WS-3254_9547_CA_LAB_20191224

#=CL#
December 24, 2019
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92457956
92457956
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1900 Center Park Dr
Charlotte, NC 28217
Jerry's Place
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 25
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CERTIFICATIONS
Pace Project No.:
Project:
92457956
Jerry's Place
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 25
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SAMPLE SUMMARY
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID Matrix Date Collected Date Received
92457956001 MW-2 Water 12/12/19 14:20 12/18/19 08:17
92457956002 MW-3 Water 12/12/19 15:00 12/18/19 08:17
92457956003 MW-4 Water 12/12/19 15:50 12/18/19 08:17
92457956004 MW-5 Water 12/12/19 13:35 12/18/19 08:17
92457956005 WSW-5 Water 12/12/19 13:00 12/18/19 08:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 25
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SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92457956001 MW-2 SM 6200B 63 PASI-CCL
92457956002 MW-3 SM 6200B 63 PASI-CCL
92457956003 MW-4 SM 6200B 63 PASI-CCL
92457956004 MW-5 SM 6200B 63 PASI-CCL
92457956005 WSW-5 SM 6200B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 25
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SUMMARY OF DETECTION
Pace Project No.:
Project:
92457956
Jerry's Place
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92457956001 MW-2
Benzene 583 ug/L 12/22/19 13:516.2SM 6200B
Ethylbenzene 1230 ug/L 12/22/19 13:516.2SM 6200B
Isopropylbenzene (Cumene)75.7 ug/L 12/22/19 13:516.2SM 6200B
Naphthalene 504 ug/L 12/22/19 13:5125.0SM 6200B
n-Propylbenzene 200 ug/L 12/22/19 13:516.2SM 6200B
Toluene 1040 ug/L 12/22/19 13:516.2SM 6200B
1,2,4-Trimethylbenzene 1530 ug/L 12/22/19 13:516.2SM 6200B
1,3,5-Trimethylbenzene 414 ug/L 12/22/19 13:516.2SM 6200B
m&p-Xylene 2940 ug/L 12/22/19 13:5112.5SM 6200B
o-Xylene 1710 ug/L 12/22/19 13:516.2SM 6200B
92457956002 MW-3
Benzene 17.0 ug/L 12/22/19 13:152.5SM 6200B
Ethylbenzene 145 ug/L 12/22/19 13:152.5SM 6200B
Isopropylbenzene (Cumene)64.0 ug/L 12/22/19 13:152.5SM 6200B
Naphthalene 299 ug/L 12/22/19 13:1510.0SM 6200B
n-Propylbenzene 166 ug/L 12/22/19 13:152.5SM 6200B
Toluene 11.4 ug/L 12/22/19 13:152.5SM 6200B
1,2,4-Trimethylbenzene 796 ug/L 12/22/19 13:152.5SM 6200B
1,3,5-Trimethylbenzene 196 ug/L 12/22/19 13:152.5SM 6200B
m&p-Xylene 235 ug/L 12/22/19 13:155.0SM 6200B
o-Xylene 250 ug/L 12/22/19 13:152.5SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 25
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-2 Lab ID:92457956001 Collected:12/12/19 14:20 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 583 ug/L 12/22/19 13:51 71-43-26.2 3.0 12.5
Bromobenzene ND ug/L 12/22/19 13:51 108-86-16.2 2.7 12.5
Bromochloromethane ND ug/L 12/22/19 13:51 74-97-56.2 3.2 12.5
Bromodichloromethane ND ug/L 12/22/19 13:51 75-27-46.2 2.3 12.5
Bromoform ND ug/L 12/22/19 13:51 75-25-26.2 5.1 12.5
Bromomethane ND ug/L 12/22/19 13:51 74-83-962.5 21.5 12.5
n-Butylbenzene ND ug/L 12/22/19 13:51 104-51-86.2 4.4 12.5
sec-Butylbenzene ND ug/L 12/22/19 13:51 135-98-86.2 3.1 12.5
tert-Butylbenzene ND ug/L 12/22/19 13:51 98-06-66.2 3.1 12.5
Carbon tetrachloride ND ug/L 12/22/19 13:51 56-23-56.2 2.9 12.5
Chlorobenzene ND ug/L 12/22/19 13:51 108-90-76.2 2.8 12.5
Chloroethane ND ug/L 12/22/19 13:51 75-00-312.5 7.3 12.5
Chloroform ND ug/L 12/22/19 13:51 67-66-36.2 4.4 12.5
Chloromethane ND ug/L 12/22/19 13:51 74-87-312.5 5.2 12.5
2-Chlorotoluene ND ug/L 12/22/19 13:51 95-49-86.2 2.6 12.5
4-Chlorotoluene ND ug/L 12/22/19 13:51 106-43-46.2 2.6 12.5
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 13:51 96-12-812.5 4.8 12.5
Dibromochloromethane ND ug/L 12/22/19 13:51 124-48-16.2 5.0 12.5
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 13:51 106-93-46.2 2.9 12.5
Dibromomethane ND ug/L 12/22/19 13:51 74-95-36.2 3.9 12.5
1,2-Dichlorobenzene ND ug/L 12/22/19 13:51 95-50-16.2 3.0 12.5
1,3-Dichlorobenzene ND ug/L 12/22/19 13:51 541-73-16.2 3.1 12.5
1,4-Dichlorobenzene ND ug/L 12/22/19 13:51 106-46-76.2 3.1 12.5
Dichlorodifluoromethane ND ug/L 12/22/19 13:51 75-71-86.2 3.6 12.5
1,1-Dichloroethane ND ug/L 12/22/19 13:51 75-34-36.2 3.0 12.5
1,2-Dichloroethane ND ug/L 12/22/19 13:51 107-06-26.2 3.3 12.5
