-mobilized to the site to excavate contaminated soil below the dispenser islands and collect additional soil samples on March 20, 2020 (Figure 5). The post-excavation assessment
is described above in Section 2. A 24-hour report was prepared and submitted to NCDEQ.
6. Document any soil excavation activities.

Soil was excavated from the sides and both ends of each of the three USTs. Excavated soil was stockpiled
on site and the USTs were removed from the excavation using chains and the trackhoe. The former tank pit
was then backfilled with fill from the tank pit and clean fill sourced from offsite. Soil was also excavated from below the former dispensers to remediate contaminated soil in this area. The
contaminated soil was then shipped to a remediation facility and the excavation was backfilled with clean fill sourced from offsite. 7. Document site investigation.
The USTs were closed as described above. Contaminated soil was removed from below the dispenser islands and post excavation confirmation soil samples were collected. Contaminated soil has been removed
from the property. Groundwater and bedrock were not encountered in the excavations. Soil sample locations are shown on Figures 4 and 5. North-South and East-West cross-sections are shown in Figures 6, 7 and 8. Initial soil samples were collected on February 28, March 2 and March 4, 2020
(Figure 4). Five additional soil samples were collected after removing contaminated soil from below the dispensers on March 20, 2020 (Figure 5). The sample times and dates are listed on the Chain of Custody
Records (Appendix B). Initial soil samples were stored on ice and shipped to REDLab, LLC in Charlotte, NC via FedEx.
Confirmation soil samples were stored on ice and shipped to Prism Laboratories Inc. in Charlotte, NC via FedEx. Samples S-2, S-3, S-4 and S-5 contained DRO concentrations above the NCDEQ Action Levels
(Figure 4). The post-excavation, confirmation soil samples collected from the dispenser island excavation did not contain petroleum constituents above the MSCCs.
8. Present conclusions and recommendations, referencing maps
The source of soil contamination was the dispenser islands. Excavation limits are shown in Figures 3, 7
and 8. Elevated concentrations of TPH DRO were detected in soil samples S-2, S-3, S-4 and S-5, collected below the former dispenser islands (Figure 4). The post-excavation confirmation soil samples collected
from the dispenser island excavation did not contain petroleum constituents above the MSCCs. No further assessment work is necessary for this release.
E. Free Product Investigation and Recovery Report Free product was not observed during the UST closure.
F. Groundwater and Surface Water Investigation There was no groundwater or surface water investigation completed during the UST closure.
G. Initial Response and Abatement Action The tanks were excavated and removed from the tank pit excavation. The PID did not detect petroleum
vapors above 1.0 ppm in the soil removed from the tank pit excavation. This soil was used to backfill the excavation. The initial soil samples were collected under the tanks, along the lines and below the
dispensers. These samples were analyzed by REDLab, LLC in Charlotte, NC.
Contaminated soil below the dispenser islands was excavated and transported to a remediation facility. These samples were collected to be analyzed for volatile organic compounds by Waypoint Analytical in
Charlotte, NC. A 24-hour report was prepared for NCDEQ. The post-excavation confirmation soil samples collected from the dispenser island excavation did not contain petroleum constituents above the MSCCs.
H. Excavation of Contaminated Soil
A petroleum odor and some staining were observed in the soil below the dispensers. Soil excavation was limited to the volume of soil that was necessary to remove contamination from below the former
dispensers. A total of 102.29 tons of contaminated soil was excavated and transported to Evo Corporation in Winston-Salem for remediation (Appendix D). The PID did not detect petroleum vapors in the soil
samples collected from the dispenser island excavation. Clean fill from offsite was used to backfill the
excavation. The post-excavation confirmation soil samples collected from the dispenser island excavation
did not contain petroleum constituents above the MSCCs. I. Conclusions Elevated concentrations of diesel range organics were detected in samples S-1, S-2, S-3, S-4, S-5 and S-6.
Only the diesel range organics were detected above the NCDEQ Action Levels. This soil has been excavated and sent to a remediation facility.
Seramur & Associates does not recommend any further assessment work for this release. On behalf of Millers Creek Crossroads, LLC, Seramur & Associates requests a Notice of No Further Action for this release.

J. Tables and Figures
Table B-3a: Summary of Soil Samples Collected During UST Closure with PID Readings Revision Date:04/20/2020 Incident Name: Millers Creek Facility ID #: 00-0-0000001965
ft. BGS = feet below ground surface BDL = below detection level
mg/kg =milligrams per kilogram

Analytical Method (e.g., VOC by 8015C)  UVF UVF PID
Contaminant of Concern  TPH GRO (mg/kg) TPH DRO (mg/kg) Volatile Organic Compounds Sample ID Date Collected (mm/dd/yy)
Source Area Sample Depth (ft BGS)
Incident Phase
S-1 2/28/20 Dispenser 1 0.0 ft Closure <2.1 87.1 0.3
S-2 2/28/20 Dispenser 2 0.0 ft Closure <49.6 11,415.0 1.1
S-3 2/28/20 Dispenser 3 0.0 ft Closure <71.9 936.0 22.5
S-4 2/28/20 Dispenser 4 0.0 ft Closure <73.1 796.0 83.4
S-5 2/28/20 Dispenser 5 0.0 ft Closure <90.4 7,479.0 0.0
S-6 2/28/20 Dispenser 6 0.0 ft Closure <2.7 77.5 0.0
S-7 3/02/20 Product Line 1.0 ft Closure <0.27 0.23 0.0
S-8 3/02/20 Product Line 1.0 ft Closure <0.4 0.9 0.0
S-9 3/02/20 Product Line 1.0 ft Closure <0.5 1.0 0.0
S-10 3/02/20 Product Line 1.0 ft Closure <0.5 1.2 0.0
S-11 3/02/20 Product Line 1.0 ft Closure <0.5 0.07 0.0
S-13 3/04/20 UST 001 13.7 ft Closure <0.6 6.9 0.5
S-14 3/04/20 UST 002 9.4 ft Closure <0.7 4.0 0.4
S-15 3/04/20 UST 003 9.4 ft Closure <0.5 0.7 0.3
S-16 3/04/20 UST 002 9.4 ft Closure <0.6 2.2 0.3
S-17 3/04/20 UST 003 9.4 ft Closure <0.6 0.09 0.4
S-18 3/04/20 UST 001 13.7 ft Closure <0.4 1.0 0.2
S-19 3/04/20 UST 002 9.4 ft Closure <0.8 1.9 0.3
S-20 3/04/20 UST 003 9.4 ft Closure 5.7 2.2 0.9
S-21 3/04/20 Heating Oil
UST 4.5 ft Closure <0.6 1.6 0.2
NC DEQ Action Level (mg/kg) 50 100 N/A
Table B-3b: List of Soil Samples Collected During Post-Excavation Confirmation Revision Date: 04/20/20 Incident Name: Millers Creek Facility ID#: 00-0-0000001965
Analytical Method (e.g., VOC by EPA 8260)  MADEP VPH 8260D
Contaminant of Concern  C9-C12 Aliphatics Acetone Sample ID Date Collected (mm/dd/yy)
Source Area
Sample Depth (ft. BGS)
Incident Phase
S-22 03/20/20 Dispenser 6.0 Closure 5.0 J --
S-23 03/20/20 Dispenser 6.0 Closure -- 0.013 J
S-24 03/20/20 Dispenser 6.0 Closure -- --
S-25 03/20/20 Dispenser 6.0 Closure -- --
S-26 03/20/20 Dispenser 6.0 Closure -- --
Soil to Groundwater MSCC (mg/kg) 540 24 Residential MSCC (mg/kg) 1,500 14,000
Industrial/Commercial MSCC (mg/kg) 40,000 360,000
MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface
mg/kg =milligrams per kilogram

N
Figure 2
Site Layout
Location of former
dispenser islands
Location of former
UST System
0 25 50
Feet
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
0 3015
Feet N
A’
A
B
B’
E
E’
C
C’
D
D’
Figure 3
Gasoline UST
Site Plan
Explanation
A A’
- Approx. Extent
of Excavation
- Approx. Cross
Section Lines
Former Performance
Properties Building
UST
System
Canopy
Dispenser
Islands
Product
Lines
001002
003
March 20, 2020
Excavation
February 28, 2020
Excavation
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
0 3015
Feet N
Figure 4
Soil Analytical
Results
- Locations of Soil Samples
- Petroleum Constituent
Concentrations Detected as
GRO (upper) and
DRO (lower)
- Below Detection Limits
Explanation
BDL
S-6
BDL
77.5
S-5
BDL
7,479
S-4
BDL
796 S-3
BDL
936
S-8
BDL
0.90
S-7
BDL
0.23 S-2
BDL
11,415
S-1
BDL
87.1
S-9
BDL
1.0
S-10
BDL
1.2
S-11
BDL
0.07
S-18
BDL
1.0
S-13
BDL
6.9S-19
BDL
1.9
S-20
5.7
2.2
S-16
BDL
2.2
S-14
BDL
4.0
S-17
BDL
0.09S-15
BDL
0.7
S-21
BDL
1.6
5.7
2.2
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
0 3015
Feet N
S-22
5.0
ND S-25
ND
ND
S-24
ND
ND S-26
ND
ND
S-23
ND
0.013
Figure 5
Confirmation Soil
Analytical Results
- Locations of Soil Samples
- Estimated Concentrations of
C9-C12 Aliphatics detected
by MADEP VPH (upper) and
Acetone detected by EPA
Method 8260B (lower)
- Not Detected
Explanation
5.0
0.013
ND
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
Figure 6
Cross Sections
A-A’ and B-B’
0 5 10
Feet
North
A
South
A’Ground Surface
Approximate
Extent of
Excavation
S-16
BDL
2.2
S-17
BDL
0.09
West
B
East
B’Ground Surface
S-19
BDL
1.9
S-16
BDL
2.2
S-14
BDL
4.0
Explanation
- Locations of soil samples
BDL
2.2
- Petroleum Constituent Concentrations
Detected as GRO (upper) and
DRO (lower)
BDL - Below Detection Limits
5
15
FeetS-13
BDL
6.9
UST 001 UST 002 UST 003
0 6 12
Feet
6
Feet
12
Approximate
Extent of
Excavation
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
S-3
BDL
936
S-4
BDL
796
S-5
BDL
7,479
S-6
BDL
77.5
C C’
North SouthDispenser IslandGround Surface
0 6
Feet
6
Feet
12
Approximate
Extent of
Excavation
12
D D’
North SouthDispenser Island Ground Surface
0 6
Feet
6
Feet
12
Approximate
Extent of
Excavation
12
S-2
BDL
11,415
S-1
BDL
87.1
Fuel Lines
Figure 7
Cross Sections
C-C’ and D-D’
Explanation
- Locations of soil samples
BDL
936
- Petroleum Constituent Concentrations
Detected as GRO (upper) and
DRO (lower)
BDL - Below Detection Limits
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
Figure 8
Cross Section
E-E’
0 5 10
Feet
Ground Surface
Approximate
Extent of
Excavation
West
E
East
E’
Explanation
- Locations of initial closure soil samples
- Locations of risk-based soil samples
BDL
2.2
- Petroleum Constituent Concentrations
Detected by UVF Method as
GRO (upper) and DRO (lower)
BDL - Below Detection Limits ND - Petroleum Constituents Not Detected
5
10
Feet
Performance Properties
2976 North NC Hwy 16
Millers Creek, NC 28651
Seramur & Associates, PC
Boone, NC
Dispenser Islands
S-4
BDL
796
S-2
BDL
11,415
S-7
BDL
0.23
S-22
5.0
ND
S-24
ND
ND
S-23
ND
0.013
- Estimated Concentrations of
C9-C12 Aliphatics detected
by MADEP VPH (upper) and
Acetone detected by EPA
Method 8260B (lower)
5.0
0.013
Appendix A
UST-2A Form

Appendix B
Laboratory Results

Hydrocarbon Analysis ResultsClient:SERAMUR & ASSOCIATESSamples taken2/28 & 3/2Address:165 KNOLL DRIVESamples extracted2/28 & 3/2BOONE NC 28607Samples analysedFriday, March 06, 2020Contact:KEITH SERAMUR & JOEY ANDERSONOperatorMAX MOYERProject:VANNOYT03308MatrixSample IDDilution usedBTEX GRO DRO TPHTotal Aromatics16 EPA PAHsBaPHC Fingerprint MatchC6-C9 C5-C10 C10-C35 C5-C35 C10-C35C5:10C10:C18C18+Soil S-184.0 <2.1 <2.187.1 87.1 39.8 2 0.042 0 84.4 15.6 V.Deg.PHC 91.7%,(FCM)Soil S-21979.0 <49.5 <49.5 11415 11415 873 16.7 0.023 0 95.1 4.9 Motor oil 98.8%,(FCM)Soil S-32874.0 <71.9 <71.9 936 936 293 17.2 0.92 0 81.8 18.2 V.Deg.Light Fuel 96.3%,(FCM)Soil S-42923.0 <73.1 <73.1 796 796 238.5 13.9 0.69 0 81.4 18.6V.Deg.Light Fuel 96.6%,(FCM),(PFM)Soil S-53615.0 <90.4 <90.4 7479 7479 3832 140.4 0.82 0 97.2 2.8 Deg.Diesel 95.8%,(FCM)Soil S-6108.0 <2.7 <2.777.5 77.5 42.2 2.3 0.071 0 69.3 30.7 V.Deg.PHC 61.6%,(FCM)Soil S-711.0 <0.27 <0.27 0.23 0.23 0.09 0.005 <0.003 0 71 29 V.Deg.PHC 81.9%,(FCM)Soil S-819.0 <0.4 <0.40.9 0.9 0.4 0.021 <0.001 0 72.6 27.4 V.Deg.PHC 71.2%,(FCM)Soil S-922.0 <0.5 <0.51 1 0.4 0.023 <0.002 45 43.4 11.6 V.Deg.PHC 85%,(FCM)Soil S-1020.0 <0.5 <0.51.2 1.2 0.7 0.04 <0.001 0 86.7 13.3 V.Deg.PHC 81.4%,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK91.5%Analysis by QED HC‐1 AnalyserConcentration values in mg/kg for soil and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detectedHC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only : % Ratios estimated carbon number proportions : (OCR)/(Q) = Outside cal range, values and HC match estimates : ND = Not Detected(B) = Blank Drift : (M) = Adjusted value : (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result : (BO) = Background Organics detected : SB = sample selected as site background% Ratios
