WS-6406_24174_CA_LAB_20101222

December 22, 2010
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9284004
9284004
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR-UST Section
1637 Mail Service Center
Raleigh, NC 27699
CARAWAY GROCERY 2010296
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9284004001 3337 OLD LEXINGTON RD SM 6200B 64 PASI-CTLS
9284004002 3338 OLD LEXINGTON RD SM 6200B 64 PASI-CTLS
9284004003 3354 OLD LEXINGTON RD SM 6200B 64 PASI-CTLS
9284004004 3334 OLD LEXINGTON RD SM 6200B 64 PASI-CTLS
9284004005 3256 OLD LEXINGTON RD SM 6200B 64 PASI-CTLS
9284004006 1275 BACK CREEK RD.SM 6200B 64 PASI-CTLS
9284004007 2353 SMYRNA GROVE DR.SM 6200B 64 PASI-CTLS
9284004008 SMYRNA GROVE MHP-LOT 2 SM 6200B 64 PASI-CTLS
9284004009 SMYRNA GROVE MHP-LOT 6 SM 6200B 64 PASI-CTLS
9284004010 1255 BACK CREEK RD.SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Method:
Client:Pyramid_FTF
SM 6200B
Date:December 22, 2010
Description:6200B MSV
General Information:
10 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: MSV/13444
CH: The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.
• LCS (Lab ID: 541051)
• Chloromethane
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: MSV/13468
L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: 542095)
• Dichlorodifluoromethane
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3337 OLD LEXINGTON RD Lab ID:9284004001 Collected:12/10/10 14:15 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 21:07 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 21:07 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 21:07 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 21:07 75-27-40.50
Bromoform ND ug/L 1 12/16/10 21:07 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 21:07 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 21:07 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 21:07 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 21:07 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 21:07 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 21:07 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 21:07 75-00-31.0
Chloroform ND ug/L 1 12/16/10 21:07 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 21:07 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 21:07 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 21:07 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 21:07 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 21:07 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 21:07 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 21:07 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 21:07 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 21:07 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 21:07 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 21:07 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 21:07 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 21:07 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 21:07 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 21:07 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 21:07 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 21:07 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 21:07 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 21:07 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 21:07 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 21:07 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 21:07 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 21:07 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 21:07 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 21:07 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 21:07 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 21:07 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 21:07 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 21:07 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 21:07 103-65-10.50
Styrene ND ug/L 1 12/16/10 21:07 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 21:07 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 21:07 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 21:07 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 5 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3337 OLD LEXINGTON RD Lab ID:9284004001 Collected:12/10/10 14:15 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 21:07 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 21:07 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 21:07 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 21:07 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 21:07 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 21:07 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 21:07 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 21:07 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 21:07 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 21:07 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 21:07 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 21:07 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 21:07 95-47-60.50
1,2-Dichloroethane-d4 (S)104 %1 12/16/10 21:07 17060-07-070-130
Dibromofluoromethane (S)106 %1 12/16/10 21:07 1868-53-770-130
4-Bromofluorobenzene (S)98 %1 12/16/10 21:07 460-00-470-130
Toluene-d8 (S)98 %1 12/16/10 21:07 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 6 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3338 OLD LEXINGTON RD Lab ID:9284004002 Collected:12/10/10 14:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 01:22 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 01:22 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 01:22 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 01:22 75-27-40.50
Bromoform ND ug/L 1 12/16/10 01:22 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 01:22 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 01:22 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 01:22 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 01:22 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 01:22 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 01:22 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 01:22 75-00-31.0
