WS-3254_9547_CA_MRP_20151014

GROUNDWATER MONITORING REPORT
JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NORTH CAROLINA

NCDEQ INCIDENT NUMBER: 9547
NCDEQ CONTRACT NUMBER: N14007i-C

ECS PROJECT 09.26074

PREPARED FOR:

NCDEQ, UST SECTION
RALEIGH, NORTH CAROLINA

OCTOBER 14, 2015

October 14, 2015

Mr. Herbert Berger
NCDEQ, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Reference: Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074

Dear Mr. Berger:

As authorized by your acceptance of ECS Carolinas, LLP’s (ECS) Task Authorization Request
No. 2 dated September, 2015, ECS has prepared a Groundwater Monitoring Report for the
above referenced site. This report includes a description of the work performed, the results
obtained, and our conclusions and recommendations.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us at (336)
856-7150.

Sincerely,

ECS CAROLINAS, LLP

Ken Vilagos
Environmental Staff Scientist

John M. Stewart, P.G.
Principal Geologist
Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

1

SITE INFORMATION

Site Name: Jerry’s Place

Site Address: 983 Highway 21
State Road, North Carolina 28676

Facility ID Number: 0-008572

NCDEQ Incident Number: 9547

Site Risk Ranking: High (Assigned)

Land Use Category: Residential (Assigned)

Latitude/Longitude: 36.3259656 N / 80.867567 W

Responsible Party: Jerry Harris
163 Royall Road
Thurmond, North Carolina 28683

Current Property Owner: Ted Roberts
983 Highway 21
State Road, North Carolina 28676

Primary Contact: Mr. Herbert Berger
NCDEQ, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Primary Consultant: ECS Carolinas, LLP
4811 Koger Boulevard
Greensboro, North Carolina 27407
[phone]

Laboratory: Pace Analytical Services, Inc.
9800 Kincey Ave.
Huntersville, North Carolina 28078
[phone]
Laboratory Certification No. 37706 and 12

Release Information:

The subject site is Jerry’s Place located at 983 Highway 21 in State Road, Surry County, North
Carolina. Based on information provided to ECS, four underground storage tanks (USTs) were
Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

3

TABLE OF CONTENTS
1.0 PROJECT INFORMATION ................................................................................................... 4
2.0 GROUNDWATER ASSESSMENT ........................................................................................ 4
3.0 RESULTS ............................................................................................................................. 5
4.0 CONCLUSIONS .................................................................................................................... 6
5.0 RECOMMENDATIONS ......................................................................................................... 7

FIGURES

Figure 1 Site Location Map
Figure 2 Aerial Site Map
Figure 3 Site Map
Figure 4 Water- Supply Well Location Map
Figure 5 Groundwater Elevation Map
Figure 6 Benzene Isoconcentration Map
Figure 6A Toluene Isoconcentration Map
Figure 6B N-Propylbenzene Isoconcentration Map
Figure 6C Ethylbenzene Isoconcentration Map
Figure 6D Isopropylbenzene Isoconcentration Map
Figure 6E Naphthalene Isoconcentration Map
Figure 6F Total Xylenes Isoconcentration Map
Figure 6G 1,2,4-Trimethylbenzene Isoconcentration Map
Figure 6H 1,3,5-Trimethylbenzene Isoconcentration Map

TABLES

Table 1 Monitoring Well Information and Groundwater Elevation Data
Table 2 Summary of Groundwater Analytical Results sampled (Monitoring Wells)
Table 3 Historical Summary of Groundwater Analytical Results (Monitoring Wells)
Table 4 Summary of Groundwater Analytical Results (Water-Supply Wells)
Table 5 Geochemical Measurements

APPENDIX

Appendix A Laboratory Data Sheets and Chain of Custody Record
Appendix B Field Data Sheets
Appendix C Water-Supply Well Sampling Authorization
Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

4

1.0 PROJECT INFORMATION

The subject site is Jerry’s Place located at 983 Highway 21 in State Road, Surry County, North
Carolina (Figure 1 and Figure 2). Based on information provided to ECS, four 4,000-gallon
gasoline underground storage tanks (USTs) were removed from the site in October 1992.
During closure activities, free product was observed flowing into a test pit that was excavated to
a depth of approximately 19 feet below the ground surface (bgs). Petroleum hydrocarbons
were detected in soil samples collected from the tank basin and dispenser areas. The closure
was concluded by soil excavation and remediation of approximately 1,029 tons of soil. Between
1993 and 1994, eight monitoring wells (MW-1 through MW-8) and two recovery wells (RW-5
and RW-6) were installed at the site. Monitoring well MW-1 is presumed destroyed and
recovery well RW-6 is presumed paved over based on a 2008 report. An aggressive fluid vapor
recovery (AFVR) event was conducted in 1996 and a mobile multi-phase extraction (MMPE)
event was conducted in 2001. Free product was not observed following the MMPE event until
2008 when 0.05 feet of free product was measured in MW-2. Groundwater samples were
collected from various monitoring wells on the site in 1993, 2009, 2010, 2011, and most
recently by ECS in 2014. The contaminant concentrations in the impacted wells have generally
decreased since the 1993 sampling event. Sixteen water-supply wells have been identified
within 1,000 feet of the site. Methyl-tert-butyl-ether (MTBE) has been detected in one water
supply well (WS-5) since 2009; however, the concentrations have been below the North
Carolina 2L Groundwater Quality Standard (NC2LGWQS). Municipal water is not available to
the site or surrounding properties. The nearest surface water body is a stream located
approximately 230 feet east of the source area. The estimated quantity of the release is
unknown.

2.0 GROUNDWATER ASSESSMENT

2.1 Monitoring Well Sampling

On September 22, 2015, ECS personnel collected samples from four monitoring and recovery
wells (MW-2/RW-2, MW-3/RW-3, MW-4/RW-4, and MW-5). The locations of the wells are
shown on Figure 3. Prior to sampling, the wells were purged using a new disposable
polyethylene bailer and new length of nylon cord. The wells were developed/purged by
evacuating a minimum of three well volumes using the bailer and cord. The wells were
developed/purged to remove sand, silt and other fine sediments and to promote communication
between the surrounding formation and the sand pack surrounding the well’s screened interval.
After purging was completed, the sampler wearing a new pair of disposable nitrile gloves for each
sampling point poured the groundwater sample from the bailer into laboratory prepared
containers. Each container was labeled and placed in a cooler containing ice to maintain the
samples at approximately 4 Celsius. The sample containers were then delivered to Pace
Analytical Services, Inc. (Pace) in Huntersville, North Carolina to be analyzed for volatile
organic compounds (VOCs) using Standard Method 6200B. A Chain of Custody Record was
maintained and is included in the Appendix A.

Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

5

2.2 Water Supply Well Sampling

On September 22, 2015 ECS collected a sample from one water-supply well (WSW-5) located in
the vicinity of the site. The location of the well is shown on Figure 4. ECS personnel obtained
written permission from the property owner prior to sampling each well (Appendix C). Prior to
sampling, the well and household plumbing were purged by allowing the water to run for
approximately 20 minutes. After purging was completed, the sampler wearing a new pair of
disposable nitrile gloves, poured the water sample into laboratory prepared containers. Each
container was labeled and placed in a cooler containing ice to maintain the samples at
approximately 4 Celsius. The sample containers were then delivered to Pace to be analyzed
for VOCs using EPA Method 6200B.

2.3 Groundwater Chemistry

Prior to collecting the groundwater samples, geochemical parameters (temperature, pH,
dissolved oxygen, and conductivity) were measured using a YSI Model 560 meter. The turbidity
was observed during the sampling and recorded on the Groundwater Sampling Data Sheets
(Appendix B).

2.4 Groundwater Flow Direction

On September 22, 2015, ECS measured the static water level (SWL) in four monitoring and
recovery wells using a decontaminated electronic water level meter. The static water levels and
top of casing elevations were used to calculate groundwater flow direction. The static water level
measurements can be found on Table 1.

3.0 RESULTS

3.1 Groundwater Flow Direction

Groundwater at the site is flowing to the southwest under a gradient of 0.033ft/ft as determined
between MW-3/RW-3 and MW-4 (Figure 5).

3.2 Monitoring Well Sampling Results

Laboratory analysis of groundwater samples collected from monitoring wells MW-2/RW-2, MW-
3/RW-3, MW-4/RW-4, and MW-5 detected targeted compounds that exceed their respective
North Carolina 2L Groundwater Quality Standard (NC2LGWQS); however, the concentrations did
not exceed their respective Gross Contaminant Levels (GCLs). No free product was observed in
the site monitoring wells. A summary of the current and historical groundwater analytical results
are included in Table 2 and Table 3. The laboratory data sheets are included in the Appendix B.
Using the laboratory analytical results of the groundwater samples collected from the groundwater
monitoring wells, isoconcentration maps showing the horizontal extent for the compounds which
were detected above the NC2LGWQS are included as Figure 6 through Figure 6H.

Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

6

3.3 Water Supply Well Sampling Results

Laboratory analysis of groundwater sample WSW- 5 detected methyl-tert butyl ether (MTBE) at a
concentration of 2.6 parts per billion (ppb); however, the concentration does not exceed its
NC2LGWQS of 20 ppb. A summary of the current and historical groundwater analytical results
are included in Table 4.

3.4 Groundwater Chemistry

Based on the geochemical data, the average groundwater temperature was 17.4° C and the
average conductivity was 0.129mS/cm. The pH ranged from a low of 5.45 to 8.86 and the
dissolved oxygen (DO) ranged from 4.30 mg/l to 8.66mg/l. The geochemical measurements are
shown on Table 5.

4.0 CONCLUSIONS

ECS has completed the groundwater monitoring sampling at the site. ECS sampled four Type II
monitoring wells and one water-supply well. Based on on-site groundwater measurements and
laboratory analytical results, ECS concludes the following:

 The groundwater elevations as determined on September 22, 2015, were used to
prepare a potentiometric map of the groundwater surface of the site. The groundwater
flow direction is generally to the south-southeast across the site;

 Laboratory analysis of groundwater samples collected from monitoring wells MW-2/RW-2,
MW-3/RW-3, MW-4/RW-4, and RW-5 detected targeted compounds that exceed their
respective NC2LGWQS; however, the concentrations did not exceed their respective
GCLs.

 No free product was detected in the monitoring wells;

 The concentrations of petroleum related hydrocarbons have generally decreased in each
well sampled since the 1993 sampling event.

 Laboratory analysis of groundwater sample WSW- 5 detected MTBE at a concentration of
2.6 ppb; however, the concentration does not exceed its NC2LGWQS of 20 ppb.
Groundwater Monitoring Report
Task Authorization Request No. 2 – Jerry’s Place
983 Highway 21
State Road, Surry County, North Carolina
NCDEQ Incident No.: 9547
NCDEQ Contract No. N14007i-C
ECS Project 09.26074
October 14, 2015

7

5.0 RECOMMENDATIONS

Based on the results of this sampling event and those performed by others, ECS has the
following recommendations:

 Sample the on-site water supply well (WSW-5) semi-annually;

 Abandon monitoring wells MW-6, MW-7, and MW-8. Monitoring well MW-6 is the
upgradient well and MW-7 and MW-8 have either been dry or when sampled, clean, since
1994. Monitoring MW-5 is positioned in a more downgradient direction and should used
as the down gradient sentinel well;

 Install O-SOXs in monitoring wells MW-2 and MW-3/RW-3;

 Sample MW-2, MW-3/RW-3, MW-4/RW-4, and MW-5 six months following installation of
the O-SOX.