Hydrocarbon Analysis ResultsClient:SERAMUR & ASSOCIATESSamples taken3/2 & 3/4Address:165 KNOLL DRIVESamples extracted3/2 & 3/4BOONE NC 28607Samples analysedFriday, March 06, 2020Contact:KEITH SERAMUR & JOEY ANDERSONOperatorMAX MOYERProject:VANNOYT03308MatrixSample IDDilution usedBTEX GRO DRO TPHTotal Aromatics16 EPA PAHsBaPHC Fingerprint MatchC6-C9 C5-C10 C10-C35 C5-C35 C10-C35C5:10C10:C18C18+Soil S-1123.0 <0.5 <0.50.07 0.07 0.07 0.007 <0.007 0 85.2 14.8 Residual HCSoil S-1325.0 <0.6 <0.66.9 6.9 3.5 0.16 0.002 0 87.8 12.2 V.Deg.Light Fuel 90.5%,(FCM)Soil S-1430.0 <0.7 <0.74 4 2 0.04 <0.001 0 93.4 6.6 V.Deg.PHC 79.3%,(FCM)Soil S-1522.0 <0.5 <0.50.7 0.7 0.6 0.07 <0.005 0 97.6 2.4 Residual PHCSoil S-1626.0 <0.6 <0.62.2 2.2 0.9 0.05 <0.003 0 95.6 4.4 V.Deg.Light Fuel 78.2%,(FCM)Soil S-1724.0 <0.6 <0.60.09 0.09 0.09 0.01 <0.007 0 84.6 15.4 Residual HCSoil S-1818.0 <0.4 <0.41 1 0.3 0.019 <0.0 0 95.4 4.6 V.Deg.Light Fuel 91.4%,(FCM)Soil S-1932.0 <0.8 <0.81.9 1.9 0.8 0.04 <0.002 0 90.1 9.9 V.Deg.Diesel 92.8%,(FCM)Soil S-2028.0 <0.75.7 2.2 7.92 0.6 0.04 0.001 91.5 7 1.4 No Match foundSoil S-2126.0 <0.6 <0.61.6 1.6 1.5 0.22 0.038 0 84.6 15.4 V.Deg.PHC,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK97.1%Analysis by QED HC‐1 AnalyserConcentration values in mg/kg for soil and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detectedHC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only : % Ratios estimated carbon number proportions : (OCR)/(Q) = Outside cal range, values and HC match estimates : ND = Not Detected(B) = Blank Drift : (M) = Adjusted value : (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result : (BO) = Background Organics detected : SB = sample selected as site background% Ratios
QED Hydrocarbon Fingerprints
Project: VANNOY Friday, March 06, 2020
QED Hydrocarbon Fingerprints
Project: VANNOY Friday, March 06, 2020
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
3/31/20 9:43
Keith C. Seramur PGPC
Keith Seramur
165 Knoll Dr.
Boone, NC 28607
Project: Vannoy
Lab Submittal Date: 03/24/2020
Work Order: 0030321
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Senior Project Manager
Angela D. Overcash
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 41
Sample Receipt Summary
03/31/2020
Work Order: 0030321
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0030321-01 03/20/20 12:26S-22 03/24/20 10:45Solid
0030321-02 03/20/20 13:15S-23 03/24/20 10:45Solid
0030321-03 03/20/20 13:20S-24 03/24/20 10:45Solid
0030321-04 03/20/20 13:25S-25 03/24/20 10:45Solid
0030321-05 03/20/20 13:30S-26 03/24/20 10:45Solid
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 41
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0030321
03/31/2020
Summary of Detections
5.0 J mg/kg dry0030321-01 S-22 C9-C12 Aliphatics MADEP VPH
0.013 J mg/kg dry0030321-02 S-23 Acetone 8260D
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-22
Sample ID: 0030321-01
Work Order: 0030321
Time Collected: 03/20/20 12:26
Time Submitted: 03/24/20 10:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P0C04951323/26/20 14:06 ZRCmg/kg dry 1.6C9-C18 Aliphatics
BRL MADEP EPH P0C04951323/26/20 14:06 ZRCmg/kg dry 5.5C19-C36 Aliphatics
BRL MADEP EPH P0C04951323/26/20 14:06 ZRCmg/kg dry 8.9C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14084 %1-Chlorooctadecane
40-14084 %o-Terphenyl
40-14070 %2-Fluorobiphenyl
40-14073 %2-Bromonaphthalene
General Chemistry Parameters
76.8 *SM2540 G P0C050710.100 3/26/20 7:15 EDV% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.151,2,4-Trichlorobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.141,2-Dichlorobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.131,3-Dichlorobenzene
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.141,4-Dichlorobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0131-Methylnaphthalene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.182,4,5-Trichlorophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.212,4,6-Trichlorophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.172,4-Dichlorophenol
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.182,4-Dimethylphenol
BRL 8270E P0C049711.9 3/25/20 18:39 JMVmg/kg dry 0.502,4-Dinitrophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.232,4-Dinitrotoluene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.222,6-Dinitrotoluene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.212-Chloronaphthalene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.162-Chlorophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0172-Methylnaphthalene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.162-Methylphenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.142-Nitrophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.173,3’-Dichlorobenzidine
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.193/4-Methylphenol
BRL 8270E P0C049711.9 3/25/20 18:39 JMVmg/kg dry 0.474,6-Dinitro-2-methylphenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.204-Bromophenyl phenyl ether
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.164-Chloro-3-methylphenol
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.104-Chloroaniline
BRL 8270E P0C049711.3 3/25/20 18:39 JMVmg/kg dry 0.264-Chlorophenyl phenyl ether
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.214-Nitrophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.020Acenaphthene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.017Acenaphthylene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0095Anthracene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.18Azobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.010Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-22
Sample ID: 0030321-01
Work Order: 0030321
Time Collected: 03/20/20 12:26
Time Submitted: 03/24/20 10:45
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0077Benzo(a)pyrene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0079Benzo(b)fluoranthene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0084Benzo(g,h,i)perylene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0091Benzo(k)fluoranthene
BRL 8270E P0C049712.6 3/25/20 18:39 JMVmg/kg dry 0.71Benzoic Acid
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.16Benzyl alcohol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.14Bis(2-Chloroethyl)ether
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.19Bis(2-Ethylhexyl)phthalate
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.15Butyl benzyl phthalate
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.010Chrysene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.025Dibenzo(a,h)anthracene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.23Dibenzofuran
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.22Diethyl phthalate
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.21Dimethyl phthalate
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.21Di-n-butyl phthalate
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.22Di-n-octyl phthalate
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0097Fluoranthene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.015Fluorene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.19Hexachlorobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.19Hexachlorobutadiene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.29Hexachlorocyclopentadiene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.14Hexachloroethane
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.024Indeno(1,2,3-cd)pyrene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.18Isophorone
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.018Naphthalene
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.18Nitrobenzene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.20N-Nitroso-di-n-propylamine
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.24N-Nitrosodiphenylamine
BRL 8270E P0C049711.3 3/25/20 18:39 JMVmg/kg dry 0.55Pentachlorophenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.0094Phenanthrene
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.14Phenol
BRL 8270E P0C049710.86 3/25/20 18:39 JMVmg/kg dry 0.012Pyrene
BRL 8270E P0C049710.43 3/25/20 18:39 JMVmg/kg dry 0.082Pyridine
Surrogate Recovery Control Limits
39-13276 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11575 %2-Fluorophenol
37-12273 %Nitrobenzene-d5
34-12174 %Phenol-d5
54-12774 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-22
Sample ID: 0030321-01
Work Order: 0030321
Time Collected: 03/20/20 12:26
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000761,1,1,2-Tetrachloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000921,1,1-Trichloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000681,1,2-Trichloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00111,1-Dichloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00111,1-Dichloroethylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000971,1-Dichloropropylene
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.000901,2,3-Trichlorobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000711,2,3-Trichloropropane
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.000601,2,4-Trichlorobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000661,2,4-Trimethylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000561,2-Dibromoethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000701,2-Dichlorobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000741,2-Dichloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000941,2-Dichloropropane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000791,3,5-Trimethylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000781,3-Dichlorobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000521,3-Dichloropropane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000791,4-Dichlorobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000782,2-Dichloropropane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000842-Chlorotoluene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.000714-Chlorotoluene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00164-Isopropyltoluene
BRL 8260D P0C049410.025 3/25/20 13:43 TBLmg/kg dry 0.0016Acetone
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00098Benzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00087Bromobenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0010Bromochloromethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00059Bromodichloromethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00048Bromoform
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0031Bromomethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0012Carbon Tetrachloride
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00098Chlorobenzene
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0012Chloroethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00077Chloroform
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0019Chloromethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00098cis-1,2-Dichloroethylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00062cis-1,3-Dichloropropylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00042Dibromochloromethane
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0018Dichlorodifluoromethane
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00094Ethylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00092Isopropyl Ether
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00073Isopropylbenzene (Cumene)
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0016m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-22
Sample ID: 0030321-01
Work Order: 0030321
Time Collected: 03/20/20 12:26
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.025 3/25/20 13:43 TBLmg/kg dry 0.00043Methyl Butyl Ketone (2-Hexanone)
BRL 8260D P0C049410.025 3/25/20 13:43 TBLmg/kg dry 0.0015Methyl Ethyl Ketone (2-Butanone)
BRL 8260D P0C049410.025 3/25/20 13:43 TBLmg/kg dry 0.00051Methyl Isobutyl Ketone
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0010Methylene Chloride
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00088Methyl-tert-Butyl Ether
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.00063Naphthalene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00059n-Butylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00091n-Propylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00067o-Xylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00068sec-Butylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00061Styrene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00074tert-Butylbenzene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0011Tetrachloroethylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0010Toluene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0012trans-1,2-Dichloroethylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.00054trans-1,3-Dichloropropylene
BRL 8260D P0C049410.0063 3/25/20 13:43 TBLmg/kg dry 0.0012Trichloroethylene
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0017Trichlorofluoromethane
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.00068Vinyl acetate
BRL 8260D P0C049410.013 3/25/20 13:43 TBLmg/kg dry 0.0012Vinyl chloride
BRL 8260D P0C049410.019 3/25/20 13:43 TBLmg/kg dry 0.0023Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P0C0526100203/26/20 18:56 TBLmg/kg dry 3.9C5-C8 Aliphatics
5.0 MADEP VPH P0C0526100203/26/20 18:56 TBLJmg/kg dry 1.8C9-C12 Aliphatics
BRL MADEP VPH P0C0526100203/26/20 18:56 TBLmg/kg dry 1.9C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130113 %2,5-Dibromotoluene (PID)
