Loading...
HomeMy WebLinkAboutWS-4439_14407_CA_MRP_20230531_LSA A CONSULTECH ENVIRONMENTAL, LLC. P.O.Box 5306, Cary, NC 27512 (919) 234-4238, (919) 234-4239 Fax May 31, 2023 North Carolina Department of Environmental Quality Division of Waste Management, UST Section 1628 Mail Service Center Raleigh, NC 27699-1628 Attention: Mr. Scott Ryals Reference: Limited Site Assessment Report Former Cedarock Baptist Mission 6061 S. Highway 49 Burlington, Alamance County, NC Incident Nos: 14407 Dear Mr. Ryals: Please find attached a Limited Site Assessment report for the above referenced facility. Please contact the undersigned if you have any questions or comments regarding the report. Respectively, Consultech Environmental, LLC. John D. Liebig Project Manager B CONSULTECH ENVIRONMENTAL, LLC. P.O.Box 5306, Cary, NC 27512 (919) 234-4238, (919) 234-4239 Fax Prepared by: Consultech Environmental, LLC. 2021 Energy Drive Apex, NC 27502 May 31, 2023 LIMITED SITE ASSESSMENT REPORT Former Cedarock Baptist Mission 6061 South Highway 49 Burlington, Alamance County, North Carolina NCDEQ Incident No: 14407 i 2. Contact Information UST Owner/Operator: Address: Cedarock Baptist Mission PO Box 353 Graham, NC 27253 Tel: (336) 229-0699 Property Owner: Travis Graves 4824 Friendship Rock Creek Road Burlington, NC 27215 Consultant/Contractor: Consultech Environmental, LLC. Address: Tel: 2021 Energy Drive Apex, NC 27502 (919) 234-4238 Analytical Laboratory: Eurofins Test America. Cert # 314 Address: Tel: 3355 McLemore Drive Pensacola, FL 32514 (854) 474-1001 3. Information about Release Date Discovered: 5/3/1990 Estimated Quantity of Release: Unknown Cause of Release: USTs Source of Release (Dispenser/Piping/UST): Unknown Size and Contents of UST System(s) from which the release occurred: 1 2,000-gallon gasoline, 1 550-gallon kerosene, 1 550-gallon gasoline, 1 1,000-gallon gasoline Criteria Used to Classify Risk Water supply well within 1,000 ft of confirmed release 4. Certification Certification: Jeffrey L. Gerlock, L.G. I, ___________________, a Licensed Geologist (#1141) with Consultech Environmental, LLC, do certify that the information contained in this report is correct and accurate to the best of my knowledge. Consultech Environmental, LLC is licensed to practice geology in the State of North Carolina. Consultech Environmental, LLC currently holds North Carolina Corporate Geology license number C-0497. A SITE INFORMATION 1. Site Identification Former Cedarock Baptist Misiion 6061 South Highway 49 Burlington, Alamance County, North Carolina Date of Report: May 31, 2023 Facility I.D.: UST Incident No.: 14407 Site Risk: High Land Use Classification: Commercial Site Name (NCDEQ Incident Name): Former Cedarock Baptist Mission Site Street Address: 6061 South Highway 49 City/Town: Burlington Zip Code: 27215 County: Alamance Description of Geographical Data Point: Approximate center of property Location Method: Google Earth Latitude (decimal degrees): N 36.975200 Longitude (decimal degrees): W 78.465100 ii B EXECUTIVE SUMMARY The following Limited Site Assessment (LSA) report has been prepared by Consultech Environmental, LLC. (Consultech) for the Former Cedarock Baptist Mission (site) located at 6061 South NC Highway 49 in Burlington, North Carolina. This LSA has been prepared to address the release of petroleum hydrocarbon compounds from an underground storage tank (UST) system that was located on the site. The site previously contained one 2,000-gallon gasoline UST, one 550-gallon kerosene UST, one 550-gallon gasoline UST, and one 1,000-gallon gasoline UST. All four USTs were removed from the site on April 4, 1990. The release was assigned Incident number 14407 by the North Carolina Department of Environmental Quality (NCDEQ), UST Section. The results of the LSA are summarized below: Type of Contaminant Gasoline, kerosene Source of Release UST Tanks Amount of Release Unknown Initial Abatement/Emergency Response Information None Hydrogeology Groundwater was encountered at a depth of 35 feet below ground surface Soil and Groundwater Assessment Soil samples collected during UST closure indicated TPH concentrations above action levels. No petroleum constituents were detected during the current LSA at concentrations above the current North Carolina Department of Environmental Quality (NCDEQ), Division of Waste Management (DWM) UST Section regulatory standards (MSCCs). No petroleum constituents were detected in monitoring well MW-1 at concentrations above the 2L groundwater quality standards. Risk Classification The site should be classified as high risk due to the presence of a water supply well within 1,000 feet of a confirmed release. Current Soil and Groundwater Remediation Standards Soil: Soil to Groundwater MSCC. Groundwater: North Carolina Administrative Code, Title 15A, Department of Environmental Quality, Subchapter 2L, Classifications and Water Quality Standards Applicable to the Groundwaters of North Carolina, Revised April 1, 2023 (NC 2L groundwater standards). Recommendations No Further Action iii C TABLE OF CONTENTS A SITE INFORMATION ............................................................................................ I B EXECUTIVE SUMMARY ...................................................................................... II C TABLE OF CONTENTS ...................................................................................... III D SITE HISTORY AND SOURCE CHARACTERIZATION ...................................... 4 D.1 OWNER-OPERATOR INFORMATION ................................................................................ 4 D.2 UST SYSTEM INFORMATION .......................................................................................... 4 D.3 NON-UST INFORMATION ............................................................................................... 4 D.4 PREVIOUS SITE ASSESSMENT ACTIVITY......................................................................... 4 D.5 SITE AND VICINITY CHARACTERISTICS (LAND USE OF THE SITE AND SURROUNDING AREA, TOPOGRAPHY, VEGETATION, SURFACE WATER, WELLS, BUILDINGS, SURFACE COVER, SOIL TYPE, DEPTH TO AND NATURE OF BEDROCK, DEPTH TO GROUNDWATER, DIRECTION OF GROUNDWATER FLOW). ................................................................................................. 4 D.6 SUMMARY OF ABATEMENT ACTIONS, ASSESSMENT REPORTS AND CORRECTIVE ACTIONS4 E RISK CHARACTERIZATION ............................................................................... 4 F RECEPTOR INFORMATION ............................................................................... 7 F.1 WATER SUPPLY WELLS ................................................................................................ 7 F.2 PUBLIC WATER SUPPLIES ............................................................................................ 7 F.3 SURFACE WATER ......................................................................................................... 7 F.4 WELLHEAD PROTECTION AREAS ................................................................................... 7 F.5 DEEP AQUIFERS OF THE COASTAL PLAIN PHYSIOGRAPHIC PROVINCE ............................ 7 F.6 SUBSURFACE STRUCTURES .......................................................................................... 7 G LAND USE ........................................................................................................... 7 G.1 PROPERTY OWNERS AND OCCUPANTS .......................................................................... 7 H SITE GEOLOGY AND HYDROGEOLOGY .......................................................... 7 I SAMPLING RESULTS ......................................................................................... 7 J CONCLUSIONS AND RECOMMENDATIONS .................................................... 8 TABLES Table 1 Receptor Information Table 2 Property Owners/Occupants Table 3 Soil Analytical Results Table 4 Groundwater Analytical Results FIGURES Figure 1 Project Location Map Figure 2 Site Map Figure 3 Receptor Map LIST OF APPENDICES APPENDIX A Laboratory Analytical Reports APPENDIX B Monitoring Well Completion Record 4 D SITE HISTORY AND SOURCE CHARACTERIZATION The site is located at 6061 South NC Highway 49 in Burlington, North Carolina. The property location is shown on Figure 1. D.1 Owner-Operator Information The UST system owner is Cedarock Baptist Mission. D.2 UST System Information The site previously contained one 2,000-gallon gasoline UST, one 550-gallon kerosene UST, one 550-gallon gasoline UST, and one 1,000-gallon gasoline UST. D.3 Non-UST Information No information was found in the conductance of the LSA that indicated the presence of aboveground storage tanks. D.4 Previous Site Assessment Activity Soil samples collected during UST closure indicated TPH concentrations above action levels. No additional previous site assessment activities were performed. D.5 Site and Vicinity Characteristics (land use of the site and surrounding area, topography, vegetation, surface water, wells, buildings, surface cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow). The site is located at 6061 South NC Highway 49. The site is currently a Baptist church. The site contains a large church building, two outbuildings, and gravel parking lot. The site is surrounded by commercial and residential properties and bounded to the southeast by NC Highway 49 and to the southwest by Spanish Oak Hill Road. Topography in the region slopes moderately to the southeast. The site property and all surrounding properties utilize groundwater for drinking purposes. Surrounding property use can be seen on Figure 3. D.6 Summary of Abatement Actions, Assessment Reports and Corrective Actions No previous abatement actions are known to have occurred. A letter dated May 1, 1990 was submitted to NCDEQ by the Cedarock Baptist Mission reporting results of the soil sampling conducted during UST closure. No corrective actions have been performed. E RISK CHARACTERIZATION Limited Site Assessment Risk Classification and Land Use Form Part I – Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non- drinking purposes? NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? YES 3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release? NO 5 4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there is no other source of water supply other than the groundwater)? YES 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? NO If yes, describe. Not applicable. 6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the environment? NO If yes, describe. Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release? NO If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? 8. Is the source area of the release located within an approved or planned wellhead protection area as defined in 42 USC 300h-7(e)? NO If yes, describe. Not applicable. 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of North Carolina” published by the Department in 1985? NO If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water? No 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established by the Department? NO Part II - Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO Describe. Not applicable 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? YES Describe. The property is currently used as a church. 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? NO 6 Describe. 4. Do children visit the property? YES Explain. Children visit the church. 5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? NO Explain. 6. Do pavement, buildings, or other structures cap the contaminated soil? NO Describe. The former USTs were located in a grassy lawn. If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? 7. What is the zoning status of the property? Commercial 8. Is the use of the property likely to change in the next 20 years? NO Explain. Based on the site location, the site will likely remain a church, however, it cannot be determined at this time what use will occur over the next 20 years. Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source area of the release): 1. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? 185 feet southeast of the center of the former UST location. 2. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? Living Word Missionary Baptist Church is located on the site property. 3. What is the zoning status of properties in the surrounding area? • West: Not zoned • North: Residential • East: Residential • South: Not zoned 4. Briefly characterize the use and activities of the land in the surrounding area. Surrounding properties are utilized for both residential and commercial purposes. Residences are located northeast and southeast of the site. Land use and property owners/occupant information is Included in Table 2. 7 F RECEPTOR INFORMATION F.1 Water Supply Wells Fifteen water supply wells were identified within 1500 feet of the former UST basin. F.2 Public Water Supplies The site and vicinity properties utilize groundwater for drinking purposes. Water supply well information is contained in Table 1 and Figure 3. F.3 Surface Water No surface water is located within 1500 feet from the site. F.4 Wellhead Protection Areas Wellhead Protection Areas are administered by the North Carolina Division of Environmental Quality, Public Water Supply (PWS) Section. According to the PWS, no Wellhead Protection Areas are located within 1,500 feet of the source area. F.5 Deep Aquifers of the Coastal Plain Physiographic Province The site property is not located in the Coastal Plain Physiographic Province. F.6 Subsurface Structures There is no basement at the site buildings. Utilities are located along NC Highway 49. The utilities included natural gas lines and aboveground power and communication lines. The utilities are located outside of the former UST location. G LAND USE G.1 Property Owners and Occupants The site is used as the Living Word Missionary Baptist Church. A list of the adjacent property owners is Included in Table 2. H SITE GEOLOGY AND HYDROGEOLOGY According to the 1985 Geologic Map of North Carolina, the site is located in the Piedmont Physiographic Province. Underlying geology consists of megacrystic, well foliated metamorphosed granitic rock. Soil encountered at the site consisted of a light brown silty clay to 35 feet with a saturated gravel layer encountered at 35 feet. Based on the topography, groundwater is expected to flow southeast from the site. I SAMPLING RESULTS On March 2, 2023, Ground Zero Environmental, Inc. drilled one soil boring (MW-1) within the former UST location. The boring was drilled using hollow stem augers to a depth of 13 feet, where auger refusal was encountered. The soil boring location is shown in Figure 2. Soil samples were collected from MW-1 at five-foot intervals (5 and 10 feet). The soil samples were placed into appropriate laboratory- supplied containers, the samples were then placed on ice, and shipped under chain-of-custody to Eurofins Environment Testing in Pensacola, FL for analysis for volatile organic compounds (VOCs) by EPA Method 8260, semivolatile organic 8 compounds (SVOCs), extractable petroleum hydrocarbons (EPH), and volatile petroleum hydrocarbons (VPH) by the MADEP method. Minor concentrations of acetone and toluene were detected in the two soil samples; these constituents were detected at concentrations below applicable soil to water MSCCs. No other contaminant concentrations were detected above laboratory detection limits. Soil analytical data is summarized in Table 3 while the soil laboratory analytical report is contained in Appendix A. On April 17, 2023, South Atlantic Environmental Drilling and Construction Company (SAEDACCO) drilled and installed a monitoring well (MW-1) to a total depth of 38 feet using air rotary techniques. A groundwater sample was collected from MW-1 on April 19, 2023. The samples were placed into appropriate laboratory- supplied containers, the samples were then placed on ice, and shipped under chain-of-custody to Eurofins Environment Testing in Pensacola, FL for analysis for VOCs by EPA Method 8260, SVOCs by EPA Method 625.1, EPH/VPH by the MADEP method, and lead by USEPA Method 6010D. A summary of groundwater analytical data indicates estimated concentrations of benzene and phenol of 0.290 and 1.27 micrograms per liter (ug/L), respectively. No exceedances of NCAC 2L groundwater quality standards for any contaminants were detected. Groundwater analytical data is summarized in Table 4 while the groundwater laboratory analytical report is contained in Appendix A. The monitoring well location is shown in Figure 2. A well completion form is contained in Appendix B. J CONCLUSIONS AND RECOMMENDATIONS The following conclusions were reached regarding the release from the Former West End Service Station: • The site previously contained one 2,000-gallon gasoline UST, one 550-gallon kerosene UST, one 550-gallon gasoline UST, and one 1,000-gallon gasoline UST which were removed on April 4, 1990. • Soil samples collected during UST closure indicated TPH concentrations above action levels. • The site property and surrounding properties utilize groundwater for drinking purposes. • Low concentrations of acetone and toluene were detected in soil samples collected at five and ten feet in the tank basin; these constituents were detected at concentrations below applicable soil to water MSCCs. • Low levels of benzene and phenol were detected in the groundwater in well MW-1 installed in the tank basin. No constituents were detected in the groundwater in well MW-1 at concentrations above the NCAC 2L groundwater quality standards. • Consultech recommends the incident be assigned a No Further Action status. TABLES Revision Date 5/24/23 Incident Number / Name:14407/Former Cedarock Baptist Mission Public and Private Water Supply Wells WSW-1 Travis Graves/ Living World Baptist Church 6061 S NC HWY 49 336-266-0460 35.97489, -79.46521 Water for church 50 Up WSW-2 Richard Strader 6043 S NC HWY 49 35.97557, -79.46482 200 Down WSW-3 David Albright 6062 S NC HWY 49 35.97509, -79.46434 200 Down WSW-4 Coty and LindaBlalock 6033 S NCHWY 49 35.97579,-79.46455 350 Down WSW-5 Russell Lampron 6025 S NC HWY 49 603-724-5768 35.97603, -79.46438 Drinking/b athing ~90 450 Down WSW-6 Randall Murray 6145 S NCHWY 49 336-516-5600 35.97382,-79.46712 Drinking/bathing ~60'750 Down WSW-7 Shaun Greeson 5965 S NC HWY 49 35.97695, -79.46358 850 Down WSW-8 David Greeson 5963 S NC HWY 49 336-263-7460 35.97746, -79.46421 Drinking/b athing 980 Down WSW-9 Tanner Greeson 5959 S NC HWY 49 35.97786, -79.46381 1100 Down WSW-10 Ityra Robinson 5955 S NC HWY 49 35.97739, -79.46307 1100 Down WSW-11 Billy Coleman 5952 S NC HWY 49 35.97706 , -79.46235 1100 Down WSW-12 Leonard and ChristinaRobertson 5923 S NCHWY 49 35.97797,-79.46255 1300 Down WSW-13 Wanda Murray 6211 S NCHWY 49 35.97179,-79.46759 1350 Down WSW-14 Paul Kivett 5930 S NC HWY 49 336-263-0030 35.97788, -79.46176 Bathing only 1400 Down WSW-15 Christopher and Jamie Murray 6225 S NC HWY 49 35.97183, -79.4676 1450 Down UK: Unknown Receptor ID DescriptionLatitude/Longitudeofanysignificantpoint(s)*PhoneNumberUsageDistancefromsourceareaofrelease(ft.)Upordown-gradientNotes:Receptor distances were obtained from Google Earth and were approximated from the center of the former UST basin. Latitude and longitude obtained from field measurements, Alamance County GIS, or Google Earth. Table 