WS-6093_22446_MRP_20230227

Monitoring Report

Moody’s Grocery
NCDEQ Incident #22446
912 Old Highway 21
State Road, Wilkes County, North Carolina
ATC Project #SLC2244602

February 27, 2023

Monitoring Report February 27, 2023
Moody’s Grocery, Incident # 22446, State Road, Wilkes Co., NC ATC Project #SLC2244602

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION.................................................................................... 1
2.0 EXECUTIVE SUMMARY .................................................................................. 2
3.0 SITE DESCRIPTION .......................................................................................... 3
3.1 Site Characterization ............................................................................ 3
3.2 Site Background ................................................................................... 3
3.3 Site and Regional Geology ................................................................... 6
3.4 Site and Regional Hydrogeology .......................................................... 6
4.0 GROUNDWATER CHARACTERIZATION .................................................... 7
4.1 Water Supply Wells .............................................................................. 7
4.2 Groundwater Levels ............................................................................. 7
4.3 Groundwater Quality ............................................................................ 7
5.0 CONCLUSIONS AND RECOMMENDATIONS .............................................. 8
TABLES

Table 1 Water Supply Well Information
Table 2 Water Supply Well Analytical Results
Table 3 Well Construction Details
Table 4 Groundwater Elevation Data
Table 5 Field Parameters
Table 6 Recent Groundwater Analytical Results
Table 7 Historical Groundwater Analytical Results

FIGURES
Figure 1 Site Location Map
Figure 2 Water Supply Well Location Map
Figure 3 Site Map
Figure 4 Groundwater Elevation Map
Figure 5 Groundwater Quality Map

APPENDICES

Appendix A Field Notes and Photo Log
Appendix B Laboratory Analytical Report

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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) has completed a Monitoring Report (GMR),
documenting the December 28, 2022, and January 13, 2023, sampling of three on-site monitoring
wells and one water supply well at Moody’s Grocery located at 912 Old Highway 21, State Road,
Wilkes County, North Carolina. The GMR is being performed based on a December 8, 2022, Task
Authorization (TA-02) by the Trust Fund Branch of the Underground Storage Tank (UST) Section,
Division of Waste Management, North Carolina Department of Environmental Quality (NCDEQ).
The work is being performed as part of the State Lead Contract #N122019A between NCDEQ and
ATC.

Former petroleum USTs at the site released product to the subsurface prior to their
decommissioning in 1998 and subsequent removal in 2000.

During January 2019 site activities, ATC conducted soil gas sampling in MW-1, and installed
Provectus® Oxygen Releasing Socks (ORS) in MW-1. The approved work included the installation
of one monitoring well (MW-5); the measurement of the top of casing of MW-5; the sampling of
wells MW-1 and MW-5; the measurement of water levels in wells MW-2, MW-3, and MW-4; and
the sampling of five water supply wells (WSW 1, WSW-2, WSW-4, WSW-937, and WSW-955).

On February 20 and 21, 2020, ATC installed groundwater monitoring well MW-5, at a location
downgradient of the former UST basin. On February 21, 2020, ATC gauged and sampled
groundwater monitoring wells MW-4 and MW-5. Monitoring well MW-4 was sampled instead of
MW-1, and therefore, monitoring well MW-1 was sampled on April 10, 2020 along with the
measurement of water levels in all monitoring wells. Site water supply well WSW-1 was also
sampled.

The current scope of work included obtaining groundwater samples from monitoring wells MW-1,
MW-4, and MW-5, and water supply wells WSW-1 and WSW-2. The water samples were analyzed
for the presence of VOCs indicative of the presence of dissolved petroleum

Laboratory results from the December 28, 2022, and January 13, 2023, sampling events indicate the
following:

 Light non-aqueous phase liquid (LNAPL) was not found during the sampling event;
 Monitoring well MW-1 contained benzene, naphthalene, and 1,2-dichloroethane (1,2-
DCA) above the 15A NCAC 02L .0202 groundwater quality standards (2L Standards).
 Monitoring well MW-5 contained benzene, toluene, ethylbenzene, total xylenes, 1,2-
DCA, 1,2,4-trimethylbenzene, and 1,2-dibromoethane (EDB) in excess of the 2L
Standards. The benzene and EDB concentrations also exceeded the respective Gross
Contamination Levels (GCLs) of 5,000 micrograms per liter (µg/L) and 50 µg/L;
 Volatile Organic Compounds (VOCs) were not detected in monitoring well MW-4;
 Laboratory analysis of the sample obtained from WSW-1 did not identify any detectable
concentrations of petroleum constituents;
 Based on the January 13, 2023, groundwater elevations, groundwater flow is to the
southeast;
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 Based on historical data, VOC concentrations in MW-1 appear to vary seasonally.
Concentrations of VOCs in MW-5 appear to be generally stable;
 Based on the analytical results from monitoring well MW-5 the extent of VOCs in
groundwater is not delineated to the east and southeast of MW-1 and MW-5. In addition,
VOC concentrations are higher in well MW-5 than in the “source” well MW-1,
suggesting that higher concentrations may be present in the groundwater west of MW-1;
and
 VOC concentrations in MW-5 constructed with a screened interval 40-50 feet indicate
that the constituent plume has moved to the southeast of the source area at depth.

Based on the well MW-5 sampling results and groundwater flow direction, ATC recommends
the installation and sampling of four additional monitoring wells. These additional wells include
one shallow well (MW-5S) adjacent to MW-5 to be screened across the groundwater surface to
evaluate possible higher concentrations in the shallow groundwater; one shallow well (MW-6)
southwest of MW-1 to evaluate possible higher concentrations in the source area. Two
monitoring wells (MW-7 and MW-8) are recommended downgradient of the source area on the
adjacent property Air rotary drilling will be needed for the installation of the deep monitoring
well. Subsequent assessment and remediation activities would be evaluated following receipt of
the groundwater quality data from the new monitoring wells.

3.0 SITE DESCRIPTION
3.1 Site Characterization
The NCDEQ retained ATC to provide environmental consulting services for Moody’s Grocery,
located at 912 Old Highway 21, in State Road, Wilkes County, North Carolina. Figure 1 depicts the
site on a topographic map. The site currently operates as a retail convenience store that no longer
has retail petroleum operations. The site is located near the intersection of Mining Church Road
and Old Highway 21.

3.2 Site Background
The site was developed with a single-story gasoline station in circa 1962 and is currently
occupied by Moody’s Grocery. Historical records indicate that Moody’s Grocery was a retail
petroleum facility until 1998, including one 6,000-gallon gasoline UST, two 3,000-gallon
gasoline USTs, and one 550-gallon kerosene UST and associated piping and dispensers. The
UST system ceased operation in 1998 and was removed in March 2000. During the 2000 UST
removal, a 550-gallon UST of unknown content was found below the dispenser island.
According to the property owner, Don Moody, the UST had been taken out of service in 1962
due to non-use. Soil analytical results indicated petroleum impact above the state action level of
10 milligrams per kilogram (mg/kg) in the area of the UST basin for the two 3,000-gallon
gasoline USTs, one 550-gallon kerosene UST, and 550-gallon UST of unknown content.

During a modified Limited Site Assessment (LSA) in December 2002, monitoring wells MW-1
and MW-2 were installed to a depth of 60 feet below ground surface. Monitoring well MW-1
was installed in the former gasoline UST basin and monitoring well MW-2 was installed in the
former kerosene UST basin. Groundwater analytical results from both monitoring wells indicated
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target petroleum constituents exceeded the 2L Standards. In addition, a well receptor survey
identified 31 potable wells within 1,500 feet of the source area, including on-site potable well
WSW-1. Because municipal water was not supplied to the area and due to the groundwater
impact, the site was ranked as High Risk.

Between 2002 and 2005, additional assessment was performed that included monitoring of the
two site monitoring wells, water supply well WSW-1, and six nearby water supply wells.
Groundwater analytical results from 2005 indicated detectable concentrations of naphthalene and
total xylenes in well WSW-1 that did not exceed the 2L Standard. Groundwater impact above 2L
Standards for benzene and 1,2-dichloroethane were identified in potable well WSW-6, located
approximately 500 feet east southeast of the source area, and 2L Standards were exceeded for
benzene, methyl tertiary butyl ether (MTBE), 1,4-dicholorobenzene, and 1,2-dichloroethane for
potable well WSW-2, located approximately 170 feet east of the source area. Due to the impact
in the potable wells, a point of entry (POE) filtration system was installed by the NCDEQ on
wells WSW-2 and WSW-6. A March 2008 NCDEQ correspondence indicated that the NCDEQ
planned to remove the POE filtration system from well WSW-6 because petroleum
concentrations had not been detected since February 2008. The POE system was removed on
August 5, 2013.

ATC performed groundwater monitoring at the site in July 2014. Groundwater impact was
identified above 2L Standards in monitoring wells MW-1 and MW-2. None of the water supply
wells that were sampled contained impact above 2L Standards. An updated receptor survey was
completed identifying 32 water supply wells within 1,500 feet of the site, 21 of which are located
within 1,000 feet of the site. Two water supply wells (WSW-4 and WSW-4616) are located
downgradient and within 500 feet of the site. Five additional wells (WSW-5, WSW-250, WSW-
255, WSW-259, and WSW-4562) are also located downgradient from the site, and are within
1,000 feet of the site.

In July 2015, ATC completed a groundwater monitoring event for the site. Results from the
groundwater monitoring event indicated remaining impact above 2L Standards in monitoring well
MW-1. Other petroleum constituents in wells MW-1 and MW-2 were below 2L Standards. No
petroleum constituents were detected in wells MW-3, MW-4, or in the three water supply wells
(WSW-1, WSW-3, and WSW-6) which were sampled.

In November, 2017, ATC completed a groundwater monitoring event which indicated remaining
VOC impact above 2L Standards in monitoring wells MW-1 and MW-3. Following the sampling
event, ATC installed ORS in monitoring well MW-1.

On June 14, 2018, ATC collected groundwater samples from monitoring wells MW-1, MW-2,
MW-3, and MW-4. Benzene, 1,2-dichloroethane, ethylene dibromide (EDB), and isopropyl ether
concentrations exceeded the 2L Standards in monitoring well MW-1. Note that the concentrations
decreased by 37 percent (isopropyl benzene) to 87 percent (benzene) compared to the November
2017 sampling results, excluding EBD which was not detected in November 2017 (elevated
detection limit).

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On January 8, 2019, ATC collected a soil vapor sample from monitoring well MW-1 to assess
remaining soil impact in the vadose zone soils. Following collection of the soil-gas sample, ATC
installed new ORS in monitoring well MW-1. Based on the January 2019 work, ATC
recommended installation of one additional monitoring well (MW-5) to further characterize
groundwater impact; and conducting soil vapor extraction using a new SVE well near MW-1 in
an effort to remove petroleum from the subsurface and expedite subsequent remediation by
natural attenuation.

On February 20 and 21, 2020, ATC installed groundwater monitoring well MW-5, at a location
downgradient of the former UST basin. On February 21, 2020, ATC gauged and sampled
groundwater monitoring wells MW-4 and MW-5. Monitoring well MW-1 was sampled on April
10, 2020, along with the measurement of water levels in all monitoring wells. Site water supply well
WSW-1 was also sampled. Groundwater monitoring wells MW-1 and MW-5 contained VOCs in
excess of the 2L standard and EDB was detected in MW-5 in excess of the GCL. Laboratory
analysis of the sample obtained from WSW-1 did not identify any detectable concentrations of
petroleum constituents.

ATC recommended the installation of downgradient wells to evaluate the horizontal extent of
contaminant migration

ATC obtained groundwater samples from MW-1, MW-2, MW3-, MW-4, MW-5 and WSW-1 and
WSW-2. Laboratory results from February 4, 2021, sampling event indicate the following: light
non-aqueous phase liquid (LNAPL) was not found in the monitoring well network. Monitoring
well MW-1 contained benzene, total xylenes, diisopropyl ether (DIPE), naphthalene, 1,2-
dichloroethane and (1,2-DCA) above the 15A NCAC 02L .0202 groundwater quality standards
(2L Standards). Monitoring well MW-5 contained benzene, toluene, ethylbenzene, total xylenes,
methyl tert butyl ether (MTBE), DIPE, naphthalene, 1,2,-DCA, ethylene dibromide (EDB), and
1,2,4-trimethylbenzene in excess of the 2L Standards. The benzene and EDB concentrations also
exceeded the Gross Contamination Level (GCL). Volatile Organic Compounds (VOCs) were not
detected in monitoring wells MW-2, MW-3, and MW-4. Laboratory analysis of the sample
obtained from WSW-1 did not identify any detectable concentrations of petroleum constituents.
Based on the February 4, 2021, groundwater elevations, groundwater flow is to the southeast.

Based on historical data, ATC concluded that VOC concentrations in MW-1 appear to vary
seasonally. Concentrations of VOCs in MW-5 appear to be increasing. Analytical results from
monitoring well MW-5 suggested the extent of VOCs in groundwater is not delineated to the east
and southeast of MW-1 and MW-5. In addition, VOC concentrations are higher in well MW-5
than in the “source” well MW-1, suggesting that higher concentrations may be present in the
groundwater west of MW-1. VOC concentrations in MW-5 constructed with a screened interval
40-50 feet indicate that the constituent plume has moved to the southeast of the source area at
depth.

ATC recommended the installation and sampling of two additional monitoring wells. These
additional wells include one shallow well (MW-5S) adjacent to MW-5 to be screened across the
groundwater surface to evaluate possible higher concentrations in the shallow groundwater and
Monitoring Report February 27, 2023
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one shallow well (MW-6) west of MW-1 to evaluate possible higher concentrations in the source
area.

3.3 Site and Regional Geology

According to the Geologic Map of North Carolina, dated 1985, the property lies within the Blue
Ridge Physiographic Province, in the Slate of Copperhill Formation of the Ocoee Supergroup.
The metamorphic rock of the Slate of Copperhill Formation is comprised of slate, phyllite, and
metagraywacke that indicates graded bedding. In most areas, the upper Blue Ridge subsurface
consists of unconsolidated residual soil, variously known as residuum, saprolite, or partially
weathered rock (PWR) that has developed from in-place weathering of the underlying
metamorphic bedrock. The residual soils vary in consistency and depth based on local
conditions. Bedrock can be found at the surface as outcrops and to depths of greater than 100 feet
in areas of easily weathered rock types. Sites near streams and rivers in the Blue Ridge may also
contain alluvium deposited during flood events.

Boring logs from the May 2010 letter report by Terraine indicated that the site subsurface
consisted of brown to red clay in the upper approximately 14 feet of subsurface soils, followed
by reddish brown to yellowish brown silt or clayey silt from approximately 20 ft bgs to the
termination of the boring, which varied from 52 ft bgs in boring MW-3 to 45 ft bgs in boring
MW-4. Bedrock was encountered at well MW-2 at a depth of 50 ft bgs. During the drilling for
well MW-5, clayey silt and silt was observed to the termination depth of 50 ft bgs. Air rotary
drilling was needed to drill deeper than 29 ft bgs, where auger refusal was encountered due to
dense silt. Neither partially weathered rock nor bedrock were encountered, and depth to top of
bedrock is unknown.

3.4 Site and Regional Hydrogeology

The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and rivers
to as deep as 50 feet or more beneath upland surfaces in some parts of the Blue Ridge. ATC
encountered groundwater between 26.80 (MW-5) and 32.42 (MW2) feet below tops of casing
(TOC) in the monitoring wells at the site during the February 4, 2021, monitoring event.

Permeability varies with lithology and is typically relatively low in residual soils, with higher
permeability in saprolite or PWR due to relict rock texture and variable susceptibility to
weathering exhibited by different minerals in the rock. Groundwater flow in residual soils or
alluvium is usually in rough concurrence with local topographic conditions and is toward local
drainage features. Based on the existing site wells, the groundwater flow appears to channel to
the central part of the site and flows south-southeast.

The bedrock fractures or other planar features of the Blue Ridge Physiographic Province
generally constitute the bedrock aquifer, with the surrounding rock material being effectively
impermeable. Along with fractures, contacts between rock bodies probably constitute zones of
significant groundwater occurrence in the bedrock. The surrounding material and overlying
residuum tend to make the bedrock aquifer a semi-confined aquifer. That is, the overlying water
and soil weight normally results in pressure that causes water in a borehole, which intersects a
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fracture or other feature, to rise above the elevation of the fracture or feature. Most modern
water supply wells in the Blue Ridge consist of a casing set through the residual soils into the
upper bedrock followed by an open borehole into the bedrock where water bearing fractures
were encountered during the drilling. Except for attempted sampling of nearby water supply
wells, evaluation of bedrock water quality or hydrology was beyond the scope of the GMR.

4.0 GROUNDWATER CHARACTERIZATION
On December 28, 2022, ATC visited the site to conduct the approved sampling. ATC sampled
monitoring well MW-1 and water supply well WSW-1. However due to freezing temperatures,
water within the MW-4 and MW-5 well vaults had frozen solid. ATC returned to the site on
January 13, 2023, and sampled wells MW-4 and MW-5, and measured the water levels in wells
MW-1 and MW-3. Access to water supply well WSW-2 was not available on either date.

4.1 Water Supply Wells
Twenty-one water supply wells have been identified within 1,000 feet of the site, with nine of the
wells within 500 feet of the site. Groundwater flow at the site is to the southeast, with two most
at-risk wells: on-site well WSW-1 and the well immediately to the east of the site, WSW-2.
Seven of the water supply wells are located downgradient of the site. Figure 2 depicts the
locations of the water supply wells on an aerial overlay with radial distances from the site. Table
1 summarizes water supply well and other receptor information.

On December 28, 2022, ATC collected a groundwater sample from the on-site water supply well
(WSW-1). Water supply well WSW-2 was not accessible during both sampling events and could
not be sampled. Field notes and photographs from December 28, 2022, and January 13, 2023,
sampling events are presented as Appendix A. Laboratory analysis of the water supply well sample
did not identify any detectable concentrations of petroleum constituents. A summary of current and
historical water supply well analytical data is included in Table 2.