70-130122 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-23
Sample ID: 0030321-02
Work Order: 0030321
Time Collected: 03/20/20 13:15
Time Submitted: 03/24/20 10:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P0C04951313/26/20 14:42 ZRCmg/kg dry 1.5C9-C18 Aliphatics
BRL MADEP EPH P0C04951313/26/20 14:42 ZRCmg/kg dry 5.2C19-C36 Aliphatics
BRL MADEP EPH P0C04951313/26/20 14:42 ZRCmg/kg dry 8.4C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14080 %1-Chlorooctadecane
40-14077 %o-Terphenyl
40-14071 %2-Fluorobiphenyl
40-14073 %2-Bromonaphthalene
General Chemistry Parameters
79.1 *SM2540 G P0C050710.100 3/26/20 7:15 EDV% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.151,2,4-Trichlorobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.141,2-Dichlorobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.121,3-Dichlorobenzene
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.131,4-Dichlorobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0131-Methylnaphthalene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.182,4,5-Trichlorophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.202,4,6-Trichlorophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.162,4-Dichlorophenol
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.172,4-Dimethylphenol
BRL 8270E P0C049711.9 3/25/20 19:02 JMVmg/kg dry 0.492,4-Dinitrophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.222,4-Dinitrotoluene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.222,6-Dinitrotoluene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.202-Chloronaphthalene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.162-Chlorophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0162-Methylnaphthalene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.162-Methylphenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.142-Nitrophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.173,3’-Dichlorobenzidine
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.183/4-Methylphenol
BRL 8270E P0C049711.9 3/25/20 19:02 JMVmg/kg dry 0.464,6-Dinitro-2-methylphenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.204-Bromophenyl phenyl ether
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.164-Chloro-3-methylphenol
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.104-Chloroaniline
BRL 8270E P0C049711.3 3/25/20 19:02 JMVmg/kg dry 0.254-Chlorophenyl phenyl ether
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.214-Nitrophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.019Acenaphthene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.016Acenaphthylene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0092Anthracene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.18Azobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.010Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-23
Sample ID: 0030321-02
Work Order: 0030321
Time Collected: 03/20/20 13:15
Time Submitted: 03/24/20 10:45
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0074Benzo(a)pyrene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0077Benzo(b)fluoranthene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0082Benzo(g,h,i)perylene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0088Benzo(k)fluoranthene
BRL 8270E P0C049712.5 3/25/20 19:02 JMVmg/kg dry 0.69Benzoic Acid
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.16Benzyl alcohol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.19Bis(2-Ethylhexyl)phthalate
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.14Butyl benzyl phthalate
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0098Chrysene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.024Dibenzo(a,h)anthracene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.22Dibenzofuran
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.21Diethyl phthalate
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.20Dimethyl phthalate
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.21Di-n-butyl phthalate
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.22Di-n-octyl phthalate
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0095Fluoranthene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.014Fluorene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.18Hexachlorobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.19Hexachlorobutadiene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.29Hexachlorocyclopentadiene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.13Hexachloroethane
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.023Indeno(1,2,3-cd)pyrene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.18Isophorone
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.018Naphthalene
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.18Nitrobenzene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.19N-Nitroso-di-n-propylamine
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.23N-Nitrosodiphenylamine
BRL 8270E P0C049711.3 3/25/20 19:02 JMVmg/kg dry 0.53Pentachlorophenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.0091Phenanthrene
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.14Phenol
BRL 8270E P0C049710.83 3/25/20 19:02 JMVmg/kg dry 0.012Pyrene
BRL 8270E P0C049710.42 3/25/20 19:02 JMVmg/kg dry 0.080Pyridine
Surrogate Recovery Control Limits
39-13274 %2,4,6-Tribromophenol
44-11572 %2-Fluorobiphenyl
35-11574 %2-Fluorophenol
37-12269 %Nitrobenzene-d5
34-12171 %Phenol-d5
54-12773 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-23
Sample ID: 0030321-02
Work Order: 0030321
Time Collected: 03/20/20 13:15
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000791,1,1,2-Tetrachloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000951,1,1-Trichloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000701,1,2-Trichloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00121,1-Dichloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00121,1-Dichloroethylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00101,1-Dichloropropylene
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.000931,2,3-Trichlorobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000741,2,3-Trichloropropane
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.000621,2,4-Trichlorobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000691,2,4-Trimethylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000581,2-Dibromoethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000721,2-Dichlorobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000771,2-Dichloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000971,2-Dichloropropane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000811,3,5-Trimethylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000811,3-Dichlorobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000541,3-Dichloropropane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000821,4-Dichlorobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000812,2-Dichloropropane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000872-Chlorotoluene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.000744-Chlorotoluene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00164-Isopropyltoluene
0.013 8260D P0C049410.026 3/25/20 14:14 TBLJmg/kg dry 0.0017Acetone
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0010Benzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00090Bromobenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0011Bromochloromethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00062Bromodichloromethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00050Bromoform
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0032Bromomethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0013Carbon Tetrachloride
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0010Chlorobenzene
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0012Chloroethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00079Chloroform
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0020Chloromethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0010cis-1,2-Dichloroethylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00064cis-1,3-Dichloropropylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00043Dibromochloromethane
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0018Dichlorodifluoromethane
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00097Ethylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00095Isopropyl Ether
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00075Isopropylbenzene (Cumene)
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0017m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-23
Sample ID: 0030321-02
Work Order: 0030321
Time Collected: 03/20/20 13:15
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.026 3/25/20 14:14 TBLmg/kg dry 0.00045Methyl Butyl Ketone (2-Hexanone)
BRL 8260D P0C049410.026 3/25/20 14:14 TBLmg/kg dry 0.0015Methyl Ethyl Ketone (2-Butanone)
BRL 8260D P0C049410.026 3/25/20 14:14 TBLmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0010Methylene Chloride
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00091Methyl-tert-Butyl Ether
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.00065Naphthalene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00061n-Butylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00094n-Propylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00069o-Xylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00070sec-Butylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00063Styrene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00077tert-Butylbenzene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0012Tetrachloroethylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0010Toluene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0012trans-1,2-Dichloroethylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.00055trans-1,3-Dichloropropylene
BRL 8260D P0C049410.0065 3/25/20 14:14 TBLmg/kg dry 0.0013Trichloroethylene
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0017Trichlorofluoromethane
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.00070Vinyl acetate
BRL 8260D P0C049410.013 3/25/20 14:14 TBLmg/kg dry 0.0013Vinyl chloride
BRL 8260D P0C049410.019 3/25/20 14:14 TBLmg/kg dry 0.0023Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P0C0526100203/26/20 19:25 TBLmg/kg dry 4.0C5-C8 Aliphatics
BRL MADEP VPH P0C0526100203/26/20 19:25 TBLmg/kg dry 1.8C9-C12 Aliphatics
BRL MADEP VPH P0C0526100203/26/20 19:25 TBLmg/kg dry 1.9C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130111 %2,5-Dibromotoluene (PID)
70-130120 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-24
Sample ID: 0030321-03
Work Order: 0030321
Time Collected: 03/20/20 13:20
Time Submitted: 03/24/20 10:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P0C04951323/26/20 15:19 ZRCmg/kg dry 1.6C9-C18 Aliphatics
BRL MADEP EPH P0C04951323/26/20 15:19 ZRCmg/kg dry 5.4C19-C36 Aliphatics
BRL MADEP EPH P0C04951323/26/20 15:19 ZRCmg/kg dry 8.7C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14083 %1-Chlorooctadecane
40-14080 %o-Terphenyl
40-14064 %2-Fluorobiphenyl
40-14057 %2-Bromonaphthalene
General Chemistry Parameters
78.4 *SM2540 G P0C050710.100 3/26/20 7:15 EDV% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.151,2,4-Trichlorobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.141,2-Dichlorobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.121,3-Dichlorobenzene
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.131,4-Dichlorobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0131-Methylnaphthalene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.182,4,5-Trichlorophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.202,4,6-Trichlorophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.162,4-Dichlorophenol
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.172,4-Dimethylphenol
BRL 8270E P0C049711.9 3/25/20 19:25 JMVmg/kg dry 0.492,4-Dinitrophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.222,4-Dinitrotoluene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.222,6-Dinitrotoluene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.212-Chloronaphthalene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.162-Chlorophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0162-Methylnaphthalene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.162-Methylphenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.142-Nitrophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.173,3’-Dichlorobenzidine
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.183/4-Methylphenol
BRL 8270E P0C049711.9 3/25/20 19:25 JMVmg/kg dry 0.464,6-Dinitro-2-methylphenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.204-Bromophenyl phenyl ether
