WS-6406_24174_CA_LAB_20140825

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2401 Brentwood Road
Suite 107 I
Raleigh, NC 27604
Attention: Thomas Perdue
PH14008Lot Number:
70149641Project Number:
Caraway GroceryProject Name:
08/25/2014Date Completed:
Nisreen Saikaly
Project Manager
*PH14008*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Terracon Consultants, Inc.
Lot Number: PH14008
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: PH14008

Sample Number Sample ID Matrix Date Sampled Date Received
001 08/12/2014 1431MW-5 Aqueous 08/14/2014
002 08/12/2014 1534MW-1A Aqueous 08/14/2014
003 08/12/2014 1625MW-4 Aqueous 08/14/2014
004 08/12/2014 1723MW-3 Aqueous 08/14/2014
005 08/12/2014 2039MW-14 Aqueous 08/14/2014
006 08/12/2014 2137MW-9 Aqueous 08/14/2014
007 08/12/2014 2224MW-12 Aqueous 08/14/2014
(7 samples)
Page: 3 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, Inc.
Lot Number: PH14008

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 MW-5 Aqueous Benzene SM 6200B-810 ug/L 6
001 MW-5 Aqueous sec-Butylbenzene SM 6200B-13 J ug/L 6
001 MW-5 Aqueous Ethylbenzene SM 6200B-800 ug/L 6
001 MW-5 Aqueous Isopropylbenzene (Cumene)SM 6200B-85 ug/L 6
001 MW-5 Aqueous Naphthalene SM 6200B-130 ug/L 6
001 MW-5 Aqueous n-Propylbenzene SM 6200B-140 ug/L 6
001 MW-5 Aqueous Toluene SM 6200B-1400 ug/L 7
001 MW-5 Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B-160 ug/L 7
001 MW-5 Aqueous 1,2,4-Trimethylbenzene SM 6200B-570 ug/L 7
001 MW-5 Aqueous m+p - Xylenes SM 6200B-2100 ug/L 7
001 MW-5 Aqueous o - Xylenes SM 6200B-860 ug/L 7
002 MW-1A Aqueous Benzene SM 6200B-4300 ug/L 8
002 MW-1A Aqueous n-Butylbenzene SM 6200B-37 ug/L 8
002 MW-1A Aqueous sec-Butylbenzene SM 6200B-16 J ug/L 8
002 MW-1A Aqueous Diisopropyl ether (IPE)SM 6200B-30 ug/L 8
002 MW-1A Aqueous Ethylbenzene SM 6200B-1800 ug/L 8
002 MW-1A Aqueous Isopropylbenzene (Cumene)SM 6200B-120 ug/L 8
002 MW-1A Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-61 ug/L 8
002 MW-1A Aqueous Naphthalene SM 6200B-180 ug/L 8
002 MW-1A Aqueous Toluene SM 6200B-1500 ug/L 9
002 MW-1A Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B-360 ug/L 9
002 MW-1A Aqueous 1,2,4-Trimethylbenzene SM 6200B-1100 ug/L 9
002 MW-1A Aqueous m+p - Xylenes SM 6200B-3700 ug/L 9
002 MW-1A Aqueous o - Xylenes SM 6200B-890 ug/L 9
003 MW-4 Aqueous Benzene SM 6200B-5200 ug/L 10
003 MW-4 Aqueous sec-Butylbenzene SM 6200B-16 J ug/L 10
003 MW-4 Aqueous Diisopropyl ether (IPE)SM 6200B-60 ug/L 10
003 MW-4 Aqueous Ethylbenzene SM 6200B-1700 ug/L 10
003 MW-4 Aqueous Isopropylbenzene (Cumene)SM 6200B-110 ug/L 10
003 MW-4 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-320 ug/L 10
003 MW-4 Aqueous Naphthalene SM 6200B-230 ug/L 10
003 MW-4 Aqueous n-Propylbenzene SM 6200B-260 ug/L 10
003 MW-4 Aqueous Toluene SM 6200B-2500 ug/L 11
003 MW-4 Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B-390 ug/L 11
003 MW-4 Aqueous 1,2,4-Trimethylbenzene SM 6200B-1200 ug/L 11
003 MW-4 Aqueous m+p - Xylenes SM 6200B-3500 ug/L 11
003 MW-4 Aqueous o - Xylenes SM 6200B-1200 ug/L 11
004 MW-3 Aqueous Benzene SM 6200B-160 ug/L 12
004 MW-3 Aqueous n-Butylbenzene SM 6200B-6.6 ug/L 12
004 MW-3 Aqueous sec-Butylbenzene SM 6200B-9.3 ug/L 12
004 MW-3 Aqueous tert-Butylbenzene SM 6200B-3.5 ug/L 12
004 MW-3 Aqueous Chloroethane SM 6200B-0.58 ug/L 12
004 MW-3 Aqueous Chloroform SM 6200B-1.8 ug/L 12
004 MW-3 Aqueous 1,2-Dichloroethane SM 6200B-12 ug/L 12
004 MW-3 Aqueous Diisopropyl ether (IPE)SM 6200B-10 ug/L 12
Page: 4 of 30
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Executive Summary (Continued)
Lot Number: PH14008
Sample Sample ID Matrix Parameter Method Result Q Units Page
004 MW-3 Aqueous Ethylbenzene SM 6200B-30 ug/L 12
004 MW-3 Aqueous Isopropylbenzene (Cumene)SM 6200B-9.6 ug/L 12
004 MW-3 Aqueous p-Isopropyltoluene (p-Cymene)SM 6200B-1.9 ug/L 12
004 MW-3 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-7.1 ug/L 12
004 MW-3 Aqueous Naphthalene SM 6200B-23 ug/L 12
004 MW-3 Aqueous n-Propylbenzene SM 6200B-15 ug/L 12
004 MW-3 Aqueous Toluene SM 6200B-4.2 ug/L 13
004 MW-3 Aqueous 1,2,4-Trimethylbenzene SM 6200B-9.7 ug/L 13
004 MW-3 Aqueous m+p - Xylenes SM 6200B-6.9 ug/L 13
004 MW-3 Aqueous o - Xylenes SM 6200B-1.9 ug/L 13
005 MW-14 Aqueous Benzene SM 6200B-0.27 J ug/L 14
005 MW-14 Aqueous Naphthalene SM 6200B-0.21 J ug/L 14
005 MW-14 Aqueous Toluene SM 6200B-0.53 ug/L 15
005 MW-14 Aqueous m+p - Xylenes SM 6200B-0.29 J ug/L 15
006 MW-9 Aqueous Benzene SM 6200B-2.0 ug/L 16
006 MW-9 Aqueous sec-Butylbenzene SM 6200B-1.4 ug/L 16
006 MW-9 Aqueous 1,2-Dichloroethane SM 6200B-1.3 ug/L 16
006 MW-9 Aqueous Diisopropyl ether (IPE)SM 6200B-0.59 ug/L 16
006 MW-9 Aqueous Ethylbenzene SM 6200B-0.31 J ug/L 16
006 MW-9 Aqueous Isopropylbenzene (Cumene)SM 6200B-0.69 ug/L 16
006 MW-9 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-1.4 ug/L 16
006 MW-9 Aqueous Toluene SM 6200B-0.18 J ug/L 17
006 MW-9 Aqueous m+p - Xylenes SM 6200B-0.45 J ug/L 17
007 MW-12 Aqueous Benzene SM 6200B-7800 ug/L 18
007 MW-12 Aqueous sec-Butylbenzene SM 6200B-21 J ug/L 18
007 MW-12 Aqueous Diisopropyl ether (IPE)SM 6200B-46 ug/L 18
007 MW-12 Aqueous Ethylbenzene SM 6200B-2900 ug/L 18
007 MW-12 Aqueous Isopropylbenzene (Cumene)SM 6200B-160 ug/L 18
007 MW-12 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-99 ug/L 18
007 MW-12 Aqueous Naphthalene SM 6200B-330 ug/L 18
007 MW-12 Aqueous n-Propylbenzene SM 6200B-360 ug/L 18
007 MW-12 Aqueous Toluene SM 6200B-3600 ug/L 19
007 MW-12 Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B-640 ug/L 19
007 MW-12 Aqueous 1,2,4-Trimethylbenzene SM 6200B-2200 ug/L 19
007 MW-12 Aqueous m+p - Xylenes SM 6200B-6000 ug/L 19
007 MW-12 Aqueous o - Xylenes SM 6200B-2700 ug/L 19
(81 detections)
Page: 5 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-5
PH14008-001
08/12/2014 1431
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 1921 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 810 1ug/L1.425
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L1.425
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L2.825
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L8.525
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.5125
