WS-3254_9547_CA_MRP_20200107

GROUNDWATER MONITORING REPORT
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NORTH CAROLINA

NCDEQ INCIDENT NUMBER: 9547
NCDEQ CONTRACT NUMBER: N17006

ECS PROJECT 49:6166-A

PREPARED FOR:

NCDEQ, UST SECTION
RALEIGH, NORTH CAROLINA

JANUARY 7, 2020

January 7, 2020

Mr. Herbert Berger, P.G.
NCDEQ, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Reference: Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. 17006
ECS Project 49:6166-A

Dear Mr. Berger:

As authorized by your acceptance of ECS Southeast, LLP’s (ECS) Task Authorization Request
No. 2 dated November 12, 2019, ECS has prepared a Groundwater Monitoring Report for the
above referenced site. This report includes a description of the work performed, the results
obtained, and our conclusions and recommendations.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us at (336)
856-7150.

Sincerely,

ECS SOUTHEAST, LLP

Scott Young, P.G. Roger A. Smith, P.G.
Environmental Project Manager Principal Geologist
[e-mail] [e-mail]

Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project 49:6166-A
January 7, 2020

SITE INFORMATION

Site Name: Jerry’s Place

Site Address: 983 US Highway 21
State Road, North Carolina 28676

Facility ID Number: 0-008572

NCDEQ Incident Number: 9547

Site Risk Ranking: High

Land Use Category: Commercial

Latitude/Longitude: 36.3259656 N / 80.867567 W

Responsible Party: Jerry Harris
163 Royall Road
Thurmond, North Carolina 28683

Current Property Owner: Ted and Jamie Roberts
1300 N. Bridge St. Ste. 100
Elkin, North Carolina 28621

Primary Contact: Mr. Herbert Berger
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Primary Consultant: ECS Southeast, LLP
1812 Center Park Drive, Suite D
Charlotte, North Carolina 28217
[phone]

Laboratory: Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
[phone]
Laboratory Certification No. 12

Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project 49:6166-A
January 7, 2020

TABLE OF CONTENTS
1.0 PROJECT INFORMATION ................................................................................................... 5
2.0 GROUNDWATER ASSESSMENT ........................................................................................ 5
2.1 Groundwater Measurement ....................................................................................... 5
2.2 Monitoring Well Sampling .......................................................................................... 5
2.3 Water Supply Well Sampling ..................................................................................... 6
3.0 RESULTS ............................................................................................................................. 6
3.1 Groundwater Flow Direction ...................................................................................... 6
3.2 Monitoring Well Sampling Results ............................................................................. 6
3.3 Water Supply Well Sampling Results ........................................................................ 6
4.0 CONCLUSIONS AND RECOMMENDATIONS ...................................................................... 6

FIGURES

Figure 1 USGS Topographic Map
Figure 2 Aerial Site Map
Figure 3 Monitoring Well Location Map
Figure 4 Groundwater Contour Map
Figure 5 Groundwater Analytical Map

TABLES

Table 1 Monitoring Well Information and Groundwater Elevation Data
Table 2 Summary of Current and Historical Monitoring Well Groundwater Analytical
Results
Table 3 Summary of Current and Historical Water Supply Well Groundwater
Analytical Results

APPENDIX

Appendix A Site Photographs
Appendix B Laboratory Analytical Report and Chain of Custody Record
Appendix C Field Sampling Notes
Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project 49:6166-A
January 7, 2020

1.0 PROJECT INFORMATION

The subject site is Jerry’s Place located at 983 US Highway 21 in State Road, Surry County,
North Carolina (Figures 1 and 2). Photographs of the site are included in Appendix A. Based
on information provided to ECS, four 4,000-gallon gasoline USTs were removed from the site in
October 1992. During closure activities, Light Non-Aqueous Phase Liquid (LNAPL) was
observed flowing into a test pit that was excavated to a depth of approximately 19 feet bgs.
Petroleum hydrocarbons were detected in soil samples collected from the UST basin and
dispenser areas. The closure was concluded by soil excavation and remediation of
approximately 1,029 tons of soil. Between 1993 and 1994, eight monitoring wells (MW-1
through MW-8) and two recovery wells (RW-5 and RW-6) were installed at the site. Monitoring
well MW-1 is presumed destroyed and recovery well RW-6 is presumed paved over based on a
2008 report. An aggressive fluid vapor recovery (AFVR) event was conducted in 1996 and a
mobile multi-phase extraction (MMPE) event was conducted in 2001. LNAPL was not observed
following the MMPE event until 2008 when 0.05 feet of LNAPL was measured in monitoring well
MW-2. Groundwater samples were collected from various monitoring wells on the site in 1993,
2009, 2010, 2011, 2014, 2015, and 2018. The contaminant concentrations in the impacted
monitoring wells have generally decreased since the 1993 sampling event. Sixteen water-
supply wells have been identified within 1,000 feet of the site. Methyl-tert-butyl-ether (MTBE)
has been detected in one water supply well (WSW-5) since 2009; however, the concentrations
have been below the North Carolina 2L Groundwater Quality Standard (NC2LGWQS. Municipal
water is not available to the site or surrounding properties. The nearest surface water body is a
stream located approximately 230 feet east of the source area. The estimated quantity of the
release is unknown. The site is currently occupied by Swift Automotive Paint and Body Shop
Supplies.

2.0 GROUNDWATER ASSESSMENT

2.1 Groundwater Measurement

On December 12, 2019, ECS measured the static water level (SWL) in monitoring wells MW-2,
MW-3, MW-4, and MW-5 using a decontaminated electronic water level meter. The static water
levels and top of casing elevations were used to calculate groundwater flow direction. The static
water level measurements can be found on Table 1.

2.2 Monitoring Well Sampling

Following the collection of the groundwater measurements, ECS personnel collected groundwater
samples from monitoring wells MW-2, MW-3, MW-4, and MW-5. The locations of the wells are
shown on Figure 3. Prior to sampling, the monitoring wells were purged using a new disposable
polyethylene bailer and new length of nylon cord. The monitoring wells were purged by
evacuating a minimum of three well volumes using the bailer and cord. After purging was
completed, the groundwater sample was poured from the bailer into laboratory prepared
containers. Each container was labeled and placed in a cooler containing ice to maintain the
samples at approximately four degrees Celsius. The sample containers were then submitted to
Pace Analytical Services, LLC (Pace), a North Carolina certified laboratory, in Huntersville,
Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project 49:6166-A
January 7, 2020

North Carolina to be analyzed for volatile organic compounds (VOCs) using Standard Method
6200B. A Chain of Custody Record was maintained and is included in Appendix B. A copy of
the groundwater sampling notes are included in Appendix C.

2.3 Water Supply Well Sampling

On December 12, 2019, ECS collected a sample from water-supply well WSW-5. The location of
the well is shown on Figure 3. Prior to sampling, the water supply well and plumbing were purged
by allowing the water to run for approximately 15 minutes. After purging was completed, the
sampler wearing a new pair of disposable nitrile gloves, poured the water sample into laboratory
prepared containers. Each container was labeled and placed in a cooler containing ice to
maintain the samples at approximately four degrees Celsius. The sample containers were then
submitted to Pace to be analyzed for VOCs using Standard Method 6200B.

3.0 RESULTS

3.1 Groundwater Flow Direction

Based on the groundwater measurement collected at the site on December 12, 2019, the
groundwater at the site is generally to the southeast as depicted on Figure 4.

3.2 Monitoring Well Sampling Results

Review of the laboratory analytical report of groundwater samples collected from monitoring wells
MW-2 and MW-3 indicated multiple targeted compounds greater than the NC2LGWQS; however,
the concentrations were not greater than the Gross Contaminant Levels (GCLs). Compounds
were not detected in the samples collected from monitoring wells MW-4 and MW-5 at
concentrations greater than the laboratory method reporting limits. A summary of the current and
historical groundwater analytical results is included in Table 2. The current analytical results are
depicted on Figure 5. A copy of the laboratory analytical report are included in Appendix B.