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.164-Chloro-3-methylphenol
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.104-Chloroaniline
BRL 8270E P0C049711.3 3/25/20 19:25 JMVmg/kg dry 0.264-Chlorophenyl phenyl ether
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.214-Nitrophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.019Acenaphthene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.017Acenaphthylene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0093Anthracene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.18Azobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.010Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-24
Sample ID: 0030321-03
Work Order: 0030321
Time Collected: 03/20/20 13:20
Time Submitted: 03/24/20 10:45
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0075Benzo(a)pyrene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0078Benzo(b)fluoranthene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0083Benzo(g,h,i)perylene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0089Benzo(k)fluoranthene
BRL 8270E P0C049712.5 3/25/20 19:25 JMVmg/kg dry 0.70Benzoic Acid
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.16Benzyl alcohol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.19Bis(2-Ethylhexyl)phthalate
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.15Butyl benzyl phthalate
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0099Chrysene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.024Dibenzo(a,h)anthracene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.23Dibenzofuran
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.22Diethyl phthalate
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.20Dimethyl phthalate
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.21Di-n-butyl phthalate
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.22Di-n-octyl phthalate
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0096Fluoranthene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.015Fluorene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.18Hexachlorobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.19Hexachlorobutadiene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.29Hexachlorocyclopentadiene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.13Hexachloroethane
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.024Indeno(1,2,3-cd)pyrene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.18Isophorone
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.018Naphthalene
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.18Nitrobenzene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.19N-Nitroso-di-n-propylamine
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.23N-Nitrosodiphenylamine
BRL 8270E P0C049711.3 3/25/20 19:25 JMVmg/kg dry 0.54Pentachlorophenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.0092Phenanthrene
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.14Phenol
BRL 8270E P0C049710.84 3/25/20 19:25 JMVmg/kg dry 0.012Pyrene
BRL 8270E P0C049710.42 3/25/20 19:25 JMVmg/kg dry 0.080Pyridine
Surrogate Recovery Control Limits
39-13281 %2,4,6-Tribromophenol
44-11574 %2-Fluorobiphenyl
35-11577 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12173 %Phenol-d5
54-12775 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-24
Sample ID: 0030321-03
Work Order: 0030321
Time Collected: 03/20/20 13:20
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000831,1,1,2-Tetrachloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00101,1,1-Trichloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000491,1,2,2-Tetrachloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000731,1,2-Trichloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00121,1-Dichloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00121,1-Dichloroethylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00101,1-Dichloropropylene
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.000971,2,3-Trichlorobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000771,2,3-Trichloropropane
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.000651,2,4-Trichlorobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000721,2,4-Trimethylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000611,2-Dibromoethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000761,2-Dichlorobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000811,2-Dichloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00101,2-Dichloropropane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000851,3,5-Trimethylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000841,3-Dichlorobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000571,3-Dichloropropane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000861,4-Dichlorobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000842,2-Dichloropropane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000912-Chlorotoluene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.000774-Chlorotoluene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00174-Isopropyltoluene
BRL 8260D P0C049410.027 3/25/20 14:44 TBLmg/kg dry 0.0017Acetone
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011Benzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00094Bromobenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011Bromochloromethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00064Bromodichloromethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00052Bromoform
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0033Bromomethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0013Carbon Tetrachloride
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011Chlorobenzene
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0013Chloroethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00083Chloroform
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0021Chloromethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011cis-1,2-Dichloroethylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00067cis-1,3-Dichloropropylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00045Dibromochloromethane
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0019Dichlorodifluoromethane
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0010Ethylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00099Isopropyl Ether
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00079Isopropylbenzene (Cumene)
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0017m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-24
Sample ID: 0030321-03
Work Order: 0030321
Time Collected: 03/20/20 13:20
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.027 3/25/20 14:44 TBLmg/kg dry 0.00047Methyl Butyl Ketone (2-Hexanone)
BRL 8260D P0C049410.027 3/25/20 14:44 TBLmg/kg dry 0.0016Methyl Ethyl Ketone (2-Butanone)
BRL 8260D P0C049410.027 3/25/20 14:44 TBLmg/kg dry 0.00055Methyl Isobutyl Ketone
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011Methylene Chloride
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00095Methyl-tert-Butyl Ether
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.00068Naphthalene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00063n-Butylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00098n-Propylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00072o-Xylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00073sec-Butylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00066Styrene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00080tert-Butylbenzene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0012Tetrachloroethylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0011Toluene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0013trans-1,2-Dichloroethylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.00058trans-1,3-Dichloropropylene
BRL 8260D P0C049410.0068 3/25/20 14:44 TBLmg/kg dry 0.0013Trichloroethylene
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0018Trichlorofluoromethane
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.00073Vinyl acetate
BRL 8260D P0C049410.014 3/25/20 14:44 TBLmg/kg dry 0.0013Vinyl chloride
BRL 8260D P0C049410.020 3/25/20 14:44 TBLmg/kg dry 0.0024Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P0C0526100193/26/20 19:54 TBLmg/kg dry 3.7C5-C8 Aliphatics
BRL MADEP VPH P0C0526100193/26/20 19:54 TBLmg/kg dry 1.6C9-C12 Aliphatics
BRL MADEP VPH P0C0526100193/26/20 19:54 TBLmg/kg dry 1.8C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130119 %2,5-Dibromotoluene (PID)
70-130128 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-25
Sample ID: 0030321-04
Work Order: 0030321
Time Collected: 03/20/20 13:25
Time Submitted: 03/24/20 10:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P0C04951293/26/20 15:55 ZRCmg/kg dry 1.4C9-C18 Aliphatics
BRL MADEP EPH P0C04951293/26/20 15:55 ZRCmg/kg dry 4.8C19-C36 Aliphatics
BRL MADEP EPH P0C04951293/26/20 15:55 ZRCmg/kg dry 7.8C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14083 %1-Chlorooctadecane
40-14074 %o-Terphenyl
40-14070 %2-Fluorobiphenyl
40-14074 %2-Bromonaphthalene
General Chemistry Parameters
85.1 *SM2540 G P0C050710.100 3/26/20 7:15 EDV% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.141,2,4-Trichlorobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.131,2-Dichlorobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.111,3-Dichlorobenzene
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.121,4-Dichlorobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0121-Methylnaphthalene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.162,4,5-Trichlorophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.192,4,6-Trichlorophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.152,4-Dichlorophenol
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.162,4-Dimethylphenol
BRL 8270E P0C049711.8 3/25/20 19:48 JMVmg/kg dry 0.452,4-Dinitrophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.212,4-Dinitrotoluene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.202,6-Dinitrotoluene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.192-Chloronaphthalene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.152-Chlorophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0152-Methylnaphthalene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.152-Methylphenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.132-Nitrophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.153,3’-Dichlorobenzidine
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.173/4-Methylphenol
BRL 8270E P0C049711.8 3/25/20 19:48 JMVmg/kg dry 0.434,6-Dinitro-2-methylphenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.184-Bromophenyl phenyl ether
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.154-Chloro-3-methylphenol
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.0944-Chloroaniline
BRL 8270E P0C049711.2 3/25/20 19:48 JMVmg/kg dry 0.244-Chlorophenyl phenyl ether
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.194-Nitrophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.018Acenaphthene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.015Acenaphthylene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0086Anthracene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.17Azobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0093Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-25
Sample ID: 0030321-04
Work Order: 0030321
Time Collected: 03/20/20 13:25
Time Submitted: 03/24/20 10:45
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0069Benzo(a)pyrene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0071Benzo(b)fluoranthene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0076Benzo(g,h,i)perylene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0082Benzo(k)fluoranthene
BRL 8270E P0C049712.3 3/25/20 19:48 JMVmg/kg dry 0.64Benzoic Acid
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.15Benzyl alcohol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.15bis(2-Chloroethoxy)methane
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.12Bis(2-Chloroethyl)ether
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.14Bis(2-chloroisopropyl)ether
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.17Bis(2-Ethylhexyl)phthalate
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.13Butyl benzyl phthalate
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0091Chrysene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.022Dibenzo(a,h)anthracene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.21Dibenzofuran
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.20Diethyl phthalate
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.19Dimethyl phthalate
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.19Di-n-butyl phthalate
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.20Di-n-octyl phthalate