FIGURES
SOURCE:

USGS TOPOGRAPHIC MAP
ELKIN NORTH, NC QUADRANGLE
DATED 1971, REVISED 1994

FIGURE 1
SITE LOCATION MAP

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
SITE
APPROXIMATE SITE BOUNDARY
SCALE (IN FEET)
2,000 1,000 0 2,000

SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 2
AERIAL SITE MAP

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 3
MONITORING WELL LOCATION MAP

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

EXISTING
BUILDING
SOURCE:

GOOGLE EARTH WEBSITE
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 4
WATER SUPPLY WELL LOCATION MAP

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

500’
1000’’
1500’
WSW-16
WSW-15
WSW-14
WSW-13
WSW-1
WSW-3
WSW-6
WSW-5
WSW-12
WSW-4
WSW-11
WSW-10
WSW-9
WSW-2
WSW-8
WSW-7
SCALE (IN FEET)
500 250 0 500

SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 5
GROUNDWATER ELEVATION MAP

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

(75.71)
(72.96)
(73.59)
(75.55)
NM
NM
NM
NM
NM
75
73
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6
ISOCONCENTRATION MAP OF BENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

1,410
<0.5
14.4
79.1
NS
NS
NS
NS
NS
BQL
50
1,400
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6A
ISOCONCENTRATION MAP OF TOLUENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

1,210
<0.5
<0.5
23.5
NS
NS
NS
NS
NS
<0.5
1,000
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6B
ISOCONCENTRATION MAP OF
N-PROPYLBENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

<0.5
<0.5
1.4
174
NS
NS
NS
NS
NS
<0.5
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6C
ISOCONCENTRATION MAP OF
ETHYLBENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

1,270
<0.5
<0.5
234
NS
NS
NS
NS
NS
<0.5
1,200
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6D
ISOCONCENTRATION MAP OF
ISOPROPYL BENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

100
<0.5
23.1
78.7
NS
NS
NS
NS
NS
<0.5
50
100
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6E
ISOCONCENTRATION MAP OF
NAPTHALENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

403
<0.5
13.5
175
NS
NS
NS
NS
NS
<0.5
150
400
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6F
ISOCONCENTRATION MAP OF
TOTAL XYLENES

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

4,750
<0.5
<0.5
1,010
NS
NS
NS
NS
NS
<0.5
4,500
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6G
ISOCONCENTRATION MAP OF
1,2,4-TRIMETHYLBENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

2,010
<0.5
<0.5
1,160
NS
NS
NS
NS
NS
<0.5
2,000
EXISTING
BUILDING
SOURCE:

SURRY COUNTY GIS
AERIAL PHOTOGRAPH, DATED 2013

FIGURE 6H
ISOCONCENTRATION MAP OF
1,3,5-TRIMETHYLBENZENE

JERRY’S PLACE
983 HIGHWAY 21
STATE ROAD, SURRY COUNTY, NC
INCIDENT #9547
ECS PROJECT NO. 09.26074
APPROXIMATE SITE BOUNDARY
LEGEND
1. News Topic
2. Office Building with The Floyd
Group, Edward Jones Investments,
and a hair salon
3. Cross Roads Shopping Center
4. The House of Lora
5. WW Auto Works
6. BudBuilt.com
7. Bonnie Mist Car Wash
8. Office Building with Neal York Life
Insurance Company and TLC
Jewelers
9. McDonald’s
10. Piedmont Cleaners
Current/Former Drycleaner

Former Phillips 66 Service Station


1

1 2 3 4 5
6 7 8 9 10
11 12 13 14 15
    
 