3.3 Water Supply Well Sampling Results

Review of the laboratory analytical report of the sample collected from water supply well WSW-5
did not indicate any compounds at concentrations greater than the laboratory method reporting
limits. A summary of the current and historical water supply well analytical results are presented
in Table 3.

4.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the results of this groundwater sampling event, ECS concludes that benzene
concentrations in the samples collected from wells MW-2/RW-2 and MW-3/RW-3 in December
2019 decreased by 55 and 69 percent, respectively as compared to the samples collected in
February 2018. However, total volatile organic compound concentrations in the samples collected
from these wells in December 2019 increased by 112 and 34 percent, respectively, as compared
to the samples collected in February 2018. Compound concentrations in the samples collected
Groundwater Monitoring Report
Jerry’s Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project 49:6166-A
January 7, 2020

from wells MW-4/RW-4 and MW-5 in December 2019 have decreased to below laboratory
method detection limits. Based on the direction of groundwater flow at the site, the groundwater
plume has been defined.

ECS recommends installing remedial devices in wells MW-2/RW-2 and MW-3/RW-3 and
conducting sampling of the wells approximately six months following remedial device installation.

FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
ELKIN NORTH, NC QUADRANGLE
DATED 1971, REVISED 1994
FIGURE 1
USGS TOPOGRAPHIC MAP
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 49:6166-A
SITE
APPROXIMATE SITE BOUNDARY
SCALE (IN FEET)2,000 1,000 0 2,000
SOURCE:
SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013
FIGURE 2AERIAL SITE MAP
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 49:6166-A
APPROXIMATE SITE BOUNDARY
SCALE (IN FEET)100 50 0 100
SOURCE:
S&ME MONITORING REPORT, DATED 2010
FIGURE 3MONITORING WELL LOCATION MAP
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 49:6166-A
SCALE (IN FEET)100 50 0 100
EXISTING BUILDING
SOURCE:
S&ME MONITORING REPORT
DATED 2010
FIGURE 4GROUNDWATER CONTOUR MAP
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 49:6166-A
SCALE (IN FEET)100 50 0 100
(79.09)
(75.47)
(75.99)
(78.82)
NM
NM
NM
NM
NM
EXISTING BUILDING
79.0
78.0
77.0
76.0
SOURCE:
S&ME MONITORING REPORT
DATED 2010
FIGURE 5GROUNDWATER ANALYTICAL MAP
JERRY’S PLACE
983 US HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 49:6166-A
SCALE (IN FEET)100 50 0 100
EXISTING BUILDING
MW-2/RW-2
Benzene 583Ethylbenzene1,230Isopropylbenzene76Naphthalene504
n-Propylbenzene 200
Toluene 1,040
1,2,4-Trimethylbenzene 1,530
1,3,5-Trimethylbenzene 414
Xylenes (total)4,650
MW-3/RW-3
Benzene 17
Ethylbenzene 145
Isopropylbenzene 64
Naphthalene 299
n-Propylbenzene 166
Toluene 11.4
1,2,4-Trimethylbenzene 796
1,3,5-Trimethylbenzene 196
Xylenes (total)485
MW-4/RW-4
BRL
MW-5
BRL
Results presented in micrograms per liter (µg/L)
BOLD = concentration greater than NC2LGWQSBRL = below reporting limit