4.2 Groundwater Levels
On January 13, 2023, water levels were gauged in monitoring wells MW-1, MW-2, MW-3, MW-
4, and MW-5. Well construction details are presented in Table 3 and the groundwater elevation
data is presented in Table 4. Figure 3 depicts a site map. Groundwater elevations were then
calculated based on the measured elevations, which are referenced to an on-site benchmark of
1,330.00 feet at the well MW-1 TOC. Depth to groundwater elevation data are summarized in
Table 4. Based on the results of the January 13, 2023, groundwater measurements, groundwater
flow is to the southeast with a gradient of approximately 0.037 feet/foot. A groundwater elevation
contour map is presented in Figure 4.

4.3 Groundwater Quality
On December 28, 2022, a groundwater sample was collected from monitoring well MW-1. On
January 13, 2023, groundwater samples were collected from monitoring wells MW-4 and MW-5.
During sampling activities, a three-volume well purge was implemented prior to groundwater
sample collection to ensure a representative groundwater sample. The samples were collected in
laboratory-supplied, preserved containers; entered into chain of custody control; placed on ice; and
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shipped to North Carolina accredited Pace Analytical Services, Inc. in Huntersville, North Carolina.
The water samples were analyzed by EPA Method 6200B for VOCs including petroleum
constituents. The analytical reports are included in Appendix B.

Groundwater field parameters including temperature, dissolved oxygen, conductivity, pH, and
oxidation-reduction potential were measured during the monitoring event. Field parameter readings
for each well are presented in Table 5. Groundwater analytical results from the December 28, 2022,
and January 13, 2023, monitoring events are summarized in Table 6. Historical groundwater
analytical results are shown in Table 7. The groundwater analytical results were compared to the 2L
Standards and GCLs. Groundwater analytical results indicate the following:

 Monitoring well MW-1 contained benzene, naphthalene, and 1,2-DCA above the 2L
Standards.
 Monitoring well MW-5 contained benzene, toluene, ethylbenzene, total xylenes, 1,2-
DCA, 1,2,4-trimethylbenzene, and EDB in excess of the 2L Standards. The benzene
(9,350 µg/L) and EDB (152 µg/L) concentrations also exceeded the respective GCLs of
5,000 µg/L and 50 µg/L;
 VOCs were not detected in monitoring well MW-4;
 Laboratory analysis of the sample obtained from WSW-1 did not identify any detectable
concentrations of petroleum constituents;

Figure 5 depicts a groundwater quality map with detected constituents above 2L Standards.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a field blank was
collected, and a data review of the laboratory reports was conducted. During the review, it was
found that the samples were received from the laboratory in acceptable condition and properly
preserved. The samples were analyzed within correct holding times and reported within the lab
report, and the chain of custody was properly completed by all parties. The laboratory QC report
shows that an internal blank was analyzed for each method that was used for the original
samples. The laboratory fortified blank (LFB) and laboratory control sample (LCS) data results
were also provided for each analytical method. ATC collected a field blank during the December
28, 2022, groundwater monitoring activities. No concentrations of petroleum constituents were
detected in the field blank. Refer to the laboratory reports in Appendix B for details regarding QA
results for the laboratory samples and any noted exceptions. Overall, ATC concludes that the
laboratory results are usable and any exceptions do not significantly impact the conclusions
presented in this report.

5.0 CONCLUSIONS AND RECOMMENDATIONS
On behalf of the Trust Fund Branch of the UST Section, ATC has completed a GMR documenting
the December 28, 2022, and January 13, 2023, groundwater monitoring events for Moody’s
Grocery, located at 912 Old Highway 21, State Road, Wilkes County, North Carolina. The
following conclusions were derived from groundwater monitoring activities and analytical reports:

 LNAPL was not found during sampling activities;
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 Monitoring well MW-1 contained benzene, naphthalene, and 1,2-DCA above the 2L
Standards.
 Monitoring well MW-5 contained benzene, toluene, ethylbenzene, total xylenes, 1,2-
DCA, 1,2,4-trimethylbenzene, and EDB in excess of the 2L Standards. The benzene and
EDB concentrations also exceeded the respective GCLs of 5,000 µg/L and 50 µg/L;
 VOCs were not detected in monitoring well MW-4;
 Laboratory analysis of the sample obtained from WSW-1 did not identify any detectable
concentrations of petroleum constituents;
 Based on the January 13, 2023, groundwater elevations, groundwater flow is to the
southeast;
 Based on historical data, VOC concentrations in MW-1 appear to vary seasonally.
Concentrations of VOCs in MW-5 appear to be generally stable;
 Based on the analytical results from monitoring well MW-5 the extent of VOCs in
groundwater is not delineated to the east and southeast of MW-1 and MW-5. In addition,
VOC concentrations are higher in well MW-5 than in the “source” well MW-1,
suggesting that higher concentrations may be present in the groundwater west of MW-1.
 VOC concentrations in MW-5 constructed with a screened interval 40-50 feet indicate
that the constituent plume has moved to the southeast of the source area at depth.

Based on the well MW-5 sampling results and groundwater flow direction ATC recommends the
installation and sampling of four additional monitoring wells. These additional wells include one
shallow well (MW-5S) adjacent to MW-5 to be screened across the groundwater surface to
evaluate possible higher concentrations in the shallow groundwater; one shallow well (MW-6)
southwest of MW-1 to evaluate possible higher concentrations in the source area. Two
monitoring wells (MW-7 and MW-8) are recommended downgradient of the source area on the
adjacent property Air rotary drilling will be needed for the installation of the deep monitoring
well. Subsequent assessment and remediation activities would be evaluated following receipt of
the groundwater quality data from the new monitoring wells.

