WS-4653_15063_CA_LAB_20200225

#=CL#
February 25, 2020
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92465237
92465237
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
WILLIAM'S GROCERY
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on February 14, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 56
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 56
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Lab ID Sample ID Matrix Date Collected Date Received
92465237001 MW-1 Water 02/13/20 15:02 02/14/20 08:55
92465237002 MW-2 Water 02/13/20 13:39 02/14/20 08:55
92465237003 MW-3 Water 02/13/20 14:21 02/14/20 08:55
92465237004 MW-4 Water 02/13/20 12:56 02/14/20 08:55
92465237005 MW-5 Water 02/13/20 10:37 02/14/20 08:55
92465237006 MW-6 Water 02/13/20 11:19 02/14/20 08:55
92465237007 MW-12 Water 02/13/20 09:43 02/14/20 08:55
92465237008 RW-1 Water 02/13/20 15:56 02/14/20 08:55
92465237009 WSW-1 Water 02/12/20 15:38 02/14/20 08:55
92465237010 WSW-2 Water 02/12/20 16:36 02/14/20 08:55
92465237011 WSW-5 Water 02/12/20 16:05 02/14/20 08:55
92465237012 WSW-7 Water 02/12/20 14:37 02/14/20 08:55
92465237013 WSW-9 Water 02/12/20 14:36 02/14/20 08:55
92465237014 FB-1 Water 02/12/20 16:26 02/14/20 08:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 56
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92465237001 MW-1 SM 6200B 70 PASI-CCL
92465237002 MW-2 SM 6200B 70 PASI-CCL
92465237003 MW-3 SM 6200B 70 PASI-CCL
92465237004 MW-4 SM 6200B 70 PASI-CCL
92465237005 MW-5 SM 6200B 70 PASI-CCL
92465237006 MW-6 SM 6200B 70 PASI-CCL
92465237007 MW-12 SM 6200B 70 PASI-CCL
92465237008 RW-1 SM 6200B 70 PASI-CCL
92465237009 WSW-1 EPA 504.1 2 PASI-CPKS
SM 6200B 69 PASI-CCL
92465237010 WSW-2 EPA 504.1 2 PASI-CBAJ
SM 6200B 69 PASI-CCL
92465237011 WSW-5 EPA 504.1 2 PASI-CPKS
SM 6200B 69 PASI-CCL
92465237012 WSW-7 EPA 504.1 2 PASI-CBAJ
SM 6200B 69 PASI-CCL
92465237013 WSW-9 EPA 504.1 2 PASI-CPKS
SM 6200B 69 PASI-CCL
92465237014 FB-1 SM 6200B 70 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-1 Lab ID:92465237001 Collected:02/13/20 15:02 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol 59600 ug/L 02/19/20 13:13 75-85-4200008100200
tert-Amylmethyl ether <592 ug/L 02/19/20 13:13 994-05-82000592200
Benzene 19500 ug/L 02/19/20 13:13 71-43-2 M110048.0 200
Bromobenzene <43.0 ug/L 02/19/20 13:13 108-86-110043.0 200
Bromochloromethane <51.6 ug/L 02/19/20 13:13 74-97-510051.6 200
Bromodichloromethane <37.0 ug/L 02/19/20 13:13 75-27-410037.0 200
Bromoform <81.0 ug/L 02/19/20 13:13 75-25-210081.0 200
Bromomethane <344 ug/L 02/19/20 13:13 74-83-91000344200
tert-Butyl Alcohol 286000 ug/L 02/19/20 13:13 75-65-0 M140003520200
n-Butylbenzene <70.6 ug/L 02/19/20 13:13 104-51-810070.6 200
sec-Butylbenzene <49.2 ug/L 02/19/20 13:13 135-98-810049.2 200
tert-Butylbenzene <50.0 ug/L 02/19/20 13:13 98-06-610050.0 200
tert-Butyl Formate <3560 ug/L 02/19/20 13:13 762-75-440003560200
Carbon tetrachloride <46.4 ug/L 02/19/20 13:13 56-23-510046.4 200
Chlorobenzene <45.0 ug/L 02/19/20 13:13 108-90-710045.0 200
Chloroethane <117 ug/L 02/19/20 13:13 75-00-3200117200
Chloroform <70.6 ug/L 02/19/20 13:13 67-66-310070.6 200
Chloromethane <83.0 ug/L 02/19/20 13:13 74-87-320083.0 200
2-Chlorotoluene <41.4 ug/L 02/19/20 13:13 95-49-810041.4 200
4-Chlorotoluene <41.2 ug/L 02/19/20 13:13 106-43-410041.2 200
1,2-Dibromo-3-chloropropane <77.0 ug/L 02/19/20 13:13 96-12-820077.0 200
Dibromochloromethane <80.4 ug/L 02/19/20 13:13 124-48-110080.4 200
1,2-Dibromoethane (EDB)1130 ug/L 02/19/20 13:13 106-93-410046.2 200
Dibromomethane <62.0 ug/L 02/19/20 13:13 74-95-310062.0 200
1,2-Dichlorobenzene <48.0 ug/L 02/19/20 13:13 95-50-110048.0 200
1,3-Dichlorobenzene <50.0 ug/L 02/19/20 13:13 541-73-110050.0 200
1,4-Dichlorobenzene <49.8 ug/L 02/19/20 13:13 106-46-710049.8 200
Dichlorodifluoromethane <56.8 ug/L 02/19/20 13:13 75-71-810056.8 200
1,1-Dichloroethane <48.8 ug/L 02/19/20 13:13 75-34-310048.8 200
1,2-Dichloroethane 2280 ug/L 02/19/20 13:13 107-06-210052.6 200
1,1-Dichloroethene <43.6 ug/L 02/19/20 13:13 75-35-410043.6 200
cis-1,2-Dichloroethene <41.4 ug/L 02/19/20 13:13 156-59-210041.4 200
trans-1,2-Dichloroethene <51.4 ug/L 02/19/20 13:13 156-60-510051.4 200
1,2-Dichloropropane <36.6 ug/L 02/19/20 13:13 78-87-510036.6 200
1,3-Dichloropropane <68.2 ug/L 02/19/20 13:13 142-28-910068.2 200
2,2-Dichloropropane <56.2 ug/L 02/19/20 13:13 594-20-710056.2 200
1,1-Dichloropropene <69.6 ug/L 02/19/20 13:13 563-58-610069.6 200
cis-1,3-Dichloropropene <71.4 ug/L 02/19/20 13:13 10061-01-510071.4 200
trans-1,3-Dichloropropene <78.8 ug/L 02/19/20 13:13 10061-02-610078.8 200
Diisopropyl ether 590 ug/L 02/19/20 13:13 108-20-310066.8 200
Ethanol <19800 ug/L 02/19/20 13:13 64-17-54000019800200
Ethylbenzene 2000 ug/L 02/19/20 13:13 100-41-410048.0 200
Ethyl-tert-butyl ether <762 ug/L 02/19/20 13:13 637-92-32000762200
Hexachloro-1,3-butadiene <240 ug/L 02/19/20 13:13 87-68-3400240200
Isopropylbenzene (Cumene)<47.6 ug/L 02/19/20 13:13 98-82-810047.6 200
Methylene Chloride <300 ug/L 02/19/20 13:13 75-09-2400300200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-1 Lab ID:92465237001 Collected:02/13/20 15:02 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether 36500 ug/L 02/19/20 13:13 1634-04-4 M110088.8 200
Naphthalene 710 ug/L 02/19/20 13:13 91-20-3400132200
n-Propylbenzene 167 ug/L 02/19/20 13:13 103-65-110048.2 200
Styrene <51.2 ug/L 02/19/20 13:13 100-42-510051.2 200
1,1,1,2-Tetrachloroethane <84.4 ug/L 02/19/20 13:13 630-20-610084.4 200
1,1,2,2-Tetrachloroethane <38.6 ug/L 02/19/20 13:13 79-34-510038.6 200
Tetrachloroethene <46.4 ug/L 02/19/20 13:13 127-18-410046.4 200
Toluene 26400 ug/L 02/19/20 13:13 108-88-3 M110045.6 200
1,2,3-Trichlorobenzene <156 ug/L 02/19/20 13:13 87-61-6400156200
1,2,4-Trichlorobenzene <87.2 ug/L 02/19/20 13:13 120-82-140087.2 200
1,1,1-Trichloroethane <55.6 ug/L 02/19/20 13:13 71-55-610055.6 200
1,1,2-Trichloroethane <46.4 ug/L 02/19/20 13:13 79-00-510046.4 200
Trichloroethene <46.4 ug/L 02/19/20 13:13 79-01-610046.4 200
Trichlorofluoromethane <67.2 ug/L 02/19/20 13:13 75-69-420067.2 200
1,2,3-Trichloropropane <54.2 ug/L 02/19/20 13:13 96-18-410054.2 200
1,2,4-Trimethylbenzene 2260 ug/L 02/19/20 13:13 95-63-610038.6 200
1,3,5-Trimethylbenzene 558 ug/L 02/19/20 13:13 108-67-810045.4 200
Vinyl chloride <81.4 ug/L 02/19/20 13:13 75-01-420081.4 200
Xylene (Total)15300 ug/L 02/19/20 13:13 1330-20-7200100200
m&p-Xylene 10600 ug/L 02/19/20 13:13 179601-23-120088.2 200
o-Xylene 4730 ug/L 02/19/20 13:13 95-47-610047.4 200
Surrogates
1,2-Dichloroethane-d4 (S)107 %02/19/20 13:13 17060-07-070-130 200
4-Bromofluorobenzene (S)100 %02/19/20 13:13 460-00-470-130 200
Toluene-d8 (S)100 %02/19/20 13:13 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-2 Lab ID:92465237002 Collected:02/13/20 13:39 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <202 ug/L 02/19/20 12:55 75-85-45002025
tert-Amylmethyl ether <14.8 ug/L 02/19/20 12:55 994-05-850.0 14.8 5
Benzene 16.1 ug/L 02/19/20 12:55 71-43-22.5 1.2 5
Bromobenzene <1.1 ug/L 02/19/20 12:55 108-86-12.5 1.1 5
Bromochloromethane <1.3 ug/L 02/19/20 12:55 74-97-52.5 1.3 5
Bromodichloromethane <0.92 ug/L 02/19/20 12:55 75-27-42.5 0.92 5
Bromoform <2.0 ug/L 02/19/20 12:55 75-25-22.5 2.0 5
Bromomethane <8.6 ug/L 02/19/20 12:55 74-83-925.0 8.6 5
tert-Butyl Alcohol <88.0 ug/L 02/19/20 12:55 75-65-010088.0 5
n-Butylbenzene <1.8 ug/L 02/19/20 12:55 104-51-82.5 1.8 5
sec-Butylbenzene <1.2 ug/L 02/19/20 12:55 135-98-82.5 1.2 5
tert-Butylbenzene <1.2 ug/L 02/19/20 12:55 98-06-62.5 1.2 5
tert-Butyl Formate <89.0 ug/L 02/19/20 12:55 762-75-410089.0 5
Carbon tetrachloride <1.2 ug/L 02/19/20 12:55 56-23-52.5 1.2 5
Chlorobenzene <1.1 ug/L 02/19/20 12:55 108-90-72.5 1.1 5
Chloroethane <2.9 ug/L 02/19/20 12:55 75-00-35.0 2.9 5
Chloroform <1.8 ug/L 02/19/20 12:55 67-66-32.5 1.8 5
Chloromethane <2.1 ug/L 02/19/20 12:55 74-87-35.0 2.1 5
2-Chlorotoluene <1.0 ug/L 02/19/20 12:55 95-49-82.5 1.0 5
4-Chlorotoluene <1.0 ug/L 02/19/20 12:55 106-43-42.5 1.0 5
1,2-Dibromo-3-chloropropane <1.9 ug/L 02/19/20 12:55 96-12-85.0 1.9 5
Dibromochloromethane <2.0 ug/L 02/19/20 12:55 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)<1.2 ug/L 02/19/20 12:55 106-93-42.5 1.2 5
Dibromomethane <1.6 ug/L 02/19/20 12:55 74-95-32.5 1.6 5
1,2-Dichlorobenzene <1.2 ug/L 02/19/20 12:55 95-50-12.5 1.2 5
1,3-Dichlorobenzene <1.2 ug/L 02/19/20 12:55 541-73-12.5 1.2 5
1,4-Dichlorobenzene <1.2 ug/L 02/19/20 12:55 106-46-72.5 1.2 5
Dichlorodifluoromethane <1.4 ug/L 02/19/20 12:55 75-71-82.5 1.4 5
1,1-Dichloroethane <1.2 ug/L 02/19/20 12:55 75-34-32.5 1.2 5
1,2-Dichloroethane <1.3 ug/L 02/19/20 12:55 107-06-22.5 1.3 5
1,1-Dichloroethene <1.1 ug/L 02/19/20 12:55 75-35-42.5 1.1 5
cis-1,2-Dichloroethene <1.0 ug/L 02/19/20 12:55 156-59-22.5 1.0 5
trans-1,2-Dichloroethene <1.3 ug/L 02/19/20 12:55 156-60-52.5 1.3 5
1,2-Dichloropropane <0.92 ug/L 02/19/20 12:55 78-87-52.5 0.92 5
1,3-Dichloropropane <1.7 ug/L 02/19/20 12:55 142-28-92.5 1.7 5
2,2-Dichloropropane <1.4 ug/L 02/19/20 12:55 594-20-72.5 1.4 5
1,1-Dichloropropene <1.7 ug/L 02/19/20 12:55 563-58-62.5 1.7 5
cis-1,3-Dichloropropene <1.8 ug/L 02/19/20 12:55 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene <2.0 ug/L 02/19/20 12:55 10061-02-62.5 2.0 5
Diisopropyl ether <1.7 ug/L 02/19/20 12:55 108-20-32.5 1.7 5
Ethanol <494 ug/L 02/19/20 12:55 64-17-510004945
Ethylbenzene 77.9 ug/L 02/19/20 12:55 100-41-42.5 1.2 5
Ethyl-tert-butyl ether <19.0 ug/L 02/19/20 12:55 637-92-350.0 19.0 5
Hexachloro-1,3-butadiene <6.0 ug/L 02/19/20 12:55 87-68-310.0 6.0 5
Isopropylbenzene (Cumene)<1.2 ug/L 02/19/20 12:55 98-82-82.5 1.2 5
Methylene Chloride <7.5 ug/L 02/19/20 12:55 75-09-210.0 7.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-2 Lab ID:92465237002 Collected:02/13/20 13:39 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether <2.2 ug/L 02/19/20 12:55 1634-04-42.5 2.2 5
Naphthalene 18.1 ug/L 02/19/20 12:55 91-20-310.0 3.3 5
n-Propylbenzene <1.2 ug/L 02/19/20 12:55 103-65-12.5 1.2 5
Styrene 2.6 ug/L 02/19/20 12:55 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane <2.1 ug/L 02/19/20 12:55 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane <0.96 ug/L 02/19/20 12:55 79-34-52.5 0.96 5
Tetrachloroethene <1.2 ug/L 02/19/20 12:55 127-18-42.5 1.2 5
Toluene 490 ug/L 02/19/20 12:55 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene <3.9 ug/L 02/19/20 12:55 87-61-610.0 3.9 5
1,2,4-Trichlorobenzene <2.2 ug/L 02/19/20 12:55 120-82-110.0 2.2 5
1,1,1-Trichloroethane <1.4 ug/L 02/19/20 12:55 71-55-62.5 1.4 5
1,1,2-Trichloroethane <1.2 ug/L 02/19/20 12:55 79-00-52.5 1.2 5
Trichloroethene <1.2 ug/L 02/19/20 12:55 79-01-62.5 1.2 5
Trichlorofluoromethane <1.7 ug/L 02/19/20 12:55 75-69-45.0 1.7 5
1,2,3-Trichloropropane <1.4 ug/L 02/19/20 12:55 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 46.2 ug/L 02/19/20 12:55 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene <1.1 ug/L 02/19/20 12:55 108-67-82.5 1.1 5
Vinyl chloride <2.0 ug/L 02/19/20 12:55 75-01-45.0 2.0 5
Xylene (Total)380 ug/L 02/19/20 12:55 1330-20-75.0 2.5 5
m&p-Xylene 266 ug/L 02/19/20 12:55 179601-23-15.0 2.2 5
o-Xylene 114 ug/L 02/19/20 12:55 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)100 %02/19/20 12:55 17060-07-070-130 5
4-Bromofluorobenzene (S)99 %02/19/20 12:55 460-00-470-130 5
Toluene-d8 (S)103 %02/19/20 12:55 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-3 Lab ID:92465237003 Collected:02/13/20 14:21 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <10100 ug/L 02/19/20 21:25 75-85-42500010100250
tert-Amylmethyl ether <740 ug/L 02/19/20 21:25 994-05-82500740250
Benzene 14200 ug/L 02/19/20 21:25 71-43-212560.0 250
Bromobenzene <53.8 ug/L 02/19/20 21:25 108-86-112553.8 250
Bromochloromethane <64.5 ug/L 02/19/20 21:25 74-97-512564.5 250
Bromodichloromethane <46.2 ug/L 02/19/20 21:25 75-27-412546.2 250
Bromoform <101 ug/L 02/19/20 21:25 75-25-2125101250
Bromomethane <430 ug/L 02/19/20 21:25 74-83-9 M11250430250
tert-Butyl Alcohol <4400 ug/L 02/19/20 21:25 75-65-050004400250
n-Butylbenzene <88.2 ug/L 02/19/20 21:25 104-51-812588.2 250
sec-Butylbenzene <61.5 ug/L 02/19/20 21:25 135-98-812561.5 250
tert-Butylbenzene <62.5 ug/L 02/19/20 21:25 98-06-612562.5 250
tert-Butyl Formate <4450 ug/L 02/19/20 21:25 762-75-450004450250
Carbon tetrachloride <58.0 ug/L 02/19/20 21:25 56-23-512558.0 250
Chlorobenzene <56.2 ug/L 02/19/20 21:25 108-90-712556.2 250
Chloroethane <146 ug/L 02/19/20 21:25 75-00-3250146250
Chloroform <88.2 ug/L 02/19/20 21:25 67-66-312588.2 250
Chloromethane <104 ug/L 02/19/20 21:25 74-87-3250104250
2-Chlorotoluene <51.8 ug/L 02/19/20 21:25 95-49-812551.8 250
4-Chlorotoluene <51.5 ug/L 02/19/20 21:25 106-43-412551.5 250
1,2-Dibromo-3-chloropropane <96.2 ug/L 02/19/20 21:25 96-12-825096.2 250
Dibromochloromethane <100 ug/L 02/19/20 21:25 124-48-1125100250
1,2-Dibromoethane (EDB)716 ug/L 02/19/20 21:25 106-93-412557.8 250
Dibromomethane <77.5 ug/L 02/19/20 21:25 74-95-312577.5 250
1,2-Dichlorobenzene <60.0 ug/L 02/19/20 21:25 95-50-112560.0 250
1,3-Dichlorobenzene <62.5 ug/L 02/19/20 21:25 541-73-112562.5 250
1,4-Dichlorobenzene <62.2 ug/L 02/19/20 21:25 106-46-712562.2 250
Dichlorodifluoromethane <71.0 ug/L 02/19/20 21:25 75-71-812571.0 250
1,1-Dichloroethane <61.0 ug/L 02/19/20 21:25 75-34-312561.0 250
1,2-Dichloroethane 201 ug/L 02/19/20 21:25 107-06-212565.8 250
