WS-4653_15063_CA_LAB_20210407

#=CL#
April 07, 2021
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92531085
92531085
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
WILLIAMS GROCERY
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on April 02, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
cc:Al Quarles, ATC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 47
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 47
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Lab ID Sample ID Matrix Date Collected Date Received
92531085001 MW-1 Water 04/02/21 12:00 04/02/21 17:34
92531085002 MW-3 Water 04/02/21 13:15 04/02/21 17:34
92531085003 MW-5 Water 04/02/21 14:15 04/02/21 17:34
92531085004 MW-12 Water 04/02/21 11:30 04/02/21 17:34
92531085005 AS-1 Water 04/02/21 12:30 04/02/21 17:34
92531085006 TRIP BLANK Water 04/02/21 00:00 04/02/21 17:34
92531085007 WSW-1 Water 04/02/21 14:30 04/02/21 17:34
92531085008 WSW-2 Water 04/02/21 15:50 04/02/21 17:34
92531085009 WSW-6 Water 04/02/21 15:10 04/02/21 17:34
92531085010 WSW-7 Water 04/02/21 15:40 04/02/21 17:34
92531085011 FB-1 Water 04/02/21 14:30 04/02/21 17:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 47
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92531085001 MW-1 SM 6200B 70 PASI-CSAS
92531085002 MW-3 SM 6200B 70 PASI-CSAS
92531085003 MW-5 SM 6200B 70 PASI-CSAS
92531085004 MW-12 SM 6200B 70 PASI-CSAS
92531085005 AS-1 SM 6200B 70 PASI-CSAS
92531085006 TRIP BLANK SM 6200B 70 PASI-CSAS
92531085007 WSW-1 EPA 504.1 2 PASI-CBAJ
SM 6200B 70 PASI-CSAS
92531085008 WSW-2 EPA 504.1 2 PASI-CBAJ
SM 6200B 70 PASI-CSAS
92531085009 WSW-6 EPA 504.1 2 PASI-CBAJ
SM 6200B 70 PASI-CSAS
92531085010 WSW-7 EPA 504.1 2 PASI-CBAJ
SM 6200B 70 PASI-CSAS
92531085011 FB-1 EPA 504.1 2 PASI-CBAJ
SM 6200B 70 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-1 Lab ID:92531085001 Collected:04/02/21 12:00 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol 12600 ug/L 04/06/21 17:02 75-85-4125004550125
tert-Amylmethyl ether <332 ug/L 04/06/21 17:02 994-05-81250332125
Benzene 15100 ug/L 04/06/21 17:02 71-43-262.5 43.1 125
Bromobenzene <36.2 ug/L 04/06/21 17:02 108-86-162.5 36.2 125
Bromochloromethane <58.5 ug/L 04/06/21 17:02 74-97-562.5 58.5 125
Bromodichloromethane <38.4 ug/L 04/06/21 17:02 75-27-462.5 38.4 125
Bromoform <42.6 ug/L 04/06/21 17:02 75-25-262.5 42.6 125
Bromomethane <208 ug/L 04/06/21 17:02 74-83-9625208125
tert-Butyl Alcohol 16000 ug/L 04/06/21 17:02 75-65-062503350125
n-Butylbenzene <61.2 ug/L 04/06/21 17:02 104-51-862.5 61.2 125
sec-Butylbenzene <50.0 ug/L 04/06/21 17:02 135-98-862.5 50.0 125
tert-Butylbenzene <40.4 ug/L 04/06/21 17:02 98-06-662.5 40.4 125
tert-Butyl Formate <3680 ug/L 04/06/21 17:02 762-75-462503680125
Carbon tetrachloride <41.6 ug/L 04/06/21 17:02 56-23-562.5 41.6 125
Chlorobenzene <35.5 ug/L 04/06/21 17:02 108-90-762.5 35.5 125
Chloroethane <81.1 ug/L 04/06/21 17:02 75-00-312581.1 125
Chloroform <44.1 ug/L 04/06/21 17:02 67-66-362.5 44.1 125
Chloromethane <67.5 ug/L 04/06/21 17:02 74-87-312567.5 125
2-Chlorotoluene <40.1 ug/L 04/06/21 17:02 95-49-862.5 40.1 125
4-Chlorotoluene <40.5 ug/L 04/06/21 17:02 106-43-462.5 40.5 125
1,2-Dibromo-3-chloropropane <42.5 ug/L 04/06/21 17:02 96-12-812542.5 125
Dibromochloromethane <44.9 ug/L 04/06/21 17:02 124-48-162.5 44.9 125
1,2-Dibromoethane (EDB)809 ug/L 04/06/21 17:02 106-93-462.5 34.0 125
Dibromomethane <49.2 ug/L 04/06/21 17:02 74-95-362.5 49.2 125
1,2-Dichlorobenzene <42.4 ug/L 04/06/21 17:02 95-50-162.5 42.4 125
1,3-Dichlorobenzene <42.5 ug/L 04/06/21 17:02 541-73-162.5 42.5 125
1,4-Dichlorobenzene <41.6 ug/L 04/06/21 17:02 106-46-762.5 41.6 125
Dichlorodifluoromethane <43.2 ug/L 04/06/21 17:02 75-71-862.5 43.2 125
1,1-Dichloroethane <45.9 ug/L 04/06/21 17:02 75-34-362.5 45.9 125
1,2-Dichloroethane 1060 ug/L 04/06/21 17:02 107-06-262.5 40.2 125
1,1-Dichloroethene <43.5 ug/L 04/06/21 17:02 75-35-462.5 43.5 125
cis-1,2-Dichloroethene <48.0 ug/L 04/06/21 17:02 156-59-262.5 48.0 125
trans-1,2-Dichloroethene <49.5 ug/L 04/06/21 17:02 156-60-562.5 49.5 125
1,2-Dichloropropane <44.4 ug/L 04/06/21 17:02 78-87-562.5 44.4 125
1,3-Dichloropropane <35.5 ug/L 04/06/21 17:02 142-28-962.5 35.5 125
2,2-Dichloropropane <48.5 ug/L 04/06/21 17:02 594-20-762.5 48.5 125
1,1-Dichloropropene <53.4 ug/L 04/06/21 17:02 563-58-662.5 53.4 125
cis-1,3-Dichloropropene <45.6 ug/L 04/06/21 17:02 10061-01-562.5 45.6 125
trans-1,3-Dichloropropene <45.4 ug/L 04/06/21 17:02 10061-02-662.5 45.4 125
Diisopropyl ether 291 ug/L 04/06/21 17:02 108-20-362.5 38.5 125
Ethanol <9020 ug/L 04/06/21 17:02 64-17-5250009020125
Ethylbenzene 1730 ug/L 04/06/21 17:02 100-41-462.5 38.0 125
Ethyl-tert-butyl ether <405 ug/L 04/06/21 17:02 637-92-31250405125
Hexachloro-1,3-butadiene <191 ug/L 04/06/21 17:02 87-68-3250191125
Isopropylbenzene (Cumene)76.7 ug/L 04/06/21 17:02 98-82-862.5 41.6 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-1 Lab ID:92531085001 Collected:04/02/21 12:00 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <244 ug/L 04/06/21 17:02 75-09-2250244125
Methyl-tert-butyl ether 8260 ug/L 04/06/21 17:02 1634-04-462.5 52.8 125
Naphthalene 738 ug/L 04/06/21 17:02 91-20-325080.6 125
n-Propylbenzene <42.5 ug/L 04/06/21 17:02 103-65-162.5 42.5 125
Styrene 40.0J ug/L 04/06/21 17:02 100-42-562.5 36.5 125
1,1,1,2-Tetrachloroethane <38.9 ug/L 04/06/21 17:02 630-20-662.5 38.9 125
1,1,2,2-Tetrachloroethane <28.1 ug/L 04/06/21 17:02 79-34-562.5 28.1 125
Tetrachloroethene <36.5 ug/L 04/06/21 17:02 127-18-462.5 36.5 125
Toluene 21700 ug/L 04/06/21 17:02 108-88-362.5 60.6 125
1,2,3-Trichlorobenzene <101 ug/L 04/06/21 17:02 87-61-6250101125
1,2,4-Trichlorobenzene <79.9 ug/L 04/06/21 17:02 120-82-125079.9 125
1,1,1-Trichloroethane <41.5 ug/L 04/06/21 17:02 71-55-662.5 41.5 125
1,1,2-Trichloroethane <40.6 ug/L 04/06/21 17:02 79-00-562.5 40.6 125
Trichloroethene <47.9 ug/L 04/06/21 17:02 79-01-662.5 47.9 125
Trichlorofluoromethane <37.2 ug/L 04/06/21 17:02 75-69-412537.2 125
1,2,3-Trichloropropane <32.6 ug/L 04/06/21 17:02 96-18-462.5 32.6 125
1,2,4-Trimethylbenzene 2200 ug/L 04/06/21 17:02 95-63-662.5 61.9 125
1,3,5-Trimethylbenzene 658 ug/L 04/06/21 17:02 108-67-862.5 41.5 125
Vinyl chloride <48.2 ug/L 04/06/21 17:02 75-01-412548.2 125
Xylene (Total)12800 ug/L 04/06/21 17:02 1330-20-712542.2 125
m&p-Xylene 8690 ug/L 04/06/21 17:02 179601-23-112588.6 125
o-Xylene 4080 ug/L 04/06/21 17:02 95-47-662.5 42.2 125
Surrogates
1,2-Dichloroethane-d4 (S)99 %04/06/21 17:02 17060-07-070-130 125
4-Bromofluorobenzene (S)98 %04/06/21 17:02 460-00-470-130 125
Toluene-d8 (S)102 %04/06/21 17:02 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-3 Lab ID:92531085002 Collected:04/02/21 13:15 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7280 ug/L 04/06/21 17:20 75-85-4200007280200
tert-Amylmethyl ether <532 ug/L 04/06/21 17:20 994-05-82000532200
Benzene 15300 ug/L 04/06/21 17:20 71-43-210069.0 200
Bromobenzene <58.0 ug/L 04/06/21 17:20 108-86-110058.0 200
Bromochloromethane <93.6 ug/L 04/06/21 17:20 74-97-510093.6 200
Bromodichloromethane <61.4 ug/L 04/06/21 17:20 75-27-410061.4 200
Bromoform <68.2 ug/L 04/06/21 17:20 75-25-210068.2 200
Bromomethane <332 ug/L 04/06/21 17:20 74-83-91000332200
tert-Butyl Alcohol <5360 ug/L 04/06/21 17:20 75-65-0100005360200
n-Butylbenzene <98.0 ug/L 04/06/21 17:20 104-51-810098.0 200
sec-Butylbenzene <80.0 ug/L 04/06/21 17:20 135-98-810080.0 200
tert-Butylbenzene <64.6 ug/L 04/06/21 17:20 98-06-610064.6 200
tert-Butyl Formate <5880 ug/L 04/06/21 17:20 762-75-4100005880200
Carbon tetrachloride <66.6 ug/L 04/06/21 17:20 56-23-510066.6 200
Chlorobenzene <56.8 ug/L 04/06/21 17:20 108-90-710056.8 200
Chloroethane <130 ug/L 04/06/21 17:20 75-00-3200130200
Chloroform <70.6 ug/L 04/06/21 17:20 67-66-310070.6 200
Chloromethane <108 ug/L 04/06/21 17:20 74-87-3200108200
2-Chlorotoluene <64.2 ug/L 04/06/21 17:20 95-49-810064.2 200
4-Chlorotoluene <64.8 ug/L 04/06/21 17:20 106-43-410064.8 200
1,2-Dibromo-3-chloropropane <68.0 ug/L 04/06/21 17:20 96-12-820068.0 200
Dibromochloromethane <71.8 ug/L 04/06/21 17:20 124-48-110071.8 200
1,2-Dibromoethane (EDB)673 ug/L 04/06/21 17:20 106-93-410054.4 200
Dibromomethane <78.8 ug/L 04/06/21 17:20 74-95-310078.8 200
1,2-Dichlorobenzene <67.8 ug/L 04/06/21 17:20 95-50-110067.8 200
1,3-Dichlorobenzene <68.0 ug/L 04/06/21 17:20 541-73-110068.0 200
1,4-Dichlorobenzene <66.6 ug/L 04/06/21 17:20 106-46-710066.6 200
Dichlorodifluoromethane <69.2 ug/L 04/06/21 17:20 75-71-810069.2 200
1,1-Dichloroethane <73.4 ug/L 04/06/21 17:20 75-34-310073.4 200
1,2-Dichloroethane 195 ug/L 04/06/21 17:20 107-06-210064.4 200
1,1-Dichloroethene <69.6 ug/L 04/06/21 17:20 75-35-410069.6 200
cis-1,2-Dichloroethene <76.8 ug/L 04/06/21 17:20 156-59-210076.8 200
trans-1,2-Dichloroethene <79.2 ug/L 04/06/21 17:20 156-60-510079.2 200
1,2-Dichloropropane <71.0 ug/L 04/06/21 17:20 78-87-510071.0 200
1,3-Dichloropropane <56.8 ug/L 04/06/21 17:20 142-28-910056.8 200
2,2-Dichloropropane <77.6 ug/L 04/06/21 17:20 594-20-710077.6 200
1,1-Dichloropropene <85.4 ug/L 04/06/21 17:20 563-58-610085.4 200
cis-1,3-Dichloropropene <73.0 ug/L 04/06/21 17:20 10061-01-510073.0 200
trans-1,3-Dichloropropene <72.6 ug/L 04/06/21 17:20 10061-02-610072.6 200
Diisopropyl ether <61.6 ug/L 04/06/21 17:20 108-20-310061.6 200
Ethanol <14400 ug/L 04/06/21 17:20 64-17-54000014400200
Ethylbenzene 2220 ug/L 04/06/21 17:20 100-41-410060.8 200
Ethyl-tert-butyl ether <648 ug/L 04/06/21 17:20 637-92-32000648200
Hexachloro-1,3-butadiene <306 ug/L 04/06/21 17:20 87-68-3400306200
Isopropylbenzene (Cumene)106 ug/L 04/06/21 17:20 98-82-810066.6 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-3 Lab ID:92531085002 Collected:04/02/21 13:15 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <390 ug/L 04/06/21 17:20 75-09-2400390200
Methyl-tert-butyl ether <84.4 ug/L 04/06/21 17:20 1634-04-410084.4 200
Naphthalene 990 ug/L 04/06/21 17:20 91-20-3400129200
n-Propylbenzene <68.0 ug/L 04/06/21 17:20 103-65-110068.0 200
Styrene 75.4J ug/L 04/06/21 17:20 100-42-510058.4 200
1,1,1,2-Tetrachloroethane <62.2 ug/L 04/06/21 17:20 630-20-610062.2 200
1,1,2,2-Tetrachloroethane <45.0 ug/L 04/06/21 17:20 79-34-510045.0 200
Tetrachloroethene <58.4 ug/L 04/06/21 17:20 127-18-410058.4 200
Toluene 28400 ug/L 04/06/21 17:20 108-88-310097.0 200
1,2,3-Trichlorobenzene <161 ug/L 04/06/21 17:20 87-61-6400161200
1,2,4-Trichlorobenzene <128 ug/L 04/06/21 17:20 120-82-1400128200
1,1,1-Trichloroethane <66.4 ug/L 04/06/21 17:20 71-55-610066.4 200
1,1,2-Trichloroethane <65.0 ug/L 04/06/21 17:20 79-00-510065.0 200
Trichloroethene <76.6 ug/L 04/06/21 17:20 79-01-610076.6 200
Trichlorofluoromethane <59.6 ug/L 04/06/21 17:20 75-69-420059.6 200
1,2,3-Trichloropropane <52.2 ug/L 04/06/21 17:20 96-18-410052.2 200
1,2,4-Trimethylbenzene 2730 ug/L 04/06/21 17:20 95-63-610099.0 200
1,3,5-Trimethylbenzene <66.4 ug/L 04/06/21 17:20 108-67-810066.4 200
Vinyl chloride <77.2 ug/L 04/06/21 17:20 75-01-420077.2 200
Xylene (Total)15000 ug/L 04/06/21 17:20 1330-20-720067.6 200
m&p-Xylene 10100 ug/L 04/06/21 17:20 179601-23-1200142200
o-Xylene 4930 ug/L 04/06/21 17:20 95-47-610067.6 200
Surrogates
1,2-Dichloroethane-d4 (S)99 %04/06/21 17:20 17060-07-070-130 200
4-Bromofluorobenzene (S)98 %04/06/21 17:20 460-00-470-130 200
Toluene-d8 (S)100 %04/06/21 17:20 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-5 Lab ID:92531085003 Collected:04/02/21 14:15 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 04:14 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 04:14 994-05-810.0 2.7 1