TABLES
Water Supply
Well Name/ID
Parcel
Identification Property Owner(s)Property Address County Owner Address Usage
WSW-1 0602043 Don & Peggy Moody 912 Old Highway 21
State Road, NC 28676 Wilkes 1050 Old Highway 21
State Road, NC 28676 Potable Water
WSW-2 0604032 Donna & Dwight Moody
336-699-8464 (Dwight, cell#)
934 Old Highway 21
State Road, NC 28676 Wilkes 934 Old Highway 21
State Road, NC 28676 Potable Water
WSW-3 49900289747 Roger Hanes 893 Old Highway 21
State Road, NC 28676 Surry 184 Dewitt Road
Glade Valley, NC 28267 Potable Water
WSW-4 0605430 Bradley S. Holbrook 265 Hidden Chambers Drive
State Road, NC 28676 Wilkes 265 Hidden Chambers Drive
State Road, NC 28676 Potable Water
WSW-5 0605327 Robert & Meredith Shaw 276 Hidden Chambers Drive
State Road, NC 28676 Wilkes 276 Hidden Chambers Drive
State Road, NC 28676 Potable Water
WSW-6 0604808 Don & Peggy Moody 1020 Old Highway 21
State Road, NC 28676 Wilkes 1050 Old Highway 21
State Road, NC 28676 Potable Water
WSW-250 0605328 Billy & Tammy Anderson 250 Hidden Chambers Road
State Road, NC 28676 Wilkes 221 Colbert Place
Traphill, NC 28685 Potable Water
WSW-255 0605431 Michael & Mary Ann Pardue 255 Hidden Chambers Road
State Road, NC 28676 Wilkes 255 Hidden Chambers Road
State Road, NC 28676 Potable Water
WSW-259 0604326 Ruth Hutton 259 Mountain Spring Street
State Road, NC 28676 Wilkes 259 Mountain Spring Road
State Road, NC 28676 Potable Water
WSW-717 494401285620 Jerry & Teresa Sparks 717 Old Highway 21
State Road, NC 28676 Surry 717 Old Highway 21
State Road, NC 28676 Potable Water
WSW-743 494400284314 Shanda Vestal & Roger L. Gentry 743 Old Highway 21
State Road, NC 28676 Surry 743 Old Highway 21
State Road, NC 28676 Potable Water
WSW-767 494400286206 Bobby & Betty Hanes 767 Old Highway 21
State Road, NC 28676 Surry 781 Old Highway 21
State Road, NC 28676 Potable Water
WSW-781 494400286206 Bobby & Betty Hanes 781 Old Highway 21
State Road, NC 28676 Surry 781 Old Highway 21
State Road, NC 28676 Potable Water
WSW-805 494400286206 Bobby & Betty Hanes 805 Old Highway 21
State Road, NC 28676 Surry 781 Old Highway 21
State Road, NC 28676 Potable Water
NCDEQ INCIDENT #22446
912 OLD HIGHWAY 21
MOODY'S GROCERY
WATER SUPPLY WELL INFORMATION
TABLE 1
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
Page 1 of 2
Water Supply
Well Name/ID
Parcel
Identification Property Owner(s)Property Address County Owner Address Usage
NCDEQ INCIDENT #22446
912 OLD HIGHWAY 21
MOODY'S GROCERY
WATER SUPPLY WELL INFORMATION
TABLE 1
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
WSW-835 494400287113 Michelle Cherney 835 Old Highway 21
State Road, NC 28676 Surry 835 Old Highway 21
State Road, NC 28676 Potable Water
WSW-857 494400288029 Betty Lou Hanes 857 Old Highway 21
State Road, NC 28676 Surry 857 Old Highway 21
State Road, NC 28676 Potable Water
WSW-937 494400372928 James Pennell 937 Old Highway 21
State Road, NC 28676 Surry 937 Old Highway 21
State Road, NC 28676 Potable Water
WSW-955 494401384033 Freddie & Tara Vanhoy 955 Old Highway 21
State Road, NC 28676 Surry 955 Old Highway 21
State Road, NC 28676 Potable Water
WSW-1163 494401379777 Joshua & Mellony Price 1163 Old Highway 21
State Road, NC 28676 Surry 1163 Old Highway 21
State Road, NC 28676 Potable Water
WSW-4562 0605865 Robin Poplin 4562 Mining Ridge Church Road
State Road, NC 28676 Wilkes 4562 Mining Ridge Church Road
State Road, NC 28676 Potable Water
WSW-4616 0602655 Buford & Annie Lee Shore 4616 Mining Ridge Church Road
State Road, NC 28676 Wilkes 15206 Martha Street
Van Nuys, CA 91411 Potable Water
Page 2 of 2
Well
ID Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl TertiaryButyl EtherIsopropyl Ether Ethylene Dibromide (6200B/504.1)NaphthaleneAcetonen-ButylbenzeneChloroform1,4-Dichlorobenzene1,2-Dichloroethane1,2-Dichloropropane4-Isopropyltoluene4-Methyl-2-Pentanonen-Propylbenzenesec-ButylbenzeneStyrene1,2,4-Trimethyl-benzene1,3,5-Trimethyl-benzeneChloromethane1 600 600 500 20 70 0.02 6 6,000 70 70 6 0.4 0.6 25 ---70 70 70 400 400 3
10/4/2001 ND ND ND ND ND ND ND ND NA NA NA NA ND NA NA NA NA NA NA ND ND NA
9/12/2002 ND ND ND ND ND 2 NA NA NA NA ND ND 1.2 NA NA NA NA NA NA ND ND NA
9/9/2004 ND ND ND ND ND 1.4 ND ND NA NA NA NA ND ND ND ND ND NA NA ND ND NA
11/7/2005 ND ND ND 1.35 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
9/24/2008 ND ND ND ND ND ND ND ND ND ND ND ND 0.69 ND ND ND ND ND ND ND ND NA
3/9/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
12/4/2011
9/20/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
1/28/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
7/10/2014 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 <4.7 <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
7/10/2015 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 5.6 B, J <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
6/14/2018 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <5.0 <50 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0
02/20/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 NA <0.50 <0.50 <0.50 <0.50 <0.50 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <1.0
02/04/2021 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.011 <0.66 NA <0.35 <0.35 <0.25 <0.26 <0.18 NA NA <0.24 <0.25 <0.26 <0.19 <0.23 <0.42
12/28/2022 <0.34 <0.24 <0.30 <1.05 <0.42 <0.31 <0.27/<0.00 <0.64 NA <0.49 <0.32 <0.65 <0.32 NA NA <0.3
3 NA <0.34 <0.29 <0.50 <0.33
10/4/2001 ND ND ND ND ND ND ND NA ND ND NA NA ND NA NA NA NA NA NA ND ND NA
9/12/2002 150 ND ND ND 64 360 NA NA NA NA 12 16 6 NA NA NA NA NA NA ND ND NA
11/7/2005 1.02 ND ND ND 1.71 3.88 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
1/7/2008 52.1 ND ND ND 69.8 ND 99.9 ND ND ND ND ND 4.65 ND ND ND ND ND ND ND ND NA
9/24/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
3/9/2010
12/4/2011
9/20/2012
1/28/2013
7/10/2014 0.17 J <0.09 <0.092 <0.29 1.7 1.4 <0.089 <0.12 <4.7 <0.054 <0.14 <0.046 0.82 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 0.38 J
7/10/2015
2/20/2020
9/12/2002 ND ND ND ND ND ND NA ND NA NA ND ND ND NA NA NA NA NA NA ND ND NA
9/9/2004 ND ND ND ND ND ND ND ND NA NA NA NA ND ND ND ND ND ND ND ND ND NA
11/7/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
9/24/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
3/9/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
9/20/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
1/28/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
7/10/2014
7/10/2015 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 7.3 B, J <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
2/20/2020
9/24/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
3/9/2010 ND ND ND ND ND ND ND ND 1.4 J ND ND ND ND ND ND ND ND ND ND ND ND NA
9/20/2012
3/9/2010 ND ND ND ND ND ND ND ND 1.4 J ND ND ND ND ND ND ND ND ND ND ND ND NA
7/10/2014 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 <4.7 <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
7/10/2015
2/20/2020
10/4/2001 ND ND ND ND ND ND ND ND ND ND NA NA ND NA NA NA NA NA NA ND ND NA
9/12/2002 ND ND ND ND ND ND NA NA NA NA ND ND ND NA NA NA NA NA NA ND ND NA
9/9/2004 ND ND ND ND ND ND ND ND NA NA NA NA ND ND ND ND ND ND ND ND ND NA
11/7/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
9/24/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
3/9/2010 ND ND ND ND ND 0.95 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
12/4/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
9/20/2012
1/28/2013 ND ND ND ND ND ND ND ND ND ND ND ND 0.32 J ND ND ND ND ND ND ND ND NA
7/10/2014 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 <4.7 <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
7/10/2015
2/20/2020
10/4/2001 320 46 25 278 ND 25 ND ND ND ND NA NA 1 NA NA NA NA NA NA 530 14 NA
9/12/2002 250 87 19 228 ND 27 NA NA NA NA ND ND 6.8 NA NA NA NA NA NA 48 22 NA
11/7/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
2/12/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
3/9/2010 210 26 13 116 ND 20 ND 3.9 68 0.97 J 6.8 ND 6.9 1.2 ND 14 1.2 0.62 ND 22 11 NA
12/4/2011
9/20/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA
1/28/2013 ND ND 0.3 ND ND 7.2 ND ND ND ND ND ND 1.4 ND ND ND ND ND ND 1.2 ND NA
7/10/2014
7/10/2015 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 8.3 B, J <0.054 <0.14 <0.046 <0.19 <0.11 <0.12 <1.5 <0.094 <0.084 <0.12 <0.18 <0.10 <0.32
2/20/2020
9/12/2002 ND ND ND ND ND ND NA NA NA NA ND ND ND NA NA NA NA NA NA ND ND NA
9/9/2004 ND ND ND ND ND ND ND ND NA NA NA NA NA ND ND ND ND ND ND ND ND NA
1/20/2012
1/28/2013
7/10/2014
7/10/2015
2/20/2020
WSW-4616 2/20/2020
Notes:
"<" or ND = Not Detected at or above the laboratory detection limit
Concentrations are reported in micrograms per liter (µg/L)
J = Estimated value below method reporting limit
B= Constituent is found in the associated blank as well as in the sample
WSW-1
2L Standard
TABLE 2
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
NCDEQ INCIDENT #22446
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
912 OLD HIGHWAY 21
MOODY'S GROCERY
WATER SUPPLY WELL ANALYTICAL RESULTS
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Resident Denied Acess
WSW-2
WSW-3
WSW-4
WSW-5
WSW-6
WSW-7
Not Sampled
Not Located
Not Located
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Page 1 of 1
Well
ID
Date
Installed
Well
Diameter
(inches)
Total
Depth
(feet)
Screen
Interval
(feet)
Top of
Casing
(feet)
MW-1 Unknown 2 60 Unknown 1,330.00
MW-2 Unknown 2 60 Unknown 1,330.65
MW-3 3/2/2010 2 52 37-52 1,329.84
MW-4 3/2/2010 2 45 30-45 1,320.36
MW-5 2/21/2020 2 50 40-50 1,321.88
WELL CONSTRUCTION DETAILS
TABLE 3
NCDEQ INCIDENT #22446
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
912 OLD HIGHWAY 21
MOODY'S GROCERY
Well ID Gauging Date
Screen
Interval
(feet)
Depth to
Groundwater
(feet)
*TOC
Elevation
(feet)
Groundwater
Elevation
(feet)
12/4/2002 47.95 1,330.00 1,282.05
4/15/2004 36.86 1,293.14
11/7/2005 39.67 1,290.33
9/24/2008 47.09 1,282.91
3/9/2010 42.95 1,287.05
12/4/2011 43.55 1,286.45
9/20/2012 40.93 1,289.07
7/10/2014 36.59 1,293.41
7/10/2015 41.86 1,288.14
11/21/2017 43.29 1,286.71
6/14/2018 43.89 1,286.11
4/10/2020 36.39 1,293.61
2/4/2021 32.33 1,297.67
12/28/2022 41.08 1,288.92
1/13/2023 40.86 1,289.14
12/4/2002 49.06 1,281.59
4/15/2004 36.95 1,293.70
11/7/2005 39.88 1,290.77
9/24/2008 47.35 1,283.30
3/9/2010 43.30 1,287.35
12/4/2011 44.01 1,286.64
9/20/2012 41.33 1,289.32
7/10/2014 36.80 1,293.85
7/10/2015 42.22 1,288.43
11/21/2017 43.69 1,286.96
6/14/2018 43.81 1,286.84
4/10/2020 36.62 1,294.03
2/4/2021 32.42 1,298.23
12/28/2022 41.55 1,289.10
MW-1 Unknown
MW-2 Unknown 1,330.65
TABLE 4
NCDEQ INCIDENT #22446
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
912 OLD HIGHWAY 21
MOODY'S GROCERY
GROUNDWATER ELEVATION DATA
Page 1 of 2
Well ID Gauging Date
Screen
Interval
(feet)
Depth to
Groundwater
(feet)
*TOC
Elevation
(feet)
Groundwater
Elevation
(feet)
TABLE 4
NCDEQ INCIDENT #22446
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
912 OLD HIGHWAY 21
MOODY'S GROCERY
GROUNDWATER ELEVATION DATA
3/9/2010 42.58 1,287.26
12/4/2011 43.37 1,286.47
9/20/2012 40.65 1,289.19
7/10/2014 36.14 1,293.70
7/10/2015 41.54 1,288.30
11/21/2017 43.02 1,286.82
6/14/2018 43.08 1,286.76
4/10/2020 35.89 1,293.95
2/4/2021 31.73 1,298.11
1/13/2023 39.73 1,290.11
3/9/2010 35.12 1,285.24
12/4/2011 36.57 1,283.79
9/20/2012 33.93 1,286.43
7/10/2014 29.90 1,290.46
7/10/2015 35.01 1,285.35
11/21/2017 36.58 1,283.78
6/14/2018 35.72 1,284.64
2/21/2020 29.99 1,290.37
4/10/2020 29.30 1,291.06
2/4/2021 25.91 1,294.45
1/13/2023 33.95 1,286.41
2/21/2020 30.90 1,290.98
4/10/2020 29.78 1,292.10
2/4/2021 26.80 1,295.08
1/13/2023 34.22 1,287.66
Notes:
TOC = Top Of Casing Elevations were based on an arbitrary elevation, measured in feet above mean sea level.
MW-5 40-50 1,321.88
MW-3 37-52 1,329.84
MW-4 30-45 1,320.36
Page 2 of 2
Well
ID Date Temperature
(◦C)
Conductivity
(µS/cm)
pH
(s.u.)
Oxidation-
Reduction
Potential
(mV)
Dissolved
Oxygen
(mg/L)
MW-1 12/28/2022 14.91 0.428 5.8 196 5.2
MW-4 1/13/2023 15.72 0.153 6.2 213 7.5
MW-5 1/13/2023 13.59 0.275 5.6 240 11.2
Notes:
°C = degrees Celsius
µS/cm = microSiemens per centimeter
s.u. = Standard Units
mV = millivolts
mg/L = milligrams per Liter
NCDEQ INCIDENT #22446
TABLE 5
FIELD PARAMETERS
MOODY'S GROCERY
912 OLD HIGHWAY 21
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
TABLE 6
RECENT GROUNDWATER ANALYTICAL RESULTS
MOODY'S GROCERY
912 OLD HIGHWAY 21
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
NCDEQ INCIDENT #22446
Sample ID Constituent
of Concern
BenzeneTolueneEthylbenzeneTotal XylenesDiisopropyl etherNaphthalenen-Butylbenzene1,2-DichloroethaneIsopropylbenzene (Cumene)n-Propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenetert-Amyl Alcohol1 600 600 500 70 6 70 0.4 70 70 400 400 N/A
5,000 260,000 80,000 50,000 70,000 6,000 5,900 400 25,000 26,100 28,500 24,100 40,000
MW-1 12/28/2022 167 29.0 11.9 80.3 30.5 7.6 1.2 8.8 1.4 1.2 21.7 9.6 80.1J
MW-4 01/13/2023 <0.34 <0.24 <0.30 <1.05 <0.31 <0.64 <0.49 <0.32 <0.33 <0.34 <0.50 <0.33 <36.4
MW-5 01/13/2023 9,350 5,790 675 5,320 <42.2 2,240 <49.0 650 <33.3 <34.0 747 250 <3640
WSW#1 12/28/2022 <0.34 <0.24 <0.30 <1.05 <0.31 <0.64 <0.49 <0.32 <0.33 <0.34 <0.50 <0.33 <36.4
FB 12/28/2022 <0.34 <0.24 <0.30 <1.05 <0.31 <0.64 <0.49 <0.32 <0.33 <0.34 <0.50 <0.33 <36.4
TRIP BLANK 12/28/2022 <0.34 <0.24 <0.30 <1.05 <0.31 <0.64 <0.49 <0.32 <0.33 <0.34 <0.50 <0.33 <36.4
Notes:
Concentrations are reported in micrograms per liter (µg/L)
"<" or ND = Not Detected at or above the laboratory reporting limit
J = Estimated value below method reporting limit
Concentrations in bold print exceed the 15A NCAC 02L Groundwater Standard (2L Standard).
GCL = Gross Contamination Level
Concentrations in underlined print exceed the GCL
2L Standards
GCL Standards
TABLE 7
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
MOODY'S GROCERY
912 OLD HIGHWAY 21
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
NCDEQ INCIDENT #22446
Monitoring
Well Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl TertiaryButyl EtherIsopropyl Ether1,2-Dibromoethane(Ethylene dibromide or EDB)NaphthaleneAcetonen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChloroethane1,2-DichloroethaneMathyl Butyl KetoneMethyl Ethyl KetoneMethy Isobutyl KetoneIsopropylbenzenep-Isopropyltoluenen-PropylbenzeneStyrene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadtert-Amyl Alcohol1 600 600 500 20 70 0.02 6 6,000 70 70 70 3,000 0.4 40 4,000 100 70 25 70 70 400 400 15 40
5,000 260,000 80,000 50,000 20,000 70,000 50 6,000 6,000,000 5,900 8,500 14,750 ---400 40,000 4,000,000 100,000 30,500 11,700 26,100 70,000 28,500 24,100 15,000 40,000
12/4/2002 400 730 120 740 47 170 NA 24 NA NA NA NA NA 31 NA --NA NA NA NA NA NA NA 6 NA
4/15/2004 270 730 76 410 37 130 NA ND NA NA NA NA NA ND NA --NA NA NA NA NA NA NA NA NA
11/7/2005 121 138 42.1 229 22.7 64.5 ND NA NA NA NA NA ND 5.14 NA --NA NA NA NA NA NA NA NA NA
5/2/2007 156 156 20.4 148 7.76 64.9 0.82 5.59 ND 0.57 ND ND ND 11.5 ND --ND 0.99 ND 1.39 ND 19.4 9.16 NA NA
9/24/2008 184 157 17.7 113 3.7 69.8 1.52 ND ND ND ND ND ND 17.3 ND --ND 0.86 ND 1.35 ND 14.4 5.89 NA NA
3/9/2010 300 150 26 117 17 81 2.3 7.8 3.4 J ND 0.69 0.61 ND 11 ND --ND 1.9 1.2 1.6 ND 23 11 NA NA
12/4/2011 1000 500 140 840 22 170 0.33 35 ND ND 0.5 0.67 3.3 44 26 --9.6 9.6 3.6 11 2.3 100 44 NA NA
9/20/2012 200 92 25 230 3.3 60 ND 14 ND ND ND ND ND 12 1.7 --ND 2.1 1 1.7 ND 44 18 NA NA
7/10/2014 330 350 71 600 <0.9 75 <0.89 <1.2 <47 <0.54 <0.84 <0.96 <1.6 <1.9 <15 --<15 2.3 J 2.6 J 2.6 J <1.2 110 32 NA NA
7/10/2015 570 300 130 670 4.4 110 <0.44 48 <23 2.6 1.4 J <0.48 <0.80 <0.97 <7.6 --<7.3 1.3 J 4.2 3.6 <0.60 140 46 NA NA
11/21/2017 1,100 510 240 710 <12 190 <3.7 26 140 J 8.2 J <12 <12 <50 69 91 J 130 44 J 12 J 6.8 J 9.8 J <12 140 51 NA NA
6/14/2018 140 57 8.4 76 6.9 120 0.75 3.2 J 72 0.15 J <0.50 <0.50 <0.50 25 15 <5.0 8.2 0.49 J 0.55 0.51 <0.50 9.4 6.7 NA NA
04/10/2020 479 150 21.1 197 <1.1 94.2 <0.58 16.2 NA <0.88 <0.62 <0.62 <0.88 26.2 NA NA NA 2.6 NA <0.60 <0.64 42.2 19.7 NA 313
02/04/2021 1,130 454 75 650 <4.4 159 <2.3 48.1 NA <3.5 <2.5 <2.5 <3.5 44.1 NA NA NA 6.9 NA <2.4 <2.6 130 52.8 NA 630J
12/28/2022 167 29.0 11.9 80.3 <0.84 30.5 <0.54 7.6 NA 1.2 <0.80 <0.65 <1.3 8.8 NA NA NA 1.4 NA 1.2 <0.58 21.7 9.6 NA 80.1J
12/4/2002 4.2 22 6.6 26 ND 1.4 NA 2.1 NA NA NA NA NA ND NA --NA NA NA NA NA NA NA NA NA
4/15/2004 ND ND ND 5.5 3.3 200 NA 1.4 NA NA NA NA NA 45 NA --NA NA NA NA NA NA NA NA NA
11/7/2005 14.7 3.9 8.24 11.1 ND 175 ND NA NA NA NA NA ND 25.8 NA --NA NA NA NA NA NA NA NA NA
5/2/2007 ND ND ND ND 0.51 29.9 ND ND ND ND ND ND ND 4.46 ND --ND ND ND ND ND ND ND NA NA
9/24/2008 ND ND ND ND ND 22.4 ND ND ND ND ND ND ND 1.1 ND --ND ND ND ND ND ND ND NA NA
3/9/2010 ND ND ND ND ND 4.2 ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND NA NA
12/4/2011 ND ND ND ND 0.75 J 9.1 ND ND ND ND ND ND ND 1.1 ND --ND ND ND ND ND ND ND NA NA
9/20/2012 ND ND ND ND 2 13 ND ND ND ND ND ND ND 1.4 ND --ND ND ND ND ND ND ND NA NA
7/10/2014 <0.079 <0.090 <0.092 <0.29 4.3 17 <0.089 <0.12 <4.7 <0.054 <0.084 <0.096 <0.16 2.8 <1.5 --<1.5 0.19 J 0.38 J <0.094 <0.12 <0.18 <0.10 NA NA
7/10/2015 <0.079 <0.090 <0.092 0.19 J 1.5 7.4 <0.089 1.6 6.2 B, J <0.054 <0.084 <0.096 <0.16 <0.19 <1.5 --<1.5 0.83 0.66 <0.094 <0.12 0.26 J <0.10 NA NA
11/21/2017 <0.50 <0.50 <0.50 <1.5 0.48 J 1.1 <0.15 <5.0 <50 <0.50 <0.50 <0.50 <0.50 0.40 J <5.0 <5.0 <5.0 0.57 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
6/14/2018 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <5.0 <50 <0.50 <0.50 <0.50 <0.50 <1.0 <5.0 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
02/04/2021 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.23 <0.66 NA <0.35 <0.25 <0.25 <0.35 <0.26 NA NA NA <0.24 NA <0.24 <0.26 <0.19 <0.23 NA <40.5
3/9/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND 62 NA
12/4/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.51 ND --ND ND ND ND ND ND ND NA NA
9/20/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.52 ND --ND ND ND ND ND ND ND NA NA
7/10/2014 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 <4.7 <0.054 <0.084 <0.096 <0.16 <0.19 <1.5 --<1.5 <0.11 <0.12 <0.094 <0.12 <0.18 <0.10 NA NA
7/10/2015 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 6.4 B, J <0.054 <0.084 <0.096 <0.16 <0.19 <1.5 --<1.5 <0.11 <0.12 <0.094 <0.12 <0.18 <0.10 NA NA
11/21/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.15 <5.0 <50 <0.50 <0.50 <0.50 <2.0 0.56 <5.0 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
6/14/2018 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <5.0 <50 <0.50 <0.50 <0.50 <0.50 <1.0 <5.0 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
02/04/2021 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.23 <0.66 NA <0.35 <0.25 <0.25 <0.35 0.32J NA NA NA <0.24 NA <0.24 <0.26 <0.19 <0.23 NA <40.5
2L Standard
GCL
MW-2
MW-3
MW-1
Page 1 of 2
TABLE 7
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
MOODY'S GROCERY
912 OLD HIGHWAY 21
STATE ROAD, WILKES COUNTY, NORTH CAROLINA
NCDEQ INCIDENT #22446
Monitoring
Well Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl TertiaryButyl EtherIsopropyl Ether1,2-Dibromoethane(Ethylene dibromide or EDB)NaphthaleneAcetonen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChloroethane1,2-DichloroethaneMathyl Butyl KetoneMethyl Ethyl KetoneMethy Isobutyl KetoneIsopropylbenzenep-Isopropyltoluenen-PropylbenzeneStyrene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadtert-Amyl Alcohol1 600 600 500 20 70 0.02 6 6,000 70 70 70 3,000 0.4 40 4,000 100 70 25 70 70 400 400 15 40
5,000 260,000 80,000 50,000 20,000 70,000 50 6,000 6,000,000 5,900 8,500 14,750 ---400 40,000 4,000,000 100,000 30,500 11,700 26,100 70,000 28,500 24,100 15,000 40,000
2L Standard
GCL
3/9/2010 ND ND ND ND ND ND ND ND 1.4 J ND ND ND ND ND ND --ND ND ND ND ND ND ND ND NA
12/4/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND NA NA
9/20/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND NA NA
7/10/2014 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 <4.7 <0.054 <0.084 <0.096 <0.16 <0.19 <1.5 --<1.5 <0.11 <0.12 <0.094 <0.12 <0.18 <0.10 NA NA
7/10/2015 <0.079 <0.09 <0.092 <0.29 <0.09 <0.18 <0.089 <0.12 5.3 B, J <0.054 <0.084 <0.096 <0.16 <0.19 <1.5 --<1.5 <0.11 <0.12 <0.094 <0.12 <0.18 <0.10 NA NA
11/21/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.15 <5.0 <50 <0.50 <0.50 <0.50 <2.0 <0.50 <5.0 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
6/14/2018 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <5.0 <50 <0.50 <0.50 <0.50 <0.50 <1.0 <5.0 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA
02/21/2020 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <2.0 NA <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA <0.50 NA <0.50 <0.50 <0.50 <0.50 NA <100
02/04/2021 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.23 <0.66 NA <0.35 <0.25 <0.25 <0.35 <0.26 NA NA NA <0.24 NA <0.24 <0.26 <0.19 <0.23 NA <40.5
01/13/2023 <0.34 <0.24 <0.30 <1.05 <0.42 <0.31 <0.27 <0.64 NA <0.49 <0.40 <0.32 <0.65 <0.32 NA NA NA <0.33 NA <0.34 <0.29 <0.50 <0.33 NA <36.4
02/21/2020 4,140 6,960 1,010 7,450 28.7 1,040 57.0 438 NA <25.0 <25.0 <25.0 <25.0 250 NA NA NA 34.9 NA 89.7 <25.0 1,110 294 NA 3,560J
02/04/2021 6,920 6,260 1,040 7,350 54.4 1,240 119 499 NA <17.6 <12.3 <12.5 <17.6 355 NA NA NA 47.4 NA <12.0 <12.8 1,090 339 NA 5,700
01/13/2023 9,350 5,790 675 5,320 <42.2 2,240 152 300 NA <49.0 <40.0 <32.3 <64.9 650 NA NA NA <33.3 NA <34.0 <29.2 747 250 NA <36.4
Notes:
Concentrations are reported in micrograms per liter (µg/L)Concentrations in bold print exceed the 15A 2L NCAC Groundwater Standard (2L Standard).
"<" or ND = Not Detected at or above the laboratory detection/reporting limit GCL = Gross Contamination Level
J = Estimated value below method reporting limit Concentrations in underlined print exceed the GCL
MW-4
MW-5
Page 2 of 2

FIGURES
SITE
CAD FILE PREP. BY REV. BY SCALE PROJECT NO.
TITLE
DATE
REFERENCE: USGS 7.5-MINUTE MAP, THURMOND, NORTH CAROLINA.
DATED 2016
LATITUDE:ƒ1257+
LONGITUDE:ƒ:(67
SITE
500'
1,000'
CAD FILE PREP. BY REV. BY SCALE PROJECT NO.
TITLE
DATE
IMAGE SOURCE: NC GEOSPATIAL DATABASE
WSW-717
WSW-743
WSW-767
WSW-781
WSW-805
WSW-835
WSW-857
WSW-4616
WSW-4562
WSW-4
WSW-255
WSW-259
WSW-250
WSW-5
WSW-955
WSW-937
WSW-2
WSW-6
WSW-1163
WSW-3
WSW-1
EXPLANATION
WATER SUPPLY WELL LOCATION
MINING RIDGE CHURCH ROAD (SR 1913)RESIDENCEOLD HIGHWAY 21ResidenceFORMER MOODY'SGROCERYRETAINING WALLUSTUSTUSTUSTUSTMW-2MW-3MW-4MW-1MW-5ASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28217
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILESource: NC GeospatialDatabase
MINING RIDGE CHURCH ROAD (SR 1913)RESIDENCEOLD HIGHWAY 21ResidenceMOODY'S GROCERYRETAINING WALLUSTUSTUSTUSTUSTMW-2MW-3MW-4MW-1MW-5WSW-1(704) 529-3200
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE LEGENDMonitoring Well LocationDepth to Groundwater (ft)1297.671. Groundwater elevations measured
01/13/2023 1,286.411,290.11NM1,289.14Groundwater Elevation Contour LineGroundwater Elevation Flow DirectionProperty Line(Dashed Where Inferred)1,287.66Water Supply Well LocationGROUNDWATER ELEVATION CONTOUR MAPMOODY'S GROCERY - INCIDENT #22446
912 OLD HIGHWAY 21
STATE ROAD, NORTH CAROLINA
LB NF AS SHOWN 01/13/2023 CIRK394548
41,290.01,289.01,288.01,287.0
MINING RIDGE CHURCH ROAD (SR 1913)RESIDENCEOLD HIGHWAY 21ResidenceMOODY'S GROCERYRETAINING WALLUSTUSTUSTUSTUSTMW-2MW-3MW-4MW-1MW-5WSW-1(704) 529-3200
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE LEGENDMonitoring Well LocationProperty LineWater Supply Well LocationGROUNDWATER QUALITY MAPMOODY'S GROCERY - INCIDENT #22446
912 OLD HIGHWAY 21
STATE ROAD, NORTH CAROLINA
LB NF AS SHOWN 01/13/2023 CIRK394548
5
Not SampledNSNSNS