1,1-Dichloroethene <54.5 ug/L 02/19/20 21:25 75-35-412554.5 250
cis-1,2-Dichloroethene <51.8 ug/L 02/19/20 21:25 156-59-212551.8 250
trans-1,2-Dichloroethene <64.2 ug/L 02/19/20 21:25 156-60-512564.2 250
1,2-Dichloropropane <45.8 ug/L 02/19/20 21:25 78-87-512545.8 250
1,3-Dichloropropane <85.2 ug/L 02/19/20 21:25 142-28-912585.2 250
2,2-Dichloropropane <70.2 ug/L 02/19/20 21:25 594-20-712570.2 250
1,1-Dichloropropene <87.0 ug/L 02/19/20 21:25 563-58-612587.0 250
cis-1,3-Dichloropropene <89.2 ug/L 02/19/20 21:25 10061-01-512589.2 250
trans-1,3-Dichloropropene <98.5 ug/L 02/19/20 21:25 10061-02-612598.5 250
Diisopropyl ether <83.5 ug/L 02/19/20 21:25 108-20-312583.5 250
Ethanol <24700 ug/L 02/19/20 21:25 64-17-55000024700250
Ethylbenzene 2940 ug/L 02/19/20 21:25 100-41-412560.0 250
Ethyl-tert-butyl ether <952 ug/L 02/19/20 21:25 637-92-32500952250
Hexachloro-1,3-butadiene <300 ug/L 02/19/20 21:25 87-68-3500300250
Isopropylbenzene (Cumene)<59.5 ug/L 02/19/20 21:25 98-82-812559.5 250
Methylene Chloride <375 ug/L 02/19/20 21:25 75-09-2500375250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 9 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-3 Lab ID:92465237003 Collected:02/13/20 14:21 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether 121J ug/L 02/19/20 21:25 1634-04-4125111250
Naphthalene 1030 ug/L 02/19/20 21:25 91-20-3500165250
n-Propylbenzene 361 ug/L 02/19/20 21:25 103-65-112560.2 250
Styrene 88.9J ug/L 02/19/20 21:25 100-42-512564.0 250
1,1,1,2-Tetrachloroethane <106 ug/L 02/19/20 21:25 630-20-6125106250
1,1,2,2-Tetrachloroethane <48.2 ug/L 02/19/20 21:25 79-34-512548.2 250
Tetrachloroethene <58.0 ug/L 02/19/20 21:25 127-18-412558.0 250
Toluene 34600 ug/L 02/19/20 21:25 108-88-312557.0 250
1,2,3-Trichlorobenzene <195 ug/L 02/19/20 21:25 87-61-6500195250
1,2,4-Trichlorobenzene <109 ug/L 02/19/20 21:25 120-82-1500109250
1,1,1-Trichloroethane <69.5 ug/L 02/19/20 21:25 71-55-612569.5 250
1,1,2-Trichloroethane <58.0 ug/L 02/19/20 21:25 79-00-512558.0 250
Trichloroethene <58.0 ug/L 02/19/20 21:25 79-01-612558.0 250
Trichlorofluoromethane <84.0 ug/L 02/19/20 21:25 75-69-425084.0 250
1,2,3-Trichloropropane <67.8 ug/L 02/19/20 21:25 96-18-412567.8 250
1,2,4-Trimethylbenzene 3560 ug/L 02/19/20 21:25 95-63-612548.2 250
1,3,5-Trimethylbenzene 942 ug/L 02/19/20 21:25 108-67-812556.8 250
Vinyl chloride <102 ug/L 02/19/20 21:25 75-01-4 M1250102250
Xylene (Total)19600 ug/L 02/19/20 21:25 1330-20-7250125250
m&p-Xylene 13400 ug/L 02/19/20 21:25 179601-23-1250110250
o-Xylene 6160 ug/L 02/19/20 21:25 95-47-612559.2 250
Surrogates
1,2-Dichloroethane-d4 (S)103 %02/19/20 21:25 17060-07-070-130 250
4-Bromofluorobenzene (S)100 %02/19/20 21:25 460-00-470-130 250
Toluene-d8 (S)99 %02/19/20 21:25 2037-26-570-130 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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[phone]
Page 10 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-4 Lab ID:92465237004 Collected:02/13/20 12:56 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 17:32 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 17:32 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 17:32 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 17:32 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 17:32 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 17:32 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 17:32 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 17:32 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 17:32 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 17:32 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 17:32 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 17:32 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 17:32 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 17:32 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 17:32 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 17:32 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 17:32 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 17:32 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 17:32 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 17:32 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 17:32 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 17:32 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 02/19/20 17:32 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 02/19/20 17:32 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 17:32 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 17:32 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 17:32 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 17:32 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 17:32 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 17:32 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 17:32 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 17:32 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 17:32 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 17:32 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 17:32 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 17:32 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 17:32 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 17:32 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 17:32 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 17:32 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 17:32 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 17:32 100-41-40.50 0.24 1
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 17:32 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 17:32 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 17:32 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 17:32 75-09-22.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-4 Lab ID:92465237004 Collected:02/13/20 12:56 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 17:32 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 17:32 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 17:32 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 17:32 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 17:32 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 17:32 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 17:32 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 17:32 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 17:32 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 17:32 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 17:32 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 17:32 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 17:32 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 17:32 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 17:32 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 17:32 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 17:32 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 17:32 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 17:32 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 17:32 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 17:32 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/19/20 17:32 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/19/20 17:32 460-00-470-130 1
Toluene-d8 (S)103 %02/19/20 17:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-5 Lab ID:92465237005 Collected:02/13/20 10:37 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol 137 ug/L 02/19/20 17:50 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 17:50 994-05-810.0 3.0 1
Benzene 50.3 ug/L 02/19/20 17:50 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 17:50 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 17:50 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 17:50 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 17:50 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 17:50 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 17:50 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 17:50 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 17:50 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 17:50 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 17:50 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 17:50 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 17:50 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 17:50 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 17:50 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 17:50 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 17:50 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 17:50 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 17:50 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 17:50 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 02/19/20 17:50 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 02/19/20 17:50 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 17:50 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 17:50 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 17:50 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 17:50 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 17:50 75-34-30.50 0.24 1
1,2-Dichloroethane 15.1 ug/L 02/19/20 17:50 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 17:50 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 17:50 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 17:50 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 17:50 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 17:50 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 17:50 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 17:50 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 17:50 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 17:50 10061-02-60.50 0.39 1
Diisopropyl ether 0.68 ug/L 02/19/20 17:50 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 17:50 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 17:50 100-41-40.50 0.24 1
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 17:50 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 17:50 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 17:50 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 17:50 75-09-22.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-5 Lab ID:92465237005 Collected:02/13/20 10:37 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether 3.9 ug/L 02/19/20 17:50 1634-04-40.50 0.44 1
Naphthalene 0.78J ug/L 02/19/20 17:50 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 17:50 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 17:50 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 17:50 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 17:50 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 17:50 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 17:50 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 17:50 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 17:50 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 17:50 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 17:50 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 17:50 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 17:50 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 17:50 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 17:50 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 17:50 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 17:50 75-01-41.0 0.41 1
Xylene (Total)4.0 ug/L 02/19/20 17:50 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 17:50 179601-23-11.0 0.44 1
o-Xylene 4.0 ug/L 02/19/20 17:50 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %02/19/20 17:50 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/19/20 17:50 460-00-470-130 1
Toluene-d8 (S)103 %02/19/20 17:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-6 Lab ID:92465237006 Collected:02/13/20 11:19 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 18:08 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 18:08 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 18:08 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 18:08 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 18:08 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 18:08 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 18:08 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 18:08 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 18:08 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 18:08 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 18:08 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 18:08 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 18:08 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 18:08 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 18:08 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 18:08 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 18:08 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 18:08 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 18:08 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 18:08 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 18:08 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 18:08 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 02/19/20 18:08 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 02/19/20 18:08 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 18:08 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 18:08 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 18:08 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 18:08 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 18:08 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 18:08 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 18:08 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 18:08 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 18:08 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 18:08 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 18:08 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 18:08 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 18:08 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 18:08 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 18:08 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 18:08 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 18:08 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 18:08 100-41-40.50 0.24 1
