WS-10167_45316_CA_LSA_20230214

LIMITED SITE ASSESSMENT

SANDY CROSS MINI MART-C
2078 NC-49 North
Burlington, Alamance County, NC 27217
Facility ID #: 00-0-0000024196; UST Incident #: 45316
LATITUDE: N 36.138515o; LONGITUDE: W -79.345175o (From GPS)
FEBRUARY 14, 2023
UST OWNER:
F. Fanous Group Inc., 2073 N NC Highway 49, Burlington, NC 27217
Phone Number: [phone]
PROPERTY OWNER/OCCUPANT:
F. Fanous Group Inc., 2073 N NC Highway 49, Burlington, NC 27217
CONSULTANT: Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405 Phone Number: [phone]
LABORATORY: Pace Analytical Services, Inc., 9800 Kincey Ave, Suite 100, Huntersville, NC 28078 Phone Number: [phone]; State Certification #12
RELEASE INFORMATION: Date Discovered: 12/10/19 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release: UST System Size and Contents: (1) 4,000 Gallon + (2) 6,000 Gallon Gasoline USTs; (1) 8,000 Gallon and (1) 1,000 Gallon Diesel USTs; (1) 550 Gallon Kerosene UST
The Limited Site Assessment Report for this site has been prepared by Henry Nemargut Engineering Services (sole proprietorship) under the direct supervision of a licensed engineer. I certify that the information contained in this report is correct and accurate to the best of my knowledge:
Henry Nemargut, P.E. North Carolina License #17669

February 14, 2023

Mr. Ossama Touma
F. Fanous Group, Inc.
3427 Silverlake Courtest
Jamestown, NC 27282

Reference: Limited Site Assessment Report
Sandy Cross Mini Mart-C
2078 NC-49 North
Burlington, Alamance County, North Carolina 27215
Facility ID#: 00-0-0000024196; Incident #45316

Dear Mr. Touma:
In accordance with the requirements of the Guidelines of the North Carolina Department of Environmental Quality (NCDEQ), contained herein is a Limited Site Assessment Report for the release which occurred at the above referenced facility. These activities have been conducted following the release of petroleum which occurred in the vicinity of a (6) underground storage tanks (USTs). All activities were conducted in accordance with NCDEQ guidelines and the requirements of 15A NCAC 2N.

Mr. Touma, if you have questions regarding this report please contact my office.

Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

TABLE OF CONTENTS

Page

1.0 Site History, Source Characterization & Initial Abatement 1

2.0 Risk Characterization 1

3.0 Receptor Information 5

4.0 Site Geology and Soil Assessment 6

5.0 Groundwater Investigation 8

6.0 Conclusions and Recommendations 9

LIST OF FIGURES

Figure 1: Project Location/U.S.G.S. Topographic Map
Figure 2: Site Layout and Former UST Locations
Figure 3: Subsurface Utilities Map
Figure 4: Adjacent Properties Map
Figure 5: Receptor Map
Figure 6: Site Layout, Soil Sample Locations & Soil Contaminant Maps
Figure 7: Site Layout and Monitor Well Locations
Figure 8: Benzene Concentration Map

LIST OF TABLES

Table 1: Site History
Table 2: Adjacent Property Owners
Table 3: Supply Well Information
Table 4: Laboratory Analytical Results –Risk Based Soil Samples
Table 5: Laboratory Analytical Results – Water Samples

APPENDICES

Appendix A: Laboratory Analytical Laboratory Results
Appendix B: Well Construction Records
Page - 1
LIMITED SITE ASSESSMENT
Sandy Cross Mini Mart-C
2078 NC-49 North, Burlington, North Carolina
Facility ID#: 00-0-0000024196; GW Incident #: 45316

1.0 - SITE HISTORY, SOURCE CHARACTERIZATION & INITIAL ABATEMENT

F. Fanous Group, Inc. owned USTs which are operated at the Sandy Cross Mini Mart
facility located at 2078 NC-49 North in Burlington, North Carolina. Figure 1 illustrates
the location of this facility on the Burlington NE Quadrangle U.S.G.S. Topo Map. This
property contains 1 permanent structure which is currently vacant. The site last
contained (2) 6,000 gallon + (1) 4,000 gallon gasoline USTs; (1) 550 gallon kerosene
UST, and (1) 8,000 gallon diesel USTs which were last in use at this facility in July,
2018. On December 10, 2019, these 5 USTs were closed at this facility. Figure 2
illustrates the overall layout of this site and the locations of the USTs closed at the site in
2019. At least 2 USTs were formerly in use at this site dating back to prior to 1986. A
release was noted during UST closure activities for these USTs conducted on 3/25/1986
(Incident #3199). Table 1 summarizes the UST history for the site.

A release from the latest UST system was confirmed on 12/10/2020 and reported to on-
site NCDEQ personnel based on the presence of free product beneath the T4/T5 USTs
(Incident #45316). This release was confirmed upon receipt of analytical results from
soil samples collected during the tank closure and abatement activities. The site and
adjacent properties are used for residential and commercial purposes. Municipal water
supplies are available to most properties within 1,500’; however, private potable supply
wells are in use within 1,500’.

A Limited Site Assessment (LSA) has been conducted in response to this release in order
to classify the risk of the site for the release source originating at the USTs owned by F.
Fanous Group Inc. The findings of the LSA conducted for this site are contained herein.

2.0 - RISK CHARACTERIZATION AND LAND USE FORM

Part I Groundwater/Surface water/Vapor impact
Low Risk

1. Has discharge or release contaminated any water supply wells including any used
for non-drinking purposes?

NO

2. Is a water supply well used for drinking water located within 1,000 feet of the
source area the discharge or release?

YES
Page - 2

3. Is a water supply well used for any purpose (e.g., irrigation, washing cars,
industrial cooling water, filling swimming pools) located within 250 feet of the
source area of the discharge or release?

NO

4. Does groundwater within 500 feet of the source area of the discharge or release
have the potential for future use in that there is no other source of water supply
other than the groundwater?

NO

5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space or pose any other serious threat to
public health, public safety or the environment?

NO

6. Are there any factors that would cause the discharge or release to pose an
imminent danger to public health, public safety or the environment?

NO

Intermediate Risk

7. Is a surface body located within 500 feet of the source area of the discharge or
release?

NO

If yes, does the maximum groundwater contaminant concentration exceed the
surface water quality standards and criteria found in 15A NCAC 2B .0200 by a
factor of 10?

N/A

8. Is the source area of the discharge or release located within a designated wellhead
protection area as defined in 42 USC 300h-7(e)?

NO

9. Is the discharge or release located in the Coastal Plain physiographic region as
designated on a map entitled "Geology of North Carolina" published by the
Department in 1985?
Page - 3

NO

If yes, is the source area of the discharge or release located in an area in which
there is recharge to an unconfined or semi-confined deeper aquifer that is being
used or may be used as a source of drinking water?

N/A

10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 7 in guidelines) by the department?

NO

Part II-Land Use

Property containing Source Area of Discharge or Release

The questions below pertain to the property containing the source area of the release.

1. Does the property contain one or more primary or secondary residences
(permanent or temporary)?

NO

2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly?

NO

3. Does the property contain a commercial (e.g., retail, warehouse, office/business
space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and
development, chemical/petroleum bulk storage, etc.) enterprise, an inactive
commercial or industrial enterprise, or is the land undeveloped?

YES

4. Do children visit the property?

NO

Explain.

THE FACILITY IS CLOSED AND VACANT

Page - 4
5. Is access to the property reliably restricted consistent with its use?

YES

6. Do pavement, buildings, or other structures cap the contaminated soil?

NO

If yes, what mechanisms are in place or can be put into place to insure that the
contaminated soil will remain capped in the foreseeable future?

N/A

7. What is the zoning status of the property?

COMMERCIAL RETAIL

8. Is the use of the property likely to change in the next 20 years?

NO

Property Surrounding Source Area of Discharge or Release.

9. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?

220’

10. What is the distance from the source area of the release to the nearest school,
daycare center, hospital, playground, park, recreation area, church, nursing home,
or other place of public assembly?

THERE ARE NO PLACES OF ASSEMBLY WITHIN 1500’ OF THE SITE.

11. What is the zoning status of properties in the surrounding areas?

COMMERCIAL MULTI-USE, FARM & RESIDENTIAL

12. Briefly characterize the use and activities of the land in the surrounding area.

COMMERCIAL MULTI-USE, FARM & RESIDENTIAL

3.0 - RECEPTOR INFORMATION

Page - 5
3.1 Water Supply Wells

A supply well survey has been conducted within a 1,500' radius of the release area. This
survey was performed by interviews conducted with owners and occupants of properties
located within 1,500’ of the release sources. During this reconnaissance (2) water supply
wells (potable) were found to be located within a 1,000’ radius. The out-of-service on-
site former water supply well is located within 180’ from the UST release source area.
An in-use supply well owned and operated by John David Bruner is located 465’ from
the UST source area and is the closest potable water supply well. An additional water
supply well is believed to be located 520’ from the source area on a property owned by
Kimery Rudd Braxton. The house on the property is located > 1000’ from the release
source and is occupied; however, attempts to contact the site occupant have been un-
successful. Table 3 lists information for the wells identified during this investigation.
Figure 5 depicts the approximate locations of these wells on a Google Earth Aerial map.

3.2 Public Water Supplies

Public water supplies are available to all properties along NC Highway 49 and annexed
properties to the east of NC Highway 49; however, properties within 1,500’ of the release
site along Sandy Cross Road do not yet have access to municipal water supply.

3.3 Surface Water

The partial Burlington NE Quadrangle U.S.G.S. Topographic Map included as Figure 1
indicates that the release site is located atop a ridge at an approximate elevation of 655’
amsl. Surface waters in the vicinity of the release area generally drain towards the
west/northwest towards the headwaters of Boyd’s Creek. Boyd’s Creek empties into the
Haw River which lies within the Cape Fear River Basin.

3.4 Wellhead Protection Areas

No wellhead protection areas are known to exist within the area of this release.

3.5 Deep Aquifers in the Coastal Plain Physiographic Region

This release is not located in the coastal plain.

3.6 Subsurface Structures

Subsurface lines/structures are not present within the petroleum affected area at this site.
Subsurface utilities are present in the form of water, communication, & storm drain lines.
Underground utility lines are mostly located on the east side of NC Hwy 49 and along the
southern side of Sandy Cross Road, outside of the impacted areas within the property
boundaries. Figure 3 illustrates the locations of subsurface utilities near the subject
property.

Page - 6
3.7 Land Use

The possibility of human exposure to soil contamination at 2078 NC-49 North site is
minimal. Petroleum impacted soils identified at the site are predominantly located > 2’
from surface. Contamination at this facility lies within a commercial site.

3.8 Property Owners and Occupants

Figure 4 illustrates the surrounding properties, and Table 2 contains information
regarding the adjacent property owners. This information was obtained from Alamance
County Tax records.

4.0 - SITE GEOLOGY AND SOIL INVESTIGATION

4.1 Site Geology

The site is situated in the Carolina Slate Belt. According to the Geological Map of North
Carolina local geology of the region is underlain with metamorphosed granitic rock.
Weathered bedrock was encountered at a depth of 12’ below surface in diesel UST basin
area monitoring well MW-13. Competent bedrock was encountered in the gasoline UST
source area monitoring well MW-14 boring at a depth of 11’ feet below surface.

4.2 Soils Investigation

The soils at the project site consist of silt with varying clay, sand and weathered rock
content. Soil boring logs are contained on well construction records included as
Appendix B.

Soil samples were collected from the perimeter of the UST remedial excavation to obtain
risk-based analytical data for the site following IAA excavation. The wall soil samples
collected from the perimeter of the T4/T5 remedial excavation were submitted to Pace
Analytical, Inc. for analyses by EPA Methods 8260 and MADEP Methods for VPH, as
appropriate based on tank contents. Laboratory results from the UST wall samples
indicate that contamination at this site exceeds NCDEQ Lowest Maximum Soil
Contaminant Concentrations (MSCCs) for 9 compounds/compound groups; however, no
compounds were detected at levels above Residential MSCCs. Figure 6 illustrates the
locations of the post remedial excavation soil samples collected at the subject site. The
soil samples were obtained as specified in the collection, preservation, and handling
section of the specific method. Each container was labeled with sample location,
analyses to be performed, time, date, and the sampler's name. They were then placed in a
cooler and chilled with ice to approximately 4oC in preparation for transportation to the
analytical laboratory utilizing EPA approved chain of custody procedures. Additional
samples from each pit wall were containerized for possible analyses via risk-based
methods.

Page - 7
On January 18, 2023 during installation of LSA monitoring wells MW-13 and MW-14,
additional borings were placed to collect soil samples at piping and dispenser areas
indicating elevated TPH contaminant concentrations. Gasoline UST system samples
were labeled GP1 and GD1, with kerosene dispenser area soil sample labeled KD, and
were submitted to Pace Analytical, Inc. for analyses by EPA Method 8260/8270 and
MADEP Methods for VPH/EPH, as appropriate based on tank/piping contents. The soil
samples were obtained as specified in the collection, preservation, and handling section
of the specific method. Each container was labeled with sample location, analyses to be
performed, time, date, and the sampler's name. They were then placed in a cooler and
chilled with ice to approximately 4oC in preparation for transportation to the analytical
laboratory utilizing EPA approved chain of custody procedures.

Laboratory results from the LSA soil samples indicate that contamination at this site
exceeds NCDEQ Lowest Maximum Soil Contaminant Concentrations (MSCCs) for 8
compounds/compound groups. C9-C22 aromatics were detected in gasoline dispenser
sample GD1 at a level above Residential MSCCs. Figure 6 illustrates the locations of the
risk-based soil samples collected at the subject site, and Table 4 summarizes the
laboratory results for the “Risk-Based” soil samples from 2078 NC-49 North in
Burlington, NC. A copy of the soil analytical report and the chain of custody records for
the risk-based soil samples collected at 2078 NC-49 North during UST closure is
contained in the previously submitted IAA report. Soil analytical results from LSA soil
samples are contained in Appendix A.

5.0 – GROUNDWATER INVESTIGATION

5.1 Monitoring Well Installation

A total of (2) North Carolina Type II groundwater monitoring wells was installed on-site
to complete LSA activities. Per discussion with Mindy Lepard of the Winston Salem
Regional Office, (2) source area monitoring wells were installed during LSA activities,
since previously installed monitoring well MW-3 was located within 10’ of the GD1
source area. Figure 7 illustrates the locations of the new monitor wells, denoted as MW-
13 and MW-14 which were installed to complete LSA activities. The monitoring wells
installed at the site were constructed of 2-inch Schedule 40 PVC pipe with 3’-4’ feet of
casing and 8’-10’ of 0.010 inch slotted screen. Based on the assumption that the
contaminants being addressed were primarily hydrocarbon constituents with specific
gravities of less than 1.0, the Type II monitoring wells were installed so that the screened
interval intersected the shallow groundwater table at the time of installation. Well
construction records for the monitor wells constructed at this site for LSA activities are
included in Appendix B.

Free product was not detected in any of the monitoring wells sampled at the site during
LSA activities conducted on January 18, 2023.

Page - 8
5.2 Monitor Well Sampling and Analyses

On January 18, 2023, source area monitor wells MW-3, MW-13 and MW-14 were
sampled for analyses utilizing EPA Methods 6200B, 625 + 10 peaks, Lead, and MADEP
Methods for VPH/EPH as appropriate based on UST system contents. Before sampling,
the monitor wells were developed and purged using disposable balers. Following
development of the groundwater monitoring well, samples were obtained from the
disposable balers. The supply well was also sampled with a disposable baler. All
samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results from the monitoring well network installed at the site
indicate the presence of 16 compounds/compound groups above 15 NCAC 2L Standards.
Benzene was noted at a concentration of 2,030 ug/l in MW-3, above its 2L Standard of 1
ug/l and above its GCL Standards of 5,000 ug/l. C5-C8 Aliphatics were noted at a
concentration of 26,000 ug/l in MW-3 above their 2L Standard of 400 ug/l. No
compounds were detected at levels above GCLs. Table 5 summarizes the laboratory
analytical results for the groundwater samples collected for LSA Activities. Appendix A
contains a copy of the laboratory analytical report and chain of custody record for the
groundwater samples collected during LSA activities at this site.

6.0 - CONCLUSIONS AND RECOMMENDATIONS

6.1 General Summary

Limited Site Assessment activities at 2078 NC-49 North have been completed. From a
review of all information gathered during this project, Henry Nemargut Engineering
Services makes the following conclusions:

o A well reconnaissance of the site was performed which identified (2) potable
wells within 1,000’ of the release source area. An in-use supply well owned and
operated by John David Bruner is located 465’ from the UST source area and is
the closest potable water supply well. An additional water supply well is believed
to be located 520’ from the source area on a property owned by Kimery Rudd
Braxton. The house on the property is located > 1000’ from the release source
and is occupied; however, attempts to contact the site occupant have been un-
successful. Municipal water supplies are not available to any properties within
1500’ of this site.

Page - 9
o Public water supplies are available to all properties along NC Highway 49 and
annexed properties to the east of NC Highway 49; however, properties within
1,500’ of the release site along Sandy Cross Road do not yet have access to
municipal water supply.

o Results from the risk-based samples obtained during IAA/LSA activities were
above current NCDEQ lowest MSCCs for 9 compounds/compound groups for
samples collected in the former UST remedial excavation and former dispenser
locations. C9-C22 aromatics were detected in gasoline dispenser sample GD1 at
a level above Residential MSCCs.

o Per discussion with Mindy Lepard of the Winston Salem Regional Office, (2)
source area monitoring wells were installed during LSA activities, since
previously installed monitoring well MW-3 was located within 10’ of the GD1
source area. These wells were screened to intersect the top of the shallow water
table observed at the site. Free product was not detected in any of these
monitoring wells during a site check conducted on January 18, 2023.

o Laboratory analytical results from LSA monitoring well network indicate the
presence of 16 compounds/compound groups above 15 NCAC 2L Standards.
Benzene was noted at a concentration of 2,030 ug/l in MW-3, above its 2L
Standard of 1 ug/l and above its GCL Standards of 5,000 ug/l. C5-C8 Aliphatics
were noted at a concentration of 26,000 ug/l in MW-3 above their 2L Standard of
400 ug/l. No compounds were detected at levels above GCLs.

6.2 Recommendations

Based upon a review of all information gathered during this project, Henry Nemargut
Engineering Services makes the following recommendations:

o A site ranking should be assigned by the NCDEQ to determine the need for any
further action at this site.

o A copy of this report has been forwarded to the following address:

Ms. Mindy Lepard
NCDEQ – UST Section
450 West Hanes Mill Rd, Suite 300
Winston Salem, NC 27105-7407

Page - 10
6.3 Limitations

This report has been prepared for the exclusive use of F. Fanous Group Inc. for the
specific application to the referenced site located in Alamance County, North Carolina.
The evaluation was conducted based on the scope of work and level of effort desired by
the client and with resources adequate only for the scope of work. Our findings have
been developed in accordance with generally accepted standards for Limited Site
Assessments in the State of North Carolina, available information and our professional
judgment. No other warranty is expressed or implied.

