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HomeMy WebLinkAboutWS-6406_24174_CA_LAB_20220504  Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   5/16/2022 Withers & Ravenel Liz Allyn 115 Mackenan Dr. BUILDING 117 Cary, NC, 27511 Ref: Analytical Testing Lab Report Number: 22-126-0010 Client Project Description: Caraway Grocery 02172214.23 Dear Liz Allyn: Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/6/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Angela D Overcash Senior Project Manager Page 1 of 77 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202237735State ProgramNorth Carolina 12/31/2022402State ProgramNorth Carolina 07/31/202299012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/22-126-0010 Page 2 of 77 Report Number: Sample Summary Table Client Project Description: 22-126-0010 Caraway Grocery 02172214.23 Lab No Client Sample ID Matrix Date Collected Date Received 05/04/2022 10:20Aqueous 89248 MW-1A 05/06/2022 14:25 05/04/2022 10:05Aqueous 89249 MW-3 05/06/2022 14:25 05/04/2022 09:45Aqueous 89250 MW-4 05/06/2022 14:25 05/04/2022 09:30Aqueous 89251 MW-5 05/06/2022 14:25 05/04/2022 09:05Aqueous 89252 MW-6 05/06/2022 14:25 05/04/2022 08:50Aqueous 89253 MW-10 05/06/2022 14:25 05/04/2022 08:20Aqueous 89254 MW-12 05/06/2022 14:25 05/04/2022 08:35Aqueous 89255 MW-12D 05/06/2022 14:25 05/04/2022 08:05Aqueous 89256 MW-13 05/06/2022 14:25 05/03/2022 15:45Aqueous 89257 MW-15 05/06/2022 14:25 05/03/2022 16:00Aqueous 89258 MW-16 05/06/2022 14:25 05/04/2022 10:30Aqueous 89259 FB 05/06/2022 14:25 05/04/2022 10:45Aqueous 89260 SW-1 05/06/2022 14:25 05/04/2022 11:00Aqueous 89261 SW-7 05/06/2022 14:25 05/04/2022 11:15Aqueous 89262 SW-8 05/06/2022 14:25 Page 3 of 77 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 22-126-0010 Report Limit Project:Caraway Grocery V 89248MW-1A 2.08 05/13/2022 04:256200BDi-Isopropyl Ether (DIPE)µg/L 0.500 1.15 05/13/2022 04:256200BMethyl tert-butyl ether (MTBE)µg/L 1.00 V 89249MW-3 267 05/13/2022 21:106200BBenzeneµg/L 50.0 3.37 05/13/2022 07:186200Bn-Butylbenzene µg/L 0.500 7.78 05/13/2022 07:186200Bsec-Butyl benzene µg/L 0.500 2.26 05/13/2022 07:186200Btert-Butyl benzene µg/L 2.00 10.0 05/13/2022 07:186200BDi-Isopropyl Ether (DIPE)µg/L 0.500 8.28 05/13/2022 07:186200BEthylbenzeneµg/L 0.500 21.5 05/13/2022 07:186200BIsopropylbenzeneµg/L 0.500 1.39 05/13/2022 07:186200B4-Isopropyl toluene µg/L 0.500 13.3 05/13/2022 07:186200BMethyl tert-butyl ether (MTBE)µg/L 1.00 98.4 05/13/2022 07:186200BNaphthaleneµg/L 1.00 31.2 05/13/2022 07:186200Bn-Propylbenzene µg/L 0.500 6.81 05/13/2022 07:186200BTolueneµg/L 0.500 47.9 05/13/2022 07:186200B1,2,4-Trimethylbenzene µg/L 0.500 18.6 05/13/2022 07:186200B1,3,5-Trimethylbenzene µg/L 0.500 4.33 05/13/2022 07:186200Bo-Xylene µg/L 0.500 56.9 05/13/2022 07:186200Bm,p-Xylene µg/L 1.00 61.2 05/13/2022 07:186200BXylene (Total)µg/L 0.500 V 89250MW-4 2100 05/13/2022 21:346200BBenzeneµg/L 50.0 29.2 05/13/2022 07:426200Bn-Butylbenzene µg/L 5.00 23.2 05/13/2022 07:426200Bsec-Butyl benzene µg/L 5.00 8.46 05/13/2022 07:426200BDi-Isopropyl Ether (DIPE)µg/L 5.00 2250 05/13/2022 21:346200BEthylbenzeneµg/L 50.0 160 05/13/2022 07:426200BIsopropylbenzeneµg/L 5.00 12.1 05/13/2022 07:426200B4-Isopropyl toluene µg/L 5.00 23.5 05/13/2022 07:426200BMethyl tert-butyl ether (MTBE)µg/L 10.0 480 05/13/2022 07:426200BNaphthaleneµg/L 10.0 368 05/13/2022 07:426200Bn-Propylbenzene µg/L 5.00 886 05/13/2022 07:426200BTolueneµg/L 5.00 1480 05/13/2022 21:346200B1,2,4-Trimethylbenzene µg/L 50.0 280 05/13/2022 07:426200B1,3,5-Trimethylbenzene µg/L 5.00 593 05/13/2022 07:426200Bo-Xylene µg/L 5.00 4040 05/13/2022 21:346200Bm,p-Xylene µg/L 100 Page 4 of 77 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 22-126-0010 Report Limit Project:Caraway Grocery V 89250MW-4 4630 05/13/2022 07:426200BXylene (Total)µg/L 5.00 V 89251MW-5 817 05/13/2022 21:596200BBenzeneµg/L 50.0 33.5 05/13/2022 06:536200Bn-Butylbenzene µg/L 0.500 17.9 05/13/2022 06:536200Bsec-Butyl benzene µg/L 0.500 2.85 05/13/2022 06:536200BDi-Isopropyl Ether (DIPE)µg/L 0.500 1.59 05/13/2022 06:536200B1,2-Dibromoethane µg/L 0.500 5.88 05/13/2022 06:536200B1,2-Dichloroethane µg/L 0.500 1660 05/13/2022 21:596200BEthylbenzeneµg/L 50.0 6.12 05/13/2022 06:536200B2-Hexanone µg/L 1.00 115 05/13/2022 21:596200BIsopropylbenzeneµg/L 50.0 6.71 05/13/2022 06:536200B4-Isopropyl toluene µg/L 0.500 214 05/13/2022 21:596200BNaphthaleneµg/L 100 232 05/13/2022 21:596200Bn-Propylbenzene µg/L 50.0 2270 05/13/2022 21:596200BTolueneµg/L 50.0 1320 05/13/2022 21:596200B1,2,4-Trimethylbenzene µg/L 50.0 288 05/13/2022 21:596200B1,3,5-Trimethylbenzene µg/L 50.0 1600 05/13/2022 21:596200Bo-Xylene µg/L 50.0 4910 05/13/2022 21:596200Bm,p-Xylene µg/L 100 6510 05/13/2022 21:596200BXylene (Total)µg/L 50.0 V 89254MW-12 4390 05/13/2022 20:456200BBenzeneµg/L 500 80.3 05/13/2022 08:076200Bn-Butylbenzene µg/L 5.00 55.0 05/13/2022 08:076200Bsec-Butyl benzene µg/L 5.00 11.0 05/13/2022 08:076200BDi-Isopropyl Ether (DIPE)µg/L 5.00 3790 05/13/2022 20:456200BEthylbenzeneµg/L 500 11.7 05/13/2022 08:076200B2-Hexanone µg/L 10.0 273 05/13/2022 08:076200BIsopropylbenzeneµg/L 5.00 27.1 05/13/2022 08:076200B4-Isopropyl toluene µg/L 5.00 106 05/13/2022 08:076200B4-Methyl-2-Pentanone µg/L 10.0 711 05/13/2022 08:076200BNaphthaleneµg/L 10.0 722 05/13/2022 08:076200Bn-Propylbenzene µg/L 5.00 539 05/13/2022 08:076200BTolueneµg/L 5.00 3030 05/13/2022 20:456200B1,2,4-Trimethylbenzene µg/L 500 908 05/13/2022 20:456200B1,3,5-Trimethylbenzene µg/L 500 1720 05/13/2022 20:456200Bo-Xylene µg/L 500 Page 5 of 77 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 22-126-0010 Report Limit Project:Caraway Grocery V 89254MW-12 8080 05/13/2022 20:456200Bm,p-Xylene µg/L 1000 9800 05/13/2022 20:456200BXylene (Total)µg/L 500 V 89255MW-12D 7.47 05/13/2022 05:396200BDi-Isopropyl Ether (DIPE)µg/L 0.500 18.7 05/13/2022 05:396200BMethyl tert-butyl ether (MTBE)µg/L 1.00 V 89256MW-13 348 05/13/2022 06:046200BEthanolµg/L 200 V 89257MW-15 2.60 05/13/2022 06:296200Bsec-Butyl benzene µg/L 0.500 1.78 05/13/2022 06:296200BIsopropylbenzeneµg/L 0.500 V 89258MW-16 40.2 05/13/2022 04:016200BBenzeneµg/L 0.500 1.30 05/13/2022 04:016200BDi-Isopropyl Ether (DIPE)µg/L 0.500 1.22 05/13/2022 04:016200B1,2-Dichloroethane µg/L 0.500 19.0 05/13/2022 04:016200BEthylbenzeneµg/L 0.500 2.13 05/13/2022 04:016200BIsopropylbenzeneµg/L 0.500 2.13 05/13/2022 04:016200BNaphthaleneµg/L 1.00 4.26 05/13/2022 04:016200Bn-Propylbenzene µg/L 0.500 2.60 05/13/2022 04:016200BTolueneµg/L 0.500 11.1 05/13/2022 04:016200B1,2,4-Trimethylbenzene µg/L 0.500 1.95 05/13/2022 04:016200B1,3,5-Trimethylbenzene µg/L 0.500 1.36 05/13/2022 04:016200Bo-Xylene µg/L 0.500 18.6 05/13/2022 04:016200Bm,p-Xylene µg/L 1.00 20.0 05/13/2022 04:016200BXylene (Total)µg/L 0.500 V 89260SW-1 0.682 05/13/2022 02:476200BChloroformµg/L 0.500 Page 6 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-1A 89248 Matrix: 5/4/2022 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 04:25 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 04:25 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 04:25 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 04:25 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 7 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-1A 89248 Matrix: 5/4/2022 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 04:25 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 