APPENDIX A

FIELD NOTES AND PHOTO LOG
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: SLC2244602
REVIEWED BY: AQ SCALE: NTS DATE: 2/2023
Moody’s Grocery
912 Old Highway 21
State Road, Wilkes County, NC 28676
NCDEQ UST Incident # 22446
Photo # 2: Monitoring well MW-4, with block of ice filling well vault (12/28/2022)
Photo # 1: MW-4 looking east toward adjoining property with WSW-2 (12/28/2022)
MW-4
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: SLC2244602
REVIEWED BY: AQ SCALE: NTS DATE: 2/2023
Moody’s Grocery
912 Old Highway 21
State Road, Wilkes County, NC 28676
NCDEQ UST Incident # 22446
Photo # 4: Adjoining property with WSW-2 looking WSW, UST site building to the right, note change in
elevation and vegetation (12/28/2022)
Photo # 3: Adjoining property with WSW-2 looking SW, UST site building to the right (12/28/2022)
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: SLC2244602
REVIEWED BY: AQ SCALE: NTS DATE: 2/2023
Moody’s Grocery
912 Old Highway 21
State Road, Wilkes County, NC 28676
NCDEQ UST Incident # 22446
Photo # 6: Adjoining property with WSW-2 looking SE from rear of house (1/13/2023)
Photo # 5: Adjoining property with WSW-2 looking E from rear of house, note vegetation (12/28/2022)
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: SLC2244602
REVIEWED BY: AQ SCALE: NTS DATE: 2/2023
Moody’s Grocery
912 Old Highway 21
State Road, Wilkes County, NC 28676
NCDEQ UST Incident # 22446
Photo # 8: Adjacent property with WSW-2, in concrete cylinder cover left side of photo, residence to the right
side of photo
Photo # 7: Adjacent property with WSW-2, front of house looking west toward UST site building (1/13/2023)
WSW-2