The data presented in this report are indicative of conditions at the precise locations
sampled and the time the sample was collected. Additionally, the data obtained from the
samples would be interpreted as meaningful with respect to the parameters in the
laboratory reports. No additional information can be logically inferred from this data.

FIGURES
Alamance County
Alamance County GISAlamance County Tax Department
Heavy Industrial Development Applicants
APPLIED FOR PERMIT
PERMIT APPROVED
PERMIT RENEWED
UNDER CONSTRUCTION
February 13, 2023
0 0.04 0.080.02 mi
0 0.065 0.130.0325 km
1:2,400

µ
Sandy Cross Receptor
NCDEQ GW Incident #45316
Legend
900 ft
N➤➤N
Image © 2023 CNES / Airbus
Image © 2023 CNES / Airbus
Image © 2023 CNES / Airbus

TABLES
TABLE 1: SITE HISTORY

Sandy Cross Mini Mart, Facility ID# 0-024196; GW Incident #Pending
2078 NC-49 North, Burlington, NC 27215

Property Ownership:

F. Fanous Group Inc.
2073 N NC Highway 49, Burlington, NC 27217
6/4/2015 to Present
Previous Owner:
Sandy Cross MiniMart, Inc.

Tank owner:

F. Fanous Group Inc.
2073 N NC Highway 49, Burlington, NC 27217
6/4/2015 to Present

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents
A Unknown 1,000 3/25/86 Closed Gasoline
1 8/5/85 4,000 12/10/19 Closed Gasoline
2 8/5/85 1,000 5/30/96 Closed Diesel
2A 6/1/90 8,000 12/10/19 Closed Diesel
3 8/5/85 550 12/10/19 Closed Kerosene
4 1/1/84 6,000 12/10/19 Closed Gasoline
5 1/1/84 6,000 12/10/19 Closed Gasoline

TABLE 2: ADJACENT PROPERTY OWNERS
Sandy Cross Mini Mart
2078 N NC Highway 49
Burlington, NC 27215

MAP ID PARCEL ID OWNER INFORMATION

Project 155085 F. Fanous Group Inc.
Site 2073 N Highway 49
Burlington, NC 27217

1 155267 Bason Ella West Life Estate
3181 Bason Road
Mebane, NC 27302

2 154911 Martin Marietta Materials Inc.
c/o Baden Tax Management LLC
PO Box 8240
Fort Wayne, IN 46898-8040

3 154918 John David Bruner
2745 Sandy Cross Rd
Burlington, NC 27217

WellIdentification IW-0 SW-1 SW-2 IW-3Owner Name F. Fanous Group Inc. John David Bruner Kimery Rudd Braxton etal Cormic & Ana RoneOwner Address 2073 N NC Hwy 49 2745 Sandy Cross Road 3640 Russell Road 2041 N NC 49 HighwayBurlington, NC 27217 Burlington, NC 27217 Graham, NC 27253 Burlington, NC 27217Site Address 600 Cedar Point Blvd 2745 Sandy Cross Road 2664 Sandy Cross Rd 2041 N NC 49 Highway2078 N NC Hwy 49 Burlington, NC 27217 Burlington, NC 27217 Burlington, NC 27217OccupantUnoccupied 578-1592(H)/213-0511(M) Unknown - Occupied Cormic & Ana RoneParcel Number155085154918154728155083UseNot in usePotablePotable?Not in useDistance180'465'520'625'County Water?YESNO NO YesDepth of WellUnknownUnknownUnknownUnknownWell DiameterUnknownUnknownUnknownUnknownWell YieldUnknownUnknownUnknownUnknownDepth to Pump UnknownUnknownUnknownUnknownDepth of Casing UnknownUnknownUnknownUnknownStatic WaterUnknownUnknownUnknownUnknown2078 N NC Highway 49, Burlington, NC 27217TABLE 3SUPPLY WELL INFORMATION1,000' RADIUSSandy Cross Mini Mart
Sample LocationGP1 GD1 KDSoil/Water MSCC Residential MSCC Ind/Comm MSCCDate1/18/2023 1/18/2023 1/18/2023(note units) (note units) (note units)Sample depth3'3'3' Method 8260 (ug/kg)Benzene45.9 1010 12807.212,00059,400n-ButylbenzeneBDL BDL BDL2,400782,000 11,600,000sec-ButylbenzeneBDL BDL BDL2,200 1,560,000 23,300,000Ethylbenzene61303004438,00060,300297,000IsopropylbenzeneBDL BDL BDL1,300 1,560,000 23,300,000p-IsopropyltolueneBDL BDL BDL1201,560,000 23,300,000NaphthaleneBDL BDL BDL2005,50027,000Chloroform BDL BDL BDL34021,000105,000n-PropylbenzeneBDL BDL BDL1,400 1,560,000 23,300,000StyreneBDL BDL BDL9003,120,000 46,700,000Diisopropyl etherBDL BDL BDL320NSE2,330,000TolueneBDL 3770 34.25,400 1,250,000 18,600,0001,2,4-TrimethylbenzeneBDL BDL BDL6,600156,000 2,330,0001,3,5-TrimethylbenzeneBDL BDL BDL6,600156,000 2,330,0001,2 DichloroethaneBDL BDL BDL30116,000573,000MTBEBDL BDL85.585156,000 1,810,000sec-butylbenzeneBDL BDL BDL2,200 1,560,000 23,300,000Xylenes (total)16478,4002626,000 3,120,000 46,700,000Method 8270 (ug/kg)1-MethylnaphthaleneNRNR7225422,800112,0002-MethylnaphthaleneNR NR 9331,50062,500934,000PhenanthreneNR NR BDL644697,000NaphthaleneNR NR4322005,50027,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile AliphaticsBDL740166893924,528C9 - C12 Volatile AliphaticsBDL 440 39NSENSENSEC9-C18 Extractable Aliphatics BDL BDL 194NSENSENSEC9-C18 Aliphatics (total)0 440 2335401,50040,000C19-C36 Extractable AliphaticsNRNRNRNSE31,000810,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDL47041NSENSENSEC11 - C22 Extractable Aromatics BDL BDL 56.2NSENSENSEC9 - C22 Aromatics (total)047097.23146912264BDL = below detection limitsNR = analyses not requestedNSE = no standard establishedTABLE 4Laboratory Analytical Results - Risk Based Soil SamplesSandy Cross Mini Mart, 2078 N NC Highway 49, Burlington, NC 27217
Sample LocationT4N T4/5E T4/5W T5SSoil/Water MSCC Residential MSCC Ind/Comm MSCCDate12/10/2019 12/10/2019 12/10/2019 12/10/2019(note units) (note units) (note units)Sample depth6'6'6'6' Method 8260 (ug/kg)BenzeneBDL BDL BDL6,0107.212,00059,400n-ButylbenzeneBDL BDL 2,210 7202,400782,000 11,600,000sec-ButylbenzeneBDL BDL BDL BDL2,2001,560,000 23,300,000EthylbenzeneBDL 235,130 6,7108,00060,300297,000IsopropylbenzeneBDL BDL 1,070 6361,3001,560,000 23,300,000p-IsopropyltolueneBDL BDL BDL BDL1201,560,000 23,300,000NaphthaleneBDL BDL3,330 2,4402005,50027,000n-PropylbenzeneBDL 8.33,990BDL1,4001,560,000 23,300,000TolueneBDL 73.3 BDL7,0905,4001,250,000 18,600,0001,2,4-TrimethylbenzeneBDL 13.2 6,11014,0006,600156,000 2,330,0001,3,5-TrimethylbenzeneBDL BDL BDL 4,3906,600156,000 2,330,000MTBEBDL BDL BDL BDL85156,000 1,810,000sec-butylbenzeneBDL BDL BDL BDL2,2001,560,000 23,300,000Xylenes (total)BDL 21.2 4,22028,7006,0003,120,000 46,700,000Method 8270 (ug/kg)FluoreneNRNRNRNR47,00016,400,000620,000FluorantheneNR NR NR NR290,000 16,400,000 620,000PhenanthreneNR NR NR NR56,000 12,264,000 469,0001-MethylnaphthaleneNR NR NR NR4100,00020,0002-MethylnaphthaleneNR NR NR NR3,6001,635,00063,000NaphthaleneNR NR NR NR1608176000313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile AliphaticsBDL 3.4486 1126824,528939C9 - C12 Volatile Aliphatics17.5 12.4 262 187NSENSENSEC9-C18 Extractable Aliphatics NR NR NR NRNSENSENSEC9-C18 Aliphatics (total)17.5 12.4 262 18754040,0001,500C19-C36 Extractable AliphaticsNRNRNRNRNSE810,00031,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile Aromatics65.812088NSENSENSEC11 - C22 Extractable Aromatics NR NR NR NRNSENSENSEC9 - C22 Aromatics (total)6.35.812087.93112264469BDL = below detection limitsNR = analyses not requestedNSE = no standard establishedTABLE 4 (Continued)Laboratory Analytical Results - Risk Based Soil SamplesSandy Cross Mini Mart, 2078 NC-49, Burlington, NC 27215
Constituent MW-3 MW-13 MW-14 GCL 2L Standard
Date 1/18/2023 1/18/2023 1/18/2023
Standard Method 602 (ug/L)
Benzene 2030 BDL 211 5,000 1
Toluene 5090 BDL 31.5 260,000 600
Ethylbenzene 602 BDL 1180 84,500 600
Xylenes (total)5950 BDL 1468.5 85,500 500
Acetone BDL BDL BDL 6,000,000 6000
p-Isopropyltoluene BDL BDL BDL NSE NSE
Isopropylbenzene 28.3 BDL 73.5 25,000 70
Diisopropyl Ether (DIPE)108 BDL BDL 70,000 70
Naphthalene 380 BDL 394 6,000 6
n-propylbenzene 73.8 BDL 219 30,000 70
n-butylbenzene BDL BDL BDL 6,900 70
sec-butylbenzene BDL BDL BDL 8,500 70
Chlorobenzene BDL BDL BDL 50,000 50
1,4-Dichlorobenzene BDL BDL BDL 20,000 20
tert-Butyl Alcohol (TBA)3730 BDL 775 10,000 10
Methyl-tert-butyl-ether (MTBE)608 BDL 81.2 20,000 20
tert-Amyl Alcohol (TAA)6190 BDL 930 40,000 40
1,2,4-Trimethylbenzene 1470 BDL 177 28,500 400
1,3,5-Trimethylbenzene 808 BDL BDL 25,000 400
Total 6200B Compounds 27068.1 0 5540.7 NSE NSE
Method 625 (ug/L)
Phenol NR 65.3 NR 30,000 30
Naphthalene NR BDL NR 6,000 6
1-Methylnaphthalene NR BDL NR 1,000 1
2-Methylnaphthalene NR BDL NR 125,000 30
TOTAL TICs NR 3357.5 NR NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 26000 BDL 5200 NSE 400
C9-C12 Volatile Aliphatics BDL BDL BDL NSE NSE
C9-C18 Extractable Aliphatics NR BDL NR NSE 700
C9-C18 Aliphatics (total)0 0 0 NSE 700
C19-C36 Extractable Aliphatics NR BDL NR NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics 12000 BDL 4500 NSE NSE
C11-C22 Extractable Aromatics NR BDL NR NSE NSE
C9-C22 Aromatics (total)12,000 0 4,500 NSE 200
NR = Analyses Not Requested
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 5
SUMMARY OF GROUNDWATER ANALYTICAL RESULTSSandy Cross Mini Mart2078 N NC Highway 49, Burlington, NC 27217