04:25 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 04:25 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 04:25 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 04:25 6200BJLB 2.08 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 04:25 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 04:25 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 04:25 6200BJLB 1.15 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 04:25 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 8 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-1A 89248 Matrix: 5/4/2022 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 04:25 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 04:25 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 04:25 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 04:25 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 9 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-1A 89248 Matrix: 5/4/2022 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 04:25 6200B Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/13/22 04:251 JLB V18665 Surrogate: Dibromofluoromethane 104 Limits: 70-130%05/13/22 04:251 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%05/13/22 04:251 JLB V18665 Surrogate: Toluene-d8 100 Limits: 70-130%05/13/22 04:251 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 10 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-3 89249 Matrix: 5/4/2022 10:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 07:18 6200BJLB 267 µg/L 50.0Benzene 100 05/13/22 21:10 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 07:18 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 07:18 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 07:18 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 07:18 6200BJLB 3.37 µg/L 0.500n-Butylbenzene 1 05/13/22 07:18 6200BJLB 7.78 µg/L 0.500sec-Butyl benzene 1 05/13/22 07:18 6200BJLB 2.26 µg/L 2.00tert-Butyl benzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 07:18 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 07:18 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 07:18 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 11 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-3 89249 Matrix: 5/4/2022 10:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 07:18 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 07:18 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 07:18 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 07:18 6200BJLB 8.28 µg/L 0.500Ethylbenzene 1 05/13/22 07:18 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 07:18 6200BJLB 10.0 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 07:18 6200BJLB 21.5 µg/L 0.500Isopropylbenzene 1 05/13/22 07:18 6200BJLB 1.39 µg/L 0.5004-Isopropyl toluene 1 05/13/22 07:18 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 07:18 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 07:18 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 07:18 6200BJLB 13.3 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 07:18 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 12 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-3 89249 Matrix: 5/4/2022 10:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 07:18 6200BJLB 98.4 µg/L 1.00Naphthalene 1 05/13/22 07:18 6200BJLB 31.2 µg/L 0.500n-Propylbenzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 07:18 6200BJLB 6.81 µg/L 0.500Toluene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 07:18 6200BJLB 47.9 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 07:18 6200BJLB 18.6 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 07:18 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 07:18 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 07:18 6200BJLB 56.9 µg/L 1.00m,p-Xylene 1 05/13/22 07:18 6200BJLB 4.33 µg/L 0.500o-Xylene 1 05/13/22 07:18 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 13 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-3 89249 Matrix: 5/4/2022 10:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 61.2 µg/L 0.500Xylene (Total)1 05/13/22 07:18 6200B Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%05/13/22 07:181 JLB V18665 Surrogate: Dibromofluoromethane 94.0 Limits: 70-130%05/13/22 07:181 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 85.4 Limits: 70-130%05/13/22 07:181 JLB V18665 Surrogate: Toluene-d8 96.6 Limits: 70-130%05/13/22 07:181 JLB V18665 Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/13/22 21:10100 JLB V18682 Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%05/13/22 21:10100 JLB V18682 Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%05/13/22 21:10100 JLB V18682 Surrogate: Toluene-d8 99.6 Limits: 70-130%05/13/22 21:10100 JLB V18682 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 14 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-4 89250 Matrix: 5/4/2022 9:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <100 µg/L 100Acetone 10 05/13/22 07:42 6200BJLB 2100 µg/L 50.0Benzene 100 05/13/22 21:34 6200BJLB <5.00 µg/L 5.00Bromobenzene 10 05/13/22 07:42 6200BJLB <10.0 µg/L 10.0Bromochloromethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Bromodichloromethane 10 05/13/22 07:42 6200BJLB <50.0 µg/L 50.0Bromoform 10 05/13/22 07:42 6200BJLB <10.0 µg/L 10.0Bromomethane 10 05/13/22 07:42 6200BJLB 29.2 µg/L 5.00n-Butylbenzene 10 05/13/22 07:42 6200BJLB 23.2 µg/L 5.00sec-Butyl benzene 10 05/13/22 07:42 6200BJLB <20.0 µg/L 20.0tert-Butyl benzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Carbon Tetrachloride 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Chlorobenzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Chlorodibromomethane 10 05/13/22 07:42 6200BJLB <10.0 µg/L 10.0Chloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Chloroform 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Chloromethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.002-Chlorotoluene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.004-Chlorotoluene 10 05/13/22 07:42 6200BJLB <20.0 µg/L 20.01,2-Dibromo-3-Chloropropane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2-Dibromoethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Dibromomethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2-Dichlorobenzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,3-Dichlorobenzene 10 05/13/22 07:42 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 15 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-4 89250 Matrix: 5/4/2022 9:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <5.00 µg/L 5.001,4-Dichlorobenzene 10 05/13/22 07:42 6200BJLB <50.0 µg/L 50.0Dichlorodifluoromethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1-Dichloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2-Dichloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1-Dichloroethene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00cis-1,2-Dichloroethene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00trans-1,2-Dichloroethene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2-Dichloropropane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,3-Dichloropropane 10 05/13/22 07:42 6200BJLB <20.0 µg/L 20.02,2-Dichloropropane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1-Dichloropropene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00cis-1,3-Dichloropropene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00trans-1,3-Dichloropropene 