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 18:08 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 18:08 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 18:08 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 18:08 75-09-22.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Page 15 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-6 Lab ID:92465237006 Collected:02/13/20 11:19 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 18:08 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 18:08 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 18:08 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 18:08 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 18:08 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 18:08 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 18:08 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 18:08 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 18:08 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 18:08 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 18:08 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 18:08 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 18:08 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 18:08 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 18:08 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 18:08 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 18:08 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 18:08 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 18:08 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 18:08 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 18:08 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/19/20 18:08 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/19/20 18:08 460-00-470-130 1
Toluene-d8 (S)105 %02/19/20 18:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Page 16 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-12 Lab ID:92465237007 Collected:02/13/20 09:43 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/21/20 12:43 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/21/20 12:43 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/21/20 12:43 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/21/20 12:43 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/21/20 12:43 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/21/20 12:43 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/21/20 12:43 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/21/20 12:43 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/21/20 12:43 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/21/20 12:43 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/21/20 12:43 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/21/20 12:43 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/21/20 12:43 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/21/20 12:43 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/21/20 12:43 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/21/20 12:43 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/21/20 12:43 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/21/20 12:43 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/21/20 12:43 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/21/20 12:43 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/21/20 12:43 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/21/20 12:43 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 02/21/20 12:43 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 02/21/20 12:43 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/21/20 12:43 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/21/20 12:43 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/21/20 12:43 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/21/20 12:43 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/21/20 12:43 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/21/20 12:43 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/21/20 12:43 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/21/20 12:43 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/21/20 12:43 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/21/20 12:43 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/21/20 12:43 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/21/20 12:43 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/21/20 12:43 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/21/20 12:43 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/21/20 12:43 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/21/20 12:43 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/21/20 12:43 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/21/20 12:43 100-41-40.50 0.24 1
Ethyl-tert-butyl ether <3.8 ug/L 02/21/20 12:43 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/21/20 12:43 87-68-3 L22.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/21/20 12:43 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/21/20 12:43 75-09-22.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:MW-12 Lab ID:92465237007 Collected:02/13/20 09:43 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether <0.44 ug/L 02/21/20 12:43 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/21/20 12:43 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/21/20 12:43 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/21/20 12:43 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/21/20 12:43 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/21/20 12:43 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/21/20 12:43 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/21/20 12:43 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/21/20 12:43 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/21/20 12:43 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/21/20 12:43 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/21/20 12:43 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/21/20 12:43 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/21/20 12:43 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/21/20 12:43 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/21/20 12:43 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/21/20 12:43 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/21/20 12:43 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/21/20 12:43 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/21/20 12:43 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/21/20 12:43 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %02/21/20 12:43 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %02/21/20 12:43 460-00-470-130 1
Toluene-d8 (S)104 %02/21/20 12:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:RW-1 Lab ID:92465237008 Collected:02/13/20 15:56 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol 2210 ug/L 02/21/20 13:38 75-85-4100040510
tert-Amylmethyl ether <29.6 ug/L 02/21/20 13:38 994-05-810029.6 10
Benzene 1200 ug/L 02/21/20 13:38 71-43-25.0 2.4 10
Bromobenzene <2.2 ug/L 02/21/20 13:38 108-86-15.0 2.2 10
Bromochloromethane <2.6 ug/L 02/21/20 13:38 74-97-55.0 2.6 10
Bromodichloromethane <1.8 ug/L 02/21/20 13:38 75-27-45.0 1.8 10
Bromoform <4.0 ug/L 02/21/20 13:38 75-25-25.0 4.0 10
Bromomethane <17.2 ug/L 02/21/20 13:38 74-83-950.0 17.2 10
tert-Butyl Alcohol <176 ug/L 02/21/20 13:38 75-65-020017610
n-Butylbenzene <3.5 ug/L 02/21/20 13:38 104-51-85.0 3.5 10
sec-Butylbenzene <2.5 ug/L 02/21/20 13:38 135-98-85.0 2.5 10
tert-Butylbenzene <2.5 ug/L 02/21/20 13:38 98-06-65.0 2.5 10
tert-Butyl Formate <178 ug/L 02/21/20 13:38 762-75-420017810
Carbon tetrachloride <2.3 ug/L 02/21/20 13:38 56-23-55.0 2.3 10
Chlorobenzene <2.2 ug/L 02/21/20 13:38 108-90-75.0 2.2 10
Chloroethane <5.8 ug/L 02/21/20 13:38 75-00-310.0 5.8 10
Chloroform <3.5 ug/L 02/21/20 13:38 67-66-35.0 3.5 10
Chloromethane <4.2 ug/L 02/21/20 13:38 74-87-310.0 4.2 10
2-Chlorotoluene <2.1 ug/L 02/21/20 13:38 95-49-85.0 2.1 10
4-Chlorotoluene <2.1 ug/L 02/21/20 13:38 106-43-45.0 2.1 10
1,2-Dibromo-3-chloropropane <3.8 ug/L 02/21/20 13:38 96-12-810.0 3.8 10
Dibromochloromethane <4.0 ug/L 02/21/20 13:38 124-48-15.0 4.0 10
1,2-Dibromoethane (EDB)<2.3 ug/L 02/21/20 13:38 106-93-45.0 2.3 10
Dibromomethane <3.1 ug/L 02/21/20 13:38 74-95-35.0 3.1 10
1,2-Dichlorobenzene <2.4 ug/L 02/21/20 13:38 95-50-15.0 2.4 10
1,3-Dichlorobenzene <2.5 ug/L 02/21/20 13:38 541-73-15.0 2.5 10
1,4-Dichlorobenzene <2.5 ug/L 02/21/20 13:38 106-46-75.0 2.5 10
Dichlorodifluoromethane <2.8 ug/L 02/21/20 13:38 75-71-85.0 2.8 10
1,1-Dichloroethane <2.4 ug/L 02/21/20 13:38 75-34-35.0 2.4 10
1,2-Dichloroethane 74.9 ug/L 02/21/20 13:38 107-06-25.0 2.6 10
1,1-Dichloroethene <2.2 ug/L 02/21/20 13:38 75-35-45.0 2.2 10
cis-1,2-Dichloroethene <2.1 ug/L 02/21/20 13:38 156-59-25.0 2.1 10
trans-1,2-Dichloroethene <2.6 ug/L 02/21/20 13:38 156-60-55.0 2.6 10
1,2-Dichloropropane <1.8 ug/L 02/21/20 13:38 78-87-55.0 1.8 10
1,3-Dichloropropane <3.4 ug/L 02/21/20 13:38 142-28-95.0 3.4 10
2,2-Dichloropropane <2.8 ug/L 02/21/20 13:38 594-20-75.0 2.8 10
1,1-Dichloropropene <3.5 ug/L 02/21/20 13:38 563-58-65.0 3.5 10
cis-1,3-Dichloropropene <3.6 ug/L 02/21/20 13:38 10061-01-55.0 3.6 10
trans-1,3-Dichloropropene <3.9 ug/L 02/21/20 13:38 10061-02-65.0 3.9 10
Diisopropyl ether 28.7 ug/L 02/21/20 13:38 108-20-35.0 3.3 10
Ethanol <989 ug/L 02/21/20 13:38 64-17-5200098910
Ethylbenzene 28.5 ug/L 02/21/20 13:38 100-41-45.0 2.4 10
Ethyl-tert-butyl ether <38.1 ug/L 02/21/20 13:38 637-92-310038.1 10
Hexachloro-1,3-butadiene <12.0 ug/L 02/21/20 13:38 87-68-3 L220.0 12.0 10
Isopropylbenzene (Cumene)<2.4 ug/L 02/21/20 13:38 98-82-85.0 2.4 10
Methylene Chloride <15.0 ug/L 02/21/20 13:38 75-09-220.0 15.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:RW-1 Lab ID:92465237008 Collected:02/13/20 15:56 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether 57.9 ug/L 02/21/20 13:38 1634-04-45.0 4.4 10
Naphthalene 20.1 ug/L 02/21/20 13:38 91-20-320.0 6.6 10
n-Propylbenzene 2.5J ug/L 02/21/20 13:38 103-65-15.0 2.4 10
Styrene <2.6 ug/L 02/21/20 13:38 100-42-55.0 2.6 10
1,1,1,2-Tetrachloroethane <4.2 ug/L 02/21/20 13:38 630-20-65.0 4.2 10
1,1,2,2-Tetrachloroethane <1.9 ug/L 02/21/20 13:38 79-34-55.0 1.9 10
Tetrachloroethene <2.3 ug/L 02/21/20 13:38 127-18-45.0 2.3 10
Toluene 202 ug/L 02/21/20 13:38 108-88-35.0 2.3 10
1,2,3-Trichlorobenzene <7.8 ug/L 02/21/20 13:38 87-61-620.0 7.8 10
1,2,4-Trichlorobenzene <4.4 ug/L 02/21/20 13:38 120-82-120.0 4.4 10
1,1,1-Trichloroethane <2.8 ug/L 02/21/20 13:38 71-55-65.0 2.8 10
1,1,2-Trichloroethane <2.3 ug/L 02/21/20 13:38 79-00-55.0 2.3 10
Trichloroethene <2.3 ug/L 02/21/20 13:38 79-01-65.0 2.3 10
Trichlorofluoromethane <3.4 ug/L 02/21/20 13:38 75-69-410.0 3.4 10
1,2,3-Trichloropropane <2.7 ug/L 02/21/20 13:38 96-18-45.0 2.7 10
1,2,4-Trimethylbenzene 16.8 ug/L 02/21/20 13:38 95-63-65.0 1.9 10
1,3,5-Trimethylbenzene 9.4 ug/L 02/21/20 13:38 108-67-85.0 2.3 10
Vinyl chloride <4.1 ug/L 02/21/20 13:38 75-01-410.0 4.1 10
Xylene (Total)161 ug/L 02/21/20 13:38 1330-20-710.0 5.0 10
m&p-Xylene 50.9 ug/L 02/21/20 13:38 179601-23-110.0 4.4 10
o-Xylene 111 ug/L 02/21/20 13:38 95-47-65.0 2.4 10
Surrogates
1,2-Dichloroethane-d4 (S)100 %02/21/20 13:38 17060-07-070-130 10
4-Bromofluorobenzene (S)99 %02/21/20 13:38 460-00-470-130 10
Toluene-d8 (S)102 %02/21/20 13:38 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-1 Lab ID:92465237009 Collected:02/12/20 15:38 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.011 ug/L 02/24/20 03:25 106-93-402/23/20 14:340.020 0.011 1
Surrogates