APPENDIX A

LABORATORY ANALYTICAL RESULTS
#=CL#
February 06, 2023
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92647996
92647996
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
SANDY CROSS MINI MART
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on January 19, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 65
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 65
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Lab ID Sample ID Matrix Date Collected Date Received
92647996001 GP1 Solid 01/18/23 08:40 01/19/23 16:30
92647996002 GD1 Solid 01/18/23 09:30 01/19/23 16:30
92647996003 KD Solid 01/18/23 09:50 01/19/23 16:30
92647996004 MW3 Water 01/18/23 14:00 01/19/23 16:30
92647996005 MW13 Water 01/18/23 14:20 01/19/23 16:30
92647996006 MW14 Water 01/18/23 14:40 01/19/23 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 65
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92647996001 GP1 EPA 8260D 10 PASI-CSAS
SW-846 1 PASI-CKDF
92647996002 GD1 EPA 8260D 10 PASI-CSAS
SW-846 1 PASI-CKDF
92647996003 KD MADEP EPH 7 PASI-CBAJ
EPA 8270E 75 PASI-CBPJ
EPA 8260D 10 PASI-CSAS
SW-846 1 PASI-CKDF
92647996004 MW3 SM 6200B 69 PASI-CLMB
92647996005 MW13 MADEP EPH 7 PASI-CBAJ
EPA 625.1 68 PASI-CPKS
SM 6200B 66 PASI-CLMB
92647996006 MW14 SM 6200B 69 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 65
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92647996001 GP1
Benzene 45.9 ug/kg 01/24/23 00:2426.1EPA 8260D
Ethylbenzene 61.0 ug/kg 01/24/23 00:2426.1EPA 8260D
Xylene (Total)164 ug/kg 01/24/23 00:2452.1EPA 8260D
m&p-Xylene 124 ug/kg 01/24/23 00:2452.1EPA 8260D
o-Xylene 40.3 ug/kg 01/24/23 00:2426.1EPA 8260D
Percent Moisture 26.4 %01/20/23 17:09 N20.10SW-846
92647996002 GD1
Benzene 1010 ug/kg 01/25/23 01:1277.8EPA 8260D
Ethylbenzene 30300 ug/kg 01/25/23 01:1277.8EPA 8260D
Toluene 3770 ug/kg 01/25/23 01:1277.8EPA 8260D
Xylene (Total)78400 ug/kg 01/25/23 01:12156EPA 8260D
m&p-Xylene 73400 ug/kg 01/25/23 01:12156EPA 8260D
o-Xylene 5020 ug/kg 01/25/23 01:1277.8EPA 8260D
Percent Moisture 20.3 %01/20/23 17:09 N20.10SW-846
92647996003 KD
Aliphatic (C09-C18)194 mg/kg 01/26/23 11:01 N232.3MADEP EPH
Aromatic (C11-C22)56.2 mg/kg 01/25/23 19:05 N212.9MADEP EPH
1-Methylnaphthalene 722 ug/kg 01/26/23 10:21420EPA 8270E
2-Methylnaphthalene 933 ug/kg 01/26/23 10:21420EPA 8270E
Naphthalene 432 ug/kg 01/26/23 10:21420EPA 8270E
Benzene 1280 ug/kg 01/23/23 21:177.2EPA 8260D
Ethylbenzene 443 ug/kg 01/23/23 21:177.2EPA 8260D
Methyl-tert-butyl ether 85.5 ug/kg 01/23/23 21:177.2EPA 8260D
Toluene 34.2 ug/kg 01/23/23 21:177.2EPA 8260D
Xylene (Total)262 ug/kg 01/23/23 21:1714.4EPA 8260D
m&p-Xylene 199 ug/kg 01/23/23 21:1714.4EPA 8260D
o-Xylene 63.2 ug/kg 01/23/23 21:177.2EPA 8260D
Percent Moisture 21.2 %01/20/23 17:09 N20.10SW-846
92647996004 MW3
tert-Amyl Alcohol 6190 ug/L 01/25/23 19:484000SM 6200B
Benzene 2030 ug/L 01/25/23 19:4820.0SM 6200B
tert-Butyl Alcohol 3720 ug/L 01/25/23 19:482000SM 6200B
Diisopropyl ether 108 ug/L 01/25/23 19:4820.0SM 6200B
Ethylbenzene 602 ug/L 01/25/23 19:4820.0SM 6200B
Isopropylbenzene (Cumene)28.3 ug/L 01/25/23 19:4820.0SM 6200B
Methyl-tert-butyl ether 608 ug/L 01/25/23 19:4820.0SM 6200B
Naphthalene 380 ug/L 01/25/23 19:4880.0SM 6200B
n-Propylbenzene 73.8 ug/L 01/25/23 19:4820.0SM 6200B
Toluene 5090 ug/L 01/25/23 19:4820.0SM 6200B
1,2,4-Trimethylbenzene 1470 ug/L 01/25/23 19:4820.0SM 6200B
1,3,5-Trimethylbenzene 808 ug/L 01/25/23 19:4820.0SM 6200B
m&p-Xylene 3400 ug/L 01/25/23 19:4840.0SM 6200B
o-Xylene 2550 ug/L 01/25/23 19:4820.0SM 6200B
92647996005 MW13
Phenol 65.3 ug/L 01/26/23 10:1650.0EPA 625.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 65
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92647996005 MW13
3.803:Unknown 166J ug/L 01/26/23 10:16EPA 625.1
6.006:Unknown 209J ug/L 01/26/23 10:16EPA 625.1
6.276:Unknown 142J ug/L 01/26/23 10:16EPA 625.1
13.822:10-Methylnonadecane 56.1J ug/L 01/26/23 10:16 NEPA 625.1
14.225:Unknown 68.8J ug/L 01/26/23 10:16EPA 625.1
14.643:Heneicosane 77.9J ug/L 01/26/23 10:16 NEPA 625.1
15.079:10-Methylnonadecane 70.7J ug/L 01/26/23 10:16 NEPA 625.1
15.534:Eicosane 95.4J ug/L 01/26/23 10:16 NEPA 625.1
16.005:Tetratriacontane 81.6J ug/L 01/26/23 10:16 NEPA 625.1
16.489:10-Methylnonadecane 2390J ug/L 01/26/23 10:16 NEPA 625.1
92647996006 MW14
Benzene 211 ug/L 01/25/23 19:125.0SM 6200B
tert-Butyl Alcohol 775 ug/L 01/25/23 19:12500SM 6200B
Ethylbenzene 1180 ug/L 01/25/23 19:125.0SM 6200B
Isopropylbenzene (Cumene)73.5 ug/L 01/25/23 19:125.0SM 6200B
Methyl-tert-butyl ether 81.2 ug/L 01/25/23 19:125.0SM 6200B
Naphthalene 394 ug/L 01/25/23 19:1220.0SM 6200B
n-Propylbenzene 219 ug/L 01/25/23 19:125.0SM 6200B
Toluene 31.5 ug/L 01/25/23 19:125.0SM 6200B
1,2,4-Trimethylbenzene 930 ug/L 01/25/23 19:125.0SM 6200B
1,3,5-Trimethylbenzene 188 ug/L 01/25/23 19:125.0SM 6200B
m&p-Xylene 1460 ug/L 01/25/23 19:1210.0SM 6200B
o-Xylene 8.5 ug/L 01/25/23 19:125.0SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:GP1 Lab ID:92647996001 Collected:01/18/23 08:40 Received:01/19/23 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene 45.9 ug/kg 01/24/23 00:24 71-43-201/23/23 19:1626.1 1
Ethylbenzene 61.0 ug/kg 01/24/23 00:24 100-41-401/23/23 19:1626.1 1
Methyl-tert-butyl ether ND ug/kg 01/24/23 00:24 1634-04-401/23/23 19:1626.1 1
Toluene ND ug/kg 01/24/23 00:24 108-88-301/23/23 19:1626.1 1
Xylene (Total)164 ug/kg 01/24/23 00:24 1330-20-701/23/23 19:1652.1 1
m&p-Xylene 124 ug/kg 01/24/23 00:24 179601-23-101/23/23 19:1652.1 1
o-Xylene 40.3 ug/kg 01/24/23 00:24 95-47-601/23/23 19:1626.1 1
Surrogates
Toluene-d8 (S)100 %01/24/23 00:24 2037-26-501/23/23 19:1670-130 1
4-Bromofluorobenzene (S)108 %01/24/23 00:24 460-00-401/23/23 19:1670-130 1
1,2-Dichloroethane-d4 (S)109 %01/24/23 00:24 17060-07-001/23/23 19:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.4 %01/20/23 17:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:GD1 Lab ID:92647996002 Collected:01/18/23 09:30 Received:01/19/23 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene 1010 ug/kg 01/25/23 01:12 71-43-201/24/23 15:0977.8 12.5
Ethylbenzene 30300 ug/kg 01/25/23 01:12 100-41-401/24/23 15:0977.8 12.5
Methyl-tert-butyl ether ND ug/kg 01/25/23 01:12 1634-04-401/24/23 15:0977.8 12.5
Toluene 3770 ug/kg 01/25/23 01:12 108-88-301/24/23 15:0977.8 12.5
Xylene (Total)78400 ug/kg 01/25/23 01:12 1330-20-701/24/23 15:0915612.5
m&p-Xylene 73400 ug/kg 01/25/23 01:12 179601-23-101/24/23 15:0915612.5
o-Xylene 5020 ug/kg 01/25/23 01:12 95-47-601/24/23 15:0977.8 12.5
Surrogates
Toluene-d8 (S)101 %01/25/23 01:12 2037-26-501/24/23 15:0970-130 12.5
4-Bromofluorobenzene (S)109 %01/25/23 01:12 460-00-401/24/23 15:0970-130 12.5
1,2-Dichloroethane-d4 (S)120 %01/25/23 01:12 17060-07-001/24/23 15:0970-130 12.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.3 %01/20/23 17:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:KD Lab ID:92647996003 Collected:01/18/23 09:50 Received:01/19/23 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)194 mg/kg 01/26/23 11:01 N201/24/23 11:0932.3 2.5
Aliphatic (C19-C36)ND mg/kg 01/26/23 11:01 N201/24/23 11:0932.3 2.5
Aromatic (C11-C22)56.2 mg/kg 01/25/23 19:05 N201/24/23 11:0912.9 1
Surrogates
1-Chlorooctadecane (S)65 %01/26/23 11:01 3386-33-201/24/23 11:0940-140 2.5
o-Terphenyl (S)87 %01/25/23 19:05 84-15-101/24/23 11:0940-140 1
2-Fluorobiphenyl (S)152 %01/25/23 19:05 321-60-8 S501/24/23 11:0940-140 1
2-Bromonaphthalene (S)184 %01/25/23 19:05 580-13-2 S501/24/23 11:0940-140 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 01/26/23 10:21 83-32-901/25/23 11:044201
Acenaphthylene ND ug/kg 01/26/23 10:21 208-96-801/25/23 11:044201
Aniline ND ug/kg 01/26/23 10:21 62-53-301/25/23 11:044201
Anthracene ND ug/kg 01/26/23 10:21 120-12-701/25/23 11:044201
Benzo(a)anthracene ND ug/kg 01/26/23 10:21 56-55-301/25/23 11:044201
Benzo(a)pyrene ND ug/kg 01/26/23 10:21 50-32-801/25/23 11:044201
Benzo(b)fluoranthene ND ug/kg 01/26/23 10:21 205-99-201/25/23 11:044201
Benzo(g,h,i)perylene ND ug/kg 01/26/23 10:21 191-24-201/25/23 11:044201
Benzo(k)fluoranthene ND ug/kg 01/26/23 10:21 207-08-901/25/23 11:044201
Benzoic Acid ND ug/kg 01/26/23 10:21 65-85-001/25/23 11:0421001
Benzyl alcohol ND ug/kg 01/26/23 10:21 100-51-601/25/23 11:048401
4-Bromophenylphenyl ether ND ug/kg 01/26/23 10:21 101-55-301/25/23 11:044201
Butylbenzylphthalate ND ug/kg 01/26/23 10:21 85-68-701/25/23 11:044201
4-Chloro-3-methylphenol ND ug/kg 01/26/23 10:21 59-50-701/25/23 11:048401
4-Chloroaniline ND ug/kg 01/26/23 10:21 106-47-801/25/23 11:048401
bis(2-Chloroethoxy)methane ND ug/kg 01/26/23 10:21 111-91-101/25/23 11:044201
bis(2-Chloroethyl) ether ND ug/kg 01/26/23 10:21 111-44-401/25/23 11:044201
2-Chloronaphthalene ND ug/kg 01/26/23 10:21 91-58-701/25/23 11:044201
2-Chlorophenol ND ug/kg 01/26/23 10:21 95-57-801/25/23 11:044201
4-Chlorophenylphenyl ether ND ug/kg 01/26/23 10:21 7005-72-301/25/23 11:044201
Chrysene ND ug/kg 01/26/23 10:21 218-01-901/25/23 11:044201
Dibenz(a,h)anthracene ND ug/kg 01/26/23 10:21 53-70-301/25/23 11:044201
Dibenzofuran ND ug/kg 01/26/23 10:21 132-64-901/25/23 11:044201
1,2-Dichlorobenzene ND ug/kg 01/26/23 10:21 95-50-101/25/23 11:044201
1,3-Dichlorobenzene ND ug/kg 01/26/23 10:21 541-73-101/25/23 11:044201
1,4-Dichlorobenzene ND ug/kg 01/26/23 10:21 106-46-701/25/23 11:044201
3,3'-Dichlorobenzidine ND ug/kg 01/26/23 10:21 91-94-101/25/23 11:048401
2,4-Dichlorophenol ND ug/kg 01/26/23 10:21 120-83-201/25/23 11:044201
Diethylphthalate ND ug/kg 01/26/23 10:21 84-66-201/25/23 11:044201
2,4-Dimethylphenol ND ug/kg 01/26/23 10:21 105-67-901/25/23 11:044201
Dimethylphthalate ND ug/kg 01/26/23 10:21 131-11-301/25/23 11:044201
Di-n-butylphthalate ND ug/kg 01/26/23 10:21 84-74-201/25/23 11:044201
4,6-Dinitro-2-methylphenol ND ug/kg 01/26/23 10:21 534-52-101/25/23 11:048401
2,4-Dinitrophenol ND ug/kg 01/26/23 10:21 51-28-501/25/23 11:0421001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:KD Lab ID:92647996003 Collected:01/18/23 09:50 Received:01/19/23 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dinitrotoluene ND ug/kg 01/26/23 10:21 121-14-201/25/23 11:044201
2,6-Dinitrotoluene ND ug/kg 01/26/23 10:21 606-20-201/25/23 11:044201
Di-n-octylphthalate ND ug/kg 01/26/23 10:21 117-84-001/25/23 11:044201
bis(2-Ethylhexyl)phthalate ND ug/kg 01/26/23 10:21 117-81-7 v101/25/23 11:044201
Fluoranthene ND ug/kg 01/26/23 10:21 206-44-001/25/23 11:044201
Fluorene ND ug/kg 01/26/23 10:21 86-73-701/25/23 11:044201
Hexachloro-1,3-butadiene ND ug/kg 01/26/23 10:21 87-68-301/25/23 11:044201
Hexachlorobenzene ND ug/kg 01/26/23 10:21 118-74-101/25/23 11:044201
Hexachlorocyclopentadiene ND ug/kg 01/26/23 10:21 77-47-4 v201/25/23 11:044201
Hexachloroethane ND ug/kg 01/26/23 10:21 67-72-101/25/23 11:044201
Indeno(1,2,3-cd)pyrene ND ug/kg 01/26/23 10:21 193-39-501/25/23 11:044201
Isophorone ND ug/kg 01/26/23 10:21 78-59-101/25/23 11:044201
1-Methylnaphthalene 722 ug/kg 01/26/23 10:21 90-12-001/25/23 11:044201
2-Methylnaphthalene 933 ug/kg 01/26/23 10:21 91-57-601/25/23 11:044201
2-Methylphenol(o-Cresol)ND ug/kg 01/26/23 10:21 95-48-701/25/23 11:044201
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/26/23 10:21 15831-10-401/25/23 11:044201
Naphthalene 432 ug/kg 01/26/23 10:21 91-20-301/25/23 11:044201
2-Nitroaniline ND ug/kg 01/26/23 10:21 88-74-401/25/23 11:0421001
3-Nitroaniline ND ug/kg 01/26/23 10:21 99-09-201/25/23 11:0421001
4-Nitroaniline ND ug/kg 01/26/23 10:21 100-01-601/25/23 11:048401
Nitrobenzene ND ug/kg 01/26/23 10:21 98-95-301/25/23 11:044201
2-Nitrophenol ND ug/kg 01/26/23 10:21 88-75-501/25/23 11:044201
4-Nitrophenol ND ug/kg 01/26/23 10:21 100-02-701/25/23 11:0421001
N-Nitrosodimethylamine ND ug/kg 01/26/23 10:21 62-75-901/25/23 11:044201
N-Nitroso-di-n-propylamine ND ug/kg 01/26/23 10:21 621-64-701/25/23 11:044201
N-Nitrosodiphenylamine ND ug/kg 01/26/23 10:21 86-30-601/25/23 11:044201
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/26/23 10:21 108-60-101/25/23 11:044201
Pentachlorophenol ND ug/kg 01/26/23 10:21 87-86-501/25/23 11:048401
Phenanthrene ND ug/kg 01/26/23 10:21 85-01-801/25/23 11:044201
Phenol ND ug/kg 01/26/23 10:21 108-95-201/25/23 11:044201
Pyrene ND ug/kg 01/26/23 10:21 129-00-001/25/23 11:044201
Pyridine ND ug/kg 01/26/23 10:21 110-86-101/25/23 11:044201
1,2,4-Trichlorobenzene ND ug/kg 01/26/23 10:21 120-82-101/25/23 11:044201
2,4,5-Trichlorophenol ND ug/kg 01/26/23 10:21 95-95-401/25/23 11:044201
2,4,6-Trichlorophenol ND ug/kg 01/26/23 10:21 88-06-201/25/23 11:044201
Surrogates
Nitrobenzene-d5 (S)58 %01/26/23 10:21 4165-60-001/25/23 11:0410-130 1
2-Fluorobiphenyl (S)52 %01/26/23 10:21 321-60-801/25/23 11:0410-130 1
Terphenyl-d14 (S)72 %01/26/23 10:21 1718-51-001/25/23 11:0410-130 1
Phenol-d6 (S)58 %01/26/23 10:21 13127-88-301/25/23 11:0410-130 1
2-Fluorophenol (S)59 %01/26/23 10:21 367-12-401/25/23 11:0410-130 1
2,4,6-Tribromophenol (S)74 %01/26/23 10:21 118-79-601/25/23 11:0410-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:KD Lab ID:92647996003 Collected:01/18/23 09:50 Received:01/19/23 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene 1280 ug/kg 01/23/23 21:17 71-43-201/23/23 19:167.2 1
Ethylbenzene 443 ug/kg 01/23/23 21:17 100-41-401/23/23 19:167.2 1
Methyl-tert-butyl ether 85.5 ug/kg 01/23/23 21:17 1634-04-401/23/23 19:167.2 1
Toluene 34.2 ug/kg 01/23/23 21:17 108-88-301/23/23 19:167.2 1
Xylene (Total)262 ug/kg 01/23/23 21:17 1330-20-701/23/23 19:1614.4 1
m&p-Xylene 199 ug/kg 01/23/23 21:17 179601-23-101/23/23 19:1614.4 1
o-Xylene 63.2 ug/kg 01/23/23 21:17 95-47-601/23/23 19:167.2 1
Surrogates
Toluene-d8 (S)102 %01/23/23 21:17 2037-26-501/23/23 19:1670-130 1
4-Bromofluorobenzene (S)143 %01/23/23 21:17 460-00-4 S501/23/23 19:1670-130 1
1,2-Dichloroethane-d4 (S)118 %01/23/23 21:17 17060-07-001/23/23 19:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %01/20/23 17:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW3 Lab ID:92647996004 Collected:01/18/23 14:00 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol 6190 ug/L 01/25/23 19:48 75-85-4400040
tert-Amylmethyl ether ND ug/L 01/25/23 19:48 994-05-840040
Benzene 2030 ug/L 01/25/23 19:48 71-43-220.0 40
Bromobenzene ND ug/L 01/25/23 19:48 108-86-120.0 40
Bromochloromethane ND ug/L 01/25/23 19:48 74-97-520.0 40
Bromodichloromethane ND ug/L 01/25/23 19:48 75-27-420.0 40
Bromoform ND ug/L 01/25/23 19:48 75-25-220.0 40
Bromomethane ND ug/L 01/25/23 19:48 74-83-920040
tert-Butyl Alcohol 3720 ug/L 01/25/23 19:48 75-65-0200040
n-Butylbenzene ND ug/L 01/25/23 19:48 104-51-820.0 40
sec-Butylbenzene ND ug/L 01/25/23 19:48 135-98-820.0 40
tert-Butylbenzene ND ug/L 01/25/23 19:48 98-06-620.0 40
tert-Butyl Formate ND ug/L 01/25/23 19:48 762-75-4200040
Carbon tetrachloride ND ug/L 01/25/23 19:48 56-23-520.0 40
Chlorobenzene ND ug/L 01/25/23 19:48 108-90-720.0 40
Chloroethane ND ug/L 01/25/23 19:48 75-00-340.0 40
Chloroform ND ug/L 01/25/23 19:48 67-66-320.0 40
Chloromethane ND ug/L 01/25/23 19:48 74-87-340.0 40
2-Chlorotoluene ND ug/L 01/25/23 19:48 95-49-820.0 40
4-Chlorotoluene ND ug/L 01/25/23 19:48 106-43-420.0 40
1,2-Dibromo-3-chloropropane ND ug/L 01/25/23 19:48 96-12-840.0 40
Dibromochloromethane ND ug/L 01/25/23 19:48 124-48-120.0 40
1,2-Dibromoethane (EDB)ND ug/L 01/25/23 19:48 106-93-420.0 40
Dibromomethane ND ug/L 01/25/23 19:48 74-95-320.0 40
1,2-Dichlorobenzene ND ug/L 01/25/23 19:48 95-50-120.0 40
1,3-Dichlorobenzene ND ug/L 01/25/23 19:48 541-73-120.0 40
1,4-Dichlorobenzene ND ug/L 01/25/23 19:48 106-46-720.0 40
Dichlorodifluoromethane ND ug/L 01/25/23 19:48 75-71-820.0 40
1,1-Dichloroethane ND ug/L 01/25/23 19:48 75-34-320.0 40
1,2-Dichloroethane ND ug/L 01/25/23 19:48 107-06-220.0 40
1,1-Dichloroethene ND ug/L 01/25/23 19:48 75-35-420.0 40
cis-1,2-Dichloroethene ND ug/L 01/25/23 19:48 156-59-220.0 40
trans-1,2-Dichloroethene ND ug/L 01/25/23 19:48 156-60-520.0 40
1,2-Dichloropropane ND ug/L 01/25/23 19:48 78-87-520.0 40
1,3-Dichloropropane ND ug/L 01/25/23 19:48 142-28-920.0 40
2,2-Dichloropropane ND ug/L 01/25/23 19:48 594-20-720.0 40
1,1-Dichloropropene ND ug/L 01/25/23 19:48 563-58-620.0 40
cis-1,3-Dichloropropene ND ug/L 01/25/23 19:48 10061-01-520.0 40
trans-1,3-Dichloropropene ND ug/L 01/25/23 19:48 10061-02-620.0 40
Diisopropyl ether 108 ug/L 01/25/23 19:48 108-20-320.0 40
Ethanol ND ug/L 01/25/23 19:48 64-17-5800040
Ethylbenzene 602 ug/L 01/25/23 19:48 100-41-420.0 40