10 05/13/22 07:42 6200BJLB <2000 µg/L 2000Ethanol 10 05/13/22 07:42 6200BJLB 2250 µg/L 50.0Ethylbenzene 100 05/13/22 21:34 6200BJLB <30.0 µg/L 30.0Hexachlorobutadiene 10 05/13/22 07:42 6200BJLB 8.46 µg/L 5.00Di-Isopropyl Ether (DIPE)10 05/13/22 07:42 6200BJLB 160 µg/L 5.00Isopropylbenzene 10 05/13/22 07:42 6200BJLB 12.1 µg/L 5.004-Isopropyl toluene 10 05/13/22 07:42 6200BJLB <10.0 µg/L 10.02-Hexanone 10 05/13/22 07:42 6200BJLB <50.0 µg/L 50.0Methyl Ethyl Ketone (MEK)10 05/13/22 07:42 6200BJLB <20.0 µg/L 20.0Methylene Chloride 10 05/13/22 07:42 6200BJLB 23.5 µg/L 10.0Methyl tert-butyl ether (MTBE)10 05/13/22 07:42 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 16 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-4 89250 Matrix: 5/4/2022 9:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.04-Methyl-2-Pentanone 10 05/13/22 07:42 6200BJLB 480 µg/L 10.0Naphthalene 10 05/13/22 07:42 6200BJLB 368 µg/L 5.00n-Propylbenzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Styrene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1,1,2-Tetrachloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1,2,2-Tetrachloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Tetrachloroethene 10 05/13/22 07:42 6200BJLB 886 µg/L 5.00Toluene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2,3-Trichlorobenzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2,4-Trichlorobenzene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1,1-Trichloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,1,2-Trichloroethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Trichloroethene 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Trichlorofluoromethane 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.001,2,3-Trichloropropane 10 05/13/22 07:42 6200BJLB 1480 µg/L 50.01,2,4-Trimethylbenzene 100 05/13/22 21:34 6200BJLB 280 µg/L 5.001,3,5-Trimethylbenzene 10 05/13/22 07:42 6200BJLB <50.0 µg/L 50.0Vinyl Acetate 10 05/13/22 07:42 6200BJLB <5.00 µg/L 5.00Vinyl Chloride 10 05/13/22 07:42 6200BJLB 4040 µg/L 100m,p-Xylene 100 05/13/22 21:34 6200BJLB 593 µg/L 5.00o-Xylene 10 05/13/22 07:42 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 17 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-4 89250 Matrix: 5/4/2022 9:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 4630 µg/L 5.00Xylene (Total)10 05/13/22 07:42 6200B Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%05/13/22 07:4210 JLB V18665 Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%05/13/22 07:4210 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%05/13/22 07:4210 JLB V18665 Surrogate: Toluene-d8 100 Limits: 70-130%05/13/22 07:4210 JLB V18665 Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%05/13/22 21:34100 JLB V18682 Surrogate: Dibromofluoromethane 101 Limits: 70-130%05/13/22 21:34100 JLB V18682 Surrogate: 1,2-Dichloroethane - d4 99.0 Limits: 70-130%05/13/22 21:34100 JLB V18682 Surrogate: Toluene-d8 96.8 Limits: 70-130%05/13/22 21:34100 JLB V18682 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 18 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-5 89251 Matrix: 5/4/2022 9:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 06:53 6200BJLB 817 µg/L 50.0Benzene 100 05/13/22 21:59 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 06:53 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 06:53 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 06:53 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 06:53 6200BJLB 33.5 µg/L 0.500n-Butylbenzene 1 05/13/22 06:53 6200BJLB 17.9 µg/L 0.500sec-Butyl benzene 1 05/13/22 06:53 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 06:53 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 06:53 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 06:53 6200BJLB 1.59 µg/L 0.5001,2-Dibromoethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 06:53 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 19 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-5 89251 Matrix: 5/4/2022 9:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 06:53 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 06:53 6200BJLB 5.88 µg/L 0.5001,2-Dichloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 06:53 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 06:53 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 06:53 6200BJLB 1660 µg/L 50.0Ethylbenzene 100 05/13/22 21:59 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 06:53 6200BJLB 2.85 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 06:53 6200BJLB 115 µg/L 50.0Isopropylbenzene 100 05/13/22 21:59 6200BJLB 6.71 µg/L 0.5004-Isopropyl toluene 1 05/13/22 06:53 6200BJLB 6.12 µg/L 1.002-Hexanone 1 05/13/22 06:53 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 06:53 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 06:53 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 06:53 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 20 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-5 89251 Matrix: 5/4/2022 9:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 06:53 6200BJLB 214 µg/L 100Naphthalene 100 05/13/22 21:59 6200BJLB 232 µg/L 50.0n-Propylbenzene 100 05/13/22 21:59 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 06:53 6200BJLB 2270 µg/L 50.0Toluene 100 05/13/22 21:59 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 06:53 6200BJLB 1320 µg/L 50.01,2,4-Trimethylbenzene 100 05/13/22 21:59 6200BJLB 288 µg/L 50.01,3,5-Trimethylbenzene 100 05/13/22 21:59 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 06:53 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 06:53 6200BJLB 4910 µg/L 100m,p-Xylene 100 05/13/22 21:59 6200BJLB 1600 µg/L 50.0o-Xylene 100 05/13/22 21:59 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 21 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-5 89251 Matrix: 5/4/2022 9:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 6510 µg/L 50.0Xylene (Total)100 05/13/22 21:59 6200B Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/13/22 06:531 JLB V18665 Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%05/13/22 06:531 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/13/22 06:531 JLB V18665 Surrogate: Toluene-d8 98.2 Limits: 70-130%05/13/22 06:531 JLB V18665 Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/13/22 21:59100 JLB V18682 Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%05/13/22 21:59100 JLB V18682 Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%05/13/22 21:59100 JLB V18682 Surrogate: Toluene-d8 100 Limits: 70-130%05/13/22 21:59100 JLB V18682 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 22 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-6 89252 Matrix: 5/4/2022 9:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 04:50 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 04:50 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 04:50 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 04:50 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 23 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-6 89252 Matrix: 5/4/2022 9:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 04:50 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 04:50 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 04:50 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 04:50 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 04:50 