SCALE (IN FEET)
100 50 0 100

599
<0.5
<0.5
333
NS
NS
NS
NS
NS
<0.5
500
EXISTING
BUILDING

TABLES
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 1: MONITORING WELL INFORMATION AND GROUNDWATER ELEVATION DATA
WELL ID #DATE WATER
LEVEL MEASURED
WELL
CASING
DIAMETER
(in)
SCREEN
INTERVAL
TOP OF CASING
ELEVATION*
(ft.)
DEPTH TO WATER
FROM TOP OF
CASING (ft.)
GROUNDWATER
ELEVATION** (ft.)
5/24/1993 16.2 85.25
1/31/1994 21.51 79.94
3/15/1994 19.77 81.68
5/24/1993 13.3 84.69
1/31/1994 17.92(P) 18.70(W)79.95**
3/15/1994 16.28(P) 16.97(W)81.61**
10/7/2009 19.97 78.02
4/22/2010 15.31 82.68
9/13/2011 22.04 75.95
6/27/2014 17.36 80.63
9/22/2015 22.28 75.71
5/24/1993 12.8 84.06
1/31/1994 17.35 79.51
3/15/1994 15.68 81.18
10/7/2009 19.14 77.72
4/22/2010 14.7 82.16
9/13/2011 21.51 75.35
9/22/2015 21.31 75.55
5/24/1993 15.95 79.99
1/31/1994 19.88 76.06
3/15/1994 18.71 77.23
10/7/2009 20.99 74.95
4/22/2010 17.41 78.53
9/13/2011 22.64 73.3
6/27/2014 18.55 77.39
9/22/2015 22.35 73.59
5/24/1993 1.98 78.59
1/31/1994 4.99 75.58
3/15/1994 4.14 76.43
10/7/2009 5.88 74.69
4/22/2010 3.38 77.19
9/13/2011 7.51 73.06
6/27/2014 4.3 76.27
9/22/2015 7.61 72.96
1/31/1994 19.25 80.38
3/15/1994 17.36 82.27
10/7/2009 21.22 78.41
4/22/2010 16.19 83.44
9/13/2011 23.36 76.27
6/27/2014 18.4 81.23
1/31/1994 24.1 73.1
3/15/1994 22.81 74.39
10/7/2009 24.43 72.77
4/22/2010 21.83 75.37
9/13/2011 DRY <72.05
9/28/2011 DRY <72.05
6/27/2014 23.4 73.8
1/31/1994 23.96 74.55
3/15/1994 22.42 76.09
10/7/2009 24.38 74.13
4/22/2010 21.1 77.41
9/13/2011 DRY <73.46
9/28/2011 DRY <73.46
6/27/2014 22.98 75.53
NOTES:
* Reference point for Elevation Measurements: Previous benchmark Assumed Elevation: 100.00 ft.
** If free product is present, groundwater elevation is calculated by : [Top of Casing Elevation - DW] + [FP thickness x 0.8581]
ft BGS: feet below ground surface
ft. AGS: ft above ground surface
ND: Free product not detected
(P)- Free Product
(W)- Water
12 - 32
15.5 - 25.5
101.45
97.2
99.63
80.57
95.94
96.86
97.99
MW-8
MW-6
9 - 154
98.51
15.5 - 25.5
15.5 - 25.5
15.5 - 25.5
2 - 12
10 - 30
2
2
4
4
4
2
2
MW-7
MW-2/RW-2
MW-3/RW-3
MW-4/RW-4
MW-5
MW-1
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 2: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS FOR 9/22/15
Sample Identification MW-2/RW-2 MW-3/RW-3 MW-4/RW-4 MW-5 WSW-5
Sample Date 9/22/2015 9/22/2015 9/22/2015 9/22/2015 9/22/2015
Acetone <25 <25 <25 <25 <25 6,000 6,000,000
Benzene 1,410 79.1 14.4 <0.5 <0.5 1 5,000
n-Butylbenzene <0.5 <0.5 <0.5 <0.5 <0.5 70 6,900
tert-Butylbenzene <0.5 <0.5 <0.5 <5 <0.5 70 15,000
Toluene 1,120 23.5 <0.5 <5 <0.5 600 260,000
Isopropyl ether 20.6 <0.5 1.1 <0.5 <0.5 70 70,000
n-Propylbenzene <0.5 174 1.4 <0.5 <0.5 70 30,000
Ethylbenzene 1,270 234 <0.5 <1 <0.5 600 84,500
Isopropyl benzene 100 78.7 23.1 <0.5 <0.5 70 25,000
Methyl Tert Butyl Ether 74 <0.5 8.9 0.75 2.6 20 20,000
Naphthalene 403 175 13.5 <0.5 <0.5 6 6,000
Methyl ethyl ketone <0.5 <0.5 <0.5 <0.5 <0.5 4,000 4,000,000
2-Hexanone <0.5 <0.5 <0.5 <5 <0.5 280 280,000
p-Isopropyltoluene <0.5 <0.5 <0.5 <0.5 <0.5 25 11,700
sec-Butylbenzene <0.5 17.8 3.8 <0.5 <0.5 70 8,500
Xylenes (total)4,750 1,010 <1 <0.5 <1 500 85,500
1,2,4-Trimethylbenzene 2,010 1,160 <0.5 <0.5 <0.5 400 28,500
1,3,5-Trimethylbenzene 599 333 <0.5 <0.5 <0.5 400 25,500
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard
GCL = Gross Contamination Level
Value exceeds NC2LGWQS = BOLD
Value exceeds GCL = BOLD
GCLNC2LGWQS
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 3: HISTORICAL SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Sample Identification MW-1
Sample Date 5/24/1993 5/23/1993 10/7/2009 4/22/2010 9/13/2011 6/27/2014 9/22/2015 5/24/1993 10/7/2009 4/22/2010 9/13/2011 6/27/2014 9/22/2015
Acetone NA NA 2,400 1,700 230J <25 <25 NA 600 130 <60 <25 <25 6,000 6,000,000
Benzene 5 14,000 2,400 1,700 2,300 1,830 1,410 9,200 600 130 180 93.8 79.1 1 5,000
n-Butylbenzene NA NA 26 63 23 21 <0.5 NA 50 76 44 23.3 <0.5 70 6,900
tert-Butylbenzene NA NA <5 <20 <1.4 <0.5 <0.5 NA <5 <20 <4.3 <5 <0.5 70 15,000
Toluene <1 54,000 800 1,400 4,000 6,390 1,120 26,000 1,500 750 210 80.2 23.5 600 260,000
Isopropyl ether NA NA 70 78 56 16 20.6 NA 16 <20 <1.7 <20 <0.5 70 70,000
n-Propylbenzene NA NA ND ND 180 224 <0.5 NA ND ND 250 185 174 70 30,000
Ethylbenzene <1 2000 960 1,200 1,300 1,530 1,270 1,100 910 840 730 381 234 600 84,500
Isopropyl benzene NA NA 95 100 91 80 100 NA 120 130 100 84.9 78.7 70 25,000
Methyl Tert Butyl Ether 41 25,000 380 260 220 <0.5 74 17,000 79 56 <2.2 <0.5 <0.5 20 20,000
Naphthalene NA NA 590 600 560 761 403 NA 570 660 490 448 175 6 6,000
Methyl ethyl ketone NA NA 130 170 <33 <25 <0.5 NA 270 300 <33 <25 <0.5 4,000 4,000,000
2-Hexanone NA NA NA <5 100 <5 <0.5 NA NA <4.5 32J <5 <0.5 280 280,000
p-Isopropyltoluene NA NA 13 40 <2.4 28.8 <0.5 NA 21 45 <2.4 22.1 <0.5 25 11,700
sec-Butylbenzene NA NA 17 44 20 <0.5 <0.5 NA 29 52 34 15.9 17.8 70 8,500
Xylenes (total)<1 17,000 1,230 3,800 5,500 7,320 4,750 7,900 5,600 6,700 3,900 2,060 1,010 500 85,500
1,2,4-Trimethylbenzene NA NA 350 1,300 1,500 2,300 2,010 NA 2,300 2,900 2,000 1,350 1,160 400 28,500
1,3,5-Trimethylbenzene NA NA 100 420 460 600 599 NA 620 840 570 393 333 400 25,500
Sample Identification
Sample Date 5/24/1993 10/7/2009 4/22/2010 9/13/2011 6/27/2014 9/22/2015 5/24/1993 10/7/2009 4/22/2010 9/13/2011 6/27/2014 9/22/2015
Acetone NA NA NA <15 <25 <25 NA 11 <0.5 <1.5 <25 <25 6,000 6,000,000
Benzene 540 430 250 190 7.55 14.4 4 11 <0.5 <0.054 <0.5 <0.5 1 5,000
n-Butylbenzene NA 19 8.5 12 0.63 <0.5 NA 1.4 <1 <0.059 <0.5 <0.5 70 6,900
tert-Butylbenzene NA 0.91 0.83 <1.1 <5 <0.5 NA <0.5 <0.5 <.11 <5 <5 70 15,000
Toluene 92 3.8 2.4 <0.57 <5 <0.5 19 <0.5 <0.5 <0.057 <5 <5 600 260,000
Isopropyl ether NA 9.2 6.8 <0.42 0.85 1.1 NA <0.5 <0.5 <0.41 <0.5 <0.5 70 70,000
n-Propylbenzene NA ND ND 20 2.42 1.4 NA ND ND <0.059 <0.5 <0.5 70 30,000
Ethylbenzene <1 5.3 1.5 <5 <1 <0.5 2 2.3 <0.5 <0.054 <1 <1 600 84,500
Isopropyl benzene NA 110 50 93 15.5 23.1 NA 2.9 <0.5 <0.034 <0.5 <0.5 70 25,000
Methyl Tert Butyl Ether 380 62 59 42 7.14 8.9 48 3.8 0.92 <0.056 <0.5 0.75 20 20,000
Naphthalene NA 520 140 210 5.43 13.5 NA 6.8 <1 <0.094 <0.5 <0.5 6 6,000
Methyl ethyl ketone NA 34 14 <8.3 <25 <0.5 NA 0.66 <0.5 <.83 <0.5 <0.5 4,000 4,000,000
2-Hexanone NA NA <0.11 <1.1 <5 <0.5 NA NA <1.1 <.11 <5 <5 280 280,000
p-Isopropyltoluene NA 4.1 2.3 <5.9 <2.5 <0.5 NA 0.98 <0.5 <0.059 <0.5 <0.5 25 11,700
sec-Butylbenzene NA 12 6.5 11 2.3 3.8 NA 1.1 <0.5 <0.054 <0.5 <0.5 70 8,500
Xylenes (total)450 15.4 11 10.7J <5 <1 23 6.6 <1 <0.11 <0.5 <0.5 500 85,500
1,2,4-Trimethylbenzene NA 12 7.6 <.38 0.8 <0.5 NA 5.5 <0.5 <0.038 <0.5 <0.5 400 28,500
1,3,5-Trimethylbenzene NA 3.6 1.6 <.38 <0.5 <0.5 NA 0.98 <0.5 <0.038 <0.5 <0.5 400 25,500
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard NA = Not Analyzed for This Compound
GCL = Gross Contaminant Level J-Value = Estimated value between laboratory reporting limit and method detection limit
NA-FP= Not sampled; Free Product Value exceeds NC2LGWQS = BOLD
NA = Not Sampled Value exceeds GCL = BOLD
GCLMW-2/RW-2 MW-3/RW-3
MW-4/RW-4
NC2LGWQS
MW-5 NC2LGWQS GCL
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 3: HISTORICAL SUMMARY OF GROUNDWATER ANALYTICAL RESULTS (Continued)
Sample Identification
Sample Date 1/31/1994 10/7/2009 4/22/2010 9/13/2011 6/27/2014 1/31/1994 10/7/2009 4/22/2010 9/13/2011 6/27/2014
Acetone NA <0.5 <0.5 <1.5 <25 NA DRY <0.5 DRY <25 6,000 6,000,000
Benzene <1 <0.5 <0.5 <.054 <0.5 <1 DRY <0.5 DRY <0.5 1 5,000
n-Butylbenzene NA <1 <1 <.059 <0.5 NA DRY <1 DRY <0.5 70 6,900
tert-Butylbenzene NA <0.5 <0.5 <.11 <5 NA DRY <0.5 DRY <5 70 15,000
Toluene <1 <0.5 <0.5 <0.057 <5 <1 DRY <0.5 DRY <5 600 260,000
Isopropyl ether NA <0.5 <0.5 <.41 <0.5 NA DRY <0.5 DRY <0.5 70 70,000
n-Propylbenzene NA ND ND <0.059 <0.5 NA DRY ND DRY <0.5 70 30,000
Ethylbenzene <1 <0.5 <0.5 <0.054 <1 <1 DRY <0.5 DRY <1 600 84,500
Isopropyl benzene NA <0.5 <0.5 <0.034 <0.5 NA DRY <0.5 DRY <0.5 70 25,000
Methyl Tert Butyl Ether <1 <0.5 <0.5 <0.056 <0.5 <1 DRY <0.5 DRY <0.5 20 20,000
Naphthalene NA <2 <1 <.0094 <0.5 NA DRY <1 DRY <0.5 6 6,000
Methyl ethyl ketone NA <0.5 <0.5 <0.83 <0.5 NA DRY <0.5 DRY <0.5 4,000 4,000,000
2-Hexanone NA NA <.11 <0.11 <5 NA DRY <0.11 DRY <5 280 280,000