Ethyl-tert-butyl ether ND ug/L 01/25/23 19:48 637-92-340040
Hexachloro-1,3-butadiene ND ug/L 01/25/23 19:48 87-68-380.0 40
Isopropylbenzene (Cumene)28.3 ug/L 01/25/23 19:48 98-82-820.0 40
Methylene Chloride ND ug/L 01/25/23 19:48 75-09-2 IH80.0 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW3 Lab ID:92647996004 Collected:01/18/23 14:00 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 608 ug/L 01/25/23 19:48 1634-04-420.0 40
Naphthalene 380 ug/L 01/25/23 19:48 91-20-380.0 40
n-Propylbenzene 73.8 ug/L 01/25/23 19:48 103-65-120.0 40
Styrene ND ug/L 01/25/23 19:48 100-42-520.0 40
1,1,1,2-Tetrachloroethane ND ug/L 01/25/23 19:48 630-20-620.0 40
1,1,2,2-Tetrachloroethane ND ug/L 01/25/23 19:48 79-34-520.0 40
Tetrachloroethene ND ug/L 01/25/23 19:48 127-18-420.0 40
Toluene 5090 ug/L 01/25/23 19:48 108-88-320.0 40
1,2,3-Trichlorobenzene ND ug/L 01/25/23 19:48 87-61-680.0 40
1,2,4-Trichlorobenzene ND ug/L 01/25/23 19:48 120-82-180.0 40
1,1,1-Trichloroethane ND ug/L 01/25/23 19:48 71-55-620.0 40
1,1,2-Trichloroethane ND ug/L 01/25/23 19:48 79-00-520.0 40
Trichloroethene ND ug/L 01/25/23 19:48 79-01-620.0 40
Trichlorofluoromethane ND ug/L 01/25/23 19:48 75-69-440.0 40
1,2,3-Trichloropropane ND ug/L 01/25/23 19:48 96-18-420.0 40
1,2,4-Trimethylbenzene 1470 ug/L 01/25/23 19:48 95-63-620.0 40
1,3,5-Trimethylbenzene 808 ug/L 01/25/23 19:48 108-67-820.0 40
Vinyl chloride ND ug/L 01/25/23 19:48 75-01-440.0 40
m&p-Xylene 3400 ug/L 01/25/23 19:48 179601-23-140.0 40
o-Xylene 2550 ug/L 01/25/23 19:48 95-47-620.0 40
Surrogates
1,2-Dichloroethane-d4 (S)89 %01/25/23 19:48 17060-07-070-130 40
4-Bromofluorobenzene (S)97 %01/25/23 19:48 460-00-470-130 40
Toluene-d8 (S)104 %01/25/23 19:48 2037-26-570-130 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW13 Lab ID:92647996005 Collected:01/18/23 14:20 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 01/25/23 10:43 N201/24/23 10:261021
Aliphatic (C19-C36)ND ug/L 01/25/23 10:43 N201/24/23 10:261021
Aromatic (C11-C22)ND ug/L 01/25/23 10:43 N201/24/23 10:261021
Surrogates
1-Chlorooctadecane (S)30 %01/25/23 10:43 3386-33-2 S201/24/23 10:2640-140 1
o-Terphenyl (S)67 %01/25/23 10:43 84-15-101/24/23 10:2640-140 1
2-Fluorobiphenyl (S)102 %01/25/23 10:43 321-60-801/24/23 10:2640-140 1
2-Bromonaphthalene (S)110 %01/25/23 10:43 580-13-201/24/23 10:2640-140 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 01/26/23 10:16 83-32-901/24/23 10:4450.0 1
Acenaphthylene ND ug/L 01/26/23 10:16 208-96-801/24/23 10:4450.0 1
Anthracene ND ug/L 01/26/23 10:16 120-12-701/24/23 10:4450.0 1
Benzo(a)anthracene ND ug/L 01/26/23 10:16 56-55-301/24/23 10:4450.0 1
Benzo(a)pyrene ND ug/L 01/26/23 10:16 50-32-801/24/23 10:4450.0 1
Benzo(b)fluoranthene ND ug/L 01/26/23 10:16 205-99-201/24/23 10:4450.0 1
Benzo(g,h,i)perylene ND ug/L 01/26/23 10:16 191-24-201/24/23 10:4450.0 1
Benzo(k)fluoranthene ND ug/L 01/26/23 10:16 207-08-901/24/23 10:4450.0 1
4-Bromophenylphenyl ether ND ug/L 01/26/23 10:16 101-55-301/24/23 10:4450.0 1
Butylbenzylphthalate ND ug/L 01/26/23 10:16 85-68-701/24/23 10:4450.0 1
4-Chloro-3-methylphenol ND ug/L 01/26/23 10:16 59-50-701/24/23 10:4450.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/26/23 10:16 111-91-101/24/23 10:441001
bis(2-Chloroethyl) ether ND ug/L 01/26/23 10:16 111-44-401/24/23 10:4450.0 1
2-Chloronaphthalene ND ug/L 01/26/23 10:16 91-58-701/24/23 10:4450.0 1
2-Chlorophenol ND ug/L 01/26/23 10:16 95-57-801/24/23 10:4450.0 1
4-Chlorophenylphenyl ether ND ug/L 01/26/23 10:16 7005-72-301/24/23 10:4450.0 1
Chrysene ND ug/L 01/26/23 10:16 218-01-901/24/23 10:4450.0 1
Dibenz(a,h)anthracene ND ug/L 01/26/23 10:16 53-70-301/24/23 10:4450.0 1
3,3'-Dichlorobenzidine ND ug/L 01/26/23 10:16 91-94-101/24/23 10:441001
2,4-Dichlorophenol ND ug/L 01/26/23 10:16 120-83-201/24/23 10:4450.0 1
Diethylphthalate ND ug/L 01/26/23 10:16 84-66-201/24/23 10:4450.0 1
2,4-Dimethylphenol ND ug/L 01/26/23 10:16 105-67-901/24/23 10:441001
Dimethylphthalate ND ug/L 01/26/23 10:16 131-11-301/24/23 10:4450.0 1
Di-n-butylphthalate ND ug/L 01/26/23 10:16 84-74-201/24/23 10:4450.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/26/23 10:16 534-52-101/24/23 10:441001
2,4-Dinitrophenol ND ug/L 01/26/23 10:16 51-28-501/24/23 10:445001
2,4-Dinitrotoluene ND ug/L 01/26/23 10:16 121-14-201/24/23 10:4450.0 1
2,6-Dinitrotoluene ND ug/L 01/26/23 10:16 606-20-201/24/23 10:4450.0 1
Di-n-octylphthalate ND ug/L 01/26/23 10:16 117-84-001/24/23 10:4450.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/26/23 10:16 117-81-701/24/23 10:4450.0 1
Fluoranthene ND ug/L 01/26/23 10:16 206-44-001/24/23 10:4450.0 1
Fluorene ND ug/L 01/26/23 10:16 86-73-701/24/23 10:4450.0 1
Hexachloro-1,3-butadiene ND ug/L 01/26/23 10:16 87-68-301/24/23 10:4450.0 1
Hexachlorobenzene ND ug/L 01/26/23 10:16 118-74-101/24/23 10:4450.0 1
Hexachlorocyclopentadiene ND ug/L 01/26/23 10:16 77-47-401/24/23 10:441001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW13 Lab ID:92647996005 Collected:01/18/23 14:20 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Hexachloroethane ND ug/L 01/26/23 10:16 67-72-101/24/23 10:4450.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/26/23 10:16 193-39-501/24/23 10:4450.0 1
Isophorone ND ug/L 01/26/23 10:16 78-59-101/24/23 10:441001
Naphthalene ND ug/L 01/26/23 10:16 91-20-301/24/23 10:4450.0 1
Nitrobenzene ND ug/L 01/26/23 10:16 98-95-301/24/23 10:4450.0 1
2-Nitrophenol ND ug/L 01/26/23 10:16 88-75-501/24/23 10:4450.0 1
4-Nitrophenol ND ug/L 01/26/23 10:16 100-02-701/24/23 10:441001
N-Nitrosodimethylamine ND ug/L 01/26/23 10:16 62-75-901/24/23 10:4450.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/26/23 10:16 621-64-701/24/23 10:4450.0 1
N-Nitrosodiphenylamine ND ug/L 01/26/23 10:16 86-30-601/24/23 10:441001
2,2'-Oxybis(1-chloropropane)ND ug/L 01/26/23 10:16 108-60-101/24/23 10:4450.0 1
Pentachlorophenol ND ug/L 01/26/23 10:16 87-86-501/24/23 10:441001
Phenanthrene ND ug/L 01/26/23 10:16 85-01-801/24/23 10:4450.0 1
Phenol 65.3 ug/L 01/26/23 10:16 108-95-201/24/23 10:4450.0 1
Pyrene ND ug/L 01/26/23 10:16 129-00-001/24/23 10:4450.0 1
1,2,4-Trichlorobenzene ND ug/L 01/26/23 10:16 120-82-101/24/23 10:4450.0 1
2,4,6-Trichlorophenol ND ug/L 01/26/23 10:16 88-06-201/24/23 10:441001
Surrogates
Nitrobenzene-d5 (S)102 %01/26/23 10:16 4165-60-001/24/23 10:4410-120 1
2-Fluorobiphenyl (S)69 %01/26/23 10:16 321-60-801/24/23 10:4415-120 1
Terphenyl-d14 (S)123 %01/26/23 10:16 1718-51-001/24/23 10:4411-131 1
Phenol-d6 (S)60 %01/26/23 10:16 13127-88-301/24/23 10:4410-120 1
2-Fluorophenol (S)63 %01/26/23 10:16 367-12-401/24/23 10:4410-120 1
2,4,6-Tribromophenol (S)94 %01/26/23 10:16 118-79-601/24/23 10:4410-137 1
Tentatively Identified Compounds
Unknown 166J ug/L 01/26/23 10:1601/24/23 10:441
Unknown 209J ug/L 01/26/23 10:1601/24/23 10:441
Unknown 142J ug/L 01/26/23 10:1601/24/23 10:441
10-Methylnonadecane 56.1J ug/L 01/26/23 10:16 56862-62-5 N01/24/23 10:441
Unknown 68.8J ug/L 01/26/23 10:1601/24/23 10:441
Heneicosane 77.9J ug/L 01/26/23 10:16 629-94-7 N01/24/23 10:441
10-Methylnonadecane 70.7J ug/L 01/26/23 10:16 56862-62-5 N01/24/23 10:441
Eicosane 95.4J ug/L 01/26/23 10:16 112-95-8 N01/24/23 10:441
Tetratriacontane 81.6J ug/L 01/26/23 10:16 14167-59-0 N01/24/23 10:441
10-Methylnonadecane 2390J ug/L 01/26/23 10:16 56862-62-5 N01/24/23 10:441
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 01/25/23 16:50 75-85-41001
tert-Amylmethyl ether ND ug/L 01/25/23 16:50 994-05-810.0 1
Benzene ND ug/L 01/25/23 16:50 71-43-20.50 1
Bromobenzene ND ug/L 01/25/23 16:50 108-86-10.50 1
Bromochloromethane ND ug/L 01/25/23 16:50 74-97-50.50 1
Bromodichloromethane ND ug/L 01/25/23 16:50 75-27-40.50 1
Bromoform ND ug/L 01/25/23 16:50 75-25-20.50 1
Bromomethane ND ug/L 01/25/23 16:50 74-83-95.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW13 Lab ID:92647996005 Collected:01/18/23 14:20 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Butyl Alcohol ND ug/L 01/25/23 16:50 75-65-050.0 1
n-Butylbenzene ND ug/L 01/25/23 16:50 104-51-80.50 1
sec-Butylbenzene ND ug/L 01/25/23 16:50 135-98-80.50 1
tert-Butylbenzene ND ug/L 01/25/23 16:50 98-06-60.50 1
tert-Butyl Formate ND ug/L 01/25/23 16:50 762-75-450.0 1
Carbon tetrachloride ND ug/L 01/25/23 16:50 56-23-50.50 1
Chlorobenzene ND ug/L 01/25/23 16:50 108-90-70.50 1
Chloroethane ND ug/L 01/25/23 16:50 75-00-31.0 1
Chloroform ND ug/L 01/25/23 16:50 67-66-30.50 1
Chloromethane ND ug/L 01/25/23 16:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 01/25/23 16:50 95-49-80.50 1
4-Chlorotoluene ND ug/L 01/25/23 16:50 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 01/25/23 16:50 96-12-81.0 1
Dibromochloromethane ND ug/L 01/25/23 16:50 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 01/25/23 16:50 106-93-40.50 1
Dibromomethane ND ug/L 01/25/23 16:50 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 01/25/23 16:50 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 01/25/23 16:50 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 01/25/23 16:50 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 01/25/23 16:50 75-71-80.50 1
1,1-Dichloroethane ND ug/L 01/25/23 16:50 75-34-30.50 1
1,2-Dichloroethane ND ug/L 01/25/23 16:50 107-06-20.50 1
1,1-Dichloroethene ND ug/L 01/25/23 16:50 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 01/25/23 16:50 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 01/25/23 16:50 156-60-50.50 1
1,2-Dichloropropane ND ug/L 01/25/23 16:50 78-87-50.50 1
1,3-Dichloropropane ND ug/L 01/25/23 16:50 142-28-90.50 1
2,2-Dichloropropane ND ug/L 01/25/23 16:50 594-20-70.50 1
1,1-Dichloropropene ND ug/L 01/25/23 16:50 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 01/25/23 16:50 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 01/25/23 16:50 10061-02-60.50 1
Diisopropyl ether ND ug/L 01/25/23 16:50 108-20-30.50 1
Ethanol ND ug/L 01/25/23 16:50 64-17-52001
Ethylbenzene ND ug/L 01/25/23 16:50 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 01/25/23 16:50 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 01/25/23 16:50 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 01/25/23 16:50 98-82-80.50 1
Methylene Chloride ND ug/L 01/25/23 16:50 75-09-2 IH2.0 1
Methyl-tert-butyl ether ND ug/L 01/25/23 16:50 1634-04-40.50 1
Naphthalene ND ug/L 01/25/23 16:50 91-20-32.0 1
n-Propylbenzene ND ug/L 01/25/23 16:50 103-65-10.50 1
Styrene ND ug/L 01/25/23 16:50 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 01/25/23 16:50 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 01/25/23 16:50 79-34-50.50 1
Tetrachloroethene ND ug/L 01/25/23 16:50 127-18-40.50 1
Toluene ND ug/L 01/25/23 16:50 108-88-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW13 Lab ID:92647996005 Collected:01/18/23 14:20 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichlorobenzene ND ug/L 01/25/23 16:50 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 01/25/23 16:50 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 01/25/23 16:50 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 01/25/23 16:50 79-00-50.50 1
Trichloroethene ND ug/L 01/25/23 16:50 79-01-60.50 1
Trichlorofluoromethane ND ug/L 01/25/23 16:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/25/23 16:50 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 01/25/23 16:50 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 01/25/23 16:50 108-67-80.50 1
Vinyl chloride ND ug/L 01/25/23 16:50 75-01-41.0 1
m&p-Xylene ND ug/L 01/25/23 16:50 179601-23-11.0 1
o-Xylene ND ug/L 01/25/23 16:50 95-47-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW14 Lab ID:92647996006 Collected:01/18/23 14:40 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 01/25/23 19:12 75-85-4100010
tert-Amylmethyl ether ND ug/L 01/25/23 19:12 994-05-810010
Benzene 211 ug/L 01/25/23 19:12 71-43-25.0 10
Bromobenzene ND ug/L 01/25/23 19:12 108-86-15.0 10
Bromochloromethane ND ug/L 01/25/23 19:12 74-97-55.0 10
Bromodichloromethane ND ug/L 01/25/23 19:12 75-27-45.0 10
Bromoform ND ug/L 01/25/23 19:12 75-25-25.0 10
Bromomethane ND ug/L 01/25/23 19:12 74-83-950.0 10
tert-Butyl Alcohol 775 ug/L 01/25/23 19:12 75-65-050010
n-Butylbenzene ND ug/L 01/25/23 19:12 104-51-85.0 10
sec-Butylbenzene ND ug/L 01/25/23 19:12 135-98-85.0 10
tert-Butylbenzene ND ug/L 01/25/23 19:12 98-06-65.0 10
tert-Butyl Formate ND ug/L 01/25/23 19:12 762-75-450010
Carbon tetrachloride ND ug/L 01/25/23 19:12 56-23-55.0 10
Chlorobenzene ND ug/L 01/25/23 19:12 108-90-75.0 10
Chloroethane ND ug/L 01/25/23 19:12 75-00-310.0 10
Chloroform ND ug/L 01/25/23 19:12 67-66-35.0 10
Chloromethane ND ug/L 01/25/23 19:12 74-87-310.0 10
2-Chlorotoluene ND ug/L 01/25/23 19:12 95-49-85.0 10
4-Chlorotoluene ND ug/L 01/25/23 19:12 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 01/25/23 19:12 96-12-810.0 10
Dibromochloromethane ND ug/L 01/25/23 19:12 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 01/25/23 19:12 106-93-45.0 10
Dibromomethane ND ug/L 01/25/23 19:12 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 01/25/23 19:12 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 01/25/23 19:12 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 01/25/23 19:12 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 01/25/23 19:12 75-71-85.0 10
1,1-Dichloroethane ND ug/L 01/25/23 19:12 75-34-35.0 10
1,2-Dichloroethane ND ug/L 01/25/23 19:12 107-06-25.0 10
1,1-Dichloroethene ND ug/L 01/25/23 19:12 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 01/25/23 19:12 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 01/25/23 19:12 156-60-55.0 10
1,2-Dichloropropane ND ug/L 01/25/23 19:12 78-87-55.0 10
1,3-Dichloropropane ND ug/L 01/25/23 19:12 142-28-95.0 10
2,2-Dichloropropane ND ug/L 01/25/23 19:12 594-20-75.0 10
1,1-Dichloropropene ND ug/L 01/25/23 19:12 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 01/25/23 19:12 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 01/25/23 19:12 10061-02-65.0 10
Diisopropyl ether ND ug/L 01/25/23 19:12 108-20-35.0 10
Ethanol ND ug/L 01/25/23 19:12 64-17-5200010
Ethylbenzene 1180 ug/L 01/25/23 19:12 100-41-45.0 10
Ethyl-tert-butyl ether ND ug/L 01/25/23 19:12 637-92-310010
Hexachloro-1,3-butadiene ND ug/L 01/25/23 19:12 87-68-320.0 10
Isopropylbenzene (Cumene)73.5 ug/L 01/25/23 19:12 98-82-85.0 10
Methylene Chloride ND ug/L 01/25/23 19:12 75-09-2 IH20.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Sample:MW14 Lab ID:92647996006 Collected:01/18/23 14:40 Received:01/19/23 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 81.2 ug/L 01/25/23 19:12 1634-04-45.0 10
Naphthalene 394 ug/L 01/25/23 19:12 91-20-320.0 10
n-Propylbenzene 219 ug/L 01/25/23 19:12 103-65-15.0 10
Styrene ND ug/L 01/25/23 19:12 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 01/25/23 19:12 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 01/25/23 19:12 79-34-55.0 10
Tetrachloroethene ND ug/L 01/25/23 19:12 127-18-45.0 10
Toluene 31.5 ug/L 01/25/23 19:12 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 01/25/23 19:12 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 01/25/23 19:12 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 01/25/23 19:12 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 01/25/23 19:12 79-00-55.0 10
Trichloroethene ND ug/L 01/25/23 19:12 79-01-65.0 10
Trichlorofluoromethane ND ug/L 01/25/23 19:12 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 01/25/23 19:12 96-18-45.0 10
1,2,4-Trimethylbenzene 930 ug/L 01/25/23 19:12 95-63-65.0 10
1,3,5-Trimethylbenzene 188 ug/L 01/25/23 19:12 108-67-85.0 10
Vinyl chloride ND ug/L 01/25/23 19:12 75-01-410.0 10
m&p-Xylene 1460 ug/L 01/25/23 19:12 179601-23-110.0 10
o-Xylene 8.5 ug/L 01/25/23 19:12 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)92 %01/25/23 19:12 17060-07-070-130 10
4-Bromofluorobenzene (S)97 %01/25/23 19:12 460-00-470-130 10
Toluene-d8 (S)106 %01/25/23 19:12 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751673
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996004, 92647996005, 92647996006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3905993
Associated Lab Samples:92647996004, 92647996005, 92647996006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/25/23 15:57
1,1,1-Trichloroethane ug/L ND 0.50 01/25/23 15:57
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/25/23 15:57
1,1,2-Trichloroethane ug/L ND 0.50 01/25/23 15:57
1,1-Dichloroethane ug/L ND 0.50 01/25/23 15:57