1 Receptor Information Former Cedarock Baptist Mission 6061 S NC HWY 49 Burlington, Alamance County, North Carolina No other receptors were identified within 1500' of the site UpordowngradientOther Receptors (Public water supplies, reservoirs, supply lines, surface water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface structures)WellUseWellDepth(ftBGS)TypeofWellWellCasingDepth(ft.BGS)WellScreenIntervalDistancefromsourceareaofrelease(ft.)Receptor ID WellOwner/UserAddressPhoneNumberLatitude/Longitude Revision Date 5/24/23 Incident Number / Name: 14407/Former Cedarock Baptist Mission Tax Parcel Number/ Map ID Owner/ Occupant Name Property Address Owner Address 119491 Donald and Joyce Johnson 2707 SPANISH OAK HILL RD 4605 GALLANT LN WINSTON SALEM, NC 27101 119511 Richard Strader 6043 S NC HWY 49 6043 SOUTH NC HWY 49 BURLINGTON, NC 27215 119237 Randall Murray S NC HWY 49 STEWART,TRUSTEE 7707 JEFFERSON CIRCLE COLLEYVILLE, TX 76034 119280 David Albright 6062 S NC 49 HWY 6062 SOUTH NC HWY 49 BURLINGTON, NC 27215 119257 Debra Albright 6044 S NC 49 HWY 1935 DELAINE DR BURLINGTON, NC 27215 Table 2 Adjacent Property Owners/Occupants Former Cedarock Baptist Mission 6061 S NC HWY 49 Burlington, Alamance County, North Carolina SampleSampleDepth(ft)DateSampledTPH5030 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8270 8270 8270 8270 8270 8270 EPH EPH EPH VPH VPH VPH MW-1 5 3/2/2023 NS 0.157 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-1 10 3/2/2023 NS 0.0503 ND 0.00135 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND SS #1 NA 4/5/1990 <10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS SS #2 NA 4/5/1990 <10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS SS #3 NA 4/5/1990 55 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS SS #4 NA 4/5/1990 <10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA 24 0.0072 5.4 8 6 0.2 6.6 6.6 1.3 0.023 0.085 0.054 1.5 0.2 55 64 640 540 NS 31 68 540 NS NA 14000 12 1250 60.3 3120 5.5 156 156 1560 93.8 156 22.8 62.5 5.5 625 469 4600 1650 31200 469 625 1650 469 Notes:Analytical results reported in mg/kg ND: Compound not detected above laboratory detection limit. NA: No Standard NS: Not sampled J: Estimated concentration above MDL but below RL Bold Values indicate concentrations above Soil to Water MSCC Soil to Water MSCC Residential Soil Cleanup Levels Table 3 Soil Analytical Data Former Cedarock Baptist Mission 6061 S NC HWY 49, Burlington, Alamance County, North Carolina 1-Methylnaphthalene2-MethylnaphthaleneC9-C10AromaticsAnalytical Method -> Contaminant of Concern ->C5-C8AliphaticsC9-C12AliphaticsC19-C36AliphaticsC11-C22AromaticsBenzeneC9-C18AliphaticsNaphthaleneAcetoneIsopropylbenzeneEthylbenzeneTolueneXylenesMethyleneChlorideMTBEAnthraceneFluorenePhenanthrene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneNaphthalene SampleLocationDateSampled6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 6200B 625 625 625 625 625 625 625 625 625 625 6010D VPH VPH VPH EPH EPH EPH MW-2 4/19/2023 0.290 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.27 J 0.044 ND ND ND ND ND ND 1 70 600 70 70 20 6 600 400 400 500 0.005 0.05 200 0.5 NS NS NS 1 30 30 15 400 700 200 700 10000 200 5000 70000 84500 25000 70000 20000 6000 260000 28500 25000 85500 0.8 0.75 200 0.5 NS NS NS 1000 12000 30000 15000 NS NS NS NS NS NS Notes:Analytical results reported in ug/L. ND: Compound not detected above laboratory detection limit. NS No standard. J indicates estimated concentration above MDL but below RL 1-MethylnaphthaleneToluene1,2,4-TrimethylbenzeneC9-C10AromaticsC9-C18AliphaticsC19-C36AliphaticsC11-C22AromaticsGW Gross Contaminant Levels Di-n-butylphthalateAnalytical Method -> NC 2L GW Standard C5-C8Aliphatics2-MethylnaphthalenePhenolLeadBenzo[b]fluorantheneBenzo[g,h,i]peryleneBenzo[k]fluorantheneDiethylphthalateDimethylphthalateTable 4Groundwater Analytical DataFormer Cedarock Baptist Mission 6061 S NC HWY 49, Burlington, Alamance County, North Carolina Contaminant of Concern ->BenzeneChloroformEthylbenzeneIsopropylbenzene1,3,5-TrimethylbenzeneXylenes(Total)Benzo[a]pyreneIsopropylEtherMTBENaphthaleneC9-C12Aliphatics FIGURES Approximate Scale 1” = 1,000’ 500’ 1978 Snow Camp, NC 7.5’ USGS Topographic Map Site Location Map Former Cedarock Baptist Mission Incident (#14407) 6061 S NC HWY 49, Burlington, Alamance County, NC Consultech Environmental, LLC 2021 Energy Drive, Apex, NC 27502 Compiled By: ZAB Figure No: 1 Checked By: RBS Date: May 15, 2023 SITE N Approximate Scale 1” = 50’ 25’ Google Earth 2018 Site Map Former Cedarock Baptist Mission Incident (#14407) 6061 S NC HWY 49, Burlington, Alamance County, NC Consultech Environmental, LLC 2021 Energy Drive, Apex, NC 27502 Compiled By: ZAB Figure No: 2 Checked By: RBS Date: May 12, 2023 Map Key Well Location Previous Soil Sample Locations MW-1 Overhead Utility Lines SS #1 SS #2 SS #4 SS #3 NC Highway 49 Spanish Oak Hill Road Approximate Scale 1” = 600 400 Alamance County GIS Receptor Map Former Cedarock Baptist Mission Incident (#14407) 6061 S NC HWY 49, Burlington, Alamance County, NC Consultech Environmental, LLC 2021 Energy Drive Apex, NC 27502 Drawn By: ZAB Figure No: 3 Checked By: RBS Date: April 24, 2023 N WSW-1 WSW-2 WSW-3 WSW-4 WSW-5 WSW-6 WSW-13 WSW-15 WSW-6 WSW-7 WSW-8 WSW-9 WSW-10 WSW-12 WSW-14 WSW-11 APPENDIX A Laboratory Analytical Reports ANALYTICAL REPORT PREPARED FOR Attn: Raj Shah Consultech Environmental LLC 2021 Energy Drive Apex, North Carolina 27502 Generated 3/14/2023 6:23:17 PM JOB DESCRIPTION Former Cedar Rock Baptist Misson JOB NUMBER 400-234011-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 40 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and relate only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without written approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on this page, or the telephone number at the bottom of the page. Eurofins Environment Testing Southeast LLC, Pensacola Certifications and Approvals: Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida (E81010), Illinois (200041), Iowa (367), Kansas (E-10253), Kentucky UST (53), Louisiana (30748), Maryland (233), Massachusetts (M-FL094), Michigan (9912), New Hampshire (250510), New Jersey (FL006), North Carolina (314), Oklahoma (9810), Pennsylvania (68-00467), Rhode Island (LAO00307), South Carolina (96026), Tennessee (TN02907), Texas (T104704286-10-2), Virginia (00008), Washington (C2043), West Virginia (136), USDA Foreign Soil Permit (P330-08-00006). The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 3/14/2023 6:23:17 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Laboratory Job ID: 400-234011-1 Page 3 of 40 Eurofins Pensacola3/14/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Job ID: 400-234011-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-234011-1 Receipt The samples were received on 3/3/2023 9:28 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.4°C GC/MS VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The following samples were diluted due to the nature of the sample matrix: MW-1 5' (400-234011-1), (400-234011-I-1-A MS) and (400-234011-I-1-B MSD). Elevated reporting limits (RLs) are provided. Method 8270E: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-615463 and analytical batch 400-615540 were outside control limits for one or more analytes, see QC Sample Results for detail. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits. Method 8270E: The laboratory control sample (LCS) for preparation batch 400-615463 and analytical batch 400-615540 recovered outside control limits for the following analytes: Hexachlorobenzene, Benzo[b]fluoranthene and Benzo[a]anthracene. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported. Method 8270E: The continuing calibration verification (CCV) associated with batch 400-615540 recovered outside acceptance criteria, low biased, for Bis(2-chloroethyl)ether, Bis(2-chloroethoxy)methane and Pyridine. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the associated samples were non-detect for the analyte(s), the data are reported. Method 8270E: The continuing calibration verification (CCV) associated with batch 400-615587 recovered outside acceptance criteria, low biased, for Hexachlorocyclopentadiene. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the associated samples were non-detect for the analyte(s), the data are reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following samples were diluted because the base dilution for VPH soil analysis is 1:50: MW-1 5' (400-234011-1) and MW-1 10' (400-234011-2). No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 4 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 ☼Acetone RL 0.0330 mg/Kg MDL 0.0158 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.157 8260D Client Sample ID: MW-1 10'Lab Sample ID: 400-234011-2 ☼Acetone RL 0.0208 mg/Kg MDL 0.0100 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0503 8260D ☼Toluene 0.00416 mg/Kg0.000833 Total/NA10.00135 J 8260D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 5 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID Client Sample ID Matrix Collected Received 400-234011-1 MW-1 5'Solid 03/02/23 09:30 03/03/23 09:28 400-234011-2 MW-1 10'Solid 03/02/23 09:45 03/03/23 09:28 Eurofins PensacolaPage 6 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-1Client Sample ID: MW-1 5' Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.00145 U 0.00659 0.00145 mg/Kg ☼03/10/23 07:47 03/10/23 10:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00659 0.00145 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00145 U1,1,1-Trichloroethane 0.00659 0.00108 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00108 U1,1,2,2-Tetrachloroethane 0.00659 0.00103 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00103 U1,1,2-Trichloroethane 0.00659 0.00109 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00109 U1,1-Dichloroethane 0.00659 0.00112 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00112 U1,1-Dichloroethene 0.00659 0.00109 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00109 U1,1-Dichloropropene 0.00659 0.00145 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00145 U1,2,3-Trichlorobenzene 0.00659 0.00106 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00106 U1,2,3-Trichloropropane 0.00659 0.00121 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00121 U1,2,4-Trichlorobenzene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 U1,2,4-Trimethylbenzene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 U1,2-Dibromoethane 0.00659 0.000936 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000936 U1,2-Dichlorobenzene 0.00659 0.00108 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00108 U1,2-Dichloroethane 0.00659 0.00100 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00100 U1,2-Dichloropropane 0.00659 0.00109 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00109 U1,3,5-Trimethylbenzene 0.00659 0.00125 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00125 U1,3-Dichlorobenzene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 U1,3-Dichloropropane 0.00659 0.00113 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00113 U1,4-Dichlorobenzene 0.00659 0.00145 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00145 U2,2-Dichloropropane 0.0330 0.00791 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00791 U2-Butanone (MEK) 0.00659 0.00107 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00107 U2-Chlorotoluene 0.0330 0.00659 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00659 U2-Hexanone 0.00659 0.00129 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00129 U4-Chlorotoluene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 U4-Isopropyltoluene 0.0330 0.00659 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00659 U4-Methyl-2-pentanone (MIBK) 0.0330 0.0158 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼0.157Acetone 0.00659 0.000884 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000884 UBenzene 0.00659 0.00171 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00171 UBromobenzene 0.00659 0.00107 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00107 UBromochloromethane 0.00659 0.00121 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00121 UBromodichloromethane 0.00659 0.00171 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00171 UBromoform 0.00659 0.00330 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00330 UBromomethane 0.00659 0.00224 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00224 UCarbon tetrachloride 0.00659 0.000686 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000686 UChlorobenzene 0.00659 0.00158 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00158 UChloroethane 0.00659 0.00659 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00659 UChloroform 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 UChloromethane 0.00659 0.00100 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00100 Ucis-1,2-Dichloroethene 0.00659 0.00158 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00158 Ucis-1,3-Dichloropropene 0.00659 0.00158 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00158 UDibromochloromethane 0.00659 0.00171 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00171 UDichlorodifluoromethane 0.132 0.0976 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.0976 UEthanol 0.00659 0.000805 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000805 UEthylbenzene 0.00659 0.000725 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000725 UIsopropyl ether 0.00659 0.000897 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.000897 UIsopropylbenzene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 UMethyl tert-butyl ether 0.0198 0.0132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.0132 UMethylene Chloride 0.00659 0.00396 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00396 UNaphthalene Eurofins Pensacola Page 7 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-1Client Sample ID: MW-1 5' Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.00127 U 0.00659 0.00127 mg/Kg ☼03/10/23 07:47 03/10/23 10:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00659 0.00119 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00119 UN-Propylbenzene 0.00659 0.00125 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00125 Usec-Butylbenzene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 UStyrene 0.00659 0.00145 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00145 Utert-Butylbenzene 0.00659 0.00396 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00396 UTetrachloroethene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 UToluene 0.00659 0.00127 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00127 Utrans-1,2-Dichloroethene 0.00659 0.00145 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00145 Utrans-1,3-Dichloropropene 0.00659 0.00132 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00132 UTrichloroethene 0.00659 0.00113 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00113 UTrichlorofluoromethane 0.0330 0.00251 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00251 UVinyl acetate 0.00659 0.00106 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00106 UVinyl chloride 0.0132 0.00251 mg/Kg 03/10/23 07:47 03/10/23 10:39 1☼<0.00251 UXylenes, Total 4-Bromofluorobenzene 92 67-130 03/10/23 07:47 03/10/23 10:39 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 105 03/10/23 07:47 03/10/23 10:39 177-127 Toluene-d8 (Surr)96 03/10/23 07:47 03/10/23 10:39 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0870 U 0.870 0.0870 mg/Kg ☼03/08/23 10:17 03/08/23 23:53 2 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U1,2-Dichlorobenzene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U1,3-Dichlorobenzene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U1,4-Dichlorobenzene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U1-Methylnaphthalene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,4,5-Trichlorophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,4,6-Trichlorophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,4-Dichlorophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,4-Dimethylphenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,4-Dinitrotoluene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2,6-Dinitrotoluene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2-Chloronaphthalene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2-Chlorophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2-Methylnaphthalene 0.870 0.211 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.211 U2-Methylphenol 0.870 0.184 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.184 U2-Nitroaniline 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U2-Nitrophenol 1.74 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U3 & 4 Methylphenol 0.870 0.206 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.206 U3-Nitroaniline 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U4,6-Dinitro-2-methylphenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U4-Bromophenyl phenyl ether 0.870 0.213 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.213 U4-Chloro-3-methylphenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U4-Chloroaniline 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U4-Chlorophenyl phenyl ether 0.870 0.298 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.298 U4-Nitroaniline 0.870 0.290 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.290 U4-Nitrophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UAcenaphthene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UAcenaphthylene Eurofins Pensacola Page 8 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-1Client Sample ID: MW-1 5' Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.113 U 0.870 0.113 mg/Kg ☼03/08/23 10:17 03/08/23 23:53 2 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UAnthracene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 U *+Benzo[a]anthracene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 UBenzo[a]pyrene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 U *+Benzo[b]fluoranthene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 UBenzo[g,h,i]perylene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 UBenzo[k]fluoranthene 2.61 0.922 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.922 U F1Benzoic acid 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 Ubis (2-chloroisopropyl) ether 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UBis(2-chloroethoxy)methane 0.870 0.242 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.242 UBis(2-chloroethyl)ether 0.870 0.213 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.213 UBis(2-ethylhexyl) phthalate 0.870 0.187 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.187 UButyl benzyl phthalate 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UChrysene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 UDibenz(a,h)anthracene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UDibenzofuran 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UDiethyl phthalate 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UDimethyl phthalate 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UDi-n-butyl phthalate 0.870 0.316 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.316 UDi-n-octyl phthalate 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UFluoranthene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UFluorene 