Chloroform 0.83 ug/L 1 12/16/10 01:22 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 01:22 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 01:22 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 01:22 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 01:22 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 01:22 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 01:22 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 01:22 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 01:22 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 01:22 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 01:22 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 01:22 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 01:22 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 01:22 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 01:22 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 01:22 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 01:22 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 01:22 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 01:22 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 01:22 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 01:22 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 01:22 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 01:22 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 01:22 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 01:22 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 01:22 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 01:22 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 01:22 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 01:22 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 01:22 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 01:22 103-65-10.50
Styrene ND ug/L 1 12/16/10 01:22 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 01:22 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 01:22 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 01:22 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 7 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3338 OLD LEXINGTON RD Lab ID:9284004002 Collected:12/10/10 14:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 01:22 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 01:22 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 01:22 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 01:22 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 01:22 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 01:22 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 01:22 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 01:22 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 01:22 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 01:22 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 01:22 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 01:22 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 01:22 95-47-60.50
1,2-Dichloroethane-d4 (S)114 %1 12/16/10 01:22 17060-07-070-130
Dibromofluoromethane (S)115 %1 12/16/10 01:22 1868-53-770-130
4-Bromofluorobenzene (S)95 %1 12/16/10 01:22 460-00-470-130
Toluene-d8 (S)102 %1 12/16/10 01:22 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 8 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3354 OLD LEXINGTON RD Lab ID:9284004003 Collected:12/10/10 14:35 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 21:30 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 21:30 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 21:30 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 21:30 75-27-40.50
Bromoform ND ug/L 1 12/16/10 21:30 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 21:30 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 21:30 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 21:30 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 21:30 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 21:30 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 21:30 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 21:30 75-00-31.0
Chloroform ND ug/L 1 12/16/10 21:30 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 21:30 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 21:30 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 21:30 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 21:30 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 21:30 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 21:30 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 21:30 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 21:30 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 21:30 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 21:30 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 21:30 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 21:30 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 21:30 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 21:30 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 21:30 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 21:30 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 21:30 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 21:30 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 21:30 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 21:30 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 21:30 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 21:30 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 21:30 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 21:30 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 21:30 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 21:30 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 21:30 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 21:30 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 21:30 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 21:30 103-65-10.50
Styrene ND ug/L 1 12/16/10 21:30 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 21:30 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 21:30 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 21:30 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 9 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3354 OLD LEXINGTON RD Lab ID:9284004003 Collected:12/10/10 14:35 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 21:30 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 21:30 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 21:30 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 21:30 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 21:30 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 21:30 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 21:30 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 21:30 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 21:30 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 21:30 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 21:30 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 21:30 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 21:30 95-47-60.50
1,2-Dichloroethane-d4 (S)106 %1 12/16/10 21:30 17060-07-070-130
Dibromofluoromethane (S)107 %1 12/16/10 21:30 1868-53-770-130
4-Bromofluorobenzene (S)98 %1 12/16/10 21:30 460-00-470-130
Toluene-d8 (S)100 %1 12/16/10 21:30 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 10 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3334 OLD LEXINGTON RD Lab ID:9284004004 Collected:12/10/10 14:45 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 02:08 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 02:08 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 02:08 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 02:08 75-27-40.50