1-Chloro-2-bromopropane (S)79 %02/24/20 03:25 301-79-5602/23/20 14:3470-130 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 18:26 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 18:26 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 18:26 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 18:26 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 18:26 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 18:26 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 18:26 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 18:26 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 18:26 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 18:26 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 18:26 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 18:26 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 18:26 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 18:26 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 18:26 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 18:26 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 18:26 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 18:26 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 18:26 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 18:26 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 18:26 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 18:26 124-48-10.50 0.40 1
Dibromomethane <0.31 ug/L 02/19/20 18:26 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 18:26 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 18:26 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 18:26 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 18:26 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 18:26 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 18:26 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 18:26 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 18:26 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 18:26 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 18:26 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 18:26 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 18:26 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 18:26 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 18:26 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 18:26 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 18:26 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 18:26 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 18:26 100-41-40.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 21 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-1 Lab ID:92465237009 Collected:02/12/20 15:38 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 18:26 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 18:26 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 18:26 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 18:26 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 18:26 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 18:26 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 18:26 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 18:26 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 18:26 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 18:26 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 18:26 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 18:26 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 18:26 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 18:26 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 18:26 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 18:26 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 18:26 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 18:26 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 18:26 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 18:26 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 18:26 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 18:26 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 18:26 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 18:26 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 18:26 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %02/19/20 18:26 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/19/20 18:26 460-00-470-130 1
Toluene-d8 (S)101 %02/19/20 18:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-2 Lab ID:92465237010 Collected:02/12/20 16:36 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.011 ug/L 02/24/20 21:46 106-93-402/24/20 16:270.020 0.011 1
Surrogates
1-Chloro-2-bromopropane (S)105 %02/24/20 21:46 301-79-5602/24/20 16:2770-130 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 18:44 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 18:44 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 18:44 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 18:44 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 18:44 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 18:44 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 18:44 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 18:44 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 18:44 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 18:44 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 18:44 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 18:44 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 18:44 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 18:44 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 18:44 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 18:44 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 18:44 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 18:44 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 18:44 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 18:44 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 18:44 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 18:44 124-48-10.50 0.40 1
Dibromomethane <0.31 ug/L 02/19/20 18:44 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 18:44 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 18:44 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 18:44 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 18:44 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 18:44 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 18:44 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 18:44 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 18:44 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 18:44 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 18:44 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 18:44 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 18:44 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 18:44 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 18:44 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 18:44 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 18:44 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 18:44 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 18:44 100-41-40.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-2 Lab ID:92465237010 Collected:02/12/20 16:36 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 18:44 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 18:44 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 18:44 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 18:44 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 18:44 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 18:44 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 18:44 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 18:44 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 18:44 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 18:44 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 18:44 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 18:44 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 18:44 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 18:44 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 18:44 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 18:44 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 18:44 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 18:44 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 18:44 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 18:44 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 18:44 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 18:44 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 18:44 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 18:44 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 18:44 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/19/20 18:44 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/19/20 18:44 460-00-470-130 1
Toluene-d8 (S)104 %02/19/20 18:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-5 Lab ID:92465237011 Collected:02/12/20 16:05 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.011 ug/L 02/24/20 03:49 106-93-402/23/20 14:340.020 0.011 1
Surrogates
1-Chloro-2-bromopropane (S)76 %02/24/20 03:49 301-79-5602/23/20 14:3470-130 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 19:02 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 19:02 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 19:02 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 19:02 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 19:02 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 19:02 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 19:02 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 19:02 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 19:02 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 19:02 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 19:02 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 19:02 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 19:02 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 19:02 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 19:02 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 19:02 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 19:02 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 19:02 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 19:02 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 19:02 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 19:02 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 19:02 124-48-10.50 0.40 1
Dibromomethane <0.31 ug/L 02/19/20 19:02 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 19:02 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 19:02 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 19:02 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 19:02 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 19:02 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 19:02 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 19:02 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 19:02 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 19:02 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 19:02 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 19:02 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 19:02 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 19:02 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 19:02 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 19:02 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 19:02 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 19:02 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 19:02 100-41-40.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-5 Lab ID:92465237011 Collected:02/12/20 16:05 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 19:02 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 19:02 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 19:02 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 19:02 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 19:02 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 19:02 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 19:02 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 19:02 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 19:02 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 19:02 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 19:02 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 19:02 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 19:02 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 19:02 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 19:02 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 19:02 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 19:02 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 19:02 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 19:02 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 19:02 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 19:02 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 19:02 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 19:02 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 19:02 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 19:02 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/19/20 19:02 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/19/20 19:02 460-00-470-130 1
Toluene-d8 (S)102 %02/19/20 19:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-7 Lab ID:92465237012 Collected:02/12/20 14:37 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.011 ug/L 02/24/20 21:57 106-93-402/24/20 16:270.020 0.011 1
Surrogates