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L1025
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.8425
sec-Butylbenzene 135-98-8 SM 6200B-20 13 J 1ug/L0.5225
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L1.925
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L4.325
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L8.525
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L8.525
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L8.525
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L8.725
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L3.025
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.9525
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L8.525
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L3.125
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L4.725
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L8.525
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L8.525
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L8.525
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L3.525
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L2.725
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L1.225
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L4.725
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L4.425
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L4.025
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L4.125
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.9525
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L3.025
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L3.725
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L4.525
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L9.025
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L2.625
Ethylbenzene 100-41-4 SM 6200B-20 800 1ug/L8.525
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L8.525
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 85 1ug/L1.425
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.8925
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 ND 1ug/L0.9525
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L8.525
Naphthalene 91-20-3 SM 6200B-20 130 1ug/L8.525
n-Propylbenzene 103-65-1 SM 6200B-20 140 1ug/L1.225
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.7525
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-5
PH14008-001
08/12/2014 1431
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 1921 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L2.925
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.6525
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.7225
Toluene 108-88-3 SM 6200B-20 1400 1ug/L8.525
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L1525
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L8.525
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L8.525
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L1.425
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L1.625
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L1.225
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L2.525
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L1725
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 160 1ug/L8.525
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 570 1ug/L8.525
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L3.325
m+p - Xylenes 179601-23-1 SM 6200B-20 2100 1ug/L8.525
o - Xylenes 95-47-6 SM 6200B-20 860 1ug/L8.525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 100 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-1A
PH14008-002
08/12/2014 1534
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 1944 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 4300 1ug/L1.425
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L1.425
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L2.825
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L8.525
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.5125
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L1025
n-Butylbenzene 104-51-8 SM 6200B-20 37 1ug/L0.8425
sec-Butylbenzene 135-98-8 SM 6200B-20 16 J 1ug/L0.5225
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L1.925
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L4.325
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L8.525
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L8.525
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L8.525
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L8.725
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L3.025
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.9525
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L8.525
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L3.125
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L4.725
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L8.525
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L8.525
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L8.525
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L3.525
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L2.725
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L1.225
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L4.725
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L4.425
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L4.025
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L4.125
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.9525
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L3.025
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L3.725
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L4.525
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L9.025
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 30 1ug/L2.625
Ethylbenzene 100-41-4 SM 6200B-20 1800 1ug/L8.525
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L8.525
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 120 1ug/L1.425
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.8925
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 61 1ug/L0.9525
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L8.525
Naphthalene 91-20-3 SM 6200B-20 180 1ug/L8.525