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 04:50 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 04:50 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 24 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-6 89252 Matrix: 5/4/2022 9:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 04:50 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 04:50 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 04:50 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 04:50 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 25 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-6 89252 Matrix: 5/4/2022 9:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 04:50 6200B Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/13/22 04:501 JLB V18665 Surrogate: Dibromofluoromethane 103 Limits: 70-130%05/13/22 04:501 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%05/13/22 04:501 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 04:501 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 26 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-10 89253 Matrix: 5/4/2022 8:50 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 05:15 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 05:15 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 05:15 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 05:15 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 27 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-10 89253 Matrix: 5/4/2022 8:50 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 05:15 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 05:15 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 05:15 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 05:15 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 05:15 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 05:15 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 05:15 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 28 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-10 89253 Matrix: 5/4/2022 8:50 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 05:15 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 05:15 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 05:15 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 05:15 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 29 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-10 89253 Matrix: 5/4/2022 8:50 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 05:15 6200B Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/13/22 05:151 JLB V18665 Surrogate: Dibromofluoromethane 105 Limits: 70-130%05/13/22 05:151 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/13/22 05:151 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 05:151 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 30 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12 89254 Matrix: 5/4/2022 8:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <100 µg/L 100Acetone 10 05/13/22 08:07 6200BJLB 4390 µg/L 500Benzene 1000 05/13/22 20:45 6200BJLB <5.00 µg/L 5.00Bromobenzene 10 05/13/22 08:07 6200BJLB <10.0 µg/L 10.0Bromochloromethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Bromodichloromethane 10 05/13/22 08:07 6200BJLB <50.0 µg/L 50.0Bromoform 10 05/13/22 08:07 6200BJLB <10.0 µg/L 10.0Bromomethane 10 05/13/22 08:07 6200BJLB 80.3 µg/L 5.00n-Butylbenzene 10 05/13/22 08:07 6200BJLB 55.0 µg/L 5.00sec-Butyl benzene 10 05/13/22 08:07 6200BJLB <20.0 µg/L 20.0tert-Butyl benzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Carbon Tetrachloride 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Chlorobenzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Chlorodibromomethane 10 05/13/22 08:07 6200BJLB <10.0 µg/L 10.0Chloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Chloroform 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Chloromethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.002-Chlorotoluene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.004-Chlorotoluene 10 05/13/22 08:07 6200BJLB <20.0 µg/L 20.01,2-Dibromo-3-Chloropropane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2-Dibromoethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Dibromomethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2-Dichlorobenzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,3-Dichlorobenzene 10 05/13/22 08:07 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 31 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12 89254 Matrix: 5/4/2022 8:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <5.00 µg/L 5.001,4-Dichlorobenzene 10 05/13/22 08:07 6200BJLB <50.0 µg/L 50.0Dichlorodifluoromethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1-Dichloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2-Dichloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1-Dichloroethene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00cis-1,2-Dichloroethene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00trans-1,2-Dichloroethene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2-Dichloropropane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,3-Dichloropropane 10 05/13/22 08:07 6200BJLB <20.0 µg/L 20.02,2-Dichloropropane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1-Dichloropropene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00cis-1,3-Dichloropropene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00trans-1,3-Dichloropropene 10 05/13/22 08:07 6200BJLB <2000 µg/L 2000Ethanol 10 05/13/22 08:07 6200BJLB 3790 µg/L 500Ethylbenzene 1000 05/13/22 20:45 6200BJLB <30.0 µg/L 30.0Hexachlorobutadiene 10 05/13/22 08:07 6200BJLB 11.0 µg/L 5.00Di-Isopropyl Ether (DIPE)10 05/13/22 08:07 6200BJLB 273 µg/L 5.00Isopropylbenzene 10 05/13/22 08:07 6200BJLB 27.1 µg/L 5.004-Isopropyl toluene 10 05/13/22 08:07 6200BJLB 11.7 µg/L 10.02-Hexanone 10 05/13/22 08:07 6200BJLB <50.0 µg/L 50.0Methyl Ethyl Ketone (MEK)10 05/13/22 08:07 6200BJLB <20.0 µg/L 20.0Methylene Chloride 10 05/13/22 08:07 6200BJLB <10.0 µg/L 10.0Methyl tert-butyl ether (MTBE)10 05/13/22 08:07 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 32 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12 89254 Matrix: 5/4/2022 8:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 106 µg/L 10.04-Methyl-2-Pentanone 10 05/13/22 08:07 6200BJLB 711 µg/L 10.0Naphthalene 10 05/13/22 08:07 6200BJLB 722 µg/L 5.00n-Propylbenzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Styrene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1,1,2-Tetrachloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1,2,2-Tetrachloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Tetrachloroethene 10 05/13/22 08:07 6200BJLB 539 µg/L 5.00Toluene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2,3-Trichlorobenzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2,4-Trichlorobenzene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1,1-Trichloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,1,2-Trichloroethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Trichloroethene 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Trichlorofluoromethane 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.001,2,3-Trichloropropane 10 05/13/22 08:07 6200BJLB 3030 µg/L 5001,2,4-Trimethylbenzene 1000 05/13/22 20:45 6200BJLB 908 µg/L 5001,3,5-Trimethylbenzene 1000 05/13/22 20:45 6200BJLB <50.0 µg/L 50.0Vinyl Acetate 10 05/13/22 08:07 6200BJLB <5.00 µg/L 5.00Vinyl Chloride 10 05/13/22 08:07 6200BJLB 8080 µg/L 1000m,p-Xylene 1000 05/13/22 20:45 6200BJLB 1720 µg/L 500o-Xylene 1000 05/13/22 20:45 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 33 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12 89254 Matrix: 5/4/2022 8:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 9800 µg/L 500Xylene (Total)1000 05/13/22 20:45 6200B Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%05/13/22 08:0710 JLB V18665 Surrogate: Dibromofluoromethane 100 Limits: 70-130%05/13/22 08:0710 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%05/13/22 08:0710 JLB V18665 Surrogate: Toluene-d8 99.0 Limits: 70-130%05/13/22 08:0710 JLB V18665 Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%05/13/22 20:451000 JLB V18682 Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%05/13/22 20:451000 JLB V18682 Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%05/13/22 20:451000 JLB V18682 Surrogate: Toluene-d8 99.6 Limits: 70-130%05/13/22 20:451000 JLB V18682 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 34 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12D 89255 Matrix: 5/4/2022 8:35 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 05:39 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 05:39 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 05:39 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 05:39 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 35 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12D 89255 Matrix: 5/4/2022 8:35 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 05:39 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 05:39 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 05:39 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 05:39 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 05:39 6200BJLB 7.47 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 05:39 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 05:39 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 05:39 6200BJLB 18.7 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 05:39 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 36 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12D 89255 Matrix: 5/4/2022 8:35 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 05:39 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 05:39 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 05:39 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 05:39 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 37 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-12D 89255 Matrix: 5/4/2022 8:35 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 05:39 6200B Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%05/13/22 05:391 JLB V18665 Surrogate: Dibromofluoromethane 104 Limits: 70-130%05/13/22 05:391 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%05/13/22 05:391 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 05:391 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 38 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-13 89256 Matrix: 5/4/2022 8:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 06:04 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 06:04 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 06:04 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 06:04 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 39 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-13 89256 Matrix: 5/4/2022 8:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 06:04 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 06:04 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 06:04 6200BJLB 348 µg/L 200Ethanol 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 06:04 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 06:04 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 06:04 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 06:04 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 40 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-13 89256 Matrix: 5/4/2022 8:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 06:04 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 06:04 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 06:04 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 06:04 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 41 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-13 89256 Matrix: 5/4/2022 8:05 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 06:04 6200B Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/13/22 06:041 JLB V18665 Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/13/22 06:041 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%05/13/22 06:041 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 06:041 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 42 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-15 89257 Matrix: 5/3/2022 15:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 06:29 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 06:29 6200BJLB 2.60 µg/L 0.500sec-Butyl benzene 1 05/13/22 06:29 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 06:29 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 06:29 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 43 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-15 89257 Matrix: 5/3/2022 15:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 06:29 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 06:29 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 06:29 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 06:29 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 06:29 6200BJLB 1.78 µg/L 0.500Isopropylbenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 06:29 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 06:29 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 06:29 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 44 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-15 89257 Matrix: 5/3/2022 15:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 06:29 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 06:29 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 06:29 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 06:29 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 45 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-15 89257 Matrix: 5/3/2022 15:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 06:29 6200B Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/13/22 06:291 JLB V18665 Surrogate: Dibromofluoromethane 105 Limits: 70-130%05/13/22 06:291 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/13/22 06:291 JLB V18665 Surrogate: Toluene-d8 100 Limits: 70-130%05/13/22 06:291 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 46 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-16 89258 Matrix: 5/3/2022 16:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 04:01 6200BJLB 40.2 µg/L 0.500Benzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 04:01 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 04:01 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 04:01 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 04:01 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 04:01 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 04:01 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 