TABLES
Page 1 of 2
TABLE 1
MONITORING WELL INFORMATION AND GROUNDWATER ELEVATION DATA
Jerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Well ID Casing Diameter (in)Screened Interval (x to y ft)Top of Casing Elevation (ft)Date Measured
Depth to
Water (ft BTOC)
Depth to
LNAPL (ft BTOC)
LNAPL Thickness (ft)Groundwater Elevation* (ft)
05/24/93 16.20 NM NA 85.25
01/31/94 21.51 NM NA 79.94
03/15/94 19.77 NM NA 19.77
05/24/93 13.30 NM NA 84.69
01/31/94 18.70 17.92 0.78 79.36
03/15/94 16.97 16.28 0.69 81.08
09/24/08 Unknown Unknown 0.05 Unknown
10/07/09 19.97 NM NA 78.02
04/22/10 15.31 NM NA 82.68
09/13/11 22.04 NM NA 75.95
06/27/14 17.36 NM NA 80.63
09/22/15 22.28 NM NA 75.71
02/20/18 23.00 NM NA 74.99
12/12/19 18.90 NM NA 79.09
05/24/93 12.80 NM NA 84.06
01/31/94 17.35 NM NA 79.51
03/15/94 15.68 NM NA 81.18
10/07/09 19.14 NM NA 77.72
04/22/10 14.70 NM NA 82.16
09/13/11 21.51 NM NA 75.35
09/22/15 21.31 NM NA 75.55
02/20/18 22.75 NM NA 74.11
12/12/19 18.04 NM NA 78.82
05/24/93 15.95 NM NA 79.99
01/31/94 19.88 NM NA 76.06
03/15/94 18.71 NM NA 77.23
10/07/09 20.99 NM NA 74.95
04/22/10 17.41 NM NA 78.53
09/13/11 22.64 NM NA 73.30
06/27/14 18.55 NM NA 77.39
09/22/15 22.35 NM NA 73.59
02/20/18 23.25 NM NA 72.69
12/12/19 19.95 NM NA 75.99
05/24/93 1.98 NM NA 78.59
01/31/94 4.99 NM NA 75.58
03/15/94 4.14 NM NA 76.43
10/07/09 5.88 NM NA 74.69
04/22/10 3.38 NM NA 77.19
09/13/11 7.51 NM NA 73.06
06/27/14 4.30 NM NA 76.27
09/22/15 7.61 NM NA 72.96
02/20/18 6.73 NM NA 73.84
12/12/19 5.10 NM NA 75.47
01/31/94 19.25 NM NA 80.38
03/15/94 17.36 NM NA 82.27
10/07/09 21.22 NM NA 78.41
04/22/10 16.19 NM NA 83.44
09/13/11 23.36 NM NA 76.27
06/27/14 18.40 NM NA 81.23
2.0
15.5
101.45
99.63
MW-1
MW-2/RW-2
MW-4/RW-4
MW-3/RW-3
2.0
4.0
4.0
4.0
25.5toMW-6
15.0to
97.9932.0to12.0
9.0
2.0 to 12.0 95.94
96.8630.0to10.0
80.5725.5to15.52.0MW-5
Page 2 of 2
TABLE 1
MONITORING WELL INFORMATION AND GROUNDWATER ELEVATION DATA
Jerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Well ID Casing Diameter (in)Screened Interval (x to y ft)Top of Casing Elevation (ft)Date Measured
Depth to
Water (ft BTOC)
Depth to
LNAPL (ft BTOC)
LNAPL Thickness (ft)Groundwater Elevation* (ft)
01/31/94 24.10 NM NA 73.10
03/15/94 22.81 NM NA 74.39
10/07/09 24.43 NM NA 72.77
04/22/10 21.83 NM NA 75.37
09/13/11 DRY NM NA NA
09/28/11 DRY NM NA NA
06/27/14 23.40 NM NA 73.80
01/31/94 23.96 NM NA 74.55
03/15/94 22.42 NM NA 76.09
10/07/09 24.38 NM NA 74.13
04/22/10 21.10 NM NA 77.41
09/13/11 DRY NM NA NA
09/28/11 DRY NM NA NA
06/27/14 22.98 NM NA 75.53
Notes:
Top-of-casing elevations referenced to arbitrary benchmark of 100.00 feet
* If LNAPL is present, groundwater elevation is calculated by : [Top of Casing Elevation - DW] + [FP thickness x 0.8581]
in = inches
ft = feet
ft BTOC = feet below top-of-casing
LNAPL = Light Non-Aqueous Phase Liquid
NM = Not measured
NA = Not applicable
98.51
15.5
15.5
97.20
25.5to
2.0
2.0
25.5toMW-7
MW-8
Page 1 of 3
TABLE 2
SUMMARY OF CURRENT AND HISTORICAL GROUNDWATER ANALYTICAL DATAJerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Voaltile Organic Compounds by Standard Method 6200B or equivalent
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneEthylbenzeneIsopropylbenzeneIsopropyl etherp-IsopropyltolueneMethyl butyl ketoneMethyl ethyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)NC2LGWQS 6,000 1 70 70 70 600 70 70 25 280 4,000 20 6 70 600 400 400 500
GCLs 6,000,000 5,000 6,900 8,500 15,000 84,500 25,000 70,000 11,700 280,000 4,000,000 20,000 6,000 30,000 260,000 28,500 25,500 85,500
Sample DateSample ID
MW-1 05/24/93 NA 5 NA NA NA <1 NA NA NA NA NA 41 NA NA <1 NA NA <1
05/23/93 NA 14,000 NA NA NA 2000 NA NA NA NA NA 25,000 NA NA 54,000 NA NA 17,000
10/07/09 2,400 2,400 26 17 <5 960 95 70 13 NA 130 380 590 <5 800 350 100 1,230
04/22/10 1,700 1,700 63 44 <20 1,200 100 78 40 <5 170 260 600 <20 1,400 1,300 420 3,800
09/13/11 230J 2,300 23 20 <1.4 1,300 91 56 <2.4 100 <33 220 560 180 4,000 1,500 460 5,500
06/27/14 <25 1,830 21 <0.5 <0.5 1,530 80 16 28.8 <5 <25 <0.5 761 224 6,390 2,300 600 7,320
09/22/15 <25 1,410 <0.5 <0.5 <0.5 1,270 100 20.6 <0.5 <0.5 <0.5 74 403 <0.5 1,120 2,010 599 4,750
02/20/18 <25 1,300 20 14 <0.5 750 110 19.0 <0.5 8.4 J <0.5 51 230 150 150 590 230 1,200
12/12/19 NA 583 <6.2 <6.2 <6.2 1,230 76 <6.2 NA NA NA <6.2 504 200 1,040 1,530 414 4,650
05/24/93 NA 9,200 NA NA NA 1,100 NA NA NA NA NA 17,000 NA NA 26,000 NA NA 7,900
10/07/09 600 600 50 29 <5 910 120 16 21 NA 270 79 570 <5 1,500 2,300 620 5,600
04/22/10 130 130 76 52 <20 840 130 <20 45 <4.5 300 56 660 <20 750 2,900 840 6,700
09/13/11 <60 180 44 34 <4.3 730 100 <1.7 <2.4 32J <33 <2.2 490 250 210 2,000 570 3,900
06/27/14 <25 93.8 23.3 15.9 <5 381 84.9 <20 22.1 <5 <25 <0.5 448 185 80.2 1,350 393 2,060
09/22/15 <25 79.1 <0.5 17.8 <0.5 234 78.7 <0.5 <0.5 <0.5 <0.5 <0.5 175 174 23.5 1,160 333 1,010
02/20/18 <25 54 28 19 <0.5 110 68 <0.5 <0.5 <0.5 <0.5 <0.5 160 140 4.3 580 170 290
12/12/19 NA 17 <2.5 <2.5 <2.5 145 64 <2.5 NA NA NA <2.5 299 166 11.4 796 196 485
05/24/93 NA 540 NA NA NA <1 NA NA NA NA NA 380 NA NA 92 NA NA 450
10/07/09 NA 430 19 12 0.91 5.3 110 9.2 4.1 NA 34 62 520 <0.11 3.8 12 3.6 15.4
04/22/10 NA 250 8.5 6.5 0.83 1.5 50 6.8 2.3 <0.11 14 59 140 <0.44 2.4 7.6 1.6 11
09/13/11 <15 190 12 11 <1.1 <5 93 <0.42 <5.9 <1.1 <8.3 42 210 20 <0.57 <0.38 <0.38 10.7J
06/27/14 <25 7.55 0.63 2.3 <5 <1 15.5 0.85 <2.5 <5 <25 7.14 5.43 2.42 <5 0.8 <0.5 <5
09/22/15 <25 14.4 <0.5 3.8 <0.5 <0.5 23.1 1.1 <0.5 <0.5 <0.5 8.9 13.5 1.4 <0.5 <0.5 <0.5 <1
02/20/18 <25 6.4 1.1 3.5 <0.5 <0.5 15 0.66 <0.5 <0.5 <0.5 4.5 4.5 1.4 <0.5 <0.5 <0.5 <1
12/12/19 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <1.5
MW-4/RW-4
MW-3/
RW-3
MW-2/
RW-2
Page 2 of 3
TABLE 2
SUMMARY OF CURRENT AND HISTORICAL GROUNDWATER ANALYTICAL DATAJerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Voaltile Organic Compounds by Standard Method 6200B or equivalent
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneEthylbenzeneIsopropylbenzeneIsopropyl etherp-IsopropyltolueneMethyl butyl ketoneMethyl ethyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)NC2LGWQS 6,000 1 70 70 70 600 70 70 25 280 4,000 20 6 70 600 400 400 500
GCLs 6,000,000 5,000 6,900 8,500 15,000 84,500 25,000 70,000 11,700 280,000 4,000,000 20,000 6,000 30,000 260,000 28,500 25,500 85,500
Sample DateSample ID
05/24/93 NA 4 NA NA NA 2 NA NA NA NA NA 48 NA NA 19 NA NA 23
10/07/09 11 11 1.4 1.1 <0.5 2.3 2.9 <0.5 0.98 NA 0.66 3.8 6.8 <0.5 <0.5 5.5 0.98 6.6
04/22/10 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.1 <0.5 0.92 <1 <0.5 <0.5 <0.5 <0.5 <1
09/13/11 <1.5 <0.054 <0.059 <0.054 <0.11 <0.054 <0.034 <0.41 <0.059 <0.11 <0.83 <0.056 <0.094 <0.059 <0.057 <0.038 <0.038 <0.11
06/27/14 <25 <0.5 <0.5 <0.5 <5 <1 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
09/22/15 <25 <0.5 <0.5 <0.5 <5 <1 <0.5 <0.5 <0.5 <5 <0.5 0.75 <0.5 <0.5 <5 <0.5 <0.5 <0.5
02/20/18 <25 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.75 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
12/12/19 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <1.5