n-Propylbenzene 103-65-1 SM 6200B-20 ND 1ug/L1.225
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.7525
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-1A
PH14008-002
08/12/2014 1534
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 1944 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L2.925
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.6525
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.7225
Toluene 108-88-3 SM 6200B-20 1500 1ug/L8.525
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L1525
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L8.525
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L8.525
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L1.425
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L1.625
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L1.225
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L2.525
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L1725
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 360 1ug/L8.525
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 1100 1ug/L8.525
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L3.325
m+p - Xylenes 179601-23-1 SM 6200B-20 3700 1ug/L8.525
o - Xylenes 95-47-6 SM 6200B-20 890 1ug/L8.525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-4
PH14008-003
08/12/2014 1625
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 2008 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 5200 1ug/L1.425
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L1.425
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L2.825
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L8.525
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.5125
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L1025
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.8425
sec-Butylbenzene 135-98-8 SM 6200B-20 16 J 1ug/L0.5225
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L1.925
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L4.325
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L8.525
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L8.525
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L8.525
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L8.725
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L3.025
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.9525
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L8.525
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L3.125
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L4.725
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L8.525
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L8.525
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L8.525
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L3.525
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L2.725
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L1.225
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L4.725
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L4.425
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L4.025
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L4.125
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.9525
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L3.025
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L3.725
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L4.525
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L9.025
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 60 1ug/L2.625
Ethylbenzene 100-41-4 SM 6200B-20 1700 1ug/L8.525
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L8.525
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 110 1ug/L1.425
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.8925
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 320 1ug/L0.9525
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L8.525
Naphthalene 91-20-3 SM 6200B-20 230 1ug/L8.525
n-Propylbenzene 103-65-1 SM 6200B-20 260 1ug/L1.225
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.7525
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-4
PH14008-003
08/12/2014 1625
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 2008 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L2.925
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.6525
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.7225
Toluene 108-88-3 SM 6200B-20 2500 1ug/L8.525
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L1525
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L8.525
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L8.525
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L1.425
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L1.625
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L1.225
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L2.525
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L1725
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 390 1ug/L8.525
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 1200 1ug/L8.525
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L3.325
m+p - Xylenes 179601-23-1 SM 6200B-20 3500 1ug/L8.525
o - Xylenes 95-47-6 SM 6200B-20 1200 1ug/L8.525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-3
PH14008-004
08/12/2014 1723
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1504 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 160 1ug/L0.0270.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.0270.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.0550.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.170.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.200.50
n-Butylbenzene 104-51-8 SM 6200B-20 6.6 1ug/L0.0170.50
sec-Butylbenzene 135-98-8 SM 6200B-20 9.3 1ug/L0.0100.50
tert-Butylbenzene 98-06-6 SM 6200B-20 3.5 1ug/L0.0370.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.170.50
Chloroethane 75-00-3 SM 6200B-20 0.58 1ug/L0.170.50