Benzene 4.5 ug/L 04/06/21 04:14 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 04:14 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 04:14 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 04:14 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 04:14 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 04:14 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 04:14 75-65-050.0 26.8 1
n-Butylbenzene 0.76 ug/L 04/06/21 04:14 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 04:14 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 04:14 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 04:14 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 04:14 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 04:14 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 04:14 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 04:14 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 04:14 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 04:14 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 04:14 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 04:14 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 04:14 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 04:14 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 04:14 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 04:14 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 04:14 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 04:14 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 04:14 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 04:14 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 04:14 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 04:14 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 04:14 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 04:14 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 04:14 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 04:14 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 04:14 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 04:14 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 04:14 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 04:14 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 04/06/21 04:14 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 04:14 64-17-520072.2 1
Ethylbenzene 2.1 ug/L 04/06/21 04:14 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 04:14 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 04:14 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 04:14 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-5 Lab ID:92531085003 Collected:04/02/21 14:15 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 04/06/21 04:14 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 04:14 1634-04-40.50 0.42 1
Naphthalene 1.6J ug/L 04/06/21 04:14 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 04:14 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 04:14 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 04:14 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 04:14 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 04:14 127-18-40.50 0.29 1
Toluene 12.6 ug/L 04/06/21 04:14 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 04:14 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 04:14 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 04:14 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 04:14 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 04:14 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 04:14 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 04:14 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 9.9 ug/L 04/06/21 04:14 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 3.5 ug/L 04/06/21 04:14 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 04:14 75-01-41.0 0.39 1
Xylene (Total)17.9 ug/L 04/06/21 04:14 1330-20-71.0 0.34 1
m&p-Xylene 12.1 ug/L 04/06/21 04:14 179601-23-11.0 0.71 1
o-Xylene 5.8 ug/L 04/06/21 04:14 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %04/06/21 04:14 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %04/06/21 04:14 460-00-470-130 1
Toluene-d8 (S)101 %04/06/21 04:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-12 Lab ID:92531085004 Collected:04/02/21 11:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 03:56 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 03:56 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/06/21 03:56 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 03:56 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 03:56 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 03:56 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 03:56 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 03:56 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 03:56 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 03:56 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 03:56 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 03:56 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 03:56 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 03:56 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 03:56 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 03:56 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 03:56 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 03:56 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 03:56 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 03:56 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 03:56 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 03:56 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 03:56 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 03:56 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 03:56 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 03:56 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 03:56 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 03:56 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 03:56 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 03:56 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 03:56 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 03:56 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 03:56 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 03:56 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 03:56 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 03:56 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 03:56 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:56 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:56 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 04/06/21 03:56 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 03:56 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/06/21 03:56 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 03:56 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 03:56 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 03:56 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:MW-12 Lab ID:92531085004 Collected:04/02/21 11:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 04/06/21 03:56 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 03:56 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/06/21 03:56 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 03:56 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 03:56 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 03:56 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 03:56 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 03:56 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/06/21 03:56 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 03:56 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 03:56 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 03:56 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 03:56 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 03:56 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 03:56 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 03:56 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/06/21 03:56 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 03:56 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 03:56 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/06/21 03:56 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/06/21 03:56 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/06/21 03:56 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %04/06/21 03:56 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %04/06/21 03:56 460-00-470-130 1
Toluene-d8 (S)107 %04/06/21 03:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:AS-1 Lab ID:92531085005 Collected:04/02/21 12:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol 2070 ug/L 04/06/21 22:08 75-85-410036.4 1
tert-Amylmethyl ether 8.0J ug/L 04/06/21 22:08 994-05-810.0 2.7 1
Benzene 11.1 ug/L 04/06/21 22:08 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 22:08 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 22:08 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 22:08 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 22:08 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 22:08 74-83-95.0 1.7 1
tert-Butyl Alcohol 101 ug/L 04/06/21 22:08 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 22:08 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 22:08 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 22:08 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 22:08 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 22:08 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 22:08 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 22:08 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 22:08 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 22:08 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 22:08 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 22:08 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 22:08 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 22:08 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)0.74 ug/L 04/06/21 22:08 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 22:08 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 22:08 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 22:08 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 22:08 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 22:08 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 22:08 75-34-30.50 0.37 1
1,2-Dichloroethane 24.9 ug/L 04/06/21 22:08 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 22:08 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 22:08 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 22:08 156-60-50.50 0.40 1
1,2-Dichloropropane 0.49J ug/L 04/06/21 22:08 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 22:08 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 22:08 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 22:08 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 22:08 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 22:08 10061-02-60.50 0.36 1
Diisopropyl ether 10 ug/L 04/06/21 22:08 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 22:08 64-17-520072.2 1