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0088Fluoranthene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.013Fluorene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.17Hexachlorobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.17Hexachlorobutadiene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.27Hexachlorocyclopentadiene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.12Hexachloroethane
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.022Indeno(1,2,3-cd)pyrene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.17Isophorone
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.016Naphthalene
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.16Nitrobenzene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.18N-Nitroso-di-n-propylamine
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.21N-Nitrosodiphenylamine
BRL 8270E P0C049711.2 3/25/20 19:48 JMVmg/kg dry 0.49Pentachlorophenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.0084Phenanthrene
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.13Phenol
BRL 8270E P0C049710.77 3/25/20 19:48 JMVmg/kg dry 0.011Pyrene
BRL 8270E P0C049710.39 3/25/20 19:48 JMVmg/kg dry 0.074Pyridine
Surrogate Recovery Control Limits
39-13275 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11573 %2-Fluorophenol
37-12266 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12770 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-25
Sample ID: 0030321-04
Work Order: 0030321
Time Collected: 03/20/20 13:25
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000741,1,1,2-Tetrachloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000891,1,1-Trichloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000441,1,2,2-Tetrachloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000661,1,2-Trichloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00111,1-Dichloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00111,1-Dichloroethylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000941,1-Dichloropropylene
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.000871,2,3-Trichlorobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000691,2,3-Trichloropropane
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.000581,2,4-Trichlorobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000641,2,4-Trimethylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000541,2-Dibromoethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000681,2-Dichlorobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000721,2-Dichloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000911,2-Dichloropropane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000761,3,5-Trimethylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000761,3-Dichlorobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000511,3-Dichloropropane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000771,4-Dichlorobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000762,2-Dichloropropane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000822-Chlorotoluene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.000694-Chlorotoluene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00154-Isopropyltoluene
BRL 8260D P0C049410.024 3/25/20 15:14 TBLmg/kg dry 0.0016Acetone
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00095Benzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00084Bromobenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.0010Bromochloromethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00058Bromodichloromethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00047Bromoform
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0030Bromomethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.0012Carbon Tetrachloride
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00095Chlorobenzene
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0012Chloroethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00074Chloroform
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0018Chloromethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00096cis-1,2-Dichloroethylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00060cis-1,3-Dichloropropylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00041Dibromochloromethane
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0017Dichlorodifluoromethane
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00091Ethylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00089Isopropyl Ether
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00071Isopropylbenzene (Cumene)
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0016m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-25
Sample ID: 0030321-04
Work Order: 0030321
Time Collected: 03/20/20 13:25
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.024 3/25/20 15:14 TBLmg/kg dry 0.00042Methyl Butyl Ketone (2-Hexanone)
BRL 8260D P0C049410.024 3/25/20 15:14 TBLmg/kg dry 0.0014Methyl Ethyl Ketone (2-Butanone)
BRL 8260D P0C049410.024 3/25/20 15:14 TBLmg/kg dry 0.00050Methyl Isobutyl Ketone
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00098Methylene Chloride
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00085Methyl-tert-Butyl Ether
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.00061Naphthalene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00057n-Butylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00088n-Propylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00065o-Xylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00066sec-Butylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00059Styrene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00072tert-Butylbenzene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.0011Tetrachloroethylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00097Toluene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.0012trans-1,2-Dichloroethylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.00052trans-1,3-Dichloropropylene
BRL 8260D P0C049410.0061 3/25/20 15:14 TBLmg/kg dry 0.0012Trichloroethylene
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0016Trichlorofluoromethane
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.00066Vinyl acetate
BRL 8260D P0C049410.012 3/25/20 15:14 TBLmg/kg dry 0.0012Vinyl chloride
BRL 8260D P0C049410.018 3/25/20 15:14 TBLmg/kg dry 0.0022Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P0C0526100173/26/20 20:24 TBLmg/kg dry 3.4C5-C8 Aliphatics
BRL MADEP VPH P0C0526100173/26/20 20:24 TBLmg/kg dry 1.5C9-C12 Aliphatics
BRL MADEP VPH P0C0526100173/26/20 20:24 TBLmg/kg dry 1.6C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130116 %2,5-Dibromotoluene (PID)
70-130125 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-26
Sample ID: 0030321-05
Work Order: 0030321
Time Collected: 03/20/20 13:30
Time Submitted: 03/24/20 10:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P0C04951313/26/20 16:32 ZRCmg/kg dry 1.6C9-C18 Aliphatics
BRL MADEP EPH P0C04951313/26/20 16:32 ZRCmg/kg dry 5.2C19-C36 Aliphatics
BRL MADEP EPH P0C04951313/26/20 16:32 ZRCmg/kg dry 8.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14084 %1-Chlorooctadecane
40-14079 %o-Terphenyl
40-14070 %2-Fluorobiphenyl
40-14062 %2-Bromonaphthalene
General Chemistry Parameters
78.8 *SM2540 G P0C050710.100 3/26/20 7:15 EDV% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.151,2,4-Trichlorobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.141,2-Dichlorobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.121,3-Dichlorobenzene
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.131,4-Dichlorobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0131-Methylnaphthalene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.182,4,5-Trichlorophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.202,4,6-Trichlorophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.162,4-Dichlorophenol
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.172,4-Dimethylphenol
BRL 8270E P0C049711.9 3/25/20 20:10 JMVmg/kg dry 0.492,4-Dinitrophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.222,4-Dinitrotoluene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.222,6-Dinitrotoluene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.202-Chloronaphthalene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.162-Chlorophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0162-Methylnaphthalene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.162-Methylphenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.142-Nitrophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.173,3’-Dichlorobenzidine
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.183/4-Methylphenol
BRL 8270E P0C049711.9 3/25/20 20:10 JMVmg/kg dry 0.464,6-Dinitro-2-methylphenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.204-Bromophenyl phenyl ether
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.164-Chloro-3-methylphenol
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.104-Chloroaniline
BRL 8270E P0C049711.3 3/25/20 20:10 JMVmg/kg dry 0.264-Chlorophenyl phenyl ether
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.214-Nitrophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.019Acenaphthene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.016Acenaphthylene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0093Anthracene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.18Azobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.010Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-26
Sample ID: 0030321-05
Work Order: 0030321
Time Collected: 03/20/20 13:30
Time Submitted: 03/24/20 10:45
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0075Benzo(a)pyrene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0077Benzo(b)fluoranthene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0082Benzo(g,h,i)perylene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0089Benzo(k)fluoranthene
BRL 8270E P0C049712.5 3/25/20 20:10 JMVmg/kg dry 0.69Benzoic Acid
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.16Benzyl alcohol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.19Bis(2-Ethylhexyl)phthalate
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.14Butyl benzyl phthalate
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0099Chrysene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.024Dibenzo(a,h)anthracene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.23Dibenzofuran
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.22Diethyl phthalate
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.20Dimethyl phthalate
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.21Di-n-butyl phthalate
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.22Di-n-octyl phthalate
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0095Fluoranthene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.014Fluorene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.18Hexachlorobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.19Hexachlorobutadiene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.29Hexachlorocyclopentadiene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.13Hexachloroethane
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.024Indeno(1,2,3-cd)pyrene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.18Isophorone
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.018Naphthalene
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.18Nitrobenzene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.19N-Nitroso-di-n-propylamine
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.23N-Nitrosodiphenylamine
BRL 8270E P0C049711.3 3/25/20 20:10 JMVmg/kg dry 0.53Pentachlorophenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.0091Phenanthrene
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.14Phenol
BRL 8270E P0C049710.84 3/25/20 20:10 JMVmg/kg dry 0.012Pyrene
BRL 8270E P0C049710.42 3/25/20 20:10 JMVmg/kg dry 0.080Pyridine
Surrogate Recovery Control Limits
39-13278 %2,4,6-Tribromophenol
44-11568 %2-Fluorobiphenyl
35-11573 %2-Fluorophenol
37-12265 %Nitrobenzene-d5
34-12171 %Phenol-d5
54-12771 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-26
Sample ID: 0030321-05
Work Order: 0030321
Time Collected: 03/20/20 13:30
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000731,1,1,2-Tetrachloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000881,1,1-Trichloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000641,1,2-Trichloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00111,1-Dichloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00111,1-Dichloroethylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000921,1-Dichloropropylene
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.000851,2,3-Trichlorobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000681,2,3-Trichloropropane