1,1-Dichloroethene ug/L ND 0.50 01/25/23 15:57
1,1-Dichloropropene ug/L ND 0.50 01/25/23 15:57
1,2,3-Trichlorobenzene ug/L ND 2.0 01/25/23 15:57
1,2,3-Trichloropropane ug/L ND 0.50 01/25/23 15:57
1,2,4-Trichlorobenzene ug/L ND 2.0 01/25/23 15:57
1,2,4-Trimethylbenzene ug/L ND 0.50 01/25/23 15:57
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/25/23 15:57
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/25/23 15:57
1,2-Dichlorobenzene ug/L ND 0.50 01/25/23 15:57
1,2-Dichloroethane ug/L ND 0.50 01/25/23 15:57
1,2-Dichloropropane ug/L ND 0.50 01/25/23 15:57
1,3,5-Trimethylbenzene ug/L ND 0.50 01/25/23 15:57
1,3-Dichlorobenzene ug/L ND 0.50 01/25/23 15:57
1,3-Dichloropropane ug/L ND 0.50 01/25/23 15:57
1,4-Dichlorobenzene ug/L ND 0.50 01/25/23 15:57
2,2-Dichloropropane ug/L ND 0.50 01/25/23 15:57
2-Chlorotoluene ug/L ND 0.50 01/25/23 15:57
4-Chlorotoluene ug/L ND 0.50 01/25/23 15:57
Benzene ug/L ND 0.50 01/25/23 15:57
Bromobenzene ug/L ND 0.50 01/25/23 15:57
Bromochloromethane ug/L ND 0.50 01/25/23 15:57
Bromodichloromethane ug/L ND 0.50 01/25/23 15:57
Bromoform ug/L ND 0.50 01/25/23 15:57
Bromomethane ug/L ND 5.0 01/25/23 15:57
Carbon tetrachloride ug/L ND 0.50 01/25/23 15:57
Chlorobenzene ug/L ND 0.50 01/25/23 15:57
Chloroethane ug/L ND 1.0 01/25/23 15:57
Chloroform ug/L ND 0.50 01/25/23 15:57
Chloromethane ug/L ND 1.0 01/25/23 15:57
cis-1,2-Dichloroethene ug/L ND 0.50 01/25/23 15:57
cis-1,3-Dichloropropene ug/L ND 0.50 01/25/23 15:57
Dibromochloromethane ug/L ND 0.50 01/25/23 15:57
Dibromomethane ug/L ND 0.50 01/25/23 15:57
Dichlorodifluoromethane ug/L ND 0.50 01/25/23 15:57
Diisopropyl ether ug/L ND 0.50 01/25/23 15:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3905993
Associated Lab Samples:92647996004, 92647996005, 92647996006
Matrix:Water
Analyzed
Ethanol ug/L ND 200 01/25/23 15:57
Ethyl-tert-butyl ether ug/L ND 10.0 01/25/23 15:57
Ethylbenzene ug/L ND 0.50 01/25/23 15:57
Hexachloro-1,3-butadiene ug/L ND 2.0 01/25/23 15:57
Isopropylbenzene (Cumene)ug/L ND 0.50 01/25/23 15:57
m&p-Xylene ug/L ND 1.0 01/25/23 15:57
Methyl-tert-butyl ether ug/L ND 0.50 01/25/23 15:57
Methylene Chloride ug/L ND 2.0 IH01/25/23 15:57
n-Butylbenzene ug/L ND 0.50 01/25/23 15:57
n-Propylbenzene ug/L ND 0.50 01/25/23 15:57
Naphthalene ug/L ND 2.0 01/25/23 15:57
o-Xylene ug/L ND 0.50 01/25/23 15:57
sec-Butylbenzene ug/L ND 0.50 01/25/23 15:57
Styrene ug/L ND 0.50 01/25/23 15:57
tert-Amyl Alcohol ug/L ND 100 01/25/23 15:57
tert-Amylmethyl ether ug/L ND 10.0 01/25/23 15:57
tert-Butyl Alcohol ug/L ND 50.0 01/25/23 15:57
tert-Butyl Formate ug/L ND 50.0 01/25/23 15:57
tert-Butylbenzene ug/L ND 0.50 01/25/23 15:57
Tetrachloroethene ug/L ND 0.50 01/25/23 15:57
Toluene ug/L ND 0.50 01/25/23 15:57
trans-1,2-Dichloroethene ug/L ND 0.50 01/25/23 15:57
trans-1,3-Dichloropropene ug/L ND 0.50 01/25/23 15:57
Trichloroethene ug/L ND 0.50 01/25/23 15:57
Trichlorofluoromethane ug/L ND 1.0 01/25/23 15:57
Vinyl chloride ug/L ND 1.0 01/25/23 15:57
1,2-Dichloroethane-d4 (S)%89 70-130 01/25/23 15:57
4-Bromofluorobenzene (S)%102 70-130 01/25/23 15:57
Toluene-d8 (S)%102 70-130 01/25/23 15:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905994LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.320 96 60-140
1,1,1-Trichloroethane ug/L 19.820 99 60-140
1,1,2,2-Tetrachloroethane ug/L 19.320 96 60-140
1,1,2-Trichloroethane ug/L 21.120 105 60-140
1,1-Dichloroethane ug/L 19.120 95 60-140
1,1-Dichloroethene ug/L 20.920 105 60-140
1,1-Dichloropropene ug/L 18.120 91 60-140
1,2,3-Trichlorobenzene ug/L 20.220 101 60-140
1,2,3-Trichloropropane ug/L 19.020 95 60-140
1,2,4-Trichlorobenzene ug/L 20.320 101 60-140
1,2,4-Trimethylbenzene ug/L 20.120 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905994LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 19.220 96 60-140
1,2-Dibromoethane (EDB)ug/L 19.720 99 60-140
1,2-Dichlorobenzene ug/L 19.820 99 60-140
1,2-Dichloroethane ug/L 19.320 97 60-140
1,2-Dichloropropane ug/L 21.820 109 60-140
1,3,5-Trimethylbenzene ug/L 20.220 101 60-140
1,3-Dichlorobenzene ug/L 20.120 100 60-140
1,3-Dichloropropane ug/L 19.720 99 60-140
1,4-Dichlorobenzene ug/L 19.320 97 60-140
2,2-Dichloropropane ug/L 19.920 99 60-140
2-Chlorotoluene ug/L 19.720 98 60-140
4-Chlorotoluene ug/L 19.220 96 60-140
Benzene ug/L 18.620 93 60-140
Bromobenzene ug/L 18.820 94 60-140
Bromochloromethane ug/L 21.120 105 60-140
Bromodichloromethane ug/L 20.520 103 60-140
Bromoform ug/L 20.020 100 60-140
Bromomethane ug/L 24.620 123 60-140
Carbon tetrachloride ug/L 20.320 102 60-140
Chlorobenzene ug/L 19.620 98 60-140
Chloroethane ug/L 25.220 126 60-140
Chloroform ug/L 19.320 96 60-140
Chloromethane ug/L 25.120 126 60-140
cis-1,2-Dichloroethene ug/L 18.920 95 60-140
cis-1,3-Dichloropropene ug/L 21.020 105 60-140
Dibromochloromethane ug/L 19.820 99 60-140
Dibromomethane ug/L 20.520 103 60-140
Dichlorodifluoromethane ug/L 24.320 122 60-140
Diisopropyl ether ug/L 17.920 89 60-140
Ethanol ug/L 782800 98 60-140
Ethyl-tert-butyl ether ug/L 35.540 89 60-140
Ethylbenzene ug/L 19.720 98 60-140
Hexachloro-1,3-butadiene ug/L 21.320 107 60-140
Isopropylbenzene (Cumene)ug/L 19.820 99 60-140
m&p-Xylene ug/L 39.940 100 60-140
Methyl-tert-butyl ether ug/L 18.120 90 60-140
Methylene Chloride ug/L 16.5 IH208260-140
n-Butylbenzene ug/L 21.420 107 60-140
n-Propylbenzene ug/L 19.720 98 60-140
Naphthalene ug/L 19.820 99 60-140
o-Xylene ug/L 20.220 101 60-140
sec-Butylbenzene ug/L 20.520 103 60-140
Styrene ug/L 20.220 101 60-140
tert-Amyl Alcohol ug/L 341400 85 60-140
tert-Amylmethyl ether ug/L 36.940 92 60-140
tert-Butyl Alcohol ug/L 181200 91 60-140
tert-Butyl Formate ug/L 147160 92 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905994LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 17.020 85 60-140
Tetrachloroethene ug/L 19.920 100 60-140
Toluene ug/L 19.820 99 60-140
trans-1,2-Dichloroethene ug/L 20.320 101 60-140
trans-1,3-Dichloropropene ug/L 21.220 106 60-140
Trichloroethene ug/L 20.320 101 60-140
Trichlorofluoromethane ug/L 20.020 100 60-140
Vinyl chloride ug/L 26.120 130 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3905995MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92647704002
3905996
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 98 60-140100 2 3020ND19.6 20.0
1,1,1-Trichloroethane ug/L 20 110 60-140110 0 3020ND22.0 22.0
1,1,2,2-Tetrachloroethane ug/L 20 97 60-140102 5 3020ND19.5 20.4
1,1,2-Trichloroethane ug/L 20 96 60-14096 1 3020ND19.2 19.3
1,1-Dichloroethane ug/L 20 103 60-140106 3 3020ND20.6 21.3
1,1-Dichloroethene ug/L 20 109 60-140108 2 3020ND21.9 21.5
1,1-Dichloropropene ug/L 20 122 60-140121 1 3020ND24.4 24.1
1,2,3-Trichlorobenzene ug/L 20 90 60-14096 7 3020ND17.9 19.2
1,2,3-Trichloropropane ug/L 20 93 60-14086 7 3020ND18.6 17.2
1,2,4-Trichlorobenzene ug/L 20 93 60-14094 1 3020ND18.6 18.8
1,2,4-Trimethylbenzene ug/L 20 104 60-140107 2 3020ND20.8 21.3
1,2-Dibromo-3-
chloropropane ug/L 20 93 60-14094 1 3020ND18.6 18.8
1,2-Dibromoethane (EDB)ug/L 20 98 60-140103 5 3020ND19.6 20.6
1,2-Dichlorobenzene ug/L 20 94 60-14098 4 3020ND18.7 19.6
1,2-Dichloroethane ug/L 20 91 60-14093 2 3020ND18.2 18.6
1,2-Dichloropropane ug/L 20 100 60-14098 2 3020ND20.0 19.7
1,3,5-Trimethylbenzene ug/L 20 105 60-140108 3 3020ND21.0 21.7
1,3-Dichlorobenzene ug/L 20 99 60-140104 5 3020ND19.7 20.7
1,3-Dichloropropane ug/L 20 102 60-140105 2 3020ND20.4 20.9
1,4-Dichlorobenzene ug/L 20 90 60-14095 5 3020ND18.1 19.1
2,2-Dichloropropane ug/L 20 109 60-140108 0 3020ND21.7 21.6
2-Chlorotoluene ug/L 20 92 60-140105 13 3020ND18.4 21.0
4-Chlorotoluene ug/L 20 97 60-140101 4 3020ND19.4 20.2
Benzene ug/L 20 103 60-140102 1 3020ND20.7 20.5
Bromobenzene ug/L 20 95 60-140100 5 3020ND19.0 19.9
Bromochloromethane ug/L 20 104 60-140106 1 3020ND20.9 21.2
Bromodichloromethane ug/L 20 98 60-14098 1 3020ND19.7 19.6
Bromoform ug/L 20 84 60-14092 10 3020ND16.7 18.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3905995MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92647704002
3905996
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 62 60-14081 26 3020ND12.4 16.2
Carbon tetrachloride ug/L 20 100 60-140100 0 3020ND19.9 20.0
Chlorobenzene ug/L 20 99 60-140100 0 3020ND19.9 19.9
Chloroethane ug/L 20 105 60-140108 2 3020ND21.0 21.5
Chloroform ug/L 20 121 60-140118 3 3020ND24.2 23.6
Chloromethane ug/L 20 78 60-14078 1 3020ND15.7 15.5
cis-1,2-Dichloroethene ug/L 20 102 60-140102 0 3020ND20.4 20.4
cis-1,3-Dichloropropene ug/L 20 104 60-140110 5 3020ND20.9 22.0
Dibromochloromethane ug/L 20 99 60-14097 2 3020ND19.8 19.4
Dibromomethane ug/L 20 94 60-14090 4 3020ND18.8 18.1
Dichlorodifluoromethane ug/L 20 70 60-14072 2 3020ND14.1 14.4
Diisopropyl ether ug/L 20 93 60-14090 3 3020ND18.5 18.0
Ethanol ug/L 800 102 60-140101 1 30800ND815805
Ethyl-tert-butyl ether ug/L 40 96 60-14092 4 3040ND38.3 36.9
Ethylbenzene ug/L 20 101 60-140103 2 3020ND20.1 20.6
Hexachloro-1,3-butadiene ug/L 20 93 60-14096 2 3020ND18.7 19.1
Isopropylbenzene
(Cumene)ug/L 20 98 60-140101 3 3020ND19.7 20.3
m&p-Xylene ug/L 40 100 60-140104 4 3040ND40.0 41.6
Methyl-tert-butyl ether ug/L 20 101 60-14095 6 3020ND20.1 18.9
Methylene Chloride ug/L 20 75 60-14077 3 3020ND15.1 15.5
n-Butylbenzene ug/L 20 109 60-140112 3 3020ND21.7 22.5
n-Propylbenzene ug/L 20 101 60-140104 3 3020ND20.3 20.8
Naphthalene ug/L 20 91 60-140101 10 3020ND18.3 20.2
o-Xylene ug/L 20 99 60-140100 1 3020ND19.7 19.9
sec-Butylbenzene ug/L 20 104 60-140109 4 3020ND20.8 21.7
Styrene ug/L 20 98 60-140101 2 3020ND19.7 20.2
tert-Amyl Alcohol ug/L 400 100 60-14098 2 30400ND398391
tert-Amylmethyl ether ug/L 40 99 60-14098 1 3040ND39.6 39.1
tert-Butyl Alcohol ug/L M120014660-140141 4 30200ND292282
tert-Butyl Formate ug/L M1160860-1406 30160NDNDND
tert-Butylbenzene ug/L 20 85 60-14089 5 3020ND17.0 17.9
Tetrachloroethene ug/L 20 93 60-14099 5 3020ND18.7 19.7
Toluene ug/L 20 95 60-14097 2 3020ND19.0 19.5
trans-1,2-Dichloroethene ug/L 20 105 60-140108 3 3020ND20.9 21.7
trans-1,3-Dichloropropene ug/L 20 97 60-14098 1 3020ND19.3 19.5
Trichloroethene ug/L 20 106 60-140107 1 3020ND21.3 21.5
Trichlorofluoromethane ug/L 20 89 60-14091 3 3020ND17.8 18.3
Vinyl chloride ug/L 20 95 60-14098 3 3020ND18.9 19.5
1,2-Dichloroethane-d4 (S)%99 70-13096
4-Bromofluorobenzene (S)%97 70-13098
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751220
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996001, 92647996003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904012
Associated Lab Samples:92647996001, 92647996003
Matrix:Solid
Analyzed
Benzene ug/kg ND 5.0 01/23/23 16:21
Ethylbenzene ug/kg ND 5.0 01/23/23 16:21
m&p-Xylene ug/kg ND 10.0 01/23/23 16:21
Methyl-tert-butyl ether ug/kg ND 5.0 01/23/23 16:21
o-Xylene ug/kg ND 5.0 01/23/23 16:21
Toluene ug/kg ND 5.0 01/23/23 16:21
Xylene (Total)ug/kg ND 10.0 01/23/23 16:21
1,2-Dichloroethane-d4 (S)%126 70-130 01/23/23 16:21
4-Bromofluorobenzene (S)%103 70-130 01/23/23 16:21
Toluene-d8 (S)%103 70-130 01/23/23 16:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904013LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/kg 500500 100 70-130
Ethylbenzene ug/kg 493500 99 70-130
m&p-Xylene ug/kg 10701000 107 70-130
Methyl-tert-butyl ether ug/kg 510500 102 70-130
o-Xylene ug/kg 507500 101 70-130
Toluene ug/kg 500500 100 70-130
Xylene (Total)ug/kg 15801500 105 70-130
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3904014MATRIX SPIKE SAMPLE:
MSSpike
Result
92647644001
Benzene ug/kg 696595 117 60-145ND
Ethylbenzene ug/kg 679595 113 53-150ND
m&p-Xylene ug/kg 14401190 121 49-156ND
Methyl-tert-butyl ether ug/kg 669595 112 54-133ND
o-Xylene ug/kg 691595 116 54-150ND
Toluene ug/kg 715595 120 52-148ND
Xylene (Total)ug/kg 21301780 119 52-153ND
1,2-Dichloroethane-d4 (S)%113 70-130
4-Bromofluorobenzene (S)%107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3904014MATRIX SPIKE SAMPLE:
MSSpike
Result
92647644001
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92647644002
3904015SAMPLE DUPLICATE:
Benzene ug/kg ND 30ND
Ethylbenzene ug/kg 55.7 4 3058.0
m&p-Xylene ug/kg 187 0 30188
Methyl-tert-butyl ether ug/kg 8.0 2 307.9
o-Xylene ug/kg 320 0 30321
Toluene ug/kg ND 30ND
Xylene (Total)ug/kg 507 0 30509
1,2-Dichloroethane-d4 (S)%105107
4-Bromofluorobenzene (S)%126129
Toluene-d8 (S)%101103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751446
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904958
Associated Lab Samples:92647996002
Matrix:Solid
Analyzed
Benzene ug/kg ND 5.0 01/24/23 23:02
Ethylbenzene ug/kg ND 5.0 01/24/23 23:02
m&p-Xylene ug/kg ND 10.0 01/24/23 23:02
Methyl-tert-butyl ether ug/kg ND 5.0 01/24/23 23:02
o-Xylene ug/kg ND 5.0 01/24/23 23:02
Toluene ug/kg ND 5.0 01/24/23 23:02
Xylene (Total)ug/kg ND 10.0 01/24/23 23:02
1,2-Dichloroethane-d4 (S)%114 70-130 01/24/23 23:02
4-Bromofluorobenzene (S)%103 70-130 01/24/23 23:02
Toluene-d8 (S)%101 70-130 01/24/23 23:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904959LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/kg 493500 99 70-130
Ethylbenzene ug/kg 492500 98 70-130
m&p-Xylene ug/kg 10501000 105 70-130
Methyl-tert-butyl ether ug/kg 516500 103 70-130
o-Xylene ug/kg 511500 102 70-130
Toluene ug/kg 500500 100 70-130
Xylene (Total)ug/kg 15601500 104 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3904960MATRIX SPIKE SAMPLE:
MSSpike
Result
92647971001
Benzene ug/kg 746625 119 60-145ND
Ethylbenzene ug/kg 593625 90 53-15027.5
m&p-Xylene ug/kg 12201240 98 49-156ND
Methyl-tert-butyl ether ug/kg 751625 120 54-133ND
o-Xylene ug/kg 617625 96 54-15017.1
Toluene ug/kg 697625 111 52-148ND
Xylene (Total)ug/kg 18401880 97 52-15317.1
1,2-Dichloroethane-d4 (S)%113 70-130
4-Bromofluorobenzene (S)%124 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3904960MATRIX SPIKE SAMPLE:
MSSpike
Result
92647971001
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92646404001
3904961SAMPLE DUPLICATE:
Benzene ug/kg ND H130ND
Ethylbenzene ug/kg ND H130ND
m&p-Xylene ug/kg ND H130ND
Methyl-tert-butyl ether ug/kg ND H130ND
o-Xylene ug/kg ND H130ND
Toluene ug/kg ND H130ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%109109
4-Bromofluorobenzene (S)%106107
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751259
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904091
Associated Lab Samples:92647996005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 01/24/23 19:33
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 01/24/23 19:33
2,4,6-Trichlorophenol ug/L ND 10.0 01/24/23 19:33
2,4-Dichlorophenol ug/L ND 5.0 01/24/23 19:33
2,4-Dimethylphenol ug/L ND 10.0 01/24/23 19:33
2,4-Dinitrophenol ug/L ND 50.0 01/24/23 19:33
2,4-Dinitrotoluene ug/L ND 5.0 01/24/23 19:33
2,6-Dinitrotoluene ug/L ND 5.0 01/24/23 19:33
2-Chloronaphthalene ug/L ND 5.0 01/24/23 19:33
2-Chlorophenol ug/L ND 5.0 01/24/23 19:33
2-Nitrophenol ug/L ND 5.0 01/24/23 19:33
3,3'-Dichlorobenzidine ug/L ND 10.0 01/24/23 19:33
4,6-Dinitro-2-methylphenol ug/L ND 10.0 01/24/23 19:33
4-Bromophenylphenyl ether ug/L ND 5.0 01/24/23 19:33
4-Chloro-3-methylphenol ug/L ND 5.0 01/24/23 19:33
4-Chlorophenylphenyl ether ug/L ND 5.0 01/24/23 19:33
4-Nitrophenol ug/L ND 10.0 01/24/23 19:33
Acenaphthene ug/L ND 5.0 01/24/23 19:33
Acenaphthylene ug/L ND 5.0 01/24/23 19:33
Anthracene ug/L ND 5.0 01/24/23 19:33
Benzo(a)anthracene ug/L ND 5.0 01/24/23 19:33
Benzo(a)pyrene ug/L ND 5.0 01/24/23 19:33
Benzo(b)fluoranthene ug/L ND 5.0 01/24/23 19:33
Benzo(g,h,i)perylene ug/L ND 5.0 01/24/23 19:33
Benzo(k)fluoranthene ug/L ND 5.0 01/24/23 19:33
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/24/23 19:33
bis(2-Chloroethyl) ether ug/L ND 5.0 01/24/23 19:33
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 01/24/23 19:33
Butylbenzylphthalate ug/L ND 5.0 01/24/23 19:33
Chrysene ug/L ND 5.0 01/24/23 19:33
Di-n-butylphthalate ug/L ND 5.0 01/24/23 19:33
Di-n-octylphthalate ug/L ND 5.0 01/24/23 19:33
Dibenz(a,h)anthracene ug/L ND 5.0 01/24/23 19:33
Diethylphthalate ug/L ND 5.0 01/24/23 19:33
Dimethylphthalate ug/L ND 5.0 01/24/23 19:33
Fluoranthene ug/L ND 5.0 01/24/23 19:33
Fluorene ug/L ND 5.0 01/24/23 19:33
Hexachloro-1,3-butadiene ug/L ND 5.0 01/24/23 19:33
Hexachlorobenzene ug/L ND 5.0 01/24/23 19:33
Hexachlorocyclopentadiene ug/L ND 10.0 01/24/23 19:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904091
Associated Lab Samples:92647996005
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 01/24/23 19:33