Bromoform ND ug/L 1 12/16/10 02:08 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 02:08 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 02:08 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 02:08 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 02:08 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 02:08 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 02:08 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 02:08 75-00-31.0
Chloroform 0.65 ug/L 1 12/16/10 02:08 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 02:08 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 02:08 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 02:08 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 02:08 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 02:08 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 02:08 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 02:08 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 02:08 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 02:08 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 02:08 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 02:08 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 02:08 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 02:08 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 02:08 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 02:08 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 02:08 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 02:08 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 02:08 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 02:08 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 02:08 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 02:08 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 02:08 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 02:08 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 02:08 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 02:08 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 02:08 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 02:08 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 02:08 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 02:08 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 02:08 103-65-10.50
Styrene ND ug/L 1 12/16/10 02:08 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 02:08 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 02:08 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 02:08 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 11 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3334 OLD LEXINGTON RD Lab ID:9284004004 Collected:12/10/10 14:45 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 02:08 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 02:08 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 02:08 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 02:08 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 02:08 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 02:08 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 02:08 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 02:08 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 02:08 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 02:08 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 02:08 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 02:08 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 02:08 95-47-60.50
1,2-Dichloroethane-d4 (S)116 %1 12/16/10 02:08 17060-07-070-130
Dibromofluoromethane (S)111 %1 12/16/10 02:08 1868-53-770-130
4-Bromofluorobenzene (S)95 %1 12/16/10 02:08 460-00-470-130
Toluene-d8 (S)103 %1 12/16/10 02:08 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 12 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3256 OLD LEXINGTON RD Lab ID:9284004005 Collected:12/10/10 15:05 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 02:31 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 02:31 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 02:31 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 02:31 75-27-40.50
Bromoform ND ug/L 1 12/16/10 02:31 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 02:31 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 02:31 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 02:31 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 02:31 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 02:31 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 02:31 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 02:31 75-00-31.0
Chloroform 0.70 ug/L 1 12/16/10 02:31 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 02:31 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 02:31 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 02:31 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 02:31 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 02:31 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 02:31 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 02:31 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 02:31 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 02:31 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 02:31 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 02:31 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 02:31 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 02:31 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 02:31 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 02:31 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 02:31 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 02:31 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 02:31 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 02:31 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 02:31 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 02:31 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 02:31 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 02:31 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 02:31 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 02:31 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 02:31 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 02:31 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 02:31 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 02:31 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 02:31 103-65-10.50
Styrene ND ug/L 1 12/16/10 02:31 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 02:31 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 02:31 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 02:31 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 13 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:3256 OLD LEXINGTON RD Lab ID:9284004005 Collected:12/10/10 15:05 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 02:31 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 02:31 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 02:31 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 02:31 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 02:31 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 02:31 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 02:31 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 02:31 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 02:31 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 02:31 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 02:31 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 02:31 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 02:31 95-47-60.50