1,1-Dichloroethene ND ug/L 12/22/19 13:51 75-35-46.2 2.7 12.5
cis-1,2-Dichloroethene ND ug/L 12/22/19 13:51 156-59-26.2 2.6 12.5
trans-1,2-Dichloroethene ND ug/L 12/22/19 13:51 156-60-56.2 3.2 12.5
1,2-Dichloropropane ND ug/L 12/22/19 13:51 78-87-56.2 2.3 12.5
1,3-Dichloropropane ND ug/L 12/22/19 13:51 142-28-96.2 4.3 12.5
2,2-Dichloropropane ND ug/L 12/22/19 13:51 594-20-76.2 3.5 12.5
1,1-Dichloropropene ND ug/L 12/22/19 13:51 563-58-66.2 4.4 12.5
cis-1,3-Dichloropropene ND ug/L 12/22/19 13:51 10061-01-56.2 4.5 12.5
trans-1,3-Dichloropropene ND ug/L 12/22/19 13:51 10061-02-66.2 4.9 12.5
Diisopropyl ether ND ug/L 12/22/19 13:51 108-20-36.2 4.2 12.5
Ethylbenzene 1230 ug/L 12/22/19 13:51 100-41-46.2 3.0 12.5
Hexachloro-1,3-butadiene ND ug/L 12/22/19 13:51 87-68-325.0 15.0 12.5
Isopropylbenzene (Cumene)75.7 ug/L 12/22/19 13:51 98-82-86.2 3.0 12.5
Methylene Chloride ND ug/L 12/22/19 13:51 75-09-225.0 18.8 12.5
Methyl-tert-butyl ether ND ug/L 12/22/19 13:51 1634-04-46.2 5.6 12.5
Naphthalene 504 ug/L 12/22/19 13:51 91-20-325.0 8.2 12.5
n-Propylbenzene 200 ug/L 12/22/19 13:51 103-65-16.2 3.0 12.5
Styrene ND ug/L 12/22/19 13:51 100-42-56.2 3.2 12.5
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 13:51 630-20-66.2 5.3 12.5
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 13:51 79-34-56.2 2.4 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 25
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-2 Lab ID:92457956001 Collected:12/12/19 14:20 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 13:51 127-18-46.2 2.9 12.5
Toluene 1040 ug/L 12/22/19 13:51 108-88-36.2 2.8 12.5
1,2,3-Trichlorobenzene ND ug/L 12/22/19 13:51 87-61-625.0 9.8 12.5
1,2,4-Trichlorobenzene ND ug/L 12/22/19 13:51 120-82-125.0 5.4 12.5
1,1,1-Trichloroethane ND ug/L 12/22/19 13:51 71-55-66.2 3.5 12.5
1,1,2-Trichloroethane ND ug/L 12/22/19 13:51 79-00-56.2 2.9 12.5
Trichloroethene ND ug/L 12/22/19 13:51 79-01-66.2 2.9 12.5
Trichlorofluoromethane ND ug/L 12/22/19 13:51 75-69-412.5 4.2 12.5
1,2,3-Trichloropropane ND ug/L 12/22/19 13:51 96-18-46.2 3.4 12.5
1,2,4-Trimethylbenzene 1530 ug/L 12/22/19 13:51 95-63-66.2 2.4 12.5
1,3,5-Trimethylbenzene 414 ug/L 12/22/19 13:51 108-67-86.2 2.8 12.5
Vinyl chloride ND ug/L 12/22/19 13:51 75-01-412.5 5.1 12.5
m&p-Xylene 2940 ug/L 12/22/19 13:51 179601-23-112.5 5.5 12.5
o-Xylene 1710 ug/L 12/22/19 13:51 95-47-66.2 3.0 12.5
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/22/19 13:51 17060-07-070-130 12.5
4-Bromofluorobenzene (S)97 %12/22/19 13:51 460-00-470-130 12.5
Toluene-d8 (S)100 %12/22/19 13:51 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
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Page 7 of 25
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-3 Lab ID:92457956002 Collected:12/12/19 15:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 17.0 ug/L 12/22/19 13:15 71-43-22.5 1.2 5
Bromobenzene ND ug/L 12/22/19 13:15 108-86-12.5 1.1 5
Bromochloromethane ND ug/L 12/22/19 13:15 74-97-52.5 1.3 5
Bromodichloromethane ND ug/L 12/22/19 13:15 75-27-42.5 0.92 5
Bromoform ND ug/L 12/22/19 13:15 75-25-22.5 2.0 5
Bromomethane ND ug/L 12/22/19 13:15 74-83-925.0 8.6 5
n-Butylbenzene ND ug/L 12/22/19 13:15 104-51-82.5 1.8 5
sec-Butylbenzene ND ug/L 12/22/19 13:15 135-98-82.5 1.2 5
tert-Butylbenzene ND ug/L 12/22/19 13:15 98-06-62.5 1.2 5
Carbon tetrachloride ND ug/L 12/22/19 13:15 56-23-52.5 1.2 5
Chlorobenzene ND ug/L 12/22/19 13:15 108-90-72.5 1.1 5
Chloroethane ND ug/L 12/22/19 13:15 75-00-35.0 2.9 5
Chloroform ND ug/L 12/22/19 13:15 67-66-32.5 1.8 5
Chloromethane ND ug/L 12/22/19 13:15 74-87-35.0 2.1 5
2-Chlorotoluene ND ug/L 12/22/19 13:15 95-49-82.5 1.0 5
4-Chlorotoluene ND ug/L 12/22/19 13:15 106-43-42.5 1.0 5
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 13:15 96-12-85.0 1.9 5
Dibromochloromethane ND ug/L 12/22/19 13:15 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 13:15 106-93-42.5 1.2 5
Dibromomethane ND ug/L 12/22/19 13:15 74-95-32.5 1.6 5
1,2-Dichlorobenzene ND ug/L 12/22/19 13:15 95-50-12.5 1.2 5
1,3-Dichlorobenzene ND ug/L 12/22/19 13:15 541-73-12.5 1.2 5
1,4-Dichlorobenzene ND ug/L 12/22/19 13:15 106-46-72.5 1.2 5
Dichlorodifluoromethane ND ug/L 12/22/19 13:15 75-71-82.5 1.4 5
1,1-Dichloroethane ND ug/L 12/22/19 13:15 75-34-32.5 1.2 5