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.000571,2,4-Trichlorobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000631,2,4-Trimethylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000531,2-Dibromoethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000671,2-Dichlorobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000711,2-Dichloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000901,2-Dichloropropane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000751,3,5-Trimethylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000741,3-Dichlorobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000501,3-Dichloropropane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000761,4-Dichlorobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000742,2-Dichloropropane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000802-Chlorotoluene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.000684-Chlorotoluene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00154-Isopropyltoluene
BRL 8260D P0C049410.024 3/25/20 15:44 TBLmg/kg dry 0.0015Acetone
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00093Benzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00083Bromobenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00098Bromochloromethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00057Bromodichloromethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00046Bromoform
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0029Bromomethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.0012Carbon Tetrachloride
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00093Chlorobenzene
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0011Chloroethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00073Chloroform
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0018Chloromethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00094cis-1,2-Dichloroethylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00059cis-1,3-Dichloropropylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00040Dibromochloromethane
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0017Dichlorodifluoromethane
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00090Ethylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00088Isopropyl Ether
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00069Isopropylbenzene (Cumene)
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0015m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 41
Laboratory Report
03/31/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-26
Sample ID: 0030321-05
Work Order: 0030321
Time Collected: 03/20/20 13:30
Time Submitted: 03/24/20 10:45
BRL 8260D P0C049410.024 3/25/20 15:44 TBLmg/kg dry 0.00041Methyl Butyl Ketone (2-Hexanone)
BRL 8260D P0C049410.024 3/25/20 15:44 TBLmg/kg dry 0.0014Methyl Ethyl Ketone (2-Butanone)
BRL 8260D P0C049410.024 3/25/20 15:44 TBLmg/kg dry 0.00049Methyl Isobutyl Ketone
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00096Methylene Chloride
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00084Methyl-tert-Butyl Ether
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.00060Naphthalene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00056n-Butylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00086n-Propylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00063o-Xylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00064sec-Butylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00058Styrene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00071tert-Butylbenzene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.0011Tetrachloroethylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00095Toluene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.0011trans-1,2-Dichloroethylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.00051trans-1,3-Dichloropropylene
BRL 8260D P0C049410.0060 3/25/20 15:44 TBLmg/kg dry 0.0012Trichloroethylene
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0016Trichlorofluoromethane
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.00065Vinyl acetate
BRL 8260D P0C049410.012 3/25/20 15:44 TBLmg/kg dry 0.0012Vinyl chloride
BRL 8260D P0C049410.018 3/25/20 15:44 TBLmg/kg dry 0.0021Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12997 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P0C0526100193/26/20 20:53 TBLmg/kg dry 3.8C5-C8 Aliphatics
BRL MADEP VPH P0C0526100193/26/20 20:53 TBLmg/kg dry 1.7C9-C12 Aliphatics
BRL MADEP VPH P0C0526100193/26/20 20:53 TBLmg/kg dry 1.8C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130109 %2,5-Dibromotoluene (PID)
70-130118 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
Blank (P0C0494-BLK1)Prepared & Analyzed: 03/25/20
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0050
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
Blank (P0C0494-BLK1)Prepared & Analyzed: 03/25/20
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
Naphthalene mg/kg wet0.000550 0.010 J
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl acetate mg/kg wetBRL0.010
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.8
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.5
LCS (P0C0494-BS1)Prepared & Analyzed: 03/25/20
1,1,1,2-Tetrachloroethane mg/kg wet0.0494 0.0050 0.05000 72-11599
1,1,1-Trichloroethane mg/kg wet0.0481 0.0050 0.05000 67-13196
1,1,2,2-Tetrachloroethane mg/kg wet0.0497 0.0050 0.05000 56-12699
1,1,2-Trichloroethane mg/kg wet0.0501 0.0050 0.05000 70-133100
1,1-Dichloroethane mg/kg wet0.0490 0.0050 0.05000 74-12798
1,1-Dichloroethylene mg/kg wet0.0488 0.0050 0.05000 67-14998
1,1-Dichloropropylene mg/kg wet0.0475 0.0050 0.05000 71-13095
1,2,3-Trichlorobenzene mg/kg wet0.0497 0.010 0.05000 68-13099
1,2,3-Trichloropropane mg/kg wet0.0505 0.0050 0.05000 60-137101
1,2,4-Trichlorobenzene mg/kg wet0.0503 0.010 0.05000 66-125101
1,2,4-Trimethylbenzene mg/kg wet0.0488 0.0050 0.05000 69-12997
1,2-Dibromoethane mg/kg wet0.0511 0.0050 0.05000 70-132102
1,2-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 72-12396
1,2-Dichloroethane mg/kg wet0.0490 0.0050 0.05000 68-12898
1,2-Dichloropropane mg/kg wet0.0507 0.0050 0.05000 73-130101
1,3,5-Trimethylbenzene mg/kg wet0.0474 0.0050 0.05000 69-12895
1,3-Dichlorobenzene mg/kg wet0.0481 0.0050 0.05000 71-12096
1,3-Dichloropropane mg/kg wet0.0499 0.0050 0.05000 75-124100
1,4-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 71-12396
2,2-Dichloropropane mg/kg wet0.0482 0.0050 0.05000 50-14296
2-Chlorotoluene mg/kg wet0.0478 0.0050 0.05000 67-12496
4-Chlorotoluene mg/kg wet0.0478 0.0050 0.05000 71-12696
4-Isopropyltoluene mg/kg wet0.0497 0.0050 0.05000 68-12999
Acetone mg/kg wet0.123 0.020 0.1000 29-198123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
LCS (P0C0494-BS1)Prepared & Analyzed: 03/25/20
Benzene mg/kg wet0.0481 0.0050 0.05000 74-12796
Bromobenzene mg/kg wet0.0476 0.0050 0.05000 73-12595
Bromochloromethane mg/kg wet0.0486 0.0050 0.05000 72-13497
Bromodichloromethane mg/kg wet0.0508 0.0050 0.05000 75-122102
Bromoform mg/kg wet0.0467 0.0050 0.05000 66-13593
Bromomethane mg/kg wet0.0440 0.010 0.05000 20-18088
Carbon Tetrachloride mg/kg wet0.0475 0.0050 0.05000 64-14395
Chlorobenzene mg/kg wet0.0479 0.0050 0.05000 74-11896
Chloroethane mg/kg wet0.0422 0.010 0.05000 33-14984
Chloroform mg/kg wet0.0492 0.0050 0.05000 73-12798
Chloromethane mg/kg wet0.0474 0.010 0.05000 45-14395
cis-1,2-Dichloroethylene mg/kg wet0.0494 0.0050 0.05000 76-13499
cis-1,3-Dichloropropylene mg/kg wet0.0519 0.0050 0.05000 71-125104
Dibromochloromethane mg/kg wet0.0515 0.0050 0.05000 73-122103
Dichlorodifluoromethane mg/kg wet0.0472 0.010 0.05000 26-14694
Ethylbenzene mg/kg wet0.0467 0.0050 0.05000 74-12893
Isopropyl Ether mg/kg wet0.0506 0.0050 0.05000 59-159101
Isopropylbenzene (Cumene)mg/kg wet0.0474 0.0050 0.05000 68-12695
m,p-Xylenes mg/kg wet0.0969 0.010 0.1000 75-12497
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0588 0.020 0.05000 61-157118
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0555 0.020 0.05000 63-149111
Methyl Isobutyl Ketone mg/kg wet0.0559 0.020 0.05000 57-162112
Methylene Chloride mg/kg wet0.0474 0.0050 0.05000 74-12995
Methyl-tert-Butyl Ether mg/kg wet0.0518 0.0050 0.05000 70-130104
Naphthalene mg/kg wet0.0526 0.010 0.05000 57-157105
n-Butylbenzene mg/kg wet0.0493 0.0050 0.05000 65-13599
n-Propylbenzene mg/kg wet0.0472 0.0050 0.05000 67-13094
o-Xylene mg/kg wet0.0488 0.0050 0.05000 74-12698
sec-Butylbenzene mg/kg wet0.0484 0.0050 0.05000 66-13197
Styrene mg/kg wet0.0521 0.0050 0.05000 77-121104
tert-Butylbenzene mg/kg wet0.0477 0.0050 0.05000 67-13295
Tetrachloroethylene mg/kg wet0.0478 0.0050 0.05000 68-13096
Toluene mg/kg wet0.0480 0.0050 0.05000 71-12996
trans-1,2-Dichloroethylene mg/kg wet0.0486 0.0050 0.05000 73-13297
trans-1,3-Dichloropropylene mg/kg wet0.0531 0.0050 0.05000 68-123106
Trichloroethylene mg/kg wet0.0490 0.0050 0.05000 75-13398
Trichlorofluoromethane mg/kg wet0.0447 0.010 0.05000 44-14689
Vinyl acetate mg/kg wet0.0522 0.010 0.05000 85-161104
Vinyl chloride mg/kg wet0.0485 0.010 0.05000 48-14797
Xylenes, total mg/kg wet0.146 0.015 0.1500 74-12697
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.5
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
Matrix Spike (P0C0494-MS1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0518 0.0065 0.06510 BRL 60-12080
1,1,1-Trichloroethane mg/kg dry0.0323 0.0065 0.06510 BRL M52-13950
1,1,2,2-Tetrachloroethane mg/kg dry0.0515 0.0065 0.06510 BRL 39-13579
1,1,2-Trichloroethane mg/kg dry0.0514 0.0065 0.06510 BRL 44-14079
1,1-Dichloroethane mg/kg dry0.0244 0.0065 0.06510 BRL M59-13737
1,1-Dichloroethylene mg/kg dry0.00134 0.0065 0.06510 BRL M, J54-1622
1,1-Dichloropropylene mg/kg dry0.0271 0.0065 0.06510 BRL M55-13742
1,2,3-Trichlorobenzene mg/kg dry0.0500 0.013 0.06510 BRL 34-12077
1,2,3-Trichloropropane mg/kg dry0.0510 0.0065 0.06510 BRL 45-13978
1,2,4-Trichlorobenzene mg/kg dry0.0498 0.013 0.06510 BRL 35-11677
1,2,4-Trimethylbenzene mg/kg dry0.0520 0.0065 0.06510 BRL 38-14280
1,2-Dibromoethane mg/kg dry0.0513 0.0065 0.06510 BRL 49-13279
1,2-Dichlorobenzene mg/kg dry0.0518 0.0065 0.06510 BRL 42-13080
1,2-Dichloroethane mg/kg dry0.0388 0.0065 0.06510 BRL 51-13160
1,2-Dichloropropane mg/kg dry0.0457 0.0065 0.06510 BRL 55-13870
1,3,5-Trimethylbenzene mg/kg dry0.0539 0.0065 0.06510 BRL 44-14083
1,3-Dichlorobenzene mg/kg dry0.0506 0.0065 0.06510 BRL 41-12978
1,3-Dichloropropane mg/kg dry0.0504 0.0065 0.06510 BRL 53-12977
1,4-Dichlorobenzene mg/kg dry0.0493 0.0065 0.06510 BRL 44-13476
2,2-Dichloropropane mg/kg dry0.0276 0.0065 0.06510 BRL 30-14742
2-Chlorotoluene mg/kg dry0.0522 0.0065 0.06510 BRL 46-13280
4-Chlorotoluene mg/kg dry0.0522 0.0065 0.06510 BRL 44-13580
4-Isopropyltoluene mg/kg dry0.0532 0.0065 0.06510 BRL 32-14482
Acetone mg/kg dry0.0682 0.026 0.1302 BRL 34-14352
Benzene mg/kg dry0.0313 0.0065 0.06510 BRL M60-13548
Bromobenzene mg/kg dry0.0506 0.0065 0.06510 BRL 45-13578
Bromochloromethane mg/kg dry0.0332 0.0065 0.06510 BRL M55-13651
Bromodichloromethane mg/kg dry0.0481 0.0065 0.06510 BRL 55-12774
Bromoform mg/kg dry0.0479 0.0065 0.06510 BRL 40-13674
Bromomethane mg/kg dry0.0430 0.013 0.06510 BRL 30-13766
Carbon Tetrachloride mg/kg dry0.0307 0.0065 0.06510 BRL M48-15347
Chlorobenzene mg/kg dry0.0501 0.0065 0.06510 BRL 57-12577
Chloroethane mg/kg dry0.0486 0.013 0.06510 BRL 16-17775
Chloroform mg/kg dry0.0421 0.0065 0.06510 BRL 56-13765
Chloromethane mg/kg dry0.0552 0.013 0.06510 BRL 40-14585
cis-1,2-Dichloroethylene mg/kg dry0.0310 0.0065 0.06510 BRL M58-14048
cis-1,3-Dichloropropylene mg/kg dry0.0510 0.0065 0.06510 BRL 42-13578
Dibromochloromethane mg/kg dry0.0543 0.0065 0.06510 BRL 49-12783
Dichlorodifluoromethane mg/kg dry0.0540 0.013 0.06510 BRL 25-15183
Ethylbenzene mg/kg dry0.0502 0.0065 0.06510 BRL 44-14477
Isopropyl Ether mg/kg dry0.0483 0.0065 0.06510 BRL 51-15574
Isopropylbenzene (Cumene)mg/kg dry0.0539 0.0065 0.06510 BRL 41-14083
m,p-Xylenes mg/kg dry0.103 0.013 0.1302 BRL 36-14879
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0486 0.026 0.06510 BRL 30-14775
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0403 0.026 0.06510 BRL 24-16062
Methyl Isobutyl Ketone mg/kg dry0.0503 0.026 0.06510 BRL 25-16377
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
Matrix Spike (P0C0494-MS1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
Methylene Chloride mg/kg dry0.0153 0.0065 0.06510 BRL M53-14423
Methyl-tert-Butyl Ether mg/kg dry0.0468 0.0065 0.06510 BRL 49-13572
Naphthalene mg/kg dry0.0521 0.013 0.06510 BRL 32-12780
n-Butylbenzene mg/kg dry0.0523 0.0065 0.06510 BRL 23-14880
n-Propylbenzene mg/kg dry0.0516 0.0065 0.06510 BRL 35-14479
o-Xylene mg/kg dry0.0512 0.0065 0.06510 BRL 43-14379
sec-Butylbenzene mg/kg dry0.0535 0.0065 0.06510 BRL 34-14482
Styrene mg/kg dry0.0557 0.0065 0.06510 BRL 42-13286
tert-Butylbenzene mg/kg dry0.0534 0.0065 0.06510 BRL 36-15082