p-Isopropyltoluene NA <0.5 <0.5 <0.059 <0.5 NA DRY <0.5 DRY <0.5 25 11,700
sec-Butylbenzene NA <0.5 <0.5 <0.054 <0.5 NA DRY <0.5 DRY <0.5 70 8,500
Xylenes (total)<1 <1 <1 <0.11 <0.5 <1 DRY <1 DRY <0.5 500 85,500
1,2,4-Trimethylbenzene NA <0.5 <0.5 <0.038 <0.5 NA DRY <0.5 DRY <0.5 400 28,500
1,3,5-Trimethylbenzene NA <0.5 <0.5 <0.038 <0.5 NA DRY <0.5 DRY <0.5 400 25,500
Sample Identification
Sample Date 3/16/1994 10/7/2009 4/22/2010 9/13/2011 6/27/2014 10/7/2009 4/22/2010 9/13/2011 6/27/2014
Acetone NA DRY <0.5 DRY <25 300 470 <.59 <25 6,000 6,000,000
Benzene 2 DRY <0.5 DRY <0.5 300 470 110 <0.5 1 5,000
n-Butylbenzene NA DRY <1 DRY <0.5 14 14 6.4 <0.5 70 6,900
tert-Butylbenzene NA DRY <0.5 DRY <5 <0.5 <5 <1.1 <5 70 15,000
Toluene 6 DRY <0.5 DRY <5 580 330 300 477 600 260,000
Isopropyl ether NA DRY <0.5 DRY <0.5 6.2 20 <.42 <0.5 70 70,000
n-Propylbenzene NA DRY ND DRY <0.5 ND ND 160 103 70 30,000
Ethylbenzene 2 DRY <0.5 DRY <1 1100 550 12000 468 600 84,500
Isopropyl benzene NA DRY <0.5 DRY <0.5 85 51 83 35.5 70 25,000
Methyl Tert Butyl Ether 1 DRY <0.5 DRY <0.5 34 68 15 <0.5 20 20,000
Naphthalene NA DRY <1 DRY <0.5 560 150 380 238 6 6,000
Methyl ethyl ketone NA DRY <0.5 DRY <0.5 170 57 <8.3 <0.5 4,000 4,000,000
2-Hexanone NA DRY <.11 DRY <5 <5 <5 7.8J <5 280 280,000
p-Isopropyltoluene NA DRY <0.5 DRY <0.5 6.3 9.8 <.59 <0.5 25 11,700
sec-Butylbenzene NA DRY <0.5 DRY <0.5 9.9 11 9.6 <0.5 70 8,500
Xylenes (total)6 DRY <1 DRY <0.5 3,300 950 2,700 1,290 500 85,500
1,2,4-Trimethylbenzene NA DRY <0.5 DRY <0.5 1,100 280 1,100 794 400 28,500
1,3,5-Trimethylbenzene NA DRY <0.5 DRY <0.5 300 84 260 164 400 25,500
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard NA = Not Analyzed for This Compound
GCL = Gross Contaminant Level J-Value = Estimated value between laboratory reporting limit and method detection limit
NA-FP= Not sampled; Free Product Value exceeds NC2LGWQS = BOLD
NA = Not Sampled Value exceeds GCL = BOLD
MW-6
MW-8 NC2LGWQSRW-5
NC2LGWQS GCL
GCL
MW-7
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 4: SUMMARY OF WATER SUPPLY WELL ANALYTICAL RESULTS
Sample Identification
Sample Date 10/7/2009 4/22/2010 10/25/2010 5/9/2011 9/13/2011 6/27/2014 10/7/2009 4/22/2010 10/25/2010 5/9/2011 9/13/2011 6/27/2014
Acetone NS <10 NS NS NS NS NS <10 <10 <10 <1.5 <25 6,000 6,000,000
Benzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.054 <0.5 1 5,000
n-Butylbenzene NS <1 NS NS NS NS NS <1 <1 <1 <.059 <0.5 70 6,900
tert-Butylbenzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.11 <5 70 15,000
Toluene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <0.057 <5 600 260,000
Isopropyl ether NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.41 <0.5 70 70,000
n-Propylbenzene NS NA NS NS NS NS NS NA NA NA <.059 <0.5 70 30,000
Ethylbenzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.054 <1 600 84,500
Isopropyl benzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.034 <0.5 70 25,000
Methyl Tert Butyl Ether NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.056 <0.5 20 20,000
Naphthalene NS <1 NS NS NS NS NS <1 <1 <1 <.094 <0.5 6 6,000
Methyl ethyl ketone NS <5 NS NS NS NS NS <5 <5 <5 <.83 <0.5 4,000 4,000,000
2-Hexanone NS <5 NS NS NS NS NS <5 <5 <5 <.11 <5 280 280,000
p-Isopropyltoluene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.059 <0.5 25 11,700
sec-Butylbenzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.054 <0.5 70 8,500
Xylenes (total)NS <1 NS NS NS NS NS <1 <1 <1 <.11 <0.5 500 85,500
1,2,4-Trimethylbenzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.038 <0.5 400 28,500
1,3,5-Trimethylbenzene NS <0.5 NS NS NS NS NS <0.5 <0.5 <0.5 <.038 <0.5 400 25,500
Sample Identification
Sample Date 10/7/2009 4/22/2010 10/25/2010 5/9/2011 9/13/2011 6/27/2014 10/7/2009 4/22/2010 10/25/2010 5/9/2011 6/27/2014 9/22/2015
Acetone NS <10 <10 <10 <1.5 <25 <10 <10 210 <10 <10 <25 6,000 6,000,000
Benzene NS <0.5 <0.5 <0.5 <.054 <0.5 2.5 <0.5 <0.5 0.58 <0.5 <0.5 1 5,000
n-Butylbenzene NS <1 <1 <1 <.059 <0.5 1.4 <1 <1 <1 <1 <0.5 70 6,900
tert-Butylbenzene NS <0.5 <0.5 <0.5 <.11 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 70 15,000
Toluene NS <0.5 <0.5 <0.5 <0.057 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 600 260,000
Isopropyl ether NS <0.5 <0.5 <0.5 <.41 <0.5 0.6 <0.5 0.84 0.53 <0.5 <0.5 70 70,000
n-Propylbenzene NS NA NA NA <.059 <0.5 NA NA NA NA NA <0.5 70 30,000
Ethylbenzene NS <0.5 <0.5 <0.5 <.054 <1 1.2 <0.5 <0.5 <0.5 <0.5 <0.5 600 84,500
Isopropyl benzene NS <0.5 <0.5 <0.5 <.034 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 70 25,000
Methyl Tert Butyl Ether NS <0.5 <0.5 <0.5 <.056 <0.5 5 2.9 11 7.4 1.73 2.6 20 20,000
Naphthalene NS <1 <1 <1 <.094 <0.5 5 <1 <1 <1 <1 <0.5 6 6,000
Methyl ethyl ketone NS <5 <5 <5 <.83 <0.5 <5 <5 220 <5 <5 <0.5 4,000 4,000,000
2-Hexanone NS <5 NA NA <.11 <5 NA <.11 <.11 <.11 <5 <0.5 280 280,000
p-Isopropyltoluene NS <0.5 <0.5 <0.5 <.059 <0.5 1 <0.5 <0.5 <0.5 <0.5 <0.5 25 11,700
sec-Butylbenzene NS <0.5 <0.5 <0.5 <.054 <0.5 1 <0.5 <0.5 <0.5 <0.5 <0.5 70 8,500
Xylenes (total)NS <1 <1 <1 <.11 <0.5 15.5 <1 <1 <1 <1 <1 500 85,500
1,2,4-Trimethylbenzene NS <0.5 <0.5 <0.5 <.038 <0.5 14 <0.5 <0.5 <0.5 <0.5 <0.5 400 28,500
1,3,5-Trimethylbenzene NS <0.5 <0.5 <0.5 <.038 <0.5 2.4 <0.5 <0.5 <0.5 <0.5 <0.5 400 25,500
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard NA = Not Analyzed for This CompouNA
GCL = Gross Contaminant Level µg/l = micrograms per liter = ppb (parts per billion)
NS-FP= Not sampled; Free Product J-Value = Estimated value between laboratory reporting limit aNA method detection limit
BQL-Below Quanitation limit Value exceeds NC2LGWQS = BOLD
NS = Not Sampled Value exceeds GCL = BOLD
WSW-2
WSW-4 WSW-5
GCLNC2LGWQSWSW-3
GCLNC2LGWQS
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
TABLE 4: SUMMARY OF WATER SUPPLY WELL ANALYTICAL RESULTS (Continued)
Sample Identification
Sample Date 10/7/2009 4/22/2010 10/25/2010 5/9/2011 9/13/2011 6/27/2014 10/7/2009 4/22/2010 10/25/2010 5/9/2011 9/13/2011 6/27/2014
Acetone NS <10 <10 <10 <1.5 <25 NS <10 NS NS NS NS 6,000 6,000,000
Benzene NS <0.5 <0.5 <0.5 <.054 <0.5 NS <0.5 NS NS NS NS 1 5,000
n-Butylbenzene NS <1 <1 <1 <.059 <0.5 NS <1 NS NS NS NS 70 6,900
tert-Butylbenzene NS <0.5 <0.5 <0.5 <.11 <5 NS <0.5 NS NS NS NS 70 15,000
Toluene NS <0.5 <0.5 <0.5 <0.057 <5 NS <0.5 NS NS NS NS 600 260,000
Isopropyl ether NS <0.5 <0.5 <0.5 <.41 <0.5 NS <0.5 NS NS NS NS 70 70,000
n-Propylbenzene NS NA NA NA <.059 <0.5 NS NS NS NS NS NS 70 30,000
Ethylbenzene NS <0.5 <0.5 <0.5 <.054 <1 NS <0.5 NS NS NS NS 600 84,500
Isopropyl benzene NS <0.5 <0.5 <0.5 <.034 <0.5 NS <0.5 NS NS NS NS 70 25,000
Methyl Tert Butyl Ether NS <0.5 <0.5 <0.5 <.056 <0.5 NS <0.5 NS NS NS NS 20 20,000
Naphthalene NS <1 <1 <1 <.094 <0.5 NS <1 NS NS NS NS 6 6,000
Methyl ethyl ketone NS <5 <5 <5 <.83 <0.5 NS <5 NS NS NS NS 4,000 4,000,000
2-Hexanone NS <5 NA NA <.11 <5 NS <5 NS NS NS NS 280 280,000
p-Isopropyltoluene NS <0.5 <0.5 <0.5 <.059 <0.5 NS <0.5 NS NS NS NS 25 11,700
sec-Butylbenzene NS <0.5 <0.5 <0.5 <.054 <0.5 NS <0.5 NS NS NS NS 70 8,500
Xylenes (total)NS <1 <1 <1 <.11 <0.5 NS <1 NS NS NS NS 500 85,500
1,2,4-Trimethylbenzene NS <0.5 <0.5 <0.5 <.038 <0.5 NS <0.5 NS NS NS NS 400 28,500
1,3,5-Trimethylbenzene NS <0.5 <0.5 <0.5 <.038 <0.5 NS <0.5 NS NS NS NS 400 25,500
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard NA = Not Analyzed for This CompouNA
GCL = Gross Contaminant Level µg/l = micrograms per liter = ppb (parts per billion)
NS-FP= Not sampled; Free Product J-Value = Estimated value between laboratory reporting limit aNA method detection limit
BQL-Below Quanitation limit Value exceeds NC2LGWQS = BOLD
NS = Not Sampled Value exceeds GCL = BOLD
WSW-6 NC2LGWQS GCLWSW-13
Jerry's Place
State Road, Surry County, North Carolina
NCDEQ Incident # 9547
ECS Project 09.26074
SAMPLE ID MW-2 MW-3 MW-4 MW-5
pH 5.49 5.45 6.00 8.86
Temperature (oC)17.25 16.15 16.06 20.21
Conductivity (mS/cm)0.195 0.169 0.068 0.087
Dissolved O2 (mg/l)8.66 4.30 5.04 4.75
Turbidity (Observed)NT NT VT NT
NOTES:
TOC = top of casing NT= Not Turbid
mS/cm = milliseimens per centimeterVT= Very Turbid
mV = millivolts ST= Slightly Turbid
°C = degress Celsius
NA= Not Analyzed (meter failure)
TABLE 5: GEOCHEMICAL MEASUREMENTS
Date Sampled 9/22/2015