APPENDIX B

LABORATORY ANALYTICAL RESULTS

#=CL#
January 23, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92646897
92646897
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
MOODY GROCERY
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92646897
MOODY GROCERY
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92646897
MOODY GROCERY
Lab ID Sample ID Matrix Date Collected Date Received
92646897001 MW4 Water 01/13/23 12:00 01/13/23 14:45
92646897002 MW5 Water 01/13/23 12:45 01/13/23 14:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92646897
MOODY GROCERY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92646897001 MW4 SM 6200B 69 PASI-CSAS
92646897002 MW5 SM 6200B 69 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646897
MOODY GROCERY
Sample:MW4 Lab ID:92646897001 Collected:01/13/23 12:00 Received:01/13/23 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 01/17/23 15:29 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 01/17/23 15:29 994-05-810.0 9.2 1
Benzene <0.34 ug/L 01/17/23 15:29 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 01/17/23 15:29 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 01/17/23 15:29 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 01/17/23 15:29 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 01/17/23 15:29 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 01/17/23 15:29 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 01/17/23 15:29 75-65-0 M150.0 26.8 1
n-Butylbenzene <0.49 ug/L 01/17/23 15:29 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 01/17/23 15:29 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 01/17/23 15:29 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 01/17/23 15:29 762-75-4 P550.0 29.4 1
Carbon tetrachloride <0.33 ug/L 01/17/23 15:29 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 01/17/23 15:29 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 01/17/23 15:29 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 01/17/23 15:29 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 01/17/23 15:29 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 01/17/23 15:29 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 01/17/23 15:29 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 01/17/23 15:29 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 01/17/23 15:29 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 01/17/23 15:29 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 01/17/23 15:29 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 01/17/23 15:29 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 01/17/23 15:29 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 01/17/23 15:29 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 01/17/23 15:29 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 01/17/23 15:29 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 01/17/23 15:29 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 01/17/23 15:29 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 01/17/23 15:29 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 01/17/23 15:29 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 01/17/23 15:29 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 01/17/23 15:29 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 01/17/23 15:29 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 01/17/23 15:29 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 01/17/23 15:29 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 01/17/23 15:29 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 01/17/23 15:29 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 01/17/23 15:29 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 01/17/23 15:29 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 01/17/23 15:29 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 01/17/23 15:29 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 01/17/23 15:29 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646897
MOODY GROCERY
Sample:MW4 Lab ID:92646897001 Collected:01/13/23 12:00 Received:01/13/23 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 01/17/23 15:29 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 01/17/23 15:29 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 01/17/23 15:29 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 01/17/23 15:29 103-65-10.50 0.34 1
Styrene <0.29 ug/L 01/17/23 15:29 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 01/17/23 15:29 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 01/17/23 15:29 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 01/17/23 15:29 127-18-40.50 0.29 1
Toluene <0.24 ug/L 01/17/23 15:29 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 01/17/23 15:29 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 01/17/23 15:29 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 01/17/23 15:29 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 01/17/23 15:29 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 01/17/23 15:29 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 01/17/23 15:29 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 01/17/23 15:29 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 01/17/23 15:29 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 01/17/23 15:29 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 01/17/23 15:29 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 01/17/23 15:29 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 01/17/23 15:29 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %01/17/23 15:29 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %01/17/23 15:29 460-00-470-130 1
Toluene-d8 (S)105 %01/17/23 15:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646897
MOODY GROCERY
Sample:MW5 Lab ID:92646897002 Collected:01/13/23 12:45 Received:01/13/23 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <3640 ug/L 01/20/23 23:57 75-85-4100003640100
tert-Amylmethyl ether <925 ug/L 01/20/23 23:57 994-05-81000925100
Benzene 9350 ug/L 01/20/23 23:57 71-43-250.0 34.5 100
Bromobenzene <29.0 ug/L 01/20/23 23:57 108-86-150.0 29.0 100
Bromochloromethane <46.8 ug/L 01/20/23 23:57 74-97-550.0 46.8 100
Bromodichloromethane <30.7 ug/L 01/20/23 23:57 75-27-450.0 30.7 100
Bromoform <34.1 ug/L 01/20/23 23:57 75-25-250.0 34.1 100
Bromomethane <166 ug/L 01/20/23 23:57 74-83-9500166100
tert-Butyl Alcohol <2680 ug/L 01/20/23 23:57 75-65-050002680100
n-Butylbenzene <49.0 ug/L 01/20/23 23:57 104-51-850.0 49.0 100
sec-Butylbenzene <40.0 ug/L 01/20/23 23:57 135-98-850.0 40.0 100
tert-Butylbenzene <32.3 ug/L 01/20/23 23:57 98-06-650.0 32.3 100
tert-Butyl Formate <2940 ug/L 01/20/23 23:57 762-75-450002940100
Carbon tetrachloride <33.3 ug/L 01/20/23 23:57 56-23-550.0 33.3 100
Chlorobenzene <28.4 ug/L 01/20/23 23:57 108-90-750.0 28.4 100
Chloroethane <64.9 ug/L 01/20/23 23:57 75-00-310064.9 100
Chloroform <43.0 ug/L 01/20/23 23:57 67-66-350.0 43.0 100
Chloromethane <54.0 ug/L 01/20/23 23:57 74-87-310054.0 100
2-Chlorotoluene <32.1 ug/L 01/20/23 23:57 95-49-850.0 32.1 100
4-Chlorotoluene <32.4 ug/L 01/20/23 23:57 106-43-450.0 32.4 100
1,2-Dibromo-3-chloropropane <34.0 ug/L 01/20/23 23:57 96-12-810034.0 100
Dibromochloromethane <35.9 ug/L 01/20/23 23:57 124-48-150.0 35.9 100
1,2-Dibromoethane (EDB)152 ug/L 01/20/23 23:57 106-93-450.0 27.2 100
Dibromomethane <39.4 ug/L 01/20/23 23:57 74-95-350.0 39.4 100
1,2-Dichlorobenzene <33.9 ug/L 01/20/23 23:57 95-50-150.0 33.9 100
1,3-Dichlorobenzene <34.0 ug/L 01/20/23 23:57 541-73-150.0 34.0 100
1,4-Dichlorobenzene <33.3 ug/L 01/20/23 23:57 106-46-750.0 33.3 100
Dichlorodifluoromethane <34.6 ug/L 01/20/23 23:57 75-71-850.0 34.6 100
1,1-Dichloroethane <36.7 ug/L 01/20/23 23:57 75-34-350.0 36.7 100
1,2-Dichloroethane 650 ug/L 01/20/23 23:57 107-06-250.0 32.2 100
1,1-Dichloroethene <34.8 ug/L 01/20/23 23:57 75-35-450.0 34.8 100
cis-1,2-Dichloroethene <38.4 ug/L 01/20/23 23:57 156-59-250.0 38.4 100
trans-1,2-Dichloroethene <39.6 ug/L 01/20/23 23:57 156-60-550.0 39.6 100
1,2-Dichloropropane <35.5 ug/L 01/20/23 23:57 78-87-550.0 35.5 100
1,3-Dichloropropane <28.4 ug/L 01/20/23 23:57 142-28-950.0 28.4 100
2,2-Dichloropropane <38.8 ug/L 01/20/23 23:57 594-20-750.0 38.8 100
1,1-Dichloropropene <42.7 ug/L 01/20/23 23:57 563-58-650.0 42.7 100
cis-1,3-Dichloropropene <36.5 ug/L 01/20/23 23:57 10061-01-550.0 36.5 100
trans-1,3-Dichloropropene <36.3 ug/L 01/20/23 23:57 10061-02-650.0 36.3 100
Diisopropyl ether 2240 ug/L 01/20/23 23:57 108-20-350.0 30.8 100
Ethanol <7220 ug/L 01/20/23 23:57 64-17-5200007220100
Ethylbenzene 675 ug/L 01/20/23 23:57 100-41-450.0 30.4 100
Ethyl-tert-butyl ether <324 ug/L 01/20/23 23:57 637-92-31000324100
Hexachloro-1,3-butadiene <153 ug/L 01/20/23 23:57 87-68-3200153100
Isopropylbenzene (Cumene)<33.3 ug/L 01/20/23 23:57 98-82-850.0 33.3 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92646897
MOODY GROCERY
Sample:MW5 Lab ID:92646897002 Collected:01/13/23 12:45 Received:01/13/23 14:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <195 ug/L 01/20/23 23:57 75-09-2200195100
Methyl-tert-butyl ether <42.2 ug/L 01/20/23 23:57 1634-04-450.0 42.2 100
Naphthalene 300 ug/L 01/20/23 23:57 91-20-320064.5 100
n-Propylbenzene <34.0 ug/L 01/20/23 23:57 103-65-150.0 34.0 100
Styrene <29.2 ug/L 01/20/23 23:57 100-42-550.0 29.2 100
1,1,1,2-Tetrachloroethane <31.1 ug/L 01/20/23 23:57 630-20-650.0 31.1 100
1,1,2,2-Tetrachloroethane <22.5 ug/L 01/20/23 23:57 79-34-550.0 22.5 100
Tetrachloroethene <29.2 ug/L 01/20/23 23:57 127-18-450.0 29.2 100
Toluene 5790 ug/L 01/20/23 23:57 108-88-350.0 23.9 100
1,2,3-Trichlorobenzene <80.6 ug/L 01/20/23 23:57 87-61-620080.6 100
1,2,4-Trichlorobenzene <63.9 ug/L 01/20/23 23:57 120-82-120063.9 100
1,1,1-Trichloroethane <33.2 ug/L 01/20/23 23:57 71-55-650.0 33.2 100
1,1,2-Trichloroethane <32.5 ug/L 01/20/23 23:57 79-00-550.0 32.5 100
Trichloroethene <38.3 ug/L 01/20/23 23:57 79-01-650.0 38.3 100
Trichlorofluoromethane <29.8 ug/L 01/20/23 23:57 75-69-410029.8 100
1,2,3-Trichloropropane <26.1 ug/L 01/20/23 23:57 96-18-450.0 26.1 100
1,2,4-Trimethylbenzene 747 ug/L 01/20/23 23:57 95-63-650.0 49.5 100
1,3,5-Trimethylbenzene 250 ug/L 01/20/23 23:57 108-67-850.0 33.2 100
Vinyl chloride <38.6 ug/L 01/20/23 23:57 75-01-410038.6 100
m&p-Xylene 3670 ug/L 01/20/23 23:57 179601-23-110070.9 100
o-Xylene 1650 ug/L 01/20/23 23:57 95-47-650.0 33.8 100
Surrogates
1,2-Dichloroethane-d4 (S)105 %01/20/23 23:57 17060-07-070-130 100
4-Bromofluorobenzene (S)100 %01/20/23 23:57 460-00-470-130 100
Toluene-d8 (S)99 %01/20/23 23:57 2037-26-570-130 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
749777
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92646897001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3897382
Associated Lab Samples:92646897001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 01/17/23 12:290.31
1,1,1-Trichloroethane ug/L <0.33 0.50 01/17/23 12:290.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 01/17/23 12:290.22
1,1,2-Trichloroethane ug/L <0.32 0.50 01/17/23 12:290.32
1,1-Dichloroethane ug/L <0.37 0.50 01/17/23 12:290.37
1,1-Dichloroethene ug/L <0.35 0.50 01/17/23 12:290.35
1,1-Dichloropropene ug/L <0.43 0.50 01/17/23 12:290.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 01/17/23 12:290.81
1,2,3-Trichloropropane ug/L <0.26 0.50 01/17/23 12:290.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 01/17/23 12:290.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/17/23 12:290.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 01/17/23 12:290.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 01/17/23 12:290.27
1,2-Dichlorobenzene ug/L <0.34 0.50 01/17/23 12:290.34
1,2-Dichloroethane ug/L <0.32 0.50 01/17/23 12:290.32
1,2-Dichloropropane ug/L <0.36 0.50 01/17/23 12:290.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 01/17/23 12:290.33
1,3-Dichlorobenzene ug/L <0.34 0.50 01/17/23 12:290.34
1,3-Dichloropropane ug/L <0.28 0.50 01/17/23 12:290.28
1,4-Dichlorobenzene ug/L <0.33 0.50 01/17/23 12:290.33
2,2-Dichloropropane ug/L <0.39 0.50 01/17/23 12:290.39
2-Chlorotoluene ug/L <0.32 0.50 01/17/23 12:290.32
4-Chlorotoluene ug/L <0.32 0.50 01/17/23 12:290.32
Benzene ug/L <0.34 0.50 01/17/23 12:290.34
Bromobenzene ug/L <0.29 0.50 01/17/23 12:290.29
Bromochloromethane ug/L <0.47 0.50 01/17/23 12:290.47
Bromodichloromethane ug/L <0.31 0.50 01/17/23 12:290.31
Bromoform ug/L <0.34 0.50 01/17/23 12:290.34
Bromomethane ug/L <1.7 5.0 01/17/23 12:291.7
Carbon tetrachloride ug/L <0.33 0.50 01/17/23 12:290.33
Chlorobenzene ug/L <0.28 0.50 01/17/23 12:290.28
Chloroethane ug/L <0.65 1.0 01/17/23 12:290.65
Chloroform ug/L <0.43 0.50 01/17/23 12:290.43
Chloromethane ug/L <0.54 1.0 01/17/23 12:290.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 01/17/23 12:290.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 01/17/23 12:290.36
Dibromochloromethane ug/L <0.36 0.50 01/17/23 12:290.36
Dibromomethane ug/L <0.39 0.50 01/17/23 12:290.39
Dichlorodifluoromethane ug/L <0.35 0.50 01/17/23 12:290.35
Diisopropyl ether ug/L <0.31 0.50 01/17/23 12:290.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3897382
Associated Lab Samples:92646897001
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 01/17/23 12:2972.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 01/17/23 12:293.2
Ethylbenzene ug/L <0.30 0.50 01/17/23 12:290.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 01/17/23 12:291.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 01/17/23 12:290.33
m&p-Xylene ug/L <0.71 1.0 01/17/23 12:290.71
Methyl-tert-butyl ether ug/L <0.42 0.50 01/17/23 12:290.42
Methylene Chloride ug/L <2.0 2.0 01/17/23 12:292.0
n-Butylbenzene ug/L <0.49 0.50 01/17/23 12:290.49
n-Propylbenzene ug/L <0.34 0.50 01/17/23 12:290.34
Naphthalene ug/L <0.64 2.0 01/17/23 12:290.64
o-Xylene ug/L <0.34 0.50 01/17/23 12:290.34
sec-Butylbenzene ug/L <0.40 0.50 01/17/23 12:290.40
Styrene ug/L <0.29 0.50 01/17/23 12:290.29
tert-Amyl Alcohol ug/L <36.4 100 01/17/23 12:2936.4
tert-Amylmethyl ether ug/L <9.2 10.0 01/17/23 12:299.2
tert-Butyl Alcohol ug/L <26.8 50.0 01/17/23 12:2926.8
tert-Butyl Formate ug/L <29.4 50.0 01/17/23 12:2929.4
tert-Butylbenzene ug/L <0.32 0.50 01/17/23 12:290.32
Tetrachloroethene ug/L <0.29 0.50 01/17/23 12:290.29
Toluene ug/L <0.24 0.50 01/17/23 12:290.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 01/17/23 12:290.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 01/17/23 12:290.36
Trichloroethene ug/L <0.38 0.50 01/17/23 12:290.38
Trichlorofluoromethane ug/L <0.30 1.0 01/17/23 12:290.30
Vinyl chloride ug/L <0.39 1.0 01/17/23 12:290.39
1,2-Dichloroethane-d4 (S)%101 70-130 01/17/23 12:29
4-Bromofluorobenzene (S)%99 70-130 01/17/23 12:29
Toluene-d8 (S)%108 70-130 01/17/23 12:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3897383LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.520 102 60-140
1,1,1-Trichloroethane ug/L 23.920 119 60-140
1,1,2,2-Tetrachloroethane ug/L 22.020 110 60-140
1,1,2-Trichloroethane ug/L 21.520 108 60-140
1,1-Dichloroethane ug/L 23.620 118 60-140
1,1-Dichloroethene ug/L 25.520 127 60-140
1,1-Dichloropropene ug/L 22.820 114 60-140
1,2,3-Trichlorobenzene ug/L 23.320 117 60-140
1,2,3-Trichloropropane ug/L 20.620 103 60-140
1,2,4-Trichlorobenzene ug/L 22.420 112 60-140
1,2,4-Trimethylbenzene ug/L 23.120 115 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3897383LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 22.620 113 60-140
1,2-Dibromoethane (EDB)ug/L 22.720 114 60-140
1,2-Dichlorobenzene ug/L 20.020 100 60-140
1,2-Dichloroethane ug/L 23.420 117 60-140
1,2-Dichloropropane ug/L 24.320 122 60-140
1,3,5-Trimethylbenzene ug/L 23.620 118 60-140
1,3-Dichlorobenzene ug/L 20.920 105 60-140
1,3-Dichloropropane ug/L 23.020 115 60-140
1,4-Dichlorobenzene ug/L 20.420 102 60-140
2,2-Dichloropropane ug/L 24.520 122 60-140
2-Chlorotoluene ug/L 21.020 105 60-140
4-Chlorotoluene ug/L 22.920 115 60-140
Benzene ug/L 22.120 110 60-140
Bromobenzene ug/L 21.920 110 60-140
Bromochloromethane ug/L 22.420 112 60-140
Bromodichloromethane ug/L 24.320 121 60-140
Bromoform ug/L 21.520 108 60-140
Bromomethane ug/L 20.720 104 60-140
Carbon tetrachloride ug/L 25.620 128 60-140
Chlorobenzene ug/L 22.320 111 60-140
Chloroethane ug/L 25.720 129 60-140
Chloroform ug/L 24.220 121 60-140
Chloromethane ug/L 25.120 126 60-140
cis-1,2-Dichloroethene ug/L 23.520 118 60-140
cis-1,3-Dichloropropene ug/L 23.920 120 60-140
Dibromochloromethane ug/L 22.820 114 60-140
Dibromomethane ug/L 23.020 115 60-140
Dichlorodifluoromethane ug/L 25.020 125 60-140
Diisopropyl ether ug/L 22.820 114 60-140
Ethanol ug/L 932800 116 60-140
Ethyl-tert-butyl ether ug/L 41.940 105 60-140
Ethylbenzene ug/L 22.120 111 60-140
Hexachloro-1,3-butadiene ug/L 23.720 119 60-140
Isopropylbenzene (Cumene)ug/L 21.920 110 60-140
m&p-Xylene ug/L 45.940 115 60-140
Methyl-tert-butyl ether ug/L 22.520 113 60-140
Methylene Chloride ug/L 23.820 119 60-140
n-Butylbenzene ug/L 25.320 126 60-140
n-Propylbenzene ug/L 23.120 116 60-140
Naphthalene ug/L 26.620 133 60-140
o-Xylene ug/L 23.020 115 60-140
sec-Butylbenzene ug/L 23.920 120 60-140
Styrene ug/L 23.420 117 60-140
tert-Amyl Alcohol ug/L 434400 108 60-140
tert-Amylmethyl ether ug/L 43.040 108 60-140
tert-Butyl Alcohol ug/L 206200 103 60-140
tert-Butyl Formate ug/L 173160 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3897383LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 20.020 100 60-140
Tetrachloroethene ug/L 21.220 106 60-140
Toluene ug/L 22.420 112 60-140
trans-1,2-Dichloroethene ug/L 23.720 119 60-140
trans-1,3-Dichloropropene ug/L 23.320 116 60-140
Trichloroethene ug/L 24.820 124 60-140
Trichlorofluoromethane ug/L 22.020 110 60-140
Vinyl chloride ug/L 24.620 123 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3897384MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92646897001
3897385
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 85 60-140100 16 3020<0.31 17.0 20.1
1,1,1-Trichloroethane ug/L 20 111 60-140124 10 3020<0.33 22.3 24.7
1,1,2,2-Tetrachloroethane ug/L 20 93 60-140106 14 3020<0.22 18.5 21.3
1,1,2-Trichloroethane ug/L 20 101 60-140108 7 3020<0.32 20.2 21.6
1,1-Dichloroethane ug/L 20 109 60-140119 9 3020<0.37 21.8 23.8
1,1-Dichloroethene ug/L 20 118 60-140132 11 3020<0.35 23.6 26.4
1,1-Dichloropropene ug/L 20 104 60-140116 11 3020<0.43 20.9 23.3
1,2,3-Trichlorobenzene ug/L 20 86 60-14099 14 3020<0.81 17.2 19.9
1,2,3-Trichloropropane ug/L 20 86 60-140104 18 3020<0.26 17.3 20.8
1,2,4-Trichlorobenzene ug/L 20 88 60-14098 11 3020<0.64 17.6 19.6
1,2,4-Trimethylbenzene ug/L 20 98 60-140116 16 3020<0.50 19.7 23.2
1,2-Dibromo-3-
chloropropane ug/L 20 94 60-140108 14 3020<0.34 18.8 21.5
1,2-Dibromoethane (EDB)ug/L 20 97 60-140111 14 3020<0.27 19.4 22.2
1,2-Dichlorobenzene ug/L 20 85 60-14099 16 3020<0.34 16.9 19.9
1,2-Dichloroethane ug/L 20 105 60-140121 14 3020<0.32 21.1 24.2
1,2-Dichloropropane ug/L 20 108 60-140120 10 3020<0.36 21.6 23.9
1,3,5-Trimethylbenzene ug/L 20 104 60-140119 13 3020<0.33 20.9 23.9
1,3-Dichlorobenzene ug/L 20 86 60-140102 17 3020<0.34 17.2 20.4
1,3-Dichloropropane ug/L 20 98 60-140113 15 3020<0.28 19.5 22.6
1,4-Dichlorobenzene ug/L 20 84 60-14096 14 3020<0.33 16.8 19.3
2,2-Dichloropropane ug/L 20 112 60-140120 6 3020<0.39 22.5 24.0
2-Chlorotoluene ug/L 20 94 60-140109 15 3020<0.32 18.8 21.8
4-Chlorotoluene ug/L 20 98 60-140110 12 3020<0.32 19.5 21.9
Benzene ug/L 20 101 60-140113 11 3020<0.34 20.2 22.6
Bromobenzene ug/L 20 93 60-140107 13 3020<0.29 18.7 21.3
Bromochloromethane ug/L 20 99 60-140115 15 3020<0.47 19.8 23.0
Bromodichloromethane ug/L 20 110 60-140115 5 3020<0.31 21.9 23.0
Bromoform ug/L 20 90 60-140102 13 3020<0.34 18.0 20.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3897384MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92646897001
3897385
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 65 60-14089 30 3020<1.7 13.1 17.7
Carbon tetrachloride ug/L 20 118 60-140128 8 3020<0.33 23.6 25.5