1,2-Dichloroethane-d4 (S)117 %1 12/16/10 02:31 17060-07-070-130
Dibromofluoromethane (S)115 %1 12/16/10 02:31 1868-53-770-130
4-Bromofluorobenzene (S)92 %1 12/16/10 02:31 460-00-470-130
Toluene-d8 (S)103 %1 12/16/10 02:31 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 14 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:1275 BACK CREEK RD.Lab ID:9284004006 Collected:12/10/10 15:10 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 02:54 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 02:54 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 02:54 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 02:54 75-27-40.50
Bromoform ND ug/L 1 12/16/10 02:54 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 02:54 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 02:54 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 02:54 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 02:54 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 02:54 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 02:54 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 02:54 75-00-31.0
Chloroform 0.88 ug/L 1 12/16/10 02:54 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 02:54 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 02:54 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 02:54 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 02:54 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 02:54 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 02:54 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 02:54 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 02:54 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 02:54 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 02:54 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 02:54 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 02:54 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 02:54 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 02:54 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 02:54 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 02:54 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 02:54 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 02:54 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 02:54 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 02:54 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 02:54 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 02:54 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 02:54 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 02:54 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 02:54 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 02:54 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 02:54 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 02:54 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 02:54 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 02:54 103-65-10.50
Styrene ND ug/L 1 12/16/10 02:54 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 02:54 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 02:54 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 02:54 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 15 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:1275 BACK CREEK RD.Lab ID:9284004006 Collected:12/10/10 15:10 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 02:54 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 02:54 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 02:54 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 02:54 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 02:54 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 02:54 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 02:54 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 02:54 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 02:54 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 02:54 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 02:54 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 02:54 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 02:54 95-47-60.50
1,2-Dichloroethane-d4 (S)117 %1 12/16/10 02:54 17060-07-070-130
Dibromofluoromethane (S)113 %1 12/16/10 02:54 1868-53-770-130
4-Bromofluorobenzene (S)95 %1 12/16/10 02:54 460-00-470-130
Toluene-d8 (S)103 %1 12/16/10 02:54 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 16 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:2353 SMYRNA GROVE DR.Lab ID:9284004007 Collected:12/10/10 15:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 21:53 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 21:53 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 21:53 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 21:53 75-27-40.50
Bromoform ND ug/L 1 12/16/10 21:53 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 21:53 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 21:53 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 21:53 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 21:53 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 21:53 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 21:53 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 21:53 75-00-31.0
Chloroform ND ug/L 1 12/16/10 21:53 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 21:53 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 21:53 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 21:53 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 21:53 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 21:53 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 21:53 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 21:53 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 21:53 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 21:53 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 21:53 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 21:53 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 21:53 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 21:53 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 21:53 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 21:53 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 21:53 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 21:53 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 21:53 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 21:53 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 21:53 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 21:53 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 21:53 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 21:53 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 21:53 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 21:53 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 21:53 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 21:53 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 21:53 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 21:53 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 21:53 103-65-10.50