Ethylbenzene 1.0 ug/L 04/06/21 22:08 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 22:08 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 22:08 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 22:08 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:AS-1 Lab ID:92531085005 Collected:04/02/21 12:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 04/06/21 22:08 75-09-22.0 2.0 1
Methyl-tert-butyl ether 24.4 ug/L 04/06/21 22:08 1634-04-40.50 0.42 1
Naphthalene 2.3 ug/L 04/06/21 22:08 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 22:08 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 22:08 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 22:08 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 22:08 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 22:08 127-18-40.50 0.29 1
Toluene 5.2 ug/L 04/06/21 22:08 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 22:08 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 22:08 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 22:08 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 22:08 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 22:08 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 22:08 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 22:08 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 1.2 ug/L 04/06/21 22:08 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 22:08 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 22:08 75-01-41.0 0.39 1
Xylene (Total)20.7 ug/L 04/06/21 22:08 1330-20-71.0 0.34 1
m&p-Xylene 4.8 ug/L 04/06/21 22:08 179601-23-11.0 0.71 1
o-Xylene 15.9 ug/L 04/06/21 22:08 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %04/06/21 22:08 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %04/06/21 22:08 460-00-470-130 1
Toluene-d8 (S)102 %04/06/21 22:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:TRIP BLANK Lab ID:92531085006 Collected:04/02/21 00:00 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/05/21 22:49 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/05/21 22:49 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/05/21 22:49 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/05/21 22:49 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/05/21 22:49 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/05/21 22:49 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/05/21 22:49 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/05/21 22:49 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/05/21 22:49 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/05/21 22:49 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/05/21 22:49 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/05/21 22:49 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/05/21 22:49 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/05/21 22:49 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/05/21 22:49 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/05/21 22:49 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/05/21 22:49 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/05/21 22:49 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/05/21 22:49 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/05/21 22:49 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/05/21 22:49 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/05/21 22:49 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/05/21 22:49 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/05/21 22:49 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/05/21 22:49 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/05/21 22:49 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/05/21 22:49 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/05/21 22:49 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/05/21 22:49 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/05/21 22:49 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/05/21 22:49 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/05/21 22:49 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/05/21 22:49 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/05/21 22:49 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/05/21 22:49 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/05/21 22:49 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/05/21 22:49 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/05/21 22:49 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/05/21 22:49 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 04/05/21 22:49 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/05/21 22:49 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/05/21 22:49 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/05/21 22:49 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/05/21 22:49 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/05/21 22:49 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 15 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:TRIP BLANK Lab ID:92531085006 Collected:04/02/21 00:00 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 04/05/21 22:49 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/05/21 22:49 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/05/21 22:49 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/05/21 22:49 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/05/21 22:49 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/05/21 22:49 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/05/21 22:49 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/05/21 22:49 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/05/21 22:49 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/05/21 22:49 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/05/21 22:49 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/05/21 22:49 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/05/21 22:49 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/05/21 22:49 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/05/21 22:49 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/05/21 22:49 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/05/21 22:49 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/05/21 22:49 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/05/21 22:49 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/05/21 22:49 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/05/21 22:49 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/05/21 22:49 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %04/05/21 22:49 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %04/05/21 22:49 460-00-470-130 1
Toluene-d8 (S)101 %04/05/21 22:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-1 Lab ID:92531085007 Collected:04/02/21 14:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.013 ug/L 04/06/21 20:14 106-93-404/06/21 09:430.020 0.013 1
Surrogates
1-Chloro-2-bromopropane (S)98 %04/06/21 20:14 301-79-5604/06/21 09:4370-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 22:26 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 22:26 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/06/21 22:26 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 22:26 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 22:26 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 22:26 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 22:26 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 22:26 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 22:26 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 22:26 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 22:26 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 22:26 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 22:26 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 22:26 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 22:26 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 22:26 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 22:26 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 22:26 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 22:26 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 22:26 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 22:26 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 22:26 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 22:26 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 22:26 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 22:26 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 22:26 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 22:26 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 22:26 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 22:26 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 22:26 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 22:26 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 22:26 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 22:26 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 22:26 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 22:26 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 22:26 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 22:26 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 22:26 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 22:26 10061-02-60.50 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-1 Lab ID:92531085007 Collected:04/02/21 14:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.31 ug/L 04/06/21 22:26 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 22:26 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/06/21 22:26 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 22:26 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 22:26 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 22:26 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 04/06/21 22:26 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 22:26 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/06/21 22:26 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 22:26 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 22:26 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 22:26 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 22:26 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 22:26 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/06/21 22:26 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 22:26 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 22:26 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 22:26 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 22:26 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 22:26 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 22:26 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 22:26 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/06/21 22:26 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 22:26 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 22:26 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/06/21 22:26 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/06/21 22:26 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/06/21 22:26 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %04/06/21 22:26 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %04/06/21 22:26 460-00-470-130 1