Chlorobenzene ug/L 20 96 60-140113 16 3020<0.28 19.2 22.6
Chloroethane ug/L 20 121 60-140134 10 3020<0.65 24.2 26.8
Chloroform ug/L 20 108 60-140121 12 3020<0.43 21.6 24.2
Chloromethane ug/L 20 118 60-140131 11 3020<0.54 23.5 26.1
cis-1,2-Dichloroethene ug/L 20 107 60-140120 11 3020<0.38 21.4 23.9
cis-1,3-Dichloropropene ug/L 20 105 60-140115 9 3020<0.36 21.0 23.0
Dibromochloromethane ug/L 20 94 60-140116 20 3020<0.36 18.9 23.1
Dibromomethane ug/L 20 97 60-140105 8 3020<0.39 19.5 21.1
Dichlorodifluoromethane ug/L 20 106 60-140118 11 3020<0.35 21.2 23.6
Diisopropyl ether ug/L 20 101 60-140115 13 3020<0.31 20.2 22.9
Ethanol ug/L 800 101 60-140117 15 30800<72.2 807 939
Ethyl-tert-butyl ether ug/L 40 90 60-140101 12 3040<3.2 36.0 40.4
Ethylbenzene ug/L 20 97 60-140112 14 3020<0.30 19.5 22.4
Hexachloro-1,3-butadiene ug/L 20 89 60-140115 25 3020<1.5 17.8 22.9
Isopropylbenzene
(Cumene)ug/L 20 95 60-140114 18 3020<0.33 19.1 22.7
m&p-Xylene ug/L 40 96 60-140113 16 3040<0.71 38.4 45.1
Methyl-tert-butyl ether ug/L 20 93 60-140102 9 3020<0.42 18.5 20.4
Methylene Chloride ug/L 20 106 60-140119 12 3020<2.0 21.2 23.9
n-Butylbenzene ug/L 20 106 60-140124 16 3020<0.49 21.2 24.8
n-Propylbenzene ug/L 20 101 60-140114 12 3020<0.34 20.2 22.7
Naphthalene ug/L 20 92 60-140113 21 3020<0.64 18.3 22.6
o-Xylene ug/L 20 94 60-140116 21 3020<0.34 18.9 23.2
sec-Butylbenzene ug/L 20 102 60-140121 17 3020<0.40 20.5 24.2
Styrene ug/L 20 93 60-140110 17 3020<0.29 18.6 22.1
tert-Amyl Alcohol ug/L 400 91 60-14099 9 30400<36.4 363 398
tert-Amylmethyl ether ug/L 40 93 60-140101 8 3040<9.2 37.2 40.3
tert-Butyl Alcohol ug/L M120012960-140141 9 30200<26.8 259 282
tert-Butyl Formate ug/L P5160660-1405 30160<29.4 <29.4 <29.4
tert-Butylbenzene ug/L 20 88 60-140101 14 3020<0.32 17.6 20.2
Tetrachloroethene ug/L 20 91 60-140106 15 3020<0.29 18.3 21.2
Toluene ug/L 20 103 60-140112 8 3020<0.24 20.6 22.3
trans-1,2-Dichloroethene ug/L 20 111 60-140124 11 3020<0.40 22.1 24.8
trans-1,3-Dichloropropene ug/L 20 100 60-140112 12 3020<0.36 20.0 22.4
Trichloroethene ug/L 20 111 60-140116 4 3020<0.38 22.1 23.1
Trichlorofluoromethane ug/L 20 109 60-140119 9 3020<0.30 21.8 23.7
Vinyl chloride ug/L 20 116 60-140125 8 3020<0.39 23.1 25.1
1,2-Dichloroethane-d4 (S)%112 70-130107
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%102 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
750552
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92646897002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3901051
Associated Lab Samples:92646897002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 01/20/23 14:510.31
1,1,1-Trichloroethane ug/L <0.33 0.50 01/20/23 14:510.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 01/20/23 14:510.22
1,1,2-Trichloroethane ug/L <0.32 0.50 01/20/23 14:510.32
1,1-Dichloroethane ug/L <0.37 0.50 01/20/23 14:510.37
1,1-Dichloroethene ug/L <0.35 0.50 01/20/23 14:510.35
1,1-Dichloropropene ug/L <0.43 0.50 01/20/23 14:510.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 01/20/23 14:510.81
1,2,3-Trichloropropane ug/L <0.26 0.50 01/20/23 14:510.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 01/20/23 14:510.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/20/23 14:510.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 01/20/23 14:510.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 01/20/23 14:510.27
1,2-Dichlorobenzene ug/L <0.34 0.50 01/20/23 14:510.34
1,2-Dichloroethane ug/L <0.32 0.50 01/20/23 14:510.32
1,2-Dichloropropane ug/L <0.36 0.50 01/20/23 14:510.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 01/20/23 14:510.33
1,3-Dichlorobenzene ug/L <0.34 0.50 01/20/23 14:510.34
1,3-Dichloropropane ug/L <0.28 0.50 01/20/23 14:510.28
1,4-Dichlorobenzene ug/L <0.33 0.50 01/20/23 14:510.33
2,2-Dichloropropane ug/L <0.39 0.50 01/20/23 14:510.39
2-Chlorotoluene ug/L <0.32 0.50 01/20/23 14:510.32
4-Chlorotoluene ug/L <0.32 0.50 01/20/23 14:510.32
Benzene ug/L <0.34 0.50 01/20/23 14:510.34
Bromobenzene ug/L <0.29 0.50 01/20/23 14:510.29
Bromochloromethane ug/L <0.47 0.50 01/20/23 14:510.47
Bromodichloromethane ug/L <0.31 0.50 01/20/23 14:510.31
Bromoform ug/L <0.34 0.50 01/20/23 14:510.34
Bromomethane ug/L <1.7 5.0 01/20/23 14:511.7
Carbon tetrachloride ug/L <0.33 0.50 01/20/23 14:510.33
Chlorobenzene ug/L <0.28 0.50 01/20/23 14:510.28
Chloroethane ug/L <0.65 1.0 01/20/23 14:510.65
Chloroform ug/L <0.43 0.50 01/20/23 14:510.43
Chloromethane ug/L <0.54 1.0 01/20/23 14:510.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 01/20/23 14:510.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 01/20/23 14:510.36
Dibromochloromethane ug/L <0.36 0.50 01/20/23 14:510.36
Dibromomethane ug/L <0.39 0.50 01/20/23 14:510.39
Dichlorodifluoromethane ug/L <0.35 0.50 01/20/23 14:510.35
Diisopropyl ether ug/L <0.31 0.50 01/20/23 14:510.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
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[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3901051
Associated Lab Samples:92646897002
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 01/20/23 14:5172.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 01/20/23 14:513.2
Ethylbenzene ug/L <0.30 0.50 01/20/23 14:510.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 01/20/23 14:511.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 01/20/23 14:510.33
m&p-Xylene ug/L <0.71 1.0 01/20/23 14:510.71
Methyl-tert-butyl ether ug/L <0.42 0.50 01/20/23 14:510.42
Methylene Chloride ug/L <2.0 2.0 01/20/23 14:512.0
n-Butylbenzene ug/L <0.49 0.50 01/20/23 14:510.49
n-Propylbenzene ug/L <0.34 0.50 01/20/23 14:510.34
Naphthalene ug/L <0.64 2.0 01/20/23 14:510.64
o-Xylene ug/L <0.34 0.50 01/20/23 14:510.34
sec-Butylbenzene ug/L <0.40 0.50 01/20/23 14:510.40
Styrene ug/L <0.29 0.50 01/20/23 14:510.29
tert-Amyl Alcohol ug/L <36.4 100 01/20/23 14:5136.4
tert-Amylmethyl ether ug/L <9.2 10.0 01/20/23 14:519.2
tert-Butyl Alcohol ug/L <26.8 50.0 01/20/23 14:5126.8
tert-Butyl Formate ug/L <29.4 50.0 01/20/23 14:5129.4
tert-Butylbenzene ug/L <0.32 0.50 01/20/23 14:510.32
Tetrachloroethene ug/L <0.29 0.50 01/20/23 14:510.29
Toluene ug/L <0.24 0.50 01/20/23 14:510.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 01/20/23 14:510.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 01/20/23 14:510.36
Trichloroethene ug/L <0.38 0.50 01/20/23 14:510.38
Trichlorofluoromethane ug/L <0.30 1.0 01/20/23 14:510.30
Vinyl chloride ug/L <0.39 1.0 01/20/23 14:510.39
1,2-Dichloroethane-d4 (S)%106 70-130 01/20/23 14:51
4-Bromofluorobenzene (S)%97 70-130 01/20/23 14:51
Toluene-d8 (S)%103 70-130 01/20/23 14:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3901052LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.220 106 60-140
1,1,1-Trichloroethane ug/L 23.120 115 60-140
1,1,2,2-Tetrachloroethane ug/L 20.820 104 60-140
1,1,2-Trichloroethane ug/L 21.920 109 60-140
1,1-Dichloroethane ug/L 23.120 115 60-140
1,1-Dichloroethene ug/L 25.320 127 60-140
1,1-Dichloropropene ug/L 24.820 124 60-140
1,2,3-Trichlorobenzene ug/L 23.720 118 60-140
1,2,3-Trichloropropane ug/L 21.020 105 60-140
1,2,4-Trichlorobenzene ug/L 23.020 115 60-140
1,2,4-Trimethylbenzene ug/L 22.720 113 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
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Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3901052LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 20.820 104 60-140
1,2-Dibromoethane (EDB)ug/L 22.720 113 60-140
1,2-Dichlorobenzene ug/L 21.820 109 60-140
1,2-Dichloroethane ug/L 22.720 114 60-140
1,2-Dichloropropane ug/L 22.820 114 60-140
1,3,5-Trimethylbenzene ug/L 22.720 113 60-140
1,3-Dichlorobenzene ug/L 22.120 110 60-140
1,3-Dichloropropane ug/L 22.320 112 60-140
1,4-Dichlorobenzene ug/L 21.120 105 60-140
2,2-Dichloropropane ug/L 23.320 116 60-140
2-Chlorotoluene ug/L 21.620 108 60-140
4-Chlorotoluene ug/L 22.520 112 60-140
Benzene ug/L 20.120 101 60-140
Bromobenzene ug/L 21.320 107 60-140
Bromochloromethane ug/L 22.420 112 60-140
Bromodichloromethane ug/L 21.620 108 60-140
Bromoform ug/L 20.720 103 60-140
Bromomethane ug/L 17.320 87 60-140
Carbon tetrachloride ug/L 22.220 111 60-140
Chlorobenzene ug/L 22.220 111 60-140
Chloroethane ug/L 26.120 131 60-140
Chloroform ug/L 22.120 110 60-140
Chloromethane ug/L 25.420 127 60-140
cis-1,2-Dichloroethene ug/L 22.920 115 60-140
cis-1,3-Dichloropropene ug/L 22.420 112 60-140
Dibromochloromethane ug/L 21.620 108 60-140
Dibromomethane ug/L 21.520 108 60-140
Dichlorodifluoromethane ug/L 23.520 117 60-140
Diisopropyl ether ug/L 22.920 114 60-140
Ethanol ug/L 879800 110 60-140
Ethyl-tert-butyl ether ug/L 43.740 109 60-140
Ethylbenzene ug/L 22.020 110 60-140
Hexachloro-1,3-butadiene ug/L 23.020 115 60-140
Isopropylbenzene (Cumene)ug/L 21.420 107 60-140
m&p-Xylene ug/L 43.940 110 60-140
Methyl-tert-butyl ether ug/L 21.620 108 60-140
Methylene Chloride ug/L 22.720 114 60-140
n-Butylbenzene ug/L 23.620 118 60-140
n-Propylbenzene ug/L 21.920 110 60-140
Naphthalene ug/L 24.620 123 60-140
o-Xylene ug/L 21.820 109 60-140
sec-Butylbenzene ug/L 22.920 114 60-140
Styrene ug/L 22.620 113 60-140
tert-Amyl Alcohol ug/L 404400 101 60-140
tert-Amylmethyl ether ug/L 43.540 109 60-140
tert-Butyl Alcohol ug/L 205200 103 60-140
tert-Butyl Formate ug/L 177160 110 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
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Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3901052LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 18.320 91 60-140
Tetrachloroethene ug/L 22.020 110 60-140
Toluene ug/L 21.220 106 60-140
trans-1,2-Dichloroethene ug/L 23.820 119 60-140
trans-1,3-Dichloropropene ug/L 22.520 112 60-140
Trichloroethene ug/L 23.320 117 60-140
Trichlorofluoromethane ug/L 20.820 104 60-140
Vinyl chloride ug/L 23.720 118 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3901053MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92647170003
3901054
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 128 60-140121 6 3020ND25.7 24.1
1,1,1-Trichloroethane ug/L M12015060-140142 5 3020ND30.0 28.4
1,1,2,2-Tetrachloroethane ug/L 20 129 60-140124 3 3020ND25.8 24.9
1,1,2-Trichloroethane ug/L 20 133 60-140127 5 3020ND26.6 25.4
1,1-Dichloroethane ug/L M12014860-140141 5 3020ND29.5 28.1
1,1-Dichloroethene ug/L M12016160-140153 6 3020ND32.3 30.6
1,1-Dichloropropene ug/L M12016360-140154 5 3020ND32.6 30.9
1,2,3-Trichlorobenzene ug/L 20 129 60-140139 8 3020ND25.8 27.9
1,2,3-Trichloropropane ug/L 20 130 60-140126 3 3020ND26.0 25.2
1,2,4-Trichlorobenzene ug/L 20 132 60-140131 1 3020ND26.3 26.2
1,2,4-Trimethylbenzene ug/L 20 139 60-140138 1 3020ND27.8 27.6
1,2-Dibromo-3-
chloropropane ug/L 20 113 60-140116 2 3020ND22.7 23.1
1,2-Dibromoethane (EDB)ug/L 20 136 60-140132 3 3020ND27.2 26.3
1,2-Dichlorobenzene ug/L 20 133 60-140133 1 3020ND26.7 26.5
1,2-Dichloroethane ug/L M12014660-140138 6 3020ND29.2 27.6
1,2-Dichloropropane ug/L M12014560-140135 7 3020ND29.0 27.1
1,3,5-Trimethylbenzene ug/L 20 138 60-140137 1 3020ND27.6 27.4
1,3-Dichlorobenzene ug/L 20 133 60-140133 0 3020ND26.7 26.6
1,3-Dichloropropane ug/L 20 137 60-140130 5 3020ND27.5 26.1
1,4-Dichlorobenzene ug/L 20 126 60-140124 1 3020ND25.2 24.9
2,2-Dichloropropane ug/L M12015260-140142 6 3020ND30.4 28.5
2-Chlorotoluene ug/L 20 135 60-140134 1 3020ND27.0 26.8
4-Chlorotoluene ug/L 20 135 60-140137 1 3020ND27.1 27.4
Benzene ug/L 20 126 60-140119 6 3020ND25.2 23.8
Bromobenzene ug/L 20 128 60-140128 0 3020ND25.6 25.6
Bromochloromethane ug/L 20 140 60-140134 5 3020ND28.0 26.7
Bromodichloromethane ug/L 20 126 60-140120 5 3020ND25.3 24.0
Bromoform ug/L 20 111 60-140106 4 3020ND22.2 21.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
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Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92646897
MOODY GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3901053MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92647170003
3901054
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 112 60-140104 8 3020ND22.5 20.8
Carbon tetrachloride ug/L 20 133 60-140123 8 3020ND26.6 24.5
Chlorobenzene ug/L 20 136 60-140129 5 3020ND27.1 25.9
Chloroethane ug/L M12016560-140156 5 3020ND32.9 31.2
Chloroform ug/L M12014560-140136 7 3020ND29.3 27.4
Chloromethane ug/L 20 138 60-140133 4 3020ND27.6 26.6
cis-1,2-Dichloroethene ug/L M12014760-140142 4 3020ND29.5 28.3
cis-1,3-Dichloropropene ug/L 20 131 60-140123 6 3020ND26.3 24.7
Dibromochloromethane ug/L 20 120 60-140116 4 3020ND24.1 23.2
Dibromomethane ug/L 20 128 60-140121 6 3020ND25.7 24.2
Dichlorodifluoromethane ug/L 20 114 60-140107 6 3020ND22.7 21.4
Diisopropyl ether ug/L M12014860-140144 3 3020ND29.7 28.8
Ethanol ug/L M180014460-140136 5 30800ND11501090
Ethyl-tert-butyl ether ug/L M14014260-140138 3 3040ND57.0 55.2
Ethylbenzene ug/L 20 138 60-140132 4 3020ND27.7 26.5
Hexachloro-1,3-butadiene ug/L 20 131 60-140131 0 3020ND26.3 26.2
Isopropylbenzene
(Cumene)ug/L 20 138 60-140133 4 3020ND27.6 26.5
m&p-Xylene ug/L M14014160-140135 4 3040ND56.2 54.0
Methyl-tert-butyl ether ug/L 20 140 60-140135 4 3020ND28.0 26.9
Methylene Chloride ug/L M12014260-140136 5 3020ND28.5 27.1
n-Butylbenzene ug/L M12014660-140145 1 3020ND29.2 29.0
n-Propylbenzene ug/L 20 138 60-140135 2 3020ND27.5 27.0
Naphthalene ug/L 20 136 60-140140 3 3020ND27.2 28.1
o-Xylene ug/L 20 139 60-140133 4 3020ND27.8 26.7
sec-Butylbenzene ug/L 20 140 60-140139 1 3020ND28.1 27.7
Styrene ug/L M12014260-140135 5 3020ND28.4 27.0
tert-Amyl Alcohol ug/L 400 129 60-140125 4 30400ND517498
tert-Amylmethyl ether ug/L 40 137 60-140131 4 3040ND54.7 52.5
tert-Butyl Alcohol ug/L M120018160-140187 3 30200ND362375
tert-Butyl Formate ug/L M1,R11605160-14037 33 30160ND81.2 58.5
tert-Butylbenzene ug/L 20 112 60-140112 0 3020ND22.4 22.4
Tetrachloroethene ug/L 20 134 60-140128 4 3020ND26.7 25.7
Toluene ug/L 20 132 60-140126 5 3020ND26.5 25.2
trans-1,2-Dichloroethene ug/L M12015760-140150 5 3020ND31.4 29.9
trans-1,3-Dichloropropene ug/L 20 131 60-140124 6 3020ND26.2 24.7
Trichloroethene ug/L M12014560-140136 7 3020ND29.0 27.1
Trichlorofluoromethane ug/L 20 129 60-140121 6 3020ND25.9 24.3
Vinyl chloride ug/L 20 134 60-140128 5 3020ND26.9 25.6
1,2-Dichloroethane-d4 (S)%108 70-130107
4-Bromofluorobenzene (S)%103 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92646897
MOODY GROCERY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
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Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92646897
MOODY GROCERY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92646897001 749777MW4SM 6200B
92646897002 750552MW5SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/23/2023 04:53 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 23
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
January 05, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92644184
92644184
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
MOODY'S GROCERY STATE ROAD, NC
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on December 28, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 29
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Lab ID Sample ID Matrix Date Collected Date Received
92644184001 MW#1 Water 12/28/22 11:35 12/28/22 14:12
92644184002 WSW#1 Water 12/28/22 12:10 12/28/22 14:12
92644184003 WSW#1 Water 12/28/22 12:10 12/28/22 14:12
92644184004 FB Water 12/28/22 10:40 12/28/22 14:12
92644184005 TRIP BLANK Water 12/28/22 00:00 12/28/22 14:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92644184001 MW#1 SM 6200B 69 PASI-CCL
92644184002 WSW#1 SM 6200B 69 PASI-CSAS
92644184003 WSW#1 EPA 504.1 2 PASI-CHH
92644184004 FB SM 6200B 69 PASI-CSAS
92644184005 TRIP BLANK SM 6200B 69 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:MW#1 Lab ID:92644184001 Collected:12/28/22 11:35 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol 80.1J ug/L 01/05/23 12:08 75-85-420072.8 2
tert-Amylmethyl ether <18.5 ug/L 01/05/23 12:08 994-05-820.0 18.5 2
Benzene 167 ug/L 01/05/23 12:08 71-43-21.0 0.69 2
Bromobenzene <0.58 ug/L 01/05/23 12:08 108-86-11.0 0.58 2
Bromochloromethane <0.94 ug/L 01/05/23 12:08 74-97-51.0 0.94 2
Bromodichloromethane <0.61 ug/L 01/05/23 12:08 75-27-41.0 0.61 2
Bromoform <0.68 ug/L 01/05/23 12:08 75-25-21.0 0.68 2
Bromomethane <3.3 ug/L 01/05/23 12:08 74-83-910.0 3.3 2
tert-Butyl Alcohol <53.6 ug/L 01/05/23 12:08 75-65-010053.6 2
n-Butylbenzene 1.2 ug/L 01/05/23 12:08 104-51-81.0 0.98 2
sec-Butylbenzene <0.80 ug/L 01/05/23 12:08 135-98-81.0 0.80 2
tert-Butylbenzene <0.65 ug/L 01/05/23 12:08 98-06-61.0 0.65 2
tert-Butyl Formate <58.8 ug/L 01/05/23 12:08 762-75-410058.8 2
Carbon tetrachloride <0.67 ug/L 01/05/23 12:08 56-23-51.0 0.67 2
Chlorobenzene <0.57 ug/L 01/05/23 12:08 108-90-71.0 0.57 2
Chloroethane <1.3 ug/L 01/05/23 12:08 75-00-32.0 1.3 2
Chloroform <0.86 ug/L 01/05/23 12:08 67-66-31.0 0.86 2
Chloromethane <1.1 ug/L 01/05/23 12:08 74-87-32.0 1.1 2
2-Chlorotoluene <0.64 ug/L 01/05/23 12:08 95-49-81.0 0.64 2
4-Chlorotoluene <0.65 ug/L 01/05/23 12:08 106-43-41.0 0.65 2
1,2-Dibromo-3-chloropropane <0.68 ug/L 01/05/23 12:08 96-12-82.0 0.68 2
Dibromochloromethane <0.72 ug/L 01/05/23 12:08 124-48-11.0 0.72 2
1,2-Dibromoethane (EDB)<0.54 ug/L 01/05/23 12:08 106-93-41.0 0.54 2
Dibromomethane <0.79 ug/L 01/05/23 12:08 74-95-31.0 0.79 2
1,2-Dichlorobenzene <0.68 ug/L 01/05/23 12:08 95-50-11.0 0.68 2
1,3-Dichlorobenzene <0.68 ug/L 01/05/23 12:08 541-73-11.0 0.68 2
1,4-Dichlorobenzene <0.67 ug/L 01/05/23 12:08 106-46-71.0 0.67 2
Dichlorodifluoromethane <0.69 ug/L 01/05/23 12:08 75-71-81.0 0.69 2
1,1-Dichloroethane <0.73 ug/L 01/05/23 12:08 75-34-31.0 0.73 2
1,2-Dichloroethane 8.8 ug/L 01/05/23 12:08 107-06-21.0 0.64 2
1,1-Dichloroethene <0.70 ug/L 01/05/23 12:08 75-35-41.0 0.70 2
cis-1,2-Dichloroethene <0.77 ug/L 01/05/23 12:08 156-59-21.0 0.77 2
trans-1,2-Dichloroethene <0.79 ug/L 01/05/23 12:08 156-60-51.0 0.79 2
1,2-Dichloropropane <0.71 ug/L 01/05/23 12:08 78-87-51.0 0.71 2
1,3-Dichloropropane <0.57 ug/L 01/05/23 12:08 142-28-91.0 0.57 2
2,2-Dichloropropane <0.78 ug/L 01/05/23 12:08 594-20-71.0 0.78 2
1,1-Dichloropropene <0.85 ug/L 01/05/23 12:08 563-58-61.0 0.85 2
cis-1,3-Dichloropropene <0.73 ug/L 01/05/23 12:08 10061-01-51.0 0.73 2
trans-1,3-Dichloropropene <0.73 ug/L 01/05/23 12:08 10061-02-61.0 0.73 2
Diisopropyl ether 30.5 ug/L 01/05/23 12:08 108-20-31.0 0.62 2
Ethanol <144 ug/L 01/05/23 12:08 64-17-54001442
Ethylbenzene 11.9 ug/L 01/05/23 12:08 100-41-41.0 0.61 2
Ethyl-tert-butyl ether <6.5 ug/L 01/05/23 12:08 637-92-320.0 6.5 2
Hexachloro-1,3-butadiene <3.1 ug/L 01/05/23 12:08 87-68-34.0 3.1 2
Isopropylbenzene (Cumene)1.4 ug/L 01/05/23 12:08 98-82-81.0 0.67 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:MW#1 Lab ID:92644184001 Collected:12/28/22 11:35 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <3.9 ug/L 01/05/23 12:08 75-09-24.0 3.9 2
Methyl-tert-butyl ether <0.84 ug/L 01/05/23 12:08 1634-04-41.0 0.84 2
Naphthalene 7.6 ug/L 01/05/23 12:08 91-20-34.0 1.3 2
n-Propylbenzene 1.2 ug/L 01/05/23 12:08 103-65-11.0 0.68 2
Styrene <0.58 ug/L 01/05/23 12:08 100-42-51.0 0.58 2
1,1,1,2-Tetrachloroethane <0.62 ug/L 01/05/23 12:08 630-20-61.0 0.62 2
1,1,2,2-Tetrachloroethane <0.45 ug/L 01/05/23 12:08 79-34-51.0 0.45 2
Tetrachloroethene <0.58 ug/L 01/05/23 12:08 127-18-41.0 0.58 2
Toluene 29.0 ug/L 01/05/23 12:08 108-88-31.0 0.48 2
1,2,3-Trichlorobenzene <1.6 ug/L 01/05/23 12:08 87-61-64.0 1.6 2
1,2,4-Trichlorobenzene <1.3 ug/L 01/05/23 12:08 120-82-14.0 1.3 2
1,1,1-Trichloroethane <0.66 ug/L 01/05/23 12:08 71-55-61.0 0.66 2
1,1,2-Trichloroethane <0.65 ug/L 01/05/23 12:08 79-00-51.0 0.65 2
Trichloroethene <0.77 ug/L 01/05/23 12:08 79-01-61.0 0.77 2
Trichlorofluoromethane <0.60 ug/L 01/05/23 12:08 75-69-42.0 0.60 2
1,2,3-Trichloropropane <0.52 ug/L 01/05/23 12:08 96-18-41.0 0.52 2
1,2,4-Trimethylbenzene 21.7 ug/L 01/05/23 12:08 95-63-61.0 0.99 2
1,3,5-Trimethylbenzene 9.6 ug/L 01/05/23 12:08 108-67-81.0 0.66 2
Vinyl chloride <0.77 ug/L 01/05/23 12:08 75-01-42.0 0.77 2