1-Chloro-2-bromopropane (S)102 %02/24/20 21:57 301-79-5602/24/20 16:2770-130 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 19:20 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 19:20 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 19:20 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 19:20 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 19:20 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 19:20 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 19:20 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 19:20 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 19:20 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 19:20 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 19:20 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 19:20 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 19:20 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 19:20 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 19:20 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 19:20 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 19:20 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 19:20 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 19:20 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 19:20 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 19:20 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 19:20 124-48-10.50 0.40 1
Dibromomethane <0.31 ug/L 02/19/20 19:20 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 19:20 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 19:20 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 19:20 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 19:20 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 19:20 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 19:20 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 19:20 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 19:20 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 19:20 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 19:20 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 19:20 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 19:20 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 19:20 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 19:20 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 19:20 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 19:20 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 19:20 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 19:20 100-41-40.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-7 Lab ID:92465237012 Collected:02/12/20 14:37 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 19:20 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 19:20 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 19:20 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 19:20 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 19:20 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 19:20 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 19:20 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 19:20 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 19:20 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 19:20 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 19:20 127-18-40.50 0.23 1
Toluene 9.3 ug/L 02/19/20 19:20 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 19:20 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 19:20 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 19:20 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 19:20 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 19:20 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 19:20 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 19:20 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 19:20 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 19:20 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 19:20 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 19:20 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 19:20 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 19:20 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/19/20 19:20 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/19/20 19:20 460-00-470-130 1
Toluene-d8 (S)104 %02/19/20 19:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-9 Lab ID:92465237013 Collected:02/12/20 14:36 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)<0.011 ug/L 02/24/20 04:12 106-93-402/23/20 14:340.019 0.011 1
Surrogates
1-Chloro-2-bromopropane (S)79 %02/24/20 04:12 301-79-5602/23/20 14:3470-130 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 19:37 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 19:37 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 19:37 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 19:37 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 19:37 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 19:37 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 19:37 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 19:37 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 19:37 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 19:37 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 19:37 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 19:37 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 19:37 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 19:37 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 19:37 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 19:37 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 19:37 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 19:37 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 19:37 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 19:37 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 19:37 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 19:37 124-48-10.50 0.40 1
Dibromomethane <0.31 ug/L 02/19/20 19:37 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 19:37 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 19:37 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 19:37 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 19:37 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 19:37 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 19:37 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 19:37 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 19:37 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 19:37 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 19:37 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 19:37 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 19:37 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 19:37 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 19:37 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 19:37 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 19:37 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 19:37 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 19:37 100-41-40.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:WSW-9 Lab ID:92465237013 Collected:02/12/20 14:36 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 19:37 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 19:37 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 19:37 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 19:37 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 19:37 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 19:37 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 19:37 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 19:37 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 19:37 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 19:37 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 19:37 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 19:37 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 19:37 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 19:37 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 19:37 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 19:37 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 19:37 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 19:37 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 19:37 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 19:37 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 19:37 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 19:37 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 19:37 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 19:37 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 19:37 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/19/20 19:37 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/19/20 19:37 460-00-470-130 1
Toluene-d8 (S)105 %02/19/20 19:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:FB-1 Lab ID:92465237014 Collected:02/12/20 16:26 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol <40.5 ug/L 02/19/20 16:57 75-85-410040.5 1
tert-Amylmethyl ether <3.0 ug/L 02/19/20 16:57 994-05-810.0 3.0 1
Benzene <0.24 ug/L 02/19/20 16:57 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 02/19/20 16:57 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 02/19/20 16:57 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 02/19/20 16:57 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 02/19/20 16:57 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 02/19/20 16:57 74-83-95.0 1.7 1
tert-Butyl Alcohol <17.6 ug/L 02/19/20 16:57 75-65-020.0 17.6 1
n-Butylbenzene <0.35 ug/L 02/19/20 16:57 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 02/19/20 16:57 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 02/19/20 16:57 98-06-60.50 0.25 1
tert-Butyl Formate <17.8 ug/L 02/19/20 16:57 762-75-420.0 17.8 1
Carbon tetrachloride <0.23 ug/L 02/19/20 16:57 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 02/19/20 16:57 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 02/19/20 16:57 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 02/19/20 16:57 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 02/19/20 16:57 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 02/19/20 16:57 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 02/19/20 16:57 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 02/19/20 16:57 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 02/19/20 16:57 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 02/19/20 16:57 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 02/19/20 16:57 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 02/19/20 16:57 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 02/19/20 16:57 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 02/19/20 16:57 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 02/19/20 16:57 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 02/19/20 16:57 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 02/19/20 16:57 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 02/19/20 16:57 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 02/19/20 16:57 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 02/19/20 16:57 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 02/19/20 16:57 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 02/19/20 16:57 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 02/19/20 16:57 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 02/19/20 16:57 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 02/19/20 16:57 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 02/19/20 16:57 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 02/19/20 16:57 108-20-30.50 0.33 1
Ethanol <98.9 ug/L 02/19/20 16:57 64-17-520098.9 1
Ethylbenzene <0.24 ug/L 02/19/20 16:57 100-41-40.50 0.24 1
Ethyl-tert-butyl ether <3.8 ug/L 02/19/20 16:57 637-92-310.0 3.8 1
Hexachloro-1,3-butadiene <1.2 ug/L 02/19/20 16:57 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)<0.24 ug/L 02/19/20 16:57 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 02/19/20 16:57 75-09-22.0 1.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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Page 31 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Sample:FB-1 Lab ID:92465237014 Collected:02/12/20 16:26 Received:02/14/20 08:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Methyl-tert-butyl ether <0.44 ug/L 02/19/20 16:57 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 02/19/20 16:57 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 02/19/20 16:57 103-65-10.50 0.24 1
Styrene <0.26 ug/L 02/19/20 16:57 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 02/19/20 16:57 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 02/19/20 16:57 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 02/19/20 16:57 127-18-40.50 0.23 1
Toluene <0.23 ug/L 02/19/20 16:57 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 02/19/20 16:57 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 02/19/20 16:57 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 02/19/20 16:57 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 02/19/20 16:57 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 02/19/20 16:57 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 02/19/20 16:57 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 02/19/20 16:57 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 02/19/20 16:57 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 02/19/20 16:57 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 02/19/20 16:57 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 02/19/20 16:57 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 02/19/20 16:57 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 02/19/20 16:57 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/19/20 16:57 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/19/20 16:57 460-00-470-130 1