Toluene-d8 (S)102 %04/06/21 22:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-2 Lab ID:92531085008 Collected:04/02/21 15:50 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.013 ug/L 04/06/21 20:29 106-93-404/06/21 09:430.020 0.013 1
Surrogates
1-Chloro-2-bromopropane (S)95 %04/06/21 20:29 301-79-5604/06/21 09:4370-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 03:02 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 03:02 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/06/21 03:02 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 03:02 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 03:02 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 03:02 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 03:02 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 03:02 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 03:02 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 03:02 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 03:02 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 03:02 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 03:02 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 03:02 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 03:02 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 03:02 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 03:02 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 03:02 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 03:02 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 03:02 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 03:02 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 03:02 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 03:02 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 03:02 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 03:02 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 03:02 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 03:02 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 03:02 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 03:02 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 03:02 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 03:02 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 03:02 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 03:02 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 03:02 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 03:02 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 03:02 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 03:02 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:02 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:02 10061-02-60.50 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-2 Lab ID:92531085008 Collected:04/02/21 15:50 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.31 ug/L 04/06/21 03:02 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 03:02 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/06/21 03:02 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 03:02 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 03:02 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 03:02 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 04/06/21 03:02 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 03:02 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/06/21 03:02 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 03:02 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 03:02 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 03:02 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 03:02 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 03:02 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/06/21 03:02 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 03:02 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 03:02 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 03:02 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 03:02 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 03:02 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 03:02 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 03:02 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/06/21 03:02 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 03:02 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 03:02 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/06/21 03:02 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/06/21 03:02 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/06/21 03:02 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %04/06/21 03:02 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %04/06/21 03:02 460-00-470-130 1
Toluene-d8 (S)102 %04/06/21 03:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-6 Lab ID:92531085009 Collected:04/02/21 15:10 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.013 ug/L 04/06/21 20:44 106-93-404/06/21 09:430.020 0.013 1
Surrogates
1-Chloro-2-bromopropane (S)97 %04/06/21 20:44 301-79-5604/06/21 09:4370-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 03:20 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 03:20 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/06/21 03:20 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 03:20 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 03:20 74-97-50.50 0.47 1
Bromodichloromethane 1.0 ug/L 04/06/21 03:20 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 03:20 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 03:20 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 03:20 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 03:20 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 03:20 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 03:20 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 03:20 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 03:20 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 03:20 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 03:20 75-00-31.0 0.65 1
Chloroform 5.4 ug/L 04/06/21 03:20 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 03:20 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 03:20 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 03:20 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 03:20 96-12-81.0 0.34 1
Dibromochloromethane 0.42J ug/L 04/06/21 03:20 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 03:20 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 03:20 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 03:20 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 03:20 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 03:20 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 03:20 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 03:20 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 03:20 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 03:20 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 03:20 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 03:20 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 03:20 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 03:20 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 03:20 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 03:20 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:20 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:20 10061-02-60.50 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-6 Lab ID:92531085009 Collected:04/02/21 15:10 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.31 ug/L 04/06/21 03:20 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 03:20 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/06/21 03:20 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 03:20 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 03:20 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 03:20 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 04/06/21 03:20 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 03:20 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/06/21 03:20 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 03:20 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 03:20 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 03:20 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 03:20 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 03:20 127-18-40.50 0.29 1
Toluene 2.5 ug/L 04/06/21 03:20 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 03:20 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 03:20 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 03:20 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 03:20 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 03:20 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 03:20 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 03:20 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/06/21 03:20 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 03:20 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 03:20 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/06/21 03:20 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/06/21 03:20 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/06/21 03:20 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %04/06/21 03:20 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %04/06/21 03:20 460-00-470-130 1
Toluene-d8 (S)107 %04/06/21 03:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-7 Lab ID:92531085010 Collected:04/02/21 15:40 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.012 ug/L 04/06/21 21:00 106-93-404/06/21 09:430.019 0.012 1
Surrogates
1-Chloro-2-bromopropane (S)101 %04/06/21 21:00 301-79-5604/06/21 09:4370-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/06/21 03:38 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/06/21 03:38 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/06/21 03:38 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/06/21 03:38 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/06/21 03:38 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/06/21 03:38 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/06/21 03:38 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/06/21 03:38 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/06/21 03:38 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/06/21 03:38 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/06/21 03:38 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/06/21 03:38 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/06/21 03:38 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/06/21 03:38 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/06/21 03:38 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/06/21 03:38 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/06/21 03:38 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/06/21 03:38 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/06/21 03:38 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/06/21 03:38 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/06/21 03:38 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/06/21 03:38 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/06/21 03:38 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/06/21 03:38 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/06/21 03:38 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/06/21 03:38 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/06/21 03:38 