1,2-Dichloroethane ND ug/L 12/22/19 13:15 107-06-22.5 1.3 5
1,1-Dichloroethene ND ug/L 12/22/19 13:15 75-35-42.5 1.1 5
cis-1,2-Dichloroethene ND ug/L 12/22/19 13:15 156-59-22.5 1.0 5
trans-1,2-Dichloroethene ND ug/L 12/22/19 13:15 156-60-52.5 1.3 5
1,2-Dichloropropane ND ug/L 12/22/19 13:15 78-87-52.5 0.92 5
1,3-Dichloropropane ND ug/L 12/22/19 13:15 142-28-92.5 1.7 5
2,2-Dichloropropane ND ug/L 12/22/19 13:15 594-20-72.5 1.4 5
1,1-Dichloropropene ND ug/L 12/22/19 13:15 563-58-62.5 1.7 5
cis-1,3-Dichloropropene ND ug/L 12/22/19 13:15 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 12/22/19 13:15 10061-02-62.5 2.0 5
Diisopropyl ether ND ug/L 12/22/19 13:15 108-20-32.5 1.7 5
Ethylbenzene 145 ug/L 12/22/19 13:15 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene ND ug/L 12/22/19 13:15 87-68-310.0 6.0 5
Isopropylbenzene (Cumene)64.0 ug/L 12/22/19 13:15 98-82-82.5 1.2 5
Methylene Chloride ND ug/L 12/22/19 13:15 75-09-210.0 7.5 5
Methyl-tert-butyl ether ND ug/L 12/22/19 13:15 1634-04-42.5 2.2 5
Naphthalene 299 ug/L 12/22/19 13:15 91-20-310.0 3.3 5
n-Propylbenzene 166 ug/L 12/22/19 13:15 103-65-12.5 1.2 5
Styrene ND ug/L 12/22/19 13:15 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 13:15 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 13:15 79-34-52.5 0.96 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-3 Lab ID:92457956002 Collected:12/12/19 15:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 13:15 127-18-42.5 1.2 5
Toluene 11.4 ug/L 12/22/19 13:15 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene ND ug/L 12/22/19 13:15 87-61-610.0 3.9 5
1,2,4-Trichlorobenzene ND ug/L 12/22/19 13:15 120-82-110.0 2.2 5
1,1,1-Trichloroethane ND ug/L 12/22/19 13:15 71-55-62.5 1.4 5
1,1,2-Trichloroethane ND ug/L 12/22/19 13:15 79-00-52.5 1.2 5
Trichloroethene ND ug/L 12/22/19 13:15 79-01-62.5 1.2 5
Trichlorofluoromethane ND ug/L 12/22/19 13:15 75-69-45.0 1.7 5
1,2,3-Trichloropropane ND ug/L 12/22/19 13:15 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 796 ug/L 12/22/19 13:15 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene 196 ug/L 12/22/19 13:15 108-67-82.5 1.1 5
Vinyl chloride ND ug/L 12/22/19 13:15 75-01-45.0 2.0 5
m&p-Xylene 235 ug/L 12/22/19 13:15 179601-23-15.0 2.2 5
o-Xylene 250 ug/L 12/22/19 13:15 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/22/19 13:15 17060-07-070-130 5
4-Bromofluorobenzene (S)96 %12/22/19 13:15 460-00-470-130 5
Toluene-d8 (S)99 %12/22/19 13:15 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-4 Lab ID:92457956003 Collected:12/12/19 15:50 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 15:21 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 15:21 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 15:21 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 15:21 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 15:21 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 15:21 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 15:21 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 15:21 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 15:21 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 15:21 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 15:21 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 15:21 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 15:21 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 15:21 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 15:21 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 15:21 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 15:21 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 15:21 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 15:21 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 15:21 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 15:21 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 15:21 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 15:21 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 15:21 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 15:21 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 15:21 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 15:21 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 15:21 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 15:21 