04:01 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 47 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-16 89258 Matrix: 5/3/2022 16:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 04:01 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 04:01 6200BJLB 1.22 µg/L 0.5001,2-Dichloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 04:01 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 04:01 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 04:01 6200BJLB 19.0 µg/L 0.500Ethylbenzene 1 05/13/22 04:01 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 04:01 6200BJLB 1.30 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 04:01 6200BJLB 2.13 µg/L 0.500Isopropylbenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 04:01 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 04:01 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 04:01 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 04:01 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 04:01 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 48 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-16 89258 Matrix: 5/3/2022 16:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 04:01 6200BJLB 2.13 µg/L 1.00Naphthalene 1 05/13/22 04:01 6200BJLB 4.26 µg/L 0.500n-Propylbenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 04:01 6200BJLB 2.60 µg/L 0.500Toluene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 04:01 6200BJLB 11.1 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 04:01 6200BJLB 1.95 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 04:01 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 04:01 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 04:01 6200BJLB 18.6 µg/L 1.00m,p-Xylene 1 05/13/22 04:01 6200BJLB 1.36 µg/L 0.500o-Xylene 1 05/13/22 04:01 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 49 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:MW-16 89258 Matrix: 5/3/2022 16:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF 20.0 µg/L 0.500Xylene (Total)1 05/13/22 04:01 6200B Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/13/22 04:011 JLB V18665 Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/13/22 04:011 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/13/22 04:011 JLB V18665 Surrogate: Toluene-d8 99.8 Limits: 70-130%05/13/22 04:011 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 50 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:FB 89259 Matrix: 5/4/2022 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 02:22 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 02:22 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 02:22 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 02:22 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 51 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:FB 89259 Matrix: 5/4/2022 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 02:22 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 02:22 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 02:22 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 02:22 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 02:22 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 02:22 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 02:22 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 52 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:FB 89259 Matrix: 5/4/2022 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 02:22 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 02:22 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 02:22 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 02:22 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 53 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:FB 89259 Matrix: 5/4/2022 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 02:22 6200B Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/13/22 02:221 JLB V18665 Surrogate: Dibromofluoromethane 101 Limits: 70-130%05/13/22 02:221 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%05/13/22 02:221 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 02:221 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 54 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-1 89260 Matrix: 5/4/2022 10:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 02:47 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 02:47 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 02:47 6200BJLB 0.682 µg/L 0.500Chloroform 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 02:47 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 02:47 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 55 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-1 89260 Matrix: 5/4/2022 10:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 02:47 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 02:47 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 02:47 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 02:47 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 02:47 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 02:47 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 02:47 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 56 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-1 89260 Matrix: 5/4/2022 10:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 02:47 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 02:47 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 02:47 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 02:47 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 57 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-1 89260 Matrix: 5/4/2022 10:45 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 02:47 6200B Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/13/22 02:471 JLB V18665 Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/13/22 02:471 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 99.0 Limits: 70-130%05/13/22 02:471 JLB V18665 Surrogate: Toluene-d8 100 Limits: 70-130%05/13/22 02:471 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 58 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-7 89261 Matrix: 5/4/2022 11:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 03:11 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 03:11 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 03:11 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 03:11 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 59 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-7 89261 Matrix: 5/4/2022 11:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 03:11 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 03:11 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 03:11 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 03:11 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 03:11 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 03:11 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 03:11 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 60 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-7 89261 Matrix: 5/4/2022 11:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 03:11 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 03:11 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 03:11 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 03:11 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 