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/06/21 03:38 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/06/21 03:38 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/06/21 03:38 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/06/21 03:38 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/06/21 03:38 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/06/21 03:38 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/06/21 03:38 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/06/21 03:38 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/06/21 03:38 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/06/21 03:38 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:38 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/06/21 03:38 10061-02-60.50 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:WSW-7 Lab ID:92531085010 Collected:04/02/21 15:40 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.31 ug/L 04/06/21 03:38 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/06/21 03:38 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/06/21 03:38 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/06/21 03:38 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/06/21 03:38 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/06/21 03:38 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 04/06/21 03:38 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/06/21 03:38 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/06/21 03:38 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/06/21 03:38 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/06/21 03:38 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/06/21 03:38 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/06/21 03:38 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/06/21 03:38 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/06/21 03:38 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/06/21 03:38 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/06/21 03:38 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/06/21 03:38 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/06/21 03:38 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/06/21 03:38 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/06/21 03:38 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/06/21 03:38 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/06/21 03:38 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/06/21 03:38 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/06/21 03:38 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/06/21 03:38 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/06/21 03:38 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/06/21 03:38 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %04/06/21 03:38 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %04/06/21 03:38 460-00-470-130 1
Toluene-d8 (S)101 %04/06/21 03:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:FB-1 Lab ID:92531085011 Collected:04/02/21 14:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.012 ug/L 04/06/21 21:15 106-93-404/06/21 09:430.019 0.012 1
Surrogates
1-Chloro-2-bromopropane (S)101 %04/06/21 21:15 301-79-5604/06/21 09:4370-130 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 04/05/21 23:07 75-85-410036.4 1
tert-Amylmethyl ether <2.7 ug/L 04/05/21 23:07 994-05-810.0 2.7 1
Benzene <0.34 ug/L 04/05/21 23:07 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 04/05/21 23:07 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 04/05/21 23:07 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 04/05/21 23:07 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 04/05/21 23:07 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 04/05/21 23:07 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 04/05/21 23:07 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 04/05/21 23:07 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 04/05/21 23:07 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 04/05/21 23:07 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 04/05/21 23:07 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 04/05/21 23:07 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 04/05/21 23:07 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 04/05/21 23:07 75-00-31.0 0.65 1
Chloroform <0.35 ug/L 04/05/21 23:07 67-66-30.50 0.35 1
Chloromethane <0.54 ug/L 04/05/21 23:07 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 04/05/21 23:07 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 04/05/21 23:07 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 04/05/21 23:07 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 04/05/21 23:07 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 04/05/21 23:07 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 04/05/21 23:07 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 04/05/21 23:07 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 04/05/21 23:07 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 04/05/21 23:07 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 04/05/21 23:07 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 04/05/21 23:07 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 04/05/21 23:07 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 04/05/21 23:07 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 04/05/21 23:07 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 04/05/21 23:07 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 04/05/21 23:07 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 04/05/21 23:07 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 04/05/21 23:07 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 04/05/21 23:07 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 04/05/21 23:07 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 04/05/21 23:07 10061-02-60.50 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Sample:FB-1 Lab ID:92531085011 Collected:04/02/21 14:30 Received:04/02/21 17:34 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Diisopropyl ether <0.31 ug/L 04/05/21 23:07 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 04/05/21 23:07 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 04/05/21 23:07 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 04/05/21 23:07 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 04/05/21 23:07 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 04/05/21 23:07 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 04/05/21 23:07 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 04/05/21 23:07 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 04/05/21 23:07 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 04/05/21 23:07 103-65-10.50 0.34 1
Styrene <0.29 ug/L 04/05/21 23:07 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 04/05/21 23:07 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 04/05/21 23:07 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 04/05/21 23:07 127-18-40.50 0.29 1
Toluene <0.48 ug/L 04/05/21 23:07 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene <0.81 ug/L 04/05/21 23:07 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 04/05/21 23:07 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 04/05/21 23:07 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 04/05/21 23:07 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 04/05/21 23:07 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 04/05/21 23:07 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 04/05/21 23:07 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 04/05/21 23:07 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 04/05/21 23:07 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 04/05/21 23:07 75-01-41.0 0.39 1
Xylene (Total)<0.34 ug/L 04/05/21 23:07 1330-20-71.0 0.34 1
m&p-Xylene <0.71 ug/L 04/05/21 23:07 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 04/05/21 23:07 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %04/05/21 23:07 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %04/05/21 23:07 460-00-470-130 1
Toluene-d8 (S)101 %04/05/21 23:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
611410
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531085003, 92531085004, 92531085006, 92531085008, 92531085009, 92531085010, 92531085011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3218870
Associated Lab Samples:92531085003, 92531085004, 92531085006, 92531085008, 92531085009, 92531085010, 92531085011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 04/05/21 22:310.31
1,1,1-Trichloroethane ug/L <0.33 0.50 04/05/21 22:310.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 04/05/21 22:310.22
1,1,2-Trichloroethane ug/L <0.32 0.50 04/05/21 22:310.32
1,1-Dichloroethane ug/L <0.37 0.50 04/05/21 22:310.37
1,1-Dichloroethene ug/L <0.35 0.50 04/05/21 22:310.35
1,1-Dichloropropene ug/L <0.43 0.50 04/05/21 22:310.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 04/05/21 22:310.81
1,2,3-Trichloropropane ug/L <0.26 0.50 04/05/21 22:310.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 04/05/21 22:310.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 04/05/21 22:310.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 04/05/21 22:310.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 04/05/21 22:310.27
1,2-Dichlorobenzene ug/L <0.34 0.50 04/05/21 22:310.34
1,2-Dichloroethane ug/L <0.32 0.50 04/05/21 22:310.32
1,2-Dichloropropane ug/L <0.36 0.50 04/05/21 22:310.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 04/05/21 22:310.33
1,3-Dichlorobenzene ug/L <0.34 0.50 04/05/21 22:310.34
1,3-Dichloropropane ug/L <0.28 0.50 04/05/21 22:310.28
1,4-Dichlorobenzene ug/L <0.33 0.50 04/05/21 22:310.33
2,2-Dichloropropane ug/L <0.39 0.50 04/05/21 22:310.39
2-Chlorotoluene ug/L <0.32 0.50 04/05/21 22:310.32
4-Chlorotoluene ug/L <0.32 0.50 04/05/21 22:310.32
Benzene ug/L <0.34 0.50 04/05/21 22:310.34
Bromobenzene ug/L <0.29 0.50 04/05/21 22:310.29
Bromochloromethane ug/L <0.47 0.50 04/05/21 22:310.47
Bromodichloromethane ug/L <0.31 0.50 04/05/21 22:310.31
Bromoform ug/L <0.34 0.50 04/05/21 22:310.34
Bromomethane ug/L <1.7 5.0 04/05/21 22:311.7
Carbon tetrachloride ug/L <0.33 0.50 04/05/21 22:310.33
Chlorobenzene ug/L <0.28 0.50 04/05/21 22:310.28
Chloroethane ug/L <0.65 1.0 04/05/21 22:310.65
Chloroform ug/L <0.35 0.50 04/05/21 22:310.35
Chloromethane ug/L <0.54 1.0 04/05/21 22:310.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 04/05/21 22:310.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 04/05/21 22:310.36
Dibromochloromethane ug/L <0.36 0.50 04/05/21 22:310.36
Dibromomethane ug/L <0.39 0.50 04/05/21 22:310.39
Dichlorodifluoromethane ug/L <0.35 0.50 04/05/21 22:310.35
Diisopropyl ether ug/L <0.31 0.50 04/05/21 22:310.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3218870
Associated Lab Samples:92531085003, 92531085004, 92531085006, 92531085008, 92531085009, 92531085010, 92531085011
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 04/05/21 22:3172.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 04/05/21 22:313.2
Ethylbenzene ug/L <0.30 0.50 04/05/21 22:310.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 04/05/21 22:311.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 04/05/21 22:310.33
m&p-Xylene ug/L <0.71 1.0 04/05/21 22:310.71
Methyl-tert-butyl ether ug/L <0.42 0.50 04/05/21 22:310.42
Methylene Chloride ug/L <2.0 2.0 04/05/21 22:312.0