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 01/24/23 19:33
Isophorone ug/L ND 10.0 01/24/23 19:33
N-Nitroso-di-n-propylamine ug/L ND 5.0 01/24/23 19:33
N-Nitrosodimethylamine ug/L ND 5.0 01/24/23 19:33
N-Nitrosodiphenylamine ug/L ND 10.0 01/24/23 19:33
Naphthalene ug/L ND 5.0 01/24/23 19:33
Nitrobenzene ug/L ND 5.0 01/24/23 19:33
Pentachlorophenol ug/L ND 10.0 01/24/23 19:33
Phenanthrene ug/L ND 5.0 01/24/23 19:33
Phenol ug/L ND 5.0 01/24/23 19:33
Pyrene ug/L ND 5.0 01/24/23 19:33
2,4,6-Tribromophenol (S)%121 10-137 01/24/23 19:33
2-Fluorobiphenyl (S)%45 15-120 01/24/23 19:33
2-Fluorophenol (S)%58 10-120 01/24/23 19:33
Nitrobenzene-d5 (S)%74 10-120 01/24/23 19:33
Phenol-d6 (S)%51 10-120 01/24/23 19:33
Terphenyl-d14 (S)%131 11-131 01/24/23 19:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904092LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 55.0100 55 44-142
2,2'-Oxybis(1-chloropropane)ug/L 59.5100 60 36-166
2,4,6-Trichlorophenol ug/L 71.3100 71 37-144
2,4-Dichlorophenol ug/L 71.5100 72 1-191
2,4-Dimethylphenol ug/L 94.3100 94 32-119
2,4-Dinitrophenol ug/L 281500 56 1-181
2,4-Dinitrotoluene ug/L 69.1100 69 39-139
2,6-Dinitrotoluene ug/L 72.2100 72 50-158
2-Chloronaphthalene ug/L 67.0100 67 60-118
2-Chlorophenol ug/L 62.1100 62 23-134
2-Nitrophenol ug/L 69.9100 70 29-182
3,3'-Dichlorobenzidine ug/L 151200 76 1-262
4,6-Dinitro-2-methylphenol ug/L 139200 70 1-181
4-Bromophenylphenyl ether ug/L 70.6100 71 53-127
4-Chloro-3-methylphenol ug/L 134200 67 22-147
4-Chlorophenylphenyl ether ug/L 68.1100 68 25-158
4-Nitrophenol ug/L 212500 42 1-132
Acenaphthene ug/L 67.0100 67 47-145
Acenaphthylene ug/L 69.2100 69 33-145
Anthracene ug/L 65.9100 66 1-166
Benzo(a)anthracene ug/L 70.6100 71 33-143
Benzo(a)pyrene ug/L 72.1100 72 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904092LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 71.2100 71 24-159
Benzo(g,h,i)perylene ug/L 70.0100 70 1-219
Benzo(k)fluoranthene ug/L 71.7100 72 11-162
bis(2-Chloroethoxy)methane ug/L 69.4100 69 33-184
bis(2-Chloroethyl) ether ug/L 66.3100 66 12-158
bis(2-Ethylhexyl)phthalate ug/L 79.7100 80 8-158
Butylbenzylphthalate ug/L 81.7100 82 1-152
Chrysene ug/L 67.2100 67 17-168
Di-n-butylphthalate ug/L 77.0100 77 1-118
Di-n-octylphthalate ug/L 82.3100 82 4-146
Dibenz(a,h)anthracene ug/L 72.6100 73 1-227
Diethylphthalate ug/L 72.0100 72 1-114
Dimethylphthalate ug/L 70.9100 71 1-112
Fluoranthene ug/L 70.5100 70 26-137
Fluorene ug/L 69.4100 69 59-121
Hexachloro-1,3-butadiene ug/L 55.4100 55 24-116
Hexachlorobenzene ug/L 68.4100 68 1-152
Hexachlorocyclopentadiene ug/L 64.4100 64 25-150
Hexachloroethane ug/L 41.9100 42 40-113
Indeno(1,2,3-cd)pyrene ug/L 72.3100 72 1-171
Isophorone ug/L 70.7100 71 21-196
N-Nitroso-di-n-propylamine ug/L 74.0100 74 1-230
N-Nitrosodimethylamine ug/L 57.9100 58 25-150
N-Nitrosodiphenylamine ug/L 71.6100 72 25-150
Naphthalene ug/L 61.9100 62 21-133
Nitrobenzene ug/L 62.3100 62 35-180
Pentachlorophenol ug/L 143200 71 14-176
Phenanthrene ug/L 69.1100 69 54-120
Phenol ug/L 43.9100 44 5-112
Pyrene ug/L 69.9100 70 52-115
2,4,6-Tribromophenol (S)%82 10-137
2-Fluorobiphenyl (S)%73 15-120
2-Fluorophenol (S)%55 10-120
Nitrobenzene-d5 (S)%74 10-120
Phenol-d6 (S)%46 10-120
Terphenyl-d14 (S)%76 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3904093MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35773372002
3904094
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M190.9 36 44-14241 12 3090.91.6U 32.9 37.2
2,2'-Oxybis(1-
chloropropane)ug/L 90.9 83 36-16672 14 3090.91.0U 75.4 65.7
2,4,6-Trichlorophenol ug/L R190.9 39 37-14459 41 3090.91.4U 35.2 53.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3904093MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35773372002
3904094
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 90.9 71 1-19184 16 3090.91.3U 64.9 76.3
2,4-Dimethylphenol ug/L 90.9 49 32-11959 19 3090.91.5U 44.5 54.0
2,4-Dinitrophenol ug/L M145501-1810 3045523.6U ND ND
2,4-Dinitrotoluene ug/L 90.9 106 39-139103 3 3090.91.5U 96.5 93.2
2,6-Dinitrotoluene ug/L 90.9 115 50-158110 4 3090.91.6U 104 100
2-Chloronaphthalene ug/L 90.9 83 60-11886 4 3090.91.6U 75.1 78.0
2-Chlorophenol ug/L 90.9 70 23-13475 6 3090.91.1U 63.6 67.9
2-Nitrophenol ug/L 90.9 77 29-18287 12 3090.91.3U 69.8 79.1
3,3'-Dichlorobenzidine ug/L 182 85 1-26287 2 301827.4U 154 157
4,6-Dinitro-2-methylphenol ug/L R1182111-18117 48 301827.1U 19.5 31.8
4-Bromophenylphenyl ether ug/L 90.9 96 53-12799 3 3090.91.6U 87.2 90.1
4-Chloro-3-methylphenol ug/L 182 87 22-14785 2 301823.0U 158 155
4-Chlorophenylphenyl ether ug/L 90.9 96 25-15895 1 3090.91.8U 87.5 86.3
4-Nitrophenol ug/L 455 2 1-1325 304556.0U ND 22.9
Acenaphthene ug/L 90.9 95 47-14599 4 3090.91.8U 86.5 89.6
Acenaphthylene ug/L 90.9 92 33-14596 4 3090.91.8U 83.9 87.2
Anthracene ug/L 90.9 98 1-16698 0 3090.92.1U 89.0 89.1
Benzo(a)anthracene ug/L 90.9 108 33-143107 1 3090.92.4U 98.0 97.3
Benzo(a)pyrene ug/L 90.9 113 17-163109 3 3090.92.5U 102 99.0
Benzo(b)fluoranthene ug/L 90.9 107 24-159100 6 3090.92.4U 97.1 91.3
Benzo(g,h,i)perylene ug/L 90.9 131 1-219128 3 3090.92.6U 119 116
Benzo(k)fluoranthene ug/L 90.9 105 11-162105 1 3090.92.5U 95.7 95.2
bis(2-
Chloroethoxy)methane ug/L 90.9 91 33-18485 6 3090.91.7U 82.5 77.5
bis(2-Chloroethyl) ether ug/L 90.9 97 12-15893 5 3090.91.7U 88.4 84.5
bis(2-Ethylhexyl)phthalate ug/L 90.9 136 8-158134 1 3090.93.4U 123 122
Butylbenzylphthalate ug/L 90.9 133 1-152129 3 3090.92.9U 121 117
Chrysene ug/L 90.9 110 17-168110 0 3090.92.5U 100 100
Di-n-butylphthalate ug/L M190.9 127 1-118120 6 3090.92.0U 115 109
Di-n-octylphthalate ug/L M190.9 153 4-146153 0 3090.93.6U 140 139
Dibenz(a,h)anthracene ug/L 90.9 133 1-227127 5 3090.92.7U 121 115
Diethylphthalate ug/L 90.9 114 1-114109 4 3090.91.9U 103 99.2
Dimethylphthalate ug/L 90.9 109 1-112107 2 3090.91.9U 99.3 97.0
Fluoranthene ug/L 90.9 115 26-137113 2 3090.92.0U 105 103
Fluorene ug/L 90.9 100 59-121101 1 3090.91.9U 91.2 92.1
Hexachloro-1,3-butadiene ug/L M190.9 22 24-11627 22 3090.91.6U 19.8 24.7
Hexachlorobenzene ug/L 90.9 101 1-152104 2 3090.92.0U 92.0 94.1
Hexachlorocyclopentadiene ug/L 90.9 46 25-15049 6 3090.91.4U 42.2 44.8
Hexachloroethane ug/L M190.9 14 40-11315 5 3090.91.3U 12.5 13.2
Indeno(1,2,3-cd)pyrene ug/L 90.9 137 1-171134 2 3090.92.6U 124 122
Isophorone ug/L 90.9 101 21-19695 6 3090.91.5U 92.1 86.6
N-Nitroso-di-n-propylamine ug/L 90.9 104 1-23095 9 3090.91.2U 94.8 86.5
N-Nitrosodimethylamine ug/L 90.9 85 25-15076 11 3090.91.7U 77.1 68.8
N-Nitrosodiphenylamine ug/L 90.9 85 25-15092 7 3090.92.7U 77.7 83.3
Naphthalene ug/L 90.9 53 21-13356 6 3090.91.9U 48.2 51.0
Nitrobenzene ug/L 90.9 84 35-18076 9 3090.91.7U 76.2 69.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3904093MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35773372002
3904094
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M1,R11821114-17620 58 301823.4U 20.0 36.4
Phenanthrene ug/L 90.9 105 54-120105 0 3090.91.8U 95.6 95.8
Phenol ug/L 90.9 41 5-11247 14 3090.91.2U 37.5 43.0
Pyrene ug/L 90.9 100 52-115103 3 3090.92.0U 91.0 93.7
2,4,6-Tribromophenol (S)%70 10-13784
2-Fluorobiphenyl (S)%71 15-12068
2-Fluorophenol (S)%35 10-12045
Nitrobenzene-d5 (S)%101 10-12089
Phenol-d6 (S)%47 10-12051
Terphenyl-d14 (S)%108 11-131104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751606
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3905544
Associated Lab Samples:92647996003
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 327 01/26/23 07:36
1,2-Dichlorobenzene ug/kg ND 327 01/26/23 07:36
1,3-Dichlorobenzene ug/kg ND 327 01/26/23 07:36
1,4-Dichlorobenzene ug/kg ND 327 01/26/23 07:36
1-Methylnaphthalene ug/kg ND 327 01/26/23 07:36
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 01/26/23 07:36
2,4,5-Trichlorophenol ug/kg ND 327 01/26/23 07:36
2,4,6-Trichlorophenol ug/kg ND 327 01/26/23 07:36
2,4-Dichlorophenol ug/kg ND 327 01/26/23 07:36
2,4-Dimethylphenol ug/kg ND 327 01/26/23 07:36
2,4-Dinitrophenol ug/kg ND 1630 01/26/23 07:36
2,4-Dinitrotoluene ug/kg ND 327 01/26/23 07:36
2,6-Dinitrotoluene ug/kg ND 327 01/26/23 07:36
2-Chloronaphthalene ug/kg ND 327 01/26/23 07:36
2-Chlorophenol ug/kg ND 327 01/26/23 07:36
2-Methylnaphthalene ug/kg ND 327 01/26/23 07:36
2-Methylphenol(o-Cresol)ug/kg ND 327 01/26/23 07:36
2-Nitroaniline ug/kg ND 1630 01/26/23 07:36
2-Nitrophenol ug/kg ND 327 01/26/23 07:36
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 01/26/23 07:36
3,3'-Dichlorobenzidine ug/kg ND 653 01/26/23 07:36
3-Nitroaniline ug/kg ND 1630 01/26/23 07:36
4,6-Dinitro-2-methylphenol ug/kg ND 653 01/26/23 07:36
4-Bromophenylphenyl ether ug/kg ND 327 01/26/23 07:36
4-Chloro-3-methylphenol ug/kg ND 653 01/26/23 07:36
4-Chloroaniline ug/kg ND 653 01/26/23 07:36
4-Chlorophenylphenyl ether ug/kg ND 327 01/26/23 07:36
4-Nitroaniline ug/kg ND 653 01/26/23 07:36
4-Nitrophenol ug/kg ND 1630 01/26/23 07:36
Acenaphthene ug/kg ND 327 01/26/23 07:36
Acenaphthylene ug/kg ND 327 01/26/23 07:36
Aniline ug/kg ND 327 01/26/23 07:36
Anthracene ug/kg ND 327 01/26/23 07:36
Benzo(a)anthracene ug/kg ND 327 01/26/23 07:36
Benzo(a)pyrene ug/kg ND 327 01/26/23 07:36
Benzo(b)fluoranthene ug/kg ND 327 01/26/23 07:36
Benzo(g,h,i)perylene ug/kg ND 327 01/26/23 07:36
Benzo(k)fluoranthene ug/kg ND 327 01/26/23 07:36
Benzoic Acid ug/kg ND 1630 01/26/23 07:36
Benzyl alcohol ug/kg ND 653 01/26/23 07:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3905544
Associated Lab Samples:92647996003
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane ug/kg ND 327 01/26/23 07:36
bis(2-Chloroethyl) ether ug/kg ND 327 01/26/23 07:36
bis(2-Ethylhexyl)phthalate ug/kg ND 327 v101/26/23 07:36
Butylbenzylphthalate ug/kg ND 327 01/26/23 07:36
Chrysene ug/kg ND 327 01/26/23 07:36
Di-n-butylphthalate ug/kg ND 327 01/26/23 07:36
Di-n-octylphthalate ug/kg ND 327 01/26/23 07:36
Dibenz(a,h)anthracene ug/kg ND 327 01/26/23 07:36
Dibenzofuran ug/kg ND 327 01/26/23 07:36
Diethylphthalate ug/kg ND 327 01/26/23 07:36
Dimethylphthalate ug/kg ND 327 01/26/23 07:36
Fluoranthene ug/kg ND 327 01/26/23 07:36
Fluorene ug/kg ND 327 01/26/23 07:36
Hexachloro-1,3-butadiene ug/kg ND 327 01/26/23 07:36
Hexachlorobenzene ug/kg ND 327 01/26/23 07:36
Hexachlorocyclopentadiene ug/kg ND 327 v201/26/23 07:36
Hexachloroethane ug/kg ND 327 01/26/23 07:36
Indeno(1,2,3-cd)pyrene ug/kg ND 327 01/26/23 07:36
Isophorone ug/kg ND 327 01/26/23 07:36
N-Nitroso-di-n-propylamine ug/kg ND 327 01/26/23 07:36
N-Nitrosodimethylamine ug/kg ND 327 01/26/23 07:36
N-Nitrosodiphenylamine ug/kg ND 327 01/26/23 07:36
Naphthalene ug/kg ND 327 01/26/23 07:36
Nitrobenzene ug/kg ND 327 01/26/23 07:36
Pentachlorophenol ug/kg ND 653 01/26/23 07:36
Phenanthrene ug/kg ND 327 01/26/23 07:36
Phenol ug/kg ND 327 01/26/23 07:36
Pyrene ug/kg ND 327 01/26/23 07:36
Pyridine ug/kg ND 327 01/26/23 07:36
2,4,6-Tribromophenol (S)%55 10-131 01/26/23 07:36
2-Fluorobiphenyl (S)%54 10-130 01/26/23 07:36
2-Fluorophenol (S)%56 10-130 01/26/23 07:36
Nitrobenzene-d5 (S)%56 10-130 01/26/23 07:36
Phenol-d6 (S)%54 10-130 01/26/23 07:36
Terphenyl-d14 (S)%60 10-130 01/26/23 07:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905545LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11101670 67 43-130
1,2-Dichlorobenzene ug/kg 12601670 76 43-130
1,3-Dichlorobenzene ug/kg 11801670 71 43-130
1,4-Dichlorobenzene ug/kg 12101670 72 44-130
1-Methylnaphthalene ug/kg 13101670 79 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905545LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 11801670 71 29-130
2,4,5-Trichlorophenol ug/kg 12201670 73 47-130
2,4,6-Trichlorophenol ug/kg 13001670 78 47-130
2,4-Dichlorophenol ug/kg 12901670 78 45-130
2,4-Dimethylphenol ug/kg 15401670 92 45-130
2,4-Dinitrophenol ug/kg 66108330 79 27-140
2,4-Dinitrotoluene ug/kg 13601670 81 46-130
2,6-Dinitrotoluene ug/kg 12801670 77 48-130
2-Chloronaphthalene ug/kg 12101670 73 46-130
2-Chlorophenol ug/kg 13201670 79 43-130
2-Methylnaphthalene ug/kg 12401670 75 47-130
2-Methylphenol(o-Cresol)ug/kg 13701670 82 42-130
2-Nitroaniline ug/kg 26603330 80 41-130
2-Nitrophenol ug/kg 13401670 80 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 13301670 80 39-130
3,3'-Dichlorobenzidine ug/kg 26203330 78 41-130
3-Nitroaniline ug/kg 27403330 82 37-130
4,6-Dinitro-2-methylphenol ug/kg 29503330 88 38-141
4-Bromophenylphenyl ether ug/kg 13101670 78 47-130
4-Chloro-3-methylphenol ug/kg 25603330 77 44-130
4-Chloroaniline ug/kg 24603330 74 41-130
4-Chlorophenylphenyl ether ug/kg 12901670 77 45-130
4-Nitroaniline ug/kg 25603330 77 42-130
4-Nitrophenol ug/kg 67608330 81 39-131
Acenaphthene ug/kg 13401670 80 49-130
Acenaphthylene ug/kg 13301670 80 50-130
Aniline ug/kg 11801670 71 38-130
Anthracene ug/kg 13101670 78 49-130
Benzo(a)anthracene ug/kg 15201670 91 51-130
Benzo(a)pyrene ug/kg 17601670 106 51-130
Benzo(b)fluoranthene ug/kg 17501670 105 49-130
Benzo(g,h,i)perylene ug/kg 19201670 115 48-140
Benzo(k)fluoranthene ug/kg 17501670 105 51-130
Benzoic Acid ug/kg 54308330 65 22-130
Benzyl alcohol ug/kg 26503330 80 43-130
bis(2-Chloroethoxy)methane ug/kg 12601670 76 43-130
bis(2-Chloroethyl) ether ug/kg 13301670 80 42-130
bis(2-Ethylhexyl)phthalate ug/kg 1790 v1167010743-130
Butylbenzylphthalate ug/kg 16301670 98 44-131
Chrysene ug/kg 13701670 82 51-130
Di-n-butylphthalate ug/kg 15401670 92 46-130
Di-n-octylphthalate ug/kg 15701670 94 45-130
Dibenz(a,h)anthracene ug/kg 19701670 118 48-130
Dibenzofuran ug/kg 12801670 77 10-130
Diethylphthalate ug/kg 14101670 85 48-130
Dimethylphthalate ug/kg 13301670 80 48-130
Fluoranthene ug/kg 12801670 77 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905545LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13701670 82 48-130
Hexachloro-1,3-butadiene ug/kg 10701670 64 39-130
Hexachlorobenzene ug/kg 13101670 78 47-130
Hexachlorocyclopentadiene ug/kg 983 v316705917-130
Hexachloroethane ug/kg 12901670 78 40-130
Indeno(1,2,3-cd)pyrene ug/kg 19501670 117 50-130
Isophorone ug/kg 12701670 76 41-130
N-Nitroso-di-n-propylamine ug/kg 14101670 85 36-130
N-Nitrosodimethylamine ug/kg 12901670 77 34-130
N-Nitrosodiphenylamine ug/kg 14301670 86 48-130
Naphthalene ug/kg 13001670 78 46-130
Nitrobenzene ug/kg 11801670 71 39-130
Pentachlorophenol ug/kg 24103330 72 42-130
Phenanthrene ug/kg 14101670 85 50-130
Phenol ug/kg 14601670 88 42-130
Pyrene ug/kg 14201670 85 50-130
Pyridine ug/kg 10701670 64 26-130
2,4,6-Tribromophenol (S)%78 10-131
2-Fluorobiphenyl (S)%64 10-130
2-Fluorophenol (S)%70 10-130
Nitrobenzene-d5 (S)%65 10-130
Phenol-d6 (S)%70 10-130
Terphenyl-d14 (S)%70 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3905546MATRIX SPIKE SAMPLE:
MSSpike
Result
92648486001
1,2,4-Trichlorobenzene ug/kg 13002240 58 16-130ND
1,2-Dichlorobenzene ug/kg 13002240 58 19-130ND
1,3-Dichlorobenzene ug/kg 12702240 57 19-130ND
1,4-Dichlorobenzene ug/kg 12902240 58 20-130ND
1-Methylnaphthalene ug/kg 22102240 63 19-130805
2,2'-Oxybis(1-chloropropane)ug/kg 11602240 52 10-130ND
2,4,5-Trichlorophenol ug/kg 13102240 59 19-130ND
2,4,6-Trichlorophenol ug/kg 14002240 63 18-130ND
2,4-Dichlorophenol ug/kg 13102240 59 16-130ND
2,4-Dimethylphenol ug/kg 17002240 76 10-130ND
2,4-Dinitrophenol ug/kg 489011200 44 10-143ND
2,4-Dinitrotoluene ug/kg 15202240 68 19-130ND
2,6-Dinitrotoluene ug/kg 13702240 61 22-130ND
2-Chloronaphthalene ug/kg 13102240 59 18-130ND
2-Chlorophenol ug/kg 13302240 60 20-130ND
2-Methylnaphthalene ug/kg 20802240 56 18-130818
2-Methylphenol(o-Cresol)ug/kg 14302240 64 13-130ND
2-Nitroaniline ug/kg 24204470 54 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3905546MATRIX SPIKE SAMPLE:
MSSpike
Result
92648486001
2-Nitrophenol ug/kg 15402240 69 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 13202240 59 13-130ND
3,3'-Dichlorobenzidine ug/kg 28704470 64 10-130ND
3-Nitroaniline ug/kg 28104470 63 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 29204470 65 10-144ND
4-Bromophenylphenyl ether ug/kg 14502240 65 18-130ND
4-Chloro-3-methylphenol ug/kg 27204470 61 16-130ND
4-Chloroaniline ug/kg 26104470 58 17-130ND
4-Chlorophenylphenyl ether ug/kg 13402240 60 17-130ND
4-Nitroaniline ug/kg 24604470 55 21-130ND
4-Nitrophenol ug/kg 541011200 48 13-131ND
Acenaphthene ug/kg 14802240 66 20-130ND
Acenaphthylene ug/kg 14102240 63 21-130ND
Aniline ug/kg 11302240 51 10-130ND
Anthracene ug/kg 13302240 60 19-130ND
Benzo(a)anthracene ug/kg 15302240 68 17-130ND
Benzo(a)pyrene ug/kg 17802240 80 14-130ND