Chloroform 67-66-3 SM 6200B-20 1.8 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.170.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.0590.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.0190.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.0610.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.0940.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.170.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 12 1ug/L0.0230.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.0870.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.0790.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.0810.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.0190.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.0600.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.0740.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.0900.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.180.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 10 1ug/L0.0520.50
Ethylbenzene 100-41-4 SM 6200B-20 30 1ug/L0.170.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.170.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 9.6 1ug/L0.0290.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 1.9 1ug/L0.0180.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 7.1 1ug/L0.0190.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.170.50
Naphthalene 91-20-3 SM 6200B-20 23 1ug/L0.170.50
n-Propylbenzene 103-65-1 SM 6200B-20 15 1ug/L0.0240.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.0150.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-3
PH14008-004
08/12/2014 1723
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1504 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.0570.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.0140.50
Toluene 108-88-3 SM 6200B-20 4.2 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.300.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.0310.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.0510.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.330.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 9.7 1ug/L0.170.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.0650.50
m+p - Xylenes 179601-23-1 SM 6200B-20 6.9 1ug/L0.170.50
o - Xylenes 95-47-6 SM 6200B-20 1.9 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-14
PH14008-005
08/12/2014 2039
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1528 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 0.27 J 1ug/L0.0270.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.0270.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.0550.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.170.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.200.50
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.0170.50
sec-Butylbenzene 135-98-8 SM 6200B-20 ND 1ug/L0.0100.50
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L0.0370.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.170.50
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L0.170.50
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.170.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.0590.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.0190.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.0610.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.0940.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.170.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L0.0230.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.0870.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.0790.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.0810.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.0190.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.0600.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.0740.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.0900.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.180.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L0.0520.50
Ethylbenzene 100-41-4 SM 6200B-20 ND 1ug/L0.170.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.170.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 ND 1ug/L0.0290.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.0180.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 ND 1ug/L0.0190.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.170.50
Naphthalene 91-20-3 SM 6200B-20 0.21 J 1ug/L0.170.50
n-Propylbenzene 103-65-1 SM 6200B-20 ND 1ug/L0.0240.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.0150.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-14
PH14008-005
08/12/2014 2039
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1528 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.0570.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.0140.50
Toluene 108-88-3 SM 6200B-20 0.53 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.300.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.0310.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.0510.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.330.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 ND 1ug/L0.170.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.0650.50
m+p - Xylenes 179601-23-1 SM 6200B-20 0.29 J 1ug/L0.170.50
o - Xylenes 95-47-6 SM 6200B-20 ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-9
PH14008-006
08/12/2014 2137
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1554 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 2.0 1ug/L0.0270.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.0270.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.0550.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.170.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.200.50
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.0170.50
sec-Butylbenzene 135-98-8 SM 6200B-20 1.4 1ug/L0.0100.50
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L0.0370.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.170.50
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L0.170.50