n-Butylbenzene ug/L <0.49 0.50 04/05/21 22:310.49
n-Propylbenzene ug/L <0.34 0.50 04/05/21 22:310.34
Naphthalene ug/L <0.64 2.0 04/05/21 22:310.64
o-Xylene ug/L <0.34 0.50 04/05/21 22:310.34
sec-Butylbenzene ug/L <0.40 0.50 04/05/21 22:310.40
Styrene ug/L <0.29 0.50 04/05/21 22:310.29
tert-Amyl Alcohol ug/L <36.4 100 04/05/21 22:3136.4
tert-Amylmethyl ether ug/L <2.7 10.0 04/05/21 22:312.7
tert-Butyl Alcohol ug/L <26.8 50.0 04/05/21 22:3126.8
tert-Butyl Formate ug/L <29.4 50.0 04/05/21 22:3129.4
tert-Butylbenzene ug/L <0.32 0.50 04/05/21 22:310.32
Tetrachloroethene ug/L <0.29 0.50 04/05/21 22:310.29
Toluene ug/L <0.48 0.50 04/05/21 22:310.48
trans-1,2-Dichloroethene ug/L <0.40 0.50 04/05/21 22:310.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 04/05/21 22:310.36
Trichloroethene ug/L <0.38 0.50 04/05/21 22:310.38
Trichlorofluoromethane ug/L <0.30 1.0 04/05/21 22:310.30
Vinyl chloride ug/L <0.39 1.0 04/05/21 22:310.39
Xylene (Total)ug/L <0.34 1.0 04/05/21 22:310.34
1,2-Dichloroethane-d4 (S)%100 70-130 04/05/21 22:31
4-Bromofluorobenzene (S)%97 70-130 04/05/21 22:31
Toluene-d8 (S)%105 70-130 04/05/21 22:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3218871LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.950 112 60-140
1,1,1-Trichloroethane ug/L 55.150 110 60-140
1,1,2,2-Tetrachloroethane ug/L 56.150 112 60-140
1,1,2-Trichloroethane ug/L 57.050 114 60-140
1,1-Dichloroethane ug/L 55.450 111 60-140
1,1-Dichloroethene ug/L 57.050 114 60-140
1,1-Dichloropropene ug/L 54.350 109 60-140
1,2,3-Trichlorobenzene ug/L 52.250 104 60-140
1,2,3-Trichloropropane ug/L 54.350 109 60-140
1,2,4-Trichlorobenzene ug/L 51.550 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3218871LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 51.850 104 60-140
1,2-Dibromo-3-chloropropane ug/L 57.850 116 60-140
1,2-Dibromoethane (EDB)ug/L 54.950 110 60-140
1,2-Dichlorobenzene ug/L 51.450 103 60-140
1,2-Dichloroethane ug/L 50.150 100 60-140
1,2-Dichloropropane ug/L 57.350 115 60-140
1,3,5-Trimethylbenzene ug/L 52.650 105 60-140
1,3-Dichlorobenzene ug/L 52.850 106 60-140
1,3-Dichloropropane ug/L 54.850 110 60-140
1,4-Dichlorobenzene ug/L 53.450 107 60-140
2,2-Dichloropropane ug/L 55.850 112 60-140
2-Chlorotoluene ug/L 52.750 105 60-140
4-Chlorotoluene ug/L 51.250 102 60-140
Benzene ug/L 56.050 112 60-140
Bromobenzene ug/L 51.750 103 60-140
Bromochloromethane ug/L 56.650 113 60-140
Bromodichloromethane ug/L 56.950 114 60-140
Bromoform ug/L 58.550 117 60-140
Bromomethane ug/L 52.250 104 60-140
Carbon tetrachloride ug/L 57.450 115 60-140
Chlorobenzene ug/L 54.350 109 60-140
Chloroethane ug/L 44.450 89 60-140
Chloroform ug/L 48.850 98 60-140
Chloromethane ug/L 51.650 103 60-140
cis-1,2-Dichloroethene ug/L 55.650 111 60-140
cis-1,3-Dichloropropene ug/L 58.150 116 60-140
Dibromochloromethane ug/L 58.850 118 60-140
Dibromomethane ug/L 54.850 110 60-140
Dichlorodifluoromethane ug/L 46.550 93 60-140
Diisopropyl ether ug/L 51.450 103 60-140
Ethanol ug/L 20302000 101 60-140
Ethyl-tert-butyl ether ug/L 106100 106 60-140
Ethylbenzene ug/L 53.950 108 60-140
Hexachloro-1,3-butadiene ug/L 48.950 98 60-140
Isopropylbenzene (Cumene)ug/L 57.350 115 60-140
m&p-Xylene ug/L 110100 110 60-140
Methyl-tert-butyl ether ug/L 51.750 103 60-140
Methylene Chloride ug/L 52.350 105 60-140
n-Butylbenzene ug/L 51.250 102 60-140
n-Propylbenzene ug/L 50.950 102 60-140
Naphthalene ug/L 51.950 104 60-140
o-Xylene ug/L 54.850 110 60-140
sec-Butylbenzene ug/L 51.450 103 60-140
Styrene ug/L 57.650 115 60-140
tert-Amyl Alcohol ug/L 10401000 104 60-140
tert-Amylmethyl ether ug/L 106100 106 60-140
tert-Butyl Alcohol ug/L 488500 98 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3218871LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Formate ug/L 441400 110 60-140
tert-Butylbenzene ug/L 44.350 89 60-140
Tetrachloroethene ug/L 54.450 109 60-140
Toluene ug/L 54.750 109 60-140
trans-1,2-Dichloroethene ug/L 55.950 112 60-140
trans-1,3-Dichloropropene ug/L 58.950 118 60-140
Trichloroethene ug/L 54.750 109 60-140
Trichlorofluoromethane ug/L 44.650 89 60-140
Vinyl chloride ug/L 51.650 103 60-140
Xylene (Total)ug/L 165150 110 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3218872MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92530999003
3218873
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 400 109 60-140113 3 30400ND435451
1,1,1-Trichloroethane ug/L 400 114 60-140115 0 30400ND457458
1,1,2,2-Tetrachloroethane ug/L 400 113 60-140114 1 30400ND451455
1,1,2-Trichloroethane ug/L 400 103 60-140109 6 30400ND412438
1,1-Dichloroethane ug/L 400 111 60-140114 2 30400ND446455
1,1-Dichloroethene ug/L 400 115 60-140121 5 30400ND460484
1,1-Dichloropropene ug/L 400 113 60-140114 1 30400ND451456
1,2,3-Trichlorobenzene ug/L 400 96 60-140109 13 30400ND382434
1,2,3-Trichloropropane ug/L 400 116 60-140118 2 30400ND463474
1,2,4-Trichlorobenzene ug/L 400 96 60-140108 11 30400ND385431
1,2,4-Trimethylbenzene ug/L E,M14002260-140186 16 30400370037904440
1,2-Dibromo-3-
chloropropane ug/L 400 111 60-140118 7 30400ND442473
1,2-Dibromoethane (EDB)ug/L 400 106 60-140110 3 30400ND425439
1,2-Dichlorobenzene ug/L 400 103 60-140109 6 30400ND412437
1,2-Dichloroethane ug/L 400 97 60-14099 2 30400ND389395
1,2-Dichloropropane ug/L 400 113 60-140114 1 30400ND452455
1,3,5-Trimethylbenzene ug/L M140036860-140429 15 30400ND14701720
1,3-Dichlorobenzene ug/L 400 100 60-140108 7 30400ND401432
1,3-Dichloropropane ug/L 400 107 60-140110 2 30400ND429439
1,4-Dichlorobenzene ug/L 400 102 60-140109 7 30400ND408436
2,2-Dichloropropane ug/L 400 94 60-14094 0 30400ND376376
2-Chlorotoluene ug/L M140012960-140143 10 30400ND516571
4-Chlorotoluene ug/L 400 93 60-14099 6 30400ND374397
Benzene ug/L 400 108 60-140111 3 30400ND434445
Bromobenzene ug/L 400 102 60-140107 5 30400ND409429
Bromochloromethane ug/L 400 108 60-140110 2 30400ND433441
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3218872MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92530999003
3218873
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 400 106 60-140114 7 30400ND424454
Bromoform ug/L 400 109 60-140110 2 30400ND434441
Bromomethane ug/L 400 95 60-140102 7 30400ND380408
Carbon tetrachloride ug/L 400 110 60-140119 8 30400ND442477
Chlorobenzene ug/L 400 106 60-140111 5 30400ND424444
Chloroethane ug/L 400 113 60-140114 1 30400ND451454
Chloroform ug/L 400 100 60-140104 4 30400ND400415
Chloromethane ug/L 400 96 60-140100 5 30400ND384402
cis-1,2-Dichloroethene ug/L 400 112 60-140114 1 30400ND449455
cis-1,3-Dichloropropene ug/L 400 106 60-140110 4 30400ND423441
Dibromochloromethane ug/L 400 110 60-140114 4 30400ND439457
Dibromomethane ug/L 400 104 60-140109 4 30400ND418434
Dichlorodifluoromethane ug/L 400 76 60-14079 4 30400ND304316
Diisopropyl ether ug/L 400 102 60-140105 3 30400ND407421
Ethanol ug/L 16000 99 60-140102 3 3016000ND1580016300
Ethyl-tert-butyl ether ug/L 800 104 60-140106 3 30800ND829851
Ethylbenzene ug/L M14008760-140155 11 30400199023402610
Hexachloro-1,3-butadiene ug/L 400 92 60-140105 13 30400ND368421
Isopropylbenzene
(Cumene)ug/L 400 107 60-140128 10 30400360790870
m&p-Xylene ug/L 800 101 60-140131 9 30800163024402680
Methyl-tert-butyl ether ug/L 400 102 60-140102 0 30400ND408409
Methylene Chloride ug/L 400 106 60-140107 1 30400ND424428
n-Butylbenzene ug/L M140015260-140158 4 30400ND606630
n-Propylbenzene ug/L M140032660-140382 16 30400ND13001530
Naphthalene ug/L 400 88 60-140130 15 3040074511001270
o-Xylene ug/L 400 106 60-140123 8 30400444868938
sec-Butylbenzene ug/L 400 114 60-140123 8 30400ND455492
Styrene ug/L 400 111 60-140117 5 3040050.1 492 518
tert-Amyl Alcohol ug/L 8000 100 60-14099 1 308000ND79907950
tert-Amylmethyl ether ug/L 800 100 60-140102 3 30800ND799819
tert-Butyl Alcohol ug/L 4000 106 60-140106 0 304000ND42504240
tert-Butyl Formate ug/L 3200 91 60-14090 2 303200ND29302880
tert-Butylbenzene ug/L 400 89 60-14094 5 30400ND355374
Tetrachloroethene ug/L 400 108 60-140111 3 30400ND431446
Toluene ug/L 400 109 60-140109 0 30400113547547
trans-1,2-Dichloroethene ug/L 400 111 60-140114 3 30400ND444458
trans-1,3-Dichloropropene ug/L 400 103 60-140107 4 30400ND412430
Trichloroethene ug/L 400 107 60-140111 4 30400ND428445
Trichlorofluoromethane ug/L 400 103 60-140105 3 30400ND410421
Vinyl chloride ug/L 400 95 60-140102 7 30400ND379407
Xylene (Total)ug/L 1200 103 60-140129 9 301200207033003620
1,2-Dichloroethane-d4 (S)%104 70-130101
4-Bromofluorobenzene (S)%104 70-130103
Toluene-d8 (S)%98 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
611675
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531085001, 92531085002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3219796
Associated Lab Samples:92531085001, 92531085002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 04/06/21 10:430.31
1,1,1-Trichloroethane ug/L <0.33 0.50 04/06/21 10:430.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 04/06/21 10:430.22
1,1,2-Trichloroethane ug/L <0.32 0.50 04/06/21 10:430.32
1,1-Dichloroethane ug/L <0.37 0.50 04/06/21 10:430.37
1,1-Dichloroethene ug/L <0.35 0.50 04/06/21 10:430.35
1,1-Dichloropropene ug/L <0.43 0.50 04/06/21 10:430.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 04/06/21 10:430.81
1,2,3-Trichloropropane ug/L <0.26 0.50 04/06/21 10:430.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 04/06/21 10:430.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 04/06/21 10:430.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 04/06/21 10:430.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 04/06/21 10:430.27
1,2-Dichlorobenzene ug/L <0.34 0.50 04/06/21 10:430.34
1,2-Dichloroethane ug/L <0.32 0.50 04/06/21 10:430.32
1,2-Dichloropropane ug/L <0.36 0.50 04/06/21 10:430.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 04/06/21 10:430.33
1,3-Dichlorobenzene ug/L <0.34 0.50 04/06/21 10:430.34
1,3-Dichloropropane ug/L <0.28 0.50 04/06/21 10:430.28
1,4-Dichlorobenzene ug/L <0.33 0.50 04/06/21 10:430.33
2,2-Dichloropropane ug/L <0.39 0.50 04/06/21 10:430.39
2-Chlorotoluene ug/L <0.32 0.50 04/06/21 10:430.32
4-Chlorotoluene ug/L <0.32 0.50 04/06/21 10:430.32
Benzene ug/L <0.34 0.50 04/06/21 10:430.34
Bromobenzene ug/L <0.29 0.50 04/06/21 10:430.29
Bromochloromethane ug/L <0.47 0.50 04/06/21 10:430.47
Bromodichloromethane ug/L <0.31 0.50 04/06/21 10:430.31
Bromoform ug/L <0.34 0.50 04/06/21 10:430.34
Bromomethane ug/L <1.7 5.0 04/06/21 10:431.7
Carbon tetrachloride ug/L <0.33 0.50 04/06/21 10:430.33
Chlorobenzene ug/L <0.28 0.50 04/06/21 10:430.28
Chloroethane ug/L <0.65 1.0 04/06/21 10:430.65
Chloroform ug/L <0.35 0.50 04/06/21 10:430.35
Chloromethane ug/L <0.54 1.0 04/06/21 10:430.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 04/06/21 10:430.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 04/06/21 10:430.36
Dibromochloromethane ug/L <0.36 0.50 04/06/21 10:430.36
Dibromomethane ug/L <0.39 0.50 04/06/21 10:430.39
Dichlorodifluoromethane ug/L <0.35 0.50 04/06/21 10:430.35
Diisopropyl ether ug/L <0.31 0.50 04/06/21 10:430.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3219796
Associated Lab Samples:92531085001, 92531085002
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 04/06/21 10:4372.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 04/06/21 10:433.2
Ethylbenzene ug/L <0.30 0.50 04/06/21 10:430.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 04/06/21 10:431.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 04/06/21 10:430.33