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 15:21 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 15:21 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 15:21 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 15:21 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 15:21 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 15:21 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 15:21 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 15:21 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 15:21 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 15:21 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 15:21 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 15:21 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 15:21 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 15:21 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 15:21 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 15:21 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 15:21 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 10 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-4 Lab ID:92457956003 Collected:12/12/19 15:50 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 15:21 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 15:21 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 15:21 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 15:21 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 15:21 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 15:21 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 15:21 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 15:21 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 15:21 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 15:21 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 15:21 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 15:21 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 15:21 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 15:21 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/22/19 15:21 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %12/22/19 15:21 460-00-470-130 1
Toluene-d8 (S)100 %12/22/19 15:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
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Page 11 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-5 Lab ID:92457956004 Collected:12/12/19 13:35 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 15:03 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 15:03 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 15:03 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 15:03 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 15:03 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 15:03 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 15:03 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 15:03 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 15:03 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 15:03 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 15:03 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 15:03 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 15:03 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 15:03 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 15:03 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 15:03 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 15:03 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 15:03 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 15:03 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 15:03 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 15:03 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 15:03 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 15:03 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 15:03 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 15:03 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 15:03 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 15:03 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 15:03 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 15:03 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 15:03 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 15:03 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 15:03 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 15:03 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 15:03 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 15:03 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 15:03 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 15:03 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 15:03 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 15:03 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 15:03 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 15:03 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 15:03 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 15:03 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 15:03 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 15:03 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 15:03 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:MW-5 Lab ID:92457956004 Collected:12/12/19 13:35 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 15:03 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 15:03 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 15:03 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 15:03 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 15:03 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 15:03 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 15:03 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 15:03 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 15:03 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 15:03 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 15:03 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 15:03 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 15:03 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 15:03 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %12/22/19 15:03 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %12/22/19 15:03 460-00-470-130 1
Toluene-d8 (S)102 %12/22/19 15:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:WSW-5 Lab ID:92457956005 Collected:12/12/19 13:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/22/19 14:45 71-43-20.50 0.24 1
Bromobenzene ND ug/L 12/22/19 14:45 108-86-10.50 0.22 1
Bromochloromethane ND ug/L 12/22/19 14:45 74-97-50.50 0.26 1
Bromodichloromethane ND ug/L 12/22/19 14:45 75-27-40.50 0.18 1
Bromoform ND ug/L 12/22/19 14:45 75-25-20.50 0.40 1
Bromomethane ND ug/L 12/22/19 14:45 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/22/19 14:45 104-51-80.50 0.35 1
sec-Butylbenzene ND ug/L 12/22/19 14:45 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 12/22/19 14:45 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 12/22/19 14:45 56-23-50.50 0.23 1
Chlorobenzene ND ug/L 12/22/19 14:45 108-90-70.50 0.22 1
Chloroethane ND ug/L 12/22/19 14:45 75-00-31.0 0.58 1
Chloroform ND ug/L 12/22/19 14:45 67-66-30.50 0.35 1
Chloromethane ND ug/L 12/22/19 14:45 74-87-31.0 0.42 1
2-Chlorotoluene ND ug/L 12/22/19 14:45 95-49-80.50 0.21 1
4-Chlorotoluene ND ug/L 12/22/19 14:45 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane ND ug/L 12/22/19 14:45 96-12-81.0 0.38 1
Dibromochloromethane ND ug/L 12/22/19 14:45 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)ND ug/L 12/22/19 14:45 106-93-40.50 0.23 1
Dibromomethane ND ug/L 12/22/19 14:45 74-95-30.50 0.31 1
1,2-Dichlorobenzene ND ug/L 12/22/19 14:45 95-50-10.50 0.24 1
1,3-Dichlorobenzene ND ug/L 12/22/19 14:45 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 12/22/19 14:45 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 12/22/19 14:45 75-71-80.50 0.28 1
1,1-Dichloroethane ND ug/L 12/22/19 14:45 75-34-30.50 0.24 1
1,2-Dichloroethane ND ug/L 12/22/19 14:45 107-06-20.50 0.26 1
1,1-Dichloroethene ND ug/L 12/22/19 14:45 75-35-40.50 0.22 1
cis-1,2-Dichloroethene ND ug/L 12/22/19 14:45 156-59-20.50 0.21 1
trans-1,2-Dichloroethene ND ug/L 12/22/19 14:45 156-60-50.50 0.26 1
1,2-Dichloropropane ND ug/L 12/22/19 14:45 78-87-50.50 0.18 1
1,3-Dichloropropane ND ug/L 12/22/19 14:45 142-28-90.50 0.34 1
2,2-Dichloropropane ND ug/L 12/22/19 14:45 594-20-70.50 0.28 1
1,1-Dichloropropene ND ug/L 12/22/19 14:45 563-58-60.50 0.35 1
cis-1,3-Dichloropropene ND ug/L 12/22/19 14:45 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/22/19 14:45 10061-02-60.50 0.39 1