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.170.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.0590.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.0190.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.0610.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.0940.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.170.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 1.3 1ug/L0.0230.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.0870.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.0790.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.0810.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.0190.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.0600.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.0740.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.0900.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.180.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 0.59 1ug/L0.0520.50
Ethylbenzene 100-41-4 SM 6200B-20 0.31 J 1ug/L0.170.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.170.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 0.69 1ug/L0.0290.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.0180.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 1.4 1ug/L0.0190.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.170.50
Naphthalene 91-20-3 SM 6200B-20 ND 1ug/L0.170.50
n-Propylbenzene 103-65-1 SM 6200B-20 ND 1ug/L0.0240.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.0150.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-9
PH14008-006
08/12/2014 2137
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 08/21/2014 1554 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.0570.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.0140.50
Toluene 108-88-3 SM 6200B-20 0.18 J 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.300.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.0310.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.0510.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.330.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.170.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 ND 1ug/L0.170.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.0650.50
m+p - Xylenes 179601-23-1 SM 6200B-20 0.45 J 1ug/L0.170.50
o - Xylenes 95-47-6 SM 6200B-20 ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-12
PH14008-007
08/12/2014 2224
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 2030 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B-20 7800 1ug/L1.425
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L1.425
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L2.825
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L8.525
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.5125
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L1025
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.8425
sec-Butylbenzene 135-98-8 SM 6200B-20 21 J 1ug/L0.5225
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L1.925
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L4.325
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L8.525
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L8.525
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L8.525
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L8.725
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L3.025
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.9525
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L8.525
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L3.125
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L4.725
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L8.525
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L8.525
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L8.525
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L3.525
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L2.725
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L1.225
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L4.725
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L4.425
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L4.025
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L4.125
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.9525
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L3.025
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L3.725
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L4.525
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L9.025
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 46 1ug/L2.625
Ethylbenzene 100-41-4 SM 6200B-20 2900 1ug/L8.525
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L8.525
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 160 1ug/L1.425
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.8925
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 99 1ug/L0.9525
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L8.525
Naphthalene 91-20-3 SM 6200B-20 330 1ug/L8.525
n-Propylbenzene 103-65-1 SM 6200B-20 360 1ug/L1.225
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.7525
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Terracon Consultants, Inc.
MW-12
PH14008-007
08/12/2014 2224
08/14/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 08/21/2014 2030 EH1 54542
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L2.925
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.6525
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.7225
Toluene 108-88-3 SM 6200B-20 3600 1ug/L8.525
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L1525
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L8.525
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L8.525
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L1.425
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L1.625
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L1.225
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L2.525
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L1725
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 640 1ug/L8.525
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 2200 1ug/L8.525
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L3.325
m+p - Xylenes 179601-23-1 SM 6200B-20 6000 1ug/L8.525
o - Xylenes 95-47-6 SM 6200B-20 2700 1ug/L8.525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 20 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ54542-001
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Benzene ND 08/21/2014 12420.50 0.027 ug/L1
Bromobenzene ND 08/21/2014 12420.50 0.027 ug/L1
Bromochloromethane ND 08/21/2014 12420.50 0.055 ug/L1