01/31/94 NA <1 NA NA NA <1 NA NA NA NA NA <1 NA NA <1 NA NA <1
10/07/09 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <2 <0.5 <0.5 <0.5 <0.5 <1
04/22/10 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.11 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <1
09/13/11 <1.5 <0.054 <0.059 <0.054 <0.11 <0.054 <0.034 <0.41 <0.059 <0.11 <0.83 <0.056 <0.0094 <0.059 <0.057 <0.038 <0.038 <0.11
06/27/14 <25 <0.5 <0.5 <0.5 <5 <1 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
01/31/94 NA <1 NA NA NA <1 NA NA NA NA NA <1 NA NA <1 NA NA <1
10/07/09 NO SAMPLE COLLECTED - INSUFFICENT WATER VOLUME
04/22/10 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.11 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <1
09/13/11 NO SAMPLE COLLECTED - INSUFFICENT WATER VOLUME
06/27/14 <25 <0.5 <0.5 <0.5 <5 <1 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
03/16/94 NA 2 NA NA NA 2 NA NA NA NA NA 1 NA NA 6 NA NA 6
10/07/09 NO SAMPLE COLLECTED - INSUFFICENT WATER VOLUME
04/22/10 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.11 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <1
09/13/11 NO SAMPLE COLLECTED - INSUFFICENT WATER VOLUME
06/27/14 <25 <0.5 <0.5 <0.5 <5 <1 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
MW-8
MW-5
MW-6
MW-7
Page 3 of 3
TABLE 2
SUMMARY OF CURRENT AND HISTORICAL GROUNDWATER ANALYTICAL DATAJerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Voaltile Organic Compounds by Standard Method 6200B or equivalent
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneEthylbenzeneIsopropylbenzeneIsopropyl etherp-IsopropyltolueneMethyl butyl ketoneMethyl ethyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)NC2LGWQS 6,000 1 70 70 70 600 70 70 25 280 4,000 20 6 70 600 400 400 500
GCLs 6,000,000 5,000 6,900 8,500 15,000 84,500 25,000 70,000 11,700 280,000 4,000,000 20,000 6,000 30,000 260,000 28,500 25,500 85,500
Sample DateSample ID
10/07/09 300 300 14 9.9 <0.5 1,100 85 6.2 6.3 <5 170 34 560 <5 580 1,100 300 3,300
04/22/10 470 470 14 11 <5 550 51 20 9.8 <5 57 68 150 <5 330 280 84 950
09/13/11 <0.59 110 6.4 9.6 <1.1 12,000 83 <0.42 <0.59 7.8J <8.3 15 380 160 300 1,100 260 2,700
06/27/14 <25 <0.5 <0.5 <0.5 <5 468 35.5 <0.5 <0.5 <5 <0.5 <0.5 238 103 477 794 164 1,290
Notes:
Only compounds detected are shown
All concentrations reported in micrograms per liter (µg/L)
NC2LGWQS = North Carolina 2L Groundwater Quality Standard
GCL= Gross Contamination Level
J = Estimated concentration between laborator method reporting limit and detection limit
NA = Not analyzed for constituent
VALUE = concentration exceeds laboratory method reporting limit
VALUE = concentration exceeds NC2LGWQS
VALUE = concentration exceeds GCL
RW-5
Page 1 of 2
TABLE 3
SUMMARY OF CURRENT AND HISTORICAL WATER SUPPLY WELL ANALYTICAL DATAJerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Voaltile Organic Compounds by Standard Method 6200B or equivalent
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneDiisopropyl etherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethyl butyl ketoneMethyl ethyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)NC2LGWQS 6,000 1 70 70 70 70 600 70 25 280 4,000 20 6 70 600 400 400 500
GCLs 6,000,000 5,000 6,900 8,500 15,000 70,000 84,500 25,000 11,700 280,000 4,000,000 20,000 6,000 30,000 260,000 28,500 25,500 85,500
10/07/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
10/25/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/09/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/27/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/07/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
10/25/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
05/09/11 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
09/13/11 <1.5 <0.054 <0.059 <0.054 <0.11 <0.41 <0.054 <0.034 <0.059 <0.11 <0.83 <0.056 <0.094 <0.059 <0.057 <0.038 <0.038 <.11
06/27/14 <25 <0.5 <0.5 <0.5 <5 <0.5 <1 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
10/07/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
10/25/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
05/09/11 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
09/13/11 <1.5 <0.054 <0.059 <0.054 <0.11 <0.41 <0.054 <0.034 <0.059 <0.11 <0.83 <0.056 <0.094 <0.059 <0.057 <0.038 <0.038 <.11
06/27/14 <25 <0.5 <0.5 <0.5 <5 <0.5 <1 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
10/07/09 <10 2.5 1.4 1 <0.5 0.6 1.2 0.66 1 NA <5 5 5 NA <0.5 14 2.4 15.5
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.11 <5 2.9 <1 NA <0.5 <0.5 <0.5 <1
10/25/10 210 <0.5 <1 <0.5 <0.5 0.84 <0.5 <0.5 <0.5 <0.11 220 11 <1 NA <0.5 <0.5 <0.5 <1
05/09/11 <10 0.58 <1 <0.5 <0.5 0.53 <0.5 <0.5 <0.5 <0.11 <5 7.4 <1 NA <0.5 <0.5 <0.5 <1
06/27/14 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 1.73 <1 NA <0.5 <0.5 <0.5 <1
09/22/15 <25 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.6 <0.5 <0.5 <0.5 <0.5 <0.5 <1
02/20/18 <25 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.2 <0.5 <0.5 <0.5 <0.5 <0.5 <1
12/12/19 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
WSW-5
Sample ID Sample Date
WSW-2
WSW-3
WSW-4
Page 2 of 2
TABLE 3
SUMMARY OF CURRENT AND HISTORICAL WATER SUPPLY WELL ANALYTICAL DATAJerry's Place
983 US Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
ECS Project No.: 49:6166-A
Voaltile Organic Compounds by Standard Method 6200B or equivalent
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneDiisopropyl etherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethyl butyl ketoneMethyl ethyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)NC2LGWQS 6,000 1 70 70 70 70 600 70 25 280 4,000 20 6 70 600 400 400 500
GCLs 6,000,000 5,000 6,900 8,500 15,000 70,000 84,500 25,000 11,700 280,000 4,000,000 20,000 6,000 30,000 260,000 28,500 25,500 85,500
Sample ID Sample Date
10/07/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
10/25/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
05/09/11 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <5 <0.5 <1 NA <0.5 <0.5 <0.5 <1
09/13/11 <1.5 <0.054 <0.059 <0.054 <0.11 <0.41 <0.054 <0.034 <0.059 <0.11 <0.83 <0.056 <0.094 <0.059 <0.057 <0.038 <0.038 <.11
06/27/14 <25 <0.5 <0.5 <0.5 <5 <0.5 <1 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5
10/07/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/22/10 <10 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <5 <0.5 <1 NS <0.5 <0.5 <0.5 <1
10/25/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/09/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/27/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
Only compounds detected are shown
All concentrations reported in micrograms per liter (µg/L)
NC2LGWQS = North Carolina 2L Groundwater Quality Standard
GCL= Gross Contamination Level
J = Estimated concentration between laborator method reporting limit and detection limit
NA = Not analyzed for constituent
NS = Not sampled
VALUE = concentration exceeds laboratory method reporting limit
VALUE = concentration exceeds NC2LGWQS
VALUE = concentration exceeds GCL
WSW-13
WSW-6