0.870 0.263 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.263 U *+Hexachlorobenzene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UHexachlorobutadiene 0.870 0.174 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.174 UHexachlorocyclopentadiene 0.870 0.0817 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0817 UHexachloroethane 0.870 0.0870 mg/Kg 03/08/23 10:17 03/09/23 12:45 2☼<0.0870 UIndeno[1,2,3-cd]pyrene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UIsophorone 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UNaphthalene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UNitrobenzene 0.870 0.100 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.100 UN-Nitrosodi-n-propylamine 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UN-Nitrosodiphenylamine 1.74 0.174 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.174 UPentachlorophenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UPhenanthrene 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UPhenol 0.870 0.0870 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.0870 UPyrene 0.870 0.395 mg/Kg 03/08/23 10:17 03/08/23 23:53 2☼<0.395 U F1Pyridine 2,4,6-Tribromophenol (Surr)69 10-150 03/08/23 10:17 03/08/23 23:53 2 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 72 03/08/23 10:17 03/08/23 23:53 227-127 2-Fluorophenol (Surr)63 03/08/23 10:17 03/08/23 23:53 225-128 Nitrobenzene-d5 (Surr)65 03/08/23 10:17 03/08/23 23:53 215-136 Phenol-d5 (Surr)63 03/08/23 10:17 03/08/23 23:53 229-130 Terphenyl-d14 (Surr)130 03/08/23 10:17 03/08/23 23:53 224-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <3.87 U 3.87 3.87 mg/Kg ☼03/03/23 09:30 03/09/23 18:13 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 2.00 2.00 mg/Kg 03/03/23 09:30 03/09/23 18:13 50☼<2.00 UC9-C12 Aliphatics Eurofins Pensacola Page 9 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-1Client Sample ID: MW-1 5' Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL <1.07 U 1.07 1.07 mg/Kg ☼03/03/23 09:30 03/09/23 18:13 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)93 70-130 03/03/23 09:30 03/09/23 18:13 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)95 03/03/23 09:30 03/09/23 18:13 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <2.09 U 2.09 2.09 mg/Kg ☼03/08/23 08:19 03/08/23 22:33 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 2.09 2.09 mg/Kg 03/08/23 08:19 03/08/23 22:33 1☼<2.09 UC19-C36 Aliphatics 3.91 3.91 mg/Kg 03/08/23 08:19 03/09/23 02:28 1☼<3.91 UC11-C22 Aromatics 1-Chlorooctadecane 71 40-140 03/08/23 08:19 03/08/23 22:33 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 70 03/08/23 08:19 03/09/23 02:28 140-140 2-Fluorobiphenyl 59 03/08/23 08:19 03/09/23 02:28 140-140 2-Bromonaphthalene 58 03/08/23 08:19 03/09/23 02:28 140-140 General Chemistry RL MDL 74.5 0.01 0.01 %03/08/23 09:46 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %03/08/23 09:46 125.5Percent Moisture (EPA Moisture) Eurofins Pensacola Page 10 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-2Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 03/02/23 09:45 Percent Solids: 85.3Date Received: 03/03/23 09:28 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL <0.000916 U 0.00416 0.000916 mg/Kg ☼03/10/23 07:47 03/10/23 11:48 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00416 0.000916 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000916 U1,1,1-Trichloroethane 0.00416 0.000683 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000683 U1,1,2,2-Tetrachloroethane 0.00416 0.000650 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000650 U1,1,2-Trichloroethane 0.00416 0.000691 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000691 U1,1-Dichloroethane 0.00416 0.000708 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000708 U1,1-Dichloroethene 0.00416 0.000691 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000691 U1,1-Dichloropropene 0.00416 0.000916 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000916 U1,2,3-Trichlorobenzene 0.00416 0.000666 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000666 U1,2,3-Trichloropropane 0.00416 0.000766 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000766 U1,2,4-Trichlorobenzene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 U1,2,4-Trimethylbenzene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 U1,2-Dibromoethane 0.00416 0.000591 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000591 U1,2-Dichlorobenzene 0.00416 0.000683 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000683 U1,2-Dichloroethane 0.00416 0.000633 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000633 U1,2-Dichloropropane 0.00416 0.000691 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000691 U1,3,5-Trimethylbenzene 0.00416 0.000791 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000791 U1,3-Dichlorobenzene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 U1,3-Dichloropropane 0.00416 0.000716 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000716 U1,4-Dichlorobenzene 0.00416 0.000916 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000916 U2,2-Dichloropropane 0.0208 0.00500 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00500 U2-Butanone (MEK) 0.00416 0.000675 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000675 U2-Chlorotoluene 0.0208 0.00416 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00416 U2-Hexanone 0.00416 0.000816 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000816 U4-Chlorotoluene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 U4-Isopropyltoluene 0.0208 0.00416 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00416 U4-Methyl-2-pentanone (MIBK) 0.0208 0.0100 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼0.0503Acetone 0.00416 0.000558 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000558 UBenzene 0.00416 0.00108 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00108 UBromobenzene 0.00416 0.000675 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000675 UBromochloromethane 0.00416 0.000766 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000766 UBromodichloromethane 0.00416 0.00108 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00108 UBromoform 0.00416 0.00208 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00208 UBromomethane 0.00416 0.00142 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00142 UCarbon tetrachloride 0.00416 0.000433 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000433 UChlorobenzene 0.00416 0.00100 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00100 UChloroethane 0.00416 0.00416 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00416 UChloroform 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 UChloromethane 0.00416 0.000633 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000633 Ucis-1,2-Dichloroethene 0.00416 0.00100 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00100 Ucis-1,3-Dichloropropene 0.00416 0.00100 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00100 UDibromochloromethane 0.00416 0.00108 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00108 UDichlorodifluoromethane 0.0833 0.0616 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.0616 UEthanol 0.00416 0.000508 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000508 UEthylbenzene 0.00416 0.000458 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000458 UIsopropyl ether 0.00416 0.000566 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000566 UIsopropylbenzene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 UMethyl tert-butyl ether 0.0125 0.00833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00833 UMethylene Chloride 0.00416 0.00250 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00250 UNaphthalene Eurofins Pensacola Page 11 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-2Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 03/02/23 09:45 Percent Solids: 85.3Date Received: 03/03/23 09:28 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL <0.000800 U 0.00416 0.000800 mg/Kg ☼03/10/23 07:47 03/10/23 11:48 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00416 0.000750 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000750 UN-Propylbenzene 0.00416 0.000791 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000791 Usec-Butylbenzene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 UStyrene 0.00416 0.000916 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000916 Utert-Butylbenzene 0.00416 0.00250 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00250 UTetrachloroethene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼0.00135 JToluene 0.00416 0.000800 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000800 Utrans-1,2-Dichloroethene 0.00416 0.000916 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000916 Utrans-1,3-Dichloropropene 0.00416 0.000833 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000833 UTrichloroethene 0.00416 0.000716 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000716 UTrichlorofluoromethane 0.0208 0.00158 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00158 UVinyl acetate 0.00416 0.000666 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.000666 UVinyl chloride 0.00833 0.00158 mg/Kg 03/10/23 07:47 03/10/23 11:48 1☼<0.00158 UXylenes, Total 4-Bromofluorobenzene 90 67-130 03/10/23 07:47 03/10/23 11:48 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 109 03/10/23 07:47 03/10/23 11:48 177-127 Toluene-d8 (Surr)96 03/10/23 07:47 03/10/23 11:48 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL <0.0378 U 0.378 0.0378 mg/Kg ☼03/08/23 10:17 03/09/23 03:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U1,2-Dichlorobenzene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U1,3-Dichlorobenzene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U1,4-Dichlorobenzene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U1-Methylnaphthalene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,4,5-Trichlorophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,4,6-Trichlorophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,4-Dichlorophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,4-Dimethylphenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,4-Dinitrotoluene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2,6-Dinitrotoluene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2-Chloronaphthalene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2-Chlorophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2-Methylnaphthalene 0.378 0.0916 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0916 U2-Methylphenol 0.378 0.0802 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0802 U2-Nitroaniline 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U2-Nitrophenol 0.756 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U3 & 4 Methylphenol 0.378 0.0893 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0893 U3-Nitroaniline 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U4,6-Dinitro-2-methylphenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U4-Bromophenyl phenyl ether 0.378 0.0928 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0928 U4-Chloro-3-methylphenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U4-Chloroaniline 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U4-Chlorophenyl phenyl ether 0.378 0.129 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.129 U4-Nitroaniline 0.378 0.126 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.126 U4-Nitrophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UAcenaphthene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UAcenaphthylene Eurofins Pensacola Page 12 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-2Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 03/02/23 09:45 Percent Solids: 85.3Date Received: 03/03/23 09:28 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <0.0492 U 0.378 0.0492 mg/Kg ☼03/08/23 10:17 03/09/23 03:15 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Aniline 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UAnthracene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U *+Benzo[a]anthracene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UBenzo[a]pyrene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 U *+Benzo[b]fluoranthene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UBenzo[g,h,i]perylene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UBenzo[k]fluoranthene 1.13 0.401 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.401 UBenzoic acid 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 Ubis (2-chloroisopropyl) ether 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UBis(2-chloroethoxy)methane 0.378 0.105 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.105 UBis(2-chloroethyl)ether 0.378 0.0928 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0928 UBis(2-ethylhexyl) phthalate 0.378 0.0813 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0813 UButyl benzyl phthalate 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UChrysene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UDibenz(a,h)anthracene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UDibenzofuran 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UDiethyl phthalate 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UDimethyl phthalate 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UDi-n-butyl phthalate 0.378 0.137 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.137 UDi-n-octyl phthalate 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UFluoranthene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UFluorene 0.378 0.115 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.115 U *+Hexachlorobenzene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UHexachlorobutadiene 0.378 0.0756 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0756 UHexachlorocyclopentadiene 0.378 0.0355 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0355 UHexachloroethane 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UIndeno[1,2,3-cd]pyrene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UIsophorone 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UNaphthalene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UNitrobenzene 0.378 0.0435 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0435 UN-Nitrosodi-n-propylamine 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UN-Nitrosodiphenylamine 0.756 0.0756 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0756 UPentachlorophenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UPhenanthrene 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UPhenol 0.378 0.0378 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.0378 UPyrene 0.378 0.172 mg/Kg 03/08/23 10:17 03/09/23 03:15 1☼<0.172 UPyridine 2,4,6-Tribromophenol (Surr)60 10-150 03/08/23 10:17 03/09/23 03:15 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 82 03/08/23 10:17 03/09/23 03:15 127-127 2-Fluorophenol (Surr)74 03/08/23 10:17 03/09/23 03:15 125-128 Nitrobenzene-d5 (Surr)78 03/08/23 10:17 03/09/23 03:15 115-136 Phenol-d5 (Surr)76 03/08/23 10:17 03/09/23 03:15 129-130 Terphenyl-d14 (Surr)90 03/08/23 10:17 03/09/23 03:15 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <2.90 U 2.90 2.90 mg/Kg ☼03/03/23 09:30 03/09/23 18:47 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.51 1.51 mg/Kg 03/03/23 09:30 03/09/23 18:47 50☼<1.51 UC9-C12 Aliphatics Eurofins Pensacola Page 13 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Lab Sample ID: 400-234011-2Client Sample ID: MW-1 10' Matrix: SolidDate Collected: 03/02/23 09:45 Percent Solids: 85.3Date Received: 03/03/23 09:28 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) RL MDL <0.806 U 0.806 0.806 mg/Kg ☼03/03/23 09:30 03/09/23 18:47 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)93 70-130 03/03/23 09:30 03/09/23 18:47 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)95 03/03/23 09:30 03/09/23 18:47 5070-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <1.86 U 1.86 1.86 mg/Kg ☼03/08/23 08:19 03/08/23 22:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.86 1.86 mg/Kg 03/08/23 08:19 03/08/23 22:50 1☼<1.86 UC19-C36 Aliphatics 3.49 3.49 mg/Kg 03/08/23 08:19 03/09/23 02:45 1☼<3.49 UC11-C22 Aromatics 1-Chlorooctadecane 82 40-140 03/08/23 08:19 03/08/23 22:50 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 74 03/08/23 08:19 03/09/23 02:45 140-140 2-Fluorobiphenyl 59 03/08/23 08:19 03/09/23 02:45 140-140 2-Bromonaphthalene 56 03/08/23 08:19 03/09/23 02:45 140-140 General Chemistry RL MDL 85.3 0.01 0.01 %03/08/23 09:46 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %03/08/23 09:46 114.7Percent Moisture (EPA Moisture) Eurofins Pensacola Page 14 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Qualifiers GC/MS VOA Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier U Indicates the analyte was analyzed for but not detected. GC/MS Semi VOA Qualifier Description *+LCS and/or LCSD is outside acceptance limits, high biased. Qualifier F1 MS and/or MSD recovery exceeds control limits. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Pensacola Page 15 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8260D - Volatile Organic Compounds by GC/MS Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (67-130)(77-127)(76-127) BFB DBFM TOL 92 105 96400-234011-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 5' 90 109 96400-234011-2 MW-1 10' 92 105 99LCS 400-615796/10-A Lab Control Sample 94 102 96MB 400-615796/12-A Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 8270E - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (10-150)(27-127)(25-128)(15-136)(29-130)(24-146) TBP FBP 2FP NBZ PHL TPHL 69 72 63 65 63 130400-234011-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 5' 127 74 62 6966 118400-234011-1 MS MW-1 5' 129 73 63 6666 123400-234011-1 MSD MW-1 5' 60 82 74 7678 90400-234011-2 MW-1 10' 146 79 69 7166 119LCS 400-615463/2-A Lab Control Sample 95 73 69 6867 126MB 400-615463/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol (Surr) FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol (Surr) NBZ = Nitrobenzene-d5 (Surr) PHL = Phenol-d5 (Surr) TPHL = Terphenyl-d14 (Surr) Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 93 95400-234011-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 5' 93 95400-234011-2 MW-1 10' 90 91LCS 400-614798/2-A Lab Control Sample 92 90LCSD 400-614798/3-A Lab Control Sample Dup 85 85MB 400-614798/1-A Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Eurofins Pensacola Page 16 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140) 1COD1 71400-234011-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 5' 70400-234011-1 MS MW-1 5' 80400-234011-1 MSD MW-1 5' 82400-234011-2 MW-1 10' 84LCS 400-615406/2-A Lab Control Sample 85LCSD 400-615406/10-A Lab Control Sample Dup 84MB 400-615406/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 70 59 58400-234011-1 Percent Surrogate Recovery (Acceptance Limits) MW-1 5' 70 59 44400-234011-1 MS MW-1 5' 80 63 49400-234011-1 MSD MW-1 5' 74 59 56400-234011-2 MW-1 10' 84 68 53LCS 400-615406/2-A Lab Control Sample 85 64 49LCSD 400-615406/10-A Lab Control Sample Dup 74 58 56MB 400-615406/1-A Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Eurofins Pensacola Page 17 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson GC/MS VOA Analysis Batch: 615778 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 615796400-234011-1 MW-1 5'Total/NA Solid 8260D 615796400-234011-2 MW-1 10'Total/NA Solid 8260D 615796MB 400-615796/12-A Method Blank Total/NA Solid 8260D 615796LCS 400-615796/10-A Lab Control Sample Total/NA Prep Batch: 615796 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-234011-1 MW-1 5'Total/NA Solid 5035400-234011-2 MW-1 10'Total/NA Solid 5035MB 400-615796/12-A Method Blank Total/NA Solid 5035LCS 400-615796/10-A Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 615463 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-234011-1 MW-1 5'Total/NA Solid 3546400-234011-2 MW-1 10'Total/NA Solid 3546MB 400-615463/1-A Method Blank Total/NA Solid 3546LCS 400-615463/2-A Lab Control Sample Total/NA Solid 3546400-234011-1 MS MW-1 5'Total/NA Solid 3546400-234011-1 MSD MW-1 5'Total/NA Analysis Batch: 615540 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 615463400-234011-1 MW-1 5'Total/NA Solid 8270E 615463MB 400-615463/1-A Method Blank Total/NA Solid 8270E 615463LCS 400-615463/2-A Lab Control Sample Total/NA Solid 8270E 615463400-234011-1 MS MW-1 5'Total/NA Solid 8270E 615463400-234011-1 MSD MW-1 5'Total/NA Analysis Batch: 615587 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 615463400-234011-2 MW-1 10'Total/NA Analysis Batch: 615673 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 615463400-234011-1 MW-1 5'Total/NA GC VOA Analysis Batch: 614759 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 614798MB 400-614798/1-A Method Blank Total/NA Solid MAVPH 614798LCS 400-614798/2-A Lab Control Sample Total/NA Solid MAVPH 614798LCSD 400-614798/3-A Lab Control Sample Dup Total/NA Prep Batch: 614798 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-234011-1 MW-1 5'Total/NA Solid 5035400-234011-2 MW-1 10'Total/NA Solid 5035MB 400-614798/1-A Method Blank Total/NA Eurofins Pensacola Page 18 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson GC VOA (Continued) Prep Batch: 614798 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035LCS 400-614798/2-A Lab Control Sample Total/NA Solid 5035LCSD 400-614798/3-A Lab Control Sample Dup Total/NA Analysis Batch: 615607 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 614798400-234011-1 MW-1 5'Total/NA Solid MAVPH 614798400-234011-2 MW-1 10'Total/NA GC Semi VOA Prep Batch: 615406 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-234011-1 MW-1 5'Total/NA Solid 3546400-234011-2 MW-1 10'Total/NA Solid 3546MB 400-615406/1-A Method Blank Total/NA Solid 3546LCS 400-615406/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-615406/10-A Lab Control Sample Dup Total/NA Solid 3546400-234011-1 MS MW-1 5'Total/NA Solid 3546400-234011-1 MSD MW-1 5'Total/NA Analysis Batch: 615554 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 615406400-234011-1 MW-1 5'Total/NA Solid MA-EPH 615406400-234011-2 MW-1 10'Total/NA Solid MA-EPH 615406MB 400-615406/1-A Method Blank Total/NA Solid MA-EPH 615406LCS 400-615406/2-A Lab Control Sample Total/NA Solid MA-EPH 615406LCSD 400-615406/10-A Lab Control Sample Dup Total/NA Solid MA-EPH 615406400-234011-1 MS MW-1 5'Total/NA Solid MA-EPH 615406400-234011-1 MSD MW-1 5'Total/NA Analysis Batch: 615555 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 615406400-234011-1 MW-1 5'Total/NA Solid MA-EPH 615406400-234011-2 MW-1 10'Total/NA Solid MA-EPH 615406MB 400-615406/1-A Method Blank Total/NA Solid MA-EPH 615406LCS 400-615406/2-A Lab Control Sample Total/NA Solid MA-EPH 615406LCSD 400-615406/10-A Lab Control Sample Dup Total/NA Solid MA-EPH 615406400-234011-1 MS MW-1 5'Total/NA Solid MA-EPH 615406400-234011-1 MSD MW-1 5'Total/NA General Chemistry Analysis Batch: 615450 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture400-234011-1 MW-1 5'Total/NA Solid Moisture400-234011-2 MW-1 10'Total/NA Eurofins Pensacola Page 19 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8260D - Volatile Organic Compounds by GC/MS Client Sample ID: Method BlankLab Sample ID: MB 400-615796/12-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615778 Prep Batch: 615796 RL MDL 1,1,1,2-Tetrachloroethane <0.00110 U 0.00500 0.00110 mg/Kg 03/10/23 07:47 03/10/23 09:19 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.00110 U 0.001100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1,1-Trichloroethane <0.000820 U 0.0008200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1,2,2-Tetrachloroethane <0.000780 U 0.0007800.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1,2-Trichloroethane <0.000830 U 0.0008300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1-Dichloroethane <0.000850 U 0.0008500.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1-Dichloroethene <0.000830 U 0.0008300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,1-Dichloropropene <0.00110 U 0.001100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2,3-Trichlorobenzene <0.000800 U 0.0008000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2,3-Trichloropropane <0.000920 U 0.0009200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2,4-Trichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2,4-Trimethylbenzene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2-Dibromoethane <0.000710 U 0.0007100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2-Dichlorobenzene <0.000820 U 0.0008200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2-Dichloroethane <0.000760 U 0.0007600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,2-Dichloropropane <0.000830 U 0.0008300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,3,5-Trimethylbenzene <0.000950 U 0.0009500.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,3-Dichlorobenzene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,3-Dichloropropane <0.000860 U 0.0008600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 11,4-Dichlorobenzene <0.00110 U 0.001100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 12,2-Dichloropropane <0.00600 U 0.006000.0250 mg/Kg 03/10/23 07:47 03/10/23 09:19 12-Butanone (MEK) <0.000810 U 0.0008100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 12-Chlorotoluene <0.00500 U 0.005000.0250 mg/Kg 03/10/23 07:47 03/10/23 09:19 12-Hexanone <0.000980 U 0.0009800.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 14-Chlorotoluene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 14-Isopropyltoluene <0.00500 U 0.005000.0250 mg/Kg 03/10/23 07:47 03/10/23 09:19 14-Methyl-2-pentanone (MIBK) <0.0120 U 0.01200.0250 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Acetone <0.000670 U 0.0006700.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Benzene <0.00130 U 0.001300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Bromobenzene <0.000810 U 0.0008100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Bromochloromethane <0.000920 U 0.0009200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Bromodichloromethane <0.00130 U 0.001300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Bromoform <0.00250 U 0.002500.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Bromomethane <0.00170 U 0.001700.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Carbon tetrachloride <0.000520 U 0.0005200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Chlorobenzene <0.00120 U 0.001200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Chloroethane <0.00500 U 0.005000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Chloroform <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Chloromethane <0.000760 U 0.0007600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1cis-1,2-Dichloroethene <0.00120 U 0.001200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1cis-1,3-Dichloropropene <0.00120 U 0.001200.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Dibromochloromethane <0.00130 U 0.001300.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Dichlorodifluoromethane <0.0740 U 0.07400.100 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Ethanol <0.000610 U 0.0006100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Ethylbenzene <0.000550 U 0.0005500.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Isopropyl ether <0.000680 U 0.0006800.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Isopropylbenzene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Methyl tert-butyl ether <0.0100 U 0.01000.0150 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Methylene Chloride Eurofins Pensacola Page 20 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-615796/12-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615778 Prep Batch: 615796 RL MDL Naphthalene <0.00300 U 0.00500 0.00300 mg/Kg 03/10/23 07:47 03/10/23 09:19 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.000960 U 0.0009600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1n-Butylbenzene <0.000900 U 0.0009000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1N-Propylbenzene <0.000950 U 0.0009500.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1sec-Butylbenzene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Styrene <0.00110 U 0.001100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1tert-Butylbenzene <0.00300 U 0.003000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Tetrachloroethene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Toluene <0.000960 U 0.0009600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1trans-1,2-Dichloroethene <0.00110 U 0.001100.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1trans-1,3-Dichloropropene <0.00100 U 0.001000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Trichloroethene <0.000860 U 0.0008600.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Trichlorofluoromethane <0.00190 U 0.001900.0250 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Vinyl acetate <0.000800 U 0.0008000.00500 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Vinyl chloride <0.00190 U 0.001900.0100 mg/Kg 03/10/23 07:47 03/10/23 09:19 1Xylenes, Total 4-Bromofluorobenzene 94 67-130 03/10/23 09:19 1 MB MB Surrogate 03/10/23 07:47 Dil FacPreparedAnalyzedQualifierLimits%Recovery 102 03/10/23 07:47 03/10/23 09:19 1Dibromofluoromethane77-127 96 03/10/23 07:47 03/10/23 09:19 1Toluene-d8 (Surr)76-127 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615796/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615778 Prep Batch: 615796 1,1,1,2-Tetrachloroethane 0.0500 0.04704 mg/Kg 94 65 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 0.0500 0.04656 mg/Kg 93 63 -130 1,1,2,2-Tetrachloroethane 0.0500 0.04831 mg/Kg 97 60 -131 1,1,2-Trichloroethane 0.0500 0.04950 mg/Kg 99 65 -130 1,1-Dichloroethane 0.0500 0.04451 mg/Kg 89 59 -130 1,1-Dichloroethene 0.0500 0.04710 mg/Kg 94 55 -137 1,1-Dichloropropene 0.0500 0.04662 mg/Kg 93 65 -130 1,2,3-Trichlorobenzene 0.0500 0.05138 mg/Kg 103 58 -135 1,2,3-Trichloropropane 0.0500 0.04822 mg/Kg 96 60 -130 1,2,4-Trichlorobenzene 0.0500 0.05043 mg/Kg 101 56 -138 1,2,4-Trimethylbenzene 0.0500 0.04771 mg/Kg 95 66 -130 1,2-Dibromoethane 0.0500 0.04943 mg/Kg 99 67 -130 1,2-Dichlorobenzene 0.0500 0.04979 mg/Kg 100 64 -130 1,2-Dichloroethane 0.0500 0.04927 mg/Kg 99 62 -130 1,2-Dichloropropane 0.0500 0.04504 mg/Kg 90 64 -130 1,3,5-Trimethylbenzene 0.0500 0.04611 mg/Kg 92 67 -130 1,3-Dichlorobenzene 0.0500 0.04787 mg/Kg 96 66 -130 1,3-Dichloropropane 0.0500 0.04824 mg/Kg 96 67 -130 1,4-Dichlorobenzene 0.0500 0.04912 mg/Kg 98 65 -130 2,2-Dichloropropane 0.0500 0.04247 mg/Kg 85 51 -132 2-Butanone (MEK)0.200 0.2009 mg/Kg 100 55 -130 2-Chlorotoluene 0.0500 0.04590 mg/Kg 92 67 -130 Eurofins Pensacola Page 21 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615796/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615778 Prep Batch: 615796 2-Hexanone 0.200 0.1963 mg/Kg 98 57 -131 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 4-Chlorotoluene 0.0500 0.04557 mg/Kg 91 66 -130 4-Isopropyltoluene 0.0500 0.04842 mg/Kg 97 68 -130 4-Methyl-2-pentanone (MIBK)0.200 0.1970 mg/Kg 98 58 -130 Acetone 0.200 0.2068 mg/Kg 103 48 -160 Benzene 0.0500 0.04597 mg/Kg 92 65 -130 Bromobenzene 0.0500 0.04589 mg/Kg 92 65 -130 Bromochloromethane 0.0500 0.04968 mg/Kg 99 65 -130 Bromodichloromethane 0.0500 0.04753 mg/Kg 95 61 -130 Bromoform 0.0500 0.04636 mg/Kg 93 52 -136 Bromomethane 0.0500 0.03953 mg/Kg 79 12 -160 Carbon tetrachloride 0.0500 0.04725 mg/Kg 94 60 -130 Chlorobenzene 0.0500 0.04697 mg/Kg 94 70 -130 Chloroethane 0.0500 0.05037 mg/Kg 101 55 -134 Chloroform 0.0500 0.04648 mg/Kg 93 62 -130 Chloromethane 0.0500 0.02902 mg/Kg 58 49 -136 cis-1,2-Dichloroethene 0.0500 0.04556 mg/Kg 91 53 -135 cis-1,3-Dichloropropene 0.0500 0.04638 mg/Kg 93 61 -130 Dibromochloromethane 0.0500 0.04861 mg/Kg 97 58 -132 Dichlorodifluoromethane 0.0500 0.03377 mg/Kg 68 34 -143 Ethanol 2.00 2.133 mg/Kg 107 29 -160 Ethylbenzene 0.0500 0.04607 mg/Kg 92 70 -130 Isopropyl ether 0.0500 0.04443 mg/Kg 89 62 -130 Isopropylbenzene 0.0500 0.04760 mg/Kg 95 70 -130 Methyl tert-butyl ether 0.0500 0.04670 mg/Kg 93 63 -130 Methylene Chloride 0.0500 0.04514 mg/Kg 90 57 -132 m-Xylene & p-Xylene 0.0500 0.04575 mg/Kg 92 70 -130 Naphthalene 0.0500 0.04991 mg/Kg 100 45 -144 n-Butylbenzene 0.0500 0.05064 mg/Kg 101 66 -130 N-Propylbenzene 0.0500 0.04739 mg/Kg 95 67 -130 o-Xylene 0.0500 0.04664 mg/Kg 93 70 -130 sec-Butylbenzene 0.0500 0.04787 mg/Kg 96 67 -130 Styrene 0.0500 0.04737 mg/Kg 95 68 -130 tert-Butylbenzene 0.0500 0.04599 mg/Kg 92 67 -130 Tetrachloroethene 0.0500 0.04837 mg/Kg 97 67 -130 Toluene 0.0500 0.04381 mg/Kg 88 70 -130 trans-1,2-Dichloroethene 0.0500 0.04642 mg/Kg 93 58 -134 trans-1,3-Dichloropropene 0.0500 0.04631 mg/Kg 93 60 -130 Trichloroethene 0.0500 0.04681 mg/Kg 94 65 -130 Trichlorofluoromethane 0.0500 0.05113 mg/Kg 102 61 -136 Vinyl acetate 0.100 0.09611 mg/Kg 96 24 -160 Vinyl chloride 0.0500 0.04202 mg/Kg 84 52 -132 Xylenes, Total 0.100 0.09239 mg/Kg 92 70 -130 4-Bromofluorobenzene 67 -130 Surrogate 92 LCS LCS Qualifier Limits%Recovery 105Dibromofluoromethane 77 -127 99Toluene-d8 (Surr)76 -127 Eurofins Pensacola Page 22 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-615463/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 RL MDL 1,2,4-Trichlorobenzene <0.0330 U 0.330 0.0330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 11,2-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 11,3-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 11,4-Dichlorobenzene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 11-Methylnaphthalene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,4,5-Trichlorophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,4,6-Trichlorophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,4-Dichlorophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,4-Dimethylphenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,4-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12,6-Dinitrotoluene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Chloronaphthalene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Chlorophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Methylnaphthalene <0.0800 U 0.08000.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Methylphenol <0.0700 U 0.07000.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Nitroaniline <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 12-Nitrophenol <0.0330 U 0.03300.660 mg/Kg 03/08/23 10:16 03/08/23 21:49 13 & 4 Methylphenol <0.0780 U 0.07800.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 13-Nitroaniline <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14,6-Dinitro-2-methylphenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Bromophenyl phenyl ether <0.0810 U 0.08100.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Chloro-3-methylphenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Chloroaniline <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Chlorophenyl phenyl ether <0.113 U 0.1130.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Nitroaniline <0.110 U 0.1100.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 14-Nitrophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Acenaphthene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Acenaphthylene <0.0430 U 0.04300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Aniline <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Anthracene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzo[a]anthracene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzo[a]pyrene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzo[b]fluoranthene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzo[g,h,i]perylene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzo[k]fluoranthene <0.350 U 0.3500.990 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Benzoic acid <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1bis (2-chloroisopropyl) ether <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Bis(2-chloroethoxy)methane <0.0920 U 0.09200.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Bis(2-chloroethyl)ether <0.0810 U 0.08100.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Bis(2-ethylhexyl) phthalate <0.0710 U 0.07100.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Butyl benzyl phthalate <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Chrysene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Dibenz(a,h)anthracene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Dibenzofuran <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Diethyl phthalate <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Dimethyl phthalate <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Di-n-butyl phthalate <0.120 U 0.1200.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Di-n-octyl phthalate Eurofins Pensacola Page 23 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-615463/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 RL MDL Fluoranthene <0.0330 U 0.330 0.0330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Fluorene <0.100 U 0.1000.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Hexachlorobenzene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Hexachlorobutadiene <0.0660 U 0.06600.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Hexachlorocyclopentadiene <0.0310 U 0.03100.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Hexachloroethane <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Indeno[1,2,3-cd]pyrene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Isophorone <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Naphthalene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Nitrobenzene <0.0380 U 0.03800.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1N-Nitrosodi-n-propylamine <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1N-Nitrosodiphenylamine <0.0660 U 0.06600.660 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Pentachlorophenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Phenanthrene <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Phenol <0.0330 U 0.03300.