Bromodichloromethane ND 08/21/2014 12420.50 0.17 ug/L1
Bromoform ND 08/21/2014 12420.50 0.010 ug/L1
Bromomethane (Methyl bromide)ND 08/21/2014 12420.50 0.20 ug/L1
tert-Butylbenzene ND 08/21/2014 12420.50 0.037 ug/L1
sec-Butylbenzene ND 08/21/2014 12420.50 0.010 ug/L1
n-Butylbenzene ND 08/21/2014 12420.50 0.017 ug/L1
Carbon tetrachloride ND 08/21/2014 12420.50 0.085 ug/L1
Chlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
Chloroethane ND 08/21/2014 12420.50 0.17 ug/L1
Chloroform ND 08/21/2014 12420.50 0.17 ug/L1
Chloromethane (Methyl chloride)ND 08/21/2014 12420.50 0.17 ug/L1
4-Chlorotoluene ND 08/21/2014 12420.50 0.019 ug/L1
2-Chlorotoluene ND 08/21/2014 12420.50 0.059 ug/L1
Dibromochloromethane ND 08/21/2014 12420.50 0.17 ug/L1
1,2-Dibromoethane (EDB)ND 08/21/2014 12420.50 0.061 ug/L1
Dibromomethane (Methylene bromide)ND 08/21/2014 12420.50 0.094 ug/L1
1,4-Dichlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
1,3-Dichlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
1,2-Dichlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
Dichlorodifluoromethane ND 08/21/2014 12420.50 0.071 ug/L1
1,2-Dichloroethane ND 08/21/2014 12420.50 0.023 ug/L1
1,1-Dichloroethane ND 08/21/2014 12420.50 0.054 ug/L1
trans-1,2-Dichloroethene ND 08/21/2014 12420.50 0.079 ug/L1
cis-1,2-Dichloroethene ND 08/21/2014 12420.50 0.087 ug/L1
1,1-Dichloroethene ND 08/21/2014 12420.50 0.094 ug/L1
2,2-Dichloropropane ND 08/21/2014 12420.50 0.060 ug/L1
1,3-Dichloropropane ND 08/21/2014 12420.50 0.019 ug/L1
1,2-Dichloropropane ND 08/21/2014 12420.50 0.081 ug/L1
trans-1,3-Dichloropropene ND 08/21/2014 12420.50 0.18 ug/L1
cis-1,3-Dichloropropene ND 08/21/2014 12420.50 0.090 ug/L1
1,1-Dichloropropene ND 08/21/2014 12420.50 0.074 ug/L1
Diisopropyl ether (IPE)ND 08/21/2014 12420.50 0.052 ug/L1
Ethylbenzene ND 08/21/2014 12420.50 0.17 ug/L1
Hexachlorobutadiene ND 08/21/2014 12420.50 0.17 ug/L1
Isopropylbenzene (Cumene)ND 08/21/2014 12420.50 0.029 ug/L1
p-Isopropyltoluene (p-Cymene)ND 08/21/2014 12420.50 0.018 ug/L1
Methyl tertiary butyl ether (MTBE)ND 08/21/2014 12420.50 0.019 ug/L1
Methylene chloride ND 08/21/2014 12420.50 0.17 ug/L1
Naphthalene ND 08/21/2014 12420.50 0.17 ug/L1
n-Propylbenzene ND 08/21/2014 12420.50 0.024 ug/L1
Styrene ND 08/21/2014 12420.50 0.015 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ54542-001
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,1,2,2-Tetrachloroethane ND 08/21/2014 12420.50 0.013 ug/L1
1,1,1,2-Tetrachloroethane ND 08/21/2014 12420.50 0.057 ug/L1
Tetrachloroethene ND 08/21/2014 12420.50 0.014 ug/L1
Toluene ND 08/21/2014 12420.50 0.17 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/21/2014 12420.50 0.30 ug/L1
1,2,4-Trichlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
1,2,3-Trichlorobenzene ND 08/21/2014 12420.50 0.17 ug/L1
1,1,2-Trichloroethane ND 08/21/2014 12420.50 0.031 ug/L1
1,1,1-Trichloroethane ND 08/21/2014 12420.50 0.029 ug/L1
Trichloroethene ND 08/21/2014 12420.50 0.024 ug/L1
Trichlorofluoromethane ND 08/21/2014 12420.50 0.051 ug/L1
1,2,3-Trichloropropane ND 08/21/2014 12420.50 0.33 ug/L1
1,2,4-Trimethylbenzene ND 08/21/2014 12420.50 0.17 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 08/21/2014 12420.50 0.17 ug/L1
Vinyl chloride ND 08/21/2014 12420.50 0.065 ug/L1
o - Xylenes ND 08/21/2014 12420.50 0.17 ug/L1
m+p - Xylenes ND 08/21/2014 12420.50 0.17 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ54542-002
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 49 08/21/2014 1108995070-1301
Bromobenzene 49 08/21/2014 1108995070-1301
Bromochloromethane 50 08/21/2014 11081015070-1301
Bromodichloromethane 51 08/21/2014 11081025070-1301
Bromoform 53 08/21/2014 11081065070-1301
Bromomethane (Methyl bromide)46 08/21/2014 1108925060-1401
tert-Butylbenzene 49 08/21/2014 1108985070-1301
sec-Butylbenzene 48 08/21/2014 1108975070-1301
n-Butylbenzene 50 08/21/2014 11081015070-1301
Carbon tetrachloride 52 08/21/2014 11081035070-1301
Chlorobenzene 49 08/21/2014 1108995070-1301
Chloroethane 48 08/21/2014 1108965042-1631
Chloroform 50 08/21/2014 1108995070-1301
Chloromethane (Methyl chloride)49 08/21/2014 1108975020-1581
4-Chlorotoluene 50 08/21/2014 1108995070-1301
2-Chlorotoluene 47 08/21/2014 1108955070-1301
Dibromochloromethane 52 08/21/2014 11081055070-1301
1,2-Dibromoethane (EDB)50 08/21/2014 11081005070-1301
Dibromomethane (Methylene bromide)49 08/21/2014 1108985070-1301
1,4-Dichlorobenzene 49 08/21/2014 1108985070-1301
1,3-Dichlorobenzene 49 08/21/2014 1108985070-1301
1,2-Dichlorobenzene 50 08/21/2014 1108995070-1301
Dichlorodifluoromethane 50 08/21/2014 1108995060-1401
1,2-Dichloroethane 49 08/21/2014 1108985070-1301
1,1-Dichloroethane 50 08/21/2014 11081005070-1301
trans-1,2-Dichloroethene 51 08/21/2014 11081015070-1301
cis-1,2-Dichloroethene 50 08/21/2014 1108995070-1301
1,1-Dichloroethene 52 08/21/2014 11081035070-1301
2,2-Dichloropropane 55 08/21/2014 11081105070-1301
1,3-Dichloropropane 49 08/21/2014 1108985070-1301
1,2-Dichloropropane 49 08/21/2014 1108995070-1301
trans-1,3-Dichloropropene 52 08/21/2014 11081045070-1301
cis-1,3-Dichloropropene 52 08/21/2014 11081055070-1301
1,1-Dichloropropene 49 08/21/2014 1108985070-1301
Diisopropyl ether (IPE)50 08/21/2014 11081005070-1301
Ethylbenzene 50 08/21/2014 1108995070-1301
Hexachlorobutadiene 52 08/21/2014 11081045070-1301
Isopropylbenzene (Cumene)48 08/21/2014 1108975070-1301
p-Isopropyltoluene (p-Cymene)50 08/21/2014 11081005070-1301
Methyl tertiary butyl ether (MTBE)49 08/21/2014 1108995070-1301
Methylene chloride 49 08/21/2014 1108985070-1301
Naphthalene 53 08/21/2014 11081055050-1401
n-Propylbenzene 48 08/21/2014 1108975070-1301
Styrene 52 08/21/2014 11081045070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ54542-002
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,2,2-Tetrachloroethane 48 08/21/2014 1108965070-1301
1,1,1,2-Tetrachloroethane 51 08/21/2014 11081015070-1301
Tetrachloroethene 49 08/21/2014 1108985070-1301
Toluene 50 08/21/2014 1108995070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 64 08/21/2014 11081295070-1301
1,2,4-Trichlorobenzene 52 08/21/2014 11081055070-1301
1,2,3-Trichlorobenzene 53 08/21/2014 11081055070-1301