Styrene ND ug/L 1 12/16/10 21:53 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 21:53 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 21:53 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 21:53 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 17 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:2353 SMYRNA GROVE DR.Lab ID:9284004007 Collected:12/10/10 15:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 21:53 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 21:53 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 21:53 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 21:53 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 21:53 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 21:53 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 21:53 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 21:53 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 21:53 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 21:53 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 21:53 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 21:53 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 21:53 95-47-60.50
1,2-Dichloroethane-d4 (S)109 %1 12/16/10 21:53 17060-07-070-130
Dibromofluoromethane (S)107 %1 12/16/10 21:53 1868-53-770-130
4-Bromofluorobenzene (S)98 %1 12/16/10 21:53 460-00-470-130
Toluene-d8 (S)100 %1 12/16/10 21:53 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 18 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:SMYRNA GROVE MHP-
LOT 2
Lab ID:9284004008 Collected:12/10/10 15:50 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 03:39 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 03:39 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 03:39 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 03:39 75-27-40.50
Bromoform ND ug/L 1 12/16/10 03:39 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 03:39 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 03:39 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 03:39 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 03:39 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 03:39 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 03:39 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 03:39 75-00-31.0
Chloroform ND ug/L 1 12/16/10 03:39 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 03:39 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 03:39 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 03:39 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 03:39 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 03:39 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 03:39 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 03:39 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 03:39 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 03:39 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 03:39 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 03:39 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 03:39 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 03:39 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 03:39 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 03:39 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 03:39 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 03:39 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 03:39 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 03:39 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 03:39 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 03:39 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 03:39 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 03:39 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 03:39 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 03:39 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 03:39 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 03:39 75-09-22.0
Methyl-tert-butyl ether 0.93 ug/L 1 12/16/10 03:39 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 03:39 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 03:39 103-65-10.50
Styrene ND ug/L 1 12/16/10 03:39 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 03:39 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 03:39 79-34-50.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 19 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:SMYRNA GROVE MHP-
LOT 2
Lab ID:9284004008 Collected:12/10/10 15:50 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 12/16/10 03:39 127-18-40.50
Toluene ND ug/L 1 12/16/10 03:39 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 03:39 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 03:39 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 03:39 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 03:39 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 03:39 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 03:39 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 03:39 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 03:39 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 03:39 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 03:39 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 03:39 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 03:39 95-47-60.50
1,2-Dichloroethane-d4 (S)118 %1 12/16/10 03:39 17060-07-070-130
Dibromofluoromethane (S)113 %1 12/16/10 03:39 1868-53-770-130
4-Bromofluorobenzene (S)95 %1 12/16/10 03:39 460-00-470-130
Toluene-d8 (S)103 %1 12/16/10 03:39 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 20 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:SMYRNA GROVE MHP-
LOT 6
Lab ID:9284004009 Collected:12/10/10 16:10 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 04:02 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 04:02 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 04:02 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 04:02 75-27-40.50
Bromoform ND ug/L 1 12/16/10 04:02 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 04:02 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 04:02 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 04:02 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 04:02 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 04:02 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 04:02 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 04:02 75-00-31.0