Diisopropyl ether ND ug/L 12/22/19 14:45 108-20-30.50 0.33 1
Ethylbenzene ND ug/L 12/22/19 14:45 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene ND ug/L 12/22/19 14:45 87-68-32.0 1.2 1
Isopropylbenzene (Cumene)ND ug/L 12/22/19 14:45 98-82-80.50 0.24 1
Methylene Chloride ND ug/L 12/22/19 14:45 75-09-22.0 1.5 1
Methyl-tert-butyl ether ND ug/L 12/22/19 14:45 1634-04-40.50 0.44 1
Naphthalene ND ug/L 12/22/19 14:45 91-20-32.0 0.66 1
n-Propylbenzene ND ug/L 12/22/19 14:45 103-65-10.50 0.24 1
Styrene ND ug/L 12/22/19 14:45 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/22/19 14:45 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane ND ug/L 12/22/19 14:45 79-34-50.50 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92457956
Jerry's Place
Sample:WSW-5 Lab ID:92457956005 Collected:12/12/19 13:00 Received:12/18/19 08:17 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 12/22/19 14:45 127-18-40.50 0.23 1
Toluene ND ug/L 12/22/19 14:45 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene ND ug/L 12/22/19 14:45 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene ND ug/L 12/22/19 14:45 120-82-12.0 0.44 1
1,1,1-Trichloroethane ND ug/L 12/22/19 14:45 71-55-60.50 0.28 1
1,1,2-Trichloroethane ND ug/L 12/22/19 14:45 79-00-50.50 0.23 1
Trichloroethene ND ug/L 12/22/19 14:45 79-01-60.50 0.23 1
Trichlorofluoromethane ND ug/L 12/22/19 14:45 75-69-41.0 0.34 1
1,2,3-Trichloropropane ND ug/L 12/22/19 14:45 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene ND ug/L 12/22/19 14:45 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene ND ug/L 12/22/19 14:45 108-67-80.50 0.23 1
Vinyl chloride ND ug/L 12/22/19 14:45 75-01-41.0 0.41 1
m&p-Xylene ND ug/L 12/22/19 14:45 179601-23-11.0 0.44 1
o-Xylene ND ug/L 12/22/19 14:45 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %12/22/19 14:45 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %12/22/19 14:45 460-00-470-130 1
Toluene-d8 (S)101 %12/22/19 14:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
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[phone]
Page 15 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
516241
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2766036
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/22/19 11:460.42
1,1,1-Trichloroethane ug/L ND 0.50 12/22/19 11:460.28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/22/19 11:460.19
1,1,2-Trichloroethane ug/L ND 0.50 12/22/19 11:460.23
1,1-Dichloroethane ug/L ND 0.50 12/22/19 11:460.24
1,1-Dichloroethene ug/L ND 0.50 12/22/19 11:460.22
1,1-Dichloropropene ug/L ND 0.50 12/22/19 11:460.35
1,2,3-Trichlorobenzene ug/L ND 2.0 12/22/19 11:460.78
1,2,3-Trichloropropane ug/L ND 0.50 12/22/19 11:460.27
1,2,4-Trichlorobenzene ug/L ND 2.0 12/22/19 11:460.44
1,2,4-Trimethylbenzene ug/L ND 0.50 12/22/19 11:460.19
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/22/19 11:460.38
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/22/19 11:460.23
1,2-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.24
1,2-Dichloroethane ug/L ND 0.50 12/22/19 11:460.26
1,2-Dichloropropane ug/L ND 0.50 12/22/19 11:460.18
1,3,5-Trimethylbenzene ug/L ND 0.50 12/22/19 11:460.23
1,3-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.25
1,3-Dichloropropane ug/L ND 0.50 12/22/19 11:460.34
1,4-Dichlorobenzene ug/L ND 0.50 12/22/19 11:460.25
2,2-Dichloropropane ug/L ND 0.50 12/22/19 11:460.28
2-Chlorotoluene ug/L ND 0.50 12/22/19 11:460.21
4-Chlorotoluene ug/L ND 0.50 12/22/19 11:460.21
Benzene ug/L ND 0.50 12/22/19 11:460.24
Bromobenzene ug/L ND 0.50 12/22/19 11:460.22
Bromochloromethane ug/L ND 0.50 12/22/19 11:460.26
Bromodichloromethane ug/L ND 0.50 12/22/19 11:460.18
Bromoform ug/L ND 0.50 12/22/19 11:460.40
Bromomethane ug/L ND 5.0 12/22/19 11:461.7
Carbon tetrachloride ug/L ND 0.50 12/22/19 11:460.23
Chlorobenzene ug/L ND 0.50 12/22/19 11:460.22
Chloroethane ug/L ND 1.0 12/22/19 11:460.58
Chloroform ug/L ND 0.50 12/22/19 11:460.35
Chloromethane ug/L ND 1.0 12/22/19 11:460.42
cis-1,2-Dichloroethene ug/L ND 0.50 12/22/19 11:460.21
cis-1,3-Dichloropropene ug/L ND 0.50 12/22/19 11:460.36
Dibromochloromethane ug/L ND 0.50 12/22/19 11:460.40
Dibromomethane ug/L ND 0.50 12/22/19 11:460.31
Dichlorodifluoromethane ug/L ND 0.50 12/22/19 11:460.28