APPENDIX A
Jerry’s Place NCDEQ Incident #9547
State Road, Surry County, North Carolina
ECS Project No. 49:6166-A
ECS Southeast, LLP Page 1
Photo 1: View of active automotive repair and painting facility onsite.
Photo 2: View of four inch monitoring well and vault (MW-4).
Jerry’s Place NCDEQ Incident #9547
State Road, Surry County, North Carolina
ECS Project No. 49:6166-A
ECS Southeast, LLP Page 2
Photo 3: View of MW-2, MW-3 locations, looking north.
Photo 4: View of car dealership onsite.

APPENDIX B
#=CL#
December 24, 2019
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92457956
92457956
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1900 Center Park Dr
Charlotte, NC 28217
Jerry's Place
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 25
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92457956
Jerry's Place
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 25
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID Matrix Date Collected Date Received
92457956001 MW-2 Water 12/12/19 14:20 12/18/19 08:17
92457956002 MW-3 Water 12/12/19 15:00 12/18/19 08:17
92457956003 MW-4 Water 12/12/19 15:50 12/18/19 08:17
92457956004 MW-5 Water 12/12/19 13:35 12/18/19 08:17
92457956005 WSW-5 Water 12/12/19 13:00 12/18/19 08:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 25
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92457956001 MW-2 SM 6200B 63 PASI-CCL
92457956002 MW-3 SM 6200B 63 PASI-CCL
92457956003 MW-4 SM 6200B 63 PASI-CCL
92457956004 MW-5 SM 6200B 63 PASI-CCL
92457956005 WSW-5 SM 6200B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 25
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92457956
Jerry's Place
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92457956001 MW-2
Benzene 583 ug/L 12/22/19 13:516.2SM 6200B
Ethylbenzene 1230 ug/L 12/22/19 13:516.2SM 6200B
Isopropylbenzene (Cumene)75.7 ug/L 12/22/19 13:516.2SM 6200B
Naphthalene 504 ug/L 12/22/19 13:5125.0SM 6200B
n-Propylbenzene 200 ug/L 12/22/19 13:516.2SM 6200B
Toluene 1040 ug/L 12/22/19 13:516.2SM 6200B
1,2,4-Trimethylbenzene 1530 ug/L 12/22/19 13:516.2SM 6200B
1,3,5-Trimethylbenzene 414 ug/L 12/22/19 13:516.2SM 6200B
m&p-Xylene 2940 ug/L 12/22/19 13:5112.5SM 6200B
o-Xylene 1710 ug/L 12/22/19 13:516.2SM 6200B
92457956002 MW-3
Benzene 17.0 ug/L 12/22/19 13:152.5SM 6200B
Ethylbenzene 145 ug/L 12/22/19 13:152.5SM 6200B
Isopropylbenzene (Cumene)64.0 ug/L 12/22/19 13:152.5SM 6200B
Naphthalene 299 ug/L 12/22/19 13:1510.0SM 6200B
n-Propylbenzene 166 ug/L 12/22/19 13:152.5SM 6200B
Toluene 11.4 ug/L 12/22/19 13:152.5SM 6200B
1,2,4-Trimethylbenzene 796 ug/L 12/22/19 13:152.5SM 6200B
1,3,5-Trimethylbenzene 196 ug/L 12/22/19 13:152.5SM 6200B
m&p-Xylene 235 ug/L 12/22/19 13:155.0SM 6200B
o-Xylene 250 ug/L 12/22/19 13:152.5SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-2 Lab ID:92457956001 Collected:12/12/19 14:20 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 583 ug/L 12/22/19 13:51 71-43-26.2 3.0 12.5
Bromobenzene ND ug/L 12/22/19 13:51 108-86-16.2 2.7 12.5
Bromochloromethane ND ug/L 12/22/19 13:51 74-97-56.2 3.2 12.5
Bromodichloromethane ND ug/L 12/22/19 13:51 75-27-46.2 2.3 12.5
Bromoform ND ug/L 12/22/19 13:51 75-25-26.2 5.1 12.5
Bromomethane ND ug/L 12/22/19 13:51 74-83-962.5 21.5 12.5
n-Butylbenzene ND ug/L 12/22/19 13:51 104-51-86.2 4.4 12.5
sec-Butylbenzene ND ug/L 12/22/19 13:51 135-98-86.2 3.1 12.5
tert-Butylbenzene ND ug/L 12/22/19 13:51 98-06-66.2 3.1 12.5
Carbon tetrachloride ND ug/L 12/22/19 13:51 56-23-56.2 2.9 12.5
Chlorobenzene ND ug/L 12/22/19 13:51 108-90-76.2 2.8 12.5
Chloroethane ND ug/L 12/22/19 13:51 75-00-312.5 7.3 12.5
Chloroform ND ug/L 12/22/19 13:51 67-66-36.2 4.4 12.5
Chloromethane ND ug/L 12/22/19 13:51 74-87-312.5 5.2 12.5
2-Chlorotoluene ND ug/L 12/22/19 13:51 95-49-86.2 2.6 12.5
4-Chlorotoluene ND ug/L 12/22/19 13:51 106-43-46.2 2.6 12.5
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 13:51 96-12-812.5 4.8 12.5
Dibromochloromethane ND ug/L 12/22/19 13:51 124-48-16.2 5.0 12.5
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 13:51 106-93-46.2 2.9 12.5
Dibromomethane ND ug/L 12/22/19 13:51 74-95-36.2 3.9 12.5
1,2-Dichlorobenzene ND ug/L 12/22/19 13:51 95-50-16.2 3.0 12.5
1,3-Dichlorobenzene ND ug/L 12/22/19 13:51 541-73-16.2 3.1 12.5
1,4-Dichlorobenzene ND ug/L 12/22/19 13:51 106-46-76.2 3.1 12.5
Dichlorodifluoromethane ND ug/L 12/22/19 13:51 75-71-86.2 3.6 12.5
1,1-Dichloroethane ND ug/L 12/22/19 13:51 75-34-36.2 3.0 12.5
1,2-Dichloroethane ND ug/L 12/22/19 13:51 107-06-26.2 3.3 12.5
1,1-Dichloroethene ND ug/L 12/22/19 13:51 75-35-46.2 2.7 12.5
cis-1,2-Dichloroethene ND ug/L 12/22/19 13:51 156-59-26.2 2.6 12.5
trans-1,2-Dichloroethene ND ug/L 12/22/19 13:51 156-60-56.2 3.2 12.5
1,2-Dichloropropane ND ug/L 12/22/19 13:51 78-87-56.2 2.3 12.5
1,3-Dichloropropane ND ug/L 12/22/19 13:51 142-28-96.2 4.3 12.5
2,2-Dichloropropane ND ug/L 12/22/19 13:51 594-20-76.2 3.5 12.5
1,1-Dichloropropene ND ug/L 12/22/19 13:51 563-58-66.2 4.4 12.5
cis-1,3-Dichloropropene ND ug/L 12/22/19 13:51 10061-01-56.2 4.5 12.5
trans-1,3-Dichloropropene ND ug/L 12/22/19 13:51 10061-02-66.2 4.9 12.5
Diisopropyl ether ND ug/L 12/22/19 13:51 108-20-36.2 4.2 12.5
Ethylbenzene 1230 ug/L 12/22/19 13:51 100-41-46.2 3.0 12.5
Hexachloro-1,3-butadiene ND ug/L 12/22/19 13:51 87-68-325.0 15.0 12.5
Isopropylbenzene (Cumene)75.7 ug/L 12/22/19 13:51 98-82-86.2 3.0 12.5
Methylene Chloride ND ug/L 12/22/19 13:51 75-09-225.0 18.8 12.5
Methyl-tert-butyl ether ND ug/L 12/22/19 13:51 1634-04-46.2 5.6 12.5
Naphthalene 504 ug/L 12/22/19 13:51 91-20-325.0 8.2 12.5
n-Propylbenzene 200 ug/L 12/22/19 13:51 103-65-16.2 3.0 12.5
Styrene ND ug/L 12/22/19 13:51 100-42-56.2 3.2 12.5
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 13:51 630-20-66.2 5.3 12.5
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 13:51 79-34-56.2 2.4 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-2 Lab ID:92457956001 Collected:12/12/19 14:20 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 13:51 127-18-46.2 2.9 12.5
Toluene 1040 ug/L 12/22/19 13:51 108-88-36.2 2.8 12.5
1,2,3-Trichlorobenzene ND ug/L 12/22/19 13:51 87-61-625.0 9.8 12.5
1,2,4-Trichlorobenzene ND ug/L 12/22/19 13:51 120-82-125.0 5.4 12.5
1,1,1-Trichloroethane ND ug/L 12/22/19 13:51 71-55-66.2 3.5 12.5
1,1,2-Trichloroethane ND ug/L 12/22/19 13:51 79-00-56.2 2.9 12.5
Trichloroethene ND ug/L 12/22/19 13:51 79-01-66.2 2.9 12.5
Trichlorofluoromethane ND ug/L 12/22/19 13:51 75-69-412.5 4.2 12.5
1,2,3-Trichloropropane ND ug/L 12/22/19 13:51 96-18-46.2 3.4 12.5
1,2,4-Trimethylbenzene 1530 ug/L 12/22/19 13:51 95-63-66.2 2.4 12.5
1,3,5-Trimethylbenzene 414 ug/L 12/22/19 13:51 108-67-86.2 2.8 12.5
Vinyl chloride ND ug/L 12/22/19 13:51 75-01-412.5 5.1 12.5
m&p-Xylene 2940 ug/L 12/22/19 13:51 179601-23-112.5 5.5 12.5
o-Xylene 1710 ug/L 12/22/19 13:51 95-47-66.2 3.0 12.5
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/22/19 13:51 17060-07-070-130 12.5
4-Bromofluorobenzene (S)97 %12/22/19 13:51 460-00-470-130 12.5
Toluene-d8 (S)100 %12/22/19 13:51 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-3 Lab ID:92457956002 Collected:12/12/19 15:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 17.0 ug/L 12/22/19 13:15 71-43-22.5 1.2 5
Bromobenzene ND ug/L 12/22/19 13:15 108-86-12.5 1.1 5
Bromochloromethane ND ug/L 12/22/19 13:15 74-97-52.5 1.3 5
Bromodichloromethane ND ug/L 12/22/19 13:15 75-27-42.5 0.92 5
Bromoform ND ug/L 12/22/19 13:15 75-25-22.5 2.0 5
Bromomethane ND ug/L 12/22/19 13:15 74-83-925.0 8.6 5
n-Butylbenzene ND ug/L 12/22/19 13:15 104-51-82.5 1.8 5
sec-Butylbenzene ND ug/L 12/22/19 13:15 135-98-82.5 1.2 5
tert-Butylbenzene ND ug/L 12/22/19 13:15 98-06-62.5 1.2 5
Carbon tetrachloride ND ug/L 12/22/19 13:15 56-23-52.5 1.2 5
Chlorobenzene ND ug/L 12/22/19 13:15 108-90-72.5 1.1 5
Chloroethane ND ug/L 12/22/19 13:15 75-00-35.0 2.9 5
Chloroform ND ug/L 12/22/19 13:15 67-66-32.5 1.8 5
Chloromethane ND ug/L 12/22/19 13:15 74-87-35.0 2.1 5
2-Chlorotoluene ND ug/L 12/22/19 13:15 95-49-82.5 1.0 5
4-Chlorotoluene ND ug/L 12/22/19 13:15 106-43-42.5 1.0 5
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 13:15 96-12-85.0 1.9 5
Dibromochloromethane ND ug/L 12/22/19 13:15 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 13:15 106-93-42.5 1.2 5
Dibromomethane ND ug/L 12/22/19 13:15 74-95-32.5 1.6 5
1,2-Dichlorobenzene ND ug/L 12/22/19 13:15 95-50-12.5 1.2 5
1,3-Dichlorobenzene ND ug/L 12/22/19 13:15 541-73-12.5 1.2 5
1,4-Dichlorobenzene ND ug/L 12/22/19 13:15 106-46-72.5 1.2 5
Dichlorodifluoromethane ND ug/L 12/22/19 13:15 75-71-82.5 1.4 5