Chloroform ND ug/L 1 12/16/10 04:02 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 04:02 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 04:02 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 04:02 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 04:02 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 04:02 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 04:02 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 04:02 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 04:02 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 04:02 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 04:02 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 04:02 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 04:02 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 04:02 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 04:02 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 04:02 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 04:02 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 04:02 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 04:02 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 04:02 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 04:02 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 04:02 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 04:02 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 04:02 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 04:02 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 04:02 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 04:02 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 04:02 75-09-22.0
Methyl-tert-butyl ether 0.50 ug/L 1 12/16/10 04:02 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 04:02 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 04:02 103-65-10.50
Styrene ND ug/L 1 12/16/10 04:02 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 04:02 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 04:02 79-34-50.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 21 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:SMYRNA GROVE MHP-
LOT 6
Lab ID:9284004009 Collected:12/10/10 16:10 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 12/16/10 04:02 127-18-40.50
Toluene ND ug/L 1 12/16/10 04:02 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 04:02 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 04:02 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 04:02 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 04:02 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 04:02 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 04:02 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 04:02 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 04:02 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 04:02 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 04:02 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 04:02 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 04:02 95-47-60.50
1,2-Dichloroethane-d4 (S)117 %1 12/16/10 04:02 17060-07-070-130
Dibromofluoromethane (S)114 %1 12/16/10 04:02 1868-53-770-130
4-Bromofluorobenzene (S)94 %1 12/16/10 04:02 460-00-470-130
Toluene-d8 (S)102 %1 12/16/10 04:02 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 22 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:1255 BACK CREEK RD.Lab ID:9284004010 Collected:12/10/10 16:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 12/16/10 04:25 71-43-20.50
Bromobenzene ND ug/L 1 12/16/10 04:25 108-86-10.50
Bromochloromethane ND ug/L 1 12/16/10 04:25 74-97-50.50
Bromodichloromethane ND ug/L 1 12/16/10 04:25 75-27-40.50
Bromoform ND ug/L 1 12/16/10 04:25 75-25-20.50
Bromomethane ND ug/L 1 12/16/10 04:25 74-83-95.0
n-Butylbenzene ND ug/L 1 12/16/10 04:25 104-51-80.50
sec-Butylbenzene ND ug/L 1 12/16/10 04:25 135-98-80.50
tert-Butylbenzene ND ug/L 1 12/16/10 04:25 98-06-60.50
Carbon tetrachloride ND ug/L 1 12/16/10 04:25 56-23-50.50
Chlorobenzene ND ug/L 1 12/16/10 04:25 108-90-70.50
Chloroethane ND ug/L 1 12/16/10 04:25 75-00-31.0
Chloroform ND ug/L 1 12/16/10 04:25 67-66-30.50
Chloromethane ND ug/L 1 12/16/10 04:25 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/16/10 04:25 95-49-80.50
4-Chlorotoluene ND ug/L 1 12/16/10 04:25 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 12/16/10 04:25 96-12-81.0
Dibromochloromethane ND ug/L 1 12/16/10 04:25 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 12/16/10 04:25 106-93-40.50
Dibromomethane ND ug/L 1 12/16/10 04:25 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 12/16/10 04:25 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 12/16/10 04:25 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 12/16/10 04:25 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 12/16/10 04:25 75-71-80.50
1,1-Dichloroethane ND ug/L 1 12/16/10 04:25 75-34-30.50
1,2-Dichloroethane ND ug/L 1 12/16/10 04:25 107-06-20.50
1,1-Dichloroethene ND ug/L 1 12/16/10 04:25 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 12/16/10 04:25 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 12/16/10 04:25 156-60-50.50
1,2-Dichloropropane ND ug/L 1 12/16/10 04:25 78-87-50.50
1,3-Dichloropropane ND ug/L 1 12/16/10 04:25 142-28-90.50
2,2-Dichloropropane ND ug/L 1 12/16/10 04:25 594-20-70.50
1,1-Dichloropropene ND ug/L 1 12/16/10 04:25 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 12/16/10 04:25 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 12/16/10 04:25 10061-02-60.50
Diisopropyl ether ND ug/L 1 12/16/10 04:25 108-20-30.50
Ethylbenzene ND ug/L 1 12/16/10 04:25 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 12/16/10 04:25 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 12/16/10 04:25 98-82-80.50
Methylene Chloride ND ug/L 1 12/16/10 04:25 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 12/16/10 04:25 1634-04-40.50
Naphthalene ND ug/L 1 12/16/10 04:25 91-20-32.0
n-Propylbenzene ND ug/L 1 12/16/10 04:25 103-65-10.50
Styrene ND ug/L 1 12/16/10 04:25 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 12/16/10 04:25 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 12/16/10 04:25 79-34-50.50
Tetrachloroethene ND ug/L 1 12/16/10 04:25 127-18-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 23 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Sample:1255 BACK CREEK RD.Lab ID:9284004010 Collected:12/10/10 16:30 Received:12/14/10 13:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 1 12/16/10 04:25 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 12/16/10 04:25 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 12/16/10 04:25 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 12/16/10 04:25 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 12/16/10 04:25 79-00-50.50
Trichloroethene ND ug/L 1 12/16/10 04:25 79-01-60.50
Trichlorofluoromethane ND ug/L 1 12/16/10 04:25 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/16/10 04:25 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 12/16/10 04:25 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 12/16/10 04:25 108-67-80.50