61 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-7 89261 Matrix: 5/4/2022 11:00 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 03:11 6200B Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/13/22 03:111 JLB V18665 Surrogate: Dibromofluoromethane 106 Limits: 70-130%05/13/22 03:111 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%05/13/22 03:111 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 03:111 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 62 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-8 89262 Matrix: 5/4/2022 11:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Benzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00Bromochloromethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 05/13/22 03:36 6200BJLB <5.00 µg/L 5.00Bromoform 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00Bromomethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 05/13/22 03:36 6200BJLB <2.00 µg/L 2.00tert-Butyl benzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00Chloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Chloroform 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Chloromethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 05/13/22 03:36 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 05/13/22 03:36 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 63 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-8 89262 Matrix: 5/4/2022 11:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 05/13/22 03:36 6200BJLB <5.00 µg/L 5.00Dichlorodifluoromethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 05/13/22 03:36 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 05/13/22 03:36 6200BJLB <200 µg/L 200Ethanol 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 05/13/22 03:36 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.002-Hexanone 1 05/13/22 03:36 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 05/13/22 03:36 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 05/13/22 03:36 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 64 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-8 89262 Matrix: 5/4/2022 11:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00Naphthalene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Styrene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Toluene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 05/13/22 03:36 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500Vinyl Chloride 1 05/13/22 03:36 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 05/13/22 03:36 6200BJLB <0.500 µg/L 0.500o-Xylene 1 05/13/22 03:36 6200BJLB Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 65 of 77 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 22-126-0010 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Liz Allyn Cary 02172214.23 Received : 05/06/2022 Caraway Grocery Report Date : 05/16/2022 Sample ID : Lab No : Sampled:SW-8 89262 Matrix: 5/4/2022 11:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Xylene (Total)1 05/13/22 03:36 6200B Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/13/22 03:361 JLB V18665 Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/13/22 03:361 JLB V18665 Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%05/13/22 03:361 JLB V18665 Surrogate: Toluene-d8 101 Limits: 70-130%05/13/22 03:361 JLB V18665 Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 66 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 Associated Lab Samples: 89248, 89249, 89250, 89251, 89252, 89253, 89254, 89255, 89256, 89257, 89258, 89259, 89260, 89261, 89262 LRB-V18664 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 05/13/22 01:3310.0< 10.0µg/LAcetone 05/13/22 01:330.500< 0.500µg/LBenzene 05/13/22 01:330.500< 0.500µg/LBromobenzene 05/13/22 01:331.00< 1.00µg/LBromochloromethane 05/13/22 01:330.500< 0.500µg/LBromodichloromethane 05/13/22 01:335.00< 5.00µg/LBromoform 05/13/22 01:331.00< 1.00µg/LBromomethane 05/13/22 01:330.500< 0.500µg/Ln-Butylbenzene 05/13/22 01:330.500< 0.500µg/Lsec-Butyl benzene 05/13/22 01:332.00< 2.00µg/Ltert-Butyl benzene 05/13/22 01:330.500< 0.500µg/LCarbon Tetrachloride 05/13/22 01:330.500< 0.500µg/LChlorobenzene 05/13/22 01:330.500< 0.500µg/LChlorodibromomethane 05/13/22 01:331.00< 1.00µg/LChloroethane 05/13/22 01:330.500< 0.500µg/LChloroform 05/13/22 01:330.500< 0.500µg/LChloromethane 05/13/22 01:330.500< 0.500µg/L2-Chlorotoluene 05/13/22 01:330.500< 0.500µg/L4-Chlorotoluene 05/13/22 01:332.00< 2.00µg/L1,2-Dibromo-3-Chloropropane 05/13/22 01:330.500< 0.500µg/L1,2-Dibromoethane 05/13/22 01:330.500< 0.500µg/LDibromomethane 05/13/22 01:330.500< 0.500µg/L1,2-Dichlorobenzene 05/13/22 01:330.500< 0.500µg/L1,3-Dichlorobenzene 05/13/22 01:330.500< 0.500µg/L1,4-Dichlorobenzene 05/13/22 01:335.00< 5.00µg/LDichlorodifluoromethane 05/13/22 01:330.500< 0.500µg/L1,1-Dichloroethane 05/13/22 01:330.500< 0.500µg/L1,2-Dichloroethane Page 1 of 8Date:05/16/2022 02:57 PM Page 67 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 Associated Lab Samples: 89248, 89249, 89250, 89251, 89252, 89253, 89254, 89255, 89256, 89257, 89258, 89259, 89260, 89261, 89262 LRB-V18664 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 05/13/22 01:330.500< 0.500µg/L1,1-Dichloroethene 05/13/22 01:330.500< 0.500µg/Lcis-1,2-Dichloroethene 05/13/22 01:330.500< 0.500µg/Ltrans-1,2-Dichloroethene 05/13/22 01:330.500< 0.500µg/L1,2-Dichloropropane 05/13/22 01:330.500< 0.500µg/L1,3-Dichloropropane 05/13/22 01:332.00< 2.00µg/L2,2-Dichloropropane 05/13/22 01:330.500< 0.500µg/L1,1-Dichloropropene 05/13/22 01:330.500< 0.500µg/Lcis-1,3-Dichloropropene 05/13/22 01:330.500< 0.500µg/Ltrans-1,3-Dichloropropene 05/13/22 01:33200< 200µg/LEthanol 05/13/22 01:330.500< 0.500µg/LEthylbenzene 05/13/22 01:333.00< 3.00µg/LHexachlorobutadiene 05/13/22 01:330.500< 0.500µg/LDi-Isopropyl Ether (DIPE) 05/13/22 01:330.500< 0.500µg/LIsopropylbenzene 05/13/22 01:330.500< 0.500µg/L4-Isopropyl toluene 05/13/22 01:331.00< 1.00µg/L2-Hexanone 05/13/22 01:335.00< 5.00µg/LMethyl Ethyl Ketone (MEK) 05/13/22 01:332.00< 2.00µg/LMethylene Chloride 05/13/22 01:331.00< 1.00µg/LMethyl tert-butyl ether (MTBE) 05/13/22 01:331.00< 1.00µg/L4-Methyl-2-Pentanone 05/13/22 01:331.00< 1.00µg/LNaphthalene 05/13/22 01:330.500< 0.500µg/Ln-Propylbenzene 05/13/22 01:330.500< 0.500µg/LStyrene 05/13/22 01:330.500< 0.500µg/L1,1,1,2-Tetrachloroethane 05/13/22 01:330.500< 0.500µg/L1,1,2,2-Tetrachloroethane 05/13/22 01:330.500< 0.500µg/LTetrachloroethene 05/13/22 01:330.500< 0.500µg/LToluene Page 2 of 8Date:05/16/2022 02:57 PM Page 68 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 Associated Lab Samples: 89248, 89249, 89250, 89251, 89252, 89253, 89254, 89255, 89256, 89257, 89258, 89259, 89260, 89261, 89262 LRB-V18664 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 05/13/22 01:330.500< 0.500µg/L1,2,3-Trichlorobenzene 05/13/22 01:330.500< 0.500µg/L1,2,4-Trichlorobenzene 05/13/22 01:330.500< 0.500µg/L1,1,1-Trichloroethane 05/13/22 01:330.500< 0.500µg/L1,1,2-Trichloroethane 05/13/22 01:330.500< 0.500µg/LTrichloroethene 05/13/22 01:330.500< 0.500µg/LTrichlorofluoromethane 05/13/22 01:330.500< 0.500µg/L1,2,3-Trichloropropane 05/13/22 01:330.500< 0.500µg/L1,2,4-Trimethylbenzene 05/13/22 01:330.500< 0.500µg/L1,3,5-Trimethylbenzene 05/13/22 01:335.00< 5.00µg/LVinyl Acetate 05/13/22 01:330.500< 0.500µg/LVinyl Chloride 05/13/22 01:331.00< 1.00µg/Lm,p-Xylene 05/13/22 01:330.500< 