m&p-Xylene 59.9 ug/L 01/05/23 12:08 179601-23-12.0 1.4 2
o-Xylene 20.4 ug/L 01/05/23 12:08 95-47-61.0 0.68 2
Surrogates
1,2-Dichloroethane-d4 (S)96 %01/05/23 12:08 17060-07-0 D370-130 2
4-Bromofluorobenzene (S)95 %01/05/23 12:08 460-00-470-130 2
Toluene-d8 (S)89 %01/05/23 12:08 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:WSW#1 Lab ID:92644184002 Collected:12/28/22 12:10 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 01/04/23 00:32 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 01/04/23 00:32 994-05-810.0 9.2 1
Benzene <0.34 ug/L 01/04/23 00:32 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 01/04/23 00:32 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 01/04/23 00:32 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 01/04/23 00:32 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 01/04/23 00:32 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 01/04/23 00:32 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 01/04/23 00:32 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 01/04/23 00:32 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 01/04/23 00:32 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 01/04/23 00:32 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 01/04/23 00:32 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 01/04/23 00:32 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 01/04/23 00:32 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 01/04/23 00:32 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 01/04/23 00:32 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 01/04/23 00:32 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 01/04/23 00:32 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 01/04/23 00:32 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 01/04/23 00:32 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 01/04/23 00:32 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 01/04/23 00:32 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 01/04/23 00:32 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 01/04/23 00:32 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 01/04/23 00:32 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 01/04/23 00:32 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 01/04/23 00:32 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 01/04/23 00:32 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 01/04/23 00:32 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 01/04/23 00:32 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 01/04/23 00:32 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 01/04/23 00:32 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 01/04/23 00:32 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 01/04/23 00:32 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 01/04/23 00:32 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 01/04/23 00:32 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 01/04/23 00:32 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 01/04/23 00:32 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 01/04/23 00:32 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 01/04/23 00:32 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 01/04/23 00:32 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 01/04/23 00:32 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 01/04/23 00:32 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 01/04/23 00:32 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:WSW#1 Lab ID:92644184002 Collected:12/28/22 12:10 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 01/04/23 00:32 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 01/04/23 00:32 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 01/04/23 00:32 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 01/04/23 00:32 103-65-10.50 0.34 1
Styrene <0.29 ug/L 01/04/23 00:32 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 01/04/23 00:32 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 01/04/23 00:32 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 01/04/23 00:32 127-18-40.50 0.29 1
Toluene <0.24 ug/L 01/04/23 00:32 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 01/04/23 00:32 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 01/04/23 00:32 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 01/04/23 00:32 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 01/04/23 00:32 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 01/04/23 00:32 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 01/04/23 00:32 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 01/04/23 00:32 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 01/04/23 00:32 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 01/04/23 00:32 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 01/04/23 00:32 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 01/04/23 00:32 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 01/04/23 00:32 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)85 %01/04/23 00:32 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %01/04/23 00:32 460-00-470-130 1
Toluene-d8 (S)106 %01/04/23 00:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:WSW#1 Lab ID:92644184003 Collected:12/28/22 12:10 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.0057 ug/L 01/03/23 21:21 106-93-412/30/22 13:560.020 0.0057 1
Surrogates
1-Chloro-2-bromopropane (S)98 %01/03/23 21:21 301-79-5612/30/22 13:5670-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:FB Lab ID:92644184004 Collected:12/28/22 10:40 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 01/03/23 21:32 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 01/03/23 21:32 994-05-810.0 9.2 1
Benzene <0.34 ug/L 01/03/23 21:32 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 01/03/23 21:32 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 01/03/23 21:32 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 01/03/23 21:32 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 01/03/23 21:32 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 01/03/23 21:32 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 01/03/23 21:32 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 01/03/23 21:32 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 01/03/23 21:32 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 01/03/23 21:32 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 01/03/23 21:32 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 01/03/23 21:32 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 01/03/23 21:32 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 01/03/23 21:32 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 01/03/23 21:32 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 01/03/23 21:32 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 01/03/23 21:32 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 01/03/23 21:32 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 01/03/23 21:32 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 01/03/23 21:32 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 01/03/23 21:32 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 01/03/23 21:32 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 01/03/23 21:32 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 01/03/23 21:32 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 01/03/23 21:32 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 01/03/23 21:32 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 01/03/23 21:32 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 01/03/23 21:32 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 01/03/23 21:32 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 01/03/23 21:32 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 01/03/23 21:32 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 01/03/23 21:32 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 01/03/23 21:32 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 01/03/23 21:32 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 01/03/23 21:32 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 01/03/23 21:32 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 01/03/23 21:32 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 01/03/23 21:32 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 01/03/23 21:32 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 01/03/23 21:32 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 01/03/23 21:32 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 01/03/23 21:32 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 01/03/23 21:32 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:FB Lab ID:92644184004 Collected:12/28/22 10:40 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 01/03/23 21:32 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 01/03/23 21:32 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 01/03/23 21:32 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 01/03/23 21:32 103-65-10.50 0.34 1
Styrene <0.29 ug/L 01/03/23 21:32 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 01/03/23 21:32 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 01/03/23 21:32 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 01/03/23 21:32 127-18-40.50 0.29 1
Toluene <0.24 ug/L 01/03/23 21:32 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 01/03/23 21:32 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 01/03/23 21:32 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 01/03/23 21:32 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 01/03/23 21:32 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 01/03/23 21:32 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 01/03/23 21:32 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 01/03/23 21:32 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 01/03/23 21:32 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 01/03/23 21:32 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 01/03/23 21:32 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 01/03/23 21:32 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 01/03/23 21:32 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)84 %01/03/23 21:32 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %01/03/23 21:32 460-00-470-130 1
Toluene-d8 (S)107 %01/03/23 21:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:TRIP BLANK Lab ID:92644184005 Collected:12/28/22 00:00 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 01/03/23 21:50 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 01/03/23 21:50 994-05-810.0 9.2 1
Benzene <0.34 ug/L 01/03/23 21:50 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 01/03/23 21:50 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 01/03/23 21:50 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 01/03/23 21:50 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 01/03/23 21:50 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 01/03/23 21:50 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 01/03/23 21:50 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 01/03/23 21:50 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 01/03/23 21:50 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 01/03/23 21:50 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 01/03/23 21:50 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 01/03/23 21:50 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 01/03/23 21:50 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 01/03/23 21:50 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 01/03/23 21:50 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 01/03/23 21:50 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 01/03/23 21:50 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 01/03/23 21:50 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 01/03/23 21:50 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 01/03/23 21:50 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 01/03/23 21:50 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 01/03/23 21:50 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 01/03/23 21:50 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 01/03/23 21:50 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 01/03/23 21:50 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 01/03/23 21:50 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 01/03/23 21:50 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 01/03/23 21:50 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 01/03/23 21:50 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 01/03/23 21:50 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 01/03/23 21:50 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 01/03/23 21:50 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 01/03/23 21:50 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 01/03/23 21:50 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 01/03/23 21:50 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 01/03/23 21:50 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 01/03/23 21:50 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 01/03/23 21:50 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 01/03/23 21:50 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 01/03/23 21:50 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 01/03/23 21:50 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 01/03/23 21:50 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 01/03/23 21:50 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Sample:TRIP BLANK Lab ID:92644184005 Collected:12/28/22 00:00 Received:12/28/22 14:12 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 01/03/23 21:50 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 01/03/23 21:50 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 01/03/23 21:50 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 01/03/23 21:50 103-65-10.50 0.34 1
Styrene <0.29 ug/L 01/03/23 21:50 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 01/03/23 21:50 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 01/03/23 21:50 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 01/03/23 21:50 127-18-40.50 0.29 1
Toluene <0.24 ug/L 01/03/23 21:50 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 01/03/23 21:50 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 01/03/23 21:50 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 01/03/23 21:50 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 01/03/23 21:50 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 01/03/23 21:50 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 01/03/23 21:50 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 01/03/23 21:50 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 01/03/23 21:50 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 01/03/23 21:50 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 01/03/23 21:50 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 01/03/23 21:50 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 01/03/23 21:50 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)82 %01/03/23 21:50 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %01/03/23 21:50 460-00-470-130 1
Toluene-d8 (S)111 %01/03/23 21:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
747036
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92644184002, 92644184004, 92644184005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3884065
Associated Lab Samples:92644184002, 92644184004, 92644184005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 01/03/23 20:380.31
1,1,1-Trichloroethane ug/L <0.33 0.50 01/03/23 20:380.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 01/03/23 20:380.22
1,1,2-Trichloroethane ug/L <0.32 0.50 01/03/23 20:380.32
1,1-Dichloroethane ug/L <0.37 0.50 01/03/23 20:380.37
1,1-Dichloroethene ug/L <0.35 0.50 01/03/23 20:380.35
1,1-Dichloropropene ug/L <0.43 0.50 01/03/23 20:380.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 01/03/23 20:380.81
1,2,3-Trichloropropane ug/L <0.26 0.50 01/03/23 20:380.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 01/03/23 20:380.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/03/23 20:380.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 01/03/23 20:380.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 01/03/23 20:380.27
1,2-Dichlorobenzene ug/L <0.34 0.50 01/03/23 20:380.34
1,2-Dichloroethane ug/L <0.32 0.50 01/03/23 20:380.32
1,2-Dichloropropane ug/L <0.36 0.50 01/03/23 20:380.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 01/03/23 20:380.33
1,3-Dichlorobenzene ug/L <0.34 0.50 01/03/23 20:380.34
1,3-Dichloropropane ug/L <0.28 0.50 01/03/23 20:380.28
1,4-Dichlorobenzene ug/L <0.33 0.50 01/03/23 20:380.33
2,2-Dichloropropane ug/L <0.39 0.50 01/03/23 20:380.39
2-Chlorotoluene ug/L <0.32 0.50 01/03/23 20:380.32
4-Chlorotoluene ug/L <0.32 0.50 01/03/23 20:380.32
Benzene ug/L <0.34 0.50 01/03/23 20:380.34
Bromobenzene ug/L <0.29 0.50 01/03/23 20:380.29
Bromochloromethane ug/L <0.47 0.50 01/03/23 20:380.47
Bromodichloromethane ug/L <0.31 0.50 01/03/23 20:380.31
Bromoform ug/L <0.34 0.50 01/03/23 20:380.34
Bromomethane ug/L <1.7 5.0 01/03/23 20:381.7
Carbon tetrachloride ug/L <0.33 0.50 01/03/23 20:380.33
Chlorobenzene ug/L <0.28 0.50 01/03/23 20:380.28
Chloroethane ug/L <0.65 1.0 01/03/23 20:380.65
Chloroform ug/L <0.43 0.50 01/03/23 20:380.43
Chloromethane ug/L <0.54 1.0 01/03/23 20:380.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 01/03/23 20:380.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 01/03/23 20:380.36
Dibromochloromethane ug/L <0.36 0.50 01/03/23 20:380.36
Dibromomethane ug/L <0.39 0.50 01/03/23 20:380.39
Dichlorodifluoromethane ug/L <0.35 0.50 01/03/23 20:380.35
Diisopropyl ether ug/L <0.31 0.50 01/03/23 20:380.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3884065
Associated Lab Samples:92644184002, 92644184004, 92644184005
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 01/03/23 20:3872.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 01/03/23 20:383.2
Ethylbenzene ug/L <0.30 0.50 01/03/23 20:380.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 01/03/23 20:381.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 01/03/23 20:380.33
m&p-Xylene ug/L <0.71 1.0 01/03/23 20:380.71
Methyl-tert-butyl ether ug/L <0.42 0.50 01/03/23 20:380.42
Methylene Chloride ug/L <2.0 2.0 01/03/23 20:382.0
n-Butylbenzene ug/L <0.49 0.50 01/03/23 20:380.49
n-Propylbenzene ug/L <0.34 0.50 01/03/23 20:380.34
Naphthalene ug/L <0.64 2.0 01/03/23 20:380.64
o-Xylene ug/L <0.34 0.50 01/03/23 20:380.34
sec-Butylbenzene ug/L <0.40 0.50 01/03/23 20:380.40
Styrene ug/L <0.29 0.50 01/03/23 20:380.29
tert-Amyl Alcohol ug/L <36.4 100 01/03/23 20:3836.4
tert-Amylmethyl ether ug/L <9.2 10.0 01/03/23 20:389.2
tert-Butyl Alcohol ug/L <26.8 50.0 01/03/23 20:3826.8
tert-Butyl Formate ug/L <29.4 50.0 01/03/23 20:3829.4
tert-Butylbenzene ug/L <0.32 0.50 01/03/23 20:380.32
Tetrachloroethene ug/L <0.29 0.50 01/03/23 20:380.29
Toluene ug/L <0.24 0.50 01/03/23 20:380.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 01/03/23 20:380.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 01/03/23 20:380.36
Trichloroethene ug/L <0.38 0.50 01/03/23 20:380.38
Trichlorofluoromethane ug/L <0.30 1.0 01/03/23 20:380.30
Vinyl chloride ug/L <0.39 1.0 01/03/23 20:380.39
1,2-Dichloroethane-d4 (S)%84 70-130 01/03/23 20:38
4-Bromofluorobenzene (S)%95 70-130 01/03/23 20:38
Toluene-d8 (S)%104 70-130 01/03/23 20:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3884066LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 59.350 119 60-140
1,1,1-Trichloroethane ug/L 54.450 109 60-140
1,1,2,2-Tetrachloroethane ug/L 54.250 108 60-140
1,1,2-Trichloroethane ug/L 57.650 115 60-140
1,1-Dichloroethane ug/L 50.550 101 60-140
1,1-Dichloroethene ug/L 51.150 102 60-140