1,1-Dichloroethane ND ug/L 12/22/19 13:15 75-34-32.5 1.2 5
1,2-Dichloroethane ND ug/L 12/22/19 13:15 107-06-22.5 1.3 5
1,1-Dichloroethene ND ug/L 12/22/19 13:15 75-35-42.5 1.1 5
cis-1,2-Dichloroethene ND ug/L 12/22/19 13:15 156-59-22.5 1.0 5
trans-1,2-Dichloroethene ND ug/L 12/22/19 13:15 156-60-52.5 1.3 5
1,2-Dichloropropane ND ug/L 12/22/19 13:15 78-87-52.5 0.92 5
1,3-Dichloropropane ND ug/L 12/22/19 13:15 142-28-92.5 1.7 5
2,2-Dichloropropane ND ug/L 12/22/19 13:15 594-20-72.5 1.4 5
1,1-Dichloropropene ND ug/L 12/22/19 13:15 563-58-62.5 1.7 5
cis-1,3-Dichloropropene ND ug/L 12/22/19 13:15 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 12/22/19 13:15 10061-02-62.5 2.0 5
Diisopropyl ether ND ug/L 12/22/19 13:15 108-20-32.5 1.7 5
Ethylbenzene 145 ug/L 12/22/19 13:15 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene ND ug/L 12/22/19 13:15 87-68-310.0 6.0 5
Isopropylbenzene (Cumene)64.0 ug/L 12/22/19 13:15 98-82-82.5 1.2 5
Methylene Chloride ND ug/L 12/22/19 13:15 75-09-210.0 7.5 5
Methyl-tert-butyl ether ND ug/L 12/22/19 13:15 1634-04-42.5 2.2 5
Naphthalene 299 ug/L 12/22/19 13:15 91-20-310.0 3.3 5
n-Propylbenzene 166 ug/L 12/22/19 13:15 103-65-12.5 1.2 5
Styrene ND ug/L 12/22/19 13:15 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 13:15 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 13:15 79-34-52.5 0.96 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
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Page 8 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-3 Lab ID:92457956002 Collected:12/12/19 15:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 13:15 127-18-42.5 1.2 5
Toluene 11.4 ug/L 12/22/19 13:15 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene ND ug/L 12/22/19 13:15 87-61-610.0 3.9 5
1,2,4-Trichlorobenzene ND ug/L 12/22/19 13:15 120-82-110.0 2.2 5
1,1,1-Trichloroethane ND ug/L 12/22/19 13:15 71-55-62.5 1.4 5
1,1,2-Trichloroethane ND ug/L 12/22/19 13:15 79-00-52.5 1.2 5
Trichloroethene ND ug/L 12/22/19 13:15 79-01-62.5 1.2 5
Trichlorofluoromethane ND ug/L 12/22/19 13:15 75-69-45.0 1.7 5
1,2,3-Trichloropropane ND ug/L 12/22/19 13:15 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 796 ug/L 12/22/19 13:15 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene 196 ug/L 12/22/19 13:15 108-67-82.5 1.1 5
Vinyl chloride ND ug/L 12/22/19 13:15 75-01-45.0 2.0 5
m&p-Xylene 235 ug/L 12/22/19 13:15 179601-23-15.0 2.2 5
o-Xylene 250 ug/L 12/22/19 13:15 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/22/19 13:15 17060-07-070-130 5
4-Bromofluorobenzene (S)96 %12/22/19 13:15 460-00-470-130 5
Toluene-d8 (S)99 %12/22/19 13:15 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-4 Lab ID:92457956003 Collected:12/12/19 15:50 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 15:21 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 15:21 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 15:21 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 15:21 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 15:21 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 15:21 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 15:21 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 15:21 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 15:21 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 15:21 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 15:21 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 15:21 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 15:21 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 15:21 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 15:21 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 15:21 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 15:21 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 15:21 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 15:21 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 15:21 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 15:21 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 15:21 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 15:21 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 15:21 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 15:21 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 15:21 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 15:21 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 15:21 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 15:21 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 15:21 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 15:21 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 15:21 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 15:21 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 15:21 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 15:21 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 15:21 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 15:21 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 15:21 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 15:21 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 15:21 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 15:21 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 15:21 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 15:21 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 15:21 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 15:21 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 15:21 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-4 Lab ID:92457956003 Collected:12/12/19 15:50 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 15:21 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 15:21 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 15:21 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 15:21 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 15:21 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 15:21 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 15:21 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 15:21 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 15:21 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 15:21 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 15:21 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 15:21 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 15:21 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 15:21 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/22/19 15:21 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %12/22/19 15:21 460-00-470-130 1
Toluene-d8 (S)100 %12/22/19 15:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-5 Lab ID:92457956004 Collected:12/12/19 13:35 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 15:03 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 15:03 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 15:03 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 15:03 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 15:03 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 15:03 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 15:03 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 15:03 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 15:03 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 15:03 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 15:03 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 15:03 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 15:03 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 15:03 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 15:03 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 15:03 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 15:03 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 15:03 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 15:03 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 15:03 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 15:03 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 15:03 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 15:03 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 15:03 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 15:03 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 15:03 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 15:03 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 15:03 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 15:03 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 15:03 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 