Benzo(b)fluoranthene ug/kg 17702240 79 11-134ND
Benzo(g,h,i)perylene ug/kg 19102240 85 12-130ND
Benzo(k)fluoranthene ug/kg 17602240 79 15-130ND
Benzoic Acid ug/kg 1820J11200 16 10-130ND
Benzyl alcohol ug/kg 26104470 58 20-130ND
bis(2-Chloroethoxy)methane ug/kg 13702240 61 16-130ND
bis(2-Chloroethyl) ether ug/kg 13702240 61 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 1800 v122408011-130ND
Butylbenzylphthalate ug/kg 17902240 80 10-130ND
Chrysene ug/kg 14402240 64 17-130ND
Di-n-butylphthalate ug/kg 14902240 67 16-130ND
Di-n-octylphthalate ug/kg 17302240 77 16-130ND
Dibenz(a,h)anthracene ug/kg 19702240 88 13-130ND
Dibenzofuran ug/kg 13702240 61 19-130ND
Diethylphthalate ug/kg 15602240 70 22-130ND
Dimethylphthalate ug/kg 15802240 71 23-130ND
Fluoranthene ug/kg 13302240 59 14-130ND
Fluorene ug/kg 15002240 60 19-130ND
Hexachloro-1,3-butadiene ug/kg 12402240 55 12-130ND
Hexachlorobenzene ug/kg 14502240 65 17-130ND
Hexachlorocyclopentadiene ug/kg 1050 v322404710-130ND
Hexachloroethane ug/kg 14302240 64 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 19602240 88 13-130ND
Isophorone ug/kg 12802240 57 17-130ND
N-Nitroso-di-n-propylamine ug/kg 15202240 68 10-130ND
N-Nitrosodimethylamine ug/kg 12502240 56 16-130ND
N-Nitrosodiphenylamine ug/kg 17102240 77 19-130ND
Naphthalene ug/kg 15302240 62 18-130ND
Nitrobenzene ug/kg 11702240 53 15-130ND
Pentachlorophenol ug/kg 26804470 60 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3905546MATRIX SPIKE SAMPLE:
MSSpike
Result
92648486001
Phenanthrene ug/kg 16002240 61 17-130ND
Phenol ug/kg 13702240 61 15-130ND
Pyrene ug/kg 18402240 70 31-130ND
Pyridine ug/kg 9062240 41 10-130ND
2,4,6-Tribromophenol (S)%63 10-131
2-Fluorobiphenyl (S)%48 10-130
2-Fluorophenol (S)%50 10-130
Nitrobenzene-d5 (S)%45 10-130
Phenol-d6 (S)%49 10-130
Terphenyl-d14 (S)%57 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92648486002
3905547SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg 180J 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92648486002
3905547SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND v130ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND v230ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6558
2-Fluorobiphenyl (S)%4741
2-Fluorophenol (S)%6055
Nitrobenzene-d5 (S)%4448
Phenol-d6 (S)%5953
Terphenyl-d14 (S)%6660
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751294
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904200
Associated Lab Samples:92647996003
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 9.9 N201/25/23 15:44
Aliphatic (C19-C36)mg/kg ND 9.9 N201/25/23 15:44
Aromatic (C11-C22)mg/kg ND 9.9 N201/25/23 15:44
1-Chlorooctadecane (S)%67 40-140 01/25/23 15:44
2-Bromonaphthalene (S)%102 40-140 01/25/23 15:44
2-Fluorobiphenyl (S)%88 40-140 01/25/23 15:44
o-Terphenyl (S)%78 40-140 01/25/23 15:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904201LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3904202
Aliphatic (C09-C18)mg/kg ND N29.9 51 40-14058ND 50
Aliphatic (C19-C36)mg/kg ND N213.2 74 40-1408310.9 50
Aromatic (C11-C22)mg/kg 26.0 N228.1 92 40-1409326.0 0 50
1-Chlorooctadecane (S)%74 40-14088
2-Bromonaphthalene (S)%84 40-14085
2-Fluorobiphenyl (S)%82 40-14082
o-Terphenyl (S)%95 40-140101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751291
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3904192
Associated Lab Samples:92647996005
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N201/25/23 09:02
Aliphatic (C19-C36)ug/L ND 100 N201/25/23 09:02
Aromatic (C11-C22)ug/L ND 100 N201/25/23 09:02
1-Chlorooctadecane (S)%53 40-140 01/25/23 09:02
2-Bromonaphthalene (S)%130 40-140 01/25/23 09:02
2-Fluorobiphenyl (S)%118 40-140 01/25/23 09:02
o-Terphenyl (S)%96 40-140 01/25/23 09:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3904193LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3904194
Aliphatic (C09-C18)ug/L 154 N23005140-14053160 4 50
Aliphatic (C19-C36)ug/L 328 N24008240-14084336 2 50
Aromatic (C11-C22)ug/L 828 N28509740-14098835 1 50
1-Chlorooctadecane (S)%62 40-14063
2-Bromonaphthalene (S)%96 40-14098
2-Fluorobiphenyl (S)%93 40-14095
o-Terphenyl (S)%97 40-140101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
750870
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92647996001, 92647996002, 92647996003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92648007001
3902578SAMPLE DUPLICATE:
Percent Moisture %21.1 N212521.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92648005008
3902579SAMPLE DUPLICATE:
Percent Moisture %20.3 N242521.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 65
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 65
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92647996
SANDY CROSS MINI MART
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92647996003 751294 751835KDMADEP EPH MADEP EPH
92647996005 751291 751570MW13MADEP EPH MADEP EPH
92647996005 751259 751500MW13EPA 625.1 EPA 625.1
92647996003 751606 751843KDEPA 3546 EPA 8270E
92647996004 751673MW3SM 6200B
92647996005 751673MW13SM 6200B
92647996006 751673MW14SM 6200B
92647996001 751220 751272GP1EPA 5035A/5030B EPA 8260D
92647996002 751446 751609GD1EPA 5035A/5030B EPA 8260D
92647996003 751220 751272KDEPA 5035A/5030B EPA 8260D
92647996001 750870GP1SW-846
92647996002 750870GD1SW-846
92647996003 750870KDSW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 05:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 65
Page 46 of 65
Page 47 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
February 6, 2023
Bonnie Vang
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: Sandy Cross Min Mart
Client Job Number:
Project Number: 92647996
Laboratory Work Order Number: 23A2336
Enclosed are results of analyses for samples as received by the laboratory on January 24, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 18
Table of Contents
Page 48 of 65
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23A2336-01 5
23A2336-02 6
23A2336-03 7
23A2336-04 8
23A2336-05 9
23A2336-06 10
Sample Preparation Information 11
QC Data 12
Petroleum Hydrocarbons Analyses - VPH 12
B329754 12
B329757 13
Flag/Qualifier Summary 15
Certifications 16
Chain of Custody/Sample Receipt 17
Page 2 of 18
Table of Contents
Page 49 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
2/6/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Bonnie Vang
92647996
23A2336
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Sandy Cross Min Mart
GP1 23A2336-01 Product/Solid MADEP-VPH-Feb
2018 Rev 2.1
GD1 23A2336-02 Product/Solid MADEP-VPH-Feb
2018 Rev 2.1
KD 23A2336-03 Product/Solid MADEP-VPH-Feb
2018 Rev 2.1
MW3 23A2336-04 Water MADEP-VPH-Feb
2018 Rev 2.1
MW13 23A2336-05 Water MADEP-VPH-Feb
2018 Rev 2.1
MW14 23A2336-06 Water MADEP-VPH-Feb
2018 Rev 2.1
[TOC_1]Sample Summary[TOC]
Page 3 of 18
Table of Contents
Page 50 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only ajusted hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.
Analyte & Samples(s) Qualified:
RL-05
C9-C12 Aliphatics
23A2336-04[MW3], 23A2336-06[MW14]
Average of 3 markers passes
Analyte & Samples(s) Qualified:
Z-01
2,2,4-Trimethylpentane
S082556-CCV1, S082815-CCV1
Decane
S082556-CCV1, S082815-CCV1
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 4 of 18
Table of Contents
Page 51 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-01
Field Sample #: GP1
Sample Matrix: Product/Solid
Sampled: 1/18/2023 08:40
[TOC_2]23A2336-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio:
Petroleum Hydrocarbons Analyses - VPH
ND 11 1/27/23 2:52 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 11 1/27/23 2:52 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 11 1/27/23 2:52 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)89.0 1/27/23 2:5270-130
2,5-Dibromotoluene (PID)87.1 1/27/23 2:5270-130
[TOC_1]Sample Results[TOC]
Page 5 of 18
Table of Contents
Page 52 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-02
Field Sample #: GD1
Sample Matrix: Product/Solid
Sampled: 1/18/2023 09:30
[TOC_2]23A2336-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio:
Petroleum Hydrocarbons Analyses - VPH
740 160 1/27/23 3:51 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
20C5-C8 Aliphatics
440 160 1/27/23 3:51 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
20C9-C12 Aliphatics
470 160 1/27/23 3:51 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
20C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)98.7 1/27/23 3:5170-130
2,5-Dibromotoluene (PID)99.0 1/27/23 3:5170-130
Page 6 of 18
Table of Contents
Page 53 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-03
Field Sample #: KD
Sample Matrix: Product/Solid
Sampled: 1/18/2023 09:50
[TOC_2]23A2336-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio:
Petroleum Hydrocarbons Analyses - VPH
16 11 1/27/23 10:44 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
39 11 1/27/23 10:44 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
41 11 1/27/23 10:44 EEHmg/Kg wet 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)113 1/27/23 10:4470-130
2,5-Dibromotoluene (PID)110 1/27/23 10:4470-130
Page 7 of 18
Table of Contents
Page 54 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-04
Field Sample #: MW3
Sample Matrix: Water
Sampled: 1/18/2023 14:00
[TOC_2]23A2336-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
26000 5000 1/27/23 8:46 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
50C5-C8 Aliphatics
ND 5000 1/27/23 8:46 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
50 RL-05C9-C12 Aliphatics
12000 5000 1/27/23 8:46 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
50C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)89.6 1/27/23 8:4670-130
2,5-Dibromotoluene (PID)91.5 1/27/23 8:4670-130
Page 8 of 18
Table of Contents
Page 55 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-05
Field Sample #: MW13
Sample Matrix: Water
Sampled: 1/18/2023 14:20
[TOC_2]23A2336-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 1/27/23 7:17 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 1/27/23 7:17 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 1/27/23 7:17 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)77.7 1/27/23 7:1770-130
2,5-Dibromotoluene (PID)79.3 1/27/23 7:1770-130
Page 9 of 18
Table of Contents
Page 56 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 1/24/2023
Work Order: 23A2336Sample Description:Project Location: Sandy Cross Min Mart
Sample ID: 23A2336-06
Field Sample #: MW14
Sample Matrix: Water
Sampled: 1/18/2023 14:40
[TOC_2]23A2336-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
5200 2500 1/27/23 9:16 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
25C5-C8 Aliphatics
ND 2500 1/27/23 9:16 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
25 RL-05C9-C12 Aliphatics
4500 2500 1/27/23 9:16 EEHg/L 1/26/23MADEP-VPH-Feb 2018
Rev 2.1
25C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)88.3 1/27/23 9:1670-130
2,5-Dibromotoluene (PID)92.4 1/27/23 9:1670-130
Page 10 of 18
Table of Contents
Page 57 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B329754 01/26/238.81 10.023A2336-01 [GP1]
B329754 01/26/2312.2 10.023A2336-02 [GD1]
B329754 01/26/239.08 10.023A2336-03 [KD]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B329757 01/26/230.1 5.0023A2336-04 [MW3]
B329757 01/26/2355.0023A2336-05 [MW13]
B329757 01/26/230.2 5.0023A2336-06 [MW14]
[TOC_1]Sample Preparation Information[TOC]
Page 11 of 18
Table of Contents
Page 58 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B329754 - MA VPH
[TOC_3]B329754[TOC]
Blank (B329754-BLK1) Prepared: 01/26/23 Analyzed: 01/27/23
C5-C8 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)82.833.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)84.233.7
LCS (B329754-BS1) Prepared: 01/26/23 Analyzed: 01/27/23
C9-C10 Aromatics mg/Kg wet10 2.50 70-13094.42.36
Benzene mg/Kg wet0.050 2.50 70-1301132.81
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301112.78
Decane mg/Kg wet0.050 2.50 70-13087.42.19
Ethylbenzene mg/Kg wet0.050 2.50 70-1301082.71
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301062.66
2-Methylpentane mg/Kg wet0.050 2.50 70-1301263.14
Naphthalene mg/Kg wet0.50 2.50 70-13097.62.44
Nonane mg/Kg wet0.050 2.50 30-1301122.80
Pentane mg/Kg wet0.050 2.50 70-1301283.21
Toluene mg/Kg wet0.050 2.50 70-1301092.73
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301052.62
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-1301092.72
m+p Xylene mg/Kg wet0.10 5.00 70-1301075.35
o-Xylene mg/Kg wet0.050 2.50 70-1301072.67
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)92.036.8
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)92.537.0
LCS Dup (B329754-BSD1) Prepared: 01/26/23 Analyzed: 01/27/23
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130105 10.42.62
Benzene mg/Kg wet0.050 2.50 2570-130107 4.822.68
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130108 3.292.69
Decane mg/Kg wet0.050 2.50 2570-13084.5 3.462.11
Ethylbenzene mg/Kg wet0.050 2.50 2570-130102 6.032.55
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130102 4.072.55
2-Methylpentane mg/Kg wet0.050 2.50 2570-130119 5.132.98
Naphthalene mg/Kg wet0.50 2.50 2570-13091.1 6.962.28
Nonane mg/Kg wet0.050 2.50 2530-130109 2.592.73
Pentane mg/Kg wet0.050 2.50 2570-130121 5.973.02
Toluene mg/Kg wet0.050 2.50 2570-130104 5.262.59
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-13097.5 7.222.44
[TOC_1]QC Data[TOC]
Page 12 of 18
Table of Contents
Page 59 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B329754 - MA VPH
LCS Dup (B329754-BSD1) Prepared: 01/26/23 Analyzed: 01/27/23
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-130104 4.942.59
m+p Xylene mg/Kg wet0.10 5.00 2570-130101 6.115.04
o-Xylene mg/Kg wet0.050 2.50 2570-13099.8 6.902.50
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.337.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)94.737.9
Batch B329757 - MA VPH
[TOC_3]B329757[TOC]
Blank (B329757-BLK1) Prepared: 01/26/23 Analyzed: 01/27/23
C5-C8 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)89.435.8
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)89.835.9
LCS (B329757-BS1) Prepared & Analyzed: 01/26/23
C9-C10 Aromatics g/L100 50.0 70-13095.347.6
Benzene g/L1.0 50.0 70-13010150.3
Butylcyclohexane g/L1.0 50.0 70-13010452.2
Decane g/L1.0 50.0 70-13079.339.6
Ethylbenzene g/L1.0 50.0 70-13098.949.4
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 70-13010150.5
2-Methylpentane g/L1.0 50.0 70-13010653.0
Naphthalene g/L5.0 50.0 70-13088.944.5
Nonane g/L1.0 50.0 70-13010753.3
Pentane g/L1.0 50.0 70-13010954.4
Toluene g/L1.0 50.0 70-13098.749.4
1,2,4-Trimethylbenzene g/L1.0 50.0 70-13095.347.6
2,2,4-Trimethylpentane g/L1.0 50.0 70-13089.744.9
m+p Xylene g/L2.0 100 70-13098.898.8
o-Xylene g/L1.0 50.0 70-13010050.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)89.735.9
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)89.435.8
Page 13 of 18
Table of Contents
Page 60 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B329757 - MA VPH
LCS Dup (B329757-BSD1) Prepared & Analyzed: 01/26/23
C9-C10 Aromatics g/L100 50.0 2570-13094.4 0.87147.2
Benzene g/L1.0 50.0 2570-130101 0.27450.4
Butylcyclohexane g/L1.0 50.0 2570-130104 0.10752.2
Decane g/L1.0 50.0 2570-13078.4 1.1539.2
Ethylbenzene g/L1.0 50.0 2570-13098.2 0.67449.1
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 2570-13099.5 1.4849.8
2-Methylpentane g/L1.0 50.0 2570-130106 0.41652.8
Naphthalene g/L5.0 50.0 2570-13086.6 2.6243.3
Nonane g/L1.0 50.0 2570-130105 1.2452.6
Pentane g/L1.0 50.0 2570-130108 0.31054.2
Toluene g/L1.0 50.0 2570-13098.4 0.28849.2
1,2,4-Trimethylbenzene g/L1.0 50.0 2570-13094.4 0.87147.2
2,2,4-Trimethylpentane g/L1.0 50.0 2570-13090.7 1.0945.3
m+p Xylene g/L2.0 100 2570-13097.9 0.85097.9
o-Xylene g/L1.0 50.0 2570-13098.5 1.7349.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)88.535.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)90.136.1
Page 14 of 18
Table of Contents
Page 61 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.RL-05
Average of 3 markers passesZ-01
[TOC_1]Flag/Qualifier Summary[TOC]
Page 15 of 18
Table of Contents
Page 62 of 65
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
Page 16 of 18
Table of Contents
Page 63 of 65
Page 17 of 18
Table of Contents
Page 64 of 65
Page 18 of 18
Table of Contents
Page 65 of 65