Tetrachloroethylene mg/kg dry0.0483 0.0065 0.06510 BRL 47-14274
Toluene mg/kg dry0.0466 0.0065 0.06510 BRL 57-13572
trans-1,2-Dichloroethylene mg/kg dry0.0130 0.0065 0.06510 BRL M58-14120
trans-1,3-Dichloropropylene mg/kg dry0.0526 0.0065 0.06510 BRL 41-12481
Trichloroethylene mg/kg dry0.0413 0.0065 0.06510 BRL 38-16463
Trichlorofluoromethane mg/kg dry0.0512 0.013 0.06510 BRL 30-15779
Vinyl acetate mg/kg dry0.0441 0.013 0.06510 BRL 61-15468
Vinyl chloride mg/kg dry0.0520 0.013 0.06510 BRL 40-15680
Xylenes, total mg/kg dry0.154 0.020 0.1953 BRL 36-14879
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.6
Matrix Spike Dup (P0C0494-MSD1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0494 0.0065 0.06510 BRL 1560-12076 5
1,1,1-Trichloroethane mg/kg dry0.0302 0.0065 0.06510 BRL 21 M52-13946 7
1,1,2,2-Tetrachloroethane mg/kg dry0.0482 0.0065 0.06510 BRL 2239-13574 7
1,1,2-Trichloroethane mg/kg dry0.0494 0.0065 0.06510 BRL 2144-14076 4
1,1-Dichloroethane mg/kg dry0.0231 0.0065 0.06510 BRL 21 M59-13736 5
1,1-Dichloroethylene mg/kg dry0.00138 0.0065 0.06510 BRL 22 M, J54-1622 3
1,1-Dichloropropylene mg/kg dry0.0250 0.0065 0.06510 BRL 19 M55-13738 8
1,2,3-Trichlorobenzene mg/kg dry0.0476 0.013 0.06510 BRL 4134-12073 5
1,2,3-Trichloropropane mg/kg dry0.0487 0.0065 0.06510 BRL 2545-13975 5
1,2,4-Trichlorobenzene mg/kg dry0.0470 0.013 0.06510 BRL 6235-11672 6
1,2,4-Trimethylbenzene mg/kg dry0.0498 0.0065 0.06510 BRL 2438-14277 4
1,2-Dibromoethane mg/kg dry0.0498 0.0065 0.06510 BRL 1549-13277 3
1,2-Dichlorobenzene mg/kg dry0.0466 0.0065 0.06510 BRL 2142-13072 11
1,2-Dichloroethane mg/kg dry0.0374 0.0065 0.06510 BRL 1351-13157 4
1,2-Dichloropropane mg/kg dry0.0435 0.0065 0.06510 BRL 1655-13867 5
1,3,5-Trimethylbenzene mg/kg dry0.0487 0.0065 0.06510 BRL 2944-14075 10
1,3-Dichlorobenzene mg/kg dry0.0503 0.0065 0.06510 BRL 2441-12977 0.6
1,3-Dichloropropane mg/kg dry0.0486 0.0065 0.06510 BRL 1553-12975 4
1,4-Dichlorobenzene mg/kg dry0.0468 0.0065 0.06510 BRL 2144-13472 5
2,2-Dichloropropane mg/kg dry0.0263 0.0065 0.06510 BRL 2030-14740 5
2-Chlorotoluene mg/kg dry0.0472 0.0065 0.06510 BRL 2946-13272 10
4-Chlorotoluene mg/kg dry0.0472 0.0065 0.06510 BRL 2344-13572 10
4-Isopropyltoluene mg/kg dry0.0509 0.0065 0.06510 BRL 2232-14478 4
Acetone mg/kg dry0.0657 0.026 0.1302 BRL 4934-14350 4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0C0494 - 5035
Matrix Spike Dup (P0C0494-MSD1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
Benzene mg/kg dry0.0295 0.0065 0.06510 BRL 20 M60-13545 6
Bromobenzene mg/kg dry0.0473 0.0065 0.06510 BRL 2545-13573 7
Bromochloromethane mg/kg dry0.0318 0.0065 0.06510 BRL 18 M55-13649 4
Bromodichloromethane mg/kg dry0.0462 0.0065 0.06510 BRL 1755-12771 4
Bromoform mg/kg dry0.0464 0.0065 0.06510 BRL 3540-13671 3
Bromomethane mg/kg dry0.0387 0.013 0.06510 BRL 3030-13759 11
Carbon Tetrachloride mg/kg dry0.0287 0.0065 0.06510 BRL 23 M48-15344 7
Chlorobenzene mg/kg dry0.0479 0.0065 0.06510 BRL 1457-12574 5
Chloroethane mg/kg dry0.0457 0.013 0.06510 BRL 4716-17770 6
Chloroform mg/kg dry0.0405 0.0065 0.06510 BRL 1856-13762 4
Chloromethane mg/kg dry0.0535 0.013 0.06510 BRL 2640-14582 3
cis-1,2-Dichloroethylene mg/kg dry0.0294 0.0065 0.06510 BRL 28 M58-14045 5
cis-1,3-Dichloropropylene mg/kg dry0.0495 0.0065 0.06510 BRL 3242-13576 3
Dibromochloromethane mg/kg dry0.0512 0.0065 0.06510 BRL 2449-12779 6
Dichlorodifluoromethane mg/kg dry0.0488 0.013 0.06510 BRL 3725-15175 10
Ethylbenzene mg/kg dry0.0475 0.0065 0.06510 BRL 1944-14473 5
Isopropyl Ether mg/kg dry0.0466 0.0065 0.06510 BRL 1351-15572 4
Isopropylbenzene (Cumene)mg/kg dry0.0487 0.0065 0.06510 BRL 2741-14075 10
m,p-Xylenes mg/kg dry0.0965 0.013 0.1302 BRL 2036-14874 7
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0470 0.026 0.06510 BRL 4230-14772 3
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0388 0.026 0.06510 BRL 4224-16060 4
Methyl Isobutyl Ketone mg/kg dry0.0490 0.026 0.06510 BRL 4425-16375 3
Methylene Chloride mg/kg dry0.0146 0.0065 0.06510 BRL 14 M53-14422 4
Methyl-tert-Butyl Ether mg/kg dry0.0455 0.0065 0.06510 BRL 2249-13570 3
Naphthalene mg/kg dry0.0492 0.013 0.06510 BRL 4432-12776 6
n-Butylbenzene mg/kg dry0.0469 0.0065 0.06510 BRL 3923-14872 11
n-Propylbenzene mg/kg dry0.0468 0.0065 0.06510 BRL 2735-14472 10
o-Xylene mg/kg dry0.0485 0.0065 0.06510 BRL 1743-14375 5
sec-Butylbenzene mg/kg dry0.0505 0.0065 0.06510 BRL 2834-14478 6
Styrene mg/kg dry0.0526 0.0065 0.06510 BRL 2842-13281 6
tert-Butylbenzene mg/kg dry0.0504 0.0065 0.06510 BRL 2936-15078 6
Tetrachloroethylene mg/kg dry0.0447 0.0065 0.06510 BRL 2647-14269 8
Toluene mg/kg dry0.0440 0.0065 0.06510 BRL 2257-13568 6
trans-1,2-Dichloroethylene mg/kg dry0.0126 0.0065 0.06510 BRL 18 M58-14119 3
trans-1,3-Dichloropropylene mg/kg dry0.0504 0.0065 0.06510 BRL 2041-12477 4
Trichloroethylene mg/kg dry0.0383 0.0065 0.06510 BRL 1838-16459 8
Trichlorofluoromethane mg/kg dry0.0474 0.013 0.06510 BRL 2730-15773 8
Vinyl acetate mg/kg dry0.0411 0.013 0.06510 BRL 3561-15463 7
Vinyl chloride mg/kg dry0.0482 0.013 0.06510 BRL 3540-15674 7
Xylenes, total mg/kg dry0.145 0.020 0.1953 BRL 2036-14874 6
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
Blank (P0C0497-BLK1)Prepared & Analyzed: 03/25/20
1,2,4-Trichlorobenzene mg/kg wetBRL0.66
1,2-Dichlorobenzene mg/kg wetBRL0.66
1,3-Dichlorobenzene mg/kg wetBRL0.66
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.66
2,4,5-Trichlorophenol mg/kg wetBRL0.66
2,4,6-Trichlorophenol mg/kg wetBRL0.66
2,4-Dichlorophenol mg/kg wetBRL0.66
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL1.5
2,4-Dinitrotoluene mg/kg wetBRL0.66
2,6-Dinitrotoluene mg/kg wetBRL0.66
2-Chloronaphthalene mg/kg wetBRL0.66
2-Chlorophenol mg/kg wetBRL0.66
2-Methylnaphthalene mg/kg wetBRL0.66
2-Methylphenol mg/kg wetBRL0.66
2-Nitrophenol mg/kg wetBRL0.66
3,3’-Dichlorobenzidine mg/kg wetBRL0.66
3/4-Methylphenol mg/kg wetBRL0.66
4,6-Dinitro-2-methylphenol mg/kg wetBRL1.5
4-Bromophenyl phenyl ether mg/kg wetBRL0.66
4-Chloro-3-methylphenol mg/kg wetBRL0.66
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL1.0
4-Nitrophenol mg/kg wetBRL0.66
Acenaphthene mg/kg wetBRL0.66
Acenaphthylene mg/kg wetBRL0.66
Anthracene mg/kg wetBRL0.66
Azobenzene mg/kg wetBRL0.66
Benzo(a)anthracene mg/kg wetBRL0.66
Benzo(a)pyrene mg/kg wetBRL0.66
Benzo(b)fluoranthene mg/kg wetBRL0.66
Benzo(g,h,i)perylene mg/kg wetBRL0.66
Benzo(k)fluoranthene mg/kg wetBRL0.66
Benzoic Acid mg/kg wetBRL2.0
Benzyl alcohol mg/kg wetBRL0.66
bis(2-Chloroethoxy)methane mg/kg wetBRL0.66
Bis(2-Chloroethyl)ether mg/kg wetBRL0.66
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.66
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.66
Dibenzo(a,h)anthracene mg/kg wetBRL0.66
Dibenzofuran mg/kg wetBRL0.66
Diethyl phthalate mg/kg wetBRL0.66
Dimethyl phthalate mg/kg wetBRL0.66
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
Blank (P0C0497-BLK1)Prepared & Analyzed: 03/25/20
Di-n-butyl phthalate mg/kg wetBRL0.66
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.66
Fluorene mg/kg wetBRL0.66
Hexachlorobenzene mg/kg wetBRL0.66
Hexachlorobutadiene mg/kg wetBRL0.66
Hexachlorocyclopentadiene mg/kg wetBRL0.66
Hexachloroethane mg/kg wetBRL0.66
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66
Isophorone mg/kg wetBRL0.66
Naphthalene mg/kg wetBRL0.66
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.66
N-Nitrosodiphenylamine mg/kg wetBRL0.66
Pentachlorophenol mg/kg wetBRL1.0
Phenanthrene mg/kg wetBRL0.66
Phenol mg/kg wetBRL0.66
Pyrene mg/kg wetBRL0.66
Pyridine mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 892.97
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 851.42
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 892.96
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 821.37
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 852.83
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 871.46
LCS (P0C0497-BS1)Prepared & Analyzed: 03/25/20
1,2,4-Trichlorobenzene mg/kg wet1.37 0.66 1.667 34-11882
1,2-Dichlorobenzene mg/kg wet1.33 0.66 1.667 33-11780
1,3-Dichlorobenzene mg/kg wet1.30 0.66 1.667 30-11578
1,4-Dichlorobenzene mg/kg wet1.28 0.33 1.667 31-11577
1-Methylnaphthalene mg/kg wet1.53 0.66 1.667 40-11992
2,4,5-Trichlorophenol mg/kg wet1.45 0.66 1.667 62-12487
2,4,6-Trichlorophenol mg/kg wet1.56 0.66 1.667 39-12694
2,4-Dichlorophenol mg/kg wet1.49 0.66 1.667 40-12290
2,4-Dimethylphenol mg/kg wet1.78 0.33 1.667 30-127107
2,4-Dinitrophenol mg/kg wet0.828 1.5 1.667 J27-12950
2,4-Dinitrotoluene mg/kg wet1.50 0.66 1.667 48-12690
2,6-Dinitrotoluene mg/kg wet1.54 0.66 1.667 46-12493
2-Chloronaphthalene mg/kg wet1.46 0.66 1.667 41-11488
2-Chlorophenol mg/kg wet1.51 0.66 1.667 34-12191
2-Methylnaphthalene mg/kg wet1.45 0.66 1.667 38-12287
2-Methylphenol mg/kg wet1.55 0.66 1.667 32-12293
2-Nitrophenol mg/kg wet1.40 0.66 1.667 36-12384
3,3’-Dichlorobenzidine mg/kg wet1.49 0.66 1.667 22-12189
3/4-Methylphenol mg/kg wet1.42 0.66 1.667 34-11985
4,6-Dinitro-2-methylphenol mg/kg wet1.40 1.5 1.667 J29-13284
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
LCS (P0C0497-BS1)Prepared & Analyzed: 03/25/20
4-Bromophenyl phenyl ether mg/kg wet1.51 0.66 1.667 46-12491
4-Chloro-3-methylphenol mg/kg wet1.49 0.66 1.667 45-12290
4-Chloroaniline mg/kg wet1.40 0.33 1.667 17-10684
4-Chlorophenyl phenyl ether mg/kg wet1.43 1.0 1.667 45-12186
4-Nitrophenol mg/kg wet1.50 0.66 1.667 30-13290
Acenaphthene mg/kg wet1.56 0.66 1.667 40-12394
Acenaphthylene mg/kg wet1.63 0.66 1.667 32-13298
Anthracene mg/kg wet1.58 0.66 1.667 47-12395
Azobenzene mg/kg wet1.67 0.66 1.667 39-125100
Benzo(a)anthracene mg/kg wet1.44 0.66 1.667 49-12687
Benzo(a)pyrene mg/kg wet1.59 0.66 1.667 45-12996
Benzo(b)fluoranthene mg/kg wet1.50 0.66 1.667 45-13290
Benzo(g,h,i)perylene mg/kg wet1.52 0.66 1.667 43-13491
Benzo(k)fluoranthene mg/kg wet1.52 0.66 1.667 47-13291
Benzoic Acid mg/kg wetBRL2.0 1.667 L10-83
Benzyl alcohol mg/kg wet1.53 0.66 1.667 29-12292
bis(2-Chloroethoxy)methane mg/kg wet1.35 0.66 1.667 36-12181
Bis(2-Chloroethyl)ether mg/kg wet1.32 0.66 1.667 31-12079
Bis(2-chloroisopropyl)ether mg/kg wet1.29 0.33 1.667 33-13177
Bis(2-Ethylhexyl)phthalate mg/kg wet1.53 0.66 1.667 51-13392
Butyl benzyl phthalate mg/kg wet1.50 0.33 1.667 48-13290
Chrysene mg/kg wet1.46 0.66 1.667 50-12487
Dibenzo(a,h)anthracene mg/kg wet0.778 0.66 1.667 45-13447
Dibenzofuran mg/kg wet1.46 0.66 1.667 44-12088
Diethyl phthalate mg/kg wet1.41 0.66 1.667 50-12485
Dimethyl phthalate mg/kg wet1.44 0.66 1.667 48-12486
Di-n-butyl phthalate mg/kg wet1.60 0.66 1.667 51-12896
Di-n-octyl phthalate mg/kg wet1.54 0.33 1.667 45-14092
Fluoranthene mg/kg wet1.55 0.66 1.667 50-12793
Fluorene mg/kg wet1.50 0.66 1.667 43-12590
Hexachlorobenzene mg/kg wet1.54 0.66 1.667 45-12292
Hexachlorobutadiene mg/kg wet1.42 0.66 1.667 32-12385
Hexachlorocyclopentadiene mg/kg wet1.35 0.66 1.667 32-11781
Hexachloroethane mg/kg wet1.29 0.66 1.667 28-11778
Indeno(1,2,3-cd)pyrene mg/kg wet1.38 0.66 1.667 45-13383
Isophorone mg/kg wet1.16 0.66 1.667 30-12269
Naphthalene mg/kg wet1.37 0.66 1.667 35-12382
Nitrobenzene mg/kg wet1.22 0.33 1.667 34-12273
N-Nitroso-di-n-propylamine mg/kg wet1.48 0.66 1.667 36-12089
N-Nitrosodiphenylamine mg/kg wet1.93 0.66 1.667 38-127116
Pentachlorophenol mg/kg wet1.68 1.0 1.667 25-133101
Phenanthrene mg/kg wet1.53 0.66 1.667 50-12192
Phenol mg/kg wet1.54 0.66 1.667 34-12192
Pyrene mg/kg wet1.59 0.66 1.667 47-12795
Pyridine mg/kg wet0.914 0.33 1.667 10-6055
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 963.19
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
LCS (P0C0497-BS1)Prepared & Analyzed: 03/25/20
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 861.44
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 943.12
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 801.34
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 892.95
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 891.49
Matrix Spike (P0C0497-MS1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
1,2,4-Trichlorobenzene mg/kg dry1.68 0.86 2.165 BRL 34-11878
1,2-Dichlorobenzene mg/kg dry1.60 0.86 2.165 BRL 33-11774
1,3-Dichlorobenzene mg/kg dry1.59 0.86 2.165 BRL 30-11574
1,4-Dichlorobenzene mg/kg dry1.57 0.43 2.165 BRL 31-11573
1-Methylnaphthalene mg/kg dry1.89 0.86 2.165 BRL 40-11987
2,4,5-Trichlorophenol mg/kg dry1.77 0.86 2.165 BRL 45-12182
2,4,6-Trichlorophenol mg/kg dry1.82 0.86 2.165 BRL 39-12684
2,4-Dichlorophenol mg/kg dry1.77 0.86 2.165 BRL 40-12282
2,4-Dimethylphenol mg/kg dry2.22 0.43 2.165 BRL 30-127103
2,4-Dinitrophenol mg/kg dry1.07 1.9 2.165 BRL J27-12949
2,4-Dinitrotoluene mg/kg dry1.85 0.86 2.165 BRL 48-12685
2,6-Dinitrotoluene mg/kg dry1.88 0.86 2.165 BRL 46-12487
2-Chloronaphthalene mg/kg dry1.77 0.86 2.165 BRL 41-11482
2-Chlorophenol mg/kg dry1.83 0.86 2.165 BRL 34-12185
2-Methylnaphthalene mg/kg dry1.77 0.86 2.165 BRL 38-12282
2-Methylphenol mg/kg dry1.84 0.86 2.165 BRL 32-12285