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Pyrene <0.150 U 0.1500.330 mg/Kg 03/08/23 10:16 03/08/23 21:49 1Pyridine 2,4,6-Tribromophenol (Surr)95 10-150 03/08/23 21:49 1 MB MB Surrogate 03/08/23 10:16 Dil FacPreparedAnalyzedQualifierLimits%Recovery 73 03/08/23 10:16 03/08/23 21:49 12-Fluorobiphenyl 27-127 69 03/08/23 10:16 03/08/23 21:49 12-Fluorophenol (Surr)25-128 67 03/08/23 10:16 03/08/23 21:49 1Nitrobenzene-d5 (Surr)15-136 68 03/08/23 10:16 03/08/23 21:49 1Phenol-d5 (Surr)29-130 126 03/08/23 10:16 03/08/23 21:49 1Terphenyl-d14 (Surr)24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615463/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 1,2,4-Trichlorobenzene 2.00 1.536 mg/Kg 77 48 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,2-Dichlorobenzene 2.00 1.531 mg/Kg 77 49 -120 1,3-Dichlorobenzene 2.00 1.396 mg/Kg 70 48 -120 1,4-Dichlorobenzene 2.00 1.546 mg/Kg 77 49 -120 1-Methylnaphthalene 2.00 1.509 mg/Kg 75 40 -120 2,4,5-Trichlorophenol 2.00 1.950 mg/Kg 97 53 -133 2,4,6-Trichlorophenol 2.00 1.808 mg/Kg 90 51 -125 2,4-Dichlorophenol 2.00 1.587 mg/Kg 79 56 -120 2,4-Dimethylphenol 2.00 1.352 mg/Kg 68 54 -120 2,4-Dinitrotoluene 2.00 2.034 mg/Kg 102 59 -133 2,6-Dinitrotoluene 2.00 1.744 mg/Kg 87 57 -123 2-Chloronaphthalene 2.00 1.714 mg/Kg 86 55 -120 2-Chlorophenol 2.00 1.564 mg/Kg 78 52 -120 2-Methylnaphthalene 2.00 1.504 mg/Kg 75 40 -120 2-Methylphenol 2.00 1.755 mg/Kg 88 51 -123 2-Nitroaniline 2.00 1.697 mg/Kg 85 55 -129 2-Nitrophenol 2.00 1.329 mg/Kg 66 53 -120 Eurofins Pensacola Page 24 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615463/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 3 & 4 Methylphenol 2.00 1.576 mg/Kg 79 47 -123 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 3-Nitroaniline 2.00 1.704 mg/Kg 85 45 -120 4,6-Dinitro-2-methylphenol 4.00 2.761 mg/Kg 69 35 -135 4-Bromophenyl phenyl ether 2.00 2.131 mg/Kg 107 51 -120 4-Chloro-3-methylphenol 2.00 1.695 mg/Kg 85 57 -124 4-Chloroaniline 2.00 1.337 mg/Kg 67 34 -120 4-Chlorophenyl phenyl ether 2.00 2.041 mg/Kg 102 56 -120 4-Nitroaniline 2.00 1.574 mg/Kg 79 52 -126 4-Nitrophenol 4.00 4.694 mg/Kg 117 38 -133 Acenaphthene 2.00 1.787 mg/Kg 89 50 -120 Acenaphthylene 2.00 1.693 mg/Kg 85 50 -120 Aniline 2.00 1.236 mg/Kg 62 36 -120 Anthracene 2.00 1.907 mg/Kg 95 52 -120 Benzo[a]anthracene 2.00 2.507 *+mg/Kg 125 55 -120 Benzo[a]pyrene 2.00 1.934 mg/Kg 97 54 -120 Benzo[b]fluoranthene 2.00 2.433 *+mg/Kg 122 55 -120 Benzo[g,h,i]perylene 2.00 1.643 mg/Kg 82 45 -120 Benzo[k]fluoranthene 2.00 2.003 mg/Kg 100 52 -120 Benzoic acid 9.23 3.036 mg/Kg 33 10 -139 bis (2-chloroisopropyl) ether 2.00 1.440 mg/Kg 72 34 -120 Bis(2-chloroethoxy)methane 2.00 1.184 mg/Kg 59 52 -120 Bis(2-chloroethyl)ether 2.00 1.250 mg/Kg 63 28 -120 Bis(2-ethylhexyl) phthalate 2.00 2.271 mg/Kg 114 58 -158 Butyl benzyl phthalate 2.00 2.009 mg/Kg 100 58 -126 Chrysene 2.00 1.588 mg/Kg 79 54 -120 Dibenz(a,h)anthracene 2.00 1.662 mg/Kg 83 49 -120 Dibenzofuran 2.00 1.788 mg/Kg 89 58 -120 Diethyl phthalate 2.00 2.086 mg/Kg 104 56 -128 Dimethyl phthalate 2.00 1.808 mg/Kg 90 58 -120 Di-n-butyl phthalate 2.00 1.968 mg/Kg 98 64 -122 Di-n-octyl phthalate 2.00 2.026 mg/Kg 101 57 -137 Fluoranthene 2.00 1.935 mg/Kg 97 49 -120 Fluorene 2.00 2.155 mg/Kg 108 47 -120 Hexachlorobenzene 2.00 2.640 *+mg/Kg 132 49 -127 Hexachlorobutadiene 2.00 2.040 mg/Kg 102 43 -120 Hexachlorocyclopentadiene 2.00 0.9461 mg/Kg 47 10 -140 Hexachloroethane 2.00 1.547 mg/Kg 77 45 -120 Indeno[1,2,3-cd]pyrene 2.00 1.566 mg/Kg 78 47 -120 Isophorone 2.00 1.296 mg/Kg 65 50 -120 Naphthalene 2.00 1.421 mg/Kg 71 41 -120 Nitrobenzene 2.00 1.303 mg/Kg 65 50 -120 N-Nitrosodi-n-propylamine 2.00 1.657 mg/Kg 83 48 -120 N-Nitrosodiphenylamine 1.98 1.532 mg/Kg 77 54 -120 Pentachlorophenol 4.00 3.213 mg/Kg 80 32 -131 Phenanthrene 2.00 1.899 mg/Kg 95 50 -120 Phenol 2.00 1.516 mg/Kg 76 51 -120 Pyrene 2.00 2.055 mg/Kg 103 54 -120 Pyridine 4.00 1.959 mg/Kg 49 29 -120 Eurofins Pensacola Page 25 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615463/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 146 LCS LCS Qualifier Limits%Recovery 792-Fluorobiphenyl 27 -127 692-Fluorophenol (Surr)25 -128 66Nitrobenzene-d5 (Surr)15 -136 71Phenol-d5 (Surr)29 -130 119Terphenyl-d14 (Surr)24 -146 Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 1,2,4-Trichlorobenzene <0.0870 U 2.67 1.980 mg/Kg 74 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits 1,2-Dichlorobenzene <0.0870 U 2.67 1.875 mg/Kg 70 40 -140☼ 1,3-Dichlorobenzene <0.0870 U 2.67 1.810 mg/Kg 68 40 -140☼ 1,4-Dichlorobenzene <0.0870 U 2.67 2.010 mg/Kg 75 40 -140☼ 1-Methylnaphthalene <0.0870 U 2.67 1.910 mg/Kg 72 40 -140☼ 2,4,5-Trichlorophenol <0.0870 U 2.67 2.485 mg/Kg 93 40 -140☼ 2,4,6-Trichlorophenol <0.0870 U 2.67 2.309 mg/Kg 87 40 -140☼ 2,4-Dichlorophenol <0.0870 U 2.67 2.116 mg/Kg 79 40 -140☼ 2,4-Dimethylphenol <0.0870 U 2.67 1.726 mg/Kg 65 40 -140☼ 2,4-Dinitrotoluene <0.0870 U 2.67 2.604 mg/Kg 98 40 -140☼ 2,6-Dinitrotoluene <0.0870 U 2.67 2.226 mg/Kg 83 40 -140☼ 2-Chloronaphthalene <0.0870 U 2.67 2.004 mg/Kg 75 40 -140☼ 2-Chlorophenol <0.0870 U 2.67 2.058 mg/Kg 77 40 -140☼ 2-Methylnaphthalene <0.0870 U 2.67 1.920 mg/Kg 72 40 -140☼ 2-Methylphenol <0.211 U 2.67 2.320 mg/Kg 87 40 -140☼ 2-Nitroaniline <0.184 U 2.67 2.235 mg/Kg 84 40 -140☼ 2-Nitrophenol <0.0870 U 2.67 1.777 mg/Kg 67 40 -140☼ 3 & 4 Methylphenol <0.0870 U 2.67 1.968 mg/Kg 74 40 -140☼ 3-Nitroaniline <0.206 U 2.67 2.145 mg/Kg 80 40 -140☼ 4,6-Dinitro-2-methylphenol <0.0870 U 5.33 3.505 mg/Kg 66 40 -140☼ 4-Bromophenyl phenyl ether <0.0870 U 2.67 2.742 mg/Kg 103 40 -140☼ 4-Chloro-3-methylphenol <0.213 U 2.67 2.284 mg/Kg 86 40 -140☼ 4-Chloroaniline <0.0870 U 2.67 1.283 mg/Kg 48 40 -140☼ 4-Chlorophenyl phenyl ether <0.0870 U 2.67 2.614 mg/Kg 98 40 -140☼ 4-Nitroaniline <0.298 U 2.67 2.260 mg/Kg 85 40 -140☼ 4-Nitrophenol <0.290 U 5.33 4.463 mg/Kg 84 40 -140☼ Acenaphthene <0.0870 U 2.67 2.007 mg/Kg 75 40 -140☼ Acenaphthylene <0.0870 U 2.67 2.093 mg/Kg 78 40 -140☼ Aniline <0.113 U 2.67 1.539 mg/Kg 58 40 -140☼ Anthracene <0.0870 U 2.67 2.449 mg/Kg 92 40 -140☼ Benzo[a]anthracene <0.0870 U *+2.67 2.930 mg/Kg 110 40 -140☼ Benzo[a]pyrene <0.0870 U *3 2.67 2.693 mg/Kg 101 40 -140☼ Benzo[b]fluoranthene <0.0870 U *3 *+2.67 3.363 mg/Kg 126 40 -140☼ Benzo[g,h,i]perylene <0.0870 U *3 2.67 2.266 mg/Kg 85 40 -140☼ Benzo[k]fluoranthene <0.0870 U *3 2.67 3.265 mg/Kg 122 40 -140☼ Benzoic acid <0.922 U F1 12.3 3.192 F1 mg/Kg 26 40 -140☼ Eurofins Pensacola Page 26 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 bis (2-chloroisopropyl) ether <0.0870 U 2.67 1.793 mg/Kg 67 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Bis(2-chloroethoxy)methane <0.0870 U 2.67 1.544 mg/Kg 58 40 -140☼ Bis(2-chloroethyl)ether <0.242 U 2.67 1.647 mg/Kg 62 40 -140☼ Bis(2-ethylhexyl) phthalate <0.213 U 2.67 3.046 mg/Kg 114 40 -140☼ Butyl benzyl phthalate <0.187 U 2.67 2.783 mg/Kg 104 40 -140☼ Chrysene <0.0870 U 2.67 2.545 mg/Kg 95 40 -140☼ Dibenz(a,h)anthracene <0.0870 U *3 2.67 2.307 mg/Kg 87 40 -140☼ Dibenzofuran <0.0870 U 2.67 2.168 mg/Kg 81 40 -140☼ Diethyl phthalate <0.0870 U 2.67 2.715 mg/Kg 102 40 -140☼ Dimethyl phthalate <0.0870 U 2.67 2.346 mg/Kg 88 40 -140☼ Di-n-butyl phthalate <0.0870 U 2.67 2.553 mg/Kg 96 40 -140☼ Di-n-octyl phthalate <0.316 U 2.67 2.831 mg/Kg 106 40 -140☼ Fluoranthene <0.0870 U 2.67 2.466 mg/Kg 92 40 -140☼ Fluorene <0.0870 U 2.67 2.409 mg/Kg 90 40 -140☼ Hexachlorobenzene <0.263 U *+2.67 3.372 mg/Kg 126 40 -140☼ Hexachlorobutadiene <0.0870 U 2.67 2.670 mg/Kg 100 40 -140☼ Hexachlorocyclopentadiene <0.174 U 2.67 1.192 mg/Kg 45 40 -140☼ Hexachloroethane <0.0817 U 2.67 1.961 mg/Kg 74 40 -140☼ Indeno[1,2,3-cd]pyrene <0.0870 U *3 2.67 2.189 mg/Kg 82 40 -140☼ Isophorone <0.0870 U 2.67 1.745 mg/Kg 65 40 -140☼ Naphthalene <0.0870 U 2.67 1.745 mg/Kg 65 40 -140☼ Nitrobenzene <0.0870 U 2.67 1.820 mg/Kg 68 40 -140☼ N-Nitrosodi-n-propylamine <0.100 U 2.67 2.060 mg/Kg 77 40 -140☼ N-Nitrosodiphenylamine <0.0870 U 2.64 1.980 mg/Kg 75 40 -140☼ Pentachlorophenol <0.174 U 5.33 3.295 mg/Kg 62 40 -140☼ Phenanthrene <0.0870 U 2.67 2.449 mg/Kg 92 40 -140☼ Phenol <0.0870 U 2.67 1.981 mg/Kg 74 40 -140☼ Pyrene <0.0870 U 2.67 2.830 mg/Kg 106 40 -140☼ Pyridine <0.395 U F1 5.33 2.156 mg/Kg 40 40 -140☼ 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 127 MS MS Qualifier Limits%Recovery 742-Fluorobiphenyl 27 -127 622-Fluorophenol (Surr)25 -128 66Nitrobenzene-d5 (Surr)15 -136 69Phenol-d5 (Surr)29 -130 118Terphenyl-d14 (Surr)24 -146 Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 1,2,4-Trichlorobenzene <0.0870 U 2.57 1.855 mg/Kg 72 40 -140 7 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD 1,2-Dichlorobenzene <0.0870 U 2.57 1.821 mg/Kg 71 40 -140 3 30☼ 1,3-Dichlorobenzene <0.0870 U 2.57 1.724 mg/Kg 67 40 -140 5 30☼ 1,4-Dichlorobenzene <0.0870 U 2.57 1.907 mg/Kg 74 40 -140 5 30☼ 1-Methylnaphthalene <0.0870 U 2.57 1.777 mg/Kg 69 40 -140 7 30☼ Eurofins Pensacola Page 27 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 2,4,5-Trichlorophenol <0.0870 U 2.57 2.370 mg/Kg 92 40 -140 5 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD 2,4,6-Trichlorophenol <0.0870 U 2.57 2.161 mg/Kg 84 40 -140 7 30☼ 2,4-Dichlorophenol <0.0870 U 2.57 1.999 mg/Kg 78 40 -140 6 30☼ 2,4-Dimethylphenol <0.0870 U 2.57 1.554 mg/Kg 60 40 -140 10 30☼ 2,4-Dinitrotoluene <0.0870 U 2.57 2.420 mg/Kg 94 40 -140 7 30☼ 2,6-Dinitrotoluene <0.0870 U 2.57 2.107 mg/Kg 82 40 -140 5 30☼ 2-Chloronaphthalene <0.0870 U 2.57 1.884 mg/Kg 73 40 -140 6 30☼ 2-Chlorophenol <0.0870 U 2.57 1.906 mg/Kg 74 40 -140 8 30☼ 2-Methylnaphthalene <0.0870 U 2.57 1.790 mg/Kg 70 40 -140 7 30☼ 2-Methylphenol <0.211 U 2.57 2.123 mg/Kg 83 40 -140 9 30☼ 2-Nitroaniline <0.184 U 2.57 2.190 mg/Kg 85 40 -140 2 30☼ 2-Nitrophenol <0.0870 U 2.57 1.698 mg/Kg 66 40 -140 5 30☼ 3 & 4 Methylphenol <0.0870 U 2.57 1.807 mg/Kg 70 40 -140 8 30☼ 3-Nitroaniline <0.206 U 2.57 1.956 mg/Kg 76 40 -140 9 30☼ 4,6-Dinitro-2-methylphenol <0.0870 U 5.14 3.311 mg/Kg 64 40 -140 6 30☼ 4-Bromophenyl phenyl ether <0.0870 U 2.57 2.641 mg/Kg 103 40 -140 4 30☼ 4-Chloro-3-methylphenol <0.213 U 2.57 2.112 mg/Kg 82 40 -140 8 30☼ 4-Chloroaniline <0.0870 U 2.57 1.188 mg/Kg 46 40 -140 8 30☼ 4-Chlorophenyl phenyl ether <0.0870 U 2.57 2.480 mg/Kg 97 40 -140 5 30☼ 4-Nitroaniline <0.298 U 2.57 2.042 mg/Kg 79 40 -140 10 30☼ 4-Nitrophenol <0.290 U 5.14 3.991 mg/Kg 78 40 -140 11 30☼ Acenaphthene <0.0870 U 2.57 1.904 mg/Kg 74 40 -140 5 30☼ Acenaphthylene <0.0870 U 2.57 1.964 mg/Kg 76 40 -140 6 30☼ Aniline <0.113 U 2.57 1.301 mg/Kg 51 40 -140 17 30☼ Anthracene <0.0870 U 2.57 2.395 mg/Kg 93 40 -140 2 30☼ Benzo[a]anthracene <0.0870 U *+2.57 3.201 mg/Kg 125 40 -140 9 30☼ Benzo[a]pyrene <0.0870 U *3 2.57 2.640 mg/Kg 103 40 -140 2 30☼ Benzo[b]fluoranthene <0.0870 U *3 *+2.57 2.675 mg/Kg 104 40 -140 23 30☼ Benzo[g,h,i]perylene <0.0870 U *3 2.57 2.274 mg/Kg 88 40 -140 0 30☼ Benzo[k]fluoranthene <0.0870 U *3 2.57 2.971 mg/Kg 116 40 -140 9 30☼ Benzoic acid <0.922 U F1 11.9 3.460 F1 mg/Kg 29 40 -140 8 30☼ bis (2-chloroisopropyl) ether <0.0870 U 2.57 1.728 mg/Kg 67 40 -140 4 30☼ Bis(2-chloroethoxy)methane <0.0870 U 2.57 1.455 mg/Kg 57 40 -140 6 30☼ Bis(2-chloroethyl)ether <0.242 U 2.57 1.599 mg/Kg 62 40 -140 3 30☼ Bis(2-ethylhexyl) phthalate <0.213 U 2.57 3.023 mg/Kg 118 40 -140 1 30☼ Butyl benzyl phthalate <0.187 U 2.57 2.866 mg/Kg 112 40 -140 3 30☼ Chrysene <0.0870 U 2.57 2.506 mg/Kg 98 40 -140 2 30☼ Dibenz(a,h)anthracene <0.0870 U *3 2.57 2.361 mg/Kg 92 40 -140 2 30☼ Dibenzofuran <0.0870 U 2.57 2.071 mg/Kg 81 40 -140 5 30☼ Diethyl phthalate <0.0870 U 2.57 2.601 mg/Kg 101 40 -140 4 30☼ Dimethyl phthalate <0.0870 U 2.57 2.242 mg/Kg 87 40 -140 5 30☼ Di-n-butyl phthalate <0.0870 U 2.57 2.519 mg/Kg 98 40 -140 1 30☼ Di-n-octyl phthalate <0.316 U 2.57 2.756 mg/Kg 107 40 -140 3 30☼ Fluoranthene <0.0870 U 2.57 2.370 mg/Kg 92 40 -140 4 30☼ Fluorene <0.0870 U 2.57 2.287 mg/Kg 89 40 -140 5 30☼ Hexachlorobenzene <0.263 U *+2.57 3.304 mg/Kg 129 40 -140 2 30☼ Hexachlorobutadiene <0.0870 U 2.57 2.535 mg/Kg 99 40 -140 5 30☼ Hexachlorocyclopentadiene <0.174 U 2.57 1.056 mg/Kg 41 40 -140 12 30☼ Hexachloroethane <0.0817 U 2.57 1.885 mg/Kg 73 40 -140 4 30☼ Eurofins Pensacola Page 28 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 615540 Prep Batch: 615463 Indeno[1,2,3-cd]pyrene <0.0870 U *3 2.57 2.165 mg/Kg 84 40 -140 1 30☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD Isophorone <0.0870 U 2.57 1.648 mg/Kg 64 40 -140 6 30☼ Naphthalene <0.0870 U 2.57 1.624 mg/Kg 63 40 -140 7 30☼ Nitrobenzene <0.0870 U 2.57 1.733 mg/Kg 67 40 -140 5 30☼ N-Nitrosodi-n-propylamine <0.100 U 2.57 1.960 mg/Kg 76 40 -140 5 30☼ N-Nitrosodiphenylamine <0.0870 U 2.55 1.871 mg/Kg 73 40 -140 6 30☼ Pentachlorophenol <0.174 U 5.14 2.963 mg/Kg 58 40 -140 11 30☼ Phenanthrene <0.0870 U 2.57 2.357 mg/Kg 92 40 -140 4 30☼ Phenol <0.0870 U 2.57 1.840 mg/Kg 72 40 -140 7 30☼ Pyrene <0.0870 U 2.57 2.851 mg/Kg 111 40 -140 1 30☼ Pyridine <0.395 U F1 5.14 2.020 F1 mg/Kg 39 40 -140 7 30☼ 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 129 MSD MSD Qualifier Limits%Recovery 732-Fluorobiphenyl 27 -127 632-Fluorophenol (Surr)25 -128 66Nitrobenzene-d5 (Surr)15 -136 66Phenol-d5 (Surr)29 -130 123Terphenyl-d14 (Surr)24 -146 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-614798/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 614759 Prep Batch: 614798 RL MDL C5-C8 Aliphatics <2.70 U 2.70 2.70 mg/Kg 03/03/23 09:30 03/03/23 15:04 50 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.40 U 1.401.40 mg/Kg 03/03/23 09:30 03/03/23 15:04 50C9-C12 Aliphatics <0.750 U 0.7500.750 mg/Kg 03/03/23 09:30 03/03/23 15:04 50C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)85 70-130 03/03/23 15:04 50 MB MB Surrogate 03/03/23 09:30 Dil FacPreparedAnalyzedQualifierLimits%Recovery 85 03/03/23 09:30 03/03/23 15:04 50a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-614798/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 614759 Prep Batch: 614798 C5-C8 Aliphatics 15.0 11.72 mg/Kg 78 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 17.5 14.13 mg/Kg 81 70 -130 C9-C10 Aromatics 2.50 1.976 mg/Kg 79 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 90 LCS LCS Qualifier Limits%Recovery 91a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Pensacola Page 29 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-614798/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 614759 Prep Batch: 614798 C5-C8 Aliphatics 15.0 14.13 mg/Kg 94 70 -130 19 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 17.5 16.15 mg/Kg 92 70 -130 13 25 C9-C10 Aromatics 2.50 2.266 mg/Kg 91 70 -130 14 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 92 LCSD LCSD Qualifier Limits%Recovery 90a,a,a-Trifluorotoluene (pid)70 -130 Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-615406/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615554 Prep Batch: 615406 RL MDL C9-C18 Aliphatics <1.60 U 1.60 1.60 mg/Kg 03/08/23 08:19 03/08/23 21:09 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.60 U 1.601.60 mg/Kg 03/08/23 08:19 03/08/23 21:09 1C19-C36 Aliphatics 1-Chlorooctadecane 84 40-140 03/08/23 21:09 1 MB MB Surrogate 03/08/23 08:19 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-615406/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 RL MDL C11-C22 Aromatics <3.00 U 3.00 3.00 mg/Kg 03/08/23 08:19 03/09/23 01:05 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl 74 40-140 03/09/23 01:05 1 MB MB Surrogate 03/08/23 08:19 Dil FacPreparedAnalyzedQualifierLimits%Recovery 58 03/08/23 08:19 03/09/23 01:05 12-Fluorobiphenyl 40-140 56 03/08/23 08:19 03/09/23 01:05 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615406/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615554 Prep Batch: 615406 C9-C18 Aliphatics 20.0 12.70 mg/Kg 64 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 21.26 mg/Kg 80 40 -140 1-Chlorooctadecane 40 -140 Surrogate 84 LCS LCS Qualifier Limits%Recovery Eurofins Pensacola Page 30 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-615406/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 C11-C22 Aromatics 56.7 50.38 mg/Kg 89 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl 40 -140 Surrogate 84 LCS LCS Qualifier Limits%Recovery 682-Fluorobiphenyl 40 -140 532-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-615406/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615554 Prep Batch: 615406 C9-C18 Aliphatics 20.0 12.53 mg/Kg 63 40 -140 1 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C19-C36 Aliphatics 26.7 21.36 mg/Kg 80 40 -140 0 50 1-Chlorooctadecane 40 -140 Surrogate 85 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-615406/10-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 C11-C22 Aromatics 56.7 42.09 mg/Kg 74 40 -140 18 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 85 LCSD LCSD Qualifier Limits%Recovery 642-Fluorobiphenyl 40 -140 492-Bromonaphthalene 40 -140 Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 615554 Prep Batch: 615406 C9-C18 Aliphatics <2.09 U 26.1 15.68 mg/Kg 60 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C19-C36 Aliphatics <2.09 U 34.9 25.78 mg/Kg 74 40 -140☼ 1-Chlorooctadecane 40 -140 Surrogate 70 MS MS Qualifier Limits%Recovery Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 C11-C22 Aromatics <3.91 U 74.1 57.15 mg/Kg 77 40 -140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits Eurofins Pensacola Page 31 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 o-Terphenyl 40 -140 Surrogate 70 MS MS Qualifier Limits%Recovery 592-Fluorobiphenyl 40 -140 442-Bromonaphthalene 40 -140 Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 615554 Prep Batch: 615406 C9-C18 Aliphatics <2.09 U 26.0 16.53 mg/Kg 64 40 -140 5 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C19-C36 Aliphatics <2.09 U 34.7 26.88 mg/Kg 78 40 -140 4 50☼ 1-Chlorooctadecane 40 -140 Surrogate 80 MSD MSD Qualifier Limits%Recovery Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 615555 Prep Batch: 615406 C11-C22 Aromatics <3.91 U 73.6 63.34 mg/Kg 86 40 -140 10 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 80 MSD MSD Qualifier Limits%Recovery 632-Fluorobiphenyl 40 -140 492-Bromonaphthalene 40 -140 Eurofins Pensacola Page 32 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 Matrix: SolidDate Collected: 03/02/23 09:30 Date Received: 03/03/23 09:28 Analysis Moisture AW03/08/23 09:461 EET PEN615450 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Prep 5035 AGW03/10/23 07:47 EET PEN615796 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.091 g 5.00 g Analysis 8260D 1 615778 03/10/23 10:39 AGW EET PENTotal/NA 5 mL 5 mL Prep 3546 615463 03/08/23 10:17 LH EET PENTotal/NA 15.29 g 1 mL Analysis 8270E 2 615540 03/08/23 23:53 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 615463 03/08/23 10:17 LH EET PENTotal/NA 15.29 g 1 mL Analysis 8270E 2 615673 03/09/23 12:45 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 614798 03/03/23 09:30 SAB EET PENTotal/NA 6.168 g 5.00 g Analysis MAVPH 50 615607 03/09/23 18:13 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.44 g 2 mL Analysis MA-EPH 1 615554 03/08/23 22:33 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.44 g 2 mL Analysis MA-EPH 1 615555 03/09/23 02:28 JAS EET PENTotal/NA Client Sample ID: MW-1 10'Lab Sample ID: 400-234011-2 Matrix: SolidDate Collected: 03/02/23 09:45 Date Received: 03/03/23 09:28 Analysis Moisture AW03/08/23 09:461 EET PEN615450 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: MW-1 10'Lab Sample ID: 400-234011-2 Matrix: SolidDate Collected: 03/02/23 09:45 Percent Solids: 85.3Date Received: 03/03/23 09:28 Prep 5035 AGW03/10/23 07:47 EET PEN615796 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 7.04 g 5.00 g Analysis 8260D 1 615778 03/10/23 11:48 AGW EET PENTotal/NA 5 mL 5 mL Prep 3546 615463 03/08/23 10:17 LH EET PENTotal/NA 15.36 g 1 mL Analysis 8270E 1 615587 03/09/23 03:15 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 614798 03/03/23 09:30 SAB EET PENTotal/NA 6.497 g 5.00 g Analysis MAVPH 50 615607 03/09/23 18:47 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.14 g 2 mL Analysis MA-EPH 1 615554 03/08/23 22:50 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.14 