APPENDIX A
#=CL#
September 29, 2015
LIMS USE: FR - JOHN STEWART
LIMS OBJECT ID: 92268940
92268940
Project:
Pace Project No.:
RE:
Mr. John Stewart
ECS Carolinas, LLP
4811 Koger Blvd
Greensboro, NC 27407
Jerry's Place 26074
Dear Mr. Stewart:
Enclosed are the analytical results for sample(s) received by the laboratory on September 23, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc:Ashley Barham, ECS Carolinas, LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92268940001 MW-2 SM 6200B 63 PASI-CCAH
92268940002 MW-3 SM 6200B 63 PASI-CCAH
92268940003 MW-4 SM 6200B 63 PASI-CCAH
92268940004 MW-5 SM 6200B 63 PASI-CCAH
92268940005 WSW-5 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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[phone]
Page 3 of 28
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92268940001 MW-2
Benzene 1410 ug/L 09/25/15 18:1810.0SM 6200B
Diisopropyl ether 20.6 ug/L 09/25/15 18:1810.0SM 6200B
Ethylbenzene 1270 ug/L 09/25/15 18:1810.0SM 6200B
Isopropylbenzene (Cumene)100 ug/L 09/25/15 18:1810.0SM 6200B
Methyl-tert-butyl ether 74.0 ug/L 09/25/15 18:1810.0SM 6200B
Naphthalene 403 ug/L 09/25/15 18:1840.0SM 6200B
n-Propylbenzene 236 ug/L 09/25/15 18:1810.0SM 6200B
Toluene 1120 ug/L 09/25/15 18:1810.0SM 6200B
1,2,4-Trimethylbenzene 2010 ug/L 09/25/15 18:1810.0SM 6200B
1,3,5-Trimethylbenzene 599 ug/L 09/25/15 18:1810.0SM 6200B
m&p-Xylene 2850 ug/L 09/25/15 18:1820.0SM 6200B
o-Xylene 1900 ug/L 09/25/15 18:1810.0SM 6200B
92268940002 MW-3
Benzene 79.1 ug/L 09/26/15 01:120.50SM 6200B
sec-Butylbenzene 17.8 ug/L 09/26/15 01:120.50SM 6200B
Ethylbenzene 234 ug/L 09/29/15 03:185.0SM 6200B
Isopropylbenzene (Cumene)78.7 ug/L 09/26/15 01:120.50SM 6200B
Naphthalene 175 ug/L 09/26/15 01:122.0SM 6200B
n-Propylbenzene 174 ug/L 09/26/15 01:120.50SM 6200B
Toluene 23.5 ug/L 09/26/15 01:120.50SM 6200B
1,2,4-Trimethylbenzene 1160 ug/L 09/29/15 03:185.0SM 6200B
1,3,5-Trimethylbenzene 333 ug/L 09/29/15 03:185.0SM 6200B
m&p-Xylene 444 ug/L 09/29/15 03:1810.0SM 6200B
o-Xylene 570 ug/L 09/29/15 03:185.0SM 6200B
92268940003 MW-4
Benzene 14.4 ug/L 09/25/15 20:140.50SM 6200B
sec-Butylbenzene 3.8 ug/L 09/25/15 20:140.50SM 6200B
Diisopropyl ether 1.1 ug/L 09/25/15 20:140.50SM 6200B
Isopropylbenzene (Cumene)23.1 ug/L 09/25/15 20:140.50SM 6200B
Methyl-tert-butyl ether 8.9 ug/L 09/25/15 20:140.50SM 6200B
Naphthalene 13.5 ug/L 09/25/15 20:142.0SM 6200B
n-Propylbenzene 1.4 ug/L 09/25/15 20:140.50SM 6200B
92268940004 MW-5
Methyl-tert-butyl ether 0.75 ug/L 09/25/15 20:300.50SM 6200B
92268940005 WSW-5
Methyl-tert-butyl ether 2.6 ug/L 09/25/15 20:470.50SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-2 Lab ID:92268940001 Collected:09/22/15 11:27 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 1410 ug/L 09/25/15 18:18 71-43-210.0 20
Bromobenzene ND ug/L 09/25/15 18:18 108-86-110.0 20
Bromochloromethane ND ug/L 09/25/15 18:18 74-97-510.0 20
Bromodichloromethane ND ug/L 09/25/15 18:18 75-27-410.0 20
Bromoform ND ug/L 09/25/15 18:18 75-25-210.0 20
Bromomethane ND ug/L 09/25/15 18:18 74-83-910020
n-Butylbenzene ND ug/L 09/25/15 18:18 104-51-810.0 20
sec-Butylbenzene ND ug/L 09/25/15 18:18 135-98-810.0 20
tert-Butylbenzene ND ug/L 09/25/15 18:18 98-06-610.0 20
Carbon tetrachloride ND ug/L 09/25/15 18:18 56-23-510.0 20
Chlorobenzene ND ug/L 09/25/15 18:18 108-90-710.0 20
Chloroethane ND ug/L 09/25/15 18:18 75-00-320.0 20
Chloroform ND ug/L 09/25/15 18:18 67-66-310.0 20
Chloromethane ND ug/L 09/25/15 18:18 74-87-320.0 20
2-Chlorotoluene ND ug/L 09/25/15 18:18 95-49-810.0 20
4-Chlorotoluene ND ug/L 09/25/15 18:18 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 09/25/15 18:18 96-12-820.0 20
Dibromochloromethane ND ug/L 09/25/15 18:18 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 09/25/15 18:18 106-93-410.0 20
Dibromomethane ND ug/L 09/25/15 18:18 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 09/25/15 18:18 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 09/25/15 18:18 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 09/25/15 18:18 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 09/25/15 18:18 75-71-810.0 20
1,1-Dichloroethane ND ug/L 09/25/15 18:18 75-34-310.0 20
1,2-Dichloroethane ND ug/L 09/25/15 18:18 107-06-210.0 20
1,1-Dichloroethene ND ug/L 09/25/15 18:18 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 09/25/15 18:18 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 09/25/15 18:18 156-60-510.0 20
1,2-Dichloropropane ND ug/L 09/25/15 18:18 78-87-510.0 20
1,3-Dichloropropane ND ug/L 09/25/15 18:18 142-28-910.0 20
2,2-Dichloropropane ND ug/L 09/25/15 18:18 594-20-710.0 20
1,1-Dichloropropene ND ug/L 09/25/15 18:18 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 09/25/15 18:18 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 09/25/15 18:18 10061-02-610.0 20
Diisopropyl ether 20.6 ug/L 09/25/15 18:18 108-20-310.0 20
Ethylbenzene 1270 ug/L 09/25/15 18:18 100-41-410.0 20
Hexachloro-1,3-butadiene ND ug/L 09/25/15 18:18 87-68-340.0 20
Isopropylbenzene (Cumene)100 ug/L 09/25/15 18:18 98-82-810.0 20
Methylene Chloride ND ug/L 09/25/15 18:18 75-09-240.0 20
Methyl-tert-butyl ether 74.0 ug/L 09/25/15 18:18 1634-04-410.0 20
Naphthalene 403 ug/L 09/25/15 18:18 91-20-340.0 20
n-Propylbenzene 236 ug/L 09/25/15 18:18 103-65-110.0 20
Styrene ND ug/L 09/25/15 18:18 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 09/25/15 18:18 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 09/25/15 18:18 79-34-510.0 20
Tetrachloroethene ND ug/L 09/25/15 18:18 127-18-410.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-2 Lab ID:92268940001 Collected:09/22/15 11:27 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 1120 ug/L 09/25/15 18:18 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 09/25/15 18:18 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 09/25/15 18:18 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 09/25/15 18:18 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 09/25/15 18:18 79-00-510.0 20
Trichloroethene ND ug/L 09/25/15 18:18 79-01-610.0 20
Trichlorofluoromethane ND ug/L 09/25/15 18:18 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 09/25/15 18:18 96-18-410.0 20
1,2,4-Trimethylbenzene 2010 ug/L 09/25/15 18:18 95-63-610.0 20
1,3,5-Trimethylbenzene 599 ug/L 09/25/15 18:18 108-67-810.0 20
Vinyl chloride ND ug/L 09/25/15 18:18 75-01-420.0 20
m&p-Xylene 2850 ug/L 09/25/15 18:18 179601-23-120.0 20
o-Xylene 1900 ug/L 09/25/15 18:18 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/25/15 18:18 17060-07-070-130 20
4-Bromofluorobenzene (S)100 %09/25/15 18:18 460-00-470-130 20
Toluene-d8 (S)100 %09/25/15 18:18 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-3 Lab ID:92268940002 Collected:09/22/15 11:00 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 79.1 ug/L 09/26/15 01:12 71-43-20.50 1
Bromobenzene ND ug/L 09/26/15 01:12 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/15 01:12 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/15 01:12 75-27-40.50 1
Bromoform ND ug/L 09/26/15 01:12 75-25-20.50 1
Bromomethane ND ug/L 09/26/15 01:12 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/15 01:12 104-51-80.50 1
sec-Butylbenzene 17.8 ug/L 09/26/15 01:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/26/15 01:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/15 01:12 56-23-50.50 1
Chlorobenzene ND ug/L 09/26/15 01:12 108-90-70.50 1
Chloroethane ND ug/L 09/26/15 01:12 75-00-31.0 1
Chloroform ND ug/L 09/26/15 01:12 67-66-30.50 1
Chloromethane ND ug/L 09/26/15 01:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/26/15 01:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/15 01:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/15 01:12 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/15 01:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/15 01:12 106-93-40.50 1
Dibromomethane ND ug/L 09/26/15 01:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/15 01:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/15 01:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/15 01:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/15 01:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/15 01:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/15 01:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/15 01:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/15 01:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/15 01:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/15 01:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/15 01:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/15 01:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/15 01:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/15 01:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/15 01:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/26/15 01:12 108-20-30.50 1
Ethylbenzene 234 ug/L 09/29/15 03:18 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 09/26/15 01:12 87-68-32.0 1
Isopropylbenzene (Cumene)78.7 ug/L 09/26/15 01:12 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/15 01:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/26/15 01:12 1634-04-40.50 1
Naphthalene 175 ug/L 09/26/15 01:12 91-20-32.0 1
n-Propylbenzene 174 ug/L 09/26/15 01:12 103-65-10.50 1
Styrene ND ug/L 09/26/15 01:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/15 01:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/15 01:12 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/15 01:12 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-3 Lab ID:92268940002 Collected:09/22/15 11:00 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 23.5 ug/L 09/26/15 01:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/15 01:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/15 01:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/15 01:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/15 01:12 79-00-50.50 1
Trichloroethene ND ug/L 09/26/15 01:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/15 01:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/15 01:12 96-18-40.50 1
1,2,4-Trimethylbenzene 1160 ug/L 09/29/15 03:18 95-63-65.0 10
1,3,5-Trimethylbenzene 333 ug/L 09/29/15 03:18 108-67-85.0 10
Vinyl chloride ND ug/L 09/26/15 01:12 75-01-41.0 1
m&p-Xylene 444 ug/L 09/29/15 03:18 179601-23-110.0 10
o-Xylene 570 ug/L 09/29/15 03:18 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)101 %09/26/15 01:12 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %09/26/15 01:12 460-00-470-130 1
Toluene-d8 (S)99 %09/26/15 01:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-4 Lab ID:92268940003 Collected:09/22/15 11:01 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 14.4 ug/L 09/25/15 20:14 71-43-20.50 1