0.500µg/Lo-Xylene 05/13/22 01:334-Bromofluorobenzene (S)103 70-130 05/13/22 01:33Dibromofluoromethane (S)104 70-130 05/13/22 01:331,2-Dichloroethane - d4 (S)101 70-130 05/13/22 01:33Toluene-d8 (S)99.6 70-130 LCS-V18664 LCSD-V18664Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 38.5 96.210341.140.0µg/LAcetone 40-160 6.5 20.0 19.8 99.010120.220.0µg/LBenzene 70-130 2.0 20.0 19.6 98.010220.320.0µg/LBromobenzene 70-130 3.5 20.0 19.5 97.599.519.920.0µg/LBromochloromethane 70-130 2.0 20.0 21.1 10610921.720.0µg/LBromodichloromethane 70-130 2.8 20.0 Page 3 of 8Date:05/16/2022 02:57 PM Page 69 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 LCS-V18664 LCSD-V18664Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 18.8 94.097.519.520.0µg/LBromoform 70-130 3.6 20.0 22.0 11011222.320.0µg/LBromomethane 60-140 1.3 20.0 19.3 96.598.519.720.0µg/Ln-Butylbenzene 70-130 2.0 20.0 19.5 97.510320.520.0µg/Lsec-Butyl benzene 70-130 5.0 20.0 20.0 10099.019.820.0µg/Ltert-Butyl benzene 70-130 1.0 20.0 22.1 11110921.720.0µg/LCarbon Tetrachloride 70-130 1.8 20.0 20.0 10099.519.920.0µg/LChlorobenzene 70-130 0.5 20.0 21.3 10711522.920.0µg/LChlorodibromomethane 70-130 7.2 20.0 15.8 79.085.517.120.0µg/LChloroethane 60-140 7.9 20.0 20.1 10110621.120.0µg/LChloroform 70-130 4.8 20.0 21.2 10611021.920.0µg/LChloromethane 60-140 3.2 20.0 19.5 97.598.519.720.0µg/L2-Chlorotoluene 70-130 1.0 20.0 19.7 98.599.519.920.0µg/L4-Chlorotoluene 70-130 1.0 20.0 20.8 10410521.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.9 20.0 21.7 10910821.520.0µg/L1,2-Dibromoethane 70-130 0.9 20.0 21.1 10611322.520.0µg/LDibromomethane 70-130 6.4 20.0 20.0 10010020.020.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0 19.2 96.099.019.820.0µg/L1,3-Dichlorobenzene 70-130 3.0 20.0 19.8 99.099.519.920.0µg/L1,4-Dichlorobenzene 70-130 0.5 20.0 18.5 92.595.019.020.0µg/LDichlorodifluoromethane 60-140 2.6 20.0 20.4 10210521.020.0µg/L1,1-Dichloroethane 70-130 2.8 20.0 20.4 10210320.620.0µg/L1,2-Dichloroethane 70-130 0.9 20.0 19.3 96.510220.420.0µg/L1,1-Dichloroethene 70-130 5.5 20.0 20.1 10197.519.520.0µg/Lcis-1,2-Dichloroethene 70-130 3.0 20.0 20.0 10010020.020.0µg/Ltrans-1,2-Dichloroethene 70-130 0.0 20.0 20.6 10310521.020.0µg/L1,2-Dichloropropane 70-130 1.9 20.0 Page 4 of 8Date:05/16/2022 02:57 PM Page 70 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 LCS-V18664 LCSD-V18664Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 20.9 10510520.920.0µg/L1,3-Dichloropropane 70-130 0.0 20.0 22.2 11111322.520.0µg/L2,2-Dichloropropane 70-130 1.3 20.0 19.8 99.010520.920.0µg/L1,1-Dichloropropene 70-130 5.4 20.0 22.2 11111022.020.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0 22.6 11311422.820.0µg/Ltrans-1,3-Dichloropropene 70-130 0.8 20.0 590 118123617500µg/LEthanol 60-140 4.4 20.0 19.3 96.597.019.420.0µg/LEthylbenzene 70-130 0.5 20.0 19.5 97.510420.720.0µg/LHexachlorobutadiene 70-130 5.9 20.0 20.9 10510420.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.9 20.0 19.3 96.598.519.720.0µg/LIsopropylbenzene 70-130 2.0 20.0 19.5 97.510120.220.0µg/L4-Isopropyl toluene 70-130 3.5 20.0 21.3 10711322.620.0µg/L2-Hexanone 60-140 5.9 20.0 18.7 93.599.519.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.2 20.0 20.3 10210120.120.0µg/LMethylene Chloride 70-130 0.9 20.0 21.2 10610721.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.4 20.0 21.7 10910721.420.0µg/L4-Methyl-2-Pentanone 60-140 1.3 20.0 20.0 10010921.720.0µg/LNaphthalene 70-130 8.1 20.0 19.4 97.099.019.820.0µg/Ln-Propylbenzene 70-130 2.0 20.0 20.4 10210320.520.0µg/LStyrene 70-130 0.4 20.0 19.4 97.099.519.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.5 20.0 21.0 10510821.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.3 20.0 19.0 95.010120.220.0µg/LTetrachloroethene 70-130 6.1 20.0 19.7 98.510020.020.0µg/LToluene 70-130 1.5 20.0 17.8 89.010621.220.0µg/L1,2,3-Trichlorobenzene 70-130 17.4 20.0 19.6 98.099.019.820.0µg/L1,2,4-Trichlorobenzene 70-130 1.0 20.0 20.1 10110521.020.0µg/L1,1,1-Trichloroethane 70-130 4.3 20.0 Page 5 of 8Date:05/16/2022 02:57 PM Page 71 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18665QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18664 LCS-V18664 LCSD-V18664Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 20.4 10210320.620.0µg/L1,1,2-Trichloroethane 70-130 0.9 20.0 19.9 99.510420.820.0µg/LTrichloroethene 70-130 4.4 20.0 20.0 10010821.620.0µg/LTrichlorofluoromethane 60-140 7.6 20.0 19.6 98.098.019.620.0µg/L1,2,3-Trichloropropane 70-130 0.0 20.0 20.2 10110020.020.0µg/L1,2,4-Trimethylbenzene 70-130 0.9 20.0 19.7 98.599.519.920.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0 22.0 11011022.020.0µg/LVinyl Acetate 60-140 0.0 20.0 19.1 95.599.019.820.0µg/LVinyl Chloride 60-140 3.5 20.0 40.0 10010240.640.0µg/Lm,p-Xylene 70-130 1.4 20.0 20.3 10210420.720.0µg/Lo-Xylene 70-130 1.9 20.0 98.898.64-Bromofluorobenzene (S)70-130 103103Dibromofluoromethane (S)70-130 1011011,2-Dichloroethane - d4 (S)70-130 100100Toluene-d8 (S)70-130 Page 6 of 8Date:05/16/2022 02:57 PM Page 72 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18682QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18681 Associated Lab Samples: 89249, 89250, 89251, 89254 LRB-V18681 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 05/13/22 13:460.500< 0.500µg/LBenzene 05/13/22 13:460.500< 0.500µg/LEthylbenzene 05/13/22 13:460.500< 0.500µg/LIsopropylbenzene 05/13/22 13:461.00< 1.00µg/LNaphthalene 05/13/22 13:460.500< 0.500µg/Ln-Propylbenzene 05/13/22 13:460.500< 0.500µg/LToluene 05/13/22 13:460.500< 0.500µg/L1,2,4-Trimethylbenzene 05/13/22 13:460.500< 0.500µg/L1,3,5-Trimethylbenzene 05/13/22 13:461.00< 1.00µg/Lm,p-Xylene 05/13/22 13:460.500< 0.500µg/Lo-Xylene 05/13/22 13:464-Bromofluorobenzene (S)105 70-130 05/13/22 13:46Dibromofluoromethane (S)98.8 70-130 05/13/22 13:461,2-Dichloroethane - d4 (S)99.6 70-130 05/13/22 13:46Toluene-d8 (S)100 70-130 LCS-V18681 LCSD-V18681Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 20.2 10110220.420.0µg/LBenzene 70-130 0.9 20.0 19.7 98.510120.220.0µg/LEthylbenzene 70-130 2.5 20.0 20.0 10098.519.720.0µg/LIsopropylbenzene 70-130 1.5 20.0 21.5 10810220.420.0µg/LNaphthalene 70-130 5.2 20.0 20.0 10098.519.720.0µg/Ln-Propylbenzene 70-130 1.5 20.0 19.6 98.010220.320.0µg/LToluene 70-130 3.5 20.0 20.5 10310020.020.0µg/L1,2,4-Trimethylbenzene 70-130 2.4 20.0 20.0 10099.019.820.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0 Page 7 of 8Date:05/16/2022 02:57 PM Page 73 of 77 Quality Control Data 22-126-0010Report No: Project Description: Client ID:Withers & Ravenel Caraway Grocery QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V18682QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V18681 LCS-V18681 LCSD-V18681Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 40.8 10210341.240.0µg/Lm,p-Xylene 70-130 0.9 20.0 20.5 10310320.620.0µg/Lo-Xylene 70-130 0.4 20.0 99.496.24-Bromofluorobenzene (S)70-130 101102Dibromofluoromethane (S)70-130 96.897.41,2-Dichloroethane - d4 (S)70-130 99.8100Toluene-d8 (S)70-130 Page 8 of 8Date:05/16/2022 02:57 PM Page 74 of 77 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:22-126-0010 Withers & Ravenel 01221 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT-15 2.2 C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angela D Overcash Date & Time:05/06/2022 15:01:21 Special precautions or instructions included? Comments: Page 75 of 77 Page 76 of 77 Page 77 of 77