2-Nitrophenol mg/kg dry1.78 0.86 2.165 BRL 36-12382
3,3’-Dichlorobenzidine mg/kg dry1.79 0.86 2.165 BRL 22-12183
3/4-Methylphenol mg/kg dry1.67 0.86 2.165 BRL 34-11977
4,6-Dinitro-2-methylphenol mg/kg dry1.69 1.9 2.165 BRL J29-13278
4-Bromophenyl phenyl ether mg/kg dry1.84 0.86 2.165 BRL 46-12485
4-Chloro-3-methylphenol mg/kg dry1.80 0.86 2.165 BRL 45-12283
4-Chloroaniline mg/kg dry1.73 0.43 2.165 BRL 17-10680
4-Chlorophenyl phenyl ether mg/kg dry1.75 1.3 2.165 BRL 45-12181
4-Nitrophenol mg/kg dry1.82 0.86 2.165 BRL 30-13284
Acenaphthene mg/kg dry1.88 0.86 2.165 BRL 40-12387
Acenaphthylene mg/kg dry1.95 0.86 2.165 BRL 32-13290
Anthracene mg/kg dry1.91 0.86 2.165 BRL 47-12388
Azobenzene mg/kg dry2.01 0.86 2.165 BRL 39-12593
Benzo(a)anthracene mg/kg dry1.76 0.86 2.165 BRL 49-12681
Benzo(a)pyrene mg/kg dry1.91 0.86 2.165 BRL 45-12988
Benzo(b)fluoranthene mg/kg dry1.89 0.86 2.165 BRL 45-13287
Benzo(g,h,i)perylene mg/kg dry1.82 0.86 2.165 BRL 43-13484
Benzo(k)fluoranthene mg/kg dry1.81 0.86 2.165 BRL 47-13284
Benzoic Acid mg/kg dryBRL2.6 2.165 BRL M10-83
Benzyl alcohol mg/kg dry1.82 0.86 2.165 BRL 29-12284
bis(2-Chloroethoxy)methane mg/kg dry1.63 0.86 2.165 BRL 36-12175
Bis(2-Chloroethyl)ether mg/kg dry1.60 0.86 2.165 BRL 31-12074
Bis(2-chloroisopropyl)ether mg/kg dry1.55 0.43 2.165 BRL 33-13171
Bis(2-Ethylhexyl)phthalate mg/kg dry1.87 0.86 2.165 BRL 51-13387
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
Matrix Spike (P0C0497-MS1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
Butyl benzyl phthalate mg/kg dry1.85 0.43 2.165 BRL 48-13286
Chrysene mg/kg dry1.77 0.86 2.165 BRL 50-12482
Dibenzo(a,h)anthracene mg/kg dry0.819 0.86 2.165 BRL M, J45-13438
Dibenzofuran mg/kg dry1.76 0.86 2.165 BRL 44-12081
Diethyl phthalate mg/kg dry1.74 0.86 2.165 BRL 50-12481
Dimethyl phthalate mg/kg dry1.75 0.86 2.165 BRL 48-12481
Di-n-butyl phthalate mg/kg dry1.97 0.86 2.165 BRL 51-12891
Di-n-octyl phthalate mg/kg dry1.93 0.43 2.165 BRL 45-14089
Fluoranthene mg/kg dry1.88 0.86 2.165 BRL 50-12787
Fluorene mg/kg dry1.82 0.86 2.165 BRL 43-12584
Hexachlorobenzene mg/kg dry1.82 0.86 2.165 BRL 45-12284
Hexachlorobutadiene mg/kg dry1.78 0.86 2.165 BRL 32-12382
Hexachlorocyclopentadiene mg/kg dry1.57 0.86 2.165 BRL 32-11773
Hexachloroethane mg/kg dry1.49 0.86 2.165 BRL 28-11769
Indeno(1,2,3-cd)pyrene mg/kg dry1.67 0.86 2.165 BRL 45-13377
Isophorone mg/kg dry1.43 0.86 2.165 BRL 30-12266
Naphthalene mg/kg dry1.68 0.86 2.165 BRL 35-12377
Nitrobenzene mg/kg dry1.52 0.43 2.165 BRL 34-12270
N-Nitroso-di-n-propylamine mg/kg dry1.75 0.86 2.165 BRL 36-12081
N-Nitrosodiphenylamine mg/kg dry2.30 0.86 2.165 BRL 38-127106
Pentachlorophenol mg/kg dry1.83 1.3 2.165 BRL 25-13385
Phenanthrene mg/kg dry1.87 0.86 2.165 BRL 50-12186
Phenol mg/kg dry1.91 0.86 2.165 BRL 34-12188
Pyrene mg/kg dry1.93 0.86 2.165 BRL 47-12789
Pyridine mg/kg dry1.12 0.43 2.165 BRL 20-15052
mg/kg dry 4.330 39-132Surrogate: 2,4,6-Tribromophenol 833.59
mg/kg dry 2.165 44-115Surrogate: 2-Fluorobiphenyl 781.68
mg/kg dry 4.330 35-115Surrogate: 2-Fluorophenol 813.49
mg/kg dry 2.165 37-122Surrogate: Nitrobenzene-d5 721.56
mg/kg dry 4.330 34-121Surrogate: Phenol-d5 793.43
mg/kg dry 2.165 54-127Surrogate: Terphenyl-d14 801.74
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
Matrix Spike Dup (P0C0497-MSD1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
1,2,4-Trichlorobenzene mg/kg dry1.46 0.86 2.163 BRL 2034-11867 14
1,2-Dichlorobenzene mg/kg dry1.36 0.86 2.163 BRL 2033-11763 16
1,3-Dichlorobenzene mg/kg dry1.34 0.86 2.163 BRL 2030-11562 18
1,4-Dichlorobenzene mg/kg dry1.34 0.43 2.163 BRL 2031-11562 16
1-Methylnaphthalene mg/kg dry1.63 0.86 2.163 BRL 2040-11975 15
2,4,5-Trichlorophenol mg/kg dry1.57 0.86 2.163 BRL 3545-12172 12
2,4,6-Trichlorophenol mg/kg dry1.65 0.86 2.163 BRL 2039-12676 10
2,4-Dichlorophenol mg/kg dry1.53 0.86 2.163 BRL 2040-12271 15
2,4-Dimethylphenol mg/kg dry1.94 0.43 2.163 BRL 2030-12790 14
2,4-Dinitrophenol mg/kg dry0.844 1.9 2.163 BRL 20 D, J27-12939 23
2,4-Dinitrotoluene mg/kg dry1.63 0.86 2.163 BRL 2048-12675 12
2,6-Dinitrotoluene mg/kg dry1.71 0.86 2.163 BRL 2046-12479 9
2-Chloronaphthalene mg/kg dry1.57 0.86 2.163 BRL 2041-11473 12
2-Chlorophenol mg/kg dry1.56 0.86 2.163 BRL 2034-12172 16
2-Methylnaphthalene mg/kg dry1.57 0.86 2.163 BRL 2038-12273 12
2-Methylphenol mg/kg dry1.65 0.86 2.163 BRL 2032-12276 11
2-Nitrophenol mg/kg dry1.47 0.86 2.163 BRL 2036-12368 19
3,3’-Dichlorobenzidine mg/kg dry1.63 0.86 2.163 BRL 2022-12175 9
3/4-Methylphenol mg/kg dry1.43 0.86 2.163 BRL 2034-11966 15
4,6-Dinitro-2-methylphenol mg/kg dry1.41 1.9 2.163 BRL 20 J29-13265 18
4-Bromophenyl phenyl ether mg/kg dry1.67 0.86 2.163 BRL 2046-12477 10
4-Chloro-3-methylphenol mg/kg dry1.58 0.86 2.163 BRL 2045-12273 13
4-Chloroaniline mg/kg dry1.52 0.43 2.163 BRL 2017-10671 13
4-Chlorophenyl phenyl ether mg/kg dry1.54 1.3 2.163 BRL 2045-12171 12
4-Nitrophenol mg/kg dry1.56 0.86 2.163 BRL 2030-13272 16
Acenaphthene mg/kg dry1.66 0.86 2.163 BRL 2040-12377 13
Acenaphthylene mg/kg dry1.75 0.86 2.163 BRL 2032-13281 11
Anthracene mg/kg dry1.76 0.86 2.163 BRL 2047-12381 8
Azobenzene mg/kg dry1.82 0.86 2.163 BRL 2039-12584 10
Benzo(a)anthracene mg/kg dry1.56 0.86 2.163 BRL 2049-12672 12
Benzo(a)pyrene mg/kg dry1.71 0.86 2.163 BRL 2045-12979 11
Benzo(b)fluoranthene mg/kg dry1.69 0.86 2.163 BRL 2045-13278 12
Benzo(g,h,i)perylene mg/kg dry1.63 0.86 2.163 BRL 2043-13475 11
Benzo(k)fluoranthene mg/kg dry1.61 0.86 2.163 BRL 2047-13275 12
Benzoic Acid mg/kg dryBRL2.6 2.163 BRL 20 M10-83
Benzyl alcohol mg/kg dry1.58 0.86 2.163 BRL 2029-12273 14
bis(2-Chloroethoxy)methane mg/kg dry1.45 0.86 2.163 BRL 2036-12167 12
Bis(2-Chloroethyl)ether mg/kg dry1.16 0.86 2.163 BRL 20 D31-12054 32
Bis(2-chloroisopropyl)ether mg/kg dry1.39 0.43 2.163 BRL 2033-13164 10
Bis(2-Ethylhexyl)phthalate mg/kg dry1.69 0.86 2.163 BRL 2051-13378 10
Butyl benzyl phthalate mg/kg dry1.64 0.43 2.163 BRL 2048-13276 12
Chrysene mg/kg dry1.56 0.86 2.163 BRL 2050-12472 13
Dibenzo(a,h)anthracene mg/kg dry0.751 0.86 2.163 BRL 20 M, J45-13435 9
Dibenzofuran mg/kg dry1.58 0.86 2.163 BRL 2044-12073 11
Diethyl phthalate mg/kg dry1.53 0.86 2.163 BRL 2050-12471 13
Dimethyl phthalate mg/kg dry1.57 0.86 2.163 BRL 2048-12473 11
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0C0497 - 3546
Matrix Spike Dup (P0C0497-MSD1)Prepared & Analyzed: 03/25/20 Source: 0030321-01
Di-n-butyl phthalate mg/kg dry1.79 0.86 2.163 BRL 2051-12883 10
Di-n-octyl phthalate mg/kg dry1.70 0.43 2.163 BRL 2045-14079 13
Fluoranthene mg/kg dry1.73 0.86 2.163 BRL 2050-12780 8
Fluorene mg/kg dry1.62 0.86 2.163 BRL 2043-12575 11
Hexachlorobenzene mg/kg dry1.66 0.86 2.163 BRL 2045-12277 9
Hexachlorobutadiene mg/kg dry1.52 0.86 2.163 BRL 2032-12370 16
Hexachlorocyclopentadiene mg/kg dry1.41 0.86 2.163 BRL 2032-11765 11
Hexachloroethane mg/kg dry1.23 0.86 2.163 BRL 2028-11757 19
Indeno(1,2,3-cd)pyrene mg/kg dry1.51 0.86 2.163 BRL 2045-13370 10
Isophorone mg/kg dry1.23 0.86 2.163 BRL 2030-12257 15
Naphthalene mg/kg dry1.47 0.86 2.163 BRL 2035-12368 13
Nitrobenzene mg/kg dry1.28 0.43 2.163 BRL 2034-12259 17
N-Nitroso-di-n-propylamine mg/kg dry1.54 0.86 2.163 BRL 2036-12071 13
N-Nitrosodiphenylamine mg/kg dry2.07 0.86 2.163 BRL 2038-12796 11
Pentachlorophenol mg/kg dry1.57 1.3 2.163 BRL 2025-13373 15
Phenanthrene mg/kg dry1.70 0.86 2.163 BRL 2050-12178 10
Phenol mg/kg dry1.55 0.86 2.163 BRL 20 D34-12172 21
Pyrene mg/kg dry1.70 0.86 2.163 BRL 2047-12779 13
Pyridine mg/kg dry0.952 0.43 2.163 BRL 6020-15044 16
mg/kg dry 4.325 39-132Surrogate: 2,4,6-Tribromophenol 733.16
mg/kg dry 2.163 44-115Surrogate: 2-Fluorobiphenyl 691.49
mg/kg dry 4.325 35-115Surrogate: 2-Fluorophenol 703.02
mg/kg dry 2.163 37-122Surrogate: Nitrobenzene-d5 611.31
mg/kg dry 4.325 34-121Surrogate: Phenol-d5 662.88
mg/kg dry 2.163 54-127Surrogate: Terphenyl-d14 711.54
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P0C0526 - MADEP VPH (S)
Blank (P0C0526-BLK1)Prepared & Analyzed: 03/26/20
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)999880
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)10710700
LCS (P0C0526-BS1)Prepared & Analyzed: 03/26/20
C5-C8 Aliphatics mg/kg wet34.4 5.0 32.00 70-130107
C9-C10 Aromatics mg/kg wet8.54 5.0 10.67 70-13080
C9-C12 Aliphatic mg/kg wet31.3 5.0 32.00 70-13098
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)919100
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)10110100
LCS Dup (P0C0526-BSD1)Prepared & Analyzed: 03/26/20
C5-C8 Aliphatics mg/kg wet35.1 5.0 32.00 5070-130110 2
C9-C10 Aromatics mg/kg wet8.82 5.0 10.67 5070-13083 3
C9-C12 Aliphatic mg/kg wet32.4 5.0 32.00 5070-130101 4
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)929230
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)10210200
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P0C0495 - 3546
Blank (P0C0495-BLK1)Prepared & Analyzed: 03/25/20
C9-C18 Aliphatics mg/kg wetBRL25
C19-C36 Aliphatics mg/kg wetBRL25
C11-C22 Aromatics mg/kg wetBRL25
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 721.45
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 741.47
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 722.88
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 753.01
LCS (P0C0495-BS1)Prepared & Analyzed: 03/25/20
C9-C18 Aliphatics mg/kg wet85.0 25 120.0 40-14071
C19-C36 Aliphatics mg/kg wet15025 160.0 40-14094
C11-C22 Aromatics mg/kg wet14825 170.0 40-14087
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 861.72
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 851.69
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 753.01
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 632.53
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 41
3/31/20
Level II QC Report
165 Knoll Dr.
Project: VannoyKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Work Order: 0030321
Time Submitted: 3/24/2020 10:45:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P0C0507 - Solids, Dry Weight
Duplicate (P0C0507-DUP1)Prepared: 03/25/20 Analyzed: 03/26/20 Source: 0030321-02
% Solids % by Weight80.8 0.100 79.1 202
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 41
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P0C04950030321-01 03/25/20 11:5010.02 2g mL
P0C04950030321-02 03/25/20 11:5010.25 2g mL
P0C04950030321-03 03/25/20 11:5010.03 2g mL
P0C04950030321-04 03/25/20 11:5010.27 2g mL
P0C04950030321-05 03/25/20 11:5010.22 2g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P0C05070030321-01 03/25/20 14:503030gg
P0C05070030321-02 03/25/20 14:503030gg
P0C05070030321-03 03/25/20 14:503030gg
P0C05070030321-04 03/25/20 14:503030gg
P0C05070030321-05 03/25/20 14:503030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P0C04970030321-01 03/25/20 11:4530.07 1g mL
P0C04970030321-02 03/25/20 11:4530.06 1g mL
P0C04970030321-03 03/25/20 11:4530.05 1g mL
P0C04970030321-04 03/25/20 11:4530.09 1g mL
P0C04970030321-05 03/25/20 11:4530.03 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P0C04940030321-01 03/25/20 8:145.2 5g mL
P0C04940030321-02 03/25/20 8:144.88 5g mL
P0C04940030321-03 03/25/20 8:144.71 5g mL
P0C04940030321-04 03/25/20 8:144.83 5g mL
P0C04940030321-05 03/25/20 8:145.32 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P0C05260030321-01 03/26/20 13:574.91 16g mL
P0C05260030321-02 03/26/20 13:574.71 16g mL
P0C05260030321-03 03/26/20 13:575.11 16g mL
P0C05260030321-04 03/26/20 13:575.16 16g mL
P0C05260030321-05 03/26/20 13:574.99 16g mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 41

Appendix C
Standard Operating Procedures
A safety meeting was conducted prior to commencing the closure work. The atmosphere in the USTs was checked for explosive vapors with an Explosimeter. The Lower Explosive Limit (LEL) readings for the gasoline USTs were below 10%. The tanks were cleaned using a pressure washer to remove residual fuel and fumes.
Soil samples from the excavations were collected out of the trackhoe bucket. Dispenser sampling was completed
with decontaminated steel spoons. Product line sampling was completed with decontaminated hand auger buckets. The hand auger buckets and steel spoons were decontaminated with non-phosphate detergent and distilled water and
isopropanol rinses.
Soil samples collected for laboratory analysis were placed in laboratory sample jars with Teflon-lined lids, chilled and Chain-of-Custody records were initiated. Initial closure soil samples were transported to REDLab, LLC in Charlotte, North Carolina for analyses. Post-excavation confirmation soil samples were transported to Waypoint Analytical in Charlotte, North Carolina for analyses. A new pair of disposable Nitrile gloves was worn while
collecting each sample. The depth and horizontal locations of the soil samples were identified either by measuring with a fiberglass tape, estimating right angles and referencing site features or with the use of a total station.

Appendix D
Disposal Manifests