Bromobenzene ND ug/L 09/25/15 20:14 108-86-10.50 1
Bromochloromethane ND ug/L 09/25/15 20:14 74-97-50.50 1
Bromodichloromethane ND ug/L 09/25/15 20:14 75-27-40.50 1
Bromoform ND ug/L 09/25/15 20:14 75-25-20.50 1
Bromomethane ND ug/L 09/25/15 20:14 74-83-95.0 1
n-Butylbenzene ND ug/L 09/25/15 20:14 104-51-80.50 1
sec-Butylbenzene 3.8 ug/L 09/25/15 20:14 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/25/15 20:14 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/25/15 20:14 56-23-50.50 1
Chlorobenzene ND ug/L 09/25/15 20:14 108-90-70.50 1
Chloroethane ND ug/L 09/25/15 20:14 75-00-31.0 1
Chloroform ND ug/L 09/25/15 20:14 67-66-30.50 1
Chloromethane ND ug/L 09/25/15 20:14 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/25/15 20:14 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/25/15 20:14 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/25/15 20:14 96-12-81.0 1
Dibromochloromethane ND ug/L 09/25/15 20:14 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/25/15 20:14 106-93-40.50 1
Dibromomethane ND ug/L 09/25/15 20:14 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/25/15 20:14 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/25/15 20:14 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/25/15 20:14 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/25/15 20:14 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/25/15 20:14 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/25/15 20:14 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/25/15 20:14 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/25/15 20:14 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/25/15 20:14 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/25/15 20:14 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/25/15 20:14 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/25/15 20:14 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/25/15 20:14 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/25/15 20:14 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/25/15 20:14 10061-02-60.50 1
Diisopropyl ether 1.1 ug/L 09/25/15 20:14 108-20-30.50 1
Ethylbenzene ND ug/L 09/25/15 20:14 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/25/15 20:14 87-68-32.0 1
Isopropylbenzene (Cumene)23.1 ug/L 09/25/15 20:14 98-82-80.50 1
Methylene Chloride ND ug/L 09/25/15 20:14 75-09-22.0 1
Methyl-tert-butyl ether 8.9 ug/L 09/25/15 20:14 1634-04-40.50 1
Naphthalene 13.5 ug/L 09/25/15 20:14 91-20-32.0 1
n-Propylbenzene 1.4 ug/L 09/25/15 20:14 103-65-10.50 1
Styrene ND ug/L 09/25/15 20:14 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/25/15 20:14 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/25/15 20:14 79-34-50.50 1
Tetrachloroethene ND ug/L 09/25/15 20:14 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-4 Lab ID:92268940003 Collected:09/22/15 11:01 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 09/25/15 20:14 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/25/15 20:14 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/25/15 20:14 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/25/15 20:14 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/25/15 20:14 79-00-50.50 1
Trichloroethene ND ug/L 09/25/15 20:14 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/25/15 20:14 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/25/15 20:14 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/25/15 20:14 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/25/15 20:14 108-67-80.50 1
Vinyl chloride ND ug/L 09/25/15 20:14 75-01-41.0 1
m&p-Xylene ND ug/L 09/25/15 20:14 179601-23-11.0 1
o-Xylene ND ug/L 09/25/15 20:14 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %09/25/15 20:14 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/25/15 20:14 460-00-470-130 1
Toluene-d8 (S)100 %09/25/15 20:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-5 Lab ID:92268940004 Collected:09/22/15 12:15 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/25/15 20:30 71-43-20.50 1
Bromobenzene ND ug/L 09/25/15 20:30 108-86-10.50 1
Bromochloromethane ND ug/L 09/25/15 20:30 74-97-50.50 1
Bromodichloromethane ND ug/L 09/25/15 20:30 75-27-40.50 1
Bromoform ND ug/L 09/25/15 20:30 75-25-20.50 1
Bromomethane ND ug/L 09/25/15 20:30 74-83-95.0 1
n-Butylbenzene ND ug/L 09/25/15 20:30 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/25/15 20:30 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/25/15 20:30 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/25/15 20:30 56-23-50.50 1
Chlorobenzene ND ug/L 09/25/15 20:30 108-90-70.50 1
Chloroethane ND ug/L 09/25/15 20:30 75-00-31.0 1
Chloroform ND ug/L 09/25/15 20:30 67-66-30.50 1
Chloromethane ND ug/L 09/25/15 20:30 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/25/15 20:30 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/25/15 20:30 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/25/15 20:30 96-12-81.0 1
Dibromochloromethane ND ug/L 09/25/15 20:30 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/25/15 20:30 106-93-40.50 1
Dibromomethane ND ug/L 09/25/15 20:30 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/25/15 20:30 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/25/15 20:30 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/25/15 20:30 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/25/15 20:30 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/25/15 20:30 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/25/15 20:30 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/25/15 20:30 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/25/15 20:30 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/25/15 20:30 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/25/15 20:30 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/25/15 20:30 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/25/15 20:30 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/25/15 20:30 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/25/15 20:30 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/25/15 20:30 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/25/15 20:30 108-20-30.50 1
Ethylbenzene ND ug/L 09/25/15 20:30 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/25/15 20:30 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/25/15 20:30 98-82-80.50 1
Methylene Chloride ND ug/L 09/25/15 20:30 75-09-22.0 1
Methyl-tert-butyl ether 0.75 ug/L 09/25/15 20:30 1634-04-40.50 1
Naphthalene ND ug/L 09/25/15 20:30 91-20-32.0 1
n-Propylbenzene ND ug/L 09/25/15 20:30 103-65-10.50 1
Styrene ND ug/L 09/25/15 20:30 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/25/15 20:30 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/25/15 20:30 79-34-50.50 1
Tetrachloroethene ND ug/L 09/25/15 20:30 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:MW-5 Lab ID:92268940004 Collected:09/22/15 12:15 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 09/25/15 20:30 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/25/15 20:30 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/25/15 20:30 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/25/15 20:30 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/25/15 20:30 79-00-50.50 1
Trichloroethene ND ug/L 09/25/15 20:30 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/25/15 20:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/25/15 20:30 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/25/15 20:30 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/25/15 20:30 108-67-80.50 1
Vinyl chloride ND ug/L 09/25/15 20:30 75-01-41.0 1
m&p-Xylene ND ug/L 09/25/15 20:30 179601-23-11.0 1
o-Xylene ND ug/L 09/25/15 20:30 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %09/25/15 20:30 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/25/15 20:30 460-00-470-130 1
Toluene-d8 (S)101 %09/25/15 20:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:WSW-5 Lab ID:92268940005 Collected:09/22/15 11:47 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/25/15 20:47 71-43-20.50 1
Bromobenzene ND ug/L 09/25/15 20:47 108-86-10.50 1
Bromochloromethane ND ug/L 09/25/15 20:47 74-97-50.50 1
Bromodichloromethane ND ug/L 09/25/15 20:47 75-27-40.50 1
Bromoform ND ug/L 09/25/15 20:47 75-25-20.50 1
Bromomethane ND ug/L 09/25/15 20:47 74-83-95.0 1
n-Butylbenzene ND ug/L 09/25/15 20:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/25/15 20:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/25/15 20:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/25/15 20:47 56-23-50.50 1
Chlorobenzene ND ug/L 09/25/15 20:47 108-90-70.50 1
Chloroethane ND ug/L 09/25/15 20:47 75-00-31.0 1
Chloroform ND ug/L 09/25/15 20:47 67-66-30.50 1
Chloromethane ND ug/L 09/25/15 20:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/25/15 20:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/25/15 20:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/25/15 20:47 96-12-81.0 1
Dibromochloromethane ND ug/L 09/25/15 20:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/25/15 20:47 106-93-40.50 1
Dibromomethane ND ug/L 09/25/15 20:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/25/15 20:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/25/15 20:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/25/15 20:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/25/15 20:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/25/15 20:47 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/25/15 20:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/25/15 20:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/25/15 20:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/25/15 20:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/25/15 20:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/25/15 20:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/25/15 20:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/25/15 20:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/25/15 20:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/25/15 20:47 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/25/15 20:47 108-20-30.50 1
Ethylbenzene ND ug/L 09/25/15 20:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/25/15 20:47 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/25/15 20:47 98-82-80.50 1
Methylene Chloride ND ug/L 09/25/15 20:47 75-09-22.0 1
Methyl-tert-butyl ether 2.6 ug/L 09/25/15 20:47 1634-04-40.50 1
Naphthalene ND ug/L 09/25/15 20:47 91-20-32.0 1
n-Propylbenzene ND ug/L 09/25/15 20:47 103-65-10.50 1