Vinyl chloride ND ug/L 1 12/16/10 04:25 75-01-41.0
m&p-Xylene ND ug/L 1 12/16/10 04:25 179601-23-11.0
o-Xylene ND ug/L 1 12/16/10 04:25 95-47-60.50
1,2-Dichloroethane-d4 (S)118 %1 12/16/10 04:25 17060-07-070-130
Dibromofluoromethane (S)112 %1 12/16/10 04:25 1868-53-770-130
4-Bromofluorobenzene (S)93 %1 12/16/10 04:25 460-00-470-130
Toluene-d8 (S)103 %1 12/16/10 04:25 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 24 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/13444
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9284004002, 9284004004, 9284004005, 9284004006, 9284004008, 9284004009, 9284004010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:541050
Associated Lab Samples:9284004002, 9284004004, 9284004005, 9284004006, 9284004008, 9284004009, 9284004010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/15/10 22:20
1,1,1-Trichloroethane ug/L ND 0.50 12/15/10 22:20
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/15/10 22:20
1,1,2-Trichloroethane ug/L ND 0.50 12/15/10 22:20
1,1-Dichloroethane ug/L ND 0.50 12/15/10 22:20
1,1-Dichloroethene ug/L ND 0.50 12/15/10 22:20
1,1-Dichloropropene ug/L ND 0.50 12/15/10 22:20
1,2,3-Trichlorobenzene ug/L ND 2.0 12/15/10 22:20
1,2,3-Trichloropropane ug/L ND 0.50 12/15/10 22:20
1,2,4-Trichlorobenzene ug/L ND 2.0 12/15/10 22:20
1,2,4-Trimethylbenzene ug/L ND 0.50 12/15/10 22:20
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/15/10 22:20
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/15/10 22:20
1,2-Dichlorobenzene ug/L ND 0.50 12/15/10 22:20
1,2-Dichloroethane ug/L ND 0.50 12/15/10 22:20
1,2-Dichloropropane ug/L ND 0.50 12/15/10 22:20
1,3,5-Trimethylbenzene ug/L ND 0.50 12/15/10 22:20
1,3-Dichlorobenzene ug/L ND 0.50 12/15/10 22:20
1,3-Dichloropropane ug/L ND 0.50 12/15/10 22:20
1,4-Dichlorobenzene ug/L ND 0.50 12/15/10 22:20
2,2-Dichloropropane ug/L ND 0.50 12/15/10 22:20
2-Chlorotoluene ug/L ND 0.50 12/15/10 22:20
4-Chlorotoluene ug/L ND 0.50 12/15/10 22:20
Benzene ug/L ND 0.50 12/15/10 22:20
Bromobenzene ug/L ND 0.50 12/15/10 22:20
Bromochloromethane ug/L ND 0.50 12/15/10 22:20
Bromodichloromethane ug/L ND 0.50 12/15/10 22:20
Bromoform ug/L ND 0.50 12/15/10 22:20
Bromomethane ug/L ND 5.0 12/15/10 22:20
Carbon tetrachloride ug/L ND 0.50 12/15/10 22:20
Chlorobenzene ug/L ND 0.50 12/15/10 22:20
Chloroethane ug/L ND 1.0 12/15/10 22:20
Chloroform ug/L ND 0.50 12/15/10 22:20
Chloromethane ug/L ND 1.0 12/15/10 22:20
cis-1,2-Dichloroethene ug/L ND 0.50 12/15/10 22:20
cis-1,3-Dichloropropene ug/L ND 0.50 12/15/10 22:20
Dibromochloromethane ug/L ND 0.50 12/15/10 22:20
Dibromomethane ug/L ND 0.50 12/15/10 22:20
Dichlorodifluoromethane ug/L ND 0.50 12/15/10 22:20
Diisopropyl ether ug/L ND 0.50 12/15/10 22:20
Ethylbenzene ug/L ND 0.50 12/15/10 22:20
Hexachloro-1,3-butadiene ug/L ND 2.0 12/15/10 22:20
Isopropylbenzene (Cumene)ug/L ND 0.50 12/15/10 22:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 25 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:541050
Associated Lab Samples:9284004002, 9284004004, 9284004005, 9284004006, 9284004008, 9284004009, 9284004010
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 12/15/10 22:20
Methyl-tert-butyl ether ug/L ND 0.50 12/15/10 22:20
Methylene Chloride ug/L ND 2.0 12/15/10 22:20
n-Butylbenzene ug/L ND 0.50 12/15/10 22:20
n-Propylbenzene ug/L ND 0.50 12/15/10 22:20
Naphthalene ug/L ND 2.0 12/15/10 22:20
o-Xylene ug/L ND 0.50 12/15/10 22:20
sec-Butylbenzene ug/L ND 0.50 12/15/10 22:20
Styrene ug/L ND 0.50 12/15/10 22:20
tert-Butylbenzene ug/L ND 0.50 12/15/10 22:20
Tetrachloroethene ug/L ND 0.50 12/15/10 22:20
Toluene ug/L ND 0.50 12/15/10 22:20
trans-1,2-Dichloroethene ug/L ND 0.50 12/15/10 22:20
trans-1,3-Dichloropropene ug/L ND 0.50 12/15/10 22:20
Trichloroethene ug/L ND 0.50 12/15/10 22:20
Trichlorofluoromethane ug/L ND 1.0 12/15/10 22:20
Vinyl chloride ug/L ND 1.0 12/15/10 22:20
1,2-Dichloroethane-d4 (S)%118 70-130 12/15/10 22:20
4-Bromofluorobenzene (S)%92 70-130 12/15/10 22:20
Dibromofluoromethane (S)%112 70-130 12/15/10 22:20
Toluene-d8 (S)%103 70-130 12/15/10 22:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
541051LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.850 90 60-140
1,1,1-Trichloroethane ug/L 44.650 89 60-140
1,1,2,2-Tetrachloroethane ug/L 49.050 98 60-140
1,1,2-Trichloroethane ug/L 50.250 100 60-140
1,1-Dichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethene ug/L 48.450 97 60-140
1,1-Dichloropropene ug/L 49.150 98 60-140
1,2,3-Trichlorobenzene ug/L 46.950 94 60-140
1,2,3-Trichloropropane ug/L 46.650 93 60-140
1,2,4-Trichlorobenzene ug/L 47.050 94 60-140
1,2,4-Trimethylbenzene ug/L 54.950 110 60-140
1,2-Dibromo-3-chloropropane ug/L 48.450 97 60-140
1,2-Dibromoethane (EDB)ug/L 47.950 96 60-140
1,2-Dichlorobenzene ug/L 47.250 94 60-140
1,2-Dichloroethane ug/L 43.650 87 60-140
1,2-Dichloropropane ug/L 52.350 105 60-140
1,3,5-Trimethylbenzene ug/L 54.250 108 60-140
1,3-Dichlorobenzene ug/L 48.050 96 60-140
1,3-Dichloropropane ug/L 51.250 102 60-140
1,4-Dichlorobenzene ug/L 44.650 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 26 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
541051LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 41.550 83 60-140
2-Chlorotoluene ug/L 51.850 104 60-140
4-Chlorotoluene ug/L 52.450 105 60-140
Benzene ug/L 51.650 103 60-140
Bromobenzene ug/L 49.650 99 60-140
Bromochloromethane ug/L 44.950 90 60-140
Bromodichloromethane ug/L 47.050 94 60-140
Bromoform ug/L 44.950 90 60-140
Bromomethane ug/L 53.950 108 60-140
Carbon tetrachloride ug/L 43.850 88 60-140
Chlorobenzene ug/L 46.850 94 60-140
Chloroethane ug/L 48.250 96 60-140
Chloroform ug/L 45.350 91 60-140
Chloromethane ug/L 61.8 CH5012460-140
cis-1,2-Dichloroethene ug/L 49.450 99 60-140
cis-1,3-Dichloropropene ug/L 53.250 106 60-140
Dibromochloromethane ug/L 45.650 91 60-140
Dibromomethane ug/L 41.350 83 60-140
Dichlorodifluoromethane ug/L 46.650 93 60-140
Diisopropyl ether ug/L 57.250 114 60-140
Ethylbenzene ug/L 50.550 101 60-140
Hexachloro-1,3-butadiene ug/L 40.950 82 60-140
Isopropylbenzene (Cumene)ug/L 55.150 110 60-140
m&p-Xylene ug/L 105100 105 60-140
Methyl-tert-butyl ether ug/L 49.350 99 60-140
Methylene Chloride ug/L 62.350 125 60-140
n-Butylbenzene ug/L 55.950 112 60-140
n-Propylbenzene ug/L 53.550 107 60-140
Naphthalene ug/L 53.950 108 60-140
o-Xylene ug/L 53.350 107 60-140
sec-Butylbenzene ug/L 56.050 112 60-140
Styrene ug/L 54.350 109 60-140
tert-Butylbenzene ug/L 53.450 107 60-140
Tetrachloroethene ug/L 43.450 87 60-140
Toluene ug/L 50.050 100 60-140
trans-1,2-Dichloroethene ug/L 49.350 99 60-140
trans-1,3-Dichloropropene ug/L 51.550 103 60-140
Trichloroethene ug/L 46.350 93 60-140
Trichlorofluoromethane ug/L 44.550 89 60-140
Vinyl chloride ug/L 55.750 111 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%97 70-130
Dibromofluoromethane (S)%102 70-130
Toluene-d8 (S)%105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 27 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/13468