APPENDIX B

WELL CONSTRUCTION RECORDS

1215(6,'(17,$/:(//&216758&7,215(&25'
1RUWK&DUROLQD'HSDUWPHQWRI(QYLURQPHQWDQG1DWXUDO5HVRXUFHV'LYLVLRQRI:DWHU4XDOLW\
:(//&2175$&725&(57,),&$7,21BBBBBBBBBBBBBBBBBBBBBBBBBBB
:(//&2175$&725
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
:HOO&RQWUDFWRU,QGLYLGXDO1DPH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
:HOO&RQWUDFWRU&RPSDQ\1DPH
675((7$''5(66 BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ 6WDWH=LS&RGH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
$UHDFRGH 3KRQHQXPEHU
:(//,1)250$7,21
6,7(:(//,'LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
67$7(:(//3(50,7LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBB
':4RU27+(53(50,7LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBB
:(//86(&KHFN$SSOLFDEOH%R[0RQLWRULQJ ട 0XQLFLSDO3XEOLF ട
,QGXVWULDO&RPPHUFLDOട $JULFXOWXUDOട 5HFRYHU\ട,QMHFWLRQ ട
,UULJDWLRQട2WKHUടOLVWXVHBBBBBBBBBBBBBBBBBBBBBBBBBBBB
'$7('5,//('BBBBBBBBBBBBBBBBBBBBB
7,0(&203/(7('BBBBBBBBBBBBBBBBBB$0 ട30ട
:(///2&$7,21
&,7<BBBBBBBBBBBBBBBBBBBBBBBB&2817<BBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
6WUHHW1DPH1XPEHUV&RPPXQLW\6XEGLYLVLRQ/RW1R3DUFHO=LS&RGH
7232*5$3+,&/$1'6(77,1*
ട6ORSHട9DOOH\ട)ODWട5LGJHട2WKHUBBBBBBBBBBBBBBBBBB
FKHFNDSSURSULDWHER[
/$7,78'( BBBBBBBBBBBBBBBBBB
/21*,78'(BBBBBBBBBBBBBBBBBBB
/DWLWXGHORQJLWXGHVRXUFHട*36ട7RSRJUDSKLFPDS
ORFDWLRQRIZHOOPXVWEHVKRZQRQD86*6WRSRPDSDQG
DWWDFKHGWRWKLVIRUPLIQRWXVLQJ*36
)$&,/,7<LVWKHQDPHRIWKHEXVLQHVVZKHUHWKHZHOOLVORFDWHG
)$&,/,7<,'LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
1$0(2))$&,/,7<BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
675((7$''5(66BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ6WDWH=LS&RGH
&217$&73(5621BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
0$,/,1*$''5(66BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ6WDWH=LS&RGH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
$UHDFRGH  3KRQHQXPEHU
:(//'(7$,/6
D727$/'(37+BBBBBBBBBBBBBBBBBBB
E'2(6:(//5(3/$&((;,67,1*:(//"<(6ട12ട
F:$7(5/(9(/%HORZ7RSRI&DVLQJBBBBBBBBBBBB)7
8VH³´LI$ERYH7RSRI&DVLQJ
G7232)&$6,1*,6BBBBBBBBBB)7$ERYH/DQG6XUIDFH


7RSRIFDVLQJWHUPLQDWHGDWRUEHORZODQGVXUIDFHPD\UHTXLUH
DYDULDQFHLQDFFRUGDQFHZLWK$1&$&&
H<,(/'JSPBBBBBBBBBBB0(7+2'2)7(67BBBBBBBBBBBBBB
I',6,1)(&7,217\SHBBBBBBBBBBBBBB$PRXQWBBBBBBBBBBBBB
J:$7(5=21(6GHSWK
)URPBBBBBBB7RBBBBBBB )URPBBBBBBB7RBBBBBBB
)URPBBBBBBB7RBBBBBBB)URPBBBBBBB7RBBBBBBB
)URPBBBBBBB7RBBBBBBB)URPBBBBBBB7RBBBBBBB
&$6,1*7KLFNQHVV
'HSWK 'LDPHWHU:HLJKW0DWHULDO
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
*5287 'HSWK0DWHULDO0HWKRG
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
6&5((1 'HSWK'LDPHWHU6ORW6L]H0DWHULDO
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
6$1'*5$9(/3$&.
'HSWK6L]H 0DWHULDO
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
'5,//,1*/2*
)URP 7R)RUPDWLRQ'HVFULSWLRQ
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
5(0$5.6
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
,'2+(5(%<&(57,)<7+$77+,6:(//:$6&216758&7(',1$&&25'$1&(:,7+
$1&$&&:(//&216758&7,2167$1'$5'6$1'7+$7$&23<2)7+,6
5(&25'+$6%((13529,'('727+(:(//2:1(5
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
6,*1$785(2)&(57,),(':(//&2175$&725'$7(
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
35,17('1$0(2)3(5621&216758&7,1*7+(:(//
6XEPLWWKHRULJLQDOWRWKH'LYLVLRQRI:DWHU4XDOLW\ZLWKLQGD\V$WWQ,QIRUPDWLRQ0JW
0DLO6HUYLFH&HQWHU±5DOHLJK1& 3KRQH1RH[W)RUP*:E
5HY
0D\EHLQGHJUHHV
PLQXWHVVHFRQGVRU
LQDGHFLPDOIRUPDW
3426
Henry Nemargut
Henry Nemargut Engineering Services
2211 Chestnut Street
Wilmington NC 28405
910 762-5475
MW-13
X
1/18/2023
11:00
Burlington Alamance
2078 N. NC 49 Highway
XX XX
36.138515
-79.354175
X
00-0-0000024196
Sandy Cross Mini Mart
2078 N NC Highway 49
Burlington NC 27217
Ossama Touma
2073 N NC Hwy 49
Burlington NC 27217
336 577-5277
14'
X
4.82'
0
0'4'2"Sch 40 PVC
0'3'Portland Pour
3'4'Bentonite Pour
4'14'2 0.01 PVC
4'14'#2 Filter Sand
0'2'orange-red, Silt w/clay
2'4'red-gray, Clay w/silt
4'12'beige, Silt w/sand & trace clay
12' 15'beige, Silt w/sand (weathered rock)
HENRY NEMARGUT 2/14/2023
1215(6,'(17,$/:(//&216758&7,215(&25'
1RUWK&DUROLQD'HSDUWPHQWRI(QYLURQPHQWDQG1DWXUDO5HVRXUFHV'LYLVLRQRI:DWHU4XDOLW\
:(//&2175$&725&(57,),&$7,21BBBBBBBBBBBBBBBBBBBBBBBBBBB
:(//&2175$&725
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
:HOO&RQWUDFWRU,QGLYLGXDO1DPH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
:HOO&RQWUDFWRU&RPSDQ\1DPH
675((7$''5(66 BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ 6WDWH=LS&RGH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
$UHDFRGH 3KRQHQXPEHU
:(//,1)250$7,21
6,7(:(//,'LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
67$7(:(//3(50,7LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBB
':4RU27+(53(50,7LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBB
:(//86(&KHFN$SSOLFDEOH%R[0RQLWRULQJ ട 0XQLFLSDO3XEOLF ട
,QGXVWULDO&RPPHUFLDOട $JULFXOWXUDOട 5HFRYHU\ട,QMHFWLRQ ട
,UULJDWLRQട2WKHUടOLVWXVHBBBBBBBBBBBBBBBBBBBBBBBBBBBB
'$7('5,//('BBBBBBBBBBBBBBBBBBBBB
7,0(&203/(7('BBBBBBBBBBBBBBBBBB$0 ട30ട
:(///2&$7,21
&,7<BBBBBBBBBBBBBBBBBBBBBBBB&2817<BBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
6WUHHW1DPH1XPEHUV&RPPXQLW\6XEGLYLVLRQ/RW1R3DUFHO=LS&RGH
7232*5$3+,&/$1'6(77,1*
ട6ORSHട9DOOH\ട)ODWട5LGJHട2WKHUBBBBBBBBBBBBBBBBBB
FKHFNDSSURSULDWHER[
/$7,78'( BBBBBBBBBBBBBBBBBB
/21*,78'(BBBBBBBBBBBBBBBBBBB
/DWLWXGHORQJLWXGHVRXUFHട*36ട7RSRJUDSKLFPDS
ORFDWLRQRIZHOOPXVWEHVKRZQRQD86*6WRSRPDSDQG
DWWDFKHGWRWKLVIRUPLIQRWXVLQJ*36
)$&,/,7<LVWKHQDPHRIWKHEXVLQHVVZKHUHWKHZHOOLVORFDWHG
)$&,/,7<,'LIDSSOLFDEOHBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
1$0(2))$&,/,7<BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
675((7$''5(66BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ6WDWH=LS&RGH
&217$&73(5621BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
0$,/,1*$''5(66BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
&LW\RU7RZQ6WDWH=LS&RGH
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
$UHDFRGH  3KRQHQXPEHU
:(//'(7$,/6
D727$/'(37+BBBBBBBBBBBBBBBBBBB
E'2(6:(//5(3/$&((;,67,1*:(//"<(6ട12ട
F:$7(5/(9(/%HORZ7RSRI&DVLQJBBBBBBBBBBBB)7
8VH³´LI$ERYH7RSRI&DVLQJ
G7232)&$6,1*,6BBBBBBBBBB)7$ERYH/DQG6XUIDFH


7RSRIFDVLQJWHUPLQDWHGDWRUEHORZODQGVXUIDFHPD\UHTXLUH
DYDULDQFHLQDFFRUGDQFHZLWK$1&$&&
H<,(/'JSPBBBBBBBBBBB0(7+2'2)7(67BBBBBBBBBBBBBB
I',6,1)(&7,217\SHBBBBBBBBBBBBBB$PRXQWBBBBBBBBBBBBB
J:$7(5=21(6GHSWK
)URPBBBBBBB7RBBBBBBB )URPBBBBBBB7RBBBBBBB
)URPBBBBBBB7RBBBBBBB)URPBBBBBBB7RBBBBBBB
)URPBBBBBBB7RBBBBBBB)URPBBBBBBB7RBBBBBBB
&$6,1*7KLFNQHVV
'HSWK 'LDPHWHU:HLJKW0DWHULDO
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
*5287 'HSWK0DWHULDO0HWKRG
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBBBB
6&5((1 'HSWK'LDPHWHU6ORW6L]H0DWHULDO
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
)URPBBBBBBB7RBBBBBBB)WBBBBBBLQBBBBBBLQBBBBBBBBB
6$1'*5$9(/3$&.
'HSWK6L]H 0DWHULDO
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
)URPBBBBBBBB7RBBBBBBB)WBBBBBBBBBBBBBBBBBBBBBBBB
'5,//,1*/2*
)URP 7R)RUPDWLRQ'HVFULSWLRQ
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
5(0$5.6
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
,'2+(5(%<&(57,)<7+$77+,6:(//:$6&216758&7(',1$&&25'$1&(:,7+
$1&$&&:(//&216758&7,2167$1'$5'6$1'7+$7$&23<2)7+,6
5(&25'+$6%((13529,'('727+(:(//2:1(5
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
6,*1$785(2)&(57,),(':(//&2175$&725'$7(
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
35,17('1$0(2)3(5621&216758&7,1*7+(:(//
6XEPLWWKHRULJLQDOWRWKH'LYLVLRQRI:DWHU4XDOLW\ZLWKLQGD\V$WWQ,QIRUPDWLRQ0JW
0DLO6HUYLFH&HQWHU±5DOHLJK1& 3KRQH1RH[W)RUP*:E
5HY
0D\EHLQGHJUHHV
PLQXWHVVHFRQGVRU
LQDGHFLPDOIRUPDW
3426
Henry Nemargut
Henry Nemargut Engineering Services
2211 Chestnut Street
Wilmington NC 28405
910 762-5475
MW-14
X
1/18/2023
1:00 xx
Burlington Alamance
2078 N. NC 49 Highway
XX XX
36.138515
-79.354175
X
00-0-0000024196
Sandy Cross Mini Mart
2078 N NC Highway 49
Burlington NC 27217
Ossama Touma
2073 N NC Hwy 49
Burlington NC 27217
336 577-5277
11'
X
6.53'
0
0'3'2"Sch 40 PVC
0'2'Portland Pour
2'3'Bentonite Pour
3'11'2 0.01 PVC
3'11'#2 Filter Sand
0'7'red-brown, Clay w/silt (fill)
7'10'gray, Clay w/silt
10' 11'gray, Silt w/sand (weathered rock)
auger refusal @ 11'
HENRY NEMARGUT 2/14/2023