15:03 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 15:03 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 15:03 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 15:03 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 15:03 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 15:03 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 15:03 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 15:03 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 15:03 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 15:03 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 15:03 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 15:03 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 15:03 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 15:03 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 15:03 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 15:03 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-5 Lab ID:92457956004 Collected:12/12/19 13:35 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 15:03 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 15:03 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 15:03 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 15:03 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 15:03 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 15:03 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 15:03 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 15:03 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 15:03 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 15:03 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 15:03 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 15:03 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 15:03 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 15:03 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %12/22/19 15:03 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %12/22/19 15:03 460-00-470-130 1
Toluene-d8 (S)102 %12/22/19 15:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:WSW-5 Lab ID:92457956005 Collected:12/12/19 13:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 14:45 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 14:45 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 14:45 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 14:45 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 14:45 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 14:45 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 14:45 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 14:45 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 14:45 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 14:45 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 14:45 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 14:45 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 14:45 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 14:45 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 14:45 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 14:45 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 14:45 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 14:45 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 14:45 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 14:45 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 14:45 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 14:45 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 14:45 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 14:45 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 14:45 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 14:45 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 14:45 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 14:45 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 14:45 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 14:45 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 14:45 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 14:45 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 14:45 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 14:45 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 14:45 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 14:45 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 14:45 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 14:45 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 14:45 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 14:45 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 14:45 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 14:45 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 14:45 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 14:45 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 14:45 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 14:45 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 14 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:WSW-5 Lab ID:92457956005 Collected:12/12/19 13:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 14:45 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 14:45 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 14:45 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 14:45 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 14:45 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 14:45 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 14:45 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 14:45 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 14:45 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 14:45 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 14:45 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 14:45 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 14:45 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 14:45 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %12/22/19 14:45 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %12/22/19 14:45 460-00-470-130 1
Toluene-d8 (S)101 %12/22/19 14:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 15 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
516241
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2766036
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/22/19 11:460.42
1,1,1-Trichloroethane ug/L ND 0.50 12/22/19 11:460.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/22/19 11:460.19
1,1,2-Trichloroethane ug/L ND 0.50 12/22/19 11:460.23
1,1-Dichloroethane ug/L ND 0.50 12/22/19 11:460.24
1,1-Dichloroethene ug/L ND 0.50 12/22/19 11:460.22
1,1-Dichloropropene ug/L ND 0.50 12/22/19 11:460.35
1,2,3-Trichlorobenzene ug/L ND 2.0 12/22/19 11:460.78
1,2,3-Trichloropropane ug/L ND 0.50 12/22/19 11:460.27
1,2,4-Trichlorobenzene ug/L ND 2.0 12/22/19 11:460.44
1,2,4-Trimethylbenzene ug/L ND 0.50 12/22/19 11:460.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/22/19 11:460.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/22/19 11:460.23
1,2-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.24
1,2-Dichloroethane ug/L ND 0.50 12/22/19 11:460.26
1,2-Dichloropropane ug/L ND 0.50 12/22/19 11:460.18
1,3,5-Trimethylbenzene ug/L ND 0.50 12/22/19 11:460.23
1,3-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.25
1,3-Dichloropropane ug/L ND 0.50 12/22/19 11:460.34
1,4-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.25
2,2-Dichloropropane ug/L ND 0.50 12/22/19 11:460.28
2-Chlorotoluene ug/L ND 0.50 12/22/19 11:460.21
4-Chlorotoluene ug/L ND 0.50 12/22/19 11:460.21
Benzene ug/L ND 0.50 12/22/19 11:460.24
Bromobenzene ug/L ND 0.50 12/22/19 11:460.22
Bromochloromethane ug/L ND 0.50 12/22/19 11:460.26
Bromodichloromethane ug/L ND 0.50 12/22/19 11:460.18
Bromoform ug/L ND 0.50 12/22/19 11:460.40
Bromomethane ug/L ND 5.0 12/22/19 11:461.7
Carbon tetrachloride ug/L ND 0.50 12/22/19 11:460.23
Chlorobenzene ug/L ND 0.50 12/22/19 11:460.22
Chloroethane ug/L ND 1.0 12/22/19 11:460.58
Chloroform ug/L ND 0.50 12/22/19 11:460.35
Chloromethane ug/L ND 1.0 12/22/19 11:460.42
cis-1,2-Dichloroethene ug/L ND 0.50 12/22/19 11:460.21
cis-1,3-Dichloropropene ug/L ND 0.50 12/22/19 11:460.36
Dibromochloromethane ug/L ND 0.50 12/22/19 11:460.40
Dibromomethane ug/L ND 0.50 12/22/19 11:460.31
Dichlorodifluoromethane ug/L ND 0.50 12/22/19 11:460.28
Diisopropyl ether ug/L ND 0.50 12/22/19 11:460.33
Ethylbenzene ug/L ND 0.50 12/22/19 11:460.24
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Huntersville, NC 28078