Diisopropyl ether ug/L ND 0.50 12/22/19 11:460.33
Ethylbenzene ug/L ND 0.50 12/22/19 11:460.24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2766036
Associated Lab Samples:92457956001, 92457956002, 92457956003, 92457956004, 92457956005
Matrix:Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 12/22/19 11:461.2
Isopropylbenzene (Cumene)ug/L ND 0.50 12/22/19 11:460.24
m&p-Xylene ug/L ND 1.0 12/22/19 11:460.44
Methyl-tert-butyl ether ug/L ND 0.50 12/22/19 11:460.44
Methylene Chloride ug/L ND 2.0 12/22/19 11:461.5
n-Butylbenzene ug/L ND 0.50 12/22/19 11:460.35
n-Propylbenzene ug/L ND 0.50 12/22/19 11:460.24
Naphthalene ug/L ND 2.0 12/22/19 11:460.66
o-Xylene ug/L ND 0.50 12/22/19 11:460.24
sec-Butylbenzene ug/L ND 0.50 12/22/19 11:460.25
Styrene ug/L ND 0.50 12/22/19 11:460.26
tert-Butylbenzene ug/L ND 0.50 12/22/19 11:460.25
Tetrachloroethene ug/L ND 0.50 12/22/19 11:460.23
Toluene ug/L ND 0.50 12/22/19 11:460.23
trans-1,2-Dichloroethene ug/L ND 0.50 12/22/19 11:460.26
trans-1,3-Dichloropropene ug/L ND 0.50 12/22/19 11:460.39
Trichloroethene ug/L ND 0.50 12/22/19 11:460.23
Trichlorofluoromethane ug/L ND 1.0 12/22/19 11:460.34
Vinyl chloride ug/L ND 1.0 12/22/19 11:460.41
1,2-Dichloroethane-d4 (S)%90 70-130 12/22/19 11:46
4-Bromofluorobenzene (S)%96 70-130 12/22/19 11:46
Toluene-d8 (S)%102 70-130 12/22/19 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2766037LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.450 111 60-140
1,1,1-Trichloroethane ug/L 54.050 108 60-140
1,1,2,2-Tetrachloroethane ug/L 52.050 104 60-140
1,1,2-Trichloroethane ug/L 51.550 103 60-140
1,1-Dichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethene ug/L 50.450 101 60-140
1,1-Dichloropropene ug/L 56.650 113 60-140
1,2,3-Trichlorobenzene ug/L 62.550 125 60-140
1,2,3-Trichloropropane ug/L 52.250 104 60-140
1,2,4-Trichlorobenzene ug/L 61.050 122 60-140
1,2,4-Trimethylbenzene ug/L 57.250 114 60-140
1,2-Dibromo-3-chloropropane ug/L 57.250 114 60-140
1,2-Dibromoethane (EDB)ug/L 55.750 111 60-140
1,2-Dichlorobenzene ug/L 57.750 115 60-140
1,2-Dichloroethane ug/L 47.950 96 60-140
1,2-Dichloropropane ug/L 52.650 105 60-140
1,3,5-Trimethylbenzene ug/L 56.350 113 60-140
1,3-Dichlorobenzene ug/L 56.750 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2766037LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 55.850 112 60-140
1,4-Dichlorobenzene ug/L 57.850 116 60-140
2,2-Dichloropropane ug/L 62.850 126 60-140
2-Chlorotoluene ug/L 55.050 110 60-140
4-Chlorotoluene ug/L 56.450 113 60-140
Benzene ug/L 52.750 105 60-140
Bromobenzene ug/L 57.550 115 60-140
Bromochloromethane ug/L 52.350 105 60-140
Bromodichloromethane ug/L 53.650 107 60-140
Bromoform ug/L 57.150 114 60-140
Bromomethane ug/L 53.250 106 60-140
Carbon tetrachloride ug/L 56.150 112 60-140
Chlorobenzene ug/L 54.550 109 60-140
Chloroethane ug/L 58.650 117 60-140
Chloroform ug/L 50.650 101 60-140
Chloromethane ug/L 41.250 82 60-140
cis-1,2-Dichloroethene ug/L 50.150 100 60-140
cis-1,3-Dichloropropene ug/L 55.750 111 60-140
Dibromochloromethane ug/L 58.250 116 60-140
Dibromomethane ug/L 55.650 111 60-140
Dichlorodifluoromethane ug/L 48.150 96 60-140
Diisopropyl ether ug/L 51.250 102 60-140
Ethylbenzene ug/L 53.850 108 60-140
Hexachloro-1,3-butadiene ug/L 57.550 115 60-140
Isopropylbenzene (Cumene)ug/L 56.150 112 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 54.850 110 60-140
Methylene Chloride ug/L 46.850 94 60-140
n-Butylbenzene ug/L 58.450 117 60-140
n-Propylbenzene ug/L 54.950 110 60-140
Naphthalene ug/L 62.050 124 60-140
o-Xylene ug/L 55.050 110 60-140
sec-Butylbenzene ug/L 56.350 113 60-140
Styrene ug/L 58.050 116 60-140
tert-Butylbenzene ug/L 47.650 95 60-140
Tetrachloroethene ug/L 55.350 111 60-140
Toluene ug/L 51.550 103 60-140
trans-1,2-Dichloroethene ug/L 51.050 102 60-140
trans-1,3-Dichloropropene ug/L 55.050 110 60-140
Trichloroethene ug/L 53.550 107 60-140
Trichlorofluoromethane ug/L 49.950 100 60-140
Vinyl chloride ug/L 51.850 104 60-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2766038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457416003
2766039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 110 60-140105 4 30200ND220211
1,1,1-Trichloroethane ug/L 200 109 60-140107 2 30200ND219214
1,1,2,2-Tetrachloroethane ug/L 200 105 60-140100 5 30200ND210201