g 2 mL Analysis MA-EPH 1 615555 03/09/23 02:45 JAS EET PENTotal/NA Eurofins Pensacola Page 33 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Client Sample ID: Method Blank Lab Sample ID: MB 400-614798/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SAB03/03/23 09:30 EET PEN614798 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 614759 03/03/23 15:04 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-615406/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR03/08/23 08:19 EET PEN615406 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 615554 03/08/23 21:09 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 615555 03/09/23 01:05 JAS EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-615463/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH03/08/23 10:16 EET PEN615463 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 615540 03/08/23 21:49 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-615796/12-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 AGW03/10/23 07:47 EET PEN615796 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 615778 03/10/23 09:19 AGW EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-614798/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SAB03/03/23 09:30 EET PEN614798 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 614759 03/03/23 11:27 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-615406/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR03/08/23 08:19 EET PEN615406 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 615554 03/08/23 21:43 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 615555 03/09/23 01:38 JAS EET PENTotal/NA Eurofins Pensacola Page 34 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-615463/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH03/08/23 10:16 EET PEN615463 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 615540 03/08/23 22:51 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-615796/10-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 AGW03/10/23 07:47 EET PEN615796 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 615778 03/10/23 08:21 AGW EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-614798/3-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 SAB03/03/23 09:30 EET PEN614798 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 614759 03/03/23 11:58 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-615406/10-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 KR03/08/23 08:19 EET PEN615406 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 615554 03/09/23 00:14 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 615555 03/09/23 04:09 JAS EET PENTotal/NA Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MS Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Prep 3546 LH03/08/23 10:17 EET PEN615463 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.11 g 1 mL Analysis 8270E 2 615540 03/08/23 23:12 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.41 g 2 mL Analysis MA-EPH 1 615554 03/08/23 22:00 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.41 g 2 mL Analysis MA-EPH 1 615555 03/09/23 01:55 JAS EET PENTotal/NA Eurofins Pensacola Page 35 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Client Sample ID: MW-1 5'Lab Sample ID: 400-234011-1 MSD Matrix: SolidDate Collected: 03/02/23 09:30 Percent Solids: 74.5Date Received: 03/03/23 09:28 Prep 3546 LH03/08/23 10:17 EET PEN615463 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.68 g 1 mL Analysis 8270E 2 615540 03/08/23 23:32 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.50 g 2 mL Analysis MA-EPH 1 615554 03/08/23 22:17 JAS EET PENTotal/NA Prep 3546 615406 03/08/23 08:19 KR EET PENTotal/NA 15.50 g 2 mL Analysis MA-EPH 1 615555 03/09/23 02:12 JAS EET PENTotal/NA Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 36 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-234011-1Client: Consultech Environmental LLC Project/Site: Former Cedar Rock Baptist Misson Method Method Description LaboratoryProtocol SW8468260DVolatile Organic Compounds by GC/MS EET PEN SW8468270ESemivolatile Organic Compounds (GC/MS)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN EPAMoisturePercent Moisture EET PEN SW8463546Microwave Extraction EET PEN SW8465035Closed System Purge and Trap EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 37 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Consultech Environmental LLC Job ID: 400-234011-1 Project/Site: Former Cedar Rock Baptist Misson Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte Moisture Solid Percent Moisture Moisture Solid Percent Solids Eurofins Pensacola Page 38 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 39 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Consultech Environmental LLC Job Number: 400-234011-1 Login Number: 234011 Question Answer Comment Creator: Whitley, Adrian List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.0.4°C IR11 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 40 of 40 3/14/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 ANALYTICAL REPORT PREPARED FOR Attn: Raj Shah Consultech Environmental LLC 2021 Energy Drive Apex, North Carolina 27502 Generated 5/2/2023 4:26:22 PM JOB DESCRIPTION Cedarock Baptist JOB NUMBER 400-236420-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 34 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 5/2/2023 4:26:22 PM Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Laboratory Job ID: 400-236420-1 Page 3 of 34 Eurofins Pensacola5/2/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Job ID: 400-236420-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-236420-1 Receipt The sample was received on 4/20/2023 12:52 PM. Unless otherwise noted below, the sample arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.6°C GC/MS VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 625.1: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for preparation batch 400-622342 and analytical batch 400-622523 recovered outside control limits for the following analytes: 4-Nitroaniline. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported. Method 625.1: The continuing calibration verification (CCV) associated with batch 400-622523 recovered above the upper control limit for 2,2'-oxybis(1-chloropropane), 3-Nitroaniline and 4-Chloroaniline. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAEPH: The method blank for preparation batch 400-621869 contained C11-C22 Aromatics above the reporting limit (RL). None of the samples associated with this method blank contained the target compound; therefore, re-extraction and/or re-analysis of samples were not performed. Method MAEPH: The surrogate recovery for the LCSD was outside control limits; however, the recovery for the spiked target analyte was within control limits; therefore, the data is reported.(LCSD 400-621869/3-A) No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 4 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Client Sample ID: MW-2 Lab Sample ID: 400-236420-1 Benzene RL 1.00 ug/L MDL 0.130 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.290 SM6200-B Phenol 9.82 ug/L1.08 Total/NA11.27 J 625.1 Lead 0.0100 mg/L0.00200 Total/NA10.0440 6010D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 5 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Lab Sample ID Client Sample ID Matrix Collected Received 400-236420-1 MW-2 Water 04/19/23 15:00 04/20/23 12:52 Eurofins PensacolaPage 6 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Lab Sample ID: 400-236420-1Client Sample ID: MW-2 Matrix: WaterDate Collected: 04/19/23 15:00 Date Received: 04/20/23 12:52 Method: SM6200-B - Volatile Organic Compounds RL MDL <0.160 U 1.00 0.160 ug/L 04/25/23 18:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 1.00 0.180 ug/L 04/25/23 18:14 1<0.180 U1,1,1-Trichloroethane 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,1,2,2-Tetrachloroethane 5.00 0.210 ug/L 04/25/23 18:14 1<0.210 U1,1,2-Trichloroethane 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,1-Dichloroethane 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,1-Dichloroethene 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,1-Dichloropropene 1.00 0.900 ug/L 04/25/23 18:14 1<0.900 U1,2,3-Trichlorobenzene 5.00 0.840 ug/L 04/25/23 18:14 1<0.840 U1,2,3-Trichloropropane 1.00 0.820 ug/L 04/25/23 18:14 1<0.820 U1,2,4-Trichlorobenzene 1.00 0.820 ug/L 04/25/23 18:14 1<0.820 U1,2,4-Trimethylbenzene 1.00 0.230 ug/L 04/25/23 18:14 1<0.230 U1,2-Dibromoethane (EDB) 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,2-Dichlorobenzene 1.00 0.190 ug/L 04/25/23 18:14 1<0.190 U1,2-Dichloroethane 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,2-Dichloropropane 1.00 0.560 ug/L 04/25/23 18:14 1<0.560 U1,3,5-Trimethylbenzene 1.00 0.540 ug/L 04/25/23 18:14 1<0.540 U1,3-Dichlorobenzene 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U1,3-Dichloropropane 1.00 0.640 ug/L 04/25/23 18:14 1<0.640 U1,4-Dichlorobenzene 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 U2,2-Dichloropropane 25.0 2.60 ug/L 04/25/23 18:14 1<2.60 U2-Butanone (MEK) 1.00 0.570 ug/L 04/25/23 18:14 1<0.570 U2-Chlorotoluene 25.0 1.40 ug/L 04/25/23 18:14 1<1.40 U2-Hexanone 20.0 12.0 ug/L 04/25/23 18:14 1<12.0 U3,3-Dimethyl-1-butanol 1.00 0.560 ug/L 04/25/23 18:14 1<0.560 U4-Chlorotoluene 25.0 1.80 ug/L 04/25/23 18:14 1<1.80 U4-Methyl-2-pentanone (MIBK) 25.0 10.0 ug/L 04/25/23 18:14 1<10.0 UAcetone 1.00 0.130 ug/L 04/25/23 18:14 10.290 JBenzene 1.00 0.540 ug/L 04/25/23 18:14 1<0.540 UBromobenzene 1.00 0.210 ug/L 04/25/23 18:14 1<0.210 UBromochloromethane 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 UBromodichloromethane 5.00 0.250 ug/L 04/25/23 18:14 1<0.250 UBromoform 1.00 0.980 ug/L 04/25/23 18:14 1<0.980 UBromomethane 1.00 0.190 ug/L 04/25/23 18:14 1<0.190 UCarbon tetrachloride 1.00 0.150 ug/L 04/25/23 18:14 1<0.150 UChlorobenzene 1.00 0.760 ug/L 04/25/23 18:14 1<0.760 UChloroethane 1.00 1.00 ug/L 04/25/23 18:14 1<1.00 UChloroform 1.00 0.320 ug/L 04/25/23 18:14 1<0.320 UChloromethane 1.00 0.200 ug/L 04/25/23 18:14 1<0.200 Ucis-1,2-Dichloroethene 5.00 0.500 ug/L 04/25/23 18:14 1<0.500 Ucis-1,3-Dichloropropene 1.00 0.240 ug/L 04/25/23 18:14 1<0.240 UDibromochloromethane 1.00 0.850 ug/L 04/25/23 18:14 1<0.850 UDichlorodifluoromethane 1.00 0.200 ug/L 04/25/23 18:14 1<0.200 UDiisopropyl ether 100 24.0 ug/L 04/25/23 18:14 1<24.0 UEthanol 1.00 0.280 ug/L 04/25/23 18:14 1<0.280 UEthyl tert-butyl ether 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 UEthylbenzene 1.00 0.530 ug/L 04/25/23 18:14 1<0.530 UIsopropylbenzene 1.00 0.220 ug/L 04/25/23 18:14 1<0.220 UMethyl tert-butyl ether 5.00 3.00 ug/L 04/25/23 18:14 1<3.00 UMethylene Chloride Eurofins Pensacola Page 7 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Lab Sample ID: 400-236420-1Client Sample ID: MW-2 Matrix: WaterDate Collected: 04/19/23 15:00 Date Received: 04/20/23 12:52 Method: SM6200-B - Volatile Organic Compounds (Continued) RL MDL <0.630 U 5.00 0.630 ug/L 04/25/23 18:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier m-Xylene & p-Xylene 5.00 3.00 ug/L 04/25/23 18:14 1<3.00 UNaphthalene 1.00 0.760 ug/L 04/25/23 18:14 1<0.760 Un-Butylbenzene 1.00 0.690 ug/L 04/25/23 18:14 1<0.690 UN-Propylbenzene 5.00 0.600 ug/L 04/25/23 18:14 1<0.600 Uo-Xylene 1.00 0.710 ug/L 04/25/23 18:14 1<0.710 Up-Cymene (p-Isopropyltoluene) 1.00 0.700 ug/L 04/25/23 18:14 1<0.700 Usec-Butylbenzene 1.00 1.00 ug/L 04/25/23 18:14 1<1.00 UStyrene 10.0 4.50 ug/L 04/25/23 18:14 1<4.50 Ut-Amyl alcohol 1.00 0.230 ug/L 04/25/23 18:14 1<0.230 UTert-amyl methyl ether 10.0 2.40 ug/L 04/25/23 18:14 1<2.40 Utert-Butyl Formate 1.00 0.630 ug/L 04/25/23 18:14 1<0.630 Utert-Butylbenzene 1.00 0.900 ug/L 04/25/23 18:14 1<0.900 UTetrachloroethene 1.00 0.410 ug/L 04/25/23 18:14 1<0.410 UToluene 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 Utrans-1,2-Dichloroethene 5.00 0.200 ug/L 04/25/23 18:14 1<0.200 Utrans-1,3-Dichloropropene 1.00 0.150 ug/L 04/25/23 18:14 1<0.150 UTrichloroethene 1.00 0.520 ug/L 04/25/23 18:14 1<0.520 UTrichlorofluoromethane 25.0 0.930 ug/L 04/25/23 18:14 1<0.930 UVinyl acetate 1.00 0.500 ug/L 04/25/23 18:14 1<0.500 UVinyl chloride 10.0 1.60 ug/L 04/25/23 18:14 1<1.60 UXylenes, Total 4-Bromofluorobenzene 96 72-119 04/25/23 18:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 105 04/25/23 18:14 175-126 Toluene-d8 (Surr)100 04/25/23 18:14 164-132 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) RL MDL <0.177 U 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,2,4-Trichlorobenzene 9.82 0.147 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.147 U1-Methylnaphthalene 9.82 0.157 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.157 U2,2'-oxybis(1-chloropropane) 9.82 3.63 ug/L 04/26/23 11:14 04/27/23 15:49 1<3.63 U2,4,5-Trichlorophenol 9.82 2.55 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.55 U2,4,6-Trichlorophenol 9.82 1.96 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.96 U2,4-Dichlorophenol 9.82 1.96 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.96 U2,4-Dimethylphenol 29.5 3.34 ug/L 04/26/23 11:14 04/27/23 15:49 1<3.34 U2,4-Dinitrophenol 9.82 1.87 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.87 U2,4-Dinitrotoluene 9.82 1.87 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.87 U2,6-Dinitrotoluene 9.82 0.137 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.137 U2-Chloronaphthalene 9.82 2.16 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.16 U2-Chlorophenol 9.82 0.128 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.128 U2-Methylnaphthalene 9.82 1.77 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.77 U2-Methylphenol 9.82 2.16 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.16 U2-Nitroaniline 9.82 2.36 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.36 U2-Nitrophenol 19.6 0.383 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.383 U3 & 4 Methylphenol 9.82 2.55 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.55 U3,3'-Dichlorobenzidine 9.82 1.77 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.77 U3-Nitroaniline 9.82 1.57 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.57 U4,6-Dinitro-2-methylphenol 9.82 0.196 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.196 U4-Bromophenyl phenyl ether Eurofins Pensacola Page 8 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Lab Sample ID: 400-236420-1Client Sample ID: MW-2 Matrix: WaterDate Collected: 04/19/23 15:00 Date Received: 04/20/23 12:52 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL <3.73 U 9.82 3.73 ug/L 04/26/23 11:14 04/27/23 15:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 4-Chloro-3-methylphenol 9.82 3.34 ug/L 04/26/23 11:14 04/27/23 15:49 1<3.34 U4-Chloroaniline 9.82 1.96 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.96 U4-Chlorophenyl phenyl ether 9.82 1.47 ug/L 04/26/23 11:14 04/28/23 18:13 1<1.47 U *+4-Nitroaniline 9.82 2.06 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.06 U4-Nitrophenol 9.82 0.157 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.157 UAcenaphthene 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UAcenaphthylene 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UAnthracene 24.5 19.6 ug/L 04/26/23 11:14 04/27/23 15:49 1<19.6 UBenzidine 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UBenzo[a]anthracene 9.82 0.118 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.118 UBenzo[a]pyrene 9.82 0.147 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.147 UBenzo[b]fluoranthene 9.82 0.226 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.226 UBenzo[g,h,i]perylene 9.82 0.157 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.157 UBenzo[k]fluoranthene 29.5 7.17 ug/L 04/26/23 11:14 04/27/23 15:49 1<7.17 UBenzoic acid 9.82 1.96 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.96 UBenzyl alcohol 9.82 0.157 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.157 UBis(2-chloroethoxy)methane 9.82 2.65 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.65 UBis(2-chloroethyl)ether 9.82 4.91 ug/L 04/26/23 11:14 04/27/23 15:49 1<4.91 UBis(2-ethylhexyl) phthalate 9.82 0.187 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.187 UButyl benzyl phthalate 9.82 0.187 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.187 UChrysene 9.82 0.236 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.236 UDibenz(a,h)anthracene 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UDibenzofuran 9.82 0.236 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.236 UDiethyl phthalate 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UDimethyl phthalate 9.82 1.37 ug/L 04/26/23 11:14 04/27/23 15:49 1<1.37 UDi-n-butyl phthalate 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UDi-n-octyl phthalate 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UFluoranthene 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UFluorene 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UHexachlorobenzene 9.82 3.53 ug/L 04/26/23 11:14 04/27/23 15:49 1<3.53 UHexachlorobutadiene 19.6 2.55 ug/L 04/26/23 11:14 04/27/23 15:49 1<2.55 UHexachlorocyclopentadiene 9.82 4.12 ug/L 04/26/23 11:14 04/27/23 15:49 1<4.12 UHexachloroethane 9.82 0.216 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.216 UIndeno[1,2,3-cd]pyrene 9.82 0.137 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.137 UIsophorone 9.82 0.167 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.167 UNaphthalene 9.82 0.128 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.128 UNitrobenzene 9.82 3.24 ug/L 04/26/23 11:14 04/27/23 15:49 1<3.24 UN-Nitrosodi-n-propylamine 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UN-Nitrosodiphenylamine 19.6 1.37 ug/L 04/26/23 11:14 04/28/23 18:13 1<1.37 UPentachlorophenol 9.82 0.177 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.177 UPhenanthrene 9.82 1.08 ug/L 04/26/23 11:14 04/27/23 15:49 11.27 JPhenol 9.82 0.206 ug/L 04/26/23 11:14 04/27/23 15:49 1<0.206 UPyrene 2,4,6-Tribromophenol 50 15-135 04/26/23 11:14 04/27/23 15:49 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 71 04/26/23 11:14 04/27/23 15:49 132-109 2-Fluorophenol 57 04/26/23 11:14 04/27/23 15:49 110-104 Nitrobenzene-d5 76 04/26/23 11:14 04/27/23 15:49 131-111 Phenol-d5 42 04/26/23 11:14 04/27/23 15:49 110-110 Eurofins Pensacola Page 9 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Lab Sample ID: 400-236420-1Client Sample ID: MW-2 Matrix: WaterDate Collected: 04/19/23 15:00 Date Received: 04/20/23 12:52 Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Terphenyl-d14 85 30-129 04/26/23 11:14 04/27/23 15:49 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL <26.0 U 26.0 26.0 ug/L 04/26/23 17:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 11.0 11.0 ug/L 04/26/23 17:50 1<11.0 UC9-C12 Aliphatics 7.00 7.00 ug/L 04/26/23 17:50 1<7.00 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)96 70-130 04/26/23 17:50 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)98 04/26/23 17:50 170-130 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL <147 U 147 147 ug/L 04/21/23 23:02 04/24/23 17:34 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 147 147 ug/L 04/21/23 23:02 04/24/23 17:34 1<147 UC19-C36 Aliphatics 303 303 ug/L 04/21/23 23:02 04/25/23 00:16 1<303 UC11-C22 Aromatics 1-Chlorooctadecane 77 40-140 04/21/23 23:02 04/24/23 17:34 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 69 04/21/23 23:02 04/25/23 00:16 140-140 2-Fluorobiphenyl 112 04/21/23 23:02 04/25/23 00:16 140-140 2-Bromonaphthalene 109 04/21/23 23:02 04/25/23 00:16 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 0.0440 0.0100 0.00200 mg/L 04/22/23 12:06 04/24/23 13:03 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Lead Eurofins Pensacola Page 10 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Qualifiers GC/MS VOA Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier U Indicates the analyte was analyzed for but not detected. GC/MS Semi VOA Qualifier Description *+LCS and/or LCSD is outside acceptance limits, high biased. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description S1+Surrogate recovery exceeds control limits, high biased. Qualifier U Indicates the analyte was analyzed for but not detected. Metals Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) Eurofins Pensacola Page 11 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Glossary (Continued) These commonly used abbreviations may or may not be present in this report. TEQ Toxicity Equivalent Quotient (Dioxin) Abbreviation TNTC Too Numerous To Count Eurofins Pensacola Page 12 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: SM6200-B - Volatile Organic Compounds Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (72-119)(75-126)(64-132) BFB DBFM TOL 96 105 100400-236420-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 89 102 92LCS 400-622124/1002 Lab Control Sample 95 105 106MB 400-622124/4 Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 625.1 - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (15-135)(32-109)(10-104)(31-111)(10-110)(30-129) TBP FBP 2FP NBZ PHL TPHL 50 71 57 76 42 85400-236420-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 85 76 65 5980 87LCS 400-622342/2-A Lab Control Sample 81 75 66 5982 86LCSD 400-622342/3-A Lab Control Sample Dup 51 73 57 4278 89MB 400-622342/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol NBZ = Nitrobenzene-d5 PHL = Phenol-d5 TPHL = Terphenyl-d14 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 96 98400-236420-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 100 100LCS 400-622360/4 Lab Control Sample 99 99LCSD 400-622360/5 Lab Control Sample Dup 96 94MB 400-622360/3 Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 69 112 109400-236420-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 73 135 134LCS 400-621869/2-A Lab Control Sample 73 152 S1+151 S1+LCSD 400-621869/3-A Lab Control Sample Dup Eurofins Pensacola Page 13 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 68 132 132MB 400-621869/1-A Percent Surrogate Recovery (Acceptance Limits) Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (40-140) 1COD1 77400-236420-1 Percent Surrogate Recovery (Acceptance Limits) MW-2 79LCS 400-621869/2-A Lab Control Sample 78LCSD 400-621869/3-A Lab Control Sample Dup 69MB 400-621869/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Eurofins Pensacola Page 14 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist GC/MS VOA Analysis Batch: 622124 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water SM6200-B400-236420-1 MW-2 Total/NA Water SM6200-BMB 400-622124/4 Method Blank Total/NA Water SM6200-BLCS 400-622124/1002 Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 622342 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625400-236420-1 MW-2 Total/NA Water 625MB 400-622342/1-A Method Blank Total/NA Water 625LCS 400-622342/2-A Lab Control Sample Total/NA Water 625LCSD 400-622342/3-A Lab Control Sample Dup Total/NA Analysis Batch: 622523 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625.1 622342400-236420-1 MW-2 Total/NA Water 625.1 622342MB 400-622342/1-A Method Blank Total/NA Water 625.1 622342LCS 400-622342/2-A Lab Control Sample Total/NA Water 625.1 622342LCSD 400-622342/3-A Lab Control Sample Dup Total/NA Analysis Batch: 622778 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 625.1 622342400-236420-1 MW-2 Total/NA Water 625.1 622342MB 400-622342/1-A Method Blank Total/NA GC VOA Analysis Batch: 622360 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MAVPH400-236420-1 MW-2 Total/NA Water MAVPHMB 400-622360/3 Method Blank Total/NA Water MAVPHLCS 400-622360/4 Lab Control Sample Total/NA Water MAVPHLCSD 400-622360/5 Lab Control Sample Dup Total/NA GC Semi VOA Prep Batch: 621869 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3511400-236420-1 MW-2 Total/NA Water 3511MB 400-621869/1-A Method Blank Total/NA Water 3511LCS 400-621869/2-A Lab Control Sample Total/NA Water 3511LCSD 400-621869/3-A Lab Control Sample Dup Total/NA Analysis Batch: 622029 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 621869400-236420-1 MW-2 Total/NA Water MA-EPH 621869MB 400-621869/1-A Method Blank Total/NA Water MA-EPH 621869LCS 400-621869/2-A Lab Control Sample Total/NA Water MA-EPH 621869LCSD 400-621869/3-A Lab Control Sample Dup Total/NA Eurofins Pensacola Page 15 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist GC Semi VOA Analysis Batch: 622030 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water MA-EPH 621869400-236420-1 MW-2 Total/NA Water MA-EPH 621869MB 400-621869/1-A Method Blank Total/NA Water MA-EPH 621869LCS 400-621869/2-A Lab Control Sample Total/NA Water MA-EPH 621869LCSD 400-621869/3-A Lab Control Sample Dup Total/NA Metals Prep Batch: 621890 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3010A400-236420-1 MW-2 Total/NA Water 3010AMB 400-621890/1-A Method Blank Total/NA Water 3010ALCS 400-621890/2-A Lab Control Sample Total/NA Analysis Batch: 622118 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010D 621890400-236420-1 MW-2 Total/NA Water 6010D 621890MB 400-621890/1-A Method Blank Total/NA Water 6010D 621890LCS 400-621890/2-A Lab Control Sample Total/NA Eurofins Pensacola Page 16 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: SM6200-B - Volatile Organic Compounds Client Sample ID: Method BlankLab Sample ID: MB 400-622124/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 622124 RL MDL 1,1,1,2-Tetrachloroethane <0.160 U 1.00 0.160 ug/L 04/25/23 14:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.180 U 0.1801.00 ug/L 04/25/23 14:04 11,1,1-Trichloroethane <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,1,2,2-Tetrachloroethane <0.210 U 0.2105.00 ug/L 04/25/23 14:04 11,1,2-Trichloroethane <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,1-Dichloroethane <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,1-Dichloroethene <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,1-Dichloropropene <0.900 U 0.9001.00 ug/L 04/25/23 14:04 11,2,3-Trichlorobenzene <0.840 U 0.8405.00 ug/L 04/25/23 14:04 11,2,3-Trichloropropane <0.820 U 0.8201.00 ug/L 04/25/23 14:04 11,2,4-Trichlorobenzene <0.820 U 0.8201.00 ug/L 04/25/23 14:04 11,2,4-Trimethylbenzene <0.230 U 0.2301.00 ug/L 04/25/23 14:04 11,2-Dibromoethane (EDB) <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,2-Dichlorobenzene <0.190 U 0.1901.00 ug/L 04/25/23 14:04 11,2-Dichloroethane <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,2-Dichloropropane <0.560 U 0.5601.00 ug/L 04/25/23 14:04 11,3,5-Trimethylbenzene <0.540 U 0.5401.00 ug/L 04/25/23 14:04 11,3-Dichlorobenzene <0.500 U 0.5001.00 ug/L 04/25/23 14:04 11,3-Dichloropropane <0.640 U 0.6401.00 ug/L 04/25/23 14:04 11,4-Dichlorobenzene <0.500 U 0.5001.00 ug/L 04/25/23 14:04 12,2-Dichloropropane <2.60 U 2.6025.0 ug/L 04/25/23 14:04 12-Butanone (MEK) <0.570 U 0.5701.00 ug/L 04/25/23 14:04 12-Chlorotoluene <1.40 U 1.4025.0 ug/L 04/25/23 14:04 12-Hexanone <12.0 U 12.020.0 ug/L 04/25/23 14:04 13,3-Dimethyl-1-butanol <0.560 U 0.5601.00 ug/L 04/25/23 14:04 14-Chlorotoluene <1.80 U 1.8025.0 ug/L 04/25/23 14:04 14-Methyl-2-pentanone (MIBK) <10.0 U 10.025.0 ug/L 04/25/23 14:04 1Acetone <0.130 U 0.1301.00 ug/L 04/25/23 14:04 1Benzene <0.540 U 0.5401.00 ug/L 04/25/23 14:04 1Bromobenzene <0.210 U 0.2101.00 ug/L 04/25/23 14:04 1Bromochloromethane <0.500 U 0.5001.00 ug/L 04/25/23 14:04 1Bromodichloromethane <0.250 U 0.2505.00 ug/L 04/25/23 14:04 1Bromoform <0.980 U 0.9801.00 ug/L 04/25/23 14:04 1Bromomethane <0.190 U 0.1901.00 ug/L 04/25/23 14:04 1Carbon tetrachloride <0.150 U 0.1501.00 ug/L 04/25/23 14:04 1Chlorobenzene <0.760 U 0.7601.00 ug/L 04/25/23 14:04 1Chloroethane <1.00 U 1.001.00 ug/L 04/25/23 14:04 1Chloroform <0.320 U 0.3201.00 ug/L 04/25/23 14:04 1Chloromethane <0.200 U 0.2001.00 ug/L 04/25/23 14:04 1cis-1,2-Dichloroethene <0.500 U 0.5005.00 ug/L 04/25/23 14:04 1cis-1,3-Dichloropropene <0.240 U 0.2401.00 ug/L 04/25/23 14:04 1Dibromochloromethane <0.850 U 0.8501.00 ug/L 04/25/23 14:04 1Dichlorodifluoromethane <0.200 U 0.2001.00 ug/L 04/25/23 14:04 1Diisopropyl ether <24.0 U 24.0100 ug/L 04/25/23 14:04 1Ethanol <0.280 U 0.2801.00 ug/L 04/25/23 14:04 1Ethyl tert-butyl ether <0.500 U 0.5001.00 ug/L 04/25/23 14:04 1Ethylbenzene <0.530 U 0.5301.00 ug/L 04/25/23 14:04 1Isopropylbenzene <0.220 U 0.2201.00 ug/L 04/25/23 14:04 1Methyl tert-butyl ether Eurofins Pensacola Page 17 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-622124/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 622124 RL MDL Methylene Chloride <3.00 U 5.00 3.00 ug/L 04/25/23 14:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.630 U 0.6305.00 ug/L 04/25/23 14:04 1m-Xylene & p-Xylene <3.00 U 3.005.00 ug/L 04/25/23 14:04 1Naphthalene <0.760 U 0.7601.00 ug/L 04/25/23 14:04 1n-Butylbenzene <0.690 U 0.6901.00 ug/L 04/25/23 14:04 1N-Propylbenzene <0.600 U 0.6005.00 ug/L 04/25/23 14:04 1o-Xylene <0.710 U 0.7101.00 ug/L 04/25/23 14:04 1p-Cymene (p-Isopropyltoluene) <0.700 U 0.7001.00 ug/L 04/25/23 14:04 1sec-Butylbenzene <1.00 U 1.001.00 ug/L 04/25/23 14:04 1Styrene <4.50 U 4.5010.0 ug/L 04/25/23 14:04 1t-Amyl alcohol <0.230 U 0.2301.00 ug/L 04/25/23 14:04 1Tert-amyl methyl ether <2.40 U 2.4010.0 ug/L 04/25/23 14:04 1tert-Butyl Formate <0.630 U 0.6301.00 ug/L 04/25/23 14:04 1tert-Butylbenzene <0.900 U 0.9001.00 ug/L 04/25/23 14:04 1Tetrachloroethene <0.410 U 0.4101.00 ug/L 04/25/23 14:04 1Toluene <0.500 U 0.5001.00 ug/L 04/25/23 14:04 1trans-1,2-Dichloroethene <0.200 U 0.2005.00 ug/L 04/25/23 14:04 1trans-1,3-Dichloropropene <0.150 U 0.1501.00 ug/L 04/25/23 14:04 1Trichloroethene <0.520 U 0.5201.00 ug/L 04/25/23 14:04 1Trichlorofluoromethane <0.930 U 0.93025.0 ug/L 04/25/23 14:04 1Vinyl acetate <0.500 U 0.5001.00 ug/L 04/25/23 14:04 1Vinyl chloride <1.60 U 1.6010.0 ug/L 04/25/23 14:04 1Xylenes, Total 4-Bromofluorobenzene 95 72-119 04/25/23 14:04 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 105 04/25/23 14:04 1Dibromofluoromethane75-126 106 04/25/23 14:04 1Toluene-d8 (Surr)64-132 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622124/1002 Matrix: Water Prep Type: Total/NA Analysis Batch: 622124 1,1,1,2-Tetrachloroethane 50.0 55.63 ug/L 111 67 -131 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 50.0 56.91 ug/L 114 68 -130 1,1,2,2-Tetrachloroethane 50.0 50.41 ug/L 101 70 -131 1,1,2-Trichloroethane 50.0 50.32 ug/L 101 70 -130 1,1-Dichloroethane 50.0 57.59 ug/L 115 70 -130 1,1-Dichloroethene 50.0 54.18 ug/L 108 63 -134 1,1-Dichloropropene 50.0 55.80 ug/L 112 70 -130 1,2,3-Trichlorobenzene 50.0 53.00 ug/L 106 60 -138 1,2,3-Trichloropropane 50.0 50.56 ug/L 101 70 -130 1,2,4-Trichlorobenzene 50.0 50.06 ug/L 100 60 -140 1,2,4-Trimethylbenzene 50.0 55.74 ug/L 111 70 -130 1,2-Dibromoethane (EDB)50.0 48.88 ug/L 98 70 -130 1,2-Dichlorobenzene 50.0 54.77 ug/L 110 67 -130 1,2-Dichloroethane 50.0 55.21 ug/L 110 69 -130 1,2-Dichloropropane 50.0 57.36 ug/L 115 70 -130 Eurofins Pensacola Page 18 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622124/1002 Matrix: Water Prep Type: Total/NA Analysis Batch: 622124 1,3,5-Trimethylbenzene 50.0 55.56 ug/L 111 69 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,3-Dichlorobenzene 50.0 56.28 ug/L 113 70 -130 1,3-Dichloropropane 50.0 49.13 ug/L 98 70 -130 1,4-Dichlorobenzene 50.0 55.99 ug/L 112 70 -130 2,2-Dichloropropane 50.0 52.05 ug/L 104 52 -135 2-Butanone (MEK)200 207.9 ug/L 104 61 -145 2-Chlorotoluene 50.0 49.48 ug/L 99 70 -130 2-Hexanone 200 211.7 ug/L 106 65 -137 3,3-Dimethyl-1-butanol 125 120.6 ug/L 97 38 -144 4-Chlorotoluene 50.0 54.28 ug/L 109 70 -130 4-Methyl-2-pentanone (MIBK)200 235.2 ug/L 118 69 -138 Acetone 200 253.4 ug/L 127 43 -160 Benzene 50.0 54.64 ug/L 109 70 -130 Bromobenzene 50.0 51.71 ug/L 103 70 -132 Bromochloromethane 50.0 55.79 ug/L 112 70 -130 Bromodichloromethane 50.0 54.48 ug/L 109 67 -133 Bromoform 50.0 49.47 ug/L 99 57 -140 Bromomethane 25.0 16.11 ug/L 64 10 -160 Carbon tetrachloride 50.0 61.15 ug/L 122 61 -137 Chlorobenzene 50.0 54.86 ug/L 110 70 -130 Chloroethane 25.0 26.34 ug/L 105 55 -141 Chloroform 50.0 55.04 ug/L 110 69 -130 Chloromethane 25.0 28.49 ug/L 114 58 -137 cis-1,2-Dichloroethene 50.0 56.25 ug/L 113 68 -130 cis-1,3-Dichloropropene 50.0 53.31 ug/L 107 69 -132 Dibromochloromethane 50.0 51.35 ug/L 103 67 -135 Dichlorodifluoromethane 25.0 25.97 ug/L 104 41 -146 Diisopropyl ether 25.0 27.20 ug/L 109 64 -132 Ethanol 1000 1253 ug/L 125 20 -160 Ethyl tert-butyl ether 25.0 20.87 ug/L 83 55 -133 Ethylbenzene 50.0 53.06 ug/L 106 70 -130 Isopropylbenzene 50.0 52.74 ug/L 105 70 -130 Methyl tert-butyl ether 50.0 44.90 ug/L 90 66 -130 Methylene Chloride 50.0 53.82 ug/L 108 66 -135 m-Xylene & p-Xylene 50.0 52.73 ug/L 105 70 -130 Naphthalene 50.0 45.57 ug/L 91 47 -149 n-Butylbenzene 50.0 54.38 ug/L 109 67 -130 N-Propylbenzene 50.0 58.47 ug/L 117 70 -130 o-Xylene 50.0 50.66 ug/L 101 70 -130 p-Cymene (p-Isopropyltoluene)50.0 59.42 ug/L 119 65 -130 sec-Butylbenzene 50.0 56.49 ug/L 113 66 -130 Styrene 50.0 52.09 ug/L 104 70 -130 t-Amyl alcohol 250 189.1 ug/L 76 38 -139 Tert-amyl methyl ether 25.0 20.32 ug/L 81 52 -132 tert-Butyl Formate 125 76.59 ug/L 61 10 -160 tert-Butylbenzene 50.0 55.84 ug/L 112 64 -139 Tetrachloroethene 50.0 52.61 ug/L 105 65 -130 Toluene 50.0 50.22 ug/L 100 70 -130 trans-1,2-Dichloroethene 50.0 55.52 ug/L 111 70 -130 Eurofins Pensacola Page 19 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: SM6200-B - Volatile Organic Compounds (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622124/1002 Matrix: Water Prep Type: Total/NA Analysis Batch: 622124 trans-1,3-Dichloropropene 50.0 46.68 ug/L 93 63 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Trichloroethene 50.0 58.99 ug/L 118 70 -130 Trichlorofluoromethane 25.0 26.54 ug/L 106 65 -138 Vinyl acetate 50.0 43.60 ug/L 87 26 -160 Vinyl chloride 25.0 28.34 ug/L 113 59 -136 Xylenes, Total 100 103.4 ug/L 103 70 -130 4-Bromofluorobenzene 72 -119 Surrogate 89 LCS LCS Qualifier Limits%Recovery 102Dibromofluoromethane 75 -126 92Toluene-d8 (Surr)64 -132 Method: 625.1 - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-622342/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 RL MDL 1,2,4-Trichlorobenzene <0.180 U 10.0 0.180 ug/L 04/26/23 11:12 04/27/23 14:46 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.150 U 0.15010.0 ug/L 04/26/23 11:12 04/27/23 14:46 11-Methylnaphthalene <0.160 U 0.16010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,2'-oxybis(1-chloropropane) <3.70 U 3.7010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4,5-Trichlorophenol <2.60 U 2.6010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4,6-Trichlorophenol <2.00 U 2.0010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4-Dichlorophenol <2.00 U 2.0010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4-Dimethylphenol <3.40 U 3.4030.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4-Dinitrophenol <1.90 U 1.9010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,4-Dinitrotoluene <1.90 U 1.9010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12,6-Dinitrotoluene <0.140 U 0.14010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Chloronaphthalene <2.20 U 2.2010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Chlorophenol <0.130 U 0.13010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Methylnaphthalene <1.80 U 1.8010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Methylphenol <2.20 U 2.2010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Nitroaniline <2.40 U 2.4010.0 ug/L 04/26/23 11:12 04/27/23 14:46 12-Nitrophenol <0.390 U 0.39020.0 ug/L 04/26/23 11:12 04/27/23 14:46 13 & 4 Methylphenol <2.60 U 2.6010.0 ug/L 04/26/23 11:12 04/27/23 14:46 13,3'-Dichlorobenzidine <1.80 U 1.8010.0 ug/L 04/26/23 11:12 04/27/23 14:46 13-Nitroaniline <1.60 U 1.6010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14,6-Dinitro-2-methylphenol <0.200 U 0.20010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14-Bromophenyl phenyl ether <3.80 U 3.8010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14-Chloro-3-methylphenol <3.40 U 3.4010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14-Chloroaniline <2.00 U 2.0010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14-Chlorophenyl phenyl ether <2.10 U 2.1010.0 ug/L 04/26/23 11:12 04/27/23 14:46 14-Nitrophenol <0.160 U 0.16010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Acenaphthene <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Acenaphthylene <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Anthracene <20.0 U 20.025.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzidine <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzo[a]anthracene Eurofins Pensacola Page 20 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-622342/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 RL MDL Benzo[a]pyrene <0.120 U 10.0 0.120 ug/L 04/26/23 11:12 04/27/23 14:46 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.150 U 0.15010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzo[b]fluoranthene <0.230 U 0.23010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzo[g,h,i]perylene <0.160 U 0.16010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzo[k]fluoranthene <7.30 U 7.3030.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzoic acid <2.00 U 2.0010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Benzyl alcohol <0.160 U 0.16010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Bis(2-chloroethoxy)methane <2.70 U 2.7010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Bis(2-chloroethyl)ether <5.00 U 5.0010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Bis(2-ethylhexyl) phthalate <0.190 U 0.19010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Butyl benzyl phthalate <0.190 U 0.19010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Chrysene <0.240 U 0.24010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Dibenz(a,h)anthracene <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Dibenzofuran <0.240 U 0.24010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Diethyl phthalate <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Dimethyl phthalate <1.40 U 1.4010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Di-n-butyl phthalate <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Di-n-octyl phthalate <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Fluoranthene <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Fluorene <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Hexachlorobenzene <3.60 U 3.6010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Hexachlorobutadiene <2.60 U 2.6020.