Toluene-d8 (S)102 %02/19/20 16:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 32 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
525880
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92465237001, 92465237002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2810686
Associated Lab Samples:92465237001, 92465237002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 02/19/20 04:500.42
1,1,1-Trichloroethane ug/L <0.28 0.50 02/19/20 04:500.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 02/19/20 04:500.19
1,1,2-Trichloroethane ug/L <0.23 0.50 02/19/20 04:500.23
1,1-Dichloroethane ug/L <0.24 0.50 02/19/20 04:500.24
1,1-Dichloroethene ug/L <0.22 0.50 02/19/20 04:500.22
1,1-Dichloropropene ug/L <0.35 0.50 02/19/20 04:500.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 02/19/20 04:500.78
1,2,3-Trichloropropane ug/L <0.27 0.50 02/19/20 04:500.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 02/19/20 04:500.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 02/19/20 04:500.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 02/19/20 04:500.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 02/19/20 04:500.23
1,2-Dichlorobenzene ug/L <0.24 0.50 02/19/20 04:500.24
1,2-Dichloroethane ug/L <0.26 0.50 02/19/20 04:500.26
1,2-Dichloropropane ug/L <0.18 0.50 02/19/20 04:500.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 02/19/20 04:500.23
1,3-Dichlorobenzene ug/L <0.25 0.50 02/19/20 04:500.25
1,3-Dichloropropane ug/L <0.34 0.50 02/19/20 04:500.34
1,4-Dichlorobenzene ug/L <0.25 0.50 02/19/20 04:500.25
2,2-Dichloropropane ug/L <0.28 0.50 02/19/20 04:500.28
2-Chlorotoluene ug/L <0.21 0.50 02/19/20 04:500.21
4-Chlorotoluene ug/L <0.21 0.50 02/19/20 04:500.21
Benzene ug/L <0.24 0.50 02/19/20 04:500.24
Bromobenzene ug/L <0.22 0.50 02/19/20 04:500.22
Bromochloromethane ug/L <0.26 0.50 02/19/20 04:500.26
Bromodichloromethane ug/L <0.18 0.50 02/19/20 04:500.18
Bromoform ug/L <0.40 0.50 02/19/20 04:500.40
Bromomethane ug/L <1.7 5.0 02/19/20 04:501.7
Carbon tetrachloride ug/L <0.23 0.50 02/19/20 04:500.23
Chlorobenzene ug/L <0.22 0.50 02/19/20 04:500.22
Chloroethane ug/L <0.58 1.0 02/19/20 04:500.58
Chloroform ug/L <0.35 0.50 02/19/20 04:500.35
Chloromethane ug/L <0.42 1.0 02/19/20 04:500.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 02/19/20 04:500.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 02/19/20 04:500.36
Dibromochloromethane ug/L <0.40 0.50 02/19/20 04:500.40
Dibromomethane ug/L <0.31 0.50 02/19/20 04:500.31
Dichlorodifluoromethane ug/L <0.28 0.50 02/19/20 04:500.28
Diisopropyl ether ug/L <0.33 0.50 02/19/20 04:500.33
Ethanol ug/L <98.9 200 02/19/20 04:5098.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2810686
Associated Lab Samples:92465237001, 92465237002
Matrix:Water
AnalyzedMDL
Ethyl-tert-butyl ether ug/L <3.8 10.0 02/19/20 04:503.8
Ethylbenzene ug/L <0.24 0.50 02/19/20 04:500.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 02/19/20 04:501.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 02/19/20 04:500.24
m&p-Xylene ug/L <0.44 1.0 02/19/20 04:500.44
Methyl-tert-butyl ether ug/L <0.44 0.50 02/19/20 04:500.44
Methylene Chloride ug/L <1.5 2.0 02/19/20 04:501.5
n-Butylbenzene ug/L <0.35 0.50 02/19/20 04:500.35
n-Propylbenzene ug/L <0.24 0.50 02/19/20 04:500.24
Naphthalene ug/L <0.66 2.0 02/19/20 04:500.66
o-Xylene ug/L <0.24 0.50 02/19/20 04:500.24
sec-Butylbenzene ug/L <0.25 0.50 02/19/20 04:500.25
Styrene ug/L <0.26 0.50 02/19/20 04:500.26
tert-Amyl Alcohol ug/L <40.5 100 02/19/20 04:5040.5
tert-Amylmethyl ether ug/L <3.0 10.0 02/19/20 04:503.0
tert-Butyl Alcohol ug/L <17.6 20.0 02/19/20 04:5017.6
tert-Butyl Formate ug/L <17.8 20.0 02/19/20 04:5017.8
tert-Butylbenzene ug/L <0.25 0.50 02/19/20 04:500.25
Tetrachloroethene ug/L <0.23 0.50 02/19/20 04:500.23
Toluene ug/L <0.23 0.50 02/19/20 04:500.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 02/19/20 04:500.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 02/19/20 04:500.39
Trichloroethene ug/L <0.23 0.50 02/19/20 04:500.23
Trichlorofluoromethane ug/L <0.34 1.0 02/19/20 04:500.34
Vinyl chloride ug/L <0.41 1.0 02/19/20 04:500.41
Xylene (Total)ug/L <0.50 1.0 02/19/20 04:500.50
1,2-Dichloroethane-d4 (S)%101 70-130 02/19/20 04:50
4-Bromofluorobenzene (S)%100 70-130 02/19/20 04:50
Toluene-d8 (S)%103 70-130 02/19/20 04:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2810687LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.650 107 60-140
1,1,1-Trichloroethane ug/L 55.050 110 60-140
1,1,2,2-Tetrachloroethane ug/L 55.950 112 60-140
1,1,2-Trichloroethane ug/L 56.150 112 60-140
1,1-Dichloroethane ug/L 55.450 111 60-140
1,1-Dichloroethene ug/L 57.850 116 60-140
1,1-Dichloropropene ug/L 53.050 106 60-140
1,2,3-Trichlorobenzene ug/L 56.450 113 60-140
1,2,3-Trichloropropane ug/L 54.050 108 60-140
1,2,4-Trichlorobenzene ug/L 54.150 108 60-140
1,2,4-Trimethylbenzene ug/L 55.150 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2810687LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 58.350 117 60-140
1,2-Dibromoethane (EDB)ug/L 57.450 115 60-140
1,2-Dichlorobenzene ug/L 52.550 105 60-140
1,2-Dichloroethane ug/L 54.650 109 60-140
1,2-Dichloropropane ug/L 56.650 113 60-140
1,3,5-Trimethylbenzene ug/L 55.450 111 60-140
1,3-Dichlorobenzene ug/L 55.150 110 60-140
1,3-Dichloropropane ug/L 56.650 113 60-140
1,4-Dichlorobenzene ug/L 50.150 100 60-140
2,2-Dichloropropane ug/L 52.450 105 60-140
2-Chlorotoluene ug/L 54.950 110 60-140
4-Chlorotoluene ug/L 55.450 111 60-140
Benzene ug/L 57.150 114 60-140
Bromobenzene ug/L 52.150 104 60-140
Bromochloromethane ug/L 53.350 107 60-140
Bromodichloromethane ug/L 53.150 106 60-140
Bromoform ug/L 58.250 116 60-140
Bromomethane ug/L 58.250 116 60-140
Carbon tetrachloride ug/L 52.850 106 60-140
Chlorobenzene ug/L 52.150 104 60-140
Chloroethane ug/L 47.750 95 60-140
Chloroform ug/L 54.450 109 60-140
Chloromethane ug/L 47.850 96 60-140
cis-1,2-Dichloroethene ug/L 55.650 111 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 59.850 120 60-140
Dibromomethane ug/L 51.750 103 60-140
Dichlorodifluoromethane ug/L 50.650 101 60-140
Diisopropyl ether ug/L 51.850 104 60-140
Ethanol ug/L 22802000 114 60-140
Ethyl-tert-butyl ether ug/L 105100 105 60-140
Ethylbenzene ug/L 55.050 110 60-140
Hexachloro-1,3-butadiene ug/L 52.350 105 60-140
Isopropylbenzene (Cumene)ug/L 56.050 112 60-140
m&p-Xylene ug/L 115100 115 60-140
Methyl-tert-butyl ether ug/L 57.050 114 60-140
Methylene Chloride ug/L 49.850 100 60-140
n-Butylbenzene ug/L 53.450 107 60-140
n-Propylbenzene ug/L 55.550 111 60-140
Naphthalene ug/L 54.450 109 60-140
o-Xylene ug/L 54.050 108 60-140
sec-Butylbenzene ug/L 55.050 110 60-140
Styrene ug/L 53.350 107 60-140
tert-Amyl Alcohol ug/L 10701000 107 60-140
tert-Amylmethyl ether ug/L 109100 109 60-140
tert-Butyl Alcohol ug/L 582500 116 60-140
tert-Butyl Formate ug/L 448400 112 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2810687LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 46.950 94 60-140
Tetrachloroethene ug/L 50.950 102 60-140
Toluene ug/L 55.950 112 60-140
trans-1,2-Dichloroethene ug/L 56.550 113 60-140
trans-1,3-Dichloropropene ug/L 56.650 113 60-140
Trichloroethene ug/L 54.350 109 60-140
Trichlorofluoromethane ug/L 47.950 96 60-140
Vinyl chloride ug/L 59.250 118 60-140
Xylene (Total)ug/L 169150 113 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2810688MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465237001
2810689
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 106 60-140108 1 304000<84.4 4260 4310
1,1,1-Trichloroethane ug/L 4000 115 60-140112 2 304000<55.6 4580 4490
1,1,2,2-Tetrachloroethane ug/L 4000 111 60-140107 3 304000<38.6 4420 4290
1,1,2-Trichloroethane ug/L 4000 110 60-140111 1 304000<46.4 4390 4420
1,1-Dichloroethane ug/L 4000 113 60-140114 0 304000<48.8 4530 4540
1,1-Dichloroethene ug/L 4000 125 60-140124 0 304000<43.6 4980 4960
1,1-Dichloropropene ug/L 4000 112 60-140114 2 304000<69.6 4470 4550
1,2,3-Trichlorobenzene ug/L 4000 107 60-140105 2 304000<156 4280 4200
1,2,3-Trichloropropane ug/L 4000 110 60-140113 3 304000<54.2 4390 4520
1,2,4-Trichlorobenzene ug/L 4000 107 60-140109 2 304000<87.2 4280 4360
1,2,4-Trimethylbenzene ug/L 4000 121 60-140117 2 304000226071206950
1,2-Dibromo-3-
chloropropane ug/L 4000 105 60-140103 2 304000<77.0 4220 4140
1,2-Dibromoethane (EDB)ug/L 4000 119 60-140115 3 304000113059005740
1,2-Dichlorobenzene ug/L 4000 105 60-140105 1 304000<48.0 4180 4210
1,2-Dichloroethane ug/L 4000 110 60-140115 3 304000228067006890
1,2-Dichloropropane ug/L 4000 115 60-140119 4 304000<36.6 4580 4750
1,3,5-Trimethylbenzene ug/L 4000 117 60-140118 0 30400055852405260
1,3-Dichlorobenzene ug/L 4000 110 60-140110 0 304000<50.0 4400 4410
1,3-Dichloropropane ug/L 4000 110 60-140113 3 304000<68.2 4420 4530
1,4-Dichlorobenzene ug/L 4000 104 60-140105 1 304000<49.8 4160 4190
2,2-Dichloropropane ug/L 4000 112 60-140112 0 304000<56.2 4490 4480
2-Chlorotoluene ug/L 4000 122 60-140119 2 304000<41.4 4870 4770
4-Chlorotoluene ug/L 4000 114 60-140113 1 304000<41.2 4570 4530
Benzene ug/L M1400013860-140154 3 304000195002500025700
Bromobenzene ug/L 4000 107 60-140104 3 304000<43.0 4270 4150
Bromochloromethane ug/L 4000 102 60-140108 5 304000<51.6 4080 4300
Bromodichloromethane ug/L 4000 105 60-140101 4 304000<37.0 4220 4050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 36 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2810688MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465237001
2810689
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromoform ug/L 4000 106 60-140106 0 304000<81.0 4220 4240
Bromomethane ug/L 4000 115 60-140139 19 304000<344 4600 5550
Carbon tetrachloride ug/L 4000 111 60-140114 2 304000<46.4 4460 4550
Chlorobenzene ug/L 4000 107 60-140108 1 304000<45.0 4280 4340
Chloroethane ug/L 4000 117 60-140122 4 304000<117 4670 4870
Chloroform ug/L 4000 115 60-140116 1 304000<70.6 4600 4630
Chloromethane ug/L 4000 97 60-140103 6 304000<83.0 3870 4100
cis-1,2-Dichloroethene ug/L 4000 112 60-140114 2 304000<41.4 4490 4570
cis-1,3-Dichloropropene ug/L 4000 110 60-140111 1 304000<71.4 4390 4430
Dibromochloromethane ug/L 4000 112 60-140107 4 304000<80.4 4490 4300
Dibromomethane ug/L 4000 104 60-140103 1 304000<62.0 4160 4110
Dichlorodifluoromethane ug/L 4000 114 60-140115 0 304000<56.8 4570 4580
Diisopropyl ether ug/L 4000 105 60-140106 0 30400059048104820
Ethanol ug/L 160000 100 60-140110 10 30160000<19800 159000 176000
Ethyl-tert-butyl ether ug/L 8000 103 60-140103 0 308000<762 8240 8230
Ethylbenzene ug/L 4000 121 60-140120 1 304000200068506820
Hexachloro-1,3-butadiene ug/L 4000 106 60-140106 1 304000<240 4250 4220
Isopropylbenzene
(Cumene)ug/L 4000 119 60-140120 1 304000<47.6 4760 4790
m&p-Xylene ug/L 8000 127 60-140129 1 308000106002080020900
Methyl-tert-butyl ether ug/L E,M1400017360-140189 1 304000365004340044000
Methylene Chloride ug/L 4000 103 60-140104 1 304000<300 4120 4180
n-Butylbenzene ug/L 4000 111 60-140114 3 304000<70.6 4440 4580
n-Propylbenzene ug/L 4000 118 60-140117 1 30400016748804840
Naphthalene ug/L 4000 119 60-140106 10 30400071054804970
o-Xylene ug/L 4000 122 60-140124 1 304000473095909700
sec-Butylbenzene ug/L 4000 113 60-140115 2 304000<49.2 4520 4620
Styrene ug/L 4000 109 60-140110 1 304000<51.2 4380 4410
tert-Amyl Alcohol ug/L 80000 105 60-140108 1 308000059600144000146000
tert-Amylmethyl ether ug/L 8000 108 60-140107 1 308000<592 9170 9120
tert-Butyl Alcohol ug/L M14000014060-140145 0 3040000286000342000344000
tert-Butyl Formate ug/L 32000 107 60-140107 0 3032000<3560 34200 34300
tert-Butylbenzene ug/L 4000 96 60-14097 2 304000<50.0 3830 3880
Tetrachloroethene ug/L 4000 111 60-140108 3 304000<46.4 4450 4340
Toluene ug/L M1400012360-140144 3 304000264003140032200
trans-1,2-Dichloroethene ug/L 4000 116 60-140119 3 304000<51.4 4640 4760
trans-1,3-Dichloropropene ug/L 4000 110 60-140112 2 304000<78.8 4390 4500
Trichloroethene ug/L 4000 113 60-140115 2 304000<46.4 4500 4590
Trichlorofluoromethane ug/L 4000 108 60-140111 3 304000<67.2 4310 4430
Vinyl chloride ug/L 4000 130 60-140133 3 304000<81.4 5180 5320
Xylene (Total)ug/L 12000 125 60-140128 1 3012000153003040030600
1,2-Dichloroethane-d4 (S)%101 70-130100
4-Bromofluorobenzene (S)%104 70-130103
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 37 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
525983
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92465237003, 92465237004, 92465237005, 92465237006, 92465237009, 92465237010, 92465237011,
92465237012, 92465237013, 92465237014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2811204
Associated Lab Samples:92465237003, 92465237004, 92465237005, 92465237006, 92465237009, 92465237010, 92465237011,
92465237012, 92465237013, 92465237014
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 02/19/20 16:390.42
1,1,1-Trichloroethane ug/L <0.28 0.50 02/19/20 16:390.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 02/19/20 16:390.19
1,1,2-Trichloroethane ug/L <0.23 0.50 02/19/20 16:390.23
1,1-Dichloroethane ug/L <0.24 0.50 02/19/20 16:390.24
1,1-Dichloroethene ug/L <0.22 0.50 02/19/20 16:390.22