Styrene ND ug/L 09/25/15 20:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/25/15 20:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/25/15 20:47 79-34-50.50 1
Tetrachloroethene ND ug/L 09/25/15 20:47 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Sample:WSW-5 Lab ID:92268940005 Collected:09/22/15 11:47 Received:09/23/15 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 09/25/15 20:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/25/15 20:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/25/15 20:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/25/15 20:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/25/15 20:47 79-00-50.50 1
Trichloroethene ND ug/L 09/25/15 20:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/25/15 20:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/25/15 20:47 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/25/15 20:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/25/15 20:47 108-67-80.50 1
Vinyl chloride ND ug/L 09/25/15 20:47 75-01-41.0 1
m&p-Xylene ND ug/L 09/25/15 20:47 179601-23-11.0 1
o-Xylene ND ug/L 09/25/15 20:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %09/25/15 20:47 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/25/15 20:47 460-00-470-130 1
Toluene-d8 (S)100 %09/25/15 20:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33519
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92268940001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1566349
Associated Lab Samples:92268940001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/25/15 09:10
1,1,1-Trichloroethane ug/L ND 0.50 09/25/15 09:10
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/25/15 09:10
1,1,2-Trichloroethane ug/L ND 0.50 09/25/15 09:10
1,1-Dichloroethane ug/L ND 0.50 09/25/15 09:10
1,1-Dichloroethene ug/L ND 0.50 09/25/15 09:10
1,1-Dichloropropene ug/L ND 0.50 09/25/15 09:10
1,2,3-Trichlorobenzene ug/L ND 2.0 09/25/15 09:10
1,2,3-Trichloropropane ug/L ND 0.50 09/25/15 09:10
1,2,4-Trichlorobenzene ug/L ND 2.0 09/25/15 09:10
1,2,4-Trimethylbenzene ug/L ND 0.50 09/25/15 09:10
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/25/15 09:10
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/25/15 09:10
1,2-Dichlorobenzene ug/L ND 0.50 09/25/15 09:10
1,2-Dichloroethane ug/L ND 0.50 09/25/15 09:10
1,2-Dichloropropane ug/L ND 0.50 09/25/15 09:10
1,3,5-Trimethylbenzene ug/L ND 0.50 09/25/15 09:10
1,3-Dichlorobenzene ug/L ND 0.50 09/25/15 09:10
1,3-Dichloropropane ug/L ND 0.50 09/25/15 09:10
1,4-Dichlorobenzene ug/L ND 0.50 09/25/15 09:10
2,2-Dichloropropane ug/L ND 0.50 09/25/15 09:10
2-Chlorotoluene ug/L ND 0.50 09/25/15 09:10
4-Chlorotoluene ug/L ND 0.50 09/25/15 09:10
Benzene ug/L ND 0.50 09/25/15 09:10
Bromobenzene ug/L ND 0.50 09/25/15 09:10
Bromochloromethane ug/L ND 0.50 09/25/15 09:10
Bromodichloromethane ug/L ND 0.50 09/25/15 09:10
Bromoform ug/L ND 0.50 09/25/15 09:10
Bromomethane ug/L ND 5.0 09/25/15 09:10
Carbon tetrachloride ug/L ND 0.50 09/25/15 09:10
Chlorobenzene ug/L ND 0.50 09/25/15 09:10
Chloroethane ug/L ND 1.0 09/25/15 09:10
Chloroform ug/L ND 0.50 09/25/15 09:10
Chloromethane ug/L ND 1.0 09/25/15 09:10
cis-1,2-Dichloroethene ug/L ND 0.50 09/25/15 09:10
cis-1,3-Dichloropropene ug/L ND 0.50 09/25/15 09:10
Dibromochloromethane ug/L ND 0.50 09/25/15 09:10
Dibromomethane ug/L ND 0.50 09/25/15 09:10
Dichlorodifluoromethane ug/L ND 0.50 09/25/15 09:10
Diisopropyl ether ug/L ND 0.50 09/25/15 09:10
Ethylbenzene ug/L ND 0.50 09/25/15 09:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1566349
Associated Lab Samples:92268940001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 09/25/15 09:10
Isopropylbenzene (Cumene)ug/L ND 0.50 09/25/15 09:10
m&p-Xylene ug/L ND 1.0 09/25/15 09:10
Methyl-tert-butyl ether ug/L ND 0.50 09/25/15 09:10
Methylene Chloride ug/L ND 2.0 09/25/15 09:10
n-Butylbenzene ug/L ND 0.50 09/25/15 09:10
n-Propylbenzene ug/L ND 0.50 09/25/15 09:10
Naphthalene ug/L ND 2.0 09/25/15 09:10
o-Xylene ug/L ND 0.50 09/25/15 09:10
sec-Butylbenzene ug/L ND 0.50 09/25/15 09:10
Styrene ug/L ND 0.50 09/25/15 09:10
tert-Butylbenzene ug/L ND 0.50 09/25/15 09:10
Tetrachloroethene ug/L ND 0.50 09/25/15 09:10
Toluene ug/L ND 0.50 09/25/15 09:10
trans-1,2-Dichloroethene ug/L ND 0.50 09/25/15 09:10
trans-1,3-Dichloropropene ug/L ND 0.50 09/25/15 09:10
Trichloroethene ug/L ND 0.50 09/25/15 09:10
Trichlorofluoromethane ug/L ND 1.0 09/25/15 09:10
Vinyl chloride ug/L ND 1.0 09/25/15 09:10
1,2-Dichloroethane-d4 (S)%96 70-130 09/25/15 09:10
4-Bromofluorobenzene (S)%99 70-130 09/25/15 09:10
Toluene-d8 (S)%101 70-130 09/25/15 09:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1566350LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 60-140
1,1,1-Trichloroethane ug/L 51.650 103 60-140
1,1,2,2-Tetrachloroethane ug/L 48.950 98 60-140
1,1,2-Trichloroethane ug/L 49.750 99 60-140
1,1-Dichloroethane ug/L 49.150 98 60-140
1,1-Dichloroethene ug/L 52.150 104 60-140
1,1-Dichloropropene ug/L 54.650 109 60-140
1,2,3-Trichlorobenzene ug/L 36.650 73 60-140
1,2,3-Trichloropropane ug/L 48.950 98 60-140
1,2,4-Trichlorobenzene ug/L 38.550 77 60-140
1,2,4-Trimethylbenzene ug/L 51.450 103 60-140
1,2-Dibromo-3-chloropropane ug/L 52.850 106 60-140
1,2-Dibromoethane (EDB)ug/L 52.650 105 60-140
1,2-Dichlorobenzene ug/L 49.450 99 60-140
1,2-Dichloroethane ug/L 43.150 86 60-140
1,2-Dichloropropane ug/L 48.650 97 60-140
1,3,5-Trimethylbenzene ug/L 50.850 102 60-140
1,3-Dichlorobenzene ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1566350LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 50.150 100 60-140
1,4-Dichlorobenzene ug/L 48.450 97 60-140
2,2-Dichloropropane ug/L 41.650 83 60-140
2-Chlorotoluene ug/L 50.750 101 60-140
4-Chlorotoluene ug/L 51.750 103 60-140
Benzene ug/L 53.050 106 60-140
Bromobenzene ug/L 51.250 102 60-140
Bromochloromethane ug/L 54.650 109 60-140
Bromodichloromethane ug/L 51.150 102 60-140
Bromoform ug/L 51.850 104 60-140
Bromomethane ug/L 45.850 92 60-140
Carbon tetrachloride ug/L 53.750 107 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 44.850 90 60-140
Chloroform ug/L 50.750 101 60-140
Chloromethane ug/L 36.950 74 60-140
cis-1,2-Dichloroethene ug/L 51.650 103 60-140
cis-1,3-Dichloropropene ug/L 50.150 100 60-140
Dibromochloromethane ug/L 54.150 108 60-140
Dibromomethane ug/L 50.150 100 60-140
Dichlorodifluoromethane ug/L 49.150 98 60-140
Diisopropyl ether ug/L 47.550 95 60-140
Ethylbenzene ug/L 49.250 98 60-140
Hexachloro-1,3-butadiene ug/L 51.450 103 60-140
Isopropylbenzene (Cumene)ug/L 52.450 105 60-140
m&p-Xylene ug/L 97.6100 98 60-140
Methyl-tert-butyl ether ug/L 52.750 105 60-140
Methylene Chloride ug/L 49.050 98 60-140
n-Butylbenzene ug/L 46.450 93 60-140
n-Propylbenzene ug/L 49.450 99 60-140
Naphthalene ug/L 41.350 83 60-140
o-Xylene ug/L 50.850 102 60-140
sec-Butylbenzene ug/L 49.750 99 60-140
Styrene ug/L 53.550 107 60-140
tert-Butylbenzene ug/L 41.550 83 60-140
Tetrachloroethene ug/L 47.250 94 60-140
Toluene ug/L 50.350 101 60-140
trans-1,2-Dichloroethene ug/L 51.250 102 60-140
trans-1,3-Dichloropropene ug/L 51.150 102 60-140
Trichloroethene ug/L 46.350 93 60-140
Trichlorofluoromethane ug/L 47.450 95 60-140
Vinyl chloride ug/L 48.050 96 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1566351MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92268932001
1566352
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 99 60-140102 320<0.50 19.9 20.4
1,1,1-Trichloroethane ug/L 20 107 60-140112 520<0.50 21.4 22.4
1,1,2,2-Tetrachloroethane ug/L 20 97 60-140100 320<0.50 19.4 20.0
1,1,2-Trichloroethane ug/L 20 99 60-140101 120<0.50 19.9 20.2
1,1-Dichloroethane ug/L 20 100 60-140104 420<0.50 20.1 20.8
1,1-Dichloroethene ug/L 20 115 60-140117 220<0.50 23.0 23.5
1,1-Dichloropropene ug/L 20 115 60-140118 320<0.50 23.0 23.6
1,2,3-Trichlorobenzene ug/L 20 73 60-14080 920<2.0 14.6 16.0
1,2,3-Trichloropropane ug/L 20 95 60-14098 320<0.50 18.9 19.6
1,2,4-Trichlorobenzene ug/L 20 75 60-14080 620<2.0 15.0 15.9
1,2,4-Trimethylbenzene ug/L 20 102 60-140103 120<0.50 20.4 20.6
1,2-Dibromo-3-chloropropane ug/L 20 95 60-140100 620<1.0 18.9 20.0
1,2-Dibromoethane (EDB)ug/L 20 101 60-140104 320<0.50 20.3 20.9
1,2-Dichlorobenzene ug/L 20 97 60-140100 320<0.50 19.4 20.1
1,2-Dichloroethane ug/L 20 86 60-14090 520<0.50 17.1 18.0
1,2-Dichloropropane ug/L 20 98 60-140101 320<0.50 19.6 20.3
1,3,5-Trimethylbenzene ug/L 20 101 60-140102 120<0.50 20.2 20.5
1,3-Dichlorobenzene ug/L 20 102 60-140103 020<0.50 20.4 20.5
1,3-Dichloropropane ug/L 20 99 60-140100 120<0.50 19.8 20.0
1,4-Dichlorobenzene ug/L 20 95 60-14099 520<0.50 19.0 19.9
2,2-Dichloropropane ug/L 20 80 60-14083 420<0.50 16.0 16.7
2-Chlorotoluene ug/L 20 105 60-140105 020<0.50 21.0 21.1
4-Chlorotoluene ug/L 20 105 60-140104 020<0.50 20.9 20.8
Benzene ug/L 20 108 60-140111 220<0.50 21.7 22.1
Bromobenzene ug/L 20 102 60-140104 320<0.50 20.3 20.9
Bromochloromethane ug/L 20 111 60-140111 020<0.50 22.2 22.2
Bromodichloromethane ug/L 20 100 60-140103 320<0.50 20.1 20.6
Bromoform ug/L 20 91 60-14093 220<0.50 18.2 18.6
Bromomethane ug/L 20 81 60-14082 120<5.0 16.2 16.4
Carbon tetrachloride ug/L 20 111 60-140115 420<0.50 22.1 22.9
Chlorobenzene ug/L 20 100 60-140102 220<0.50 20.0 20.3
Chloroethane ug/L 20 98 60-14096 220<1.0 19.5 19.2
Chloroform ug/L 20 103 60-140105 220<0.50 20.6 21.1
Chloromethane ug/L 20 81 60-14081 020<1.0 16.1 16.2
cis-1,2-Dichloroethene ug/L 20 104 60-140107 320<0.50 20.9 21.5
cis-1,3-Dichloropropene ug/L 20 96 60-14099 320<0.50 19.1 19.8
Dibromochloromethane ug/L 20 99 60-140102 320<0.50 19.9 20.4
Dibromomethane ug/L 20 97 60-140101 520<0.50 19.3 20.3
Dichlorodifluoromethane ug/L 20 109 60-140114 420<0.50 21.9 22.8
Diisopropyl ether ug/L 20 95 60-14099 420<0.50 18.9 19.8
Ethylbenzene ug/L 20 100 60-140100 020<0.50 20.0 20.0
Hexachloro-1,3-butadiene ug/L 20 104 60-140103 120<2.0 20.8 20.7
Isopropylbenzene (Cumene)ug/L 20 105 60-140105 020<0.50 20.9 20.9
m&p-Xylene ug/L 40 99 60-140100 140<1.0 39.4 40.0
Methyl-tert-butyl ether ug/L 20 103 60-140106 320<0.50 20.5 21.1
Methylene Chloride ug/L 20 99 60-140102 320<2.0 19.8 20.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1566351MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92268932001
1566352
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 89 60-14090 120<0.50 17.8 18.0
n-Propylbenzene ug/L 20 101 60-140101 020<0.50 20.3 20.2
Naphthalene ug/L 20 77 60-14085 1020<2.0 15.4 17.1
o-Xylene ug/L 20 100 60-140100 020<0.50 20.0 20.0
sec-Butylbenzene ug/L 20 100 60-140100 020<0.50 20.0 20.1
Styrene ug/L 20 96 60-14099 320<0.50 19.2 19.7
tert-Butylbenzene ug/L 20 85 60-14084 020<0.50 16.9 16.9
Tetrachloroethene ug/L 20 95 60-14098 220<0.50 19.1 19.5
Toluene ug/L 20 101 60-140104 420<0.50 20.1 20.9