1,1-Dichloropropene ug/L 60.650 121 60-140
1,2,3-Trichlorobenzene ug/L 56.850 114 60-140
1,2,3-Trichloropropane ug/L 49.350 99 60-140
1,2,4-Trichlorobenzene ug/L 53.050 106 60-140
1,2,4-Trimethylbenzene ug/L 51.450 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3884066LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 58.750 117 60-140
1,2-Dibromoethane (EDB)ug/L 59.750 119 60-140
1,2-Dichlorobenzene ug/L 55.850 112 60-140
1,2-Dichloroethane ug/L 50.550 101 60-140
1,2-Dichloropropane ug/L 59.150 118 60-140
1,3,5-Trimethylbenzene ug/L 53.350 107 60-140
1,3-Dichlorobenzene ug/L 56.050 112 60-140
1,3-Dichloropropane ug/L 56.750 113 60-140
1,4-Dichlorobenzene ug/L 54.450 109 60-140
2,2-Dichloropropane ug/L 54.950 110 60-140
2-Chlorotoluene ug/L 56.050 112 60-140
4-Chlorotoluene ug/L 53.550 107 60-140
Benzene ug/L 52.750 105 60-140
Bromobenzene ug/L 56.450 113 60-140
Bromochloromethane ug/L 58.950 118 60-140
Bromodichloromethane ug/L 54.950 110 60-140
Bromoform ug/L 59.650 119 60-140
Bromomethane ug/L 34.450 69 60-140
Carbon tetrachloride ug/L 54.350 109 60-140
Chlorobenzene ug/L 55.050 110 60-140
Chloroethane ug/L 36.750 73 60-140
Chloroform ug/L 47.750 95 60-140
Chloromethane ug/L 55.250 110 60-140
cis-1,2-Dichloroethene ug/L 52.750 105 60-140
cis-1,3-Dichloropropene ug/L 59.350 119 60-140
Dibromochloromethane ug/L 53.750 107 60-140
Dibromomethane ug/L 63.150 126 60-140
Dichlorodifluoromethane ug/L 43.850 88 60-140
Diisopropyl ether ug/L 56.250 112 60-140
Ethanol ug/L 20802000 104 60-140
Ethyl-tert-butyl ether ug/L 103100 103 60-140
Ethylbenzene ug/L 53.050 106 60-140
Hexachloro-1,3-butadiene ug/L 53.850 108 60-140
Isopropylbenzene (Cumene)ug/L 53.750 107 60-140
m&p-Xylene ug/L 108100 108 60-140
Methyl-tert-butyl ether ug/L 48.750 97 60-140
Methylene Chloride ug/L 50.750 101 60-140
n-Butylbenzene ug/L 52.650 105 60-140
n-Propylbenzene ug/L 52.950 106 60-140
Naphthalene ug/L 54.650 109 60-140
o-Xylene ug/L 56.650 113 60-140
sec-Butylbenzene ug/L 51.450 103 60-140
Styrene ug/L 56.550 113 60-140
tert-Amyl Alcohol ug/L 10901000 109 60-140
tert-Amylmethyl ether ug/L 109100 109 60-140
tert-Butyl Alcohol ug/L 537500 107 60-140
tert-Butyl Formate ug/L 429400 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3884066LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 56.450 113 60-140
Toluene ug/L 51.050 102 60-140
trans-1,2-Dichloroethene ug/L 53.850 108 60-140
trans-1,3-Dichloropropene ug/L 56.550 113 60-140
Trichloroethene ug/L 62.950 126 60-140
Trichlorofluoromethane ug/L 41.150 82 60-140
Vinyl chloride ug/L 51.050 102 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3884067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644041001
3884068
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 60-140128 14 3020ND22.3 25.6
1,1,1-Trichloroethane ug/L 20 117 60-140122 5 3020ND23.4 24.5
1,1,2,2-Tetrachloroethane ug/L 20 104 60-140111 6 3020ND20.8 22.1
1,1,2-Trichloroethane ug/L 20 111 60-140120 7 3020ND22.3 24.0
1,1-Dichloroethane ug/L 20 106 60-140109 3 3020ND21.2 21.8
1,1-Dichloroethene ug/L 20 115 60-140121 5 3020ND23.0 24.2
1,1-Dichloropropene ug/L 20 119 60-140123 3 3020ND23.8 24.5
1,2,3-Trichlorobenzene ug/L 20 109 60-140120 9 3020ND21.9 24.1
1,2,3-Trichloropropane ug/L 20 92 60-140105 13 3020ND18.5 20.9
1,2,4-Trichlorobenzene ug/L 20 108 60-140114 6 3020ND21.5 22.9
1,2,4-Trimethylbenzene ug/L 20 109 60-140119 9 3020ND21.8 23.8
1,2-Dibromo-3-
chloropropane ug/L 20 112 60-140118 5 3020ND22.3 23.6
1,2-Dibromoethane (EDB)ug/L 20 116 60-140125 8 3020ND23.2 25.1
1,2-Dichlorobenzene ug/L 20 113 60-140124 9 3020ND22.6 24.8
1,2-Dichloroethane ug/L 20 98 60-140101 3 3020ND19.6 20.2
1,2-Dichloropropane ug/L 20 116 60-140122 5 3020ND23.2 24.5
1,3,5-Trimethylbenzene ug/L 20 111 60-140122 9 3020ND22.2 24.4
1,3-Dichlorobenzene ug/L 20 118 60-140130 9 3020ND23.6 26.0
1,3-Dichloropropane ug/L 20 103 60-140109 6 3020ND20.6 21.9
1,4-Dichlorobenzene ug/L 20 110 60-140123 11 3020ND22.1 24.6
2,2-Dichloropropane ug/L 20 113 60-140118 4 3020ND22.5 23.5
2-Chlorotoluene ug/L 20 114 60-140119 4 3020ND22.8 23.7
4-Chlorotoluene ug/L 20 108 60-140118 8 3020ND21.7 23.6
Benzene ug/L 20 109 60-140114 5 3020ND21.7 22.9
Bromobenzene ug/L 20 114 60-140125 9 3020ND22.8 25.1
Bromochloromethane ug/L 20 124 60-140133 7 3020ND24.7 26.5
Bromodichloromethane ug/L 20 109 60-140115 5 3020ND21.7 23.0
Bromoform ug/L 20 114 60-140129 12 3020ND22.8 25.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3884067MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644041001
3884068
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 80 60-14083 4 3020ND16.0 16.7
Carbon tetrachloride ug/L 20 127 60-140129 2 3020ND25.4 25.8
Chlorobenzene ug/L 20 115 60-140128 11 3020ND22.9 25.7
Chloroethane ug/L 20 87 60-14092 6 3020ND17.3 18.3
Chloroform ug/L 20 103 60-140106 3 3020ND20.9 21.6
Chloromethane ug/L 20 110 60-140113 2 3020ND22.0 22.5
cis-1,2-Dichloroethene ug/L 20 108 60-140113 5 3020ND21.6 22.7
cis-1,3-Dichloropropene ug/L 20 115 60-140119 3 3020ND23.0 23.8
Dibromochloromethane ug/L 20 101 60-140110 9 3020ND20.3 22.1
Dibromomethane ug/L 20 130 60-140140 8 3020ND25.9 28.0
Dichlorodifluoromethane ug/L 20 106 60-140111 4 3020ND21.2 22.1
Diisopropyl ether ug/L M1209560-140100 4 3020ND19.1 19.9
Ethanol ug/L M180010760-140108 1 30800ND856868
Ethyl-tert-butyl ether ug/L M1408360-14088 6 3040ND33.3 35.3
Ethylbenzene ug/L 20 109 60-140123 12 3020ND21.7 24.5
Hexachloro-1,3-butadiene ug/L 20 131 60-140128 2 3020ND26.2 25.6
Isopropylbenzene
(Cumene)ug/L 20 113 60-140128 12 3020ND22.7 25.6
m&p-Xylene ug/L 40 111 60-140124 11 3040ND44.5 49.6
Methyl-tert-butyl ether ug/L M1208260-14084 2 3020ND16.4 16.8
Methylene Chloride ug/L 20 102 60-140107 4 3020ND20.4 21.3
n-Butylbenzene ug/L 20 116 60-140123 6 3020ND23.1 24.6
n-Propylbenzene ug/L 20 111 60-140123 11 3020ND22.1 24.6
Naphthalene ug/L 20 98 60-140103 4 3020ND19.6 20.5
o-Xylene ug/L 20 119 60-140133 11 3020ND23.8 26.7
sec-Butylbenzene ug/L 20 115 60-140125 8 3020ND23.1 24.9
Styrene ug/L 20 112 60-140126 11 3020ND22.5 25.2
tert-Amyl Alcohol ug/L M140010560-140111 6 30400ND419445
tert-Amylmethyl ether ug/L M1409360-14099 7 3040ND37.1 39.7
tert-Butyl Alcohol ug/L 200 122 60-140128 5 30200ND244257
tert-Butyl Formate ug/L P51604260-14039 7 30160ND67.3 62.9
tert-Butylbenzene ug/L 20 98 60-140108 10 3020ND19.5 21.7
Tetrachloroethene ug/L 20 121 60-140130 7 3020ND24.2 26.0
Toluene ug/L 20 113 60-140119 5 3020ND22.7 23.8
trans-1,2-Dichloroethene ug/L 20 113 60-140118 4 3020ND22.6 23.6
trans-1,3-Dichloropropene ug/L 20 110 60-140114 3 3020ND22.0 22.7
Trichloroethene ug/L 20 130 60-140133 3 3020ND26.0 26.7
Trichlorofluoromethane ug/L 20 96 60-140102 6 3020ND19.2 20.3
Vinyl chloride ug/L 20 102 60-140106 5 3020ND20.3 21.3
1,2-Dichloroethane-d4 (S)%83 70-13080
4-Bromofluorobenzene (S)%94 70-13098
Toluene-d8 (S)%98 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
747491
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92644184001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3886011
Associated Lab Samples:92644184001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 01/05/23 11:500.31
1,1,1-Trichloroethane ug/L <0.33 0.50 01/05/23 11:500.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 01/05/23 11:500.22
1,1,2-Trichloroethane ug/L <0.32 0.50 01/05/23 11:500.32
1,1-Dichloroethane ug/L <0.37 0.50 01/05/23 11:500.37
1,1-Dichloroethene ug/L <0.35 0.50 01/05/23 11:500.35
1,1-Dichloropropene ug/L <0.43 0.50 01/05/23 11:500.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 01/05/23 11:500.81
1,2,3-Trichloropropane ug/L <0.26 0.50 01/05/23 11:500.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 01/05/23 11:500.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 01/05/23 11:500.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 01/05/23 11:500.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 01/05/23 11:500.27
1,2-Dichlorobenzene ug/L <0.34 0.50 01/05/23 11:500.34
1,2-Dichloroethane ug/L <0.32 0.50 01/05/23 11:500.32
1,2-Dichloropropane ug/L <0.36 0.50 01/05/23 11:500.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 01/05/23 11:500.33
1,3-Dichlorobenzene ug/L <0.34 0.50 01/05/23 11:500.34
1,3-Dichloropropane ug/L <0.28 0.50 01/05/23 11:500.28
1,4-Dichlorobenzene ug/L <0.33 0.50 01/05/23 11:500.33
2,2-Dichloropropane ug/L <0.39 0.50 01/05/23 11:500.39
2-Chlorotoluene ug/L <0.32 0.50 01/05/23 11:500.32
4-Chlorotoluene ug/L <0.32 0.50 01/05/23 11:500.32
Benzene ug/L <0.34 0.50 01/05/23 11:500.34
Bromobenzene ug/L <0.29 0.50 01/05/23 11:500.29
Bromochloromethane ug/L <0.47 0.50 01/05/23 11:500.47
Bromodichloromethane ug/L <0.31 0.50 01/05/23 11:500.31
Bromoform ug/L <0.34 0.50 01/05/23 11:500.34
Bromomethane ug/L <1.7 5.0 01/05/23 11:501.7
Carbon tetrachloride ug/L <0.33 0.50 01/05/23 11:500.33
Chlorobenzene ug/L <0.28 0.50 01/05/23 11:500.28
Chloroethane ug/L <0.65 1.0 01/05/23 11:500.65
Chloroform ug/L <0.43 0.50 01/05/23 11:500.43
Chloromethane ug/L <0.54 1.0 01/05/23 11:500.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 01/05/23 11:500.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 01/05/23 11:500.36
Dibromochloromethane ug/L <0.36 0.50 01/05/23 11:500.36
Dibromomethane ug/L <0.39 0.50 01/05/23 11:500.39
Dichlorodifluoromethane ug/L <0.35 0.50 01/05/23 11:500.35
Diisopropyl ether ug/L <0.31 0.50 01/05/23 11:500.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3886011
Associated Lab Samples:92644184001
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 01/05/23 11:5072.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 01/05/23 11:503.2
Ethylbenzene ug/L <0.30 0.50 01/05/23 11:500.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 01/05/23 11:501.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 01/05/23 11:500.33
m&p-Xylene ug/L <0.71 1.0 01/05/23 11:500.71
Methyl-tert-butyl ether ug/L <0.42 0.50 01/05/23 11:500.42
Methylene Chloride ug/L <2.0 2.0 01/05/23 11:502.0
n-Butylbenzene ug/L <0.49 0.50 01/05/23 11:500.49
n-Propylbenzene ug/L <0.34 0.50 01/05/23 11:500.34
Naphthalene ug/L <0.64 2.0 01/05/23 11:500.64
o-Xylene ug/L <0.34 0.50 01/05/23 11:500.34
sec-Butylbenzene ug/L <0.40 0.50 01/05/23 11:500.40
Styrene ug/L <0.29 0.50 01/05/23 11:500.29
tert-Amyl Alcohol ug/L <36.4 100 01/05/23 11:5036.4
tert-Amylmethyl ether ug/L <9.2 10.0 01/05/23 11:509.2
tert-Butyl Alcohol ug/L <26.8 50.0 01/05/23 11:5026.8
tert-Butyl Formate ug/L <29.4 50.0 01/05/23 11:5029.4
tert-Butylbenzene ug/L <0.32 0.50 01/05/23 11:500.32
Tetrachloroethene ug/L <0.29 0.50 01/05/23 11:500.29
Toluene ug/L <0.24 0.50 01/05/23 11:500.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 01/05/23 11:500.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 01/05/23 11:500.36
Trichloroethene ug/L <0.38 0.50 01/05/23 11:500.38
Trichlorofluoromethane ug/L <0.30 1.0 01/05/23 11:500.30
Vinyl chloride ug/L <0.39 1.0 01/05/23 11:500.39
1,2-Dichloroethane-d4 (S)%93 70-130 01/05/23 11:50
4-Bromofluorobenzene (S)%83 70-130 01/05/23 11:50
Toluene-d8 (S)%102 70-130 01/05/23 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3886012LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.250 116 60-140
1,1,1-Trichloroethane ug/L 54.050 108 60-140
1,1,2,2-Tetrachloroethane ug/L 53.450 107 60-140
1,1,2-Trichloroethane ug/L 55.250 110 60-140
1,1-Dichloroethane ug/L 47.250 94 60-140
1,1-Dichloroethene ug/L 53.550 107 60-140
1,1-Dichloropropene ug/L 58.350 117 60-140
1,2,3-Trichlorobenzene ug/L 52.150 104 60-140
1,2,3-Trichloropropane ug/L 53.550 107 60-140
1,2,4-Trichlorobenzene ug/L 52.350 105 60-140
1,2,4-Trimethylbenzene ug/L 52.350 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3886012LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 53.250 106 60-140
1,2-Dibromoethane (EDB)ug/L 55.650 111 60-140
1,2-Dichlorobenzene ug/L 52.150 104 60-140
1,2-Dichloroethane ug/L 50.250 100 60-140
1,2-Dichloropropane ug/L 52.950 106 60-140
1,3,5-Trimethylbenzene ug/L 51.950 104 60-140
1,3-Dichlorobenzene ug/L 53.550 107 60-140
1,3-Dichloropropane ug/L 52.250 104 60-140
1,4-Dichlorobenzene ug/L 51.550 103 60-140
2,2-Dichloropropane ug/L 50.650 101 60-140
2-Chlorotoluene ug/L 50.050 100 60-140
4-Chlorotoluene ug/L 48.850 98 60-140
Benzene ug/L 51.450 103 60-140
Bromobenzene ug/L 48.350 97 60-140
Bromochloromethane ug/L 53.850 108 60-140
Bromodichloromethane ug/L 53.250 106 60-140
Bromoform ug/L 52.750 105 60-140
Bromomethane ug/L 53.750 107 60-140
Carbon tetrachloride ug/L 55.350 111 60-140
Chlorobenzene ug/L 52.250 104 60-140
Chloroethane ug/L 49.050 98 60-140
Chloroform ug/L 46.850 94 60-140
Chloromethane ug/L 44.750 89 60-140
cis-1,2-Dichloroethene ug/L 47.350 95 60-140
cis-1,3-Dichloropropene ug/L 53.650 107 60-140
Dibromochloromethane ug/L 50.050 100 60-140
Dibromomethane ug/L 53.650 107 60-140
Dichlorodifluoromethane ug/L 44.350 89 60-140
Diisopropyl ether ug/L 46.550 93 60-140
Ethanol ug/L 18702000 94 60-140
Ethyl-tert-butyl ether ug/L 92.5100 93 60-140
Ethylbenzene ug/L 50.650 101 60-140
Hexachloro-1,3-butadiene ug/L 52.250 104 60-140
Isopropylbenzene (Cumene)ug/L 52.250 104 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 48.350 97 60-140
Methylene Chloride ug/L 47.850 96 60-140
n-Butylbenzene ug/L 53.250 106 60-140
n-Propylbenzene ug/L 47.050 94 60-140
Naphthalene ug/L 56.050 112 60-140
o-Xylene ug/L 56.050 112 60-140
sec-Butylbenzene ug/L 50.850 102 60-140
Styrene ug/L 58.850 118 60-140
tert-Amyl Alcohol ug/L 9241000 92 60-140
tert-Amylmethyl ether ug/L 106100 106 60-140
tert-Butyl Alcohol ug/L 436500 87 60-140
tert-Butyl Formate ug/L 398400 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3886012LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 43.550 87 60-140
Tetrachloroethene ug/L 53.050 106 60-140
Toluene ug/L 50.450 101 60-140
trans-1,2-Dichloroethene ug/L 49.650 99 60-140
trans-1,3-Dichloropropene ug/L 57.850 116 60-140
Trichloroethene ug/L 55.550 111 60-140
Trichlorofluoromethane ug/L 48.450 97 60-140
Vinyl chloride ug/L 48.350 97 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3886013MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644787002
3886014
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 110 60-140112 2 305000ND55205620
1,1,1-Trichloroethane ug/L 5000 100 60-140110 9 305000ND50205510
1,1,2,2-Tetrachloroethane ug/L 5000 102 60-140104 2 305000ND51105210
1,1,2-Trichloroethane ug/L 5000 108 60-140116 7 305000ND53905780
1,1-Dichloroethane ug/L 5000 96 60-140107 12 305000ND47805360
1,1-Dichloroethene ug/L 5000 115 60-140105 9 305000ND57305260
1,1-Dichloropropene ug/L 5000 107 60-140119 11 305000ND53505970
1,2,3-Trichlorobenzene ug/L 5000 99 60-140101 2 305000ND49605070
1,2,3-Trichloropropane ug/L 5000 98 60-140100 2 305000ND48905010
1,2,4-Trichlorobenzene ug/L 5000 98 60-14098 0 305000ND49104920
1,2,4-Trimethylbenzene ug/L 5000 106 60-140105 1 305000211074207350
1,2-Dibromo-3-
chloropropane ug/L 5000 95 60-140101 5 305000ND47605030
1,2-Dibromoethane (EDB)ug/L 5000 106 60-140109 2 305000ND53205440
1,2-Dichlorobenzene ug/L 5000 108 60-140102 6 305000ND54105110
1,2-Dichloroethane ug/L 5000 104 60-14098 6 305000ND52204910
1,2-Dichloropropane ug/L 5000 98 60-140106 8 305000ND48905320
1,3,5-Trimethylbenzene ug/L 5000 103 60-14099 3 30500052656805490
1,3-Dichlorobenzene ug/L 5000 107 60-140109 2 305000ND53505450
1,3-Dichloropropane ug/L 5000 102 60-140107 5 305000ND51005360
1,4-Dichlorobenzene ug/L 5000 103 60-140105 1 305000ND51605230
2,2-Dichloropropane ug/L 5000 95 60-140106 11 305000ND47305290
2-Chlorotoluene ug/L 5000 101 60-140100 1 305000ND50504980
4-Chlorotoluene ug/L 5000 98 60-14096 3 305000ND49204790
Benzene ug/L 5000 83 60-140119 14 30500075801170013500
Bromobenzene ug/L 5000 98 60-14098 0 305000ND49004920
Bromochloromethane ug/L 5000 100 60-140110 10 305000ND49905520
Bromodichloromethane ug/L 5000 95 60-140103 8 305000ND47305140
Bromoform ug/L 5000 88 60-14089 1 305000ND44204460
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3886013MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644787002
3886014
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 5000 112 60-140111 2 305000ND56205530
Carbon tetrachloride ug/L 5000 98 60-140119 19 305000ND48805930
Chlorobenzene ug/L 5000 106 60-140107 1 305000ND52805360
Chloroethane ug/L 5000 113 60-140109 4 305000ND56705450
Chloroform ug/L 5000 92 60-14097 5 305000ND46704910
Chloromethane ug/L 5000 95 60-14094 1 305000ND47604690
cis-1,2-Dichloroethene ug/L 5000 95 60-140107 12 305000ND47405370
cis-1,3-Dichloropropene ug/L 5000 99 60-140102 3 305000ND49405090
Dibromochloromethane ug/L 5000 95 60-14096 1 305000ND47604820
Dibromomethane ug/L 5000 99 60-140106 7 305000ND49305290
Dichlorodifluoromethane ug/L 5000 99 60-14095 4 305000ND49304740
Diisopropyl ether ug/L 5000 92 60-140103 11 30500057051605740
Ethanol ug/L 200000 90 60-14084 7 30200000ND179000167000
Ethyl-tert-butyl ether ug/L 10000 86 60-14098 13 3010000ND86009800
Ethylbenzene ug/L 5000 105 60-140105 0 305000262078607850
Hexachloro-1,3-butadiene ug/L 5000 102 60-140103 1 305000ND51105170
Isopropylbenzene
(Cumene)ug/L 5000 102 60-140102 0 305000ND51705170
m&p-Xylene ug/L 10000 108 60-140108 0 3010000124002320023100
Methyl-tert-butyl ether ug/L 5000 98 60-140103 5 30500021351205360
Methylene Chloride ug/L 5000 101 60-140103 2 305000ND50705170
n-Butylbenzene ug/L 5000 111 60-140105 5 305000ND55605270
n-Propylbenzene ug/L 5000 95 60-14094 1 30500020149704910
Naphthalene ug/L 5000 99 60-140104 4 305000455J54105640
o-Xylene ug/L 5000 115 60-140115 0 30500055401130011300
sec-Butylbenzene ug/L 5000 105 60-140104 1 305000ND52405180
Styrene ug/L 5000 108 60-140109 1 305000ND53905460
tert-Amyl Alcohol ug/L 100000 86 60-14088 1 30100000ND8650087600
tert-Amylmethyl ether ug/L 10000 93 60-140106 12 3010000ND934010600
tert-Butyl Alcohol ug/L 50000 85 60-14092 8 3050000ND4270046200
tert-Butyl Formate ug/L 40000 79 60-14089 12 3040000ND3140035400
tert-Butylbenzene ug/L 5000 89 60-14085 5 305000ND44704260
Tetrachloroethene ug/L 5000 115 60-140106 8 305000ND57605300
Toluene ug/L 5000 68 60-14080 1 305000363003970040300
trans-1,2-Dichloroethene ug/L 5000 109 60-140113 4 305000ND54405670
trans-1,3-Dichloropropene ug/L 5000 104 60-140108 4 305000ND51805380
Trichloroethene ug/L 5000 109 60-140114 4 305000ND54705720
Trichlorofluoromethane ug/L 5000 105 60-140100 4 305000ND52305010
Vinyl chloride ug/L 5000 102 60-140100 1 305000ND50905020
1,2-Dichloroethane-d4 (S)%98 70-13096
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746629
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92644184003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3882527
Associated Lab Samples:92644184003
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L <0.0056 0.020 01/03/23 19:120.0056
1-Chloro-2-bromopropane (S)%112 70-130 01/03/23 19:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3882528LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3882529
1,2-Dibromoethane (EDB)ug/L 0.250.24 101 70-1301040.27 8 20
1-Chloro-2-bromopropane (S)%97 70-13099
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3882531MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643393002
3882532
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L CL0.26 87 65-13589 2 200.26ND 0.22 0.23
1-Chloro-2-bromopropane
(S)
%H59870-130102
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92643393001
3882530SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L <0.0058 CL20ND
1-Chloro-2-bromopropane (S)%97 H5104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
low.CL
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92644184
MOODY'S GROCERY STATE ROAD, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92644184003 746629 746747WSW#1 EPA 504.1 EPA 504.1
92644184001 747491MW#1 SM 6200B
92644184002 747036WSW#1 SM 6200B
92644184004 747036FBSM 6200B
92644184005 747036TRIP BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/05/2023 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 29
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