m&p-Xylene ug/L <0.71 1.0 04/06/21 10:430.71
Methyl-tert-butyl ether ug/L <0.42 0.50 04/06/21 10:430.42
Methylene Chloride ug/L <2.0 2.0 04/06/21 10:432.0
n-Butylbenzene ug/L <0.49 0.50 04/06/21 10:430.49
n-Propylbenzene ug/L <0.34 0.50 04/06/21 10:430.34
Naphthalene ug/L <0.64 2.0 04/06/21 10:430.64
o-Xylene ug/L <0.34 0.50 04/06/21 10:430.34
sec-Butylbenzene ug/L <0.40 0.50 04/06/21 10:430.40
Styrene ug/L <0.29 0.50 04/06/21 10:430.29
tert-Amyl Alcohol ug/L <36.4 100 04/06/21 10:4336.4
tert-Amylmethyl ether ug/L <2.7 10.0 04/06/21 10:432.7
tert-Butyl Alcohol ug/L <26.8 50.0 04/06/21 10:4326.8
tert-Butyl Formate ug/L <29.4 50.0 04/06/21 10:4329.4
tert-Butylbenzene ug/L <0.32 0.50 04/06/21 10:430.32
Tetrachloroethene ug/L <0.29 0.50 04/06/21 10:430.29
Toluene ug/L <0.48 0.50 04/06/21 10:430.48
trans-1,2-Dichloroethene ug/L <0.40 0.50 04/06/21 10:430.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 04/06/21 10:430.36
Trichloroethene ug/L <0.38 0.50 04/06/21 10:430.38
Trichlorofluoromethane ug/L <0.30 1.0 04/06/21 10:430.30
Vinyl chloride ug/L <0.39 1.0 04/06/21 10:430.39
Xylene (Total)ug/L <0.34 1.0 04/06/21 10:430.34
1,2-Dichloroethane-d4 (S)%99 70-130 04/06/21 10:43
4-Bromofluorobenzene (S)%98 70-130 04/06/21 10:43
Toluene-d8 (S)%104 70-130 04/06/21 10:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219797LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,1-Trichloroethane ug/L 50.950 102 60-140
1,1,2,2-Tetrachloroethane ug/L 51.050 102 60-140
1,1,2-Trichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethane ug/L 51.250 102 60-140
1,1-Dichloroethene ug/L 53.950 108 60-140
1,1-Dichloropropene ug/L 51.150 102 60-140
1,2,3-Trichlorobenzene ug/L 50.450 101 60-140
1,2,3-Trichloropropane ug/L 49.450 99 60-140
1,2,4-Trichlorobenzene ug/L 50.150 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219797LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 50.850 102 60-140
1,2-Dibromo-3-chloropropane ug/L 51.750 103 60-140
1,2-Dibromoethane (EDB)ug/L 49.750 99 60-140
1,2-Dichlorobenzene ug/L 48.650 97 60-140
1,2-Dichloroethane ug/L 44.450 89 60-140
1,2-Dichloropropane ug/L 52.250 104 60-140
1,3,5-Trimethylbenzene ug/L 50.950 102 60-140
1,3-Dichlorobenzene ug/L 50.350 101 60-140
1,3-Dichloropropane ug/L 50.250 100 60-140
1,4-Dichlorobenzene ug/L 50.750 101 60-140
2,2-Dichloropropane ug/L 53.250 106 60-140
2-Chlorotoluene ug/L 50.650 101 60-140
4-Chlorotoluene ug/L 48.650 97 60-140
Benzene ug/L 50.950 102 60-140
Bromobenzene ug/L 48.950 98 60-140
Bromochloromethane ug/L 51.250 102 60-140
Bromodichloromethane ug/L 52.550 105 60-140
Bromoform ug/L 53.450 107 60-140
Bromomethane ug/L 47.350 95 60-140
Carbon tetrachloride ug/L 53.050 106 60-140
Chlorobenzene ug/L 50.850 102 60-140
Chloroethane ug/L 41.750 83 60-140
Chloroform ug/L 44.750 89 60-140
Chloromethane ug/L 48.950 98 60-140
cis-1,2-Dichloroethene ug/L 51.350 103 60-140
cis-1,3-Dichloropropene ug/L 53.950 108 60-140
Dibromochloromethane ug/L 53.550 107 60-140
Dibromomethane ug/L 50.550 101 60-140
Dichlorodifluoromethane ug/L 47.250 94 60-140
Diisopropyl ether ug/L 46.550 93 60-140
Ethanol ug/L 18402000 92 60-140
Ethyl-tert-butyl ether ug/L 96.0100 96 60-140
Ethylbenzene ug/L 50.850 102 60-140
Hexachloro-1,3-butadiene ug/L 51.150 102 60-140
Isopropylbenzene (Cumene)ug/L 54.250 108 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 46.350 93 60-140
Methylene Chloride ug/L 46.850 94 60-140
n-Butylbenzene ug/L 51.850 104 60-140
n-Propylbenzene ug/L 49.450 99 60-140
Naphthalene ug/L 49.450 99 60-140
o-Xylene ug/L 50.850 102 60-140
sec-Butylbenzene ug/L 50.150 100 60-140
Styrene ug/L 53.750 107 60-140
tert-Amyl Alcohol ug/L 9141000 91 60-140
tert-Amylmethyl ether ug/L 96.4100 96 60-140
tert-Butyl Alcohol ug/L 437500 87 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219797LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Formate ug/L 399400 100 60-140
tert-Butylbenzene ug/L 42.950 86 60-140
Tetrachloroethene ug/L 51.850 104 60-140
Toluene ug/L 50.350 101 60-140
trans-1,2-Dichloroethene ug/L 51.950 104 60-140
trans-1,3-Dichloropropene ug/L 53.550 107 60-140
Trichloroethene ug/L 50.550 101 60-140
Trichlorofluoromethane ug/L 43.250 86 60-140
Vinyl chloride ug/L 50.350 101 60-140
Xylene (Total)ug/L 155150 103 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3219798MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531085002
3219799
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 109 60-140110 1 304000<62.2 4350 4390
1,1,1-Trichloroethane ug/L 4000 110 60-140117 6 304000<66.4 4410 4670
1,1,2,2-Tetrachloroethane ug/L 4000 106 60-140105 1 304000<45.0 4230 4190
1,1,2-Trichloroethane ug/L 4000 109 60-140112 3 304000<65.0 4360 4490
1,1-Dichloroethane ug/L 4000 109 60-140112 3 304000<73.4 4380 4490
1,1-Dichloroethene ug/L 4000 119 60-140119 0 304000<69.6 4750 4760
1,1-Dichloropropene ug/L 4000 112 60-140115 3 304000<85.4 4480 4600
1,2,3-Trichlorobenzene ug/L 4000 98 60-140106 7 304000<161 3920 4220
1,2,3-Trichloropropane ug/L 4000 104 60-140101 2 304000<52.2 4150 4050
1,2,4-Trichlorobenzene ug/L 4000 98 60-140104 7 304000<128 3900 4180
1,2,4-Trimethylbenzene ug/L 4000 108 60-140110 1 304000273070407140
1,2-Dibromo-3-
chloropropane ug/L 4000 100 60-140108 8 304000<68.0 3990 4320
1,2-Dibromoethane (EDB)ug/L 4000 110 60-140109 1 30400067350805020
1,2-Dichlorobenzene ug/L 4000 103 60-140103 0 304000<67.8 4140 4120
1,2-Dichloroethane ug/L 4000 96 60-14098 2 30400019540304110
1,2-Dichloropropane ug/L 4000 113 60-140112 1 304000<71.0 4510 4470
1,3,5-Trimethylbenzene ug/L 4000 127 60-140131 3 304000<66.4 5090 5240
1,3-Dichlorobenzene ug/L 4000 105 60-140108 3 304000<68.0 4200 4330
1,3-Dichloropropane ug/L 4000 109 60-140108 1 304000<56.8 4350 4310
1,4-Dichlorobenzene ug/L 4000 107 60-140108 1 304000<66.6 4280 4340
2,2-Dichloropropane ug/L 4000 103 60-140103 0 304000<77.6 4110 4130
2-Chlorotoluene ug/L 4000 113 60-140113 0 304000<64.2 4520 4500
4-Chlorotoluene ug/L 4000 104 60-140107 3 304000<64.8 4170 4290
Benzene ug/L 4000 116 60-140100 3 304000153001990019300
Bromobenzene ug/L 4000 106 60-140109 3 304000<58.0 4250 4360
Bromochloromethane ug/L 4000 108 60-140110 2 304000<93.6 4310 4390
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3219798MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531085002
3219799
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 4000 111 60-140111 0 304000<61.4 4430 4430
Bromoform ug/L 4000 110 60-140106 3 304000<68.2 4380 4250
Bromomethane ug/L 4000 122 60-140117 4 304000<332 4860 4690
Carbon tetrachloride ug/L 4000 116 60-140117 1 304000<66.6 4630 4670
Chlorobenzene ug/L 4000 111 60-140110 1 304000<56.8 4430 4380
Chloroethane ug/L 4000 124 60-140120 3 304000<130 4970 4800
Chloroform ug/L 4000 95 60-14097 1 304000<70.6 3810 3860
Chloromethane ug/L 4000 99 60-140102 3 304000<108 3970 4100
cis-1,2-Dichloroethene ug/L 4000 110 60-140114 3 304000<76.8 4420 4570
cis-1,3-Dichloropropene ug/L 4000 110 60-140110 0 304000<73.0 4410 4400
Dibromochloromethane ug/L 4000 115 60-140113 1 304000<71.8 4580 4530
Dibromomethane ug/L 4000 108 60-140106 2 304000<78.8 4300 4230
Dichlorodifluoromethane ug/L 4000 89 60-14092 3 304000<69.2 3560 3680
Diisopropyl ether ug/L 4000 98 60-140102 4 304000<61.6 3970 4110
Ethanol ug/L 160000 91 60-14098 7 30160000<14400 146000 156000
Ethyl-tert-butyl ether ug/L 8000 101 60-140104 3 308000<648 8080 8340
Ethylbenzene ug/L 4000 109 60-140109 0 304000222066006590
Hexachloro-1,3-butadiene ug/L 4000 101 60-140105 4 304000<306 4040 4180
Isopropylbenzene
(Cumene)ug/L 4000 115 60-140115 1 30400010646904720
m&p-Xylene ug/L 8000 113 60-140110 1 308000101001910018800
Methyl-tert-butyl ether ug/L 4000 97 60-140100 3 304000<84.4 3920 4060
Methylene Chloride ug/L 4000 104 60-140105 1 304000<390 4150 4190
n-Butylbenzene ug/L 4000 105 60-140104 1 304000<98.0 4210 4170
n-Propylbenzene ug/L 4000 114 60-140116 2 304000<68.0 4550 4640
Naphthalene ug/L 4000 91 60-140101 8 30400099046505050
o-Xylene ug/L 4000 123 60-140109 6 304000493098709280
sec-Butylbenzene ug/L 4000 109 60-140111 2 304000<80.0 4350 4450
Styrene ug/L 4000 118 60-140113 4 30400075.4J 4790 4600
tert-Amyl Alcohol ug/L 80000 102 60-140109 6 3080000<7280 81800 86900
tert-Amylmethyl ether ug/L 8000 99 60-140101 2 308000<532 7880 8060
tert-Butyl Alcohol ug/L 40000 95 60-140103 8 3040000<5360 38000 41400
tert-Butyl Formate ug/L 32000 98 60-140103 5 3032000<5880 31400 33000
tert-Butylbenzene ug/L 4000 93 60-14095 3 304000<64.6 3700 3820
Tetrachloroethene ug/L 4000 109 60-140111 2 304000<58.4 4370 4440
Toluene ug/L 4000 109 60-140121 1 304000284003270033200
trans-1,2-Dichloroethene ug/L 4000 112 60-140115 3 304000<79.2 4470 4610
trans-1,3-Dichloropropene ug/L 4000 109 60-140115 5 304000<72.6 4360 4590
Trichloroethene ug/L 4000 112 60-140110 2 304000<76.6 4490 4410
Trichlorofluoromethane ug/L 4000 113 60-140112 0 304000<59.6 4500 4490
Vinyl chloride ug/L 4000 103 60-140104 2 304000<77.2 4110 4170
Xylene (Total)ug/L 12000 117 60-140109 3 3012000150002900028100
1,2-Dichloroethane-d4 (S)%98 70-130102
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%100 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
611676
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531085005, 92531085007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3219802
Associated Lab Samples:92531085005, 92531085007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 04/06/21 20:380.31
1,1,1-Trichloroethane ug/L <0.33 0.50 04/06/21 20:380.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 04/06/21 20:380.22
1,1,2-Trichloroethane ug/L <0.32 0.50 04/06/21 20:380.32
1,1-Dichloroethane ug/L <0.37 0.50 04/06/21 20:380.37
1,1-Dichloroethene ug/L <0.35 0.50 04/06/21 20:380.35
1,1-Dichloropropene ug/L <0.43 0.50 04/06/21 20:380.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 04/06/21 20:380.81
1,2,3-Trichloropropane ug/L <0.26 0.50 04/06/21 20:380.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 04/06/21 20:380.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 04/06/21 20:380.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 04/06/21 20:380.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 04/06/21 20:380.27
1,2-Dichlorobenzene ug/L <0.34 0.50 04/06/21 20:380.34
1,2-Dichloroethane ug/L <0.32 0.50 04/06/21 20:380.32
1,2-Dichloropropane ug/L <0.36 0.50 04/06/21 20:380.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 04/06/21 20:380.33
1,3-Dichlorobenzene ug/L <0.34 0.50 04/06/21 20:380.34
1,3-Dichloropropane ug/L <0.28 0.50 04/06/21 20:380.28
1,4-Dichlorobenzene ug/L <0.33 0.50 04/06/21 20:380.33
2,2-Dichloropropane ug/L <0.39 0.50 04/06/21 20:380.39
2-Chlorotoluene ug/L <0.32 0.50 04/06/21 20:380.32
4-Chlorotoluene ug/L <0.32 0.50 04/06/21 20:380.32
Benzene ug/L <0.34 0.50 04/06/21 20:380.34
Bromobenzene ug/L <0.29 0.50 04/06/21 20:380.29
Bromochloromethane ug/L <0.47 0.50 04/06/21 20:380.47
Bromodichloromethane ug/L <0.31 0.50 04/06/21 20:380.31
Bromoform ug/L <0.34 0.50 04/06/21 20:380.34
Bromomethane ug/L <1.7 5.0 04/06/21 20:381.7
Carbon tetrachloride ug/L <0.33 0.50 04/06/21 20:380.33
Chlorobenzene ug/L <0.28 0.50 04/06/21 20:380.28
Chloroethane ug/L <0.65 1.0 04/06/21 20:380.65
Chloroform ug/L <0.35 0.50 04/06/21 20:380.35
Chloromethane ug/L <0.54 1.0 04/06/21 20:380.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 04/06/21 20:380.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 04/06/21 20:380.36