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Hexachlorocyclopentadiene <4.20 U 4.2010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Hexachloroethane <0.220 U 0.22010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Indeno[1,2,3-cd]pyrene <0.140 U 0.14010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Isophorone <0.170 U 0.17010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Naphthalene <0.130 U 0.13010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Nitrobenzene <3.30 U 3.3010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1N-Nitrosodi-n-propylamine <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1N-Nitrosodiphenylamine <0.180 U 0.18010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Phenanthrene <1.10 U 1.1010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Phenol <0.210 U 0.21010.0 ug/L 04/26/23 11:12 04/27/23 14:46 1Pyrene 2,4,6-Tribromophenol 51 15-135 04/27/23 14:46 1 MB MB Surrogate 04/26/23 11:12 Dil FacPreparedAnalyzedQualifierLimits%Recovery 73 04/26/23 11:12 04/27/23 14:46 12-Fluorobiphenyl 32-109 57 04/26/23 11:12 04/27/23 14:46 12-Fluorophenol 10-104 78 04/26/23 11:12 04/27/23 14:46 1Nitrobenzene-d5 31-111 42 04/26/23 11:12 04/27/23 14:46 1Phenol-d5 10-110 89 04/26/23 11:12 04/27/23 14:46 1Terphenyl-d14 30-129 Client Sample ID: Method BlankLab Sample ID: MB 400-622342/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622778 Prep Batch: 622342 RL MDL 4-Nitroaniline <1.50 U 10.0 1.50 ug/L 04/26/23 11:12 04/28/23 17:48 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <1.40 U 1.4020.0 ug/L 04/26/23 11:12 04/28/23 17:48 1Pentachlorophenol Eurofins Pensacola Page 21 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622342/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 1,2,4-Trichlorobenzene 120 72.62 ug/L 61 57 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1-Methylnaphthalene 120 91.39 ug/L 76 53 -130 2,2'-oxybis(1-chloropropane)120 110.3 ug/L 92 63 -139 2,4,5-Trichlorophenol 120 90.77 ug/L 76 55 -140 2,4,6-Trichlorophenol 120 85.64 ug/L 71 52 -129 2,4-Dichlorophenol 120 94.42 ug/L 79 53 -122 2,4-Dimethylphenol 120 83.86 ug/L 70 42 -120 2,4-Dinitrophenol 240 232.3 ug/L 97 10 -173 2,4-Dinitrotoluene 120 105.7 ug/L 88 48 -127 2,6-Dinitrotoluene 120 103.9 ug/L 87 68 -137 2-Chloronaphthalene 120 95.86 ug/L 80 65 -120 2-Chlorophenol 120 92.58 ug/L 77 36 -120 2-Methylnaphthalene 120 93.49 ug/L 78 53 -130 2-Methylphenol 120 106.6 ug/L 89 51 -130 2-Nitroaniline 120 116.4 ug/L 97 41 -130 2-Nitrophenol 120 96.46 ug/L 80 61 -163 3 & 4 Methylphenol 120 102.0 ug/L 85 49 -130 3,3'-Dichlorobenzidine 240 319.9 ug/L 133 10 -213 3-Nitroaniline 120 140.4 ug/L 117 25 -130 4,6-Dinitro-2-methylphenol 240 232.4 ug/L 97 53 -130 4-Bromophenyl phenyl ether 120 91.71 ug/L 76 65 -120 4-Chloro-3-methylphenol 120 104.1 ug/L 87 41 -128 4-Chloroaniline 120 105.5 ug/L 88 10 -130 4-Chlorophenyl phenyl ether 120 104.1 ug/L 87 38 -145 4-Nitroaniline 120 163.4 *+ug/L 136 28 -130 4-Nitrophenol 240 232.0 ug/L 97 13 -129 Acenaphthene 120 107.0 ug/L 89 60 -132 Acenaphthylene 120 103.6 ug/L 86 54 -126 Anthracene 120 110.5 ug/L 92 43 -120 Benzidine 240 80.36 ug/L 33 5-130 Benzo[a]anthracene 120 107.3 ug/L 89 42 -133 Benzo[a]pyrene 120 117.0 ug/L 98 32 -148 Benzo[b]fluoranthene 120 116.7 ug/L 97 42 -140 Benzo[g,h,i]perylene 120 106.2 ug/L 89 10 -195 Benzo[k]fluoranthene 120 113.9 ug/L 95 25 -146 Benzoic acid 554 228.0 ug/L 41 19 -126 Benzyl alcohol 120 83.14 ug/L 69 10 -130 Bis(2-chloroethoxy)methane 120 85.71 ug/L 71 49 -165 Bis(2-chloroethyl)ether 120 95.32 ug/L 79 43 -126 Bis(2-ethylhexyl) phthalate 120 111.0 ug/L 92 29 -137 Butyl benzyl phthalate 120 107.7 ug/L 90 10 -140 Chrysene 120 109.2 ug/L 91 44 -140 Dibenz(a,h)anthracene 120 119.3 ug/L 99 10 -200 Dibenzofuran 120 106.0 ug/L 88 59 -130 Diethyl phthalate 120 124.5 ug/L 104 10 -120 Dimethyl phthalate 120 105.4 ug/L 88 10 -120 Di-n-butyl phthalate 120 117.6 ug/L 98 10 -120 Di-n-octyl phthalate 120 109.8 ug/L 92 19 -132 Eurofins Pensacola Page 22 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622342/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 Fluoranthene 120 127.2 ug/L 106 43 -121 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Fluorene 120 125.1 ug/L 104 70 -120 Hexachlorobenzene 120 108.9 ug/L 91 10 -142 Hexachlorobutadiene 120 74.44 ug/L 62 38 -120 Hexachlorocyclopentadiene 120 70.08 ug/L 58 10 -130 Hexachloroethane 120 74.38 ug/L 62 55 -120 Indeno[1,2,3-cd]pyrene 120 115.5 ug/L 96 10 -151 Isophorone 120 92.56 ug/L 77 47 -180 Naphthalene 120 87.20 ug/L 73 36 -120 Nitrobenzene 120 87.08 ug/L 73 54 -158 N-Nitrosodi-n-propylamine 120 116.9 ug/L 97 14 -198 N-Nitrosodiphenylamine 119 90.94 ug/L 76 57 -130 Pentachlorophenol 240 192.1 ug/L 80 38 -152 Phenanthrene 120 108.0 ug/L 90 65 -120 Phenol 120 68.23 ug/L 57 17 -120 Pyrene 120 102.0 ug/L 85 70 -120 2,4,6-Tribromophenol 15 -135 Surrogate 85 LCS LCS Qualifier Limits%Recovery 762-Fluorobiphenyl 32 -109 652-Fluorophenol 10 -104 80Nitrobenzene-d5 31 -111 59Phenol-d5 10 -110 87Terphenyl-d14 30 -129 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-622342/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 1,2,4-Trichlorobenzene 120 73.43 ug/L 61 57 -130 1 40 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 1-Methylnaphthalene 120 94.14 ug/L 78 53 -130 3 40 2,2'-oxybis(1-chloropropane)120 112.2 ug/L 93 63 -139 2 40 2,4,5-Trichlorophenol 120 96.74 ug/L 81 55 -140 6 40 2,4,6-Trichlorophenol 120 89.09 ug/L 74 52 -129 4 40 2,4-Dichlorophenol 120 98.65 ug/L 82 53 -122 4 40 2,4-Dimethylphenol 120 91.31 ug/L 76 42 -120 8 40 2,4-Dinitrophenol 240 246.1 ug/L 103 10 -173 6 40 2,4-Dinitrotoluene 120 104.5 ug/L 87 48 -127 1 40 2,6-Dinitrotoluene 120 105.1 ug/L 88 68 -137 1 40 2-Chloronaphthalene 120 97.93 ug/L 82 65 -120 2 24 2-Chlorophenol 120 97.47 ug/L 81 36 -120 5 40 2-Methylnaphthalene 120 95.39 ug/L 79 53 -130 2 40 2-Methylphenol 120 111.1 ug/L 93 51 -130 4 40 2-Nitroaniline 120 120.4 ug/L 100 41 -130 3 40 2-Nitrophenol 120 100.5 ug/L 84 61 -163 4 40 3 & 4 Methylphenol 120 107.3 ug/L 89 49 -130 5 40 3,3'-Dichlorobenzidine 240 321.9 ug/L 134 10 -213 1 40 Eurofins Pensacola Page 23 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-622342/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 3-Nitroaniline 120 146.2 ug/L 122 25 -130 4 40 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 4,6-Dinitro-2-methylphenol 240 238.2 ug/L 99 53 -130 2 40 4-Bromophenyl phenyl ether 120 94.82 ug/L 79 65 -120 3 40 4-Chloro-3-methylphenol 120 108.3 ug/L 90 41 -128 4 40 4-Chloroaniline 120 111.2 ug/L 93 10 -130 5 40 4-Chlorophenyl phenyl ether 120 106.3 ug/L 89 38 -145 2 40 4-Nitroaniline 120 165.1 *+ug/L 138 28 -130 1 40 4-Nitrophenol 240 227.7 ug/L 95 13 -129 2 40 Acenaphthene 120 112.2 ug/L 93 60 -132 5 40 Acenaphthylene 120 106.4 ug/L 89 54 -126 3 40 Anthracene 120 114.2 ug/L 95 43 -120 3 40 Benzidine 240 63.27 ug/L 26 5-130 24 40 Benzo[a]anthracene 120 112.0 ug/L 93 42 -133 4 40 Benzo[a]pyrene 120 121.0 ug/L 101 32 -148 3 40 Benzo[b]fluoranthene 120 124.7 ug/L 104 42 -140 7 40 Benzo[g,h,i]perylene 120 95.83 ug/L 80 10 -195 10 40 Benzo[k]fluoranthene 120 121.4 ug/L 101 25 -146 6 40 Benzoic acid 554 309.6 ug/L 56 19 -126 30 40 Benzyl alcohol 120 90.76 ug/L 76 10 -130 9 40 Bis(2-chloroethoxy)methane 120 90.76 ug/L 76 49 -165 6 40 Bis(2-chloroethyl)ether 120 92.12 ug/L 77 43 -126 3 40 Bis(2-ethylhexyl) phthalate 120 114.7 ug/L 96 29 -137 3 40 Butyl benzyl phthalate 120 109.5 ug/L 91 10 -140 2 40 Chrysene 120 113.1 ug/L 94 44 -140 4 40 Dibenz(a,h)anthracene 120 104.9 ug/L 87 10 -200 13 40 Dibenzofuran 120 108.4 ug/L 90 59 -130 2 40 Diethyl phthalate 120 126.5 ug/L 105 10 -120 2 40 Dimethyl phthalate 120 106.9 ug/L 89 10 -120 1 40 Di-n-butyl phthalate 120 122.9 ug/L 102 10 -120 4 40 Di-n-octyl phthalate 120 114.1 ug/L 95 19 -132 4 40 Fluoranthene 120 131.1 ug/L 109 43 -121 3 40 Fluorene 120 129.0 ug/L 108 70 -120 3 38 Hexachlorobenzene 120 112.8 ug/L 94 10 -142 4 40 Hexachlorobutadiene 120 74.48 ug/L 62 38 -120 0 40 Hexachlorocyclopentadiene 120 77.48 ug/L 65 10 -130 10 40 Hexachloroethane 120 74.93 ug/L 62 55 -120 1 40 Indeno[1,2,3-cd]pyrene 120 101.0 ug/L 84 10 -151 13 40 Isophorone 120 96.33 ug/L 80 47 -180 4 40 Naphthalene 120 89.40 ug/L 75 36 -120 3 40 Nitrobenzene 120 90.74 ug/L 76 54 -158 4 40 N-Nitrosodi-n-propylamine 120 122.4 ug/L 102 14 -198 5 40 N-Nitrosodiphenylamine 119 94.08 ug/L 79 57 -130 3 40 Pentachlorophenol 240 206.1 ug/L 86 38 -152 7 40 Phenanthrene 120 113.8 ug/L 95 65 -120 5 39 Phenol 120 71.67 ug/L 60 17 -120 5 40 Pyrene 120 105.8 ug/L 88 70 -120 4 40 Eurofins Pensacola Page 24 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-622342/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622523 Prep Batch: 622342 2,4,6-Tribromophenol 15 -135 Surrogate 81 LCSD LCSD Qualifier Limits%Recovery 752-Fluorobiphenyl 32 -109 662-Fluorophenol 10 -104 82Nitrobenzene-d5 31 -111 59Phenol-d5 10 -110 86Terphenyl-d14 30 -129 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-622360/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 622360 RL MDL C5-C8 Aliphatics <26.0 U 26.0 26.0 ug/L 04/26/23 12:23 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <11.0 U 11.011.0 ug/L 04/26/23 12:23 1C9-C12 Aliphatics <7.00 U 7.007.00 ug/L 04/26/23 12:23 1C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)96 70-130 04/26/23 12:23 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 94 04/26/23 12:23 1a,a,a-Trifluorotoluene (pid)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-622360/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 622360 C5-C8 Aliphatics 300 308.0 ug/L 103 70 -130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 350 348.3 ug/L 100 70 -130 C9-C10 Aromatics 50.0 49.51 ug/L 99 70 -130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 100 LCS LCS Qualifier Limits%Recovery 100a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-622360/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 622360 C5-C8 Aliphatics 300 308.8 ug/L 103 70 -130 0 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 350 350.3 ug/L 100 70 -130 1 25 C9-C10 Aromatics 50.0 48.81 ug/L 98 70 -130 1 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 99 LCSD LCSD Qualifier Limits%Recovery 99a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Pensacola Page 25 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-621869/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622030 Prep Batch: 621869 RL MDL C9-C18 Aliphatics <150 U 150 150 ug/L 04/21/23 23:02 04/24/23 13:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <150 U 150150 ug/L 04/21/23 23:02 04/24/23 13:30 1C19-C36 Aliphatics 1-Chlorooctadecane 69 40-140 04/24/23 13:30 1 MB MB Surrogate 04/21/23 23:02 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-621869/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622029 Prep Batch: 621869 RL MDL C11-C22 Aromatics 341.6 309 309 ug/L 04/21/23 23:02 04/24/23 20:01 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl 68 40-140 04/24/23 20:01 1 MB MB Surrogate 04/21/23 23:02 Dil FacPreparedAnalyzedQualifierLimits%Recovery 132 04/21/23 23:02 04/24/23 20:01 12-Fluorobiphenyl 40-140 132 04/21/23 23:02 04/24/23 20:01 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-621869/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622030 Prep Batch: 621869 C9-C18 Aliphatics 1360 1222 ug/L 90 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 1820 1490 ug/L 82 40 -140 1-Chlorooctadecane 40 -140 Surrogate 79 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-621869/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622029 Prep Batch: 621869 C11-C22 Aromatics 3860 5029 ug/L 130 40 -140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl 40 -140 Surrogate 73 LCS LCS Qualifier Limits%Recovery 1352-Fluorobiphenyl 40 -140 1342-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-621869/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622030 Prep Batch: 621869 C9-C18 Aliphatics 1360 1328 ug/L 97 40 -140 8 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Eurofins Pensacola Page 26 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-621869/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622030 Prep Batch: 621869 C19-C36 Aliphatics 1820 1403 ug/L 77 40 -140 6 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 1-Chlorooctadecane 40 -140 Surrogate 78 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-621869/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622029 Prep Batch: 621869 C11-C22 Aromatics 3860 4351 ug/L 113 40 -140 14 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 73 LCSD LCSD Qualifier Limits%Recovery 152 S1+2-Fluorobiphenyl 40 -140 151 S1+2-Bromonaphthalene 40 -140 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 400-621890/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622118 Prep Batch: 621890 RL MDL Lead <0.00200 U 0.0100 0.00200 mg/L 04/22/23 12:06 04/24/23 11:50 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-621890/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 622118 Prep Batch: 621890 Lead 1.00 0.9660 mg/L 97 80 -120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Eurofins Pensacola Page 27 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Client Sample ID: MW-2 Lab Sample ID: 400-236420-1 Matrix: WaterDate Collected: 04/19/23 15:00 Date Received: 04/20/23 12:52 Analysis SM6200-B AGW04/25/23 18:141 EET PEN622124 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Prep 625 622342 04/26/23 11:14 STC EET PENTotal/NA 254.6 mL 1 mL Analysis 625.1 1 622523 04/27/23 15:49 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 625 622342 04/26/23 11:14 STC EET PENTotal/NA 254.6 mL 1 mL Analysis 625.1 1 622778 04/28/23 18:13 VC1 EET PENTotal/NA 0.4 mL 0.4 mL Analysis MAVPH 1 622360 04/26/23 17:50 SAB EET PENTotal/NA 5 mL 5 mL Prep 3511 621869 04/21/23 23:02 JTC EET PENTotal/NA 56.1 mL 2 mL Analysis MA-EPH 1 622029 04/25/23 00:16 MP EET PENTotal/NA Prep 3511 621869 04/21/23 23:02 JTC EET PENTotal/NA 56.1 mL 2 mL Analysis MA-EPH 1 622030 04/24/23 17:34 MP EET PENTotal/NA 1 mL 1 mL Prep 3010A 621890 04/22/23 12:06 JL EET PENTotal/NA 50 mL 50 mL Completed:04/22/23 16:50 ¹ Analysis 6010D 1 622118 04/24/23 13:03 LSS EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-621869/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC04/21/23 23:02 EET PEN621869 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 55 mL 2 mL Analysis MA-EPH 1 622029 04/24/23 20:01 MP EET PENTotal/NA Prep 3511 621869 04/21/23 23:02 JTC EET PENTotal/NA 55 mL 2 mL Analysis MA-EPH 1 622030 04/24/23 13:30 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-621890/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3010A JL04/22/23 12:06 EET PEN621890 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 50 mL 50 mL Completed:04/22/23 16:50 ¹ Analysis 6010D 1 622118 04/24/23 11:50 LSS EET PENTotal/NA Client Sample ID: Method Blank Lab Sample ID: MB 400-622124/4 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B AGW04/25/23 14:041 EET PEN622124 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Eurofins Pensacola Page 28 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Client Sample ID: Method Blank Lab Sample ID: MB 400-622342/1-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 STC04/26/23 11:12 EET PEN622342 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 622523 04/27/23 14:46 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 625 622342 04/26/23 11:12 STC EET PENTotal/NA 250 mL 1 mL Analysis 625.1 1 622778 04/28/23 17:48 VC1 EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-622360/3 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SAB04/26/23 12:231 EET PEN622360 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-621869/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC04/21/23 23:02 EET PEN621869 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 55 mL 2 mL Analysis MA-EPH 1 622029 04/24/23 20:35 MP EET PENTotal/NA Prep 3511 621869 04/21/23 23:02 JTC EET PENTotal/NA 55 mL 2 mL Analysis MA-EPH 1 622030 04/24/23 14:02 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-621890/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3010A JL04/22/23 12:06 EET PEN621890 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 50 mL 50 mL Completed:04/22/23 16:50 ¹ Analysis 6010D 1 622118 04/24/23 11:55 LSS EET PENTotal/NA Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-622124/1002 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis SM6200-B AGW04/25/23 13:101 EET PEN622124 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-622342/2-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 STC04/26/23 11:12 EET PEN622342 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 622523 04/27/23 15:07 S1B EET PENTotal/NA 0.4 mL 0.4 mL Eurofins Pensacola Page 29 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-622360/4 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SAB04/26/23 13:021 EET PEN622360 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-621869/3-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 3511 JTC04/21/23 23:02 EET PEN621869 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 55 mL 2 mL Analysis MA-EPH 1 622029 04/24/23 20:52 MP EET PENTotal/NA Prep 3511 621869 04/21/23 23:02 JTC EET PENTotal/NA 55 mL 2 mL Analysis MA-EPH 1 622030 04/24/23 14:18 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-622342/3-A Matrix: WaterDate Collected: N/A Date Received: N/A Prep 625 STC04/26/23 11:12 EET PEN622342 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 250 mL 1 mL Analysis 625.1 1 622523 04/27/23 15:28 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-622360/5 Matrix: WaterDate Collected: N/A Date Received: N/A Analysis MAVPH SAB04/26/23 13:401 EET PEN622360 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5 mL 5 mL ¹ Completion dates and times are reported or not reported per method requirements or individual lab discretion. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 30 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-236420-1Client: Consultech Environmental LLC Project/Site: Cedarock Baptist Method Method Description LaboratoryProtocol SMSM6200-B Volatile Organic Compounds EET PEN EPA625.1 Semivolatile Organic Compounds (GC/MS)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8466010DMetals (ICP)EET PEN SW8463010APreparation, Total Metals EET PEN SW8463511Microextraction of Organic Compounds EET PEN SW8465030BPurge and Trap EET PEN EPA625Liquid-Liquid Extraction EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 31 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Consultech Environmental LLC Job ID: 400-236420-1 Project/Site: Cedarock Baptist Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte SM6200-B Water 2-Butanone (MEK) SM6200-B Water 2-Hexanone SM6200-B Water 3,3-Dimethyl-1-butanol SM6200-B Water 4-Methyl-2-pentanone (MIBK) SM6200-B Water Acetone SM6200-B Water Ethyl tert-butyl ether SM6200-B Water t-Amyl alcohol SM6200-B Water Tert-amyl methyl ether SM6200-B Water tert-Butyl Formate SM6200-B Water Vinyl acetate Eurofins Pensacola Page 32 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 33 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Consultech Environmental LLC Job Number: 400-236420-1 Login Number: 236420 Question Answer Comment Creator: Whitley, Adrian List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.0.6°C IR11 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 34 of 34 5/2/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 APPENDIX B Monitoring Well Completion Record John Eisenman 4439 SAEDACCO Inc X 4-17-23 MW-2 Former Cedarock Baptist Mission 6061 State Hwy 49, Burlington, NC, 27215 Alamance X X 1 38 6" Air 0 28 2"SCH-40 PVC 28 38 2".010 SCH-40 PVC 0 21 Portland Pour 26 38 Sand #2 0 38 clay/sand bentonite seal from 26-21ft 4/27/2023