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Page 16 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2766036
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Matrix:Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 12/22/19 11:461.2
Isopropylbenzene (Cumene)ug/L ND 0.50 12/22/19 11:460.24
m&p-Xylene ug/L ND 1.0 12/22/19 11:460.44
Methyl-tert-butyl ether ug/L ND 0.50 12/22/19 11:460.44
Methylene Chloride ug/L ND 2.0 12/22/19 11:461.5
n-Butylbenzene ug/L ND 0.50 12/22/19 11:460.35
n-Propylbenzene ug/L ND 0.50 12/22/19 11:460.24
Naphthalene ug/L ND 2.0 12/22/19 11:460.66
o-Xylene ug/L ND 0.50 12/22/19 11:460.24
sec-Butylbenzene ug/L ND 0.50 12/22/19 11:460.25
Styrene ug/L ND 0.50 12/22/19 11:460.26
tert-Butylbenzene ug/L ND 0.50 12/22/19 11:460.25
Tetrachloroethene ug/L ND 0.50 12/22/19 11:460.23
Toluene ug/L ND 0.50 12/22/19 11:460.23
trans-1,2-Dichloroethene ug/L ND 0.50 12/22/19 11:460.26
trans-1,3-Dichloropropene ug/L ND 0.50 12/22/19 11:460.39
Trichloroethene ug/L ND 0.50 12/22/19 11:460.23
Trichlorofluoromethane ug/L ND 1.0 12/22/19 11:460.34
Vinyl chloride ug/L ND 1.0 12/22/19 11:460.41
1,2-Dichloroethane-d4 (S)%90 70-130 12/22/19 11:46
4-Bromofluorobenzene (S)%96 70-130 12/22/19 11:46
Toluene-d8 (S)%102 70-130 12/22/19 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2766037LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.450 111 60-140
1,1,1-Trichloroethane ug/L 54.050 108 60-140
1,1,2,2-Tetrachloroethane ug/L 52.050 104 60-140
1,1,2-Trichloroethane ug/L 51.550 103 60-140
1,1-Dichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethene ug/L 50.450 101 60-140
1,1-Dichloropropene ug/L 56.650 113 60-140
1,2,3-Trichlorobenzene ug/L 62.550 125 60-140
1,2,3-Trichloropropane ug/L 52.250 104 60-140
1,2,4-Trichlorobenzene ug/L 61.050 122 60-140
1,2,4-Trimethylbenzene ug/L 57.250 114 60-140
1,2-Dibromo-3-chloropropane ug/L 57.250 114 60-140
1,2-Dibromoethane (EDB)ug/L 55.750 111 60-140
1,2-Dichlorobenzene ug/L 57.750 115 60-140
1,2-Dichloroethane ug/L 47.950 96 60-140
1,2-Dichloropropane ug/L 52.650 105 60-140
1,3,5-Trimethylbenzene ug/L 56.350 113 60-140
1,3-Dichlorobenzene ug/L 56.750 113 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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[phone]
Page 17 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2766037LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 55.850 112 60-140
1,4-Dichlorobenzene ug/L 57.850 116 60-140
2,2-Dichloropropane ug/L 62.850 126 60-140
2-Chlorotoluene ug/L 55.050 110 60-140
4-Chlorotoluene ug/L 56.450 113 60-140
Benzene ug/L 52.750 105 60-140
Bromobenzene ug/L 57.550 115 60-140
Bromochloromethane ug/L 52.350 105 60-140
Bromodichloromethane ug/L 53.650 107 60-140
Bromoform ug/L 57.150 114 60-140
Bromomethane ug/L 53.250 106 60-140
Carbon tetrachloride ug/L 56.150 112 60-140
Chlorobenzene ug/L 54.550 109 60-140
Chloroethane ug/L 58.650 117 60-140
Chloroform ug/L 50.650 101 60-140
Chloromethane ug/L 41.250 82 60-140
cis-1,2-Dichloroethene ug/L 50.150 100 60-140
cis-1,3-Dichloropropene ug/L 55.750 111 60-140
Dibromochloromethane ug/L 58.250 116 60-140
Dibromomethane ug/L 55.650 111 60-140
Dichlorodifluoromethane ug/L 48.150 96 60-140
Diisopropyl ether ug/L 51.250 102 60-140
Ethylbenzene ug/L 53.850 108 60-140
Hexachloro-1,3-butadiene ug/L 57.550 115 60-140
Isopropylbenzene (Cumene)ug/L 56.150 112 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 54.850 110 60-140
Methylene Chloride ug/L 46.850 94 60-140
n-Butylbenzene ug/L 58.450 117 60-140
n-Propylbenzene ug/L 54.950 110 60-140
Naphthalene ug/L 62.050 124 60-140
o-Xylene ug/L 55.050 110 60-140
sec-Butylbenzene ug/L 56.350 113 60-140
Styrene ug/L 58.050 116 60-140
tert-Butylbenzene ug/L 47.650 95 60-140
Tetrachloroethene ug/L 55.350 111 60-140
Toluene ug/L 51.550 103 60-140
trans-1,2-Dichloroethene ug/L 51.050 102 60-140
trans-1,3-Dichloropropene ug/L 55.050 110 60-140
Trichloroethene ug/L 53.550 107 60-140
Trichlorofluoromethane ug/L 49.950 100 60-140
Vinyl chloride ug/L 51.850 104 60-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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[phone]
Page 18 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2766038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457416003
2766039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 110 60-140105 4 30200ND220211
1,1,1-Trichloroethane ug/L 200 109 60-140107 2 30200ND219214
1,1,2,2-Tetrachloroethane ug/L 200 105 60-140100 5 30200ND210201
1,1,2-Trichloroethane ug/L 200 107 60-140105 2 30200ND214210
1,1-Dichloroethane ug/L 200 108 60-140104 3 30200ND216209
1,1-Dichloroethene ug/L 200 108 60-140103 4 30200ND216207
1,1-Dichloropropene ug/L 200 119 60-140114 4 30200ND238228
1,2,3-Trichlorobenzene ug/L 200 101 60-140109 7 30200ND207222
1,2,3-Trichloropropane ug/L 200 109 60-14099 10 30200ND219198
1,2,4-Trichlorobenzene ug/L 200 104 60-140109 4 30200ND208217
1,2,4-Trimethylbenzene ug/L 200 109 60-140107 1 30200222439437
1,2-Dibromo-3-
chloropropane ug/L 200 108 60-140108 0 30200ND216216
1,2-Dibromoethane (EDB)ug/L 200 109 60-140104 4 30200ND218208
1,2-Dichlorobenzene ug/L 200 111 60-140108 3 30200ND221215
1,2-Dichloroethane ug/L 200 100 60-14093 8 30200ND201186
1,2-Dichloropropane ug/L 200 111 60-140109 2 30200ND222219
1,3,5-Trimethylbenzene ug/L 200 112 60-140108 3 3020055.8 280 272
1,3-Dichlorobenzene ug/L 200 109 60-140107 2 30200ND218214
1,3-Dichloropropane ug/L 200 111 60-140106 5 30200ND222211
1,4-Dichlorobenzene ug/L 200 109 60-140109 1 30200ND219217
2,2-Dichloropropane ug/L 200 111 60-140106 4 30200ND221213
2-Chlorotoluene ug/L 200 114 60-140109 5 30200ND229218
4-Chlorotoluene ug/L 200 111 60-140109 2 30200ND223218
Benzene ug/L 200 95 60-140113 2 30200163018201860
Bromobenzene ug/L 200 114 60-140109 5 30200ND228218
Bromochloromethane ug/L 200 106 60-140103 3 30200ND213206
Bromodichloromethane ug/L 200 109 60-140108 1 30200ND218216
Bromoform ug/L 200 111 60-140104 6 30200ND221208
Bromomethane ug/L 200 75 60-14096 24 30200ND150192
Carbon tetrachloride ug/L 200 117 60-140112 4 30200ND234225
Chlorobenzene ug/L 200 111 60-140106 5 30200ND223213
Chloroethane ug/L 200 139 60-140140 1 30200ND277280
Chloroform ug/L 200 112 60-140105 6 30200ND223211
Chloromethane ug/L 200 73 60-14073 1 30200ND146145
cis-1,2-Dichloroethene ug/L 200 104 60-140100 4 30200ND209201
cis-1,3-Dichloropropene ug/L 200 111 60-140108 2 30200ND221216
Dibromochloromethane ug/L 200 112 60-140107 5 30200ND224214
Dibromomethane ug/L 200 113 60-140109 4 30200ND227218
Dichlorodifluoromethane ug/L 200 91 60-14085 7 30200ND182169
Diisopropyl ether ug/L 200 99 60-14096 2 3020037.7 235 230
Ethylbenzene ug/L 200 108 60-140106 1 30200240457452
Hexachloro-1,3-butadiene ug/L 200 103 60-140105 2 30200ND206211
Isopropylbenzene(Cumene)ug/L 200 113 60-140109 3 3020036.3 263 255
m&p-Xylene ug/L 400 111 60-140107 3 30400128572556
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 19 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2766038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457416003
2766039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 108 60-140100 5 30200130346331
Methylene Chloride ug/L 200 101 60-14098 2 30200ND202197
n-Butylbenzene ug/L 200 105 60-140106 1 3020022.4 233 235
n-Propylbenzene ug/L 200 107 60-140105 1 3020075.0 289 286
Naphthalene ug/L 200 111 60-140130 8 30200276497536
o-Xylene ug/L 200 111 60-140106 4 3020010.6 233 223
sec-Butylbenzene ug/L 200 115 60-140112 2 30200ND229224
Styrene ug/L 200 114 60-140111 3 30200ND229223
tert-Butylbenzene ug/L 200 97 60-14094 3 30200ND193188
Tetrachloroethene ug/L 200 112 60-140108 4 30200ND225216
Toluene ug/L 200 108 60-140106 1 3020020.3 236 232
trans-1,2-Dichloroethene ug/L 200 109 60-140104 4 30200ND217208
trans-1,3-Dichloropropene ug/L 200 102 60-140101 1 30200ND204203
Trichloroethene ug/L 200 115 60-140110 4 30200ND230221
Trichlorofluoromethane ug/L 200 108 60-140103 5 30200ND217206
Vinyl chloride ug/L 200 107 60-140104 3 30200ND214208
1,2-Dichloroethane-d4 (S)%96 70-13098
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%97 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 20 of 25
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92457956
Jerry's Place
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 21 of 25
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92457956001 516241MW-2 SM 6200B
92457956002 516241MW-3 SM 6200B
92457956003 516241MW-4 SM 6200B
92457956004 516241MW-5 SM 6200B
92457956005 516241WSW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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APPENDIX C