1,1,2-Trichloroethane 49 08/21/2014 1108985070-1301
1,1,1-Trichloroethane 51 08/21/2014 11081025070-1301
Trichloroethene 50 08/21/2014 1108995070-1301
Trichlorofluoromethane 49 08/21/2014 1108985060-1401
1,2,3-Trichloropropane 48 08/21/2014 1108965070-1301
1,2,4-Trimethylbenzene 49 08/21/2014 1108995070-1301
1,3,5-Trimethylbenzene (Mesitylene)49 08/21/2014 1108995070-1301
Vinyl chloride 50 08/21/2014 1108995060-1401
o - Xylenes 50 08/21/2014 1108995070-1301
m+p - Xylenes 50 08/21/2014 11081005070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:PQ54542-003
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Benzene 49 08/21/2014 1131985070-1300.38 201
Bromobenzene 50 08/21/2014 1131995070-1300.58 201
Bromochloromethane 51 08/21/2014 11311015070-1300.14 201
Bromodichloromethane 52 08/21/2014 11311035070-1300.70 201
Bromoform 54 08/21/2014 11311085070-1301.8 201
Bromomethane (Methyl bromide)48 08/21/2014 1131965060-1404.1 201
tert-Butylbenzene 49 08/21/2014 1131995070-1300.72 201
sec-Butylbenzene 49 08/21/2014 1131995070-1302.0 201
n-Butylbenzene 51 08/21/2014 11311025070-1301.1 201
Carbon tetrachloride 51 08/21/2014 11311035070-1300.45 201
Chlorobenzene 50 08/21/2014 11311005070-1300.60 201
Chloroethane 49 08/21/2014 1131985042-1632.5 201
Chloroform 50 08/21/2014 1131995070-1300.028 201
Chloromethane (Methyl chloride)46 08/21/2014 1131935020-1584.4 201
4-Chlorotoluene 51 08/21/2014 11311025070-1302.7 201
2-Chlorotoluene 49 08/21/2014 1131975070-1302.8 201
Dibromochloromethane 53 08/21/2014 11311065070-1300.99 201
1,2-Dibromoethane (EDB)50 08/21/2014 11311015070-1301.4 201
Dibromomethane (Methylene bromide)49 08/21/2014 1131985070-1300.11 201
1,4-Dichlorobenzene 49 08/21/2014 1131995070-1300.97 201
1,3-Dichlorobenzene 49 08/21/2014 1131995070-1300.13 201
1,2-Dichlorobenzene 50 08/21/2014 11311005070-1300.88 201
Dichlorodifluoromethane 48 08/21/2014 1131965060-1403.2 201
1,2-Dichloroethane 49 08/21/2014 1131985070-1300.11 201
1,1-Dichloroethane 50 08/21/2014 11311005070-1300.42 201
trans-1,2-Dichloroethene 51 08/21/2014 11311015070-1300.24 201
cis-1,2-Dichloroethene 50 08/21/2014 11311005070-1300.62 201
1,1-Dichloroethene 52 08/21/2014 11311045070-1301.1 201
2,2-Dichloropropane 52 08/21/2014 11311055070-1304.9 201
1,3-Dichloropropane 49 08/21/2014 1131985070-1300.16 201
1,2-Dichloropropane 49 08/21/2014 1131985070-1300.31 201
trans-1,3-Dichloropropene 53 08/21/2014 11311055070-1301.4 201
cis-1,3-Dichloropropene 52 08/21/2014 11311055070-1300.038 201
1,1-Dichloropropene 50 08/21/2014 1131995070-1300.83 201
Diisopropyl ether (IPE)53 08/21/2014 11311065070-1305.3 201
Ethylbenzene 50 08/21/2014 11311015070-1301.8 201
Hexachlorobutadiene 51 08/21/2014 11311035070-1301.3 201
Isopropylbenzene (Cumene)50 08/21/2014 1131995070-1303.0 201
p-Isopropyltoluene (p-Cymene)51 08/21/2014 11311015070-1301.0 201
Methyl tertiary butyl ether (MTBE)52 08/21/2014 11311045070-1305.5 201
Methylene chloride 48 08/21/2014 1131975070-1301.6 201
Naphthalene 51 08/21/2014 11311035050-1402.2 201
n-Propylbenzene 49 08/21/2014 1131995070-1302.4 201
Styrene 52 08/21/2014 11311045070-1300.10 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:PQ54542-003
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
1,1,2,2-Tetrachloroethane 49 08/21/2014 1131975070-1301.5 201
1,1,1,2-Tetrachloroethane 51 08/21/2014 11311035070-1301.2 201
Tetrachloroethene 50 08/21/2014 1131995070-1301.0 201
Toluene 50 08/21/2014 11311005070-1300.15 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 59 08/21/2014 11311195070-1308.1 201
1,2,4-Trichlorobenzene 51 08/21/2014 11311025070-1302.6 201
1,2,3-Trichlorobenzene 50 08/21/2014 11311005070-1304.7 201
1,1,2-Trichloroethane 50 08/21/2014 11311005070-1301.3 201
1,1,1-Trichloroethane 50 08/21/2014 11311015070-1300.80 201
Trichloroethene 50 08/21/2014 11311005070-1300.49 201
Trichlorofluoromethane 50 08/21/2014 11311015060-1403.1 201
1,2,3-Trichloropropane 49 08/21/2014 1131985070-1302.8 201
1,2,4-Trimethylbenzene 49 08/21/2014 1131995070-1300.45 201
1,3,5-Trimethylbenzene (Mesitylene)50 08/21/2014 11311015070-1302.0 201
Vinyl chloride 48 08/21/2014 1131955060-1403.9 201
o - Xylenes 50 08/21/2014 11311015070-1301.7 201
m+p - Xylenes 50 08/21/2014 11311015070-1301.2 201
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:PH14008-007MS
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 10000 08/21/2014 2053E97250070-130780050
Bromobenzene 2500 08/21/2014 2053100250070-130ND50
Bromochloromethane 2300 08/21/2014 205393250070-130ND50
Bromodichloromethane 2500 08/21/2014 2053100250070-130ND50
Bromoform 2400 08/21/2014 205394250070-130ND50
Bromomethane (Methyl bromide)2500 08/21/2014 205398250060-140ND50
n-Butylbenzene 2700 08/21/2014 2053108250070-130ND50
sec-Butylbenzene 2600 08/21/2014 2053104250070-1302150
tert-Butylbenzene 2900 08/21/2014 2053116250070-130ND50
Carbon tetrachloride 2600 08/21/2014 2053104250070-130ND50
Chlorobenzene 2500 08/21/2014 2053101250070-130ND50
Chloroethane 2700 08/21/2014 2053109250042-163ND50
Chloroform 2500 08/21/2014 205399250070-130ND50
Chloromethane (Methyl chloride)2400 08/21/2014 205394250020-158ND50
2-Chlorotoluene 2800 08/21/2014 2053111250070-130ND50
4-Chlorotoluene 2600 08/21/2014 2053103250070-130ND50
Dibromochloromethane 2500 08/21/2014 2053100250070-130ND50
1,2-Dibromoethane (EDB)2400 08/21/2014 205396250070-130ND50
Dibromomethane (Methylene bromide)2300 08/21/2014 205393250070-130ND50
1,2-Dichlorobenzene 2500 08/21/2014 205399250070-130ND50
1,3-Dichlorobenzene 2500 08/21/2014 205399250070-130ND50
1,4-Dichlorobenzene 2500 08/21/2014 205399250070-130ND50
Dichlorodifluoromethane 2600 08/21/2014 2053103250060-140ND50
1,1-Dichloroethane 2600 08/21/2014 2053102250070-130ND50
1,2-Dichloroethane 2700 08/21/2014 2053107250070-130ND50
1,1-Dichloroethene 2800 08/21/2014 2053112250070-130ND50
cis-1,2-Dichloroethene 2500 08/21/2014 205399250070-130ND50
trans-1,2-Dichloroethene 2600 08/21/2014 2053103250070-130ND50
1,2-Dichloropropane 2500 08/21/2014 205399250070-130ND50
1,3-Dichloropropane 2400 08/21/2014 205396250070-130ND50
2,2-Dichloropropane 2100 08/21/2014 205385250070-130ND50
1,1-Dichloropropene 2600 08/21/2014 2053103250070-130ND50