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9284004001, 9284004003, 9284004007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:542094
Associated Lab Samples:9284004001, 9284004003, 9284004007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/16/10 19:13
1,1,1-Trichloroethane ug/L ND 0.50 12/16/10 19:13
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/16/10 19:13
1,1,2-Trichloroethane ug/L ND 0.50 12/16/10 19:13
1,1-Dichloroethane ug/L ND 0.50 12/16/10 19:13
1,1-Dichloroethene ug/L ND 0.50 12/16/10 19:13
1,1-Dichloropropene ug/L ND 0.50 12/16/10 19:13
1,2,3-Trichlorobenzene ug/L ND 2.0 12/16/10 19:13
1,2,3-Trichloropropane ug/L ND 0.50 12/16/10 19:13
1,2,4-Trichlorobenzene ug/L ND 2.0 12/16/10 19:13
1,2,4-Trimethylbenzene ug/L ND 0.50 12/16/10 19:13
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/16/10 19:13
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/16/10 19:13
1,2-Dichlorobenzene ug/L ND 0.50 12/16/10 19:13
1,2-Dichloroethane ug/L ND 0.50 12/16/10 19:13
1,2-Dichloropropane ug/L ND 0.50 12/16/10 19:13
1,3,5-Trimethylbenzene ug/L ND 0.50 12/16/10 19:13
1,3-Dichlorobenzene ug/L ND 0.50 12/16/10 19:13
1,3-Dichloropropane ug/L ND 0.50 12/16/10 19:13
1,4-Dichlorobenzene ug/L ND 0.50 12/16/10 19:13
2,2-Dichloropropane ug/L ND 0.50 12/16/10 19:13
2-Chlorotoluene ug/L ND 0.50 12/16/10 19:13
4-Chlorotoluene ug/L ND 0.50 12/16/10 19:13
Benzene ug/L ND 0.50 12/16/10 19:13
Bromobenzene ug/L ND 0.50 12/16/10 19:13
Bromochloromethane ug/L ND 0.50 12/16/10 19:13
Bromodichloromethane ug/L ND 0.50 12/16/10 19:13
Bromoform ug/L ND 0.50 12/16/10 19:13
Bromomethane ug/L ND 5.0 12/16/10 19:13
Carbon tetrachloride ug/L ND 0.50 12/16/10 19:13
Chlorobenzene ug/L ND 0.50 12/16/10 19:13
Chloroethane ug/L ND 1.0 12/16/10 19:13
Chloroform ug/L ND 0.50 12/16/10 19:13
Chloromethane ug/L ND 1.0 12/16/10 19:13
cis-1,2-Dichloroethene ug/L ND 0.50 12/16/10 19:13
cis-1,3-Dichloropropene ug/L ND 0.50 12/16/10 19:13
Dibromochloromethane ug/L ND 0.50 12/16/10 19:13
Dibromomethane ug/L ND 0.50 12/16/10 19:13
Dichlorodifluoromethane ug/L ND 0.50 12/16/10 19:13
Diisopropyl ether ug/L ND 0.50 12/16/10 19:13
Ethylbenzene ug/L ND 0.50 12/16/10 19:13
Hexachloro-1,3-butadiene ug/L ND 2.0 12/16/10 19:13
Isopropylbenzene (Cumene)ug/L ND 0.50 12/16/10 19:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 28 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:542094
Associated Lab Samples:9284004001, 9284004003, 9284004007
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 12/16/10 19:13
Methyl-tert-butyl ether ug/L ND 0.50 12/16/10 19:13
Methylene Chloride ug/L ND 2.0 12/16/10 19:13
n-Butylbenzene ug/L ND 0.50 12/16/10 19:13
n-Propylbenzene ug/L ND 0.50 12/16/10 19:13
Naphthalene ug/L ND 2.0 12/16/10 19:13
o-Xylene ug/L ND 0.50 12/16/10 19:13
sec-Butylbenzene ug/L ND 0.50 12/16/10 19:13
Styrene ug/L ND 0.50 12/16/10 19:13
tert-Butylbenzene ug/L ND 0.50 12/16/10 19:13
Tetrachloroethene ug/L ND 0.50 12/16/10 19:13
Toluene ug/L ND 0.50 12/16/10 19:13
trans-1,2-Dichloroethene ug/L ND 0.50 12/16/10 19:13
trans-1,3-Dichloropropene ug/L ND 0.50 12/16/10 19:13
Trichloroethene ug/L ND 0.50 12/16/10 19:13
Trichlorofluoromethane ug/L ND 1.0 12/16/10 19:13
Vinyl chloride ug/L ND 1.0 12/16/10 19:13
1,2-Dichloroethane-d4 (S)%104 70-130 12/16/10 19:13
4-Bromofluorobenzene (S)%99 70-130 12/16/10 19:13
Dibromofluoromethane (S)%103 70-130 12/16/10 19:13
Toluene-d8 (S)%100 70-130 12/16/10 19:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
542095LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.350 103 60-140
1,1,1-Trichloroethane ug/L 46.850 94 60-140
1,1,2,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,2-Trichloroethane ug/L 50.950 102 60-140
1,1-Dichloroethane ug/L 46.250 92 60-140
1,1-Dichloroethene ug/L 42.550 85 60-140
1,1-Dichloropropene ug/L 50.150 100 60-140
1,2,3-Trichlorobenzene ug/L 59.250 118 60-140
1,2,3-Trichloropropane ug/L 50.850 102 60-140
1,2,4-Trichlorobenzene ug/L 47.950 96 60-140
1,2,4-Trimethylbenzene ug/L 52.850 106 60-140
1,2-Dibromo-3-chloropropane ug/L 56.050 112 60-140
1,2-Dibromoethane (EDB)ug/L 52.350 105 60-140
1,2-Dichlorobenzene ug/L 54.350 109 60-140
1,2-Dichloroethane ug/L 46.250 92 60-140
1,2-Dichloropropane ug/L 51.750 103 60-140
1,3,5-Trimethylbenzene ug/L 58.650 117 60-140
1,3-Dichlorobenzene ug/L 53.350 107 60-140
1,3-Dichloropropane ug/L 54.250 108 60-140
1,4-Dichlorobenzene ug/L 48.750 97 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 29 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
542095LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 46.850 94 60-140
2-Chlorotoluene ug/L 55.450 111 60-140
4-Chlorotoluene ug/L 56.950 114 60-140
Benzene ug/L 51.150 102 60-140
Bromobenzene ug/L 49.950 100 60-140
Bromochloromethane ug/L 48.450 97 60-140
Bromodichloromethane ug/L 50.050 100 60-140
Bromoform ug/L 55.850 112 60-140
Bromomethane ug/L 36.550 73 60-140
Carbon tetrachloride ug/L 49.050 98 60-140
Chlorobenzene ug/L 49.250 98 60-140
Chloroethane ug/L 38.150 76 60-140
Chloroform ug/L 51.050 102 60-140
Chloromethane ug/L 30.850 62 60-140
cis-1,2-Dichloroethene ug/L 46.050 92 60-140
cis-1,3-Dichloropropene ug/L 59.250 118 60-140
Dibromochloromethane ug/L 53.250 106 60-140
Dibromomethane ug/L 50.250 100 60-140
Dichlorodifluoromethane ug/L 18.6 L0503760-140
Diisopropyl ether ug/L 48.850 98 60-140
Ethylbenzene ug/L 51.850 104 60-140
Hexachloro-1,3-butadiene ug/L 51.450 103 60-140
Isopropylbenzene (Cumene)ug/L 52.250 104 60-140
m&p-Xylene ug/L 113100 113 60-140
Methyl-tert-butyl ether ug/L 47.950 96 60-140
Methylene Chloride ug/L 44.850 90 60-140
n-Butylbenzene ug/L 58.850 118 60-140
n-Propylbenzene ug/L 54.850 110 60-140
Naphthalene ug/L 51.150 102 60-140
o-Xylene ug/L 52.050 104 60-140
sec-Butylbenzene ug/L 53.550 107 60-140
Styrene ug/L 52.550 105 60-140
tert-Butylbenzene ug/L 60.550 121 60-140
Tetrachloroethene ug/L 52.050 104 60-140
Toluene ug/L 49.350 99 60-140
trans-1,2-Dichloroethene ug/L 43.950 88 60-140
trans-1,3-Dichloropropene ug/L 58.350 117 60-140
Trichloroethene ug/L 53.650 107 60-140
Trichlorofluoromethane ug/L 36.850 74 60-140
Vinyl chloride ug/L 40.050 80 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%102 70-130
Dibromofluoromethane (S)%97 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 30 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 31 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9284004
CARAWAY GROCERY 2010296
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9284004001 MSV/134683337 OLD LEXINGTON RD SM 6200B
9284004002 MSV/134443338 OLD LEXINGTON RD SM 6200B
9284004003 MSV/134683354 OLD LEXINGTON RD SM 6200B
9284004004 MSV/134443334 OLD LEXINGTON RD SM 6200B
9284004005 MSV/134443256 OLD LEXINGTON RD SM 6200B
9284004006 MSV/134441275 BACK CREEK RD.SM 6200B
9284004007 MSV/134682353 SMYRNA GROVE DR.SM 6200B
9284004008 MSV/13444SMYRNA GROVE MHP-LOT 2 SM 6200B
9284004009 MSV/13444SMYRNA GROVE MHP-LOT 6 SM 6200B
9284004010 MSV/134441255 BACK CREEK RD.SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2010 08:14 AM Page 32 of 32
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]