1,1-Dichloropropene ug/L <0.35 0.50 02/19/20 16:390.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 02/19/20 16:390.78
1,2,3-Trichloropropane ug/L <0.27 0.50 02/19/20 16:390.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 02/19/20 16:390.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 02/19/20 16:390.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 02/19/20 16:390.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 02/19/20 16:390.23
1,2-Dichlorobenzene ug/L <0.24 0.50 02/19/20 16:390.24
1,2-Dichloroethane ug/L <0.26 0.50 02/19/20 16:390.26
1,2-Dichloropropane ug/L <0.18 0.50 02/19/20 16:390.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 02/19/20 16:390.23
1,3-Dichlorobenzene ug/L <0.25 0.50 02/19/20 16:390.25
1,3-Dichloropropane ug/L <0.34 0.50 02/19/20 16:390.34
1,4-Dichlorobenzene ug/L <0.25 0.50 02/19/20 16:390.25
2,2-Dichloropropane ug/L <0.28 0.50 02/19/20 16:390.28
2-Chlorotoluene ug/L <0.21 0.50 02/19/20 16:390.21
4-Chlorotoluene ug/L <0.21 0.50 02/19/20 16:390.21
Benzene ug/L <0.24 0.50 02/19/20 16:390.24
Bromobenzene ug/L <0.22 0.50 02/19/20 16:390.22
Bromochloromethane ug/L <0.26 0.50 02/19/20 16:390.26
Bromodichloromethane ug/L <0.18 0.50 02/19/20 16:390.18
Bromoform ug/L <0.40 0.50 02/19/20 16:390.40
Bromomethane ug/L <1.7 5.0 02/19/20 16:391.7
Carbon tetrachloride ug/L <0.23 0.50 02/19/20 16:390.23
Chlorobenzene ug/L <0.22 0.50 02/19/20 16:390.22
Chloroethane ug/L <0.58 1.0 02/19/20 16:390.58
Chloroform ug/L <0.35 0.50 02/19/20 16:390.35
Chloromethane ug/L <0.42 1.0 02/19/20 16:390.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 02/19/20 16:390.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 02/19/20 16:390.36
Dibromochloromethane ug/L <0.40 0.50 02/19/20 16:390.40
Dibromomethane ug/L <0.31 0.50 02/19/20 16:390.31
Dichlorodifluoromethane ug/L <0.28 0.50 02/19/20 16:390.28
Diisopropyl ether ug/L <0.33 0.50 02/19/20 16:390.33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2811204
Associated Lab Samples:92465237003, 92465237004, 92465237005, 92465237006, 92465237009, 92465237010, 92465237011,
92465237012, 92465237013, 92465237014
Matrix:Water
AnalyzedMDL
Ethanol ug/L <98.9 200 02/19/20 16:3998.9
Ethyl-tert-butyl ether ug/L <3.8 10.0 02/19/20 16:393.8
Ethylbenzene ug/L <0.24 0.50 02/19/20 16:390.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 02/19/20 16:391.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 02/19/20 16:390.24
m&p-Xylene ug/L <0.44 1.0 02/19/20 16:390.44
Methyl-tert-butyl ether ug/L <0.44 0.50 02/19/20 16:390.44
Methylene Chloride ug/L <1.5 2.0 02/19/20 16:391.5
n-Butylbenzene ug/L <0.35 0.50 02/19/20 16:390.35
n-Propylbenzene ug/L <0.24 0.50 02/19/20 16:390.24
Naphthalene ug/L <0.66 2.0 02/19/20 16:390.66
o-Xylene ug/L <0.24 0.50 02/19/20 16:390.24
sec-Butylbenzene ug/L <0.25 0.50 02/19/20 16:390.25
Styrene ug/L <0.26 0.50 02/19/20 16:390.26
tert-Amyl Alcohol ug/L <40.5 100 02/19/20 16:3940.5
tert-Amylmethyl ether ug/L <3.0 10.0 02/19/20 16:393.0
tert-Butyl Alcohol ug/L <17.6 20.0 02/19/20 16:3917.6
tert-Butyl Formate ug/L <17.8 20.0 02/19/20 16:3917.8
tert-Butylbenzene ug/L <0.25 0.50 02/19/20 16:390.25
Tetrachloroethene ug/L <0.23 0.50 02/19/20 16:390.23
Toluene ug/L <0.23 0.50 02/19/20 16:390.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 02/19/20 16:390.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 02/19/20 16:390.39
Trichloroethene ug/L <0.23 0.50 02/19/20 16:390.23
Trichlorofluoromethane ug/L <0.34 1.0 02/19/20 16:390.34
Vinyl chloride ug/L <0.41 1.0 02/19/20 16:390.41
Xylene (Total)ug/L <0.50 1.0 02/19/20 16:390.50
1,2-Dichloroethane-d4 (S)%99 70-130 02/19/20 16:39
4-Bromofluorobenzene (S)%101 70-130 02/19/20 16:39
Toluene-d8 (S)%102 70-130 02/19/20 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2811205LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.150 110 60-140
1,1,1-Trichloroethane ug/L 54.350 109 60-140
1,1,2,2-Tetrachloroethane ug/L 56.350 113 60-140
1,1,2-Trichloroethane ug/L 55.250 110 60-140
1,1-Dichloroethane ug/L 55.250 110 60-140
1,1-Dichloroethene ug/L 57.250 114 60-140
1,1-Dichloropropene ug/L 52.450 105 60-140
1,2,3-Trichlorobenzene ug/L 55.650 111 60-140
1,2,3-Trichloropropane ug/L 53.650 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2811205LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 57.050 114 60-140
1,2,4-Trimethylbenzene ug/L 58.050 116 60-140
1,2-Dibromo-3-chloropropane ug/L 55.250 110 60-140
1,2-Dibromoethane (EDB)ug/L 57.550 115 60-140
1,2-Dichlorobenzene ug/L 54.350 109 60-140
1,2-Dichloroethane ug/L 54.550 109 60-140
1,2-Dichloropropane ug/L 56.550 113 60-140
1,3,5-Trimethylbenzene ug/L 58.450 117 60-140
1,3-Dichlorobenzene ug/L 57.450 115 60-140
1,3-Dichloropropane ug/L 57.450 115 60-140
1,4-Dichlorobenzene ug/L 53.450 107 60-140
2,2-Dichloropropane ug/L 56.150 112 60-140
2-Chlorotoluene ug/L 57.850 116 60-140
4-Chlorotoluene ug/L 59.250 118 60-140
Benzene ug/L 57.850 116 60-140
Bromobenzene ug/L 53.850 108 60-140
Bromochloromethane ug/L 53.750 107 60-140
Bromodichloromethane ug/L 53.950 108 60-140
Bromoform ug/L 58.050 116 60-140
Bromomethane ug/L 65.850 132 60-140
Carbon tetrachloride ug/L 53.750 107 60-140
Chlorobenzene ug/L 53.850 108 60-140
Chloroethane ug/L 48.850 98 60-140
Chloroform ug/L 54.650 109 60-140
Chloromethane ug/L 47.450 95 60-140
cis-1,2-Dichloroethene ug/L 55.150 110 60-140
cis-1,3-Dichloropropene ug/L 56.150 112 60-140
Dibromochloromethane ug/L 60.050 120 60-140
Dibromomethane ug/L 52.350 105 60-140
Dichlorodifluoromethane ug/L 48.250 96 60-140
Diisopropyl ether ug/L 50.950 102 60-140
Ethanol ug/L 20902000 105 60-140
Ethyl-tert-butyl ether ug/L 102100 102 60-140
Ethylbenzene ug/L 57.450 115 60-140
Hexachloro-1,3-butadiene ug/L 56.450 113 60-140
Isopropylbenzene (Cumene)ug/L 58.750 117 60-140
m&p-Xylene ug/L 119100 119 60-140
Methyl-tert-butyl ether ug/L 53.850 108 60-140
Methylene Chloride ug/L 49.450 99 60-140
n-Butylbenzene ug/L 58.850 118 60-140
n-Propylbenzene ug/L 59.150 118 60-140
Naphthalene ug/L 52.950 106 60-140
o-Xylene ug/L 56.050 112 60-140
sec-Butylbenzene ug/L 58.650 117 60-140
Styrene ug/L 55.250 110 60-140
tert-Amyl Alcohol ug/L 10001000 100 60-140
tert-Amylmethyl ether ug/L 107100 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2811205LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Alcohol ug/L 517500 103 60-140
tert-Butyl Formate ug/L 455400 114 60-140
tert-Butylbenzene ug/L 49.250 98 60-140
Tetrachloroethene ug/L 55.750 111 60-140
Toluene ug/L 56.750 113 60-140
trans-1,2-Dichloroethene ug/L 56.350 113 60-140
trans-1,3-Dichloropropene ug/L 57.050 114 60-140
Trichloroethene ug/L 55.450 111 60-140
Trichlorofluoromethane ug/L 47.950 96 60-140
Vinyl chloride ug/L 59.450 119 60-140
Xylene (Total)ug/L 175150 116 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2811206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465237003
2811207
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 111 60-140114 3 305000<106 5550 5710
1,1,1-Trichloroethane ug/L 5000 121 60-140121 0 305000<69.5 6040 6030
1,1,2,2-Tetrachloroethane ug/L 5000 111 60-140115 4 305000<48.2 5540 5760
1,1,2-Trichloroethane ug/L 5000 115 60-140119 3 305000<58.0 5770 5960
1,1-Dichloroethane ug/L 5000 118 60-140121 3 305000<61.0 5880 6060
1,1-Dichloroethene ug/L 5000 135 60-140137 2 305000<54.5 6740 6860
1,1-Dichloropropene ug/L 5000 121 60-140118 3 305000<87.0 6070 5900
1,2,3-Trichlorobenzene ug/L 5000 104 60-140113 8 305000<195 5200 5630
1,2,3-Trichloropropane ug/L 5000 112 60-140115 2 305000<67.8 5600 5730
1,2,4-Trichlorobenzene ug/L 5000 105 60-140113 7 305000<109 5270 5650
1,2,4-Trimethylbenzene ug/L 5000 114 60-140119 3 305000356092509490
1,2-Dibromo-3-
chloropropane ug/L 5000 106 60-140109 3 305000<96.2 5290 5430
1,2-Dibromoethane (EDB)ug/L 5000 119 60-140121 2 30500071666706780
1,2-Dichlorobenzene ug/L 5000 106 60-140112 5 305000<60.0 5320 5590
1,2-Dichloroethane ug/L 5000 117 60-140117 0 30500020160406050
1,2-Dichloropropane ug/L 5000 118 60-140124 4 305000<45.8 5920 6190
1,3,5-Trimethylbenzene ug/L 5000 120 60-140124 3 30500094269307150
1,3-Dichlorobenzene ug/L 5000 112 60-140118 5 305000<62.5 5580 5880
1,3-Dichloropropane ug/L 5000 116 60-140117 2 305000<85.2 5780 5870
1,4-Dichlorobenzene ug/L 5000 105 60-140109 4 305000<62.2 5250 5460
2,2-Dichloropropane ug/L 5000 117 60-140119 2 305000<70.2 5850 5950
2-Chlorotoluene ug/L 5000 117 60-140126 8 305000<51.8 5840 6300
4-Chlorotoluene ug/L 5000 115 60-140121 5 305000<51.5 5770 6040
Benzene ug/L 5000 124 60-140125 0 305000142002040020500
Bromobenzene ug/L 5000 109 60-140112 2 305000<53.8 5440 5580
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2811206MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465237003
2811207
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromochloromethane ug/L 5000 111 60-140113 2 305000<64.5 5550 5640
Bromodichloromethane ug/L 5000 107 60-140112 5 305000<46.2 5370 5620
Bromoform ug/L 5000 108 60-140113 5 305000<101 5390 5660
Bromomethane ug/L M1500012860-140166 26 305000<430 6400 8280
Carbon tetrachloride ug/L 5000 117 60-140116 1 305000<58.0 5860 5820
Chlorobenzene ug/L 5000 110 60-140112 2 305000<56.2 5490 5610
Chloroethane ug/L 5000 133 60-140125 7 305000<146 6670 6240
Chloroform ug/L 5000 123 60-140120 3 305000<88.2 6170 6020
Chloromethane ug/L 5000 110 60-140111 1 305000<104 5520 5560
cis-1,2-Dichloroethene ug/L 5000 120 60-140122 1 305000<51.8 6010 6080
cis-1,3-Dichloropropene ug/L 5000 114 60-140114 0 305000<89.2 5700 5720
Dibromochloromethane ug/L 5000 115 60-140117 2 305000<100 5730 5840
Dibromomethane ug/L 5000 107 60-140109 2 305000<77.5 5350 5470
Dichlorodifluoromethane ug/L 5000 140 60-140140 0 305000<71.0 7020 7010
Diisopropyl ether ug/L 5000 108 60-140111 2 305000<83.5 5420 5540
Ethanol ug/L 200000 117 60-140119 2 30200000<24700 233000 237000
Ethyl-tert-butyl ether ug/L 10000 107 60-140109 2 3010000<952 10700 10900
Ethylbenzene ug/L 5000 121 60-140123 1 305000294090009090
Hexachloro-1,3-butadiene ug/L 5000 106 60-140116 9 305000<300 5290 5780
Isopropylbenzene
(Cumene)
ug/L 5000 124 60-140128 3 305000<59.5 6190 6380
m&p-Xylene ug/L 10000 122 60-140125 1 3010000134002560025900
Methyl-tert-butyl ether ug/L 5000 113 60-140115 2 305000121J57605870
Methylene Chloride ug/L 5000 113 60-140113 0 305000<375 5630 5650
n-Butylbenzene ug/L 5000 116 60-140121 4 305000<88.2 5800 6040
n-Propylbenzene ug/L 5000 120 60-140124 3 30500036163706580
Naphthalene ug/L 5000 111 60-140108 2 305000103065506440
o-Xylene ug/L 5000 114 60-140119 2 30500061601190012100
sec-Butylbenzene ug/L 5000 118 60-140122 4 305000<61.5 5880 6100
Styrene ug/L 5000 110 60-140114 4 30500088.9J 5600 5800
tert-Amyl Alcohol ug/L 100000 117 60-140121 3 30100000<10100 117000 121000
tert-Amylmethyl ether ug/L 10000 109 60-140111 2 3010000<740 10900 11100
tert-Butyl Alcohol ug/L 50000 113 60-140115 2 3050000<4400 56400 57700
tert-Butyl Formate ug/L 40000 118 60-140120 2 3040000<4450 47000 48100
tert-Butylbenzene ug/L 5000 99 60-140103 4 305000<62.5 4930 5140
Tetrachloroethene ug/L 5000 115 60-140118 2 305000<58.0 5750 5880
Toluene ug/L 5000 100 60-14098 0 305000346003960039500
trans-1,2-Dichloroethene ug/L 5000 127 60-140127 0 305000<64.2 6350 6370
trans-1,3-Dichloropropene ug/L 5000 116 60-140118 2 305000<98.5 5820 5910
Trichloroethene ug/L 5000 118 60-140118 0 305000<58.0 5890 5910
Trichlorofluoromethane ug/L 5000 120 60-140119 1 305000<84.0 6000 5960
Vinyl chloride ug/L M1500014660-140145 0 305000<102 7280 7250
Xylene (Total)ug/L 15000 119 60-140123 1 3015000196003750038000
1,2-Dichloroethane-d4 (S)%101 70-130101
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
526144
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92465237007, 92465237008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2812006
Associated Lab Samples:92465237007, 92465237008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 02/21/20 10:270.42
1,1,1-Trichloroethane ug/L <0.28 0.50 02/21/20 10:270.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 02/21/20 10:270.19
1,1,2-Trichloroethane ug/L <0.23 0.50 02/21/20 10:270.23
1,1-Dichloroethane ug/L <0.24 0.50 02/21/20 10:270.24
1,1-Dichloroethene ug/L <0.22 0.50 02/21/20 10:270.22
1,1-Dichloropropene ug/L <0.35 0.50 02/21/20 10:270.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 02/21/20 10:270.78
1,2,3-Trichloropropane ug/L <0.27 0.50 02/21/20 10:270.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 02/21/20 10:270.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 02/21/20 10:270.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 02/21/20 10:270.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 02/21/20 10:270.23
1,2-Dichlorobenzene ug/L <0.24 0.50 02/21/20 10:270.24
1,2-Dichloroethane ug/L <0.26 0.50 02/21/20 10:270.26
1,2-Dichloropropane ug/L <0.18 0.50 02/21/20 10:270.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 02/21/20 10:270.23
1,3-Dichlorobenzene ug/L <0.25 0.50 02/21/20 10:270.25
1,3-Dichloropropane ug/L <0.34 0.50 02/21/20 10:270.34
1,4-Dichlorobenzene ug/L <0.25 0.50 02/21/20 10:270.25
2,2-Dichloropropane ug/L <0.28 0.50 02/21/20 10:270.28
2-Chlorotoluene ug/L <0.21 0.50 02/21/20 10:270.21
4-Chlorotoluene ug/L <0.21 0.50 02/21/20 10:270.21
Benzene ug/L <0.24 0.50 02/21/20 10:270.24
Bromobenzene ug/L <0.22 0.50 02/21/20 10:270.22
Bromochloromethane ug/L <0.26 0.50 02/21/20 10:270.26