cis-1,3-Dichloropropene 2400 08/21/2014 205397250070-130ND50
trans-1,3-Dichloropropene 2400 08/21/2014 205397250070-130ND50
Diisopropyl ether (IPE)2600 08/21/2014 2053101250070-1304650
Ethylbenzene 5600 08/21/2014 2053109250070-130290050
Hexachlorobutadiene 2700 08/21/2014 2053108250070-130ND50
Isopropylbenzene (Cumene)2700 08/21/2014 2053103250070-13016050
p-Isopropyltoluene (p-Cymene)2700 08/21/2014 2053107250070-130ND50
Methyl tertiary butyl ether (MTBE)2400 08/21/2014 205392250070-1309950
Methylene chloride 2500 08/21/2014 2053100250070-130ND50
Naphthalene 2900 08/21/2014 2053102250050-14033050
n-Propylbenzene 2900 08/21/2014 2053103250070-13036050
Styrene 2700 08/21/2014 2053107250070-130ND50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:PH14008-007MS
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 2500 08/21/2014 2053101250070-130ND50
1,1,2,2-Tetrachloroethane 2300 08/21/2014 205390250070-130ND50
Tetrachloroethene 2600 08/21/2014 2053104250070-130ND50
Toluene 6200 08/21/2014 2053101250070-130360050
1,1,2-Trichloro-1,2,2-Trifluoroethane 3100 08/21/2014 2053124250070-130ND50
1,2,3-Trichlorobenzene 2700 08/21/2014 2053107250070-130ND50
1,2,4-Trichlorobenzene 2700 08/21/2014 2053106250070-130ND50
1,1,1-Trichloroethane 2600 08/21/2014 2053103250070-130ND50
1,1,2-Trichloroethane 2400 08/21/2014 205396250070-130ND50
Trichloroethene 2600 08/21/2014 2053103250070-130ND50
Trichlorofluoromethane 2700 08/21/2014 2053107250060-140ND50
1,2,3-Trichloropropane 2200 08/21/2014 205388250070-130ND50
1,3,5-Trimethylbenzene (Mesitylene)3300 08/21/2014 2053106250070-13064050
1,2,4-Trimethylbenzene 4800 08/21/2014 2053103250070-130220050
Vinyl chloride 2600 08/21/2014 2053103250060-140ND50
m+p - Xylenes 8700 08/21/2014 2053110250070-130600050
o - Xylenes 5300 08/21/2014 2053104250070-130270050
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 93 70-130
Bromofluorobenzene 97 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:PH14008-007MD
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 10000 08/21/2014 2116E93250070-1301.1 20780050
Bromobenzene 2500 08/21/2014 211698250070-1301.7 20ND50
Bromochloromethane 2400 08/21/2014 211697250070-1304.5 20ND50
Bromodichloromethane 2500 08/21/2014 2116101250070-1300.89 20ND50
Bromoform 2400 08/21/2014 211695250070-1301.2 20ND50
Bromomethane (Methyl bromide)2400 08/21/2014 211696250060-1402.1 20ND50
n-Butylbenzene 2500 08/21/2014 2116102250070-1305.4 20ND50
sec-Butylbenzene 2500 08/21/2014 211698250070-1306.2 202150
tert-Butylbenzene 2800 08/21/2014 2116110250070-1305.2 20ND50
Carbon tetrachloride 2500 08/21/2014 2116101250070-1303.2 20ND50
Chlorobenzene 2500 08/21/2014 211699250070-1302.8 20ND50
Chloroethane 2700 08/21/2014 2116107250042-1631.6 20ND50
Chloroform 2500 08/21/2014 211698250070-1300.89 20ND50
Chloromethane (Methyl chloride)2300 08/21/2014 211691250020-1584.1 20ND50
2-Chlorotoluene 2700 08/21/2014 2116107250070-1303.7 20ND50
4-Chlorotoluene 2500 08/21/2014 211698250070-1304.2 20ND50
Dibromochloromethane 2500 08/21/2014 2116101250070-1300.39 20ND50
1,2-Dibromoethane (EDB)2400 08/21/2014 211697250070-1301.1 20ND50
Dibromomethane (Methylene bromide)2300 08/21/2014 211694250070-1300.55 20ND50
1,2-Dichlorobenzene 2400 08/21/2014 211697250070-1301.8 20ND50
1,3-Dichlorobenzene 2400 08/21/2014 211697250070-1302.3 20ND50
1,4-Dichlorobenzene 2400 08/21/2014 211695250070-1303.4 20ND50
Dichlorodifluoromethane 2400 08/21/2014 211697250060-1406.7 20ND50
1,1-Dichloroethane 2500 08/21/2014 2116100250070-1301.9 20ND50
1,2-Dichloroethane 2700 08/21/2014 2116109250070-1302.3 20ND50
1,1-Dichloroethene 2700 08/21/2014 2116110250070-1301.8 20ND50
cis-1,2-Dichloroethene 2500 08/21/2014 211698250070-1301.0 20ND50
trans-1,2-Dichloroethene 2500 08/21/2014 2116101250070-1301.8 20ND50
1,2-Dichloropropane 2400 08/21/2014 211698250070-1300.89 20ND50
1,3-Dichloropropane 2400 08/21/2014 211696250070-1300.18 20ND50
2,2-Dichloropropane 2100 08/21/2014 211682250070-1303.3 20ND50
1,1-Dichloropropene 2500 08/21/2014 211699250070-1303.8 20ND50
cis-1,3-Dichloropropene 2400 08/21/2014 211697250070-1300.36 20ND50
trans-1,3-Dichloropropene 2400 08/21/2014 211697250070-1300.18 20ND50
Diisopropyl ether (IPE)2500 08/21/2014 2116100250070-1301.1 204650
Ethylbenzene 5400 08/21/2014 2116102250070-1303.2 20290050
Hexachlorobutadiene 2600 08/21/2014 2116103250070-1304.4 20ND50
Isopropylbenzene (Cumene)2600 08/21/2014 211699250070-1304.4 2016050
p-Isopropyltoluene (p-Cymene)2500 08/21/2014 2116100250070-1306.1 20ND50
Methyl tertiary butyl ether (MTBE)2400 08/21/2014 211693250070-1301.5 209950
Methylene chloride 2500 08/21/2014 2116100250070-1300.18 20ND50
Naphthalene 2900 08/21/2014 2116104250050-1402.4 2033050
n-Propylbenzene 2800 08/21/2014 211697250070-1304.8 2036050
Styrene 2600 08/21/2014 2116105250070-1301.8 20ND50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:PH14008-007MD
54542 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 2500 08/21/2014 2116101250070-1300.45 20ND50
1,1,2,2-Tetrachloroethane 2300 08/21/2014 211691250070-1300.49 20ND50
Tetrachloroethene 2500 08/21/2014 2116100250070-1304.0 20ND50
Toluene 6100 08/21/2014 211698250070-1301.3 20360050
1,1,2-Trichloro-1,2,2-Trifluoroethane 3100 08/21/2014 2116125250070-1300.80 20ND50
1,2,3-Trichlorobenzene 2700 08/21/2014 2116108250070-1300.15 20ND50
1,2,4-Trichlorobenzene 2600 08/21/2014 2116104250070-1301.6 20ND50
1,1,1-Trichloroethane 2500 08/21/2014 2116102250070-1301.2 20ND50
1,1,2-Trichloroethane 2400 08/21/2014 211697250070-1300.97 20ND50
Trichloroethene 2500 08/21/2014 2116100250070-1302.7 20ND50
Trichlorofluoromethane 2500 08/21/2014 2116101250060-1405.5 20ND50
1,2,3-Trichloropropane 2200 08/21/2014 211690250070-1302.0 20ND50
1,3,5-Trimethylbenzene (Mesitylene)3100 08/21/2014 2116100250070-1304.9 2064050
1,2,4-Trimethylbenzene 4600 08/21/2014 211697250070-1303.3 20220050
Vinyl chloride 2500 08/21/2014 2116101250060-1402.5 20ND50
m+p - Xylenes 8500 08/21/2014 2116102250070-1302.1 20600050
o - Xylenes 5200 08/21/2014 211699250070-1302.6 20270050
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 30
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1