1,1,2-Trichloroethane ug/L 200 107 60-140105 2 30200ND214210
1,1-Dichloroethane ug/L 200 108 60-140104 3 30200ND216209
1,1-Dichloroethene ug/L 200 108 60-140103 4 30200ND216207
1,1-Dichloropropene ug/L 200 119 60-140114 4 30200ND238228
1,2,3-Trichlorobenzene ug/L 200 101 60-140109 7 30200ND207222
1,2,3-Trichloropropane ug/L 200 109 60-14099 10 30200ND219198
1,2,4-Trichlorobenzene ug/L 200 104 60-140109 4 30200ND208217
1,2,4-Trimethylbenzene ug/L 200 109 60-140107 1 30200222439437
1,2-Dibromo-3-
chloropropane ug/L 200 108 60-140108 0 30200ND216216
1,2-Dibromoethane (EDB)ug/L 200 109 60-140104 4 30200ND218208
1,2-Dichlorobenzene ug/L 200 111 60-140108 3 30200ND221215
1,2-Dichloroethane ug/L 200 100 60-14093 8 30200ND201186
1,2-Dichloropropane ug/L 200 111 60-140109 2 30200ND222219
1,3,5-Trimethylbenzene ug/L 200 112 60-140108 3 3020055.8 280 272
1,3-Dichlorobenzene ug/L 200 109 60-140107 2 30200ND218214
1,3-Dichloropropane ug/L 200 111 60-140106 5 30200ND222211
1,4-Dichlorobenzene ug/L 200 109 60-140109 1 30200ND219217
2,2-Dichloropropane ug/L 200 111 60-140106 4 30200ND221213
2-Chlorotoluene ug/L 200 114 60-140109 5 30200ND229218
4-Chlorotoluene ug/L 200 111 60-140109 2 30200ND223218
Benzene ug/L 200 95 60-140113 2 30200163018201860
Bromobenzene ug/L 200 114 60-140109 5 30200ND228218
Bromochloromethane ug/L 200 106 60-140103 3 30200ND213206
Bromodichloromethane ug/L 200 109 60-140108 1 30200ND218216
Bromoform ug/L 200 111 60-140104 6 30200ND221208
Bromomethane ug/L 200 75 60-14096 24 30200ND150192
Carbon tetrachloride ug/L 200 117 60-140112 4 30200ND234225
Chlorobenzene ug/L 200 111 60-140106 5 30200ND223213
Chloroethane ug/L 200 139 60-140140 1 30200ND277280
Chloroform ug/L 200 112 60-140105 6 30200ND223211
Chloromethane ug/L 200 73 60-14073 1 30200ND146145
cis-1,2-Dichloroethene ug/L 200 104 60-140100 4 30200ND209201
cis-1,3-Dichloropropene ug/L 200 111 60-140108 2 30200ND221216
Dibromochloromethane ug/L 200 112 60-140107 5 30200ND224214
Dibromomethane ug/L 200 113 60-140109 4 30200ND227218
Dichlorodifluoromethane ug/L 200 91 60-14085 7 30200ND182169
Diisopropyl ether ug/L 200 99 60-14096 2 3020037.7 235 230
Ethylbenzene ug/L 200 108 60-140106 1 30200240457452
Hexachloro-1,3-butadiene ug/L 200 103 60-140105 2 30200ND206211
Isopropylbenzene(Cumene)ug/L 200 113 60-140109 3 3020036.3 263 255
m&p-Xylene ug/L 400 111 60-140107 3 30400128572556
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92457956
Jerry's Place
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2766038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457416003
2766039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 108 60-140100 5 30200130346331
Methylene Chloride ug/L 200 101 60-14098 2 30200ND202197
n-Butylbenzene ug/L 200 105 60-140106 1 3020022.4 233 235
n-Propylbenzene ug/L 200 107 60-140105 1 3020075.0 289 286
Naphthalene ug/L 200 111 60-140130 8 30200276497536
o-Xylene ug/L 200 111 60-140106 4 3020010.6 233 223
sec-Butylbenzene ug/L 200 115 60-140112 2 30200ND229224
Styrene ug/L 200 114 60-140111 3 30200ND229223
tert-Butylbenzene ug/L 200 97 60-14094 3 30200ND193188
Tetrachloroethene ug/L 200 112 60-140108 4 30200ND225216
Toluene ug/L 200 108 60-140106 1 3020020.3 236 232
trans-1,2-Dichloroethene ug/L 200 109 60-140104 4 30200ND217208
trans-1,3-Dichloropropene ug/L 200 102 60-140101 1 30200ND204203
Trichloroethene ug/L 200 115 60-140110 4 30200ND230221
Trichlorofluoromethane ug/L 200 108 60-140103 5 30200ND217206
Vinyl chloride ug/L 200 107 60-140104 3 30200ND214208
1,2-Dichloroethane-d4 (S)%96 70-13098
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%97 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 25
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92457956
Jerry's Place
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 25
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92457956
Jerry's Place
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92457956001 516241MW-2 SM 6200B
92457956002 516241MW-3 SM 6200B
92457956003 516241MW-4 SM 6200B
92457956004 516241MW-5 SM 6200B
92457956005 516241WSW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/24/2019 10:13 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 25
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Page 25 of 25