Dibromochloromethane ug/L <0.36 0.50 04/06/21 20:380.36
Dibromomethane ug/L <0.39 0.50 04/06/21 20:380.39
Dichlorodifluoromethane ug/L <0.35 0.50 04/06/21 20:380.35
Diisopropyl ether ug/L <0.31 0.50 04/06/21 20:380.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3219802
Associated Lab Samples:92531085005, 92531085007
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 04/06/21 20:3872.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 04/06/21 20:383.2
Ethylbenzene ug/L <0.30 0.50 04/06/21 20:380.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 04/06/21 20:381.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 04/06/21 20:380.33
m&p-Xylene ug/L <0.71 1.0 04/06/21 20:380.71
Methyl-tert-butyl ether ug/L <0.42 0.50 04/06/21 20:380.42
Methylene Chloride ug/L <2.0 2.0 04/06/21 20:382.0
n-Butylbenzene ug/L <0.49 0.50 04/06/21 20:380.49
n-Propylbenzene ug/L <0.34 0.50 04/06/21 20:380.34
Naphthalene ug/L <0.64 2.0 04/06/21 20:380.64
o-Xylene ug/L <0.34 0.50 04/06/21 20:380.34
sec-Butylbenzene ug/L <0.40 0.50 04/06/21 20:380.40
Styrene ug/L <0.29 0.50 04/06/21 20:380.29
tert-Amyl Alcohol ug/L <36.4 100 04/06/21 20:3836.4
tert-Amylmethyl ether ug/L <2.7 10.0 04/06/21 20:382.7
tert-Butyl Alcohol ug/L <26.8 50.0 04/06/21 20:3826.8
tert-Butyl Formate ug/L <29.4 50.0 04/06/21 20:3829.4
tert-Butylbenzene ug/L <0.32 0.50 04/06/21 20:380.32
Tetrachloroethene ug/L <0.29 0.50 04/06/21 20:380.29
Toluene ug/L <0.48 0.50 04/06/21 20:380.48
trans-1,2-Dichloroethene ug/L <0.40 0.50 04/06/21 20:380.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 04/06/21 20:380.36
Trichloroethene ug/L <0.38 0.50 04/06/21 20:380.38
Trichlorofluoromethane ug/L <0.30 1.0 04/06/21 20:380.30
Vinyl chloride ug/L <0.39 1.0 04/06/21 20:380.39
Xylene (Total)ug/L <0.34 1.0 04/06/21 20:380.34
1,2-Dichloroethane-d4 (S)%96 70-130 04/06/21 20:38
4-Bromofluorobenzene (S)%97 70-130 04/06/21 20:38
Toluene-d8 (S)%107 70-130 04/06/21 20:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219803LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.950 98 60-140
1,1,1-Trichloroethane ug/L 48.550 97 60-140
1,1,2,2-Tetrachloroethane ug/L 49.150 98 60-140
1,1,2-Trichloroethane ug/L 48.650 97 60-140
1,1-Dichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethene ug/L 51.250 102 60-140
1,1-Dichloropropene ug/L 47.450 95 60-140
1,2,3-Trichlorobenzene ug/L 47.450 95 60-140
1,2,3-Trichloropropane ug/L 47.850 96 60-140
1,2,4-Trichlorobenzene ug/L 46.450 93 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
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Huntersville, NC 28078
[phone]
Page 38 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219803LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 46.950 94 60-140
1,2-Dibromo-3-chloropropane ug/L 49.950 100 60-140
1,2-Dibromoethane (EDB)ug/L 48.250 96 60-140
1,2-Dichlorobenzene ug/L 47.350 95 60-140
1,2-Dichloroethane ug/L 43.050 86 60-140
1,2-Dichloropropane ug/L 49.550 99 60-140
1,3,5-Trimethylbenzene ug/L 48.050 96 60-140
1,3-Dichlorobenzene ug/L 47.950 96 60-140
1,3-Dichloropropane ug/L 48.650 97 60-140
1,4-Dichlorobenzene ug/L 48.450 97 60-140
2,2-Dichloropropane ug/L 44.850 90 60-140
2-Chlorotoluene ug/L 48.150 96 60-140
4-Chlorotoluene ug/L 46.650 93 60-140
Benzene ug/L 49.050 98 60-140
Bromobenzene ug/L 47.150 94 60-140
Bromochloromethane ug/L 49.550 99 60-140
Bromodichloromethane ug/L 49.550 99 60-140
Bromoform ug/L 51.350 103 60-140
Bromomethane ug/L 48.350 97 60-140
Carbon tetrachloride ug/L 48.650 97 60-140
Chlorobenzene ug/L 47.950 96 60-140
Chloroethane ug/L 41.550 83 60-140
Chloroform ug/L 43.050 86 60-140
Chloromethane ug/L 47.150 94 60-140
cis-1,2-Dichloroethene ug/L 48.950 98 60-140
cis-1,3-Dichloropropene ug/L 48.450 97 60-140
Dibromochloromethane ug/L 52.350 105 60-140
Dibromomethane ug/L 47.550 95 60-140
Dichlorodifluoromethane ug/L 43.350 87 60-140
Diisopropyl ether ug/L 44.550 89 60-140
Ethanol ug/L 17902000 89 60-140
Ethyl-tert-butyl ether ug/L 93.4100 93 60-140
Ethylbenzene ug/L 47.450 95 60-140
Hexachloro-1,3-butadiene ug/L 44.550 89 60-140
Isopropylbenzene (Cumene)ug/L 50.450 101 60-140
m&p-Xylene ug/L 97.3100 97 60-140
Methyl-tert-butyl ether ug/L 44.850 90 60-140
Methylene Chloride ug/L 45.250 90 60-140
n-Butylbenzene ug/L 46.250 92 60-140
n-Propylbenzene ug/L 46.750 93 60-140
Naphthalene ug/L 48.050 96 60-140
o-Xylene ug/L 47.950 96 60-140
sec-Butylbenzene ug/L 47.150 94 60-140
Styrene ug/L 50.450 101 60-140
tert-Amyl Alcohol ug/L 8861000 89 60-140
tert-Amylmethyl ether ug/L 90.8100 91 60-140
tert-Butyl Alcohol ug/L 437500 87 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219803LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Formate ug/L 379400 95 60-140
tert-Butylbenzene ug/L 40.650 81 60-140
Tetrachloroethene ug/L 47.250 94 60-140
Toluene ug/L 47.450 95 60-140
trans-1,2-Dichloroethene ug/L 49.350 99 60-140
trans-1,3-Dichloropropene ug/L 49.350 99 60-140
Trichloroethene ug/L 47.850 96 60-140
Trichlorofluoromethane ug/L 41.850 84 60-140
Vinyl chloride ug/L 47.550 95 60-140
Xylene (Total)ug/L 145150 97 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3219804MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531231003
3219805
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 96 60-140106 10 3020ND19.2 21.1
1,1,1-Trichloroethane ug/L 20 99 60-140107 7 3020ND19.9 21.4
1,1,2,2-Tetrachloroethane ug/L 20 96 60-140105 9 3020ND19.2 21.1
1,1,2-Trichloroethane ug/L 20 93 60-140104 11 3020ND18.6 20.8
1,1-Dichloroethane ug/L 20 101 60-140105 4 3020ND20.2 21.1
1,1-Dichloroethene ug/L 20 107 60-140112 4 3020ND21.5 22.3
1,1-Dichloropropene ug/L 20 101 60-140106 5 3020ND20.2 21.2
1,2,3-Trichlorobenzene ug/L 20 105 60-140109 4 3020ND21.1 21.8
1,2,3-Trichloropropane ug/L 20 92 60-140101 10 3020ND18.3 20.3
1,2,4-Trichlorobenzene ug/L 20 104 60-140107 3 3020ND20.8 21.5
1,2,4-Trimethylbenzene ug/L 20 99 60-140108 9 3020ND19.7 21.7
1,2-Dibromo-3-
chloropropane ug/L 20 104 60-140116 11 3020ND20.8 23.3
1,2-Dibromoethane (EDB)ug/L 20 96 60-140104 8 3020ND19.1 20.8
1,2-Dichlorobenzene ug/L 20 93 60-140103 11 3020ND18.5 20.6
1,2-Dichloroethane ug/L 20 86 60-14093 8 3020ND17.3 18.6
1,2-Dichloropropane ug/L 20 98 60-140107 9 3020ND19.5 21.4
1,3,5-Trimethylbenzene ug/L 20 100 60-140110 10 3020ND19.9 22.0
1,3-Dichlorobenzene ug/L 20 94 60-140104 10 3020ND18.8 20.7
1,3-Dichloropropane ug/L 20 96 60-140106 9 3020ND19.3 21.1
1,4-Dichlorobenzene ug/L 20 95 60-140105 10 3020ND19.0 21.1
2,2-Dichloropropane ug/L 20 106 60-140111 5 3020ND21.1 22.2
2-Chlorotoluene ug/L 20 97 60-140109 11 3020ND19.5 21.8
4-Chlorotoluene ug/L 20 94 60-140103 9 3020ND18.8 20.5
Benzene ug/L 20 95 60-140105 10 3020ND19.1 21.0
Bromobenzene ug/L 20 95 60-140106 10 3020ND19.1 21.2
Bromochloromethane ug/L 20 96 60-140103 6 3020ND19.3 20.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3219804MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531231003
3219805
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 20 96 60-140107 10 3020ND19.3 21.4
Bromoform ug/L 20 97 60-140104 7 3020ND19.4 20.9
Bromomethane ug/L 20 102 60-140108 6 3020ND20.4 21.7
Carbon tetrachloride ug/L 20 101 60-140109 8 3020ND20.1 21.9
Chlorobenzene ug/L 20 96 60-140105 9 3020ND19.3 21.0
Chloroethane ug/L 20 102 60-140106 4 3020ND20.3 21.2
Chloroform ug/L 20 87 60-14092 6 3020ND17.3 18.4
Chloromethane ug/L 20 96 60-14097 1 3020ND19.2 19.5
cis-1,2-Dichloroethene ug/L 20 101 60-140108 7 3020ND20.1 21.6
cis-1,3-Dichloropropene ug/L 20 98 60-140108 9 3020ND19.7 21.5
Dibromochloromethane ug/L 20 99 60-140110 10 3020ND19.9 22.0
Dibromomethane ug/L 20 94 60-140101 7 3020ND18.8 20.3
Dichlorodifluoromethane ug/L 20 68 60-14070 2 3020ND13.6 13.9
Diisopropyl ether ug/L 20 89 60-14096 8 3020ND17.8 19.3
Ethanol ug/L 800 93 60-14098 5 30800ND748787
Ethyl-tert-butyl ether ug/L 40 93 60-14099 7 3040ND37.1 39.7
Ethylbenzene ug/L 20 97 60-140105 8 3020ND19.4 20.9
Hexachloro-1,3-butadiene ug/L 20 112 60-140117 4 3020ND22.5 23.3
Isopropylbenzene
(Cumene)ug/L 20 102 60-140110 7 3020ND20.5 22.1
m&p-Xylene ug/L 40 98 60-140107 9 3040ND39.3 42.9
Methyl-tert-butyl ether ug/L 20 89 60-14095 6 3020ND17.9 19.0
Methylene Chloride ug/L 20 94 60-140100 6 3020ND18.8 20.0
n-Butylbenzene ug/L 20 102 60-140111 8 3020ND20.4 22.1
n-Propylbenzene ug/L 20 98 60-140108 10 3020ND19.7 21.7
Naphthalene ug/L 20 101 60-140107 6 3020ND20.1 21.4
o-Xylene ug/L 20 96 60-140103 7 3020ND19.2 20.7
sec-Butylbenzene ug/L 20 100 60-140110 10 3020ND20.0 22.0
Styrene ug/L 20 95 60-140105 10 3020ND19.0 21.1
tert-Amyl Alcohol ug/L 400 87 60-14097 11 30400ND349389
tert-Amylmethyl ether ug/L 40 88 60-14097 9 3040ND35.2 38.7
tert-Butyl Alcohol ug/L 200 115 60-140130 12 30200ND230259
tert-Butyl Formate ug/L P51603260-14024 30160ND50.5 38.3J
tert-Butylbenzene ug/L 20 86 60-14095 11 3020ND17.1 19.1
Tetrachloroethene ug/L 20 101 60-140106 5 3020ND20.2 21.2
Toluene ug/L 20 93 60-140110 16 30201.6 20.1 23.6
trans-1,2-Dichloroethene ug/L 20 103 60-140109 6 3020ND20.5 21.9
trans-1,3-Dichloropropene ug/L 20 98 60-140109 10 3020ND19.6 21.8
Trichloroethene ug/L 20 95 60-140104 9 3020ND19.1 20.9
Trichlorofluoromethane ug/L 20 92 60-14098 7 3020ND18.3 19.7
Vinyl chloride ug/L 20 91 60-14095 4 3020ND18.2 19.0
Xylene (Total)ug/L 60 97 60-140106 8 3060ND58.5 63.6
1,2-Dichloroethane-d4 (S)%102 70-130101
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
611652
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531085007, 92531085008, 92531085009, 92531085010, 92531085011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3219737
Associated Lab Samples:92531085007, 92531085008, 92531085009, 92531085010, 92531085011
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L <0.013 0.020 04/06/21 16:230.013
1-Chloro-2-bromopropane (S)%91 70-130 04/06/21 16:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3219738LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3219739
1,2-Dibromoethane (EDB)ug/L 0.250.25 101 70-1301070.27 8 20
1-Chloro-2-bromopropane (S)%97 70-130100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3219741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531055002
3219742
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.25 104 65-135108 3 200.25ND 0.26 0.27
1-Chloro-2-bromopropane
(S)
%95 70-13098
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531055001
3219740SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L <0.013 20ND
1-Chloro-2-bromopropane (S)%9792
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 47
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 47
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92531085
WILLIAMS GROCERY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92531085007 611652 611816WSW-1 EPA 504.1 EPA 504.1
92531085008 611652 611816WSW-2 EPA 504.1 EPA 504.1
92531085009 611652 611816WSW-6 EPA 504.1 EPA 504.1
92531085010 611652 611816WSW-7 EPA 504.1 EPA 504.1
92531085011 611652 611816FB-1 EPA 504.1 EPA 504.1
92531085001 611675MW-1 SM 6200B
92531085002 611675MW-3 SM 6200B
92531085003 611410MW-5 SM 6200B
92531085004 611410MW-12 SM 6200B
92531085005 611676AS-1 SM 6200B
92531085006 611410TRIP BLANK SM 6200B
92531085007 611676WSW-1 SM 6200B
92531085008 611410WSW-2 SM 6200B
92531085009 611410WSW-6 SM 6200B
92531085010 611410WSW-7 SM 6200B
92531085011 611410FB-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/07/2021 01:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 47
Page 45 of 47
Page 46 of 47
Page 47 of 47