Bromodichloromethane ug/L <0.18 0.50 02/21/20 10:270.18
Bromoform ug/L <0.40 0.50 02/21/20 10:270.40
Bromomethane ug/L <1.7 5.0 02/21/20 10:271.7
Carbon tetrachloride ug/L <0.23 0.50 02/21/20 10:270.23
Chlorobenzene ug/L <0.22 0.50 02/21/20 10:270.22
Chloroethane ug/L <0.58 1.0 02/21/20 10:270.58
Chloroform ug/L <0.35 0.50 02/21/20 10:270.35
Chloromethane ug/L <0.42 1.0 02/21/20 10:270.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 02/21/20 10:270.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 02/21/20 10:270.36
Dibromochloromethane ug/L <0.40 0.50 02/21/20 10:270.40
Dibromomethane ug/L <0.31 0.50 02/21/20 10:270.31
Dichlorodifluoromethane ug/L <0.28 0.50 02/21/20 10:270.28
Diisopropyl ether ug/L <0.33 0.50 02/21/20 10:270.33
Ethanol ug/L <98.9 200 02/21/20 10:2798.9
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2812006
Associated Lab Samples:92465237007, 92465237008
Matrix:Water
AnalyzedMDL
Ethyl-tert-butyl ether ug/L <3.8 10.0 02/21/20 10:273.8
Ethylbenzene ug/L <0.24 0.50 02/21/20 10:270.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 02/21/20 10:271.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 02/21/20 10:270.24
m&p-Xylene ug/L <0.44 1.0 02/21/20 10:270.44
Methyl-tert-butyl ether ug/L <0.44 0.50 02/21/20 10:270.44
Methylene Chloride ug/L <1.5 2.0 02/21/20 10:271.5
n-Butylbenzene ug/L <0.35 0.50 02/21/20 10:270.35
n-Propylbenzene ug/L <0.24 0.50 02/21/20 10:270.24
Naphthalene ug/L <0.66 2.0 02/21/20 10:270.66
o-Xylene ug/L <0.24 0.50 02/21/20 10:270.24
sec-Butylbenzene ug/L <0.25 0.50 02/21/20 10:270.25
Styrene ug/L <0.26 0.50 02/21/20 10:270.26
tert-Amyl Alcohol ug/L <40.5 100 02/21/20 10:2740.5
tert-Amylmethyl ether ug/L <3.0 10.0 02/21/20 10:273.0
tert-Butyl Alcohol ug/L <17.6 20.0 02/21/20 10:2717.6
tert-Butyl Formate ug/L <17.8 20.0 02/21/20 10:2717.8
tert-Butylbenzene ug/L <0.25 0.50 02/21/20 10:270.25
Tetrachloroethene ug/L <0.23 0.50 02/21/20 10:270.23
Toluene ug/L <0.23 0.50 02/21/20 10:270.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 02/21/20 10:270.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 02/21/20 10:270.39
Trichloroethene ug/L <0.23 0.50 02/21/20 10:270.23
Trichlorofluoromethane ug/L <0.34 1.0 02/21/20 10:270.34
Vinyl chloride ug/L <0.41 1.0 02/21/20 10:270.41
Xylene (Total)ug/L <0.50 1.0 02/21/20 10:270.50
1,2-Dichloroethane-d4 (S)%98 70-130 02/21/20 10:27
4-Bromofluorobenzene (S)%100 70-130 02/21/20 10:27
Toluene-d8 (S)%103 70-130 02/21/20 10:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2812007LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.850 112 60-140
1,1,1-Trichloroethane ug/L 53.950 108 60-140
1,1,2,2-Tetrachloroethane ug/L 55.750 111 60-140
1,1,2-Trichloroethane ug/L 54.550 109 60-140
1,1-Dichloroethane ug/L 54.050 108 60-140
1,1-Dichloroethene ug/L 54.950 110 60-140
1,1-Dichloropropene ug/L 56.950 114 60-140
1,2,3-Trichlorobenzene ug/L 54.150 108 60-140
1,2,3-Trichloropropane ug/L 50.850 102 60-140
1,2,4-Trichlorobenzene ug/L 55.550 111 60-140
1,2,4-Trimethylbenzene ug/L 53.850 108 60-140
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2812007LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 60.650 121 60-140
1,2-Dibromoethane (EDB)ug/L 55.050 110 60-140
1,2-Dichlorobenzene ug/L 54.750 109 60-140
1,2-Dichloroethane ug/L 49.350 99 60-140
1,2-Dichloropropane ug/L 55.550 111 60-140
1,3,5-Trimethylbenzene ug/L 54.950 110 60-140
1,3-Dichlorobenzene ug/L 56.850 114 60-140
1,3-Dichloropropane ug/L 54.250 108 60-140
1,4-Dichlorobenzene ug/L 52.450 105 60-140
2,2-Dichloropropane ug/L 59.350 119 60-140
2-Chlorotoluene ug/L 55.450 111 60-140
4-Chlorotoluene ug/L 55.750 111 60-140
Benzene ug/L 53.450 107 60-140
Bromobenzene ug/L 55.050 110 60-140
Bromochloromethane ug/L 56.150 112 60-140
Bromodichloromethane ug/L 53.150 106 60-140
Bromoform ug/L 49.050 98 60-140
Bromomethane ug/L 47.650 95 60-140
Carbon tetrachloride ug/L 54.550 109 60-140
Chlorobenzene ug/L 51.750 103 60-140
Chloroethane ug/L 45.650 91 60-140
Chloroform ug/L 53.750 107 60-140
Chloromethane ug/L 47.750 95 60-140
cis-1,2-Dichloroethene ug/L 53.750 107 60-140
cis-1,3-Dichloropropene ug/L 57.550 115 60-140
Dibromochloromethane ug/L 56.450 113 60-140
Dibromomethane ug/L 53.650 107 60-140
Dichlorodifluoromethane ug/L 54.050 108 60-140
Diisopropyl ether ug/L 56.850 114 60-140
Ethanol ug/L 21202000 106 60-140
Ethyl-tert-butyl ether ug/L 103100 103 60-140
Ethylbenzene ug/L 51.350 103 60-140
Hexachloro-1,3-butadiene ug/L <1.2 L250160-140
Isopropylbenzene (Cumene)ug/L 53.850 108 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 54.150 108 60-140
Methylene Chloride ug/L 51.250 102 60-140
n-Butylbenzene ug/L 57.650 115 60-140
n-Propylbenzene ug/L 55.750 111 60-140
Naphthalene ug/L 54.650 109 60-140
o-Xylene ug/L 51.650 103 60-140
sec-Butylbenzene ug/L 55.950 112 60-140
Styrene ug/L 54.550 109 60-140
tert-Amyl Alcohol ug/L 10801000 108 60-140
tert-Amylmethyl ether ug/L 106100 106 60-140
tert-Butyl Alcohol ug/L 486500 97 60-140
tert-Butyl Formate ug/L 458400 115 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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Page 45 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2812007LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 45.150 90 60-140
Tetrachloroethene ug/L 51.250 102 60-140
Toluene ug/L 50.850 102 60-140
trans-1,2-Dichloroethene ug/L 54.650 109 60-140
trans-1,3-Dichloropropene ug/L 50.550 101 60-140
Trichloroethene ug/L 50.950 102 60-140
Trichlorofluoromethane ug/L 50.850 102 60-140
Vinyl chloride ug/L 63.350 127 60-140
Xylene (Total)ug/L 155150 103 60-140
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2812008MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465477001
2812009
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 117 60-140120 3 30200ND234240
1,1,1-Trichloroethane ug/L 200 115 60-140120 4 30200ND230240
1,1,2,2-Tetrachloroethane ug/L 200 119 60-140119 0 30200ND238239
1,1,2-Trichloroethane ug/L 200 119 60-140119 0 30200ND238239
1,1-Dichloroethane ug/L 200 116 60-140121 4 30200ND232241
1,1-Dichloroethene ug/L 200 119 60-140124 4 30200ND237248
1,1-Dichloropropene ug/L 200 120 60-140126 5 30200ND239252
1,2,3-Trichlorobenzene ug/L 200 111 60-140113 2 30200ND222226
1,2,3-Trichloropropane ug/L 200 96 60-14099 3 30200ND193198
1,2,4-Trichlorobenzene ug/L 200 111 60-140112 1 30200ND222223
1,2,4-Trimethylbenzene ug/L E20012160-140119 0 30200199022302230
1,2-Dibromo-3-
chloropropane ug/L 200 119 60-140122 2 30200ND239243
1,2-Dibromoethane (EDB)ug/L 200 112 60-140116 4 30200ND224232
1,2-Dichlorobenzene ug/L 200 116 60-140116 0 30200ND231232
1,2-Dichloroethane ug/L 200 105 60-140110 4 30200ND210219
1,2-Dichloropropane ug/L 200 120 60-140124 3 30200ND240247
1,3,5-Trimethylbenzene ug/L M120015660-140157 0 30200490802805
1,3-Dichlorobenzene ug/L 200 117 60-140118 0 30200ND234235
1,3-Dichloropropane ug/L 200 114 60-140116 2 30200ND227232
1,4-Dichlorobenzene ug/L 200 111 60-140114 2 30200ND223227
2,2-Dichloropropane ug/L 200 83 60-14093 12 30200ND166187
2-Chlorotoluene ug/L M120017160-140172 1 30200ND341344
4-Chlorotoluene ug/L 200 107 60-140106 0 30200ND213213
Benzene ug/L 200 119 60-140122 2 3020033.6 272 278
Bromobenzene ug/L 200 118 60-140118 0 30200ND237237
Bromochloromethane ug/L 200 118 60-140124 4 30200ND237248
Bromodichloromethane ug/L 200 112 60-140116 4 30200ND225233
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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Huntersville, NC 28078
[phone]
Page 46 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2812008MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465477001
2812009
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromoform ug/L 200 97 60-14099 1 30200ND195197
Bromomethane ug/L 200 100 60-140120 19 30200ND199241
Carbon tetrachloride ug/L 200 120 60-140124 4 30200ND239248
Chlorobenzene ug/L 200 116 60-140117 0 30200ND233234
Chloroethane ug/L 200 127 60-140133 5 30200ND253266
Chloroform ug/L 200 115 60-140117 2 30200ND229233
Chloromethane ug/L 200 99 60-14098 1 30200ND199196
cis-1,2-Dichloroethene ug/L 200 114 60-140119 5 30200ND227237
cis-1,3-Dichloropropene ug/L 200 111 60-140117 5 30200ND222234
Dibromochloromethane ug/L 200 114 60-140119 4 30200ND228238
Dibromomethane ug/L 200 116 60-140118 2 30200ND231236
Dichlorodifluoromethane ug/L 200 118 60-140120 2 30200ND235240
Diisopropyl ether ug/L 200 116 60-140118 2 30200ND233238
Ethanol ug/L 8000 111 60-140117 5 308000ND89009360
Ethyl-tert-butyl ether ug/L 400 103 60-140107 4 30400ND410427
Ethylbenzene ug/L 200 112 60-140114 0 30200545770773
Hexachloro-1,3-butadiene ug/L 200 109 60-140111 2 30200ND217221
Isopropylbenzene
(Cumene)ug/L 200 118 60-140121 2 3020076.8 313 318
m&p-Xylene ug/L 400 98 60-140107 1 30400262030103040
Methyl-tert-butyl ether ug/L 200 107 60-140110 3 30200ND214220
Methylene Chloride ug/L 200 112 60-140117 4 30200ND224234
n-Butylbenzene ug/L M120013860-140141 3 30200ND276283
n-Propylbenzene ug/L 200 113 60-140118 2 30200218444455
Naphthalene ug/L 200 112 60-140117 3 30200160384394
o-Xylene ug/L 200 108 60-140112 0 30200146016801680
sec-Butylbenzene ug/L 200 111 60-140112 1 30200ND221223
Styrene ug/L 200 120 60-140123 2 30200ND241246
tert-Amyl Alcohol ug/L 4000 116 60-140115 1 304000ND46404600
tert-Amylmethyl ether ug/L 400 112 60-140113 1 30400ND448453
tert-Butyl Alcohol ug/L M1200013460-140145 7 302000191J28803090
tert-Butyl Formate ug/L M116002860-14029 6 301600ND440466
tert-Butylbenzene ug/L 200 95 60-14094 1 30200ND190188
Tetrachloroethene ug/L 200 110 60-140115 4 30200ND220230
Toluene ug/L 200 117 60-140117 0 3020066.5 300 300
trans-1,2-Dichloroethene ug/L 200 115 60-140120 5 30200ND229240
trans-1,3-Dichloropropene ug/L 200 96 60-140102 6 30200ND192204
Trichloroethene ug/L 200 112 60-140114 2 30200ND224229
Trichlorofluoromethane ug/L 200 110 60-140114 4 30200ND220229
Vinyl chloride ug/L M120013960-140143 2 30200ND278285
Xylene (Total)ug/L 600 102 60-140109 1 30600407046804730
1,2-Dichloroethane-d4 (S)%100 70-130104
4-Bromofluorobenzene (S)%99 70-13099
Toluene-d8 (S)%104 70-130102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
526570
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples:92465237009, 92465237011, 92465237013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2813989
Associated Lab Samples:92465237009, 92465237011, 92465237013
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L <0.011 0.020 02/23/20 23:530.011
1-Chloro-2-bromopropane (S)%95 70-130 02/23/20 23:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2813990LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2813991
1,2-Dibromoethane (EDB)ug/L 0.240.26 96 70-1301010.25 3 20
1-Chloro-2-bromopropane (S)%97 70-130100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2813992MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92464936003
2813993
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L M10.25 56 65-13561 8 200.25ND 0.14 0.15
1-Chloro-2-bromopropane
(S)
%S25770-13063
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92464936004
2813994SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L <0.011 20ND
1-Chloro-2-bromopropane (S)%9380
REPORT OF LABORATORY ANALYSIS
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Page 48 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
526734
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples:92465237010, 92465237012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2814806
Associated Lab Samples:92465237010, 92465237012
Matrix:Water
AnalyzedMDL
1,2-Dibromoethane (EDB)ug/L <0.011 0.020 02/24/20 19:250.011
1-Chloro-2-bromopropane (S)%110 70-130 02/24/20 19:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2814807LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2814808
1,2-Dibromoethane (EDB)ug/L 0.230.25 94 70-1301100.27 17 20
1-Chloro-2-bromopropane (S)%92 70-130108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2814809MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92465067020
2814810
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.24 97 65-13595 4 200.24ND 0.23 0.22
1-Chloro-2-bromopropane
(S)
%102 70-130100
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92464963001
2814811SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L <0.011 20ND
1-Chloro-2-bromopropane (S)%105108
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 49 of 56
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 50 of 56
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92465237
WILLIAM'S GROCERY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92465237009 526570 526587WSW-1 EPA 504.1 EPA 504.1
92465237010 526734 526762WSW-2 EPA 504.1 EPA 504.1
92465237011 526570 526587WSW-5 EPA 504.1 EPA 504.1
92465237012 526734 526762WSW-7 EPA 504.1 EPA 504.1
92465237013 526570 526587WSW-9 EPA 504.1 EPA 504.1
92465237001 525880MW-1 SM 6200B
92465237002 525880MW-2 SM 6200B
92465237003 525983MW-3 SM 6200B
92465237004 525983MW-4 SM 6200B
92465237005 525983MW-5 SM 6200B
92465237006 525983MW-6 SM 6200B
92465237007 526144MW-12 SM 6200B
92465237008 526144RW-1 SM 6200B
92465237009 525983WSW-1 SM 6200B
92465237010 525983WSW-2 SM 6200B
92465237011 525983WSW-5 SM 6200B
92465237012 525983WSW-7 SM 6200B
92465237013 525983WSW-9 SM 6200B
92465237014 525983FB-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/25/2020 04:03 PM
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