trans-1,2-Dichloroethene ug/L 20 107 60-140111 320<0.50 21.4 22.1
trans-1,3-Dichloropropene ug/L 20 93 60-14096 320<0.50 18.5 19.1
Trichloroethene ug/L 20 97 60-140102 520<0.50 19.4 20.3
Trichlorofluoromethane ug/L 20 104 60-140108 320<1.0 20.8 21.5
Vinyl chloride ug/L 20 104 60-140106 220<1.0 20.8 21.3
1,2-Dichloroethane-d4 (S)%95 70-13096
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33533
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92268940002, 92268940003, 92268940004, 92268940005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1567432
Associated Lab Samples:92268940002, 92268940003, 92268940004, 92268940005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/25/15 19:57
1,1,1-Trichloroethane ug/L ND 0.50 09/25/15 19:57
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/25/15 19:57
1,1,2-Trichloroethane ug/L ND 0.50 09/25/15 19:57
1,1-Dichloroethane ug/L ND 0.50 09/25/15 19:57
1,1-Dichloroethene ug/L ND 0.50 09/25/15 19:57
1,1-Dichloropropene ug/L ND 0.50 09/25/15 19:57
1,2,3-Trichlorobenzene ug/L ND 2.0 09/25/15 19:57
1,2,3-Trichloropropane ug/L ND 0.50 09/25/15 19:57
1,2,4-Trichlorobenzene ug/L ND 2.0 09/25/15 19:57
1,2,4-Trimethylbenzene ug/L ND 0.50 09/25/15 19:57
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/25/15 19:57
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/25/15 19:57
1,2-Dichlorobenzene ug/L ND 0.50 09/25/15 19:57
1,2-Dichloroethane ug/L ND 0.50 09/25/15 19:57
1,2-Dichloropropane ug/L ND 0.50 09/25/15 19:57
1,3,5-Trimethylbenzene ug/L ND 0.50 09/25/15 19:57
1,3-Dichlorobenzene ug/L ND 0.50 09/25/15 19:57
1,3-Dichloropropane ug/L ND 0.50 09/25/15 19:57
1,4-Dichlorobenzene ug/L ND 0.50 09/25/15 19:57
2,2-Dichloropropane ug/L ND 0.50 09/25/15 19:57
2-Chlorotoluene ug/L ND 0.50 09/25/15 19:57
4-Chlorotoluene ug/L ND 0.50 09/25/15 19:57
Benzene ug/L ND 0.50 09/25/15 19:57
Bromobenzene ug/L ND 0.50 09/25/15 19:57
Bromochloromethane ug/L ND 0.50 09/25/15 19:57
Bromodichloromethane ug/L ND 0.50 09/25/15 19:57
Bromoform ug/L ND 0.50 09/25/15 19:57
Bromomethane ug/L ND 5.0 09/25/15 19:57
Carbon tetrachloride ug/L ND 0.50 09/25/15 19:57
Chlorobenzene ug/L ND 0.50 09/25/15 19:57
Chloroethane ug/L ND 1.0 09/25/15 19:57
Chloroform ug/L ND 0.50 09/25/15 19:57
Chloromethane ug/L ND 1.0 09/25/15 19:57
cis-1,2-Dichloroethene ug/L ND 0.50 09/25/15 19:57
cis-1,3-Dichloropropene ug/L ND 0.50 09/25/15 19:57
Dibromochloromethane ug/L ND 0.50 09/25/15 19:57
Dibromomethane ug/L ND 0.50 09/25/15 19:57
Dichlorodifluoromethane ug/L ND 0.50 09/25/15 19:57
Diisopropyl ether ug/L ND 0.50 09/25/15 19:57
Ethylbenzene ug/L ND 0.50 09/25/15 19:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1567432
Associated Lab Samples:92268940002, 92268940003, 92268940004, 92268940005
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 09/25/15 19:57
Isopropylbenzene (Cumene)ug/L ND 0.50 09/25/15 19:57
m&p-Xylene ug/L ND 1.0 09/25/15 19:57
Methyl-tert-butyl ether ug/L ND 0.50 09/25/15 19:57
Methylene Chloride ug/L ND 2.0 09/25/15 19:57
n-Butylbenzene ug/L ND 0.50 09/25/15 19:57
n-Propylbenzene ug/L ND 0.50 09/25/15 19:57
Naphthalene ug/L ND 2.0 09/25/15 19:57
o-Xylene ug/L ND 0.50 09/25/15 19:57
sec-Butylbenzene ug/L ND 0.50 09/25/15 19:57
Styrene ug/L ND 0.50 09/25/15 19:57
tert-Butylbenzene ug/L ND 0.50 09/25/15 19:57
Tetrachloroethene ug/L ND 0.50 09/25/15 19:57
Toluene ug/L ND 0.50 09/25/15 19:57
trans-1,2-Dichloroethene ug/L ND 0.50 09/25/15 19:57
trans-1,3-Dichloropropene ug/L ND 0.50 09/25/15 19:57
Trichloroethene ug/L ND 0.50 09/25/15 19:57
Trichlorofluoromethane ug/L ND 1.0 09/25/15 19:57
Vinyl chloride ug/L ND 1.0 09/25/15 19:57
1,2-Dichloroethane-d4 (S)%95 70-130 09/25/15 19:57
4-Bromofluorobenzene (S)%99 70-130 09/25/15 19:57
Toluene-d8 (S)%101 70-130 09/25/15 19:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1567433LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.650 101 60-140
1,1,1-Trichloroethane ug/L 49.750 99 60-140
1,1,2,2-Tetrachloroethane ug/L 51.350 103 60-140
1,1,2-Trichloroethane ug/L 49.950 100 60-140
1,1-Dichloroethane ug/L 47.450 95 60-140
1,1-Dichloroethene ug/L 50.250 100 60-140
1,1-Dichloropropene ug/L 52.050 104 60-140
1,2,3-Trichlorobenzene ug/L 42.450 85 60-140
1,2,3-Trichloropropane ug/L 51.150 102 60-140
1,2,4-Trichlorobenzene ug/L 41.750 83 60-140
1,2,4-Trimethylbenzene ug/L 49.750 99 60-140
1,2-Dibromo-3-chloropropane ug/L 56.050 112 60-140
1,2-Dibromoethane (EDB)ug/L 53.150 106 60-140
1,2-Dichlorobenzene ug/L 49.050 98 60-140
1,2-Dichloroethane ug/L 43.350 87 60-140
1,2-Dichloropropane ug/L 48.350 97 60-140
1,3,5-Trimethylbenzene ug/L 48.850 98 60-140
1,3-Dichlorobenzene ug/L 49.950 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1567433LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 50.050 100 60-140
1,4-Dichlorobenzene ug/L 47.350 95 60-140
2,2-Dichloropropane ug/L 51.150 102 60-140
2-Chlorotoluene ug/L 49.450 99 60-140
4-Chlorotoluene ug/L 50.150 100 60-140
Benzene ug/L 50.350 101 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 54.750 109 60-140
Bromodichloromethane ug/L 51.050 102 60-140
Bromoform ug/L 52.950 106 60-140
Bromomethane ug/L 39.250 78 60-140
Carbon tetrachloride ug/L 51.250 102 60-140
Chlorobenzene ug/L 48.550 97 60-140
Chloroethane ug/L 43.950 88 60-140
Chloroform ug/L 49.950 100 60-140
Chloromethane ug/L 35.450 71 60-140
cis-1,2-Dichloroethene ug/L 49.950 100 60-140
cis-1,3-Dichloropropene ug/L 52.150 104 60-140
Dibromochloromethane ug/L 53.550 107 60-140
Dibromomethane ug/L 50.150 100 60-140
Dichlorodifluoromethane ug/L 44.450 89 60-140
Diisopropyl ether ug/L 46.850 94 60-140
Ethylbenzene ug/L 47.450 95 60-140
Hexachloro-1,3-butadiene ug/L 56.850 114 60-140
Isopropylbenzene (Cumene)ug/L 51.250 102 60-140
m&p-Xylene ug/L 95.0100 95 60-140
Methyl-tert-butyl ether ug/L 53.250 106 60-140
Methylene Chloride ug/L 48.150 96 60-140
n-Butylbenzene ug/L 45.950 92 60-140
n-Propylbenzene ug/L 47.550 95 60-140
Naphthalene ug/L 46.750 93 60-140
o-Xylene ug/L 48.850 98 60-140
sec-Butylbenzene ug/L 48.150 96 60-140
Styrene ug/L 52.550 105 60-140
tert-Butylbenzene ug/L 39.950 80 60-140
Tetrachloroethene ug/L 46.250 92 60-140
Toluene ug/L 48.450 97 60-140
trans-1,2-Dichloroethene ug/L 49.250 98 60-140
trans-1,3-Dichloropropene ug/L 52.550 105 60-140
Trichloroethene ug/L 45.950 92 60-140
Trichlorofluoromethane ug/L 44.250 88 60-140
Vinyl chloride ug/L 45.250 90 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1567434MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92268985003
1567435
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 60-140109 220ND22.3 21.8
1,1,1-Trichloroethane ug/L 20 121 60-140118 320ND24.1 23.5
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140108 020ND21.6 21.6
1,1,2-Trichloroethane ug/L 20 111 60-140110 120ND22.2 21.9
1,1-Dichloroethane ug/L 20 114 60-140111 320ND22.8 22.2
1,1-Dichloroethene ug/L 20 125 60-140126 120ND24.9 25.2
1,1-Dichloropropene ug/L 20 128 60-140127 120ND25.6 25.4
1,2,3-Trichlorobenzene ug/L 20 85 60-14087 320ND16.9 17.4
1,2,3-Trichloropropane ug/L 20 111 60-140107 320ND22.1 21.4
1,2,4-Trichlorobenzene ug/L 20 85 60-14087 220ND17.1 17.4
1,2,4-Trimethylbenzene ug/L 20 119 60-140116 220ND23.8 23.3
1,2-Dibromo-3-chloropropane ug/L 20 115 60-140118 220ND23.0 23.5
1,2-Dibromoethane (EDB)ug/L 20 115 60-140115 120ND22.9 23.1
1,2-Dichlorobenzene ug/L 20 112 60-140110 320ND22.5 21.9
1,2-Dichloroethane ug/L 20 95 60-14094 120ND18.9 18.8
1,2-Dichloropropane ug/L 20 109 60-140107 320ND21.9 21.3
1,3,5-Trimethylbenzene ug/L 20 115 60-140115 020ND23.1 23.0
1,3-Dichlorobenzene ug/L 20 116 60-140115 120ND23.2 22.9
1,3-Dichloropropane ug/L 20 112 60-140109 220ND22.4 21.8
1,4-Dichlorobenzene ug/L 20 110 60-140107 320ND22.1 21.4
2,2-Dichloropropane ug/L 20 108 60-140107 020ND21.6 21.5
2-Chlorotoluene ug/L 20 117 60-140112 420ND23.4 22.4
4-Chlorotoluene ug/L 20 120 60-140117 220ND23.9 23.3
Benzene ug/L 20 121 60-140117 320ND24.2 23.5
Bromobenzene ug/L 20 117 60-140114 320ND23.5 22.8
Bromochloromethane ug/L 20 121 60-140116 420ND24.2 23.2
Bromodichloromethane ug/L 20 113 60-140110 320ND22.6 22.0
Bromoform ug/L 20 102 60-140103 120ND20.4 20.5
Bromomethane ug/L M1205060-14065 2620ND10.0 13.0
Carbon tetrachloride ug/L 20 126 60-140122 320ND25.2 24.4
Chlorobenzene ug/L 20 112 60-140110 220ND22.5 22.1
Chloroethane ug/L 20 108 60-140101 720ND21.5 20.1
Chloroform ug/L 20 115 60-140113 220ND23.1 22.5
Chloromethane ug/L 20 91 60-14078 1420ND18.1 15.7
cis-1,2-Dichloroethene ug/L 20 116 60-140115 020ND23.1 23.0
cis-1,3-Dichloropropene ug/L 20 111 60-140108 320ND22.3 21.7
Dibromochloromethane ug/L 20 110 60-140111 020ND22.1 22.2
Dibromomethane ug/L 20 110 60-140109 120ND21.9 21.8
Dichlorodifluoromethane ug/L 20 116 60-140111 520ND23.2 22.1
Diisopropyl ether ug/L 20 107 60-140103 320ND21.3 20.7
Ethylbenzene ug/L 20 111 60-140110 120ND22.2 22.0
Hexachloro-1,3-butadiene ug/L M12013760-140143 420ND27.4 28.6
Isopropylbenzene (Cumene)ug/L 20 117 60-140115 220ND23.4 23.0
m&p-Xylene ug/L 40 111 60-140110 140ND44.3 43.9
Methyl-tert-butyl ether ug/L 20 115 60-140113 120ND23.0 22.6
Methylene Chloride ug/L 20 109 60-140106 320ND21.9 21.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1567434MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92268985003
1567435
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 104 60-140104 020ND20.7 20.8
n-Propylbenzene ug/L 20 115 60-140113 220ND23.1 22.6
Naphthalene ug/L 20 96 60-14096 020ND19.2 19.1
o-Xylene ug/L 20 114 60-140110 420ND22.9 21.9
sec-Butylbenzene ug/L 20 115 60-140112 220ND22.9 22.4
Styrene ug/L 20 116 60-140113 220ND23.1 22.7
tert-Butylbenzene ug/L 20 96 60-14093 220ND19.2 18.7
Tetrachloroethene ug/L 20 110 60-140107 320ND22.0 21.3
Toluene ug/L 20 115 60-140112 220ND22.9 22.4
trans-1,2-Dichloroethene ug/L 20 119 60-140116 320ND23.9 23.2
trans-1,3-Dichloropropene ug/L 20 108 60-140109 120ND21.6 21.8
Trichloroethene ug/L 20 111 60-140108 320ND22.2 21.7
Trichlorofluoromethane ug/L 20 114 60-140113 120ND22.8 22.7
Vinyl chloride ug/L 20 113 60-140112 120ND22.7 22.4
1,2-Dichloroethane-d4 (S)%94 70-13095
4-Bromofluorobenzene (S)%97 70-13098
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92268940
Jerry's Place 26074
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92268940
Jerry's Place 26074
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92268940001 MSV/33519MW-2 SM 6200B
92268940002 MSV/33533MW-3 SM 6200B
92268940003 MSV/33533MW-4 SM 6200B
92268940004 MSV/33533MW-5 SM 6200B
92268940005 MSV/33533WSW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/29/2015 03:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 28
Page 27 of 28
